WQ0012980_Residual Annual Report Form 2021_20220117

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
En.anmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ012980
Applicant/Permittee Milwaukee Metropolitan Sewerage District
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Tom Nowicki
Email Address*
[e-mail]
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
14142252243
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Applicant/Permittee Address*
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
W00012980
Has Current Existing permit number
260 W Seeboth Street Milwaukee WI 53204
Milwaukee MSD Class A Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Milorganite_NC_2021.pdf 2.15MB
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than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
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Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 1/17/2022

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MILORGANITE
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MILORGANITE
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MILORGANITE
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MILORGANITE
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MILORGANITE
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SLOW RELEASE
Milorganite
NITROGEN FERTILIZER
Summary of Sample Results
2021
Parameter
Units
Highest
Day
Annual
Average
Federal
Limit'
Arsenic
mg/kg
9.5
4.1
41
Cadmium
mg/kg
2.7
0.48
39
Copper
mg/kg
290
240
1,500
Lead
mg/kg
40
22
300
Mercury
mg/kg
0.52
0.24
17
Molybdenum
mg/kg
15
10
75
Nickel
mg/kg
42
24
420
Selenium
mg/kg
11
4.2
100
Zinc
mg/kg
880
420
2,800
PCB Aroclors (total)
mg/kg
0.30
0.054
Dioxin Toxic Equivalent2
pg/g
13
5.1
1. Monthly average
3. Dioxin Toxic Equivalent is the sum of the concentrations of various
dioxins, furans, and polychlorinated biphenyls multiplied by individual
toxic equivalency factors, as established by the U.S. Environmental
Protection Agency

P?MMSD
PARTNERS FOR A CLEANER ENVIRONMENT
January 14, 2022
TO:
FROM: Zach Vogel
Laboratory Project Manager
Memorandum
Brett Kelly, Ilir Aliji, Dion Doege, and Sam Lieven
COPY: Pamela Bechler, Alfredo Sotomayor, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom
Nowicki, Beth Stroik, Kim Walden, Kori Kenney, Ethan Guyant, Lab File
SUBJECT: Annual Milorganite Report — 2021
Attached is the Annual Milorganite report for the year 2021. The boron and mercury analyses were performed
by Pace Analytical Services, Inc. in Green Bay, Wisconsin (Wisconsin Certification #: 405132750). The nitrogen
profile analyses were performed by Midwest Laboratories in Omaha, Nebraska when listed. All other analyses
were performed by Milwaukee Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #:
241325920, Florida NELAP Certification #: E571010).
There was no Milorganite production on the following dates:
• May 24, 2021
• May 31, 2021
• June 15 through June 17, 2021
• August 29, 2021
• October 5, 2021
• October 9 through October 18, 2021
Please contact the Central Laboratory if there are any questions or comments regarding these data. Thank you.
Data Review By:
F2axe `-(2voit&I). }-14-2c22__
Pamela Bechler Date
Laboratory Supervisor
Data/Report Review By:
` f' I- PI-ZoZz
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

MMSD Central Laboratory Certification Outline
Test
Method
Wisconsin DNR
DATCP
Florida (TNI)
Aqueousa
Solidb
Aqueousa
Aqueousa
Solidb
Alkalinity by Colorimetry
EPA 310.2
X
Aluminum by ICP
SW846 6010 C
X
X
Ammonia as N by Colorimetry
SM 4500 NH3 G
X
Ammonia as N by ISE
SM 4500 NH3 D
X
X
Ammonia as N by Titration
SM 4500 NH3 C
X
X
Antimony by ICP
EPA 200.7
X
X
Arsenic by ICP
SW846 6010 C
X
X
Arsenic by ICP
EPA 200.7
X
X
Beryllium by ICP
EPA 200.7
X
Biochemical Oxygen Demand (BOD) by 5-day Assay
SM 5210 B
X
X
Cadmium by ICP
SW846 6010 C
X
X
Cadmium by ICP
EPA 200.7
X
X
Calcium by ICP
EPA 200.7
X
Carbonaceous BOD (cBOD) by 5-day Assay
SM 5210 B
X
Chemical Oxygen Demand (COD) by Colorimetry
SM 5220 D
X
Chloride by Colorimetry
SM 4500 Cl- E
X
X
Chlorophyll -a by Colorimetry
SM 10200 H
X
Chromium, Total, by ICP
SW846 6010 C
X
X
Chromium, Total, by ICP
EPA 200.7
X
X
Cobalt by ICP
SW846 6010 C
X
X
Cobalt by ICP
EPA 200.7
X
X
Copper by ICP
SW846 6010 C
X
X
Copper by ICP
EPA 200.7
X
X
E. coil
SM 9223 B
X
Fecal Coliform in Biosolids
EPA 1680
X
Fecal Coliform
SM 9221 E
X
Fecal Coliform
SM 9222 D
X
X
Hardness, Total as CaCO3, by Calculation
SM 2340 B
X
Hexane Extractable Material (HEM, Oil & Grease)
EPA 1664 B
X
X
Iron by ICP
SW846 6010 C
X
X
Iron by ICP
EPA 200.7
X
Kjeldahl Nitrogen, Total, by Colorimetry
EPA 351.2
X
Lead by ICP
SW846 6010 C
X
X
Lead by ICP
EPA 200.7
X
X
Magnesium by ICP
EPA 200.7
X
Manganese by ICP
EPA 200.7
X
X
Molybdenum by ICP
SW846 6010 C
X
X
Molybdenum by ICP
EPA 200.7
X
X
Nickel by ICP _
SW846 6010 C
X
X
Nickel by ICP
EPA 200.7
X
X
Nitrate + Nitrite by Colorimetry
EPA 353.2
X
X
Nitrate by Colorimetry
EPA 353.2
X
X
Nitrite by Colorimetry
EPA 353.2
X
X
Organic Carbon, Total (TOC)
EPA 5310 C
X
pH
EPA 9045
X
Phosphorus, Total, by Colorimetry
EPA 365.1
X
X
Phosphorus, Total, by ICP
SW846 6010 C
X
X
Potassium by ICP
SW846 6010 C
X
X
Residue, Fixed (% Ash)
SM 2540 G
X
Residue, Nonfilterable (TSS)
SM 2540 D
X
Residue, Total (% TS)
SM 2540 G
X
X
Residue, Total (TS)
SM 2540 B
X
Residue, Volatile (% VS)
SM 2540 G
X
Residue, Volatile (VS)
SM 2540 E
X
Residue, Volatile, Nonfilterable (VSS)
SM 2540 B
X
Selenium by ICP
SW846 6010 C
X
X
Selenium by ICP
EPA 200.7
X
X
Silica Gel Treated HEM (SGT-HEM)
EPA 1664 B
X
X
Silver by ICP
EPA 200.7
X
X
Sulfide, by Titration
40 CFR Part 425
X
Thallium by ICP
EPA 200.7
X
Tin by ICP
EPA 200.7
X
X
Titanium by ICP
EPA 200.7
X
X
Total Coliform
SM 9221 B
X
Vanadium by ICP
EPA 200.7
X
X
Zinc by ICP
SW846 6010 C
X
X
Zinc by ICP
EPA 200.7
X
X
I
a Non -potable water. b Biosolids, Leachates, Soils, Tissues, and Wastes
Wisconsin Department of Natural Resources (DNR) Laboratory ID: 241325920
Wisconsin Department of Agriculture, Trade and Consumer Protection (DATCP) License Number: 115088
Florida Department of Health, Bureau of Public Health Laboratories (TNI) Laboratory ID: E571010
Revised: 08/11/2021 Page 1 of 1

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
4.9 mg/kg D.W.
2.8
11
J.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
5 mg/kg D.W. 2.8 11
J.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
5.4 mg/kg D.W. 2.8 10 J.
SW846: 6010C MMSD
01/04/21 DM0104/21000488
4 mg/kg D.W. 2.8 11 J.
SW846: 6010C MMSD
01/05/21 DM0105/21000504
5.2 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/06/21 DM0106/21000535
4.4 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
01/07/21 DM0107/21000551
4.6 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/08/21 DM0108/21000562
4.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/09/21 DM0109/21000581
4.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/10/21 DM0110/21000594
3.6 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/11/21 DM0111/21000632
4.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/12/21 DM0112/21000648
4.8 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/13/21 DM0113/21000679
3.3 mg/kg D.W.
2.8 10 J, Q3.
SW846: 6010C MMSD
01/14/21 DM0114/21000754 4.3 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
01/15/21 DM0115/21000765 3.6 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/16/21 DM0116/21000784 3.7 mg/kg D.W. 2.8 10 J.
SW846: 6010C MMSD
01/17/21 DM0117/21000797
4.6 mg/kg D.W. 2.8 11 J, Q3.
SW846: 6010C MMSD
01/18/21 DM0118/21000824
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
01/19/21 DM0119/21000842
2.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/20/21 DM0120/21000926
4.1 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
01/21/21 DM0121/21000942
6.2 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/22/21 DM0122/21000953
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
01/23/21 DM0123/21000972
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
01/24/21 DM0124/21001059
5.4 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/25/21 DM0125/21001088
4.1 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/26/21 DM0126/21001106
4.6 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
01/27/21 DM0127/21001137
4.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
01/28/21 DM0128/21001153
5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
01/29/21 DM0129/21001164
4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
01/30/21 DM0130/21001304
3.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
01/31/21 DM0131/21001317
3.1 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/01/21 DM0201/21001344
4.6 mg/kg D.W. 2.7 10 D2, J, Q3.
SW846: 6010C MMSD
02/02/21 DM0202/21001397
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
02/03/21 DM0203/21001428
3.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/04/21 DM0204/21001444
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
02/05/21 DM0205/21001455
4.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/06/21 DM0206/21001476
3.8 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/07/21 DM0207/21001489
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/08/21 DM0208/21001609
4.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/09/21 DM0209/21001625
3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/10/21 DM0210/21001656
4.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/11/21 DM0211/21001672
3.8 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
02/12/21 DM0212/21001706
4.6 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/13/21 DM0213/21001725
4.5 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
02/14/21 DM0214/21001738
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/15/21 DM0215/21001793
4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
Page 1 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
3.5 mg/kg D.W.
2.7
10
J.
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
3.1 mg/kg D.W. 2.8 11
J.
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
3.5 mg/kg D.W. 2.8 11 J.
SW846: 6010C MMSD
02/19/21 DM0219/21001986
3.2 mg/kg D.W. 2.8 10 J.
SW846: 6010C MMSD
02/20/21 DM0220/21002005
3.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/21/21 DM0221/21002072
3.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/22/21 DM0222/21002230
3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/23/21 DM0223/21002246
6.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/24/21 DM0224/21002281
3.5 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/25/21 DM0225/21002320
3.1 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
02/26/21 DM0226/21002386
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/27/21 DM0227/21002405
3.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
02/28/21 DM0228/21002478
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/01/21 DM0301/21002611 4.4 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
03/02/21 DM0302/21002629 4.2 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
03/03/21 DM0303/21002660 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/04/21 DM0304/21002717
6.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/05/21 DM0305/21002728
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/06/21 DM0306/21002747
4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/07/21 DM0307/21002858
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/08/21 DM0308/21003336
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/09/21 DM0309/21003371
5.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/10/21 DM0310/21003402
3.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/11/21 DM0311/21003456
4.1 mg/kg D.W. 2.7 10 J, Q3.
SW846: 6010C MMSD
03/12/21 DM0312/21003522
4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/13/21 DM0313/21003541
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/14/21 DM0314/21003554
4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/15/21 DM0315/21003747
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/16/21 DM0316/21003801
4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/17/21 DM0317/21003878
4.4 mg/kg D.W. 2.7 10 J, Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894
4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/19/21 DM0319/21003905
3.7 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
03/20/21 DM0320/21004076
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/21/21 DM0321/21004093
3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/22/21 DM0322/21004120
4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/23/21 DM0323/21004136
4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/24/21 DM0324/21004167
4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/25/21 DM0325/21004242
3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
03/26/21 DM0326/21004253
3.3 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
03/27/21 DM0327/21004272
3.4 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
03/28/21 DM0328/21004285
3.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
03/29/21 DM0329/21 004312
3.7 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
03/30/21 DM0330/21 004388
3.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
03/31/21 DM0331/21004600
3.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/01/21 DM0401/21004616
2.8 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/02/21 DM0402/21004627
3.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
Page 2 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
4.5 mg/kg D.W.
2.7
10
J.
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
4.4 mg/kg D.W. 2.7 10
J.
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
< 2.8 mg/kg D.W. 2.8 10
SW846: 6010C MMSD
04/06/21 DM0406/21004758 < 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
04/07/21 DM0407/21004843 3.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/08/21 DM0408/21004861 3.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/09/21 DM0409/21004912 < 2.8 mg/kg D.W. 2.8 11 SW846: 6010C MMSD
04/10/21 DM0410/21004931 2.8 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/11/21 DM0411/21005023 < 2.7 mg/kg D.W. 2.7 10 SW846: 6010C MMSD
04/12/21 DM0412/21005052 3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/13/21 DM0413/21005199 6.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/14/21 DM0414/21005230 4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/15/21 DM0415/21005248 4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/16/21 DM0416/21005259 4.8 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/17/21 DM0417/21005468 4.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/18/21 DM0418/21005481 4.4 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/19/21 DM0419/21005508 4.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
04/20/21 DM0420/21005839 < 2.8 mg/kg D.W. 2.8 11 SW846: 6010C MMSD
04/21/21 DM0421/21005870 4.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/22/21 DM0422/21005981 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/23/21 DM0423/21005992 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/24/21 DM0424/21006057 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/25/21 DM0425/21006272 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/26/21 DM0426/21006299 4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/27/21 DM0427/21006315 5.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/28/21 DM0428/21006346 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/29/21 DM0429/21006362 4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
04/30/21 DM0430/21006373 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/01/21 DM0501/21006429 4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/02/21 DM0502/21006442 3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/03/21 DM0503/21006676 4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/04/21 DM0504/21006691 5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/05/21 DM0505/21006722 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/06/21 DM0506/21006781 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/07/21 DM0507/21006834 4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/08/21 DM0508/21006981 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/09/21 DM0509/21006994 4.5 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
05/10/21 DM0510/21007021 4.4 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
05/11/21 DM0511/21007171 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/12/21 DM0512/21007202 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/13/21 DM0513/21007217 3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/14/21 DM0514/21007309 3.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/15/21 DM0515/21007328 < 2.7 mg/kg D.W. 2.7 10 SW846: 6010C MMSD
05/16/21 DM0516/21007341 3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/17/21 DM0517/21007382 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/18/21 DM0518/21007440 3.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
Page 3 of 121
SYS/rpt1MiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PaRNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
4.5 mg/kg D.W.
2.7
10
J.
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
4.3 mg/kg D.W. 2.8 11
J.
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
4.2 mg/kg D.W. 2.8 11 J.
SW846: 6010C MMSD
05/22/21 DM0522/21008072
4.4 mg/kg D.W. 2.8 11 J.
SW846: 6010C MMSD
05/23/21 DM0523/21008085
4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/25/21 DM0525/21008288
5.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/26/21 DM0526/21008319
5.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/27/21 DM0527/21008484
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/28/21 DM0528/21008495
5.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/29/21 DM0529/21008515
5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
05/30/21 DM0530/21008530
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/01/21 DM0601 /21 008902
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
06/02/21 DM0602/21008935
5.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/03/21 DM0603/21008950
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/04/21 DM0604/21009184
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/05/21 DM0605/21009203
5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/06/21 DM0606/21009287
4.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/07/21 DM0607/21009314
5.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/08/21 DM0608/21009334
4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/09/21 DM0609/21009365
3.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/10/21 DM0610/21009538
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/11/21 DM0611/21009549
5.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/12/21 DM0612/21009568
6.2 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
06/13/21 DM0613/21009602
6.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
06/14/21 DM0614/21009629
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
06/18/21 DM0618/21009979
3.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
06/19/21 DM0619/21010314
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/20/21 DM0620/21010332
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/21/21 DM0621/21010359
2.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/22/21 DM0622/21010375
3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/23/21 DM0623/21010408
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/24/21 DM0624/21010670
3.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/25/21 DM0625/21010681
4.4 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
06/26/21 DM0626/21010702
4.3 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
06/27/21 DM0627/21010807
4.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD
06/28/21 DM0628/21010860
5.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/29/21 DM0629/21010875
4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
06/30/21 DM0630/21011438
5 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
07/01/21 DM0701/21011453
4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/02/21 DM0702/21011465
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/03/21 DM0703/21011485
4 mg/kg D.W. 2.7 10 J, T9.
SW846: 6010C MMSD
07/04/21 DM0704/21011516
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/05/21 DM0705/21011572
4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/06/21 DM0706/21011693
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/07/21 DM0707/21011727
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/08/21 DM0708/21011742
5.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
Page 4 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FP CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
5.1 mg/kg D.W.
2.7
10
J.
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
4.7 mg/kg D.W. 2.7 10
J.
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
5.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
07/12/21 DM0712/21012283
4.9 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
07/13/21 DM0713/21012298
2.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/14/21 DM0714/21012332
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/15/21 DM0715/21012390
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/16/21 DM0716/21012563
5.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/17/21 DM0717/21012583
5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/18/21 DM0718/21012596
4.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/19/21 DM0719/21012624
4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/20/21 DM0720/21012639
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
07/21/21 DM0721/21012760
4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/22/21 DM0722/21012775
4.3 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
07/23/21 DM0723/21013074
4.4 mg/kg D.W. 2.8 10 J. SW846: 6010C MMSD
07/24/21 DM0724/21013378
4.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/25/21 DM0725/21013391
4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/26/21 DM0726/21013419
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/27/21 DM0727/21013434
5.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/28/21 DM0728/21013470
3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/29/21 DM0729/21013614
3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/30/21 DM0730/21013629
4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
07/31/21 DM0731/21013739
3.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/01/21 DM0801/21013752
3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/02/21 DM0802/21013891
3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/03/21 DM0803/21013906
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
08/04/21 DM0804/21013940
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
08/05/21 DM0805/21014673
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/06/21 DM0806/21014685
3.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/07/21 DM0807/21014705
4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/08/21 DM0809/21014718
3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/09/21 DM0809/21014746
4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/10/21 DM0810/21014847
9.5 mg/kg D.W. 2.7 10 D2, J, Q2.
SW846: 6010C MMSD
08/11/21 DM0811/21014867
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/12/21 DM0812/21015285
4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/13/21 DM0813/21015297
5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/14/21 DM0814/21015317
5.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/15/21 DM0815/21015330
4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/16/21 DM0816/21015410
4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/17/21 DM0817/21015425
5.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/18/21 DM0818/21016031
4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/19/21 DM0819/21016046
3.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/20/21 DM0820/21016068
4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/21/21 DM0821/21016088
4.9 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/22/21 DM0822/21016196
4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/23/21 DM0823/21016224
4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
Page 5 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
4 mg/kg D.W.
2.7
10
J.
SW846: 6010C
MMSD
08/25/21
DM0825/21 01 6327
4.1 mg/kg D.W. 2.7 10
J.
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
5.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
08/27/21 DM0827/21016407 4.3 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD
08/28/21 DM0828/21016427 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/30/21 DM0830/21016468 5.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
08/31/21 DM0831/21016483 3.2 mg/kg D.W. 2.7 10 D2, J. SW846: 6010C MMSD
09/01/21 DM0901/21016598 5.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/02/21 DM0902/21016659 5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/03/21 DM0903/21016671 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/04/21 DM0904/21017055 5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/05/21 DM0905/21017068 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/06/21 DM0906/21017096 4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/07/21 DM0907/21017306 4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/08/21 DM0908/21017338 5.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/09/21 DM0909/21017408 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/10/21 DM0910/21017420 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/11/21 DM0911/21017699 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/12/21 DM0912/21017712 3.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/13/21 DM0913/21017740 3.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/14/21 DM0914/21017755 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 4.4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 5.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 5.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 5 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 4.8 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/23/21 DM0923/21018564 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD
09/24/21 DM0924/21018818 5.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 5.3 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 5.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 4.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 4.7 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 3.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 3.4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150655-1
10/20/21 DM1 020/21 020674 4.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150655-1
Page 6 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
ARSENIC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
3.6 mg/kg D.W.
2.7
10
J.
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
7.3 mg/kg D.W. 2.7 10
J.
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
5 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 5.8 mg/kg D.W. 2.7 10 J.
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 3.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 4.5 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 5.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 3.8 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 4.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 4.8 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 4.7 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 4.1 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 5.1 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 5.1 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 3.8 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 4.2 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 4.4 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 4.6 mg/kg D.W. 2.7 10 J. SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 3.8 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 3.9 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 3.7 mg/kg D.W. 2.8 11 J. SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 4.5 mg/kg D.W. 2.8 10 J.
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 4.6 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 4.9 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 4.7 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 4.4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 5 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 3.6 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 3.6 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 4.4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 4.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 4.2 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 4.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 4.9 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 4.2 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 4.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 3.9 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 4.4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 4.9 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 3.6 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 4.5 mg/kg D.W. 2.8 11 D2, J, Q3.
SW846: 6010C
MMSD 151371-1
Page 7 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEE FL CLEktER ix�lE HERE
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
4.4 mg/kg D.W.
2.8
11
J.
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
3.8 mg/kg D.W. 2.8 11
J.
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
3.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 3.2 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 4.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 4.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 3.5 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 3.5 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 3.9 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 4 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 3.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 3.5 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 3.5 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 4.3 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 4.2 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 4.2 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 3.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 3.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 4.1 mg/kg D.W. 2.7 10 J.
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 4.4 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 4.7 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 4.8 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 4.5 mg/kg D.W. 2.8 11 J.
SW846: 6010C
MMSD 151827-1
Avg Result: 4.1 mg/kg D.W. Min LOD: 2.7 mg/kg D.W.
Max Result: 9.5 mg/kg D.W. Max LOD: 2.8 mg/kg D.W.
Page 8 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
0.38 mg/kg D.W.
0.12
0.48
J.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
0.38 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
0.36 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 0.26 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
01/05/21 DM0105/21000504 0.48 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/06/21 DM0106/21000535 0.48 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
01/07/21 DM0107/21000551 0.48 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
01/08/21 DM0108/21000562 0.4 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/09/21 DM0109/21000581 0.41 mg/kg D.W. 0.12 0.49 J. SW846: 6010C MMSD
01/10/21 DM0110/21000594 0.41 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/11/21 DM0111/21000632 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/12/21 DM0112/21000648 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/13/21 DM0113/21000679 0.4 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/14/21 DM0114/21000754 0.36 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
01/15/21 DM0115/21000765 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/16/21 DM0116/21000784 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/17/21 DM0117/21000797 0.36 mg/kg D.W. 0.12 0.48 J, Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 0.62 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
01/19/21 DM0119/21000842 0.47 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/20/21 DM0120/21000926 0.45 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/21/21 DM0121/21000942 0.45 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/22/21 DM0122/21000953 0.54 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
01/23/21 DM0123/21000972 0.49 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
01/24/21 DM0124/21001059 0.41 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/25/21 DM0125/21001088 0.32 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/26/21 DM0126/21001106 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
01/27/21 DM0127/21001137 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
01/28/21 DM0128/21001153 0.33 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
01/29/21 DM0129/21001164 0.24 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
01/30/21 DM0130/21001304 0.25 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
01/31/21 DM0131/21001317 0.26 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/01/21 DM0201/21001344 0.4 mg/kg D.W. 0.12 0.48 D2, J, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 0.62 mg/kg D.W. 0.12 0.48 D2. SW846: 6010C MMSD
02/03/21 DM0203/21001428 0.3 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/04/21 DM0204/21001444 0.61 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
02/05/21 DM0205/21001455 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/06/21 DM0206/21001476 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/07/21 DM0207/21001489 0.38 mg/kg D.W. 0.11 0.46 J. SW846: 6010C MMSD
02/08/21 DM0208/21001609 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
02/09/21 DM0209/21001625 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
02/10/21 DM0210/21001656 0.61 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
02/11/21 DM0211/21001672 0.44 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/12/21 DM0212/21001706 0.46 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/13/21 DM0213/21001725 0.48 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/14/21 DM0214/21001738 0.67 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
02/15/21 DM0215/21001793 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
Page 9 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
0.28 mg/kg D.W.
0.12
0.48
J.
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
0.24 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
0.23 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
02/19/21 DM0219/21001986 0.28 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
02/20/21 DM0220/21002005 0.29 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
02/21/21 DM0221/21002072 0.27 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
02/22/21 DM0222/21002230 0.36 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
02/23/21 DM0223/21002246 0.47 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
02/24/21 DM0224/21002281 0.3 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/25/21 DM0225/21002320 0.3 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
02/26/21 DM0226/21002386 0.59 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
02/27/21 DM0227/21002405 0.62 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
02/28/21 DM0228/21002478 0.65 mg/kg D.W. 0.12 0.47 D2. SW846: 6010C MMSD
03/01/21 DM0301/21002611 0.31 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
03/02/21 DM0302/21002629 0.69 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
03/03/21 DM0303/21002660 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/04/21 DM0304/21002717 0.59 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
03/05/21 DM0305/21002728 0.42 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/06/21 DM0306/21002747 0.42 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
03/07/21 DM0307/21002858 0.46 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/08/21 DM0308/21003336 0.46 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/09/21 DM0309/21003371 0.61 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
03/10/21 DM0310/21003402 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/11/21 DM0311/21003456 0.8 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
03/12/21 DM0312/21003522 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/13/21 DM0313/21003541 0.5 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
03/14/21 DM0314/21003554 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/15/21 DM0315/21003747 0.4 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
03/16/21 DM0316/21003801 0.71 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
03/17/21 DM0317/21003878 0.44 mg/kg D.W. 0.12 0.47 J, Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 < 0.12 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
03/19/21 DM0319/21003905 0.41 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/20/21 DM0320/21004076 0.42 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
03/21/21 DM0321/21004093 0.42 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
03/22/21 DM0322/21004120 0.39 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
03/23/21 DM0323/21004136 0.36 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/24/21 DM0324/21004167 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/25/21 DM0325/21004242 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
03/26/21 DM0326/21004253 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/27/21 DM0327/21004272 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/28/21 DM0328/21004285 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/29/21 DM0329/21004312 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/30/21 DM0330/21004388 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
03/31/21 DM0331/21004600 0.42 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/01/21 DM0401/21004616 0.43 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/02/21 DM0402/21004627 0.4 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
Page 10 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
0.42 mg/kg D.W.
0.12
0.48
J.
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
0.34 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
0.44 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
04/06/21 DM0406/21004758 0.63 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
04/07/21 DM0407/21004843 0.38 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/08/21 DM0408/21004861 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/09/21 DM0409/21004912 0.4 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/10/21 DM0410/21004931 0.4 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/11/21 DM0411/21005023 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/12/21 DM0412/21005052 0.48 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
04/13/21 DM0413/21005199 0.61 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
04/14/21 DM0414/21005230 0.38 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/15/21 DM0415/21005248 0.35 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/16/21 DM0416/21005259 0.3 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/17/21 DM0417/21005468 0.3 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/18/21 DM0418/21005481 0.32 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/19/21 DM0419/21005508 0.39 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
04/20/21 DM0420/21005839 0.72 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
04/21/21 DM0421/21005870 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/22/21 DM0422/21005981 0.35 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/23/21 DM0423/21005992 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/24/21 DM0424/21006057 0.36 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/25/21 DM0425/21006272 0.34 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/26/21 DM0426/21006299 0.62 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
04/27/21 DM0427/21006315 0.65 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
04/28/21 DM0428/21006346 0.27 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/29/21 DM0429/21006362 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
04/30/21 DM0430/21006373 0.31 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
05/01/21 DM0501/21006429 0.29 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/02/21 DM0502/21006442 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/03/21 DM0503/21006676 0.27 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
05/04/21 DM0504/21006691 0.65 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
05/05/21 DM0505/21006722 0.52 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
05/06/21 DM0506/21006781 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
05/07/21 DM0507/21006834 0.47 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
05/08/21 DM0508/21006981 0.42 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/09/21 DM0509/21006994 0.42 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
05/10/21 DM0510/21007021 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
05/11/21 DM0511/21007171 0.42 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/12/21 DM0512/21007202 0.42 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/13/21 DM0513/21007217 0.64 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
05/14/21 DM0514/21007309 0.31 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/15/21 DM0515/21007328 0.35 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/16/21 DM0516/21007341 0.34 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
05/17/21 DM0517/21007382 0.32 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
05/18/21 DM0518/21007440 0.74 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
Page 11 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
0.32 mg/kg D.W.
0.12
0.47
J.
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
0.49 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
0.47 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
05/22/21 DM0522/21008072 0.39 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C MMSD
05/23/21 DM0523/21008085 0.34 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
05/25/21 DM0525/21008288 0.4 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
05/26/21 DM0526/21008319 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/27/21 DM0527/21008484 0.64 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
05/28/21 DM0528/21008495 0.31 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/29/21 DM0529/21008515 0.34 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
05/30/21 DM0530/21008530 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/01/21 DM0601/21008902 0.76 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
06/02/21 DM0602/21008935 0.29 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/03/21 DM0603/21008950 0.33 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/04/21 DM0604/21009184 0.32 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
06/05/21 DM0605/21009203 0.28 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/06/21 DM0606/21009287 0.28 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/07/21 DM0607/21009314 0.36 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
06/08/21 DM0608/21009334 0.31 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/09/21 DM0609/21009365 0.29 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/10/21 DM0610/21009538 0.38 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/11/21 DM0611/21009549 0.66 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
06/12/21 DM0612/21009568 0.75 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
06/13/21 DM0613/21009602 0.66 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
06/14/21 DM0614/21009629 0.71 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
06/18/21 DM0618/21009979 0.44 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
06/19/21 DM0619/21010314 0.37 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/20/21 DM0620/21010332 0.39 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/21/21 DM0621/21010359 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/22/21 DM0622/21010375 0.42 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
06/23/21 DM0623/21010408 0.38 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/24/21 DM0624/21010670 0.29 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/25/21 DM0625/21010681 0.44 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
06/26/21 DM0626/21010702 0.43 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
06/27/21 DM0627/21010807 0.47 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
06/28/21 DM0628/21010860 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
06/29/21 DM0629/21010875 0.8 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
06/30/21 DM0630/21011438 0.59 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
07/01/21 DM0701/21011453 0.42 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/02/21 DM0702/21011465 0.42 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/03/21 DM0703/21011485 0.44 mg/kg D.W. 0.12 0.47 J, T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 0.38 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/05/21 DM0705/21011572 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/06/21 DM0706/21011693 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/07/21 DM0707/21011727 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/08/21 DM0708/21011742 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
Page 12 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
0.46 mg/kg D.W.
0.11
0.47
J.
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
0.44 mg/kg D.W. 0.11 0.47 J.
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
0.46 mg/kg D.W. 0.11 0.47 J.
SW846: 6010C MMSD
07/12/21 DM0712/21012283 0.46 mg/kg D.W. 0.11 0.47 J.
SW846: 6010C MMSD
07/13/21 DM0713/21012298 0.71 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
07/14/21 DM0714/21012332 0.37 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
07/15/21 DM0715/21012390 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/16/21 DM0716/21012563 0.52 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
07/17/21 DM0717/21012583 0.52 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
07/18/21 DM0718/21012596 0.46 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
07/19/21 DM0719/21012624 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/20/21 DM0720/21012639 2.5 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
07/21/21 DM0721/21012760 0.57 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
07/22/21 DM0722/21012775 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
07/23/21 DM0723/21013074 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
07/24/21 DM0724/21013378 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD
07/25/21 DM0725/21013391 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/26/21 DM0726/21013419 0.32 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/27/21 DM0727/21013434 0.61 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
07/28/21 DM0728/21013470 0.32 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
07/29/21 DM0729/21013614 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
07/30/21 DM0730/21013629 0.48 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
07/31/21 DM0731/21013739 0.5 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
08/01/21 DM0801/21013752 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
08/02/21 DM0802/21013891 0.4 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
08/03/21 DM0803/21013906 2.7 mg/kg D.W. 0.11 0.47 D2. SW846: 6010C MMSD
08/04/21 DM0804/21013940 2.7 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
08/05/21 DM0805/21014673 2.7 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
08/06/21 DM0806/21014685 0.44 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
08/07/21 DM0807/21014705 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
08/08/21 DM0809/21014718 0.44 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
08/09/21 DM0809/21014746 0.44 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
08/10/21 DM0810/21014847 0.56 mg/kg D.W. 0.12 0.47 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 0.62 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
08/12/21 DM0812/21015285 0.59 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
08/13/21 DM0813/21015297 0.62 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
08/14/21 DM0814/21015317 0.66 mg/kg D.W. 0.11 0.46 SW846: 6010C MMSD
08/15/21 DM0815/21015330 0.78 mg/kg D.W. 0.11 0.46 SW846: 6010C MMSD
08/16/21 DM0816/21015410 0.55 mg/kg D.W. 0.11 0.46 SW846: 6010C MMSD
08/17/21 DM0817/21015425 0.91 mg/kg D.W. 0.11 0.46 SW846: 6010C MMSD
08/18/21 DM0818/21016031 0.67 mg/kg D.W. 0.11 0.46 SW846: 6010C MMSD
08/19/21 DM0819/21016046 0.64 mg/kg D.W. 0.11 0.46 SW846: 6010C MMSD
08/20/21 DM0820/21016068 0.7 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
08/21/21 DM0821/21016088 0.6 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
08/22/21 DM0822/21016196 0.6 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
08/23/21 DM0823/21016224 0.54 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
Page 13 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
0.67 mg/kg D.W.
0.12
0.47
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
0.55 mg/kg D.W. 0.12 0.47
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
0.44 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C MMSD
08/27/21 DM0827/21016407 0.4 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C MMSD
08/28/21 DM0828/21016427 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
08/30/21 DM0830/21016468 0.42 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD
08/31/21 DM0831/21016483 2.4 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/01/21 DM0901/21016598 0.58 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
09/02/21 DM0902/21016659 0.69 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
09/03/21 DM0903/21016671 0.5 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD
09/04/21 DM0904/21017055 0.54 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
09/05/21 DM0905/21017068 0.48 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/06/21 DM0906/21017096 0.52 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
09/07/21 DM0907/21017306 0.52 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/08/21 DM0908/21017338 0.48 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/09/21 DM0909/21017408 0.44 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
09/10/21 DM0910/21017420 0.69 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/11/21 DM0911/21017699 0.58 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
09/12/21 DM0912/21017712 0.48 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/13/21 DM0913/21017740 0.38 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD
09/14/21 DM0914/21017755 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 0.49 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 0.64 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 0.57 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 0.55 mg/kg D.W. 0.12 0.48 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 0.45 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 0.55 mg/kg D.W. 0.12 0.47
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 0.5 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/23/21 DM0923/21018564 0.52 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD
09/24/21 DM0924/21018818 0.44 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 0.43 mg/kg D.W. 0.11 0.46 J. SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 0.44 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 0.41 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 0.46 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 0.48 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 0.47 mg/kg D.W. 0.11 0.47 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 0.44 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 0.43 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 0.48 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 0.46 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 0.46 mg/kg D.W. 0.11 0.47 J.
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 0.43 mg/kg D.W. 0.11 0.46 J. SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 0.43 mg/kg D.W. 0.11 0.46 J. SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 0.54 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD 150655-1
Page 14 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
CADMIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
0.42 mg/kg D.W.
0.11
0.47
J.
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
0.9 mg/kg D.W. 0.11 0.47
SW846: 6010C
MMSD 150703-1
10/23/21 D M 1023/21020883
0.87 mg/kg D.W. 0.11 0.46
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 0.88 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 0.85 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 0.75 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 0.82 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 0.42 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 0.42 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 0.46 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 0.45 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 0.42 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 0.48 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 0.46 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 0.46 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 0.36 mg/kg D.W. 0.11 0.47 J. SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 0.33 mg/kg D.W. 0.12 0.47 J. SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 0.32 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 0.33 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 0.33 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 0.36 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 0.35 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 0.36 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 0.4 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 0.38 mg/kg D.W. 0.12 0.48 J. SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 0.34 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 0.36 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 0.35 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 0.36 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 0.32 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 0.34 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 0.28 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 0.28 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 0.27 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 0.37 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 0.37 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 0.33 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 0.37 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 0.36 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 0.41 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 0.41 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 0.39 mg/kg D.W. 0.11 0.47 J.
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 0.46 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 0.36 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 0.37 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 0.38 mg/kg D.W. 0.12 0.48 D2, J, Q3. SW846: 6010C
MMSD 151371-1
Page 15 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FL CLER+fR ix�lE HERE
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
0.5 mg/kg D.W.
0.12
0.48
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
0.35 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
0.44 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 0.37 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 0.47 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 0.45 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 0.48 mg/kg D.W. 0.11 0.47
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 0.36 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 0.58 mg/kg D.W. 0.12 0.47
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 0.51 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 0.45 mg/kg D.W. 0.12 0.47 J.
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 0.43 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 0.41 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 0.39 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 0.39 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 0.46 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 0.45 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 0.44 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 0.43 mg/kg D.W. 0.12 0.49 J.
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 0.55 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 0.42 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 0.44 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 0.48 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 0.51 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 0.48 mg/kg D.W. 0.12 0.48 J.
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 0.5 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD 151827-1
Avg Result: 0.48 mg/kg D.W. Min LOD: 0.11 mg/kg D.W.
Max Result: 2.7 mg/kg D.W. Max LOD: 0.12 mg/kg D.W.
Page 16 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
230 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
01/04/21 DM0104/21000488 240 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
01/05/21 DM0105/21000504 240 mg/kg D.W. 6.8 26
SW846: 6010C MMSD
01/06/21 DM0106/21000535 240 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
01/07/21 DM0107/21000551 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/08/21 DM0108/21000562 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/09/21 DM0109/21000581 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/10/21 DM0110/21000594 230 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/11/21 DM0111/21000632 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/12/21 DM0112/21000648 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/13/21 DM0113/21000679 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/14/21 DM0114/21000754 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/15/21 DM0115/21000765 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/16/21 DM0116/21000784 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/17/21 DM0117/21000797 250 mg/kg D.W. 6.7 26 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/19/21 DM0119/21000842 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/20/21 DM0120/21000926 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/21/21 DM0121/21000942 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/22/21 DM0122/21000953 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/23/21 DM0123/21000972 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/24/21 DM0124/21001059 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/25/21 DM0125/21001088 220 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/26/21 DM0126/21001106 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/27/21 DM0127/21001137 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/28/21 DM0128/21001153 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/29/21 DM0129/21001164 240 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
01/30/21 DM0130/21001304 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/31/21 DM0131/21001317 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/01/21 DM0201/21001344 230 mg/kg D.W. 6.7 25 Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/03/21 DM0203/21001428 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/04/21 DM0204/21001444 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/05/21 DM0205/21001455 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/06/21 DM0206/21001476 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/07/21 DM0207/21001489 250 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
02/08/21 DM0208/21001609 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/09/21 DM0209/21001625 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/10/21 DM0210/21001656 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/11/21 DM0211/21001672 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/12/21 DM0212/21001706 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/13/21 DM0213/21001725 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/14/21 DM0214/21001738 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/15/21 DM0215/21001793 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
Page 17 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
220 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
210 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
02/19/21 DM0219/21001986 210 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
02/20/21 DM0220/21002005 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
02/21/21 DM0221/21002072 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
02/22/21 DM0222/21002230 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/23/21 DM0223/21002246 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/24/21 DM0224/21002281 210 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/25/21 DM0225/21002320 210 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
02/26/21 DM0226/21002386 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/27/21 DM0227/21002405 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/28/21 DM0228/21002478 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/01/21 DM0301/21002611 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/02/21 DM0302/21002629 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/03/21 DM0303/21002660 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/04/21 DM0304/21002717 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/05/21 DM0305/21002728 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/06/21 DM0306/21002747 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/07/21 DM0307/21002858 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/08/21 DM0308/21003336 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/09/21 DM0309/21003371 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/10/21 DM0310/21003402 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/11/21 DM0311/21003456 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/12/21 DM0312/21003522 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/13/21 DM0313/21003541 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/14/21 DM0314/21003554 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/15/21 DM0315/21003747 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/16/21 DM0316/21003801 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/17/21 DM0317/21003878 240 mg/kg D.W. 6.6 25 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/19/21 DM0319/21003905 230 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
03/20/21 DM0320/21004076 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/21/21 DM0321/21004093 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/22/21 DM0322/21004120 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/23/21 DM0323/21004136 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/24/21 DM0324/21004167 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/25/21 DM0325/21004242 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/26/21 DM0326/21004253 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/27/21 DM0327/21004272 200 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/28/21 DM0328/21004285 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
03/29/21 DM0329/21004312 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/30/21 DM0330/21004388 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
03/31/21 DM0331/21004600 200 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/01/21 DM0401/21004616 220 mg/kg D.W. 6.7 25 Q3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
Page 18 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
220 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
230 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
04/06/21 DM0406/21004758 240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
04/07/21 DM0407/21004843 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
04/08/21 DM0408/21004861 220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
04/09/21 DM0409/21004912 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/10/21 DM0410/21004931 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
04/11/21 DM0411/21005023 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/12/21 DM0412/21005052 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/13/21 DM0413/21005199 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/14/21 DM0414/21005230 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/15/21 DM0415/21005248 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/16/21 DM0416/21005259 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/17/21 DM0417/21005468 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/18/21 DM0418/21005481 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/19/21 DM0419/21005508 230 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
04/20/21 DM0420/21005839 220 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
04/21/21 DM0421/21005870 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/22/21 DM0422/21005981 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/23/21 DM0423/21005992 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/24/21 DM0424/21006057 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/25/21 DM0425/21006272 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/26/21 DM0426/21006299 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/27/21 DM0427/21006315 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/28/21 DM0428/21006346 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/29/21 DM0429/21006362 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/30/21 DM0430/21006373 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/01/21 DM0501/21006429 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/02/21 DM0502/21006442 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/03/21 DM0503/21006676 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/04/21 DM0504/21006691 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/05/21 DM0505/21006722 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/06/21 DM0506/21006781 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/07/21 DM0507/21006834 220 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
05/08/21 DM0508/21006981 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/09/21 DM0509/21006994 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
05/10/21 DM0510/21007021 210 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
05/11/21 DM0511/21007171 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/12/21 DM0512/21007202 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/13/21 DM0513/21007217 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
05/14/21 DM0514/21007309 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/15/21 DM0515/21007328 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/16/21 DM0516/21007341 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/17/21 DM0517/21007382 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/18/21 DM0518/21007440 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
Page 19 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
240 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
250 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
05/22/21 DM0522/21008072
240 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
05/23/21 DM0523/21008085
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/25/21 DM0525/21008288
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/26/21 DM0526/21008319
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/27/21 DM0527/21008484
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/28/21 DM0528/21008495
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/29/21 DM0529/21008515
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/30/21 DM0530/21008530
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/01/21 DM0601/21008902
250 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
06/02/21 DM0602/21008935
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/03/21 DM0603/21008950
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/04/21 DM0604/21009184
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/05/21 DM0605/21009203
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/06/21 DM0606/21009287
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/07/21 DM0607/21009314
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/08/21 DM0608/21009334
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/09/21 DM0609/21009365
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/10/21 DM0610/21009538
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/11/21 DM0611/21009549
230 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
06/12/21 DM0612/21009568
290 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
06/13/21 DM0613/21009602
220 mg/kg D.W. 6.7 26 Q2. SW846: 6010C MMSD
06/14/21 DM0614/21009629
230 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
06/18/21 DM0618/21009979
210 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
06/19/21 DM0619/21010314
200 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/20/21 DM0620/21010332
210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/21/21 DM0621/21010359
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/22/21 DM0622/21010375
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/23/21 DM0623/21010408
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/24/21 DM0624/21010670
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/25/21 DM0625/21010681
230 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
06/26/21 DM0626/21010702
220 mg/kg D.W. 6.8 26
SW846: 6010C MMSD
06/27/21 DM0627/21010807
230 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
06/28/21 DM0628/21010860
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/29/21 DM0629/21010875
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/30/21 DM0630/21011438
230 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
07/01/21 DM0701/21011453
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/02/21 DM0702/21011465
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/03/21 DM0703/21011485
240 mg/kg D.W. 6.6 25 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/05/21 DM0705/21011572
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/06/21 DM0706/21011693
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/07/21 DM0707/21011727
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/08/21 DM0708/21011742
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
Page 20 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FP CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/12/21 DM0712/21012283
250 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/13/21 DM0713/21012298
260 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/14/21 DM0714/21012332
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/15/21 DM0715/21012390
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/16/21 DM0716/21012563
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/17/21 DM0717/21012583
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/18/21 DM0718/21012596
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/19/21 DM0719/21012624
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/20/21 DM0720/21012639
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/21/21 DM0721/21012760
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/22/21 DM0722/21012775
240 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
07/23/21 DM0723/21013074
220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
07/24/21 DM0724/21013378
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/25/21 DM0725/21013391
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/26/21 DM0726/21013419
230 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
07/27/21 DM0727/21013434
250 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
07/28/21 DM0728/21013470
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/29/21 DM0729/21013614
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/30/21 DM0730/21013629
240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/31/21 DM0731/21013739
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/01/21 DM0801/21013752
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/02/21 DM0802/21013891
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/03/21 DM0803/21013906
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/04/21 DM0804/21013940
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/05/21 DM0805/21014673
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/06/21 DM0806/21014685
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/07/21 DM0807/21014705
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/08/21 DM0809/21014718
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/09/21 DM0809/21014746
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/10/21 DM0810/21014847
250 mg/kg D.W. 6.6 25 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/12/21 DM0812/21015285
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/13/21 DM0813/21015297
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/14/21 DM0814/21015317
240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
08/15/21 DM0815/21015330
250 mg/kg D.W. 6.4 25
SW846: 6010C MMSD
08/16/21 DM0816/21015410
290 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
08/17/21 DM0817/21015425
270 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
08/18/21 DM0818/21016031
260 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
08/19/21 DM0819/21016046
260 mg/kg D.W.
6.5 25 Q3.
SW846: 6010C MMSD
08/20/21 DM0820/21016068
280 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/21/21 DM0821/21016088
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/22/21 DM0822/21016196
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/23/21 DM0823/21016224
270 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
Page 21 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
280 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
270 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD
08/26/21
DM0826/21016342
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/27/21
DM0827/21016407
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/28/21
DM0828/21016427
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/30/21
DM0830/21016468
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/31/21
DM0831/21016483
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/01/21
DM0901/21016598
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/02/21
DM0902/21016659
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/03/21
DM0903/21016671
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/04/21
DM0904/21017055
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/05/21
DM0905/21017068
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/06/21
DM0906/21017096
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/07/21
DM0907/21017306
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/08/21
DM0908/21017338
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/09/21
DM0909/21017408
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/10/21
DM0910/21017420
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/11/21
DM0911/21017699
230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/12/21
DM0912/21017712
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/13/21
DM0913/21017740
210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/14/21
DM0914/21017755
240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 149990-1
09/15/21
DM0915/21017903
220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 149990-1
09/16/21
DM0916/21018023
260 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150012-1
09/17/21
DM0917/21018105
260 mg/kg D.W. 6.7 25
SW846: 6010C MMSD 150074-1
09/18/21
DM0918/21018125
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150074-1
09/19/21
DM0919/21018138
250 mg/kg D.W. 6.7 25
SW846: 6010C MMSD 150074-1
09/20/21
DM0920/21018236
240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 150123-1
09/21/21
DM0921/21018251
260 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150123-1
09/22/21
DM0922/21018480
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/23/21
DM0923/21018564
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/24/21
DM0924/21018818
260 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150235-1
09/25/21
DM0925/21018838
250 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150235-1
09/26/21
DM0926/21019023
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150235-1
09/27/21
DM0927/21019051
250 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150235-2
09/28/21
DM0928/21019066
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150235-3
09/29/21
DM0929/21019228
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150305-1
09/30/21
DM0930/21019243
260 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150305-1
10/01/21
DM1001/21019255
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150305-1
10/02/21
DM1002/21019384
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 250 mg/kg D.W. 6.6 25 Q3. SW846: 6010C MMSD 150305-1
10/04/21
DM1004/21019425
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150376-1
10/06/21
DM1006/21019735
260 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150431-1
10/07/21
DM1007/21019760
250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150431-1
10/08/21
DM1008/21019772
240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150445-1
10/19/21
DM1019/21020600
260 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150655-1
10/20/21
DM1020/21020674
260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150655-1
Page 22 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
COPPER ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
250 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150703-1
10/23/21 D M 1023/21020883
230 mg/kg D.W. 6.5 25
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 220 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 220 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 230 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 230 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 220 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 240 mg/kg D.W. 6.5 25 SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 260 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 250 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 260 mg/kg D.W. 6.6 25 Q3.
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 240 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 230 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 240 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 220 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 230 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 240 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 240 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 230 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 240 mg/kg D.W. 6.7 26 Q3.
SW846: 6010C
MMSD 151371-1
Page 23 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEE FL CLER+fR ix�lE HERE
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
230 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 230 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 260 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 250 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 240 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 240 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 250 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 250 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 260 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 260 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 260 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 250 mg/kg D.W. 6.8 26
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 260 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 260 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 260 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 260 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 260 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD 151827-1
Avg Result: 240 mg/kg D.W. Min LOD: 6.4 mg/kg D.W.
Max Result: 290 mg/kg D.W. Max LOD: 6.8 mg/kg D.W.
Page 24 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
IRON ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
50000 mg/kg D.W.
82
330
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
51000 mg/kg D.W. 82 330
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
01/04/21 DM0104/21000488 52000 mg/kg D.W. 82 330
SW846: 6010C MMSD
01/05/21 DM0105/21000504 51000 mg/kg D.W. 83 330
SW846: 6010C MMSD
01/06/21 DM0106/21000535 51000 mg/kg D.W. 81 330
SW846: 6010C MMSD
01/07/21 DM0107/21000551 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/08/21 DM0108/21000562 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/09/21 DM0109/21000581 51000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/10/21 DM0110/21000594 48000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/11/21 DM0111/21000632 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/12/21 DM0112/21000648 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/13/21 DM0113/21000679 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD
01/14/21 DM0114/21000754 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
01/15/21 DM0115/21000765 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/16/21 DM0116/21000784 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/17/21 DM0117/21000797 49000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/19/21 DM0119/21000842 47000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
01/20/21 DM0120/21000926 43000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/21/21 DM0121/21000942 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/22/21 DM0122/21000953 46000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/23/21 DM0123/21000972 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/24/21 DM0124/21001059 50000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/25/21 DM0125/21001088 44000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/26/21 DM0126/21001106 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/27/21 DM0127/21001137 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
01/28/21 DM0128/21001153 48000 mg/kg D.W. 81 320 SW846: 6010C MMSD
01/29/21 DM0129/21001164 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD
01/30/21 DM0130/21001304 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD
01/31/21 DM0131/21001317 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/01/21 DM0201/21001344 51000 mg/kg D.W. 81 330 Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 54000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/04/21 DM0204/21001444 51000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/05/21 DM0205/21001455 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/06/21 DM0206/21001476 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/07/21 DM0207/21001489 52000 mg/kg D.W. 79 320 SW846: 6010C MMSD
02/08/21 DM0208/21001609 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
02/09/21 DM0209/21001625 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/10/21 DM0210/21001656 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/11/21 DM0211/21001672 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/12/21 DM0212/21001706 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/13/21 DM0213/21001725 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/14/21 DM0214/21001738 55000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/15/21 DM0215/21001793 56000 mg/kg D.W. 81 330 SW846: 6010C MMSD
Page 25 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
IRON ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
55000 mg/kg D.W.
81
330
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
50000 mg/kg D.W. 82 330
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
02/19/21 DM0219/21001986 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
02/20/21 DM0220/21002005 50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
02/21/21 DM0221/21002072 50000 mg/kg D.W. 81 320
SW846: 6010C MMSD
02/22/21 DM0222/21002230 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
02/23/21 DM0223/21002246 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/24/21 DM0224/21002281 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/25/21 DM0225/21002320 53000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/26/21 DM0226/21002386 52000 mg/kg D.W. 81 320 SW846: 6010C MMSD
02/27/21 DM0227/21002405 52000 mg/kg D.W. 80 320 SW846: 6010C MMSD
02/28/21 DM0228/21002478 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/01/21 DM0301/21002611 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/02/21 DM0302/21002629 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/03/21 DM0303/21002660 42000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/04/21 DM0304/21002717 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/05/21 DM0305/21002728 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/06/21 DM0306/21002747 42000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/07/21 DM0307/21002858 41000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/08/21 DM0308/21003336 42000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/09/21 DM0309/21003371 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/10/21 DM0310/21003402 44000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/11/21 DM0311/21003456 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/12/21 DM0312/21003522 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/13/21 DM0313/21003541 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/14/21 DM0314/21003554 43000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/15/21 DM0315/21003747 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/16/21 DM0316/21003801 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/17/21 DM0317/21003878 46000 mg/kg D.W. 81 330 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/19/21 DM0319/21003905 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/20/21 DM0320/21004076 49000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/21/21 DM0321/21004093 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/22/21 DM0322/21004120 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/23/21 DM0323/21004136 48000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/24/21 DM0324/21004167 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/25/21 DM0325/21004242 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/26/21 DM0326/21004253 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/27/21 DM0327/21004272 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/28/21 DM0328/21004285 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/29/21 DM0329/21004312 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/30/21 DM0330/21004388 53000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/31/21 DM0331/21004600 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/01/21 DM0401/21004616 51000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 44000 mg/kg D.W. 82 330 SW846: 6010C MMSD
Page 26 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
IRON ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
41000 mg/kg D.W.
81
330
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
49000 mg/kg D.W. 80 320
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
52000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/06/21 DM0406/21004758 52000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/07/21 DM0407/21004843 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/08/21 DM0408/21004861 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/09/21 DM0409/21004912 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/10/21 DM0410/21004931 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/11/21 DM0411/21005023 51000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/12/21 DM0412/21005052 41000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/13/21 DM0413/21005199 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/14/21 DM0414/21005230 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/15/21 DM0415/21005248 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/16/21 DM0416/21005259 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/17/21 DM0417/21005468 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/18/21 DM0418/21005481 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/19/21 DM0419/21005508 45000 mg/kg D.W. 83 330 SW846: 6010C MMSD
04/20/21 DM0420/21005839 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/21/21 DM0421/21005870 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/22/21 DM0422/21005981 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/23/21 DM0423/21005992 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/24/21 DM0424/21006057 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/25/21 DM0425/21006272 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/26/21 DM0426/21006299 49000 mg/kg D.W. 80 320 SW846: 6010C MMSD
04/27/21 DM0427/21006315 55000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/28/21 DM0428/21006346 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/29/21 DM0429/21006362 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/30/21 DM0430/21006373 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/01/21 DM0501/21006429 43000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/02/21 DM0502/21006442 41000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/03/21 DM0503/21006676 42000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/04/21 DM0504/21006691 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/05/21 DM0505/21006722 42000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/06/21 DM0506/21006781 41000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/07/21 DM0507/21006834 40000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/08/21 DM0508/21006981 40000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/09/21 DM0509/21006994 40000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/10/21 DM0510/21007021 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
05/11/21 DM0511/21007171 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/12/21 DM0512/21007202 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/13/21 DM0513/21007217 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/14/21 DM0514/21007309 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/15/21 DM0515/21007328 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/16/21 DM0516/21007341 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/17/21 DM0517/21007382 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/18/21 DM0518/21007440 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
Page 27 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
IRON ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
48000 mg/kg D.W.
81
320
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
44000 mg/kg D.W. 82 330
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
46000 mg/kg D.W. 82 330
SW846: 6010C MMSD
05/22/21 DM0522/21008072 48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
05/23/21 DM0523/21008085 49000 mg/kg D.W. 81 330
SW846: 6010C MMSD
05/25/21 DM0525/21008288 49000 mg/kg D.W. 80 320
SW846: 6010C MMSD
05/26/21 DM0526/21008319 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/27/21 DM0527/21008484 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/28/21 DM0528/21008495 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/29/21 DM0529/21008515 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/30/21 DM0530/21008530 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/01/21 DM0601/21008902 56000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/02/21 DM0602/21008935 52000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/03/21 DM0603/21008950 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/04/21 DM0604/21009184 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/05/21 DM0605/21009203 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/06/21 DM0606/21009287 48000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/07/21 DM0607/21009314 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/08/21 DM0608/21009334 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/09/21 DM0609/21009365 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/10/21 DM0610/21009538 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/11/21 DM0611/21009549 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/12/21 DM0612/21009568 54000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/13/21 DM0613/21009602 55000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/14/21 DM0614/21009629 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/18/21 DM0618/21009979 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/19/21 DM0619/21010314 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/20/21 DM0620/21010332 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/21/21 DM0621/21010359 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/22/21 DM0622/21010375 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/23/21 DM0623/21010408 57000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/24/21 DM0624/21010670 57000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/25/21 DM0625/21010681 56000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/26/21 DM0626/21010702 55000 mg/kg D.W. 83 330 SW846: 6010C MMSD
06/27/21 DM0627/21010807 54000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/28/21 DM0628/21010860 54000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/29/21 DM0629/21010875 59000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/30/21 DM0630/21011438 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/01/21 DM0701/21011453 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/02/21 DM0702/21011465 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/03/21 DM0703/21011485 48000 mg/kg D.W. 81 330 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/05/21 DM0705/21011572 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/06/21 DM0706/21011693 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/07/21 DM0707/21011727 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/08/21 DM0708/21011742 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
Page 28 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FP CLEktER ix�lE HERE
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
52000 mg/kg D.W.
80
320
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
49000 mg/kg D.W. 80 320
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/12/21 DM0712/21012283 50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/13/21 DM0713/21012298 54000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/14/21 DM0714/21012332 53000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/15/21 DM0715/21012390 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/16/21 DM0716/21012563 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/17/21 DM0717/21012583 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/18/21 DM0718/21012596 52000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/19/21 DM0719/21012624 55000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/20/21 DM0720/21012639 62000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/21/21 DM0721/21012760 58000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/22/21 DM0722/21012775 57000 mg/kg D.W. 82 330 SW846: 6010C MMSD
07/23/21 DM0723/21013074 54000 mg/kg D.W. 82 330 SW846: 6010C MMSD
07/24/21 DM0724/21013378 55000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/25/21 DM0725/21013391 56000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/26/21 DM0726/21013419 58000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/27/21 DM0727/21013434 62000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/28/21 DM0728/21013470 60000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/29/21 DM0729/21013614 56000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/30/21 DM0730/21013629 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/31/21 DM0731/21013739 56000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/01/21 DM0801/21013752 56000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/02/21 DM0802/21013891 60000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/03/21 DM0803/21013906 61000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/04/21 DM0804/21013940 58000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/05/21 DM0805/21014673 62000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/06/21 DM0806/21014685 56000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/07/21 DM0807/21014705 55000 mg/kg D.W. 81 320 SW846: 6010C MMSD
08/08/21 DM0809/21014718 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/09/21 DM0809/21014746 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/10/21 DM0810/21014847 59000 mg/kg D.W. 81 320 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 55000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/12/21 DM0812/21015285 58000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/13/21 DM0813/21015297 52000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/14/21 DM0814/21015317 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/15/21 DM0815/21015330 44000 mg/kg D.W. 79 320 SW846: 6010C MMSD
08/16/21 DM0816/21015410 48000 mg/kg D.W. 79 320 SW846: 6010C MMSD
08/17/21 DM0817/21015425 55000 mg/kg D.W. 79 320 SW846: 6010C MMSD
08/18/21 DM0818/21016031 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/19/21 DM0819/21016046 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/20/21 DM0820/21016068 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/21/21 DM0821/21016088 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/22/21 DM0822/21016196 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/23/21 DM0823/21016224 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD
Page 29 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
IRON ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
52000 mg/kg D.W.
81
320
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
52000 mg/kg D.W. 80 320
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
51000 mg/kg D.W. 81 320
SW846: 6010C MMSD
08/27/21 DM0827/21016407 52000 mg/kg D.W. 81 320
SW846: 6010C MMSD
08/28/21 DM0828/21016427 51000 mg/kg D.W. 81 320
SW846: 6010C MMSD
08/30/21 DM0830/21016468 50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
08/31/21 DM0831/21016483 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/01/21 DM0901/21016598 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/02/21 DM0902/21016659 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/03/21 DM0903/21016671 42000 mg/kg D.W. 81 330 SW846: 6010C MMSD
09/04/21 DM0904/21017055 40000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/05/21 DM0905/21017068 41000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/06/21 DM0906/21017096 41000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/07/21 DM0907/21017306 41000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/08/21 DM0908/21017338 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/09/21 DM0909/21017408 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/10/21 DM0910/21017420 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/11/21 DM0911/21017699 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/12/21 DM0912/21017712 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
09/13/21 DM0913/21017740 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/14/21 DM0914/21017755 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 49000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 52000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 51000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/23/21 DM0923/21018564 44000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/24/21 DM0924/21018818 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 48000 mg/kg D.W. 79 320 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 49000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 44000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 53000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 52000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 51000 mg/kg D.W. 79 320 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150655-1
Page 30 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
IRON ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
46000 mg/kg D.W.
80
320
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
48000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
47000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 48000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 46000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 48000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 48000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 47000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 47000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 49000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 46000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 47000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 47000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 47000 mg/kg D.W. 81 330 Q3.
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 45000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 44000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 45000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 47000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 48000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 44000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 48000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 49000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 45000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 47000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 45000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 46000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 47000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 47000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 47000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 43000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151371-1
Page 31 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FL CLEktER ix�lE HERE
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
48000 mg/kg D.W.
82
330
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
43000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
42000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 42000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 44000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 45000 mg/kg D.W. 81 320
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 46000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 44000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 49000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 46000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 48000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 49000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 49000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 48000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 48000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 47000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 47000 mg/kg D.W. 83 340
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 47000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 46000 mg/kg D.W. 83 330
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 47000 mg/kg D.W. 81 330
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 47000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 45000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 46000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151827-1
Avg Result: 49000 mg/kg D.W. Min LOD: 79 mg/kg D.W.
Max Result: 62000 mg/kg D.W. Max LOD: 83 mg/kg D.W.
Page 32 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
16 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
16 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
15 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
01/04/21 DM0104/21000488 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/05/21 DM0105/21000504 16 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/06/21 DM0106/21000535 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/07/21 DM0107/21000551 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/08/21 DM0108/21000562 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/09/21 DM0109/21000581 16 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/10/21 DM0110/21000594 15 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/11/21 DM0111/21000632 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/12/21 DM0112/21000648 14 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/13/21 DM0113/21000679 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/14/21 DM0114/21000754
01/15/21 DM0115/21000765
01/16/21 DM0116/21000784
16 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
15 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
14 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
01/17/21 DM0117/21000797 15 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 18 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/19/21 DM0119/21000842 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/20/21 DM0120/21000926 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/21/21 DM0121/21000942 22 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/22/21 DM0122/21000953 18 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/23/21 DM0123/21000972 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/24/21 DM0124/21001059 18 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/25/21 DM0125/21001088 14 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/26/21 DM0126/21001106 16 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
01/27/21 DM0127/21001137 17 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/28/21 DM0128/21001153 16 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
01/29/21 DM0129/21001164 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
01/30/21 DM0130/21001304 19 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
01/31/21 DM0131/21001317 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/01/21 DM0201/21001344 16 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 18 mg/kg D.W. 1.3 5.3 D2. SW846: 6010C MMSD
02/03/21 DM0203/21001428 14 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/04/21 DM0204/21001444 18 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/05/21 DM0205/21001455 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/06/21 DM0206/21001476 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/07/21 DM0207/21001489 15 mg/kg D.W. 1.2 5.1 SW846: 6010C MMSD
02/08/21 DM0208/21001609 14 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
02/09/21 DM0209/21001625 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/10/21 DM0210/21001656 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/11/21 DM0211/21001672 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/12/21 DM0212/21001706 17 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/13/21 DM0213/21001725 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/14/21 DM0214/21001738 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/15/21 DM0215/21001793 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
Page 33 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
15 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
12 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
14 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
02/19/21 DM0219/21001986 12 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/20/21 DM0220/21002005 11 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
02/21/21 DM0221/21002072 11 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
02/22/21 DM0222/21002230 12 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
02/23/21 DM0223/21002246 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/24/21 DM0224/21002281 14 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
02/25/21 DM0225/21002320 12 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
02/26/21 DM0226/21002386 15 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
02/27/21 DM0227/21002405 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
02/28/21 DM0228/21002478 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/01/21 DM0301 /21002611
03/02/21 DM0302/21002629
03/03/21 DM0303/21002660
14 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
18 mg/kg D.W.
15 mg/kg D.W.
1.2 5.2
1.2 5.2
SW846: 6010C MMSD
SW846: 6010C MMSD
03/04/21 DM0304/21002717 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/05/21 DM0305/21002728 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/06/21 DM0306/21002747 15 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/07/21 DM0307/21002858 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/08/21 DM0308/21003336 14 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/09/21 DM0309/21003371 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/10/21 DM031 0/21 003402 14 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/11/21 DM0311/21003456 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/12/21 DM0312/21003522 18 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/13/21 DM0313/21003541 18 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/14/21 DM0314/21003554 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/15/21 DM0315/21003747 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/16/21 DM0316/21003801 18 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/17/21 DM0317/21003878 17 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/18/21 DM0318/21003894 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/19/21 DM0319/21003905 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/20/21 DM0320/21004076 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/21/21 DM0321/21004093 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/22/21 DM0322/21004120 15 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
03/23/21 DM0323/21004136 15 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
03/24/21 DM0324/21004167 14 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/25/21 DM0325/21004242 17 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
03/26/21 DM0326/21004253 18 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/27/21 DM0327/21004272 17 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/28/21 DM0328/21004285 18 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/29/21 DM0329/21004312 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/30/21 DM0330/21004388 22 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
03/31/21 DM0331/21004600 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/01/21 DM0401/21004616 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/02/21 DM0402/21004627 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
Page 34 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
17 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
15 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
15 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
04/06/21 DM0406/21004758 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/07/21 DM0407/21004843 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/08/21 DM0408/21004861 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/09/21 DM0409/21004912 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/10/21 DM0410/21004931 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/11/21 DM0411/21005023 24 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/12/21 DM0412/21005052 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/13/21 DM0413/21005199 23 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/14/21 DM0414/21005230 18 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/15/21 DM0415/21005248 19 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
04/16/21 DM0416/21005259 17 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/17/21 DM0417/21005468 17 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/18/21 DM0418/21005481 18 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/19/21 DM0419/21005508 17 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
04/20/21 DM0420/21005839 21 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
04/21/21 DM0421/21005870 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
04/22/21 DM0422/21005981 18 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
04/23/21 DM0423/21005992 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
04/24/21 DM0424/21006057 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
04/25/21 DM0425/21006272 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/26/21 DM0426/21006299 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
04/27/21 DM0427/21006315 19 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
04/28/21 DM0428/21006346 16 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
04/29/21 DM0429/21006362 15 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
04/30/21 DM0430/21006373 15 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/01/21 DM0501/21006429 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/02/21 DM0502/21006442 16 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/03/21 DM0503/21006676 15 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/04/21 DM0504/21006691 19 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/05/21 DM0505/21006722 17 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/06/21 DM0506/21006781 19 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/07/21 DM0507/21006834 21 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/08/21 DM0508/21006981 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/09/21 DM0509/21006994 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/10/21 DM0510/21007021 18 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/11/21 DM0511/21007171 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/12/21 DM0512/21007202 21 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
05/13/21 DM0513/21007217 22 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/14/21 DM0514/21007309 19 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
05/15/21 DM0515/21007328 19 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/16/21 DM0516/21007341 23 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/17/21 DM0517/21007382 53 mg/kg D.W. 1.2 5.2 Q3. SW846: 6010C MMSD
05/18/21 DM0518/21007440 38 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
Page 35 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
22 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
32 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
26 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
05/22/21 DM0522/21008072 27 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
05/23/21 DM0523/21008085 27 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/25/21 DM0525/21008288 21 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/26/21 DM0526/21008319 21 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/27/21 DM0527/21008484 24 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
05/28/21 DM0528/21008495 22 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/29/21 DM0529/21008515 21 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
05/30/21 DM0530/21008530 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/01/21 DM0601/21008902 31 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/02/21 DM0602/21008935 27 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
06/03/21 DM0603/21008950 21 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/04/21 DM0604/21009184 27 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/05/21 DM0605/21009203 44 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
06/06/21 DM0606/21009287 22 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/07/21 DM0607/21009314 27 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/08/21 DM0608/21009334 33 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/09/21 DM0609/21009365 20 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/10/21 DM0610/21009538 24 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/11/21 DM0611/21009549 28 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/12/21 DM0612/21009568 29 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/13/21 DM0613/21009602 47 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
06/14/21 DM0614/21009629 24 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/18/21 DM0618/21009979 21 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/19/21 DM0619/21010314 30 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/20/21 DM0620/21010332 21 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/21/21 DM0621/21010359 32 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
06/22/21 DM0622/21010375 22 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/23/21 DM0623/21010408 34 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
06/24/21 DM0624/21010670 25 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/25/21 DM0625/21010681 23 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/26/21 DM0626/21010702 27 mg/kg D.W. 1.3 5.4 SW846: 6010C MMSD
06/27/21 DM0627/21010807 26 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/28/21 DM0628/21010860 26 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
06/29/21 DM0629/21010875 28 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
06/30/21 DM0630/21011438 23 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
07/01/21 DM0701/21011453 42 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
07/02/21 DM0702/21011465 40 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/03/21 DM0703/21011485 31 mg/kg D.W. 1.3 5.3 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 29 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
07/05/21 DM0705/21011572 28 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
07/06/21 DM0706/21011693 31 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/07/21 DM0707/21011727 31 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/08/21 DM0708/21011742 32 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
Page 36 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FP CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
31 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
30 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
28 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
07/12/21 DM0712/21012283 29 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/13/21 DM0713/21012298 34 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/14/21 DM0714/21012332 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/15/21 DM0715/21012390 28 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/16/21 DM0716/21012563 34 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/17/21 DM0717/21012583 32 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
07/18/21 DM0718/21012596 33 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/19/21 DM0719/21012624 31 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/20/21 DM0720/21012639 64 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/21/21 DM0721/21012760 52 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/22/21 DM0722/21012775 69 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
07/23/21 DM0723/21013074 83 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
07/24/21 DM0724/21013378 94 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
07/25/21 DM0725/21013391 48 mg/kg D.W. 1.3 5.2 Q2. SW846: 6010C MMSD
07/26/21 DM0726/21013419 50 mg/kg D.W. 1.3 5.3 Q2. SW846: 6010C MMSD
07/27/21 DM0727/21013434 44 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
07/28/21 DM0728/21013470 29 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/29/21 DM0729/21013614 28 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/30/21 DM0730/21013629 28 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
07/31/21 DM0731/21013739 31 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
08/01/21 DM0801/21013752 26 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
08/02/21 DM0802/21013891 26 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
08/03/21 DM0803/21013906 33 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/04/21 DM0804/21013940 38 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/05/21 DM0805/21014673 35 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/06/21 DM0806/21014685 27 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/07/21 DM0807/21014705 30 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/08/21 DM0809/21014718 30 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/09/21 DM0809/21014746 35 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/10/21 DM0810/21014847 43 mg/kg D.W. 1.2 5.2 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 41 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
08/12/21 DM0812/21015285 41 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
08/13/21 DM0813/21015297 40 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/14/21 DM0814/21015317 52 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/15/21 DM0815/21015330 60 mg/kg D.W. 1.2 5.1 SW846: 6010C MMSD
08/16/21 DM0816/21015410 84 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/17/21 DM0817/21015425 58 mg/kg D.W. 1.2 5.1 SW846: 6010C MMSD
08/18/21 DM0818/21016031 59 mg/kg D.W. 1.2 5.2 Q2. SW846: 6010C MMSD
08/19/21 DM0819/21016046 49 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/20/21 DM0820/21016068 100 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/21/21 DM0821/21016088 40 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/22/21 DM0822/21016196 45 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
08/23/21 DM0823/21016224 37 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
Page 37 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
40 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
08/25/21
DM0825/21 01 6327
41 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
42 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
08/27/21 DM0827/21016407 38 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
08/28/21 DM0828/21016427 38 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
08/30/21 DM0830/21016468 39 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/31/21 DM0831/21016483 50 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/01/21 DM0901/21016598 43 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/02/21 DM0902/21016659 44 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/03/21 DM0903/21016671 48 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
09/04/21 DM0904/21017055 52 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/05/21 DM0905/21017068 49 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/06/21 DM0906/21017096 50 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/07/21 DM0907/21017306 50 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/08/21 DM0908/21017338 47 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
09/09/21 DM0909/21017408 40 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
09/10/21 DM0910/21017420 42 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
09/11/21 DM0911/21017699 40 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/12/21 DM0912/21017712 39 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
09/13/21 DM0913/21017740 40 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD
09/14/21 DM0914/21017755 39 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 41 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 45 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 48 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 43 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 40 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 38 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 42 mg/kg D.W. 1.3 5.2
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 45 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/23/21 DM0923/21018564 42 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD
09/24/21 DM0924/21018818 44 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 41 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 39 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 37 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 38 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 35 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 35 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 34 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 33 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 32 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 31 mg/kg D.W. 1.3 5.2 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 29 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 28 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 28 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 28 mg/kg D.W. 1.2 5.1 SW846: 6010C MMSD 150655-1
10/20/21 DM1 020/21 020674 32 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150655-1
Page 38 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
LEAD ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
27 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
30 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
29 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 30 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 31 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 29 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 25 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 25 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 25 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 25 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 24 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 26 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720
11/04/21 DM1104/21021735
11/05/21 DM1105/21021747
26 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150884-1
24 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150884-1
26 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 24 mg/kg D.W. 1.2 5.2 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 23 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 23 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 24 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 24 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 24 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 25 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 26 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 24 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 24 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 26 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 29 mg/kg D.W. 1.3 5.2
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 22 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 25 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 28 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 23 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 22 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 19 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 22 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 26 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 20 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 24 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 22 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 22 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 23 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 23 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 21 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 20 mg/kg D.W. 1.2 5.2
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 19 mg/kg D.W. 1.3 5.3
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 19 mg/kg D.W. 1.3 5.3 D2, Q3. SW846: 6010C MMSD 151371-1
Page 39 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEE FL CLER+fR ix�lE HERE
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
23 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
20 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
21 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 20 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 21 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 20 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 21 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 22 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 40 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 24 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 27 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 23 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 22 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 21 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 20 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 20 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 22 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 20 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 20 mg/kg D.W.
1.3 5.4
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 19 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 19 mg/kg D.W. 1.3 5.4
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 20 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 20 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 21 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 22 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 21 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151827-1
Avg Result: 26 mg/kg D.W. Min LOD: 1.2 mg/kg D.W.
Max Result: 100 mg/kg D.W. Max LOD: 1.3 mg/kg D.W.
Page 40 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
9.5 mg/kg D.W.
0.44
1.7
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
9.7 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/04/21 DM0104/21000488 9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/05/21 DM0105/21000504 9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/06/21 DM0106/21000535 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/07/21 DM0107/21000551 9.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/08/21 DM0108/21000562 9.5 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/09/21 DM0109/21000581 9.5 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/10/21 DM0110/21000594 9.1 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/11/21 DM0111/21000632 9.3 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/12/21 DM0112/21000648 9.3 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
01/13/21 DM0113/21000679 9.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/14/21 DM0114/21000754 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/15/21 DM0115/21000765 9.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/16/21 DM0116/21000784 9.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/17/21 DM0117/21000797 9.3 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 10 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/19/21 DM0119/21000842 9.4 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
01/20/21 DM0120/21000926 9.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/21/21 DM0121/21000942 9.6 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/22/21 DM0122/21000953 10 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/23/21 DM0123/21000972 10 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/24/21 DM0124/21001059 9.9 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/25/21 DM0125/21001088 8.5 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/26/21 DM0126/21001106 8.7 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
01/27/21 DM0127/21001137 8.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/28/21 DM0128/21001153 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/29/21 DM0129/21001164 10 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
01/30/21 DM0130/21001304 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
01/31/21 DM0131/21001317 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/01/21 DM0201/21001344 8.7 mg/kg D.W. 0.43 1.7 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 10 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 9.4 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
02/04/21 DM0204/21001444 9.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/05/21 DM0205/21001455 9.8 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
02/06/21 DM0206/21001476 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/07/21 DM0207/21001489 9.8 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
02/08/21 DM0208/21001609 9.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/09/21 DM0209/21001625 9.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/10/21 DM0210/21001656 9.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/11/21 DM0211/21001672 8.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/12/21 DM0212/21001706 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/13/21 DM0213/21001725 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/14/21 DM0214/21001738 15 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
02/15/21 DM0215/21001793 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
Page 41 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
10 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
9.4 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
02/19/21 DM0219/21001986 9.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/20/21 DM0220/21002005 9.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/21/21 DM0221/21002072 9.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/22/21 DM0222/21002230 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/23/21 DM0223/21002246 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/24/21 DM0224/21002281 8.9 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
02/25/21 DM0225/21002320 9.2 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
02/26/21 DM0226/21002386 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/27/21 DM0227/21002405 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
02/28/21 DM0228/21002478 9.4 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
03/01/21 DM0301/21002611 8.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/02/21 DM0302/21002629 9.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/03/21 DM0303/21002660 8.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/04/21 DM0304/21002717 8.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/05/21 DM0305/21002728 8.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/06/21 DM0306/21002747 8.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/07/21 DM0307/21002858 8.8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/08/21 DM0308/21003336 8.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/09/21 DM0309/21003371 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/10/21 DM0310/21003402 8.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/11/21 DM0311/21003456 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/12/21 DM0312/21003522 9.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/13/21 DM0313/21003541 9.8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/14/21 DM0314/21003554 8.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/15/21 DM0315/21003747 9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/16/21 DM0316/21003801 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/17/21 DM0317/21003878 9.3 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 8.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/19/21 DM0319/21003905 8.4 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
03/20/21 DM0320/21004076 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/21/21 DM0321/21004093 8.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/22/21 DM0322/21004120 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/23/21 DM0323/21004136 8.3 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/24/21 DM0324/21004167 8.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/25/21 DM0325/21004242 8.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/26/21 DM0326/21004253 8.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/27/21 DM0327/21004272 8.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
03/28/21 DM0328/21004285 8.4 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
03/29/21 DM0329/21004312 8.5 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
03/30/21 DM0330/21004388 8.1 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
03/31/21 DM0331/21004600 8 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/01/21 DM0401/21004616 8.1 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/02/21 DM0402/21004627 8.6 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
Page 42 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
8.5 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
9 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/06/21 DM0406/21004758 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/07/21 DM0407/21004843 8.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/08/21 DM0408/21004861 8.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/09/21 DM0409/21004912 8.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/10/21 DM0410/21004931 8 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/11/21 DM0411/21005023 8.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/12/21 DM0412/21005052 7.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/13/21 DM0413/21005199 8.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/14/21 DM0414/21005230 7.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/15/21 DM0415/21005248 8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/16/21 DM0416/21005259 7.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/17/21 DM0417/21005468 7.6 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/18/21 DM0418/21005481 7.8 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/19/21 DM0419/21005508 7.6 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/20/21 DM0420/21005839 8.7 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
04/21/21 DM0421/21005870 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/22/21 DM0422/21005981 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/23/21 DM0423/21005992 8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/24/21 DM0424/21006057 8.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/25/21 DM0425/21006272 8.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/26/21 DM0426/21006299 9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/27/21 DM0427/21006315 9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/28/21 DM0428/21006346 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/29/21 DM0429/21006362 8.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
04/30/21 DM0430/21006373 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/01/21 DM0501/21006429 7.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/02/21 DM0502/21006442 7.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/03/21 DM0503/21006676 7.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/04/21 DM0504/21006691 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/05/21 DM0505/21006722 8.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/06/21 DM0506/21006781 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/07/21 DM0507/21006834 8.3 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
05/08/21 DM0508/21006981 8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/09/21 DM0509/21006994 7.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/10/21 DM0510/21007021 7.6 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
05/11/21 DM0511/21007171 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/12/21 DM0512/21007202 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/13/21 DM0513/21007217 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/14/21 DM0514/21007309 7.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/15/21 DM0515/21007328 8.1 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/16/21 DM0516/21007341 8.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/17/21 DM0517/21007382 8.3 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/18/21 DM0518/21007440 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
Page 43 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
8.4 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
8.3 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
8.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
05/22/21 DM0522/21008072 8.4 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
05/23/21 DM0523/21008085 8.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/25/21 DM0525/21008288 8.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/26/21 DM0526/21008319 8.8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/27/21 DM0527/21008484 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/28/21 DM0528/21008495 8.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/29/21 DM0529/21008515 8.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
05/30/21 DM0530/21008530 8.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/01/21 DM0601/21008902 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/02/21 DM0602/21008935 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/03/21 DM0603/21008950 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/04/21 DM0604/21009184 9.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/05/21 DM0605/21009203 9.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/06/21 DM0606/21009287 9.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/07/21 DM0607/21009314 9.3 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/08/21 DM0608/21009334 9.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/09/21 DM0609/21009365 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/10/21 DM0610/21009538 9.2 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/11/21 DM0611/21009549 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/12/21 DM0612/21009568 10 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
06/13/21 DM0613/21009602 10 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
06/14/21 DM0614/21009629 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/18/21 DM0618/21009979 9.2 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
06/19/21 DM0619/21010314 9.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/20/21 DM0620/21010332 9.3 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/21/21 DM0621/21010359 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/22/21 DM0622/21010375 9.5 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/23/21 DM0623/21010408 9.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/24/21 DM0624/21010670 9.6 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/25/21 DM0625/21010681 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/26/21 DM0626/21010702 9.6 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
06/27/21 DM0627/21010807 9.8 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD
06/28/21 DM0628/21010860 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/29/21 DM0629/21010875 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
06/30/21 DM0630/21011438 9.4 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/01/21 DM0701/21011453 9.8 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/02/21 DM0702/21011465 9.7 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/03/21 DM0703/21011485 10 mg/kg D.W. 0.43 1.7 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/05/21 DM0705/21011572 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/06/21 DM0706/21011693 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/07/21 DM0707/21011727 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/08/21 DM0708/21011742 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
Page 44 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
10 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
9.9 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
10 mg/kg D.W. 0.42 1.7
SW846: 6010C MMSD
07/12/21 DM0712/21012283 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/13/21 DM0713/21012298 11 mg/kg D.W. 0.42 1.7
SW846: 6010C MMSD
07/14/21 DM0714/21012332 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/15/21 DM0715/21012390 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/16/21 DM0716/21012563 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/17/21 DM0717/21012583 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/18/21 DM0718/21012596 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/19/21 DM0719/21012624 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/20/21 DM0720/21012639 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/21/21 DM0721/21012760 15 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
07/22/21 DM0722/21012775 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/23/21 DM0723/21013074 9.9 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/24/21 DM0724/21013378 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/25/21 DM0725/21013391 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/26/21 DM0726/21013419 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/27/21 DM0727/21013434 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/28/21 DM0728/21013470 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/29/21 DM0729/21013614 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
07/30/21 DM0730/21013629 10 mg/kg D.W. 0.42 1.7 SW846: 6010C MMSD
07/31/21 DM0731/21013739 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/01/21 DM0801/21013752 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/02/21 DM0802/21013891 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/03/21 DM0803/21013906 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/04/21 DM0804/21013940 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/05/21 DM0805/21014673 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/06/21 DM0806/21014685 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/07/21 DM0807/21014705 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/08/21 DM0809/21014718 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/09/21 DM0809/21014746 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/10/21 DM0810/21014847 12 mg/kg D.W. 0.43 1.7 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/12/21 DM0812/21015285 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/13/21 DM0813/21015297 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/14/21 DM0814/21015317 11 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
08/15/21 DM0815/21015330 9.6 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
08/16/21 DM0816/21015410 13 mg/kg D.W. 0.42 1.6 Q3. SW846: 6010C MMSD
08/17/21 DM0817/21015425 11 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
08/18/21 DM0818/21016031 10 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
08/19/21 DM0819/21016046 10 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD
08/20/21 DM0820/21016068 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/21/21 DM0821/21016088 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/22/21 DM0822/21016196 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
08/23/21 DM0823/21016224 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
Page 45 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
11 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
11 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/27/21 DM0827/21016407 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/28/21 DM0828/21016427 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/30/21 DM0830/21016468 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/31/21 DM0831/21016483 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/01/21 DM0901/21016598 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/02/21 DM0902/21016659 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/03/21 DM0903/21016671 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/04/21 DM0904/21017055 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/05/21 DM0905/21017068 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/06/21 DM0906/21017096 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/07/21 DM0907/21017306 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/08/21 DM0908/21017338 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/09/21 DM0909/21017408 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/10/21 DM0910/21017420 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/11/21 DM0911/21017699 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/12/21 DM0912/21017712 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/13/21 DM0913/21017740 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/14/21 DM0914/21017755 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 11 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 11 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/23/21 DM0923/21018564 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD
09/24/21 DM0924/21018818 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 11 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 11 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 11 mg/kg D.W. 0.42 1.7 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 10 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 11 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 12 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 12 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 14 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150655-1
Page 46 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
MOLYBDENUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
12 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
12 mg/kg D.W. 0.42 1.6
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 11 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 12 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 12 mg/kg D.W. 0.42 1.6 SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 13 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 13 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 12 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 13 mg/kg D.W. 0.43 1.7 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 12 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 13 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 12 mg/kg D.W. 0.44 1.7 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 12 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 15 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 13 mg/kg D.W. 0.44 1.7 D2, Q3. SW846: 6010C MMSD 151371-1
Page 47 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEE FL CLER+fR ix�lE HERE
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
13 mg/kg D.W.
0.44
1.7
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 13 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 13 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 13 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 14 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 14 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 14 mg/kg D.W. 0.43 1.7
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 12 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 13 mg/kg D.W. 0.44 1.7
SW846: 6010C
MMSD 151827-1
Avg Result: 10 mg/kg D.W. Min LOD: 0.42 mg/kg D.W.
Max Result: 15 mg/kg D.W. Max LOD: 0.44 mg/kg D.W.
Page 48 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
19 mg/kg D.W.
0.99
3.9
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
20 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
18 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/04/21 DM0104/21000488
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
01/05/21 DM0105/21000504
20 mg/kg D.W. 1 4
SW846: 6010C MMSD
01/06/21 DM0106/21000535
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/07/21 DM0107/21000551
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/08/21 DM0108/21000562
20 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
01/09/21 DM0109/21000581
20 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/10/21 DM0110/21000594
19 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/11/21 DM0111/21000632
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
01/12/21 DM0112/21000648
20 mg/kg D.W.
0.99 3.9 Q3.
SW846: 6010C MMSD
01/13/21 DM0113/21000679
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/14/21 DM0114/21000754
01/15/21 DM0115/21000765
01/16/21 DM0116/21000784
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
19 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/17/21 DM0117/21000797
19 mg/kg D.W.
0.99 4 Q3.
SW846: 6010C MMSD
01/18/21 DM0118/21000824
24 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/19/21 DM0119/21000842
23 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
01/20/21 DM0120/21000926
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/21/21 DM0121/21000942
23 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
01/22/21 DM0122/21000953
22 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/23/21 DM0123/21000972
23 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
01/24/21 DM0124/21001059
22 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/25/21 DM0125/21001088
18 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/26/21 DM0126/21001106
19 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/27/21 DM0127/21001137
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/28/21 DM0128/21001153
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/29/21 DM0129/21001164
22 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
01/30/21 DM0130/21001304
25 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
01/31/21 DM0131/21001317
22 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/01/21 DM0201/21001344
21 mg/kg D.W.
0.98 3.9 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397
25 mg/kg D.W. 0.99 3.9 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428
22 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/04/21 DM0204/21001444
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/05/21 DM0205/21001455
23 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/06/21 DM0206/21001476
25 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/07/21 DM0207/21001489
24 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
02/08/21 DM0208/21001609
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
02/09/21 DM0209/21001625
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/10/21 DM0210/21001656
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/11/21 DM0211/21001672
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/12/21 DM0212/21001706
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/13/21 DM0213/21001725
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/14/21 DM0214/21001738
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/15/21 DM0215/21001793
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
Page 49 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FL CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
22 mg/kg D.W.
0.98
3.9
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
21 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/19/21 DM0219/21001986
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/20/21 DM0220/21002005
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
02/21/21 DM0221/21002072
20 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
02/22/21 DM0222/21002230
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/23/21 DM0223/21002246
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/24/21 DM0224/21002281
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/25/21 DM0225/21002320
20 mg/kg D.W. 1 4 SW846: 6010C MMSD
02/26/21 DM0226/21002386
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/27/21 DM0227/21002405
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
02/28/21 DM0228/21002478
25 mg/kg D.W. 0.98
3.9 Q3.
SW846: 6010C MMSD
03/01/21 DM0301/21002611
03/02/21 DM0302/21002629
03/03/21 DM0303/21002660
20 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
23 mg/kg D.W.
20 mg/kg D.W.
0.97 3.9
0.97 3.9
SW846: 6010C MMSD
SW846: 6010C MMSD
03/04/21 DM0304/21002717
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/05/21 DM0305/21002728
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/06/21 DM0306/21002747
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
03/07/21 DM0307/21002858
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/08/21 DM0308/21003336
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/09/21 DM0309/21003371
26 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/10/21 DM0310/21003402
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/11/21 DM0311/21003456
30 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/12/21 DM0312/21003522
22 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
03/13/21 DM0313/21003541
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
03/14/21 DM0314/21003554
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/15/21 DM0315/21003747
22 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
03/16/21 DM0316/21003801
27 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
03/17/21 DM0317/21003878
24 mg/kg D.W. 0.98 3.9 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/19/21 DM0319/21003905
22 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
03/20/21 DM0320/21004076
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
03/21/21 DM0321/21004093
22 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
03/22/21 DM0322/21004120
22 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
03/23/21 DM0323/21004136
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/24/21 DM0324/21004167
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/25/21 DM0325/21004242
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/26/21 DM0326/21004253
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/27/21 DM0327/21004272
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/28/21 DM0328/21004285
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
03/29/21 DM0329/21004312
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
03/30/21 DM0330/21004388
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
03/31/21 DM0331/21004600
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
04/01/21 DM0401/21004616
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
04/02/21 DM0402/21004627
23 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
Page 50 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
22 mg/kg D.W.
0.98
3.9
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
22 mg/kg D.W.
0.97 3.9
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
04/06/21 DM0406/21004758 26 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/07/21 DM0407/21004843 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/08/21 DM0408/21004861 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/09/21 DM0409/21 00491 2 21 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
04/10/21 DM0410/21004931 20 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
04/11/21 DM0411/21005023 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/12/21 DM041 2/21 005052 19 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/13/21 DM0413/21005199 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/14/21 DM0414/21005230 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/15/21 DM041 5/21 005248 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/16/21 DM0416/21005259 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/17/21 DM0417/21005468 19 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
04/18/21 DM0418/21005481 20 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
04/19/21 DM0419/21005508 19 mg/kg D.W. 1 4 SW846: 6010C MMSD
04/20/21 DM0420/21005839 24 mg/kg D.W. 1 4 SW846: 6010C MMSD
04/21/21 DM0421/21005870 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/22/21 DM0422/21005981 20 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
04/23/21 DM0423/21005992 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/24/21 DM0424/21006057 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/25/21 DM0425/21006272 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/26/21 DM0426/21006299 20 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
04/27/21 DM0427/21006315 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/28/21 DM0428/21006346 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/29/21 DM0429/21006362 19 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
04/30/21 DM0430/21006373 18 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD
05/01/21 DM0501/21006429 18 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/02/21 DM0502/21006442 18 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/03/21 DM0503/21006676 18 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/04/21 DM0504/21006691 22 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/05/21 DM0505/21006722 19 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/06/21 DM0506/21006781 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/07/21 DM0507/21006834 21 mg/kg D.W. 0.96 3.8 SW846: 6010C MMSD
05/08/21 DM0508/21006981 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/09/21 DM0509/21006994 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/10/21 DM0510/21007021 20 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
05/11/21 DM0511/21007171 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/12/21 DM0512/21007202 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/13/21 DM0513/21007217 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/14/21 DM0514/21007309 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/15/21 DM0515/21007328 21 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/16/21 DM0516/21007341 25 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/17/21 DM0517/21007382 23 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/18/21 DM0518/21007440 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
Page 51 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
24 mg/kg D.W.
0.97
3.9
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
22 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
05/22/21 DM0522/21008072 21 mg/kg D.W. 1 4
SW846: 6010C MMSD
05/23/21 DM0523/21008085 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/25/21 DM0525/21008288 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
05/26/21 DM0526/21008319 22 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/27/21 DM0527/21008484 24 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
05/28/21 DM0528/21008495 19 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/29/21 DM0529/21008515 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
05/30/21 DM0530/21008530 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/01/21 DM0601/21008902 24 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
06/02/21 DM0602/21008935 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/03/21 DM0603/21008950 20 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
06/04/21 DM0604/21009184 20 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
06/05/21 DM0605/21009203 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/06/21 DM0606/21009287 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/07/21 DM0607/21009314 19 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD
06/08/21 DM0608/21009334 24 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/09/21 DM0609/21009365 19 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/10/21 DM0610/21009538 19 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/11/21 DM0611/21009549 22 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/12/21 DM0612/21009568 23 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
06/13/21 DM0613/21009602 22 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
06/14/21 DM0614/21009629 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/18/21 DM0618/21009979 20 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
06/19/21 DM0619/21010314 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/20/21 DM0620/21010332 22 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/21/21 DM0621/21010359 22 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/22/21 DM0622/21010375 21 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
06/23/21 DM0623/21010408 21 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
06/24/21 DM0624/21010670 20 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/25/21 DM0625/21010681 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/26/21 DM0626/21010702 21 mg/kg D.W. 1 4 SW846: 6010C MMSD
06/27/21 DM0627/21010807 21 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
06/28/21 DM0628/21010860 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/29/21 DM0629/21010875 27 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
06/30/21 DM0630/21011438 21 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
07/01/21 DM0701/21011453 22 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
07/02/21 DM0702/21011465 23 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
07/03/21 DM0703/21011485 23 mg/kg D.W. 0.98 3.9 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 24 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
07/05/21 DM0705/21011572 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
07/06/21 DM0706/21011693 23 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
07/07/21 DM0707/21011727 23 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
07/08/21 DM0708/21011742 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
Page 52 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PAR111Ell FP CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
23 mg/kg D.W.
0.97
3.9
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
22 mg/kg D.W.
0.97 3.8
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
23 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
07/12/21 DM0712/21012283
22 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
07/13/21 DM0713/21012298
26 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
07/14/21 DM0714/21012332
22 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/15/21 DM0715/21012390
22 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/16/21 DM0716/21012563
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/17/21 DM0717/21012583
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/18/21 DM0718/21012596
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/19/21 DM0719/21012624
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/20/21 DM0720/21012639
25 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/21/21 DM0721/21012760
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/22/21 DM0722/21012775
22 mg/kg D.W. 0.98 3.9 Q2. SW846: 6010C MMSD
07/23/21 DM0723/21013074
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/24/21 DM0724/21013378
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/25/21 DM0725/21013391
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/26/21 DM0726/21013419
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/27/21 DM0727/21013434
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/28/21 DM0728/21013470
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/29/21 DM0729/21013614
20 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/30/21 DM0730/21013629
21 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
07/31/21 DM0731/21013739
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/01/21 DM0801/21013752
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/02/21 DM0802/21013891
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/03/21 DM0803/21013906
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/04/21 DM0804/21013940
25 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/05/21 DM0805/21014673
27 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/06/21 DM0806/21014685
21 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/07/21 DM0807/21014705
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/08/21 DM0809/21014718
22 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
08/09/21 DM0809/21014746
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
08/10/21 DM0810/21014847
29 mg/kg D.W.
0.97 3.9 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/12/21 DM0812/21015285
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/13/21 DM0813/21015297
27 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/14/21 DM0814/21015317
32 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
08/15/21 DM0815/21015330
37 mg/kg D.W.
0.95 3.8
SW846: 6010C MMSD
08/16/21 DM0816/21015410
38 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
08/17/21 DM0817/21015425
36 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
08/18/21 DM0818/21016031
33 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
08/19/21 DM0819/21016046
36 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
08/20/21 DM0820/21016068
42 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/21/21 DM0821/21016088
30 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/22/21 DM0822/21016196
31 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
08/23/21 DM0823/21016224
28 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
Page 53 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FL CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
30 mg/kg D.W.
0.98
3.9
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
27 mg/kg D.W.
0.97 3.9
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
27 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
08/27/21 DM0827/21016407 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/28/21 DM0828/21016427 27 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/30/21 DM0830/21016468 26 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
08/31/21 DM0831/21016483 28 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/01/21 DM0901/21016598 26 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD
09/02/21 DM0902/21016659 24 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/03/21 DM0903/21016671 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/04/21 DM0904/21017055 25 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/05/21 DM0905/21017068 24 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/06/21 DM0906/21017096 26 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/07/21 DM0907/21017306 24 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/08/21 DM0908/21017338 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/09/21 DM0909/21017408 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/10/21 DM0910/21017420 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/11/21 DM0911/21017699 23 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/12/21 DM0912/21017712 23 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/13/21 DM0913/21017740 22 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/14/21 DM0914/21017755 23 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 24 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 27 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 27 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 28 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 26 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 26 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 27 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 27 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD
09/23/21 DM0923/21018564 28 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD
09/24/21 DM0924/21018818 29 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 28 mg/kg D.W. 0.96 3.8 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 28 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 28 mg/kg D.W. 0.96 3.8 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 27 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 25 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 26 mg/kg D.W. 0.96 3.8 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 24 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 25 mg/kg D.W. 0.97 3.8 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 25 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 26 mg/kg D.W. 0.97 3.9
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 26 mg/kg D.W. 0.97 3.8
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 26 mg/kg D.W. 0.96 3.8 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 26 mg/kg D.W. 0.95 3.8 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 35 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD 150655-1
Page 54 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�lE HERE
Milorganite Daily Composite
NICKEL ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
26 mg/kg D.W.
0.97
3.9
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
27 mg/kg D.W.
0.97 3.8
SW846: 6010C
MMSD 150703-1
10/23/21 D M 1023/21020883
26 mg/kg D.W.
0.96 3.8
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 26 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 26 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 26 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 28 mg/kg D.W. 0.98 3.9 D2, Q2. SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 24 mg/kg D.W. 0.97 3.9
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 23 mg/kg D.W. 0.97 3.9
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 23 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 25 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 24 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 25 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720
11/04/21 DM1104/21021735
11/05/21 DM1105/21021747
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150884-1
24 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150884-1
25 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 26 mg/kg D.W. 0.97 3.9 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 25 mg/kg D.W. 0.98 3.9 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 24 mg/kg D.W. 0.99 4
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 24 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 25 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 25 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 26 mg/kg D.W. 0.99 4 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 25 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 26 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 25 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 24 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 24 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 27 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 25 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 25 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 26 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 26 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 28 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 27 mg/kg D.W. 0.99 4
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 29 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 28 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 29 mg/kg D.W. 0.97 3.9
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 28 mg/kg D.W. 0.97 3.9
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 28 mg/kg D.W. 0.97 3.8
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 28 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 27 mg/kg D.W. 0.98 3.9
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 26 mg/kg D.W. 0.99 3.9
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 27 mg/kg D.W. 0.99 4 D2, Q3.
SW846: 6010C
MMSD 151371-1
Page 55 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PAR11181 FP CLER+fR ix�lE HERE
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
26 mg/kg D.W.
0.99
3.9
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
25 mg/kg D.W. 0.99
4
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
26 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 25 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 28 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 26 mg/kg D.W.
0.98 3.9
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 26 mg/kg D.W.
0.97 3.8
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 25 mg/kg D.W.
0.98 3.9
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 26 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 25 mg/kg D.W.
0.98 3.9
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 22 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 23 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 23 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 23 mg/kg D.W. 0.99 4
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 24 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 24 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 23 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 23 mg/kg D.W. 1 4
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 24 mg/kg D.W.
0.98 3.9
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 24 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD 151827-1
Avg Result: 23 mg/kg D.W. Min LOD: 0.95 mg/kg D.W.
Max Result: 42 mg/kg D.W. Max LOD: 1 mg/kg D.W.
Page 56 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�l4[iINEEII
Milorganite Daily Composite
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
28000 mg/kg D.W.
23
89
AO.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
29000 mg/kg D.W. 23 90 AO.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
27000 mg/kg D.W. 23 89 AO.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
01/05/21 DM0105/21000504 27000 mg/kg D.W. 24 90
SW846: 6010C MMSD
01/06/21 DM0106/21000535 27000 mg/kg D.W. 23 89
SW846: 6010C MMSD
01/07/21 DM0107/21000551 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/08/21 DM0108/21000562 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/09/21 DM0109/21000581 28000 mg/kg D.W. 24 91 SW846: 6010C MMSD
01/10/21 DM0110/21000594 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/11/21 DM0111/21000632 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/12/21 DM0112/21000648 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/13/21 DM0113/21000679 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/14/21 DM0114/21000754 28000 mg/kg D.W. 23 88 AO. SW846: 6010C MMSD
01/15/21 DM0115/21000765 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/16/21 DM0116/21000784 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/17/21 DM0117/21000797 27000 mg/kg D.W. 24 90 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/19/21 DM0119/21000842 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/20/21 DM0120/21000926 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/21/21 DM0121/21000942 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/22/21 DM0122/21000953 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/23/21 DM0123/21000972 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/24/21 DM0124/21001059 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/25/21 DM0125/21001088 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/26/21 DM0126/21001106 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/27/21 DM0127/21001137 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
01/28/21 DM0128/21001153 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
01/29/21 DM0129/21001164 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD
01/30/21 DM0130/21001304 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
01/31/21 DM0131/21001317 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/01/21 DM0201/21001344 26000 mg/kg D.W. 23 89 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/03/21 DM0203/21001428 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/04/21 DM0204/21001444 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/05/21 DM0205/21001455 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD
02/06/21 DM0206/21001476 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/07/21 DM0207/21001489 28000 mg/kg D.W. 22 86 SW846: 6010C MMSD
02/08/21 DM0208/21001609 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/09/21 DM0209/21001625 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/10/21 DM0210/21001656 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/11/21 DM0211/21001672 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/12/21 DM0212/21001706 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/13/21 DM0213/21001725 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/14/21 DM0214/21001738 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/15/21 DM0215/21001793 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 57 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�l4[iINEEII
Milorganite Daily Composite
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
26000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
25000 mg/kg D.W. 23 90
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/19/21 DM0219/21001986 25000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/20/21 DM0220/21002005 24000 mg/kg D.W. 23 88
SW846: 6010C MMSD
02/21/21 DM0221/21002072 25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
02/22/21 DM0222/21002230 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/23/21 DM0223/21002246 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/24/21 DM0224/21002281 23000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/25/21 DM0225/21002320 24000 mg/kg D.W. 24 90 SW846: 6010C MMSD
02/26/21 DM0226/21002386 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/27/21 DM0227/21002405 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/28/21 DM0228/21002478 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/01/21 DM0301/21002611 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/02/21 DM0302/21002629 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/03/21 DM0303/21002660 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/04/21 DM0304/21002717 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/05/21 DM0305/21002728 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/06/21 DM0306/21002747 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/07/21 DM0307/21002858 23000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/08/21 DM0308/21003336 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/09/21 DM0309/21003371 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/10/21 DM0310/21003402 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/11/21 DM0311/21003456 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/12/21 DM0312/21003522 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/13/21 DM0313/21003541 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/14/21 DM0314/21003554 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/15/21 DM0315/21003747 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/16/21 DM0316/21003801 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD
03/17/21 DM0317/21003878 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/18/21 DM0318/21003894 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/19/21 DM0319/21003905 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD
03/20/21 DM0320/21004076 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/21/21 DM0321/21004093 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD
03/22/21 DM0322/21004120 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD
03/23/21 DM0323/21004136 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/24/21 DM0324/21004167 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/25/21 DM0325/21004242 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/26/21 DM0326/21004253 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/27/21 DM0327/21004272 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/28/21 DM0328/21004285 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/29/21 DM0329/21004312 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/30/21 DM0330/21004388 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/31/21 DM0331/21004600 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/01/21 DM0401/21004616 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/02/21 DM0402/21004627 24000 mg/kg D.W. 23 90 SW846: 6010C MMSD
Page 58 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�l4[iINEEII
Milorganite Daily Composite
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
23000 mg/kg D.W. 23 88
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
24000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/06/21 DM0406/21004758 27000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/07/21 DM0407/21004843 25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
04/08/21 DM0408/21004861 25000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/09/21 DM0409/21004912 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/10/21 DM0410/21004931 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/11/21 DM0411/21005023 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/12/21 DM0412/21005052 22000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/13/21 DM0413/21005199 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/14/21 DM0414/21005230 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/15/21 DM0415/21005248 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/16/21 DM0416/21005259 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/17/21 DM0417/21005468 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/18/21 DM0418/21005481 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/19/21 DM0419/21005508 24000 mg/kg D.W. 24 90 SW846: 6010C MMSD
04/20/21 DM0420/21005839 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
04/21/21 DM0421/21005870 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/22/21 DM0422/21005981 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/23/21 DM0423/21005992 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/24/21 DM0424/21006057 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/25/21 DM0425/21006272 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/26/21 DM0426/21006299 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/27/21 DM0427/21006315 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/28/21 DM0428/21006346 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/29/21 DM0429/21006362 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/30/21 DM0430/21006373 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/01/21 DM0501/21006429 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/02/21 DM0502/21006442 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/03/21 DM0503/21006676 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/04/21 DM0504/21006691 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/05/21 DM0505/21006722 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/06/21 DM0506/21006781 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/07/21 DM0507/21006834 24000 mg/kg D.W. 23 87 SW846: 6010C MMSD
05/08/21 DM0508/21006981 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/09/21 DM0509/21006994 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/10/21 DM0510/21007021 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/11/21 DM0511/21007171 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/12/21 DM0512/21007202 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/13/21 DM0513/21007217 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/14/21 DM0514/21007309 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/15/21 DM0515/21007328 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/16/21 DM0516/21007341 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/17/21 DM0517/21007382 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/18/21 DM0518/21007440 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 59 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�l4[iINEEII
Milorganite Daily Composite
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
25000 mg/kg D.W. 23 89
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
25000 mg/kg D.W. 23 89
SW846: 6010C MMSD
05/22/21 DM0522/21008072 25000 mg/kg D.W. 24 90
SW846: 6010C MMSD
05/23/21 DM0523/21008085 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
05/25/21 DM0525/21008288 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
05/26/21 DM0526/21008319 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/27/21 DM0527/21008484 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/28/21 DM0528/21008495 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/29/21 DM0529/21008515 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/30/21 DM0530/21008530 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/01/21 DM0601/21008902 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/02/21 DM0602/21008935 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/03/21 DM0603/21008950 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/04/21 DM0604/21009184 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/05/21 DM0605/21009203 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/06/21 DM0606/21009287 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/07/21 DM0607/21009314 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/08/21 DM0608/21009334 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/09/21 DM0609/21009365 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/10/21 DM0610/21009538 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/11/21 DM0611/21009549 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/12/21 DM0612/21009568 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/13/21 DM0613/21009602 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD
06/14/21 DM0614/21009629 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/18/21 DM0618/21009979 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/19/21 DM0619/21010314 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/20/21 DM0620/21010332 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/21/21 DM0621/21010359 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/22/21 DM0622/21010375 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/23/21 DM0623/21010408 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/24/21 DM0624/21010670 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/25/21 DM0625/21010681 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/26/21 DM0626/21010702 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD
06/27/21 DM0627/21010807 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/28/21 DM0628/21010860 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/29/21 DM0629/21010875 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/30/21 DM0630/21011438 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/01/21 DM0701/21011453 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/02/21 DM0702/21011465 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/03/21 DM0703/21011485 24000 mg/kg D.W. 23 88 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/05/21 DM0705/21011572 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/06/21 DM0706/21011693 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/07/21 DM0707/21011727 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/08/21 DM0708/21011742 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 60 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PAR111E11 FP LI.EktERligilpIEW
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
25000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
24000 mg/kg D.W. 23 87
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
24000 mg/kg D.W. 23 87
SW846: 6010C MMSD
07/12/21 DM0712/21012283 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD
07/13/21 DM0713/21012298 27000 mg/kg D.W. 23 87
SW846: 6010C MMSD
07/14/21 DM0714/21012332 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
07/15/21 DM0715/21012390 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/16/21 DM0716/21012563 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/17/21 DM0717/21012583 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/18/21 DM0718/21012596 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/19/21 DM0719/21012624 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/20/21 DM0720/21012639 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/21/21 DM0721/21012760 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/22/21 DM0722/21012775 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/23/21 DM0723/21013074 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/24/21 DM0724/21013378 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/25/21 DM0725/21013391 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/26/21 DM0726/21013419 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/27/21 DM0727/21013434 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/28/21 DM0728/21013470 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/29/21 DM0729/21013614 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/30/21 DM0730/21013629 28000 mg/kg D.W. 23 87 SW846: 6010C MMSD
07/31/21 DM0731/21013739 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/01/21 DM0801/21013752 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/02/21 DM0802/21013891 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/03/21 DM0803/21013906 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/04/21 DM0804/21013940 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/05/21 DM0805/21014673 30000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/06/21 DM0806/21014685 28000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/07/21 DM0807/21014705 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/08/21 DM0809/21014718 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/09/21 DM0809/21014746 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/10/21 DM0810/21014847 26000 mg/kg D.W. 23 88 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/12/21 DM0812/21015285 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/13/21 DM0813/21015297 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/14/21 DM0814/21015317 22000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/15/21 DM0815/21015330 20000 mg/kg D.W. 22 86 SW846: 6010C MMSD
08/16/21 DM0816/21015410 20000 mg/kg D.W. 23 86 SW846: 6010C MMSD
08/17/21 DM0817/21015425 24000 mg/kg D.W. 23 86 SW846: 6010C MMSD
08/18/21 DM0818/21016031 23000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/19/21 DM0819/21016046 23000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/20/21 DM0820/21016068 23000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/21/21 DM0821/21016088 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/22/21 DM0822/21016196 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/23/21 DM0823/21016224 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 61 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PAR111Ell FL CLEktER ix�l4[iINERI
Milorganite Daily Composite
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
25000 mg/kg D.W. 23 88
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
08/27/21 DM0827/21016407 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
08/28/21 DM0828/21016427 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
08/30/21 DM0830/21016468 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD
08/31/21 DM0831/21016483 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/01/21 DM0901/21016598 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD
09/02/21 DM0902/21016659 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/03/21 DM0903/21016671 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
09/04/21 DM0904/21017055 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/05/21 DM0905/21017068 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/06/21 DM0906/21017096 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/07/21 DM0907/21017306 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/08/21 DM0908/21017338 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/09/21 DM0909/21017408 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/10/21 DM0910/21017420 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/11/21 DM0911/21017699 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/12/21 DM0912/21017712 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/13/21 DM0913/21017740 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/14/21 DM0914/21017755 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 24000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 27000 mg/kg D.W. 23 90
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 27000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/23/21 DM0923/21018564 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/24/21 DM0924/21018818 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 27000 mg/kg D.W. 23 87
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 26000 mg/kg D.W. 22 86 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150655-1
Page 62 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FP CLEktER ix�l4[iINEEII
Milorganite Daily Composite
PHOSPHORUS ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
29000 mg/kg D.W. 23 87
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
29000 mg/kg D.W. 23 87
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 29000 mg/kg D.W. 23 88
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 30000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 27000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 26000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 26000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 26000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 25000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 27000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 28000 mg/kg D.W. 23 88 Q3.
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 27000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 28000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 28000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 27000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 27000 mg/kg D.W. 23 90
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 28000 mg/kg D.W. 24 91
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 27000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 28000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151371-1
Page 63 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PAR11181 FP LI.EktERligilpIEW
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
29000 mg/kg D.W.
23
90
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
27000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
27000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 26000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 27000 mg/kg D.W. 24 91
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 27000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 27000 mg/kg D.W. 23 87
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 27000 mg/kg D.W. 23 90
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 27000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 27000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 27000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 27000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 26000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 27000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 27000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 27000 mg/kg D.W. 23 90
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 28000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 28000 mg/kg D.W. 24 91
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 28000 mg/kg D.W. 23 90
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 28000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 29000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 28000 mg/kg D.W. 23 90
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 28000 mg/kg D.W. 23 89
SW846: 6010C
MMSD 151827-1
Avg Result: 26000 mg/kg D.W. Min LOD: 22 mg/kg D.W.
Max Result: 30000 mg/kg D.W. Max LOD: 24 mg/kg D.W.
Page 64 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
3800 mg/kg D.W.
290
860
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
4000 mg/kg D.W. 290 860
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
3600 mg/kg D.W. 290 860 Q2.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 3800 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/05/21 DM0105/21000504 3800 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/06/21 DM0106/21000535 3300 mg/kg D.W. 280 860
SW846: 6010C MMSD
01/07/21 DM0107/21000551 3300 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/08/21 DM0108/21000562 4000 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/09/21 DM0109/21000581 4100 mg/kg D.W. 290 880 SW846: 6010C MMSD
01/10/21 DM0110/21000594 4000 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/11/21 DM0111/21000632 3800 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/12/21 DM0112/21000648 4000 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/13/21 DM0113/21000679 4200 mg/kg D.W. 280 860 SW846: 6010C MMSD
01/14/21 DM0114/21000754
01/15/21 DM0115/21000765
01/16/21 DM0116/21000784
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
3900 mg/kg D.W. 290 860
SW846: 6010C MMSD
3700 mg/kg D.W. 280 860
SW846: 6010C MMSD
01/17/21 DM0117/21000797 3800 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/18/21 DM0118/21000824 3700 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/19/21 DM0119/21000842 4200 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/20/21 DM0120/21000926 4300 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/21/21 DM0121/21000942 4400 mg/kg D.W. 290 860 SW846: 6010C MMSD
01/22/21 DM0122/21000953 3900 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/23/21 DM0123/21000972 3700 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/24/21 DM0124/21001059 4000 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/25/21 DM0125/21001088 4800 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/26/21 DM0126/21001106 4500 mg/kg D.W. 290 870 SW846: 6010C MMSD
01/27/21 DM0127/21001137 4400 mg/kg D.W. 280 850 SW846: 6010C MMSD
01/28/21 DM0128/21001153 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD
01/29/21 DM0129/21001164 4600 mg/kg D.W. 280 840 SW846: 6010C MMSD
01/30/21 DM0130/21001304 4800 mg/kg D.W. 280 850 SW846: 6010C MMSD
01/31/21 DM0131/21001317 4600 mg/kg D.W. 290 860 SW846: 6010C MMSD
02/01/21 DM0201/21001344 3900 mg/kg D.W. 280 860 SW846: 6010C MMSD
02/02/21 DM0202/21001397 3800 mg/kg D.W. 290 860 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 4500 mg/kg D.W. 290 860 SW846: 6010C MMSD
02/04/21 DM0204/21001444 3900 mg/kg D.W. 280 860 SW846: 6010C MMSD
02/05/21 DM0205/21001455 4100 mg/kg D.W. 290 860 SW846: 6010C MMSD
02/06/21 DM0206/21001476 4000 mg/kg D.W. 290 860 SW846: 6010C MMSD
02/07/21 DM0207/21001489 4100 mg/kg D.W. 280 830 SW846: 6010C MMSD
02/08/21 DM0208/21001609 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
02/09/21 DM0209/21001625 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
02/10/21 DM0210/21001656 4800 mg/kg D.W. 280 850 SW846: 6010C MMSD
02/11/21 DM0211/21001672 4700 mg/kg D.W. 280 860 SW846: 6010C MMSD
02/12/21 DM0212/21001706 5300 mg/kg D.W. 290 860 SW846: 6010C MMSD
02/13/21 DM0213/21001725 4600 mg/kg D.W. 280 860 SW846: 6010C MMSD
02/14/21 DM0214/21001738 4400 mg/kg D.W. 280 850 SW846: 6010C MMSD
02/15/21 DM0215/21001793 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD
Page 65 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
4200 mg/kg D.W.
280
860
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
4800 mg/kg D.W. 290 860
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
4800 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/19/21 DM0219/21001986
5300 mg/kg D.W. 280 860
SW846: 6010C MMSD
02/20/21 DM0220/21002005 5400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/21/21 DM0221/21002072 5400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/22/21 DM0222/21002230 5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/23/21 DM0223/21002246
4300 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/24/21 DM0224/21002281
4400 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/25/21 DM0225/21002320 4600 mg/kg D.W. 290 870
SW846: 6010C MMSD
02/26/21 DM0226/21002386 4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/27/21 DM0227/21002405 4200 mg/kg D.W. 280 840
SW846: 6010C MMSD
02/28/21 DM0228/21002478
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/01/21 DM0301/21002611
03/02/21 DM0302/21002629
03/03/21 DM0303/21002660
5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
4700 mg/kg D.W. 280 850
4800 mg/kg D.W. 280 850
SW846: 6010C MMSD
SW846: 6010C MMSD
03/04/21 DM0304/21002717 4700 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/05/21 DM0305/21002728 4900 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/06/21 DM0306/21002747 5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/07/21 DM0307/21002858 4800 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/08/21 DM0308/21003336
4600 mg/kg D.W. 280 860 Q3. SW846: 6010C MMSD
03/09/21 DM0309/21003371 4000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/10/21 DM0310/21003402 3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/11/21 DM0311/21003456 3900 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/12/21 DM0312/21003522 3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/13/21 DM0313/21003541 4800 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/14/21 DM0314/21003554
4700 mg/kg D.W. 280 850 Q2. SW846: 6010C MMSD
03/15/21 DM0315/21003747 4700 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/16/21 DM0316/21003801 4300 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/17/21 DM0317/21003878
4600 mg/kg D.W. 280 850 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 4500 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/19/21 DM0319/21003905 4900 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/20/21 DM0320/21004076 4800 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/21/21 DM0321/21004093
4500 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/22/21 DM0322/21004120
4700 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/23/21 DM0323/21004136 5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/24/21 DM0324/21004167 5000 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/25/21 DM0325/21004242 5200 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/26/21 DM0326/21004253
5100 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/27/21 DM0327/21004272
5000 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/28/21 DM0328/21004285 4900 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/29/21 DM0329/21004312 5000 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/30/21 DM0330/21004388 4600 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/31/21 DM0331/21004600
5100 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/01/21 DM0401/21004616
5000 mg/kg D.W. 290 860 Q3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 4800 mg/kg D.W. 290 860
SW846: 6010C MMSD
Page 66 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
4400 mg/kg D.W.
280
860
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
4200 mg/kg D.W. 280 850
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
4600 mg/kg D.W. 280 860
SW846: 6010C MMSD
04/06/21 DM0406/21004758 4600 mg/kg D.W. 280 860
SW846: 6010C MMSD
04/07/21 DM0407/21004843 4200 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/08/21 DM0408/21004861 4400 mg/kg D.W. 280 860
SW846: 6010C MMSD
04/09/21 DM0409/21004912 4300 mg/kg D.W. 290 860 SW846: 6010C MMSD
04/10/21 DM0410/21004931 4400 mg/kg D.W. 290 860 SW846: 6010C MMSD
04/11/21 DM0411/21005023 4400 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/12/21 DM0412/21005052 4400 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/13/21 DM0413/21005199 4500 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/14/21 DM0414/21005230 4300 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/15/21 DM0415/21005248 4000 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/16/21 DM0416/21005259 4500 mg/kg D.W. 290 860 SW846: 6010C MMSD
04/17/21 DM0417/21005468 4300 mg/kg D.W. 290 860 SW846: 6010C MMSD
04/18/21 DM0418/21005481 4000 mg/kg D.W. 290 860 SW846: 6010C MMSD
04/19/21 DM0419/21005508 4200 mg/kg D.W. 290 870 SW846: 6010C MMSD
04/20/21 DM0420/21005839 4000 mg/kg D.W. 290 870 SW846: 6010C MMSD
04/21/21 DM0421/21005870 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/22/21 DM0422/21005981 4000 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/23/21 DM0423/21005992 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/24/21 DM0424/21006057 3800 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/25/21 DM0425/21006272 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/26/21 DM0426/21006299 3800 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/27/21 DM0427/21006315 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/28/21 DM0428/21006346 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/29/21 DM0429/21006362 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD
04/30/21 DM0430/21006373 4100 mg/kg D.W. 280 840 SW846: 6010C MMSD
05/01/21 DM0501/21006429 4400 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/02/21 DM0502/21006442 4500 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/03/21 DM0503/21006676 4600 mg/kg D.W. 280 860 SW846: 6010C MMSD
05/04/21 DM0504/21006691 4200 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/05/21 DM0505/21006722 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/06/21 DM0506/21006781 4300 mg/kg D.W. 280 860 SW846: 6010C MMSD
05/07/21 DM0507/21006834 3900 mg/kg D.W. 280 840 SW846: 6010C MMSD
05/08/21 DM0508/21006981 4000 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/09/21 DM0509/21006994 4300 mg/kg D.W. 280 860 SW846: 6010C MMSD
05/10/21 DM0510/21007021 3900 mg/kg D.W. 290 860 SW846: 6010C MMSD
05/11/21 DM0511/21007171 4000 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/12/21 DM0512/21007202 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/13/21 DM0513/21007217 3600 mg/kg D.W. 280 860 SW846: 6010C MMSD
05/14/21 DM0514/21007309 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/15/21 DM0515/21007328 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/16/21 DM0516/21007341 3200 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/17/21 DM0517/21007382 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/18/21 DM0518/21007440 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
Page 67 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
3300 mg/kg D.W.
280
850
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
3600 mg/kg D.W. 290 860
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
3300 mg/kg D.W. 290 860
SW846: 6010C MMSD
05/22/21 DM0522/21008072 3400 mg/kg D.W. 290 870
SW846: 6010C MMSD
05/23/21 DM0523/21008085 3700 mg/kg D.W. 280 860
SW846: 6010C MMSD
05/25/21 DM0525/21008288 3300 mg/kg D.W. 280 840
SW846: 6010C MMSD
05/26/21 DM0526/21008319 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/27/21 DM0527/21008484 3300 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/28/21 DM0528/21008495 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/29/21 DM0529/21008515 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
05/30/21 DM0530/21008530 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/01/21 DM0601/21008902 3200 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/02/21 DM0602/21008935 3500 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/03/21 DM0603/21008950 3200 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/04/21 DM0604/21009184 3200 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/05/21 DM0605/21009203 3500 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/06/21 DM0606/21009287 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/07/21 DM0607/21009314 3900 mg/kg D.W. 280 840 SW846: 6010C MMSD
06/08/21 DM0608/21009334 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/09/21 DM0609/21009365 3800 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/10/21 DM0610/21009538 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/11/21 DM0611/21009549 3400 mg/kg D.W. 280 860 SW846: 6010C MMSD
06/12/21 DM0612/21009568 3500 mg/kg D.W. 290 860 SW846: 6010C MMSD
06/13/21 DM0613/21009602 3500 mg/kg D.W. 290 860 SW846: 6010C MMSD
06/14/21 DM0614/21009629 3500 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/18/21 DM0618/21009979 3500 mg/kg D.W. 290 860 SW846: 6010C MMSD
06/19/21 DM0619/21010314 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/20/21 DM0620/21010332 3200 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/21/21 DM0621/21010359 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/22/21 DM0622/21010375 2900 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/23/21 DM0623/21010408 2900 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/24/21 DM0624/21010670 3100 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/25/21 DM0625/21010681 3300 mg/kg D.W. 280 860 SW846: 6010C MMSD
06/26/21 DM0626/21010702 3400 mg/kg D.W. 290 870 SW846: 6010C MMSD
06/27/21 DM0627/21010807 3200 mg/kg D.W. 290 860 SW846: 6010C MMSD
06/28/21 DM0628/21010860 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/29/21 DM0629/21010875 3100 mg/kg D.W. 280 850 SW846: 6010C MMSD
06/30/21 DM0630/21011438 3300 mg/kg D.W. 280 860 SW846: 6010C MMSD
07/01/21 DM0701/21011453 3300 mg/kg D.W. 280 850 SW846: 6010C MMSD
07/02/21 DM0702/21011465 3300 mg/kg D.W. 280 850 SW846: 6010C MMSD
07/03/21 DM0703/21011485 3000 mg/kg D.W. 280 850 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 3000 mg/kg D.W. 280 850 SW846: 6010C MMSD
07/05/21 DM0705/21011572 2900 mg/kg D.W. 280 850 SW846: 6010C MMSD
07/06/21 DM0706/21011693 3000 mg/kg D.W. 280 850 SW846: 6010C MMSD
07/07/21 DM0707/21011727 2800 mg/kg D.W. 280 850 SW846: 6010C MMSD
07/08/21 DM0708/21011742 3000 mg/kg D.W. 280 850 SW846: 6010C MMSD
Page 68 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FP CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
3200 mg/kg D.W.
280
850
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
3100 mg/kg D.W. 280 840
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/12/21 DM0712/21012283
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/13/21 DM0713/21012298 3100 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/14/21 DM0714/21012332 3000 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/15/21 DM0715/21012390 3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/16/21 DM0716/21012563
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/17/21 DM0717/21012583
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/18/21 DM0718/21012596 3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/19/21 DM0719/21012624 3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/20/21 DM0720/21012639 3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/21/21 DM0721/21012760
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/22/21 DM0722/21012775 3400 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/23/21 DM0723/21013074 4200 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/24/21 DM0724/21013378 3800 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/25/21 DM0725/21013391 3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/26/21 DM0726/21013419 3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/27/21 DM0727/21013434 3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/28/21 DM0728/21013470 3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/29/21 DM0729/21013614 3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/30/21 DM0730/21013629 3300 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/31/21 DM0731/21013739 3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/01/21 DM0801/21013752 3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/02/21 DM0802/21013891 3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/03/21 DM0803/21013906 2900 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/04/21 DM0804/21013940 2700 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/05/21 DM0805/21014673 3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/06/21 DM0806/21014685 3100 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/07/21 DM0807/21014705
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/08/21 DM0809/21014718 3100 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/09/21 DM0809/21014746 3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/10/21 DM0810/21014847
3500 mg/kg D.W. 280 850 D2, Q2.
SW846: 6010C MMSD
08/11/21 DM0811/21014867
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/12/21 DM0812/21015285
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/13/21 DM0813/21015297 3500 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/14/21 DM0814/21015317 3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/15/21 DM0815/21015330 2600 mg/kg D.W. 280 830
SW846: 6010C MMSD
08/16/21 DM0816/21015410
2700 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/17/21 DM0817/21015425
2800 mg/kg D.W. 280 830
SW846: 6010C MMSD
08/18/21 DM0818/21016031 2600 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/19/21 DM0819/21016046 2700 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/20/21 DM0820/21016068 2600 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/21/21 DM0821/21016088
3300 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/22/21 DM0822/21016196
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/23/21 DM0823/21016224 3100 mg/kg D.W. 280 840
SW846: 6010C MMSD
Page 69 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
3100 mg/kg D.W.
280
850
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
3300 mg/kg D.W. 280 850
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/27/21 DM0827/21016407 3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/28/21 DM0828/21016427 3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/30/21 DM0830/21016468 3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/31/21 DM0831/21016483 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/01/21 DM0901/21016598 3600 mg/kg D.W. 280 840 SW846: 6010C MMSD
09/02/21 DM0902/21016659 3800 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/03/21 DM0903/21016671 4200 mg/kg D.W. 280 860 SW846: 6010C MMSD
09/04/21 DM0904/21017055 3700 mg/kg D.W. 280 840 SW846: 6010C MMSD
09/05/21 DM0905/21017068 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/06/21 DM0906/21017096 3900 mg/kg D.W. 280 840 SW846: 6010C MMSD
09/07/21 DM0907/21017306 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/08/21 DM0908/21017338 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/09/21 DM0909/21017408 3500 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/10/21 DM0910/21017420 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/11/21 DM0911/21017699 3400 mg/kg D.W. 280 840 SW846: 6010C MMSD
09/12/21 DM0912/21017712 3600 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/13/21 DM0913/21017740 3800 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/14/21 DM0914/21017755 3500 mg/kg D.W. 280 850 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 3400 mg/kg D.W. 280 850
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 3000 mg/kg D.W. 280 860 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 3000 mg/kg D.W. 280 850 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 3000 mg/kg D.W. 290 860 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 3300 mg/kg D.W. 290 860
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 3300 mg/kg D.W. 280 850
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD
09/23/21 DM0923/21018564 4000 mg/kg D.W. 280 840 SW846: 6010C MMSD
09/24/21 DM0924/21018818 3800 mg/kg D.W. 280 840 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 3900 mg/kg D.W. 280 840 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 3800 mg/kg D.W. 280 840 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 4000 mg/kg D.W. 280 840 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 4100 mg/kg D.W. 280 850 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 3600 mg/kg D.W. 280 840 Q2. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 3900 mg/kg D.W. 280 840 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 4200 mg/kg D.W. 280 840 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 4000 mg/kg D.W. 280 840 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 3700 mg/kg D.W. 280 850 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 3100 mg/kg D.W. 280 850
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 3000 mg/kg D.W. 280 840
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 2700 mg/kg D.W. 280 840 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 3100 mg/kg D.W. 280 830 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 3400 mg/kg D.W. 280 850 SW846: 6010C MMSD 150655-1
Page 70 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
POTASSIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
3500 mg/kg D.W.
280
840
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
3800 mg/kg D.W. 280 840
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
4000 mg/kg D.W. 280 840
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 4000 mg/kg D.W. 280 850
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 4300 mg/kg D.W. 280 840 D2, Q2. SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 4200 mg/kg D.W. 280 840
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 3900 mg/kg D.W. 280 850 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 3800 mg/kg D.W. 280 850
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 3800 mg/kg D.W. 280 850
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 3700 mg/kg D.W. 280 850
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 3500 mg/kg D.W. 290 860
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 3800 mg/kg D.W. 290 860
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 4000 mg/kg D.W. 290 860 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720
11/04/21 DM1104/21021735
11/05/21 DM1105/21021747
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD 150884-1
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD 150884-1
3200 mg/kg D.W. 280 840
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 3000 mg/kg D.W. 280 850 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 3200 mg/kg D.W. 280 860 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 3600 mg/kg D.W. 280 860 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 3900 mg/kg D.W. 280 860 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 4000 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 4100 mg/kg D.W. 290 860 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 4300 mg/kg D.W. 290 860 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 4100 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 4100 mg/kg D.W. 290 860 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 3800 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 3400 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 3300 mg/kg D.W. 280 850 Q2, Q3. SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 3500 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 4000 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 4000 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 3700 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 3900 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 3500 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 3300 mg/kg D.W. 280 860
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 3400 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 3300 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 3500 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 3400 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 3400 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 3100 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 3200 mg/kg D.W. 280 840
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 3100 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 3100 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 3400 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 3500 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151371-1
Page 71 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FL CLER+fR ix�lE HERE
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
3600 mg/kg D.W.
290
860
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
3800 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
3700 mg/kg D.W. 290 870 B8.
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 3600 mg/kg D.W. 290 870 B8.
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 3700 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 3800 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 3500 mg/kg D.W. 280 840
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 3200 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 3400 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 3900 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 3800 mg/kg D.W. 280 850
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 3300 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 3000 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621
12/20/21 DM1220/21025649
12/21/21 DM1221/21025664
2900 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151645-1
3300 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151645-2
3200 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 3300 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 3300 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 3300 mg/kg D.W. 290 880
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 3400 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 3500 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 3400 mg/kg D.W. 280 860
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 3700 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 3800 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 3900 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 3900 mg/kg D.W. 290 860
SW846: 6010C
MMSD 151827-1
Avg Result: 3800 mg/kg D.W. Min LOD: 280 mg/kg D.W.
Max Result: 5400 mg/kg D.W. Max LOD: 290 mg/kg D.W.
Page 72 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
4.7 mg/kg D.W.
1.9
7.9
J.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
4.9 mg/kg D.W.
1.9 7.9
J.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
4.2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 4.8 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C MMSD
01/05/21 DM0105/21000504 4 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/06/21 DM0106/21000535 6.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/07/21 DM0107/21000551 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/08/21 DM0108/21000562 3.8 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/09/21 DM0109/21000581 4.2 mg/kg D.W. 1.9 8 J. SW846: 6010C MMSD
01/10/21 DM0110/21000594 3.6 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/11/21 DM0111/21000632 4.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/12/21 DM0112/21000648 2.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/13/21 DM0113/21000679 2.6 mg/kg D.W. 1.9 7.8 J, Q3. SW846: 6010C MMSD
01/14/21 DM0114/21000754 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/15/21 DM0115/21000765 3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/16/21 DM0116/21000784 2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/17/21 DM0117/21000797 < 1.9 mg/kg D.W. 1.9 7.9 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 7 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/19/21 DM0119/21000842 < 1.9 mg/kg D.W. 1.9 7.9 SW846: 6010C MMSD
01/20/21 DM0120/21000926 3.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/21/21 DM0121/21000942 3.5 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/22/21 DM0122/21000953 2 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/23/21 DM0123/21000972 < 1.9 mg/kg D.W. 1.9 7.9 SW846: 6010C MMSD
01/24/21 DM0124/21001059 3 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/25/21 DM0125/21001088 4.8 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/26/21 DM0126/21001106 5.4 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
01/27/21 DM0127/21001137 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/28/21 DM0128/21001153 5.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/29/21 DM0129/21001164 5.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
01/30/21 DM0130/21001304 4.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
01/31/21 DM0131/21001317 5.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/01/21 DM0201/21001344 6.2 mg/kg D.W. 1.9 7.8 D2, J, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 3 mg/kg D.W. 1.9 7.9 D2, J. SW846: 6010C MMSD
02/03/21 DM0203/21001428 5.1 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
02/04/21 DM0204/21001444 5.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/05/21 DM0205/21001455 6.6 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
02/06/21 DM0206/21001476 5.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/07/21 DM0207/21001489 5.3 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD
02/08/21 DM0208/21001609 4.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
02/09/21 DM0209/21001625 5.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/10/21 DM0210/21001656 5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/11/21 DM0211/21001672 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/12/21 DM0212/21001706 4.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/13/21 DM0213/21001725 5.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/14/21 DM0214/21001738 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/15/21 DM0215/21001793 3.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
Page 73 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
4.2 mg/kg D.W.
1.9
7.8
J.
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
5.3 mg/kg D.W.
1.9 7.9
J.
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
4.6 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C MMSD
02/19/21 DM0219/21001986 3.2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C MMSD
02/20/21 DM0220/21002005 2.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
02/21/21 DM0221 /21 002072 3.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
02/22/21 DM0222/21002230 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/23/21 DM0223/21002246 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/24/21 DM0224/21002281 3.1 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
02/25/21 DM0225/21002320 3.5 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
02/26/21 DM0226/21002386 2.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
02/27/21 DM0227/21002405 3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
02/28/21 DM0228/21002478 < 1.9 mg/kg D.W. 1.9 7.8 D2. SW846: 6010C MMSD
03/01/21 DM0301/21002611 5.7 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/02/21 DM0302/21002629 < 1.9 mg/kg D.W. 1.9 7.7 SW846: 6010C MMSD
03/03/21 DM0303/21002660 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/04/21 DM0304/21002717 5.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/05/21 DM0305/21002728 5.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/06/21 DM0306/21002747 6.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/07/21 DM0307/21002858 6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/08/21 DM0308/21003336 6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/09/21 DM0309/21003371 6.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/10/21 DM0310/21003402 3.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/11/21 DM0311/21003456 3.8 mg/kg D.W. 1.9 7.8 J, Q3. SW846: 6010C MMSD
03/12/21 DM0312/21003522 4.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/13/21 DM0313/21003541 5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/14/21 DM0314/21003554 4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/15/21 DM0315/21003747 4.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/16/21 DM0316/21003801 2.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/17/21 DM0317/21003878 3.4 mg/kg D.W. 1.9 7.8 J, Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 6.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/19/21 DM0319/21003905 6.4 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
03/20/21 DM0320/21004076 8.2 mg/kg D.W. 1.9 7.7 SW846: 6010C MMSD
03/21/21 DM0321/21004093 6.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/22/21 DM0322/21004120 5.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
03/23/21 DM0323/21004136 4.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/24/21 DM0324/21004167 4.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/25/21 DM0325/21004242 6.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/26/21 DM0326/21004253 5.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/27/21 DM0327/21004272 5.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/28/21 DM0328/21004285 5.9 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
03/29/21 DM0329/21004312 3.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
03/30/21 DM0330/21004388 4.6 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
03/31/21 DM0331/21004600 5.3 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
04/01/21 DM0401/21004616 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/02/21 DM0402/21004627 3.7 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
Page 74 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
3.5 mg/kg D.W.
1.9
7.8
J.
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
3.2 mg/kg D.W.
1.9 7.7
J.
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
3.2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C MMSD
04/06/21 DM0406/21004758 5.5 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C MMSD
04/07/21 DM0407/21004843 3.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/08/21 DM0408/21004861 4.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/09/21 DM0409/21004912 4.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/10/21 DM0410/21004931 4.5 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
04/11/21 DM0411/21005023 5.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/12/21 DM0412/21005052 3.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/13/21 DM0413/21005199 4.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/14/21 DM0414/21005230 7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/15/21 DM0415/21005248 3.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/16/21 DM0416/21005259 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/17/21 DM0417/21005468 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/18/21 DM0418/21005481 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/19/21 DM0419/21005508 5.4 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
04/20/21 DM0420/21005839 5.2 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
04/21/21 DM0421/21005870 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/22/21 DM0422/21005981 3.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
04/23/21 DM0423/21005992 4.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/24/21 DM0424/21006057 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/25/21 DM0425/21006272 5.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/26/21 DM0426/21006299 3.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
04/27/21 DM0427/21006315 3.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/28/21 DM0428/21006346 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/29/21 DM0429/21006362 4.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
04/30/21 DM0430/21006373 3.7 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/01/21 DM0501/21006429 4.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/02/21 DM0502/21006442 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/03/21 DM0503/21006676 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/04/21 DM0504/21006691 3.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/05/21 DM0505/21006722 3.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/06/21 DM0506/21006781 4.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/07/21 DM0507/21006834 3.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/08/21 DM0508/21006981 4.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/09/21 DM0509/21006994 4.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/10/21 DM0510/21007021 5.3 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
05/11/21 DM0511/21007171 5.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/12/21 DM0512/21007202 4.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/13/21 DM0513/21007217 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/14/21 DM0514/21007309 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/15/21 DM0515/21007328 4.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/16/21 DM0516/21007341 4.7 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/17/21 DM0517/21007382 6.9 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/18/21 DM0518/21007440 5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
Page 75 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
6.4 mg/kg D.W.
1.9
7.7
J.
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
5.7 mg/kg D.W.
1.9 7.8
J.
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
4.8 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C MMSD
05/22/21 DM0522/21008072 3.5 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C MMSD
05/23/21 DM0523/21008085 5.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/25/21 DM0525/21008288 5.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/26/21 DM0526/21008319 5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/27/21 DM0527/21008484 7.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
05/28/21 DM0528/21008495 5.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/29/21 DM0529/21008515 5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
05/30/21 DM0530/21008530 5.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/01/21 DM0601/21008902 5.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
06/02/21 DM0602/21008935 4.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/03/21 DM0603/21008950 6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
06/04/21 DM0604/21009184 5.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
06/05/21 DM0605/21009203 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/06/21 DM0606/21009287 4.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/07/21 DM0607/21009314 5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
06/08/21 DM0608/21009334 6.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/09/21 DM0609/21009365 5.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/10/21 DM0610/21009538 4.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/11/21 DM0611/21009549 5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/12/21 DM0612/21009568 5.8 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
06/13/21 DM0613/21009602 5.8 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
06/14/21 DM0614/21009629 3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/18/21 DM0618/21009979 4.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/19/21 DM0619/21010314 5.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/20/21 DM0620/21010332 4.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/21/21 DM0621/21010359 4.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/22/21 DM0622/21010375 4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
06/23/21 DM0623/21010408 5.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/24/21 DM0624/21010670 6.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/25/21 DM0625/21010681 6.1 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/26/21 DM0626/21010702 5.5 mg/kg D.W. 1.9 8 J. SW846: 6010C MMSD
06/27/21 DM0627/21010807 5.2 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD
06/28/21 DM0628/21010860 6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/29/21 DM0629/21010875 2.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
06/30/21 DM0630/21011438 3.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/01/21 DM0701/21011453 5.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/02/21 DM0702/21011465 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/03/21 DM0703/21011485 2.6 mg/kg D.W. 1.9 7.8 J, T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 3.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/05/21 DM0705/21011572 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/06/21 DM0706/21011693 5.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/07/21 DM0707/21011727 6.7 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/08/21 DM0708/21011742 5.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
Page 76 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FP CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
4.7 mg/kg D.W.
1.9
7.7
J.
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
5.4 mg/kg D.W.
1.9 7.7
J.
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
4.2 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C MMSD
07/12/21 DM0712/21012283 4.2 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C MMSD
07/13/21 DM0713/21012298 4.9 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/14/21 DM0714/21012332 3.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/15/21 DM0715/21012390 5.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/16/21 DM0716/21012563 4.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/17/21 DM0717/21012583 4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/18/21 DM0718/21012596 4.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/19/21 DM0719/21012624 3.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/20/21 DM0720/21012639 5.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/21/21 DM0721/21012760 4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/22/21 DM0722/21012775 3.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/23/21 DM0723/21013074 < 1.9 mg/kg D.W. 1.9 7.8 SW846: 6010C MMSD
07/24/21 DM0724/21013378 3.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/25/21 DM0725/21013391 2.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/26/21 DM0726/21013419 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/27/21 DM0727/21013434 5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/28/21 DM0728/21013470 6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/29/21 DM0729/21013614 2.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
07/30/21 DM0730/21013629 3.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
07/31/21 DM0731/21013739 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/01/21 DM0801/21013752 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/02/21 DM0802/21013891 4.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/03/21 DM0803/21013906 4.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/04/21 DM0804/21013940 6.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/05/21 DM0805/21014673 10 mg/kg D.W. 1.9 7.7 SW846: 6010C MMSD
08/06/21 DM0806/21014685 3.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/07/21 DM0807/21014705 3.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/08/21 DM0809/21014718 2.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/09/21 DM0809/21014746 3.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/10/21 DM0810/21014847 5.1 mg/kg D.W. 1.9 7.8 D2, J, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 3.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/12/21 DM0812/21015285 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/13/21 DM0813/21015297 3.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/14/21 DM0814/21015317 4.1 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD
08/15/21 DM0815/21015330 2.8 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD
08/16/21 DM0816/21015410 3 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD
08/17/21 DM0817/21015425 3.9 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD
08/18/21 DM0818/21016031 3.6 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD
08/19/21 DM0819/21016046 3.4 mg/kg D.W. 1.9 7.6 J. SW846: 6010C MMSD
08/20/21 DM0820/21016068 4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/21/21 DM0821/21016088 3.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/22/21 DM0822/21016196 4.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/23/21 DM0823/21016224 < 1.9 mg/kg D.W. 1.9 7.7 SW846: 6010C MMSD
Page 77 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
3 mg/kg D.W.
1.9
7.8
J.
SW846: 6010C
MMSD
08/25/21
DM0825/21 01 6327
3.7 mg/kg D.W.
1.9 7.7
J.
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
3.4 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C MMSD
08/27/21 DM0827/21016407 3.7 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C MMSD
08/28/21 DM0828/21016427 4.8 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
08/30/21 DM0830/21016468 2.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
08/31/21 DM0831/21016483 6.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/01/21 DM0901/21016598 5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/02/21 DM0902/21016659 3.9 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/03/21 DM0903/21016671 3.5 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/04/21 DM0904/21017055 3.2 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/05/21 DM0905/21017068 3.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/06/21 DM0906/21017096 3.4 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/07/21 DM0907/21017306 3.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/08/21 DM0908/21017338 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/09/21 DM0909/21017408 4.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/10/21 DM0910/21017420 3.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/11/21 DM0911/21017699 4.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/12/21 DM0912/21017712 3.3 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/13/21 DM0913/21017740 < 1.9 mg/kg D.W. 1.9 7.8 SW846: 6010C MMSD
09/14/21 DM0914/21017755 4.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 4.6 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 4.4 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 < 1.9 mg/kg D.W. 1.9 7.8 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 < 1.9 mg/kg D.W. 1.9 7.8 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 < 1.9 mg/kg D.W. 1.9 7.8 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 2.7 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 3.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD
09/23/21 DM0923/21018564 2.3 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD
09/24/21 DM0924/21018818 3.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 4.8 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 4.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 3.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 4.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 4.2 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 4.1 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 4.5 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 3.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 2.8 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 2.5 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 2.3 mg/kg D.W. 1.9 7.6 J. SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 4 mg/kg D.W. 1.8 7.6 J. SW846: 6010C MMSD 150655-1
10/20/21 DM1 020/21 020674 3.6 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150655-1
Page 78 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL CLEktER ix�lE HERE
Milorganite Daily Composite
SELENIUM ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
4.1 mg/kg D.W.
1.9
7.7
J.
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
< 1.9 mg/kg D.W.
1.9 7.7
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
7.3 mg/kg D.W. 1.9 7.6 J.
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034
2 mg/kg D.W.
1.9 7.7
J.
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 < 1.9 mg/kg D.W. 1.9 7.7 D2, Q2. SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 5.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 11 mg/kg D.W. 1.9 7.8 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 3.3 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 3.5 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 3.3 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 3.9 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 3.9 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 4.4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 4 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 3.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 4.8 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 3.9 mg/kg D.W. 1.9 7.7 J. SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 4.2 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 3.9 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 3.7 mg/kg D.W. 1.9 7.8 J. SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 4.2 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 5 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 4.3 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 3.8 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 4.3 mg/kg D.W. 1.9 7.9 J. SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 4.3 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 3.2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 4.4 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 3.5 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 5 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 4.7 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 4.2 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 4.2 mg/kg D.W. 1.9 8 J.
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 5 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 4.4 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 3.7 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 4.2 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 5.1 mg/kg D.W. 1.9 8 J.
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 4.1 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 3.8 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 3.1 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 2.8 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 4.7 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 4.1 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 4.4 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 4.4 mg/kg D.W. 1.9 7.9 D2, J, Q3.
SW846: 6010C
MMSD 151371-1
Page 79 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEE FL CLEktER ix�lE HERE
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
4 mg/kg D.W.
1.9
7.9
J.
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
3 mg/kg D.W.
1.9 7.9
J.
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
4.1 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 3.4 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 4.4 mg/kg D.W. 1.9 8 J.
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 4.3 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 4.2 mg/kg D.W. 1.9 7.7 J.
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 2.7 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 2.8 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 4.6 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 4.4 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 4.5 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 4.6 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 4.1 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 4 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 3.9 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 4.6 mg/kg D.W. 1.9 8 J.
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 4.2 mg/kg D.W. 1.9 8 J.
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 4 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 4.4 mg/kg D.W. 1.9 8 J.
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 5.2 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 4.8 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 4 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 3 mg/kg D.W. 1.9 7.9 J.
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 3.8 mg/kg D.W. 1.9 7.8 J.
SW846: 6010C
MMSD 151827-1
Avg Result: 4.2 mg/kg D.W. Min LOD: 1.8 mg/kg D.W.
Max Result: 11 mg/kg D.W. Max LOD: 1.9 mg/kg D.W.
Page 80 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FP CLER+fR [lulE HEED
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
5.9
0.1
SM 2540 G (1997)
MMSD
01/02/21
DM0102/21000031
6.2 % 0.1
SM 2540 G (1997) MMSD
01/03/21 DM0103/21000076
5.6 % 0.1
SM 2540 G (1997) MMSD
01/04/21 DM0104/21000488
6.1 % 0.1
SM 2540 G (1997) MMSD
01/05/21 DM0105/21000504
6.9 % 0.1
SM 2540 G (1997) MMSD
01/06/21 DM0106/21000535
5.5 % 0.1
SM 2540 G (1997) MMSD
01/07/21 DM0107/21000551 5.7 % 0.1
SM 2540 G (1997) MMSD
01/08/21 DM0108/21000562 6.4 % 0.1
SM 2540 G (1997) MMSD
01/09/21 DM0109/21000581 7.4 % 0.1 SM 2540 G (1997) MMSD
01/10/21 DM0110/21000594
6.8 % 0.1
SM 2540 G (1997) MMSD
01/11/21 DM0111/21000632
5.8 % 0.1
SM 2540 G (1997) MMSD
01/12/21 DM0112/21000648
5.8 % 0.1
SM 2540 G (1997) MMSD
01/13/21 DM0113/21000679 5.5 % 0.1 SM 2540 G (1997) MMSD
01/14/21 DM0114/21000754
01/15/21 DM0115/21000765
01/16/21 DM0116/21000784
5 % 0.1
SM 2540 G (1997) MMSD
5.7 % 0.1
SM 2540 G (1997) MMSD
5.5 % 0.1
SM 2540 G (1997) MMSD
01/17/21 DM0117/21000797 6.4 % 0.1 SM 2540 G (1997) MMSD
01/18/21 DM0118/21000824
6.6 % 0.1
SM 2540 G (1997) MMSD
01/19/21 DM0119/21000842 6.4 % 0.1 SM 2540 G (1997) MMSD
01/20/21 DM0120/21000926
5.6 % 0.1
SM 2540 G (1997) MMSD
01/21/21 DM0121/21000942 6.1 % 0.1 SM 2540 G (1997) MMSD
01/22/21 DM0122/21000953
6.8 % 0.1
SM 2540 G (1997) MMSD
01/23/21 DM0123/21000972 6.5 % 0.1 SM 2540 G (1997) MMSD
01/24/21 DM0124/21001059
6.8 % 0.1
SM 2540 G (1997) MMSD
01/25/21 DM0125/21001088
6.9 % 0.1
SM 2540 G (1997) MMSD
01/26/21 DM0126/21001106 6.6 % 0.1 SM 2540 G (1997) MMSD
01/27/21 DM0127/21001137 5.1 % 0.1 SM 2540 G (1997) MMSD
01/28/21 DM0128/21001153 4.9 % 0.1 SM 2540 G (1997) MMSD
01/29/21 DM0129/21001164
3.5 % 0.1
SM 2540 G (1997) MMSD
01/30/21 DM0130/21001304 4.6 % 0.1 SM 2540 G (1997) MMSD
01/31/21 DM0131/21001317 5.7 % 0.1 SM 2540 G (1997) MMSD
02/01/21 DM0201/21001344 5.4 % 0.1 SM 2540 G (1997) MMSD
02/02/21 DM0202/21001397 6.1 % 0.1 SM 2540 G (1997) MMSD
02/03/21 DM0203/21001428 6 % 0.1 SM 2540 G (1997) MMSD
02/04/21 DM0204/21001444 5.4 % 0.1 SM 2540 G (1997) MMSD
02/05/21 DM0205/21001455
6.2 % 0.1
SM 2540 G (1997) MMSD
02/06/21 DM0206/21001476 5.7 % 0.1 SM 2540 G (1997) MMSD
02/07/21 DM0207/21001489 2.6 % 0.1 SM 2540 G (1997) MMSD
02/08/21 DM0208/21001609 4.5 % 0.1 SM 2540 G (1997) MMSD
02/09/21 DM0209/21001625
5%
0.1
SM 2540 G (1997) MMSD
02/10/21 DM0210/21001656 5.1 % 0.1 SM 2540 G (1997) MMSD
02/11/21 DM0211/21001672
5.6 % 0.1
SM 2540 G (1997) MMSD
02/12/21 DM0212/21001706 5.7 % 0.1 SM 2540 G (1997) MMSD
02/13/21 DM0213/21001725 5.5 % 0.1 SM 2540 G (1997) MMSD
02/14/21 DM0214/21001738
5%
0.1
SM 2540 G (1997) MMSD
02/15/21 DM0215/21001793 5.1 % 0.1 SM 2540 G (1997) MMSD
Page 81 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL fLER+fR [lulE HEED
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
5.3
0.1
SM 2540 G (1997)
MMSD
02/17/21
DM0217/21001872
6.2 % 0.1
SM 2540 G (1997) MMSD
02/18/21 DM0218/21001975
5.9 % 0.1
SM 2540 G (1997) MMSD
02/19/21 DM0219/21001986
5.5 % 0.1
SM 2540 G (1997) MMSD
02/20/21 DM0220/21002005
4.4 % 0.1
SM 2540 G (1997) MMSD
02/21/21 DM0221/21002072 4.5 % 0.1
SM 2540 G (1997) MMSD
02/22/21 DM0222/21002230 4.9 % 0.1
SM 2540 G (1997) MMSD
02/23/21 DM0223/21002246 5.2 % 0.1
SM 2540 G (1997) MMSD
02/24/21 DM0224/21002281 5.9 % 0.1 SM 2540 G (1997) MMSD
02/25/21 DM0225/21002320 6.7 % 0.1 SM 2540 G (1997) MMSD
02/26/21 DM0226/21002386 4.8 % 0.1 SM 2540 G (1997) MMSD
02/27/21 DM0227/21002405 4 % 0.1 SM 2540 G (1997) MMSD
02/28/21 DM0228/21002478 4.6 % 0.1 SM 2540 G (1997) MMSD
03/01/21 DM0301/21002611 4.3 % 0.1 SM 2540 G (1997) MMSD
03/02/21 DM0302/21002629 4.4 % 0.1 SM 2540 G (1997) MMSD
03/03/21 DM0303/21002660 4.5 % 0.1 SM 2540 G (1997) MMSD
03/04/21 DM0304/21002717 5.2 % 0.1 SM 2540 G (1997) MMSD
03/05/21 DM0305/21002728
5%
0.1
SM 2540 G (1997) MMSD
03/06/21 DM0306/21002747 4.3 % 0.1 SM 2540 G (1997) MMSD
03/07/21 DM0307/21002858 5.4 % 0.1 SM 2540 G (1997) MMSD
03/08/21 DM0308/21003336
5.3 % 0.1
SM 2540 G (1997) MMSD
03/09/21 DM0309/21003371 4.6 % 0.1 SM 2540 G (1997) MMSD
03/10/21 DM0310/21003402 4.7 % 0.1 SM 2540 G (1997) MMSD
03/11/21 DM0311/21003456 5.4 % 0.1 SM 2540 G (1997) MMSD
03/12/21 DM0312/21003522 4.4 % 0.1 SM 2540 G (1997) MMSD
03/13/21 DM0313/21003541 4.2 % 0.1 SM 2540 G (1997) MMSD
03/14/21 DM0314/21003554 4.6 % 0.1 SM 2540 G (1997) MMSD
03/15/21 DM0315/21003747 4.3 % 0.1 SM 2540 G (1997) MMSD
03/16/21 DM0316/21003801
3.9 % 0.1
SM 2540 G (1997) MMSD
03/17/21 DM0317/21003878
5%
0.1
SM 2540 G (1997) MMSD
03/18/21 DM0318/21003894 5.3 % 0.1 SM 2540 G (1997) MMSD
03/19/21 DM0319/21003905 6.4 % 0.1 SM 2540 G (1997) MMSD
03/20/21 DM0320/21004076 4.3 % 0.1 SM 2540 G (1997) MMSD
03/21/21 DM0321/21004093 3.9 % 0.1 SM 2540 G (1997) MMSD
03/22/21 DM0322/21004120 4 % 0.1 SM 2540 G (1997) MMSD
03/23/21 DM0323/21004136 4.8 % 0.1 SM 2540 G (1997) MMSD
03/24/21 DM0324/21004167 5.4 % 0.1 SM 2540 G (1997) MMSD
03/25/21 DM0325/21004242 4.9 % 0.1 SM 2540 G (1997) MMSD
03/26/21 DM0326/21004253 5.6 % 0.1 SM 2540 G (1997) MMSD
03/27/21 DM0327/21004272 5.7 % 0.1 SM 2540 G (1997) MMSD
03/28/21 DM0328/21004285 6 % 0.1 SM 2540 G (1997) MMSD
03/29/21 DM0329/21004312
5.8 % 0.1
SM 2540 G (1997) MMSD
03/30/21 DM0330/21004388 5.9 % 0.1 SM 2540 G (1997) MMSD
03/31/21 DM0331/21004600 5.9 % 0.1 SM 2540 G (1997) MMSD
04/01/21 DM0401/21004616 5.8 % 0.1 SM 2540 G (1997) MMSD
04/02/21 DM0402/21004627 6.2 % 0.1 SM 2540 G (1997) MMSD
Page 82 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FP CLER+fR [lulE HEED
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
5.3
0.1
SM 2540 G (1997)
MMSD
04/04/21
DM0404/21004659
4.4 % 0.1
SM 2540 G (1997) MMSD
04/05/21 DM0405/21004742
5.5 % 0.1
SM 2540 G (1997) MMSD
04/06/21 DM0406/21004758
5.3 % 0.1
SM 2540 G (1997) MMSD
04/07/21 DM0407/21004843
5 % 0.1
SM 2540 G (1997) MMSD
04/08/21 DM0408/21004861 5.4 % 0.1
SM 2540 G (1997) MMSD
04/09/21 DM0409/21004912 5.7 % 0.1
SM 2540 G (1997) MMSD
04/10/21 DM0410/21004931 5.9 % 0.1
SM 2540 G (1997) MMSD
04/11/21 DM0411/21005023 5.1 % 0.1 SM 2540 G (1997) MMSD
04/12/21 DM0412/21005052 5.1 % 0.1 SM 2540 G (1997) MMSD
04/13/21 DM0413/21005199
5.3 % 0.1
SM 2540 G (1997) MMSD
04/14/21 DM0414/21005230 5.2 % 0.1 SM 2540 G (1997) MMSD
04/15/21 DM0415/21005248 4.8 % 0.1 SM 2540 G (1997) MMSD
04/16/21 DM0416/21005259
5.7 % 0.1
SM 2540 G (1997) MMSD
04/17/21 DM0417/21005468
5.8 % 0.1
SM 2540 G (1997) MMSD
04/18/21 DM0418/21005481
5.8 % 0.1
SM 2540 G (1997) MMSD
04/19/21 DM0419/21005508 6.8 % 0.1 SM 2540 G (1997) MMSD
04/20/21 DM0420/21005839 6.7 % 0.1 SM 2540 G (1997) MMSD
04/21/21 DM0421/21005870 4.7 % 0.1 SM 2540 G (1997) MMSD
04/22/21 DM0422/21005981 4.5 % 0.1 SM 2540 G (1997) MMSD
04/23/21 DM0423/21005992 4.7 % 0.1 SM 2540 G (1997) MMSD
04/24/21 DM0424/21006057 4.8 % 0.1 SM 2540 G (1997) MMSD
04/25/21 DM0425/21006272 5.1 % 0.1 SM 2540 G (1997) MMSD
04/26/21 DM0426/21006299 4.4 % 0.1 SM 2540 G (1997) MMSD
04/27/21 DM0427/21006315 4.8 % 0.1 SM 2540 G (1997) MMSD
04/28/21 DM0428/21006346
5%
0.1
SM 2540 G (1997) MMSD
04/29/21 DM0429/21006362 4.8 % 0.1 SM 2540 G (1997) MMSD
04/30/21 DM0430/21006373 4.1 % 0.1 SM 2540 G (1997) MMSD
05/01/21 DM0501/21006429 4.7 % 0.1 SM 2540 G (1997) MMSD
05/02/21 DM0502/21006442 4.6 % 0.1 SM 2540 G (1997) MMSD
05/03/21 DM0503/21006676 5.4 % 0.1 SM 2540 G (1997) MMSD
05/04/21 DM0504/21006691 4.4 % 0.1 SM 2540 G (1997) MMSD
05/05/21 DM0505/21006722 4.3 % 0.1 SM 2540 G (1997) MMSD
05/06/21 DM0506/21006781 5.4 % 0.1 SM 2540 G (1997) MMSD
05/07/21 DM0507/21006834 3.6 % 0.1 SM 2540 G (1997) MMSD
05/08/21 DM0508/21006981 5.2 % 0.1 SM 2540 G (1997) MMSD
05/09/21 DM0509/21006994 5.5 % 0.1 SM 2540 G (1997) MMSD
05/10/21 DM0510/21007021 6.1 % 0.1 SM 2540 G (1997) MMSD
05/11/21 DM0511/21007171 5.2 % 0.1 SM 2540 G (1997) MMSD
05/12/21 DM0512/21007202 4.8 % 0.1 SM 2540 G (1997) MMSD
05/13/21 DM0513/21007217 5.4 % 0.1 SM 2540 G (1997) MMSD
05/14/21 DM0514/21007309 4.9 % 0.1 SM 2540 G (1997) MMSD
05/15/21 DM0515/21007328 4.5 % 0.1 SM 2540 G (1997) MMSD
05/16/21 DM0516/21007341 4.3 % 0.1 SM 2540 G (1997) MMSD
05/17/21 DM0517/21007382 4.3 % 0.1 SM 2540 G (1997) MMSD
05/18/21 DM0518/21007440 5 % 0.1 SM 2540 G (1997) MMSD
Page 83 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL fLER+fR [lulE HEED
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
4.5
0.1
SM 2540 G (1997)
MMSD
05/20/21
DM0520/21007969
5.8 % 0.1
SM 2540 G (1997) MMSD
05/21/21 DM0521/21007980
6% 0.1
SM 2540 G (1997) MMSD
05/22/21 DM0522/21008072
6.6 % 0.1
SM 2540 G (1997) MMSD
05/23/21 DM0523/21008085
5.3 % 0.1
SM 2540 G (1997) MMSD
05/25/21 DM0525/21008288 4.2 % 0.1
SM 2540 G (1997) MMSD
05/26/21 DM0526/21008319 4.6 % 0.1
SM 2540 G (1997) MMSD
05/27/21 DM0527/21008484 4.4 % 0.1
SM 2540 G (1997) MMSD
05/28/21 DM0528/21008495 5.1 % 0.1 SM 2540 G (1997) MMSD
05/29/21 DM0529/21008515 5.1 % 0.1 SM 2540 G (1997) MMSD
05/30/21 DM0530/21008530
5%
0.1
SM 2540 G (1997) MMSD
06/01/21 DM0601/21008902 4.3 % 0.1 SM 2540 G (1997) MMSD
06/02/21 DM0602/21008935 4.8 % 0.1 SM 2540 G (1997) MMSD
06/03/21 DM0603/21008950 4.4 % 0.1 SM 2540 G (1997) MMSD
06/04/21 DM0604/21009184 4.3 % 0.1 SM 2540 G (1997) MMSD
06/05/21 DM0605/21009203 4.8 % 0.1 SM 2540 G (1997) MMSD
06/06/21 DM0606/21009287 4.7 % 0.1 SM 2540 G (1997) MMSD
06/07/21 DM0607/21009314 4.1 % 0.1 SM 2540 G (1997) MMSD
06/08/21 DM0608/21009334 4.6 % 0.1 SM 2540 G (1997) MMSD
06/09/21 DM0609/21009365 5.2 % 0.1 SM 2540 G (1997) MMSD
06/10/21 DM0610/21009538 5.2 % 0.1 SM 2540 G (1997) MMSD
06/11/21 DM0611/21009549 5.4 % 0.1 SM 2540 G (1997) MMSD
06/12/21 DM0612/21009568 6 % 0.1 SM 2540 G (1997) MMSD
06/13/21 DM0613/21009602 6.2 % 0.1 SM 2540 G (1997) MMSD
06/14/21 DM0614/21009629 4.7 % 0.1 SM 2540 G (1997) MMSD
06/18/21 DM0618/21009979 5.8 % 0.1 SM 2540 G (1997) MMSD
06/19/21 DM0619/21010314 4.6 % 0.1 SM 2540 G (1997) MMSD
06/20/21 DM0620/21010332 4.7 % 0.1 SM 2540 G (1997) MMSD
06/21/21 DM0621/21010359 4.9 % 0.1 SM 2540 G (1997) MMSD
06/22/21 DM0622/21010375 4.3 % 0.1 SM 2540 G (1997) MMSD
06/23/21 DM0623/21010408 4.6 % 0.1 SM 2540 G (1997) MMSD
06/24/21 DM0624/21010670 5.1 % 0.1 SM 2540 G (1997) MMSD
06/25/21 DM0625/21010681 5.6 % 0.1 SM 2540 G (1997) MMSD
06/26/21 DM0626/21010702 7.1 % 0.1 SM 2540 G (1997) MMSD
06/27/21 DM0627/21010807 6 % 0.1 SM 2540 G (1997) MMSD
06/28/21 DM0628/21010860 5.2 % 0.1 SM 2540 G (1997) MMSD
06/29/21 DM0629/21010875 4.9 % 0.1 SM 2540 G (1997) MMSD
06/30/21 DM0630/21011438
5.5 % 0.1
SM 2540 G (1997) MMSD
07/01/21 DM0701/21011453 4.8 % 0.1 SM 2540 G (1997) MMSD
07/02/21 DM0702/21011465 4.6 % 0.1 SM 2540 G (1997) MMSD
07/03/21 DM0703/21011485 5 % 0.1 T9. SM 2540 G (1997) MMSD
07/04/21 DM0704/21011516 4.8 % 0.1 SM 2540 G (1997) MMSD
07/05/21 DM0705/21011572 4.9 % 0.1 SM 2540 G (1997) MMSD
07/06/21 DM0706/21011693 4.6 % 0.1 SM 2540 G (1997) MMSD
07/07/21 DM0707/21011727 4.4 % 0.1 SM 2540 G (1997) MMSD
07/08/21 DM0708/21011742 4.7 % 0.1 SM 2540 G (1997) MMSD
Page 84 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FP LER+fR [lulE HEED
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
4.3
0.1
SM 2540 G (1997)
MMSD
07/10/21
DM0710/21012238
3.9 % 0.1
SM 2540 G (1997) MMSD
07/11/21 DM0711/21012255
3.6 % 0.1
SM 2540 G (1997) MMSD
07/12/21 DM0712/21012283
3.8 % 0.1
SM 2540 G (1997) MMSD
07/13/21 DM0713/21012298
3.7 % 0.1
SM 2540 G (1997) MMSD
07/14/21 DM0714/21012332 4.2 % 0.1
SM 2540 G (1997) MMSD
07/15/21 DM0715/21012390 4.5 % 0.1
SM 2540 G (1997) MMSD
07/16/21 DM0716/21012563 4.4 % 0.1
SM 2540 G (1997) MMSD
07/17/21 DM0717/21012583 4.9 % 0.1 SM 2540 G (1997) MMSD
07/18/21 DM0718/21012596 4.3 % 0.1 SM 2540 G (1997) MMSD
07/19/21 DM0719/21012624 4.6 % 0.1 SM 2540 G (1997) MMSD
07/20/21 DM0720/21012639 4.4 % 0.1 SM 2540 G (1997) MMSD
07/21/21 DM0721/21012760 4.8 % 0.1 SM 2540 G (1997) MMSD
07/22/21 DM0722/21012775 5.6 % 0.1 SM 2540 G (1997) MMSD
07/23/21 DM0723/21013074 5.6 % 0.1 SM 2540 G (1997) MMSD
07/24/21 DM0724/21013378 5.4 % 0.1 SM 2540 G (1997) MMSD
07/25/21 DM0725/21013391 4.8 % 0.1 SM 2540 G (1997) MMSD
07/26/21 DM0726/21013419
5%
0.1
SM 2540 G (1997) MMSD
07/27/21 DM0727/21013434 4.8 % 0.1 SM 2540 G (1997) MMSD
07/28/21 DM0728/21013470 4.2 % 0.1 SM 2540 G (1997) MMSD
07/29/21 DM0729/21013614 4.6 % 0.1 SM 2540 G (1997) MMSD
07/30/21 DM0730/21013629
3.6 % 0.1
SM 2540 G (1997) MMSD
07/31/21 DM0731/21013739
5%
0.1
SM 2540 G (1997) MMSD
08/01/21 DM0801/21013752 5 % 0.1 SM 2540 G (1997) MMSD
08/02/21 DM0802/21013891 4.9 % 0.1 SM 2540 G (1997) MMSD
08/03/21 DM0803/21013906 4.1 % 0.1 SM 2540 G (1997) MMSD
08/04/21 DM0804/21013940 4 % 0.1 SM 2540 G (1997) MMSD
08/05/21 DM0805/21014673 4.1 % 0.1 SM 2540 G (1997) MMSD
08/06/21 DM0806/21014685
3.9 % 0.1
SM 2540 G (1997) MMSD
08/07/21 DM0807/21014705 4.7 % 0.1 SM 2540 G (1997) MMSD
08/08/21 DM0809/21014718 4.3 % 0.1 SM 2540 G (1997) MMSD
08/09/21 DM0809/21014746 4.2 % 0.1 SM 2540 G (1997) MMSD
08/10/21 DM0810/21014847 4.5 % 0.1 SM 2540 G (1997) MMSD
08/11/21 DM0811/21014867
5%
0.1
SM 2540 G (1997) MMSD
08/12/21 DM0812/21015285
5%
0.1
SM 2540 G (1997) MMSD
08/13/21 DM0813/21015297 4.1 % 0.1 SM 2540 G (1997) MMSD
08/14/21 DM0814/21015317
3.2 % 0.1
SM 2540 G (1997) MMSD
08/15/21 DM0815/21015330 2.5 % 0.1 SM 2540 G (1997) MMSD
08/16/21 DM0816/21015410
3%
0.1
SM 2540 G (1997) MMSD
08/17/21 DM0817/21015425 2.8 % 0.1 SM 2540 G (1997) MMSD
08/18/21 DM0818/21016031 3.1 % 0.1 SM 2540 G (1997) MMSD
08/19/21 DM0819/21016046
3.3 % 0.1
SM 2540 G (1997) MMSD
08/20/21 DM0820/21016068 3.8 % 0.1
Dl.
SM 2540 G (1997) MMSD
08/21/21 DM0821/21016088 4 % 0.1 SM 2540 G (1997) MMSD
08/22/21 DM0822/21016196 4.3 % 0.1 SM 2540 G (1997) MMSD
08/23/21 DM0823/21016224 4.2 % 0.1 SM 2540 G (1997) MMSD
Page 85 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL fLER+fR [lulE HEED
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
4.7
0.1
SM 2540 G (1997)
MMSD
08/25/21
DM0825/21016327
4.4 % 0.1
SM 2540 G (1997) MMSD
08/26/21 DM0826/21016342
4.5 % 0.1
SM 2540 G (1997) MMSD
08/27/21 DM0827/21016407
4.8 % 0.1
SM 2540 G (1997) MMSD
08/28/21 DM0828/21016427
4.8 % 0.1
SM 2540 G (1997) MMSD
08/30/21 DM0830/21016468
3.8 % 0.1
SM 2540 G (1997) MMSD
08/31/21 DM0831/21016483 4.5 % 0.1
SM 2540 G (1997) MMSD
09/01/21 DM0901/21016598 4 % 0.1
SM 2540 G (1997) MMSD
09/02/21 DM0902/21016659 4.3 % 0.1 SM 2540 G (1997) MMSD
09/03/21 DM0903/21016671
5.3 % 0.1
SM 2540 G (1997) MMSD
09/04/21 DM0904/21017055 4.2 % 0.1 SM 2540 G (1997) MMSD
09/05/21 DM0905/21017068 4.7 % 0.1 SM 2540 G (1997) MMSD
09/06/21 DM0906/21017096 4.2 % 0.1 SM 2540 G (1997) MMSD
09/07/21 DM0907/21017306 4.4 % 0.1 SM 2540 G (1997) MMSD
09/08/21 DM0908/21017338 4.8 % 0.1 SM 2540 G (1997) MMSD
09/09/21 DM0909/21017408 4.8 % 0.1 SM 2540 G (1997) MMSD
09/10/21 DM0910/21017420 4.8 % 0.1 SM 2540 G (1997) MMSD
09/11/21 DM0911/21017699 4.2 % 0.1 SM 2540 G (1997) MMSD
09/12/21 DM0912/21017712 5.1 % 0.1 SM 2540 G (1997) MMSD 149896-1
09/13/21 DM0913/21017740 4.8 % 0.1 SM 2540 G (1997) MMSD 149920-1
09/14/21 DM0914/21017755 4.6 % 0.1 SM 2540 G (1997) MMSD 149947-1
09/15/21 DM0915/21017903 4.7 % 0.1 SM 2540 G (1997) MMSD 149977-1
09/16/21 DM0916/21018023 5.1 % 0.1 SM 2540 G (1997) MMSD 150004-1
09/17/21 DM0917/21018105 5.4 % 0.1
SM 2540 G (1997)
MMSD 150018-1
09/18/21 DM0918/21018125 5.2 % 0.1
SM 2540 G (1997)
MMSD 150021-1
09/19/21 DM0919/21018138 5.7 % 0.1 SM 2540 G (1997) MMSD 150039-1
09/20/21 DM0920/21018236
6.3 % 0.1
SM 2540 G (1997) MMSD 150063-1
09/21/21 DM0921/21018251 4.9 % 0.1 SM 2540 G (1997) MMSD 150084-1
09/22/21 DM0922/21018480 4.7 % 0.1
SM 2540 G (1997)
MMSD 150117-1
09/23/21 DM0923/21018564 4.2 % 0.1
SM 2540 G (1997)
MMSD 150139-1
09/24/21 DM0924/21018818 3.8 % 0.1 SM 2540 G (1997) MMSD 150152-1
09/25/21 DM0925/21018838 3.1 % 0.1
SM 2540 G (1997)
MMSD 150156-1
09/26/21 DM0926/21019023 4 % 0.1
SM 2540 G (1997)
MMSD 150169-1
09/27/21 DM0927/21019051 3.6 % 0.1
SM 2540 G (1997)
MMSD 150190-1
09/28/21 DM0928/21019066 4.4 % 0.1 SM 2540 G (1997) MMSD 150208-1
09/29/21 DM0929/21019228 4 % 0.1 SM 2540 G (1997) MMSD 150224-1
09/30/21 DM0930/21019243 3.7 % 0.1 SM 2540 G (1997) MMSD 150254-1
10/01/21 DM1001/21019255 4.2 % 0.1 SM 2540 G (1997) MMSD 150269-1
10/02/21 DM1002/21019384 3.9 % 0.1 SM 2540 G (1997) MMSD 150272-1
10/03/21 DM1003/21019397 4.3 % 0.1 SM 2540 G (1997) MMSD 150294-1
10/04/21 DM1004/21019425 4.8 % 0.1 SM 2540 G (1997) MMSD 150320-1
10/06/21 DM1006/21019735 4.4 % 0.1 SM 2540 G (1997) MMSD 150369-1
10/07/21 DM1007/21019760 4 % 0.1
SM 2540 G (1997)
MMSD 150391-1
10/08/21 DM1008/21019772 3.4 % 0.1 SM 2540 G (1997) MMSD 150419-1
10/19/21 DM1019/21020600 2.6 % 0.1 SM 2540 G (1997) MMSD 150592-1
10/20/21 DM1020/21020674 4.5 % 0.1
SM 2540 G (1997)
MMSD 150617-1
Page 86 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
4.2 %
0.1
SM 2540 G (1997)
MMSD
150638-1
10/22/21
DM1022/21020701
3.9 % 0.1
SM 2540 G (1997) MMSD 150659-1
10/23/21 D M 1023/21020883
3.3 % 0.1
SM 2540 G (1997) MMSD 150663-1
10/24/21 DM1024/21021034
4.3 % 0.1
SM 2540 G (1997) MMSD 150673-1
10/25/21 DM1025/21021062
4 % 0.1
SM 2540 G (1997) MMSD 150694-1
10/26/21 DM1026/21021077
3.8 % 0.1
SM 2540 G (1997)
MMSD 150716-1
10/27/21 DM1027/21021161 4.7 % 0.1
SM 2540 G (1997) MMSD 150745-1
10/28/21 DM1028/21021226 4.4 % 0.1
SM 2540 G (1997) MMSD 150773-1
10/29/21 DM1029/21021510 4.6 % 0.1 SM 2540 G (1997) MMSD 150780-1
10/30/21 DM1030/21021530 5.1 % 0.1 SM 2540 G (1997) MMSD 150784-1
10/31/21 DM1031/21021574
5.9 % 0.1
SM 2540 G (1997) MMSD 150796-1
11/01/21 DM1101/21021608 6 % 0.1
SM 2540 G (1997)
MMSD 150815-1
11/02/21 DM1102/21021623 5.8 % 0.1 SM 2540 G (1997) MMSD 150838-1
11/03/21 DM1103/21021720 4.7 % 0.1 SM 2540 G (1997) MMSD 150856-1
11/04/21 DM1104/21021735 4.1 % 0.1 SM 2540 G (1997) MMSD 150870-1
11/05/21 DM1105/21021747 3.6 % 0.1 SM 2540 G (1997) MMSD 150888-1
11/06/21 DM1106/21021767 4.4 % 0.1
SM 2540 G (1997)
MMSD 150891-1
11/07/21 DM1107/21022553 5.4 % 0.1 SM 2540 G (1997) MMSD 150902-1
11/08/21 DM1108/21022581 5.4 % 0.1 SM 2540 G (1997) MMSD 150923-1
11/09/21 DM1109/21022596 5.4 % 0.1 SM 2540 G (1997) MMSD 150940-1
11/10/21 DM1110/21022680 6.4 % 0.1 SM 2540 G (1997) MMSD 150969-1
11/11/21 DM1111/21022695 6.1 % 0.1 SM 2540 G (1997) MMSD 150977-1
11/12/21 DM1112/21022707
6.2 % 0.1
SM 2540 G (1997) MMSD 150989-1
11/13/21 DM1113/21022731 5 % 0.1 SM 2540 G (1997) MMSD 150992-1
11/14/21 DM1114/21022744 6.4 % 0.1
SM 2540 G (1997)
MMSD 151002-1
11/15/21 DM1115/21022772 5.6 % 0.1
SM 2540 G (1997)
MMSD 151022-1
11/16/21 DM1116/21022787 4.7 % 0.1
SM 2540 G (1997)
MMSD 151055-1
11/17/21 DM1117/21023039 4.9 % 0.1
SM 2540 G (1997)
MMSD 151076-1
11/18/21 DM1118/21023056 4.7 % 0.1
SM 2540 G (1997)
MMSD 151100-1
11/19/21 DM1119/21023181 5.2 % 0.1
SM 2540 G (1997)
MMSD 151125-1
11/20/21 DM1120/21023201 5.8 % 0.1
SM 2540 G (1997)
MMSD 151128-1
11/21/21 DM1121/21023214 6.5 % 0.1
SM 2540 G (1997)
MMSD 151138-1
11/22/21 DM1122/21023555 7.2 % 0.1
SM 2540 G (1997)
MMSD 151157-1
11/23/21 DM1123/21023570 5.7 % 0.1
SM 2540 G (1997)
MMSD 151179-1
11/24/21 DM1124/21023611 5.3 % 0.1
SM 2540 G (1997)
MMSD 151203-1
11/25/21 DM1125/21023795 6 % 0.1
SM 2540 G (1997)
MMSD 151207-1
11/26/21 DM1126/21023807 6.4 % 0.1
SM 2540 G (1997)
MMSD 151211-1
11/27/21 DM1127/21023827 7.3 % 0.1
SM 2540 G (1997)
MMSD 151215-1
11/28/21 DM1128/21023899 5.7 % 0.1
SM 2540 G (1997)
MMSD 151230-1
11/29/21 DM1129/21023927 4.4 % 0.1
SM 2540 G (1997)
MMSD 151260-1
11/30/21 DM1130/21024167 4.5 % 0.1
SM 2540 G (1997)
MMSD 151277-1
12/01/21 DM1201/21024282 4.1 % 0.1
SM 2540 G (1997)
MMSD 151301-1
12/02/21 DM1202/21024297 4.7 % 0.1
SM 2540 G (1997)
MMSD 151324-1
12/03/21 DM1203/21024309 4.7 % 0.1
SM 2540 G (1997)
MMSD 151349-1
12/04/21 DM1204/21024329 5.9 % 0.1
SM 2540 G (1997)
MMSD 151354-1
12/05/21 DM1205/21024739 6.5 % 0.1 SM 2540 G (1997)
MMSD 151365-1
Page 87 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
6.3
0.1
SM 2540 G (1997)
MMSD
151383-1
12/07/21
DM1207/21024782
6.5 % 0.1
SM 2540 G (1997)
MMSD 151405-1
12/08/21 DM1208/21024816
6.6 % 0.1
SM 2540 G (1997)
MMSD 151439-1
12/09/21 DM1209/21024832
6.9 % 0.1
SM 2540 G (1997)
MMSD 151455-1
12/10/21 DM1210/21024844
7.4 % 0.1
SM 2540 G (1997)
MMSD 151474-1
12/11/21 DM1211/21024864 4.6 % 0.1
SM 2540 G (1997)
MMSD 151477-1
12/12/21 DM1212/21025174
3.8 % 0.1
SM 2540 G (1997)
MMSD 151485-1
12/13/21 DM1213/21025205 6.3 % 0.1
SM 2540 G (1997)
MMSD 151511-1
12/14/21 DM1214/21025220
5%
0.1
SM 2540 G (1997)
MMSD 151536-1
12/15/21 DM1215/21025299 5.7 % 0.1
SM 2540 G (1997)
MMSD 151564-1
12/16/21 DM1216/21025314 5.1 % 0.1
SM 2540 G (1997)
MMSD 151581-1
12/17/21 DM1217/21025326 6.1 % 0.1
SM 2540 G (1997)
MMSD 151588-1
12/18/21 DM1219/21025346 5.9 % 0.1
SM 2540 G (1997)
MMSD 151591-1
12/19/21 DM1219/21025621 6.8 % 0.1 SM 2540 G (1997)
MMSD 151597-1
12/20/21 DM1220/21025649 6.6 % 0.1 SM 2540 G (1997)
MMSD 151628-1
12/21/21 DM1221/21025664
6.7 % 0.1
SM 2540 G (1997)
MMSD 151655-1
12/22/21 DM1222/21025700 6.4 % 0.1
SM 2540 G (1997)
MMSD 151675-1
12/23/21 DM1223/21025779
7%
0.1
SM 2540 G (1997)
MMSD 151688-1
12/24/21 DM1224/21025791 7.5 % 0.1
SM 2540 G (1997)
MMSD 151691-1
12/25/21 DM1225/21025811 6.2 % 0.1
SM 2540 G (1997)
MMSD 151693-1
12/26/21 DM1226/21025824
7%
0.1
SM 2540 G (1997)
MMSD 151698-1
12/27/21 DM1227/21025917 5.3 % 0.1
SM 2540 G (1997)
MMSD 151706-1
12/28/21 DM1228/21025932 5.8 % 0.1
SM 2540 G (1997)
MMSD 151727-1
12/29/21 DM1229/21025966 6.2 % 0.1
SM 2540 G (1997)
MMSD 151747-1
12/30/21 DM1230/21025981 5.9 % 0.1 SM 2540 G (1997)
MMSD 151755-1
12/31/21 DM1231/21026033 5.8 % 0.1
SM 2540 G (1997)
MMSD 151758-1
Avg Result: 5 % Min LOD: 0.1 0/0
Max Result: 7.5 % Max LOD: 0.1 0/0
Page 88 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
320 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
330 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
310 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/04/21 DM0104/21000488 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/05/21 DM0105/21000504 330 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/06/21 DM0106/21000535 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/07/21 DM0107/21000551 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/08/21 DM0108/21000562 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/09/21 DM0109/21000581 340 mg/kg D.W. 4.9 15 SW846: 6010C MMSD
01/10/21 DM0110/21000594 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/11/21 DM0111/21000632 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/12/21 DM0112/21000648 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/13/21 DM0113/21000679 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/14/21 DM0114/21000754 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/15/21 DM0115/21000765 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/16/21 DM0116/21000784 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/17/21 DM0117/21000797 350 mg/kg D.W. 4.8 15 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/19/21 DM0119/21000842 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/20/21 DM0120/21000926 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/21/21 DM0121/21000942 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/22/21 DM0122/21000953 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/23/21 DM0123/21000972 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/24/21 DM0124/21001059 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/25/21 DM0125/21001088 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/26/21 DM0126/21001106 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/27/21 DM0127/21001137 310 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/28/21 DM0128/21001153 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/29/21 DM0129/21001164 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
01/30/21 DM0130/21001304 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/31/21 DM0131/21001317 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/01/21 DM0201/21001344 340 mg/kg D.W. 4.8 15 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 370 mg/kg D.W. 4.8 15 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/04/21 DM0204/21001444 380 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/05/21 DM0205/21001455 370 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/06/21 DM0206/21001476 370 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/07/21 DM0207/21001489 370 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
02/08/21 DM0208/21001609 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/09/21 DM0209/21001625 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/10/21 DM0210/21001656 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/11/21 DM0211/21001672 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/12/21 DM0212/21001706 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/13/21 DM0213/21001725 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/14/21 DM0214/21001738 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/15/21 DM0215/21001793 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 89 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
330 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
320 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/19/21 DM0219/21001986 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/20/21 DM0220/21002005 310 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
02/21/21 DM0221/21002072 310 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
02/22/21 DM0222/21002230 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/23/21 DM0223/21002246 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/24/21 DM0224/21002281 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/25/21 DM0225/21002320 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/26/21 DM0226/21002386 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/27/21 DM0227/21002405 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
02/28/21 DM0228/21002478 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/01/21 DM0301/21002611 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/02/21 DM0302/21002629 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/03/21 DM0303/21002660 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/04/21 DM0304/21002717 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/05/21 DM0305/21002728 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/06/21 DM0306/21002747 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/07/21 DM0307/21002858 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/08/21 DM0308/21003336 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/09/21 DM0309/21003371 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/10/21 DM0310/21003402 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/11/21 DM0311/21003456 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/12/21 DM0312/21003522 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/13/21 DM0313/21003541 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/14/21 DM0314/21003554 310 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/15/21 DM0315/21003747 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/16/21 DM0316/21003801 370 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
03/17/21 DM0317/21003878 380 mg/kg D.W. 4.7 15 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/19/21 DM0319/21003905 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/20/21 DM0320/21004076 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/21/21 DM0321/21004093 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
03/22/21 DM0322/21004120 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
03/23/21 DM0323/21004136 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/24/21 DM0324/21004167 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/25/21 DM0325/21004242 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/26/21 DM0326/21004253 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/27/21 DM0327/21004272 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/28/21 DM0328/21004285 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/29/21 DM0329/21004312 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/30/21 DM0330/21004388 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/31/21 DM0331/21004600 300 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/01/21 DM0401/21004616 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/02/21 DM0402/21004627 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
Page 90 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
370 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
340 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
350 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/06/21 DM0406/21004758 360 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/07/21 DM0407/21004843 370 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
04/08/21 DM0408/21004861 340 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/09/21 DM0409/21004912 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/10/21 DM0410/21004931 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/11/21 DM0411/21005023 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/12/21 DM0412/21005052 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/13/21 DM0413/21005199 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/14/21 DM0414/21005230 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/15/21 DM0415/21005248 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/16/21 DM0416/21005259 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/17/21 DM0417/21005468 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/18/21 DM0418/21005481 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/19/21 DM0419/21005508 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/20/21 DM0420/21005839 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/21/21 DM0421/21005870 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/22/21 DM0422/21005981 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/23/21 DM0423/21005992 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/24/21 DM0424/21006057 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/25/21 DM0425/21006272 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/26/21 DM0426/21006299 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/27/21 DM0427/21006315 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/28/21 DM0428/21006346 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/29/21 DM0429/21006362 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/30/21 DM0430/21006373 330 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
05/01/21 DM0501/21006429 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/02/21 DM0502/21006442 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/03/21 DM0503/21006676 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/04/21 DM0504/21006691 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/05/21 DM0505/21006722 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/06/21 DM0506/21006781 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/07/21 DM0507/21006834 380 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
05/08/21 DM0508/21006981 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/09/21 DM0509/21006994 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/10/21 DM0510/21007021 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/11/21 DM0511/21007171 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/12/21 DM0512/21007202 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/13/21 DM0513/21007217 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/14/21 DM0514/21007309 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/15/21 DM0515/21007328 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/16/21 DM0516/21007341 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/17/21 DM0517/21007382 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/18/21 DM0518/21007440 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 91 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
370 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
360 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
370 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
05/22/21 DM0522/21008072 360 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
05/23/21 DM0523/21008085 360 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
05/25/21 DM0525/21008288 380 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
05/26/21 DM0526/21008319 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/27/21 DM0527/21008484 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/28/21 DM0528/21008495 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/29/21 DM0529/21008515 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/30/21 DM0530/21008530 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/01/21 DM0601/21008902 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/02/21 DM0602/21008935 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/03/21 DM0603/21008950 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/04/21 DM0604/21009184 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/05/21 DM0605/21009203 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/06/21 DM0606/21009287 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/07/21 DM0607/21009314 450 mg/kg D.W. 4.7 14 Q3. SW846: 6010C MMSD
06/08/21 DM0608/21009334 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/09/21 DM0609/21009365 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/10/21 DM0610/21009538 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/11/21 DM0611/21009549 390 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/12/21 DM0612/21009568 390 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/13/21 DM0613/21009602 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/14/21 DM0614/21009629 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/18/21 DM0618/21009979 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/19/21 DM0619/21010314 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/20/21 DM0620/21010332 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/21/21 DM0621/21010359 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/22/21 DM0622/21010375 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/23/21 DM0623/21010408 410 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/24/21 DM0624/21010670 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/25/21 DM0625/21010681 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/26/21 DM0626/21010702 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/27/21 DM0627/21010807 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/28/21 DM0628/21010860 400 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/29/21 DM0629/21010875 420 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/30/21 DM0630/21011438 390 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/01/21 DM0701/21011453 420 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/02/21 DM0702/21011465 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/03/21 DM0703/21011485 450 mg/kg D.W. 4.7 15 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/05/21 DM0705/21011572 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/06/21 DM0706/21011693 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/07/21 DM0707/21011727 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/08/21 DM0708/21011742 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 92 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FP CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
460 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
450 mg/kg D.W. 4.7 14
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
460 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
07/12/21 DM0712/21012283 450 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
07/13/21 DM0713/21012298 470 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
07/14/21 DM0714/21012332 440 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
07/15/21 DM0715/21012390 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/16/21 DM0716/21012563 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/17/21 DM0717/21012583 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/18/21 DM0718/21012596 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/19/21 DM0719/21012624 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/20/21 DM0720/21012639 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/21/21 DM0721/21012760 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/22/21 DM0722/21012775 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/23/21 DM0723/21013074 410 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/24/21 DM0724/21013378 410 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/25/21 DM0725/21013391 420 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/26/21 DM0726/21013419 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/27/21 DM0727/21013434 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/28/21 DM0728/21013470 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/29/21 DM0729/21013614 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/30/21 DM0730/21013629 460 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
07/31/21 DM0731/21013739 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/01/21 DM0801/21013752 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/02/21 DM0802/21013891 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/03/21 DM0803/21013906 520 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/04/21 DM0804/21013940 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/05/21 DM0805/21014673 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/06/21 DM0806/21014685 530 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/07/21 DM0807/21014705 520 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/08/21 DM0809/21014718 530 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/09/21 DM0809/21014746 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/10/21 DM0810/21014847 600 mg/kg D.W. 4.7 15 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 570 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/12/21 DM0812/21015285 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/13/21 DM0813/21015297 560 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/14/21 DM0814/21015317 540 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/15/21 DM0815/21015330 490 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/16/21 DM0816/21015410 480 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/17/21 DM0817/21015425 540 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/18/21 DM0818/21016031 500 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/19/21 DM0819/21016046 480 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/20/21 DM0820/21016068 500 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/21/21 DM0821/21016088 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/22/21 DM0822/21016196 530 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/23/21 DM0823/21016224 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 93 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
560 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
08/25/21
DM0825/21 01 6327
540 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
500 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
08/27/21 DM0827/21016407 490 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
08/28/21 DM0828/21016427 500 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
08/30/21 DM0830/21016468 530 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
08/31/21 DM0831/21016483 550 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/01/21 DM0901/21016598 560 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
09/02/21 DM0902/21016659 540 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/03/21 DM0903/21016671 570 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
09/04/21 DM0904/21017055 590 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/05/21 DM0905/21017068 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/06/21 DM0906/21017096 570 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/07/21 DM0907/21017306 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/08/21 DM0908/21017338 520 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/09/21 DM0909/21017408 510 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/10/21 DM0910/21017420 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/11/21 DM0911/21017699 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/12/21 DM0912/21017712 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/13/21 DM0913/21017740 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/14/21 DM0914/21017755 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 510 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 150012-1
09/17/21 DM0917/21018105 520 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 530 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 500 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 500 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 150123-1
09/21/21 DM0921/21018251 540 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 150123-1
09/22/21 DM0922/21018480 500 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/23/21 DM0923/21018564 500 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/24/21 DM0924/21018818 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 490 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 480 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 470 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 460 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 470 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 480 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 490 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 150431-1
10/07/21 DM1007/21019760 490 mg/kg D.W. 4.7 14
SW846: 6010C
MMSD 150431-1
10/08/21 DM1008/21019772 470 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 500 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 150655-1
10/20/21 DM1 020/21 020674 880 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150655-1
Page 94 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Daily Composite
ZINC ICP Dry wt.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
510 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
510 mg/kg D.W. 4.7 14
SW846: 6010C
MMSD 150703-1
10/23/21 DM 1023/21020883
490 mg/kg D.W. 4.6 14
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 470 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 490 mg/kg D.W. 4.7 14
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 480 mg/kg D.W. 4.7 14
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 480 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 150831-1
10/29/21 DM1029/21021510 470 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 150831-1
10/30/21 DM1030/21021530 480 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 150831-1
10/31/21 DM1031/21021574 480 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 150831-1
11/01/21 DM1101/21021608 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 150831-1
11/02/21 DM1102/21021623 490 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 470 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 500 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 490 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 480 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 490 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151039-2
11/11/21 DM1111/21022695 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 470 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 470 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151039-1
11/14/21 DM1114/21022744 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151085-1
11/16/21 DM1116/21022787 460 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151085-1
11/17/21 DM1117/21023039 480 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151122-1
11/18/21 DM1118/21023056 460 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151122-1
11/19/21 DM1119/21023181 450 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151175-1
11/20/21 DM1120/21023201 480 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151175-1
11/21/21 DM1121/21023214 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151175-1
11/22/21 DM1122/21023555 450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151175-1
11/23/21 DM1123/21023570 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151252-1
11/24/21 DM1124/21023611 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151266-1
11/25/21 DM1125/21023795 470 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151266-1
11/26/21 DM1126/21023807 430 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151266-1
11/27/21 DM1127/21023827 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151266-1
11/28/21 DM1128/21023899 470 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151266-1
11/29/21 DM1129/21023927 490 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151294-1
11/30/21 DM1130/21024167 490 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151317-1
12/01/21 DM1201/21024282 490 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151317-2
12/02/21 DM1202/21024297 480 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151342-1
12/03/21 DM1203/21024309 480 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151371-1
12/04/21 DM1204/21024329 430 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151371-1
12/05/21 DM1205/21024739 450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151371-1
Page 95 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FL CLER+fR ix�lE HERE
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
470 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
151391-1
12/07/21
DM1207/21024782
430 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151471-2
12/10/21 DM1210/21024844 480 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151498-1
12/11/21 DM1211/21024864 460 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151498-1
12/12/21 DM1212/21025174 470 mg/kg D.W. 4.7 14
SW846: 6010C
MMSD 151498-1
12/13/21 DM1213/21025205 450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151543-1
12/14/21 DM1214/21025220 470 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151576-1
12/15/21 DM1215/21025299 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151576-1
12/16/21 DM1216/21025314 460 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD 151645-1
12/17/21 DM1217/21025326 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151645-1
12/18/21 DM1219/21025346 450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151645-1
12/19/21 DM1219/21025621 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151645-1
12/20/21 DM1220/21025649 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151645-2
12/21/21 DM1221/21025664 440 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151668-1
12/22/21 DM1222/21025700 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151750-1
12/23/21 DM1223/21025779 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151750-2
12/24/21 DM1224/21025791 460 mg/kg D.W. 4.9 15
SW846: 6010C
MMSD 151750-2
12/25/21 DM1225/21025811 450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151750-2
12/26/21 DM1226/21025824 450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151750-2
12/27/21 DM1227/21025917 470 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151750-2
12/28/21 DM1228/21025932 460 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151750-2
12/29/21 DM1229/21025966 480 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151827-1
12/30/21 DM1230/21025981 480 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151827-1
12/31/21 DM1231/21026033 470 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151827-1
Avg Result: 420 mg/kg D.W. Min LOD: 4.6 mg/kg D.W.
Max Result: 880 mg/kg D.W. Max LOD: 4.9 mg/kg D.W.
Page 96 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
01/01/21
DM0101/21000012
2.8 % D.W.
0.1
0.1
AO.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
2.9%D.W. 0.1 0.1 AO.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
2.7%D.W. 0.1 0.1 AO.
SW846: 6010C MMSD
01/04/21 DM0104/21000488
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/05/21 DM0105/21000504
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/06/21 DM0106/21000535
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/07/21 DM0107/21000551
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/08/21 DM0108/21000562
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/09/21 DM0109/21000581
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
01/10/21 DM0110/21000594
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/11/21 DM0111/21000632
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/12/21 DM0112/21000648
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/13/21 DM0113/21000679
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
01/14/21 DM0114/21000754 2.8 % D.W. 0.1 0.1 AO. SW846: 6010C MMSD
01/15/21 DM0115/21000765 2.8 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
01/16/21 DM0116/21000784 2.7 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
01/17/21 DM0117/21000797
2.7%D.W. 0.1
0.1 Q3.
SW846: 6010C MMSD
01/18/21 DM0118/21000824
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
01/19/21 DM0119/21000842
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
01/20/21 DM0120/21000926
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/21/21 DM0121/21000942
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/22/21 DM01 22/21 000953
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
01/23/21 DM0123/21000972
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
01/24/21 DM0124/21001059
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
01/25/21 DM0125/21001088
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/26/21 DM0126/21001106
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/27/21 DM0127/21001137
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/28/21 DM0128/21001153
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
01/29/21 DM0129/21001164
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
01/30/21 DM0130/21001304
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
01/31/21 DM0131/21001317
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
02/01/21 DM0201/21001344
2.6%D.W. 0.1 0.1 D2, Q3.
SW846: 6010C MMSD
02/02/21 DM0202/21001397
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
02/03/21 DM0203/21001428
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
02/04/21 DM0204/21001444
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
02/05/21 DM0205/21001455
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/06/21 DM0206/21001476
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/07/21 DM0207/21001489
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
02/08/21 DM0208/21001609
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
02/09/21 DM0209/21001625
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
02/10/21 DM0210/21001656
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
02/11/21 DM0211/21001672
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
02/12/21 DM0212/21001706
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
02/13/21 DM0213/21001725
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
02/14/21 DM0214/21001738
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/15/21 DM0215/21001793
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
Page 97 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FL CLER+fR ix�lE HERE
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
02/16/21
DM0216/21001841
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
02/17/21
DM021 7/21 001872
2.5 % D.W.
0.1 0.1
SW846: 6010C
MMSD
02/18/21 DM021 8/21 001975
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
02/19/21 DM021 9/21 001986
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/20/21 DM0220/21002005 2.4 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
02/21/21 DM0221/21002072 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/22/21 DM0222/21002230 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
02/23/21 DM0223/21002246 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
02/24/21 DM0224/21002281 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
02/25/21 DM0225/21002320 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
02/26/21 DM0226/21002386 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
02/27/21 DM0227/21002405 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
02/28/21 DM0228/21002478 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/01/21 DM0301/21002611
03/02/21 DM0302/21002629
03/03/21 DM0303/21002660
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
2.6%D.W.
2.4%D.W.
0.1 0.1
0.1 0.1
SW846: 6010C MMSD
SW846: 6010C MMSD
03/04/21 DM0304/21002717 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/05/21 DM0305/21002728 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/06/21 DM0306/21002747 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/07/21 DM0307/21002858 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/08/21 DM0308/21003336 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/09/21 DM0309/21003371 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/10/21 DM031 0/21 003402 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/11/21 DM0311/21003456 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/12/21 DM0312/21003522 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/13/21 DM0313/21003541 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/14/21 DM0314/21003554 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/15/21 DM0315/21003747 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/16/21 DM0316/21003801 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/17/21 DM0317/21003878 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/18/21 DM0318/21003894 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/19/21 DM0319/21003905 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/20/21 DM0320/21004076 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/21/21 DM0321/21004093 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/22/21 DM0322/21004120 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/23/21 DM0323/21004136 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/24/21 DM0324/21004167 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/25/21 DM0325/21004242 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/26/21 DM0326/21004253 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/27/21 DM0327/21004272 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
03/28/21 DM0328/21004285 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/29/21 DM0329/21004312 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/30/21 DM0330/21004388 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
03/31/21 DM0331/21004600 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/01/21 DM0401/21004616 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/02/21 DM0402/21004627 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
Page 98 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
04/03/21
DM0403/21004646
2.3%D.W.
0.1
0.1
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
2.3 % D.W.
0.1 0.1
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/06/21 DM0406/21004758
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
04/07/21 DM0407/21004843 2.5 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
04/08/21 DM0408/21004861 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
04/09/21 DM0409/21004912 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/10/21 DM0410/21004931 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/11/21 DM0411/21005023 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/12/21 DM0412/21005052 2.2 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/13/21 DM0413/21005199 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/14/21 DM0414/21005230 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/15/21 DM0415/21005248 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/16/21 DM0416/21005259 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/17/21 DM0417/21005468 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/18/21 DM0418/21005481 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/19/21 DM0419/21005508 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/20/21 DM0420/21005839 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/21/21 DM0421/21005870 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/22/21 DM0422/21005981 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/23/21 DM0423/21005992 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/24/21 DM0424/21006057 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/25/21 DM0425/21006272 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/26/21 DM0426/21006299 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/27/21 DM0427/21006315 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/28/21 DM0428/21006346 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
04/29/21 DM0429/21006362 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
04/30/21 DM0430/21006373 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/01/21 DM0501/21006429 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
05/02/21 DM0502/21006442 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
05/03/21 DM0503/21006676 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/04/21 DM0504/21006691 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
05/05/21 DM0505/21006722 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/06/21 DM0506/21006781 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
05/07/21 DM0507/21006834 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/08/21 DM0508/21006981 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/09/21 DM0509/21006994 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/10/21 DM0510/21007021 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/11/21 DM0511/21007171 2.5 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/12/21 DM0512/21007202 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
05/13/21 DM0513/21007217 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/14/21 DM0514/21007309 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/15/21 DM0515/21007328 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/16/21 DM0516/21007341 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/17/21 DM0517/21007382 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/18/21 DM0518/21007440 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
Page 99 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
05/19/21
DM0519/21007895
2.4 % D.W.
0.1
0.1
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
2.5 % D.W.
0.1 0.1
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/22/21 DM0522/21008072
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/23/21 DM0523/21008085 2.6 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
05/25/21 DM0525/21008288 2.6 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
05/26/21 DM0526/21008319 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/27/21 DM0527/21008484 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
05/28/21 DM0528/21008495 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/29/21 DM0529/21008515 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
05/30/21 DM0530/21008530 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
06/01/21 DM0601/21008902 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/02/21 DM0602/21008935 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/03/21 DM0603/21008950 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/04/21 DM0604/21009184 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/05/21 DM0605/21009203 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/06/21 DM0606/21009287 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/07/21 DM0607/21009314 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/08/21 DM0608/21009334 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/09/21 DM0609/21009365 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/10/21 DM0610/21009538 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
06/11/21 DM0611/21009549 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/12/21 DM0612/21009568 2.9 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/13/21 DM0613/21009602 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/14/21 DM0614/21009629 2.9 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/18/21 DM0618/21009979 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/19/21 DM0619/21010314 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
06/20/21 DM0620/21010332 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
06/21/21 DM0621/21010359 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
06/22/21 DM0622/21010375 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/23/21 DM0623/21010408 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/24/21 DM0624/21010670 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/25/21 DM0625/21010681 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/26/21 DM0626/21010702 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/27/21 DM0627/21010807 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/28/21 DM0628/21010860 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/29/21 DM0629/21010875 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
06/30/21 DM0630/21011438 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/01/21 DM0701/21011453 2.5 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/02/21 DM0702/21011465 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/03/21 DM0703/21011485 2.4 % D.W. 0.1 0.1 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/05/21 DM0705/21011572 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/06/21 DM0706/21011693 2.5 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/07/21 DM0707/21011727 2.5 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/08/21 DM0708/21011742 2.5 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
Page 100 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

MMSD
PARNEfd FP CLER+fR ix�lE HERE
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
07/09/21
DM0709/21011754
2.5%D.W.
0.1
0.1
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
2.4%D.W.
0.1 0.1
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
07/12/21 DM0712/21012283
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
07/13/21 DM0713/21012298 2.7 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
07/14/21 DM0714/21012332 2.6 0/0 D.W. 0.1 0.1
SW846: 6010C MMSD
07/15/21 DM0715/21012390 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/16/21 DM0716/21012563 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
07/17/21 DM0717/21012583 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
07/18/21 DM0718/21012596 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/19/21 DM0719/21012624 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/20/21 DM0720/21012639 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/21/21 DM0721/21012760 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/22/21 DM0722/21012775 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/23/21 DM0723/21013074 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/24/21 DM0724/21013378 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/25/21 DM0725/21013391 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/26/21 DM0726/21013419 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/27/21 DM0727/21013434 2.9 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/28/21 DM0728/21013470 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/29/21 DM0729/21013614 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/30/21 DM0730/21013629 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
07/31/21 DM0731/21013739 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/01/21 DM0801/21013752 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/02/21 DM0802/21013891 2.9 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/03/21 DM0803/21013906 2.9 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/04/21 DM0804/21013940 2.9 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/05/21 DM0805/21014673 3 % D.W. 0.1 0.1 SW846: 6010C MMSD
08/06/21 DM0806/21014685 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/07/21 DM0807/21014705 2.8 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/08/21 DM0809/21014718 2.7 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/09/21 DM0809/21014746 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/10/21 DM0810/21014847 2.6 % D.W. 0.1 0.1 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 2.5 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/12/21 DM0812/21015285 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/13/21 DM0813/21015297 2.5 % D.W. 0.1 0.1 SW846: 6010C MMSD
08/14/21 DM0814/21015317 2.2 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/15/21 DM0815/21015330 2 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/16/21 DM0816/21015410 2 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/17/21 DM0817/21015425 2.4 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/18/21 DM0818/21016031 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
08/19/21 DM0819/21016046 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
08/20/21 DM0820/21016068 2.3 % D.W. 0.1 0.1 SW846: 6010C MMSD
08/21/21 DM0821/21016088 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/22/21 DM0822/21016196 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
08/23/21 DM0823/21016224 2.6 0/0 D.W. 0.1 0.1 SW846: 6010C MMSD
Page 101 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
08/24/21
DM0824/21016239
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
2.5 % D.W.
0.1 0.1
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
08/27/21 DM0827/21016407
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
08/28/21 DM0828/21016427
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
08/30/21 DM0830/21016468
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
08/31/21 DM0831/21016483
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/01/21 DM0901/21016598
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/02/21 DM0902/21016659
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/03/21 DM0903/21016671
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/04/21 DM0904/21017055
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
09/05/21 DM0905/21017068
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/06/21 DM0906/21017096
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/07/21 DM0907/21017306
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/08/21 DM0908/21017338
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/09/21 DM0909/21017408
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/10/21 DM0910/21017420
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/11/21 DM0911/21017699
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/12/21 DM0912/21017712
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/13/21 DM0913/21017740
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/14/21 DM0914/21017755
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/15/21 DM0915/21017903
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/16/21 DM0916/21018023
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
09/17/21 DM0917/21018105
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
09/18/21 DM0918/21018125
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/19/21 DM0919/21018138
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/20/21 DM0920/21018236
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/21/21 DM0921/21018251
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/22/21 DM0922/21018480
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/23/21 DM0923/21018564
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/24/21 DM0924/21018818
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/25/21 DM0925/21018838
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/26/21 DM0926/21019023
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/27/21 DM0927/21019051
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
09/28/21 DM0928/21019066
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
09/29/21 DM0929/21019228
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/30/21 DM0930/21019243
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/01/21 DM1001/21019255
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
10/02/21 DM1002/21019384
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
10/03/21 DM1003/21019397
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
10/04/21 DM1004/21019425
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/06/21 DM1006/21019735
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
10/07/21 DM1007/21019760
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
10/08/21 DM1008/21019772
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/19/21 DM1 019/21 020600
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/20/21 D M 1020/21020674
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
Page 102 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
10/21/21
DM1021/21020689
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/22/21
DM1 022/21 020701
2.9%D.W.
0.1 0.1
SW846: 6010C
MMSD
10/23/21 D M 1023/21020883
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
10/24/21 D M 1024/21021034
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
10/25/21 D M 1025/21021062
3%D.W.
0.1 0.1
SW846: 6010C MMSD
10/26/21 D M 1026/21021077
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/27/21 DM1027/21021161
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/28/21 D M 1028/21021226
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
10/29/21 DM1029/21021510
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/30/21 D M 1030/21021530
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
10/31/21 DM1031/21021574
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
11/01/21 DM1101/21021608
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
11/02/21 DM1102/21021623
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
11/03/21 DM1103/21021720
11/04/21 DM1104/21021735
11/05/21 DM1105/21021747
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/06/21 DM1106/21021767
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/07/21 D M 1107/21022553
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/08/21 DM1108/21022581
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/09/21 D M 1109/21022596
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/10/21 DM1110/21022680
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/11/21 DM1111/21022695
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/12/21 DM1112/21022707
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/13/21 DM1113/21022731
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/14/21 DM1114/21022744
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
11/15/21 DM1115/21022772
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/16/21 DM1116/21022787
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/17/21 DM1117/21023039
2.8%D.W. 0.1 0.1 Q3.
SW846: 6010C MMSD
11/18/21 DM1118/21023056
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/19/21 DM1119/21023181
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/20/21 DM1120/21023201
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/21/21 DM1121/21023214
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/22/21 D M 1122/21023555
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/23/21 D M 1123/21023570
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
11/24/21 DM1124/21023611
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/25/21 DM1125/21023795
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
11/26/21 D M 1126/21023807
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
11/27/21 D M 1127/21023827
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/28/21 D M 1128/21023899
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/29/21 DM1129/21023927
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
11/30/21 DM1130/21024167
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/01/21 DM1201/21024282
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/02/21 DM1202/21024297
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/03/21 DM1203/21024309
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/04/21 DM1204/21024329
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/05/21 DM1205/21024739
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
Page 103 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix�lE HERE
Milorganite Daily Composite
Phosphorus - Total % DW (Calc.)
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
QC Batch
ID
12/06/21
DM1206/21024767
2.9 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/07/21
DM1207/21024782
2.7%D.W.
0.1 0.1
SW846: 6010C
MMSD
12/08/21 DM1208/21024816
2.7%D.W.
0.1 0.1
SW846: 6010C
MMSD
12/09/21 DM1209/21024832
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/10/21 DM1210/21024844
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/11/21 DM1211/21024864
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/12/21 DM1212/21025174
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/13/21 DM1213/21025205
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/14/21 DM1214/21025220
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/15/21 DM1215/21025299
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/16/21 DM1216/21025314
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/17/21 DM1217/21025326
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/18/21 DM1219/21025346
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/19/21 DM1219/21025621
12/20/21 DM1220/21025649
12/21/21 DM1221/21025664
2.6%D.W.
0.1 0.1
SW846: 6010C MMSD
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/22/21 DM1222/21025700
2.7%D.W.
0.1 0.1
SW846: 6010C MMSD
12/23/21 DM1223/21025779
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/24/21 DM1224/21025791
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/25/21 DM1225/21025811
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/26/21 DM1226/21025824
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/27/21 DM1227/21025917
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
12/28/21 DM1228/21025932
2.9%D.W.
0.1 0.1
SW846: 6010C MMSD
12/29/21 DM1229/21025966
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/30/21 DM1230/21025981
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/31/21 DM1231/21026033
2.8%D.W.
0.1 0.1
SW846: 6010C MMSD
Avg Result: 2.6 % D.W.
ALUMINUM ICP Dry wt.
Min LOD: 0.1 0/0 D.W.
Max Result: 3 % D.W. Max LOD: 0.1 0/0 D.W.
Milorganite Weekly Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana ytica Met o
QC Batch
a. ID
01/09/21
W MCO2/21000596
7400 mg/kg D.W.
61
210
B8.
SW846: 6010C
MMSD
02/13/21
W MC07/21001740
5400 mg/kg D.W. 60 210 B8.
SW846: 6010C
MMSD
03/13/21 WMC11/21003556
5000 mg/kg D.W. 60 210 B8.
SW846: 6010C
MMSD
04/10/21 WMC15/21005026
5400 mg/kg D.W. 60 210 B8.
SW846: 6010C MMSD
05/08/21 WMC19/21006996
7300 mg/kg D.W. 60 210 B8. SW846: 6010C MMSD
06/12/21 WMC24/21009604
8100 mg/kg D.W. 60 210 B8. SW846: 6010C MMSD
07/10/21 WMC28/21012257
9000 mg/kg D.W. 60 210 B8. SW846: 6010C MMSD
08/07/21 WMC32/21014720
7200 mg/kg D.W. 60 210 B8. SW846: 6010C MMSD
Avg Result: 6800 mg/kg D.W. Min LOD: 60 mg/kg D.W.
Max Result: 9000 mg/kg D.W. Max LOD: 61 mg/kg D.W.
SYS/rptlMiloMonthlyDW 10/21/21 tj
Page 104 of 121
Printed: 1/13/2214:24

MMSD
PARNEfdEPA CLER+fRE HEEII
(Milo) Ammonia in Fertilizer
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/09/21
W MCO2/21000596
0.24
0.01
AOAC 920.03 (mod) Midwest
Laboratories
02/13/21
W MC07/21001740
0.23 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
03/13/21 WMC11/21003556
0.2 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
04/10/21 WMC1 5/21 005026
0.23 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
05/08/21 WMC1 9/21 006996
0.27 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
06/12/21 WMC24/21009604 0.22 % 0.01 AOAC 920.03 (mod) Midwest
Laboratories
07/10/21 WMC28/21012257
0.26 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
08/07/21 WMC32/21014720
0.25 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
09/11/21 WMC37/21017714 0.2 % 0.01 AOAC 920.03 (mod) Midwest
Laboratories
10/09/21 WMC41/21019807
0.18 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
11/13/21 W MC46/21022746
0.25 % 0.01
12/11/21 WMC50/21025262
0.25 % 0.01
Avg Result: 0.23 0/0
BORON ICP Dry wt.
Min LOD: 0.01 %
Max Result: 0.27 0/0
AOAC 920.03 (mod) Midwest
Laboratories
AOAC 920.03 (mod) Midwest
Laboratories
Max LOD: 0.01 0/0
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
W MCO2/21000596
23 mg/kg D.W.
5.4
20.6
EPA 6010
Pace -GB
02/13/21
W MC07/21001740
24 mg/kg D.W. 5.4 20.6
EPA 6010
Pace -GB
03/13/21 WMC11/21003556
24 mg/kg D.W. 5.2 20
EPA 6010
Pace -GB
04/10/21 WMC15/21005026 22 mg/kg D.W. 5.5 20.9
EPA 6010 Pace -GB
05/08/21 WMC19/21006996 20 mg/kg D.W. 1.1 4.2
EPA 6010D Pace -GB
06/12/21 WMC24/21009604 23 mg/kg D.W. 2.2 8.4
EPA 6010D Pace -GB
07/10/21 WMC28/21012257 18 mg/kg D.W. 1.1 4.2 AX. EPA 6010D Pace -GB
08/07/21 WMC32/21014720 19 mg/kg D.W. 2.1 8.1 EPA 6010D Pace -GB
09/11/21 WMC37/21017714 24 mg/kg D.W. 2.2 8.4 EPA 6010D Pace -GB
10/09/21 WMC41/21019807 24 mg/kg D.W. 2.2 8.3 EPA 6010D Pace -GB
11/13/21 WMC46/21022746 21 mg/kg D.W. 2.2 8.3 EPA 6010D Pace -GB
12/11/21 WMC50/21025262 18 mg/kg D.W. 1.1 4.2 EPA 6010D Pace -GB
Avg Result: 22 mg/kg D.W. Min LOD: 1.1 mg/kg D.W. Max Result: 24 mg/kg D.W. Max LOD: 5.5 mg/kg D.W.
Page 105 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLEktER ix�lE HERE
Milorganite Weekly Composite
CHROMIUM ICP Dry wt.
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/09/21
W MCO2/21000596
160 mg/kg D.W.
0.4
1.2
SW846: 6010C
MMSD
02/13/21
W MC07/21001740
320 mg/kg D.W. 0.4 1.2
SW846: 6010C
MMSD
03/13/21 WMC11/21003556
260 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
04/10/21 WMC15/21005026 270 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
05/08/21 WMC19/21006996 280 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
06/12/21 WMC24/21009604 250 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
07/10/21 WMC28/21012257 200 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
08/07/21 WMC32/21014720 230 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
Avg Result: 250 mg/kg D.W. Min LOD: 0.4 mg/kg D.W.
COBALT ICP Dry wt.
Max Result: 320 mg/kg D.W. Max LOD: 0.4 mg/kg D.W.
QC Batch
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab ID
01/09/21
W MCO2/21000596
2.8 mg/kg D.W.
0.3
1.2
B8.
SW846: 6010C
MMSD
02/13/21
W MC07/21001740
3 mg/kg D.W. 0.29 1.2 B8.
SW846: 6010C
MMSD
03/13/21 WMC11/21003556
3 mg/kg D.W. 0.29 1.2 B8.
SW846: 6010C MMSD
04/10/21 WMC15/21005026
3 mg/kg D.W. 0.3 1.2 B8.
SW846: 6010C MMSD
05/08/21 WMC19/21006996 3 mg/kg D.W. 0.29 1.2 68. SW846: 6010C MMSD
06/12/21 WMC24/21009604 3 mg/kg D.W. 0.3 1.2 68. SW846: 6010C MMSD
07/10/21 WMC28/21012257 3.4 mg/kg D.W. 0.29 1.2 68. SW846: 6010C MMSD
08/07/21 WMC32/21014720 3.6 mg/kg D.W. 0.29 1.2 68. SW846: 6010C MMSD
Avg Result: 3.1 mg/kg D.W. Min LOD: 0.29 mg/kg D.W.
Max Result: 3.6 mg/kg D.W. Max LOD: 0.3 mg/kg D.W.
Page 106 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FL LI.EktERligilpIEW
Milorganite Weekly Composite
MERCURY by M. 7471 (sludge)
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/02/21
WMC01/21000078
0.15 mg/kg D.W. 0.023 0.079
EPA 7471
Pace -GB
01/09/21
W MCO2/21000596
0.17 mg/kg D.W. 0.021 0.074
EPA 7471
Pace -GB
01/16/21 WMC03/21000799
0.22 mg/kg D.W. 0.022 0.077
EPA 7471
Pace -GB
01/23/21 WMC04/21001061 0.19 mg/kg D.W. 0.021 0.072
EPA 7471 Pace -GB
01/30/21 WMC05/21001319 0.39 mg/kg D.W. 0.018 0.063
EPA 7471 Pace -GB
02/06/21 WMC06/21001491 0.3 mg/kg D.W. 0.022 0.076 AX. EPA 7471 Pace -GB
02/13/21 WMC07/21001740 0.16 mg/kg D.W. 0.021 0.073
EPA 7471 Pace -GB
02/20/21 WMC08/21002074 0.24 mg/kg D.W. 0.019 0.067 EPA 7471 Pace -GB
02/27/21 WMC09/21002480 0.12 mg/kg D.W. 0.021 0.073 EPA 7471 Pace -GB
03/06/21 WMC10/21002860 0.25 mg/kg D.W. 0.02 0.068 EPA 7471 Pace -GB
03/13/21 WMC11/21003556 0.16 mg/kg D.W. 0.02 0.07 EPA 7471 Pace -GB
03/20/21 WMC12/21004095 0.21 mg/kg D.W. 0.021 0.074 EPA 7471 Pace -GB
03/27/21 WMC13/21004287 0.19 mg/kg D.W. 0.021 0.075 EPA 7471 Pace -GB
04/03/21 WMC14/21004661 0.18 mg/kg D.W. 0.02 0.071 EPA 7471 Pace -GB
04/10/21 WMC15/21005026 0.27 mg/kg D.W. 0.019 0.067 EPA 7471 Pace -GB
04/17/21 WMC16/21005483 0.18 mg/kg D.W. 0.02 0.07 EPA 7471 Pace -GB
04/24/21 WMC17/21006274 0.17 mg/kg D.W. 0.021 0.072 EPA 7471 Pace -GB
05/01/21 WMC18/21006444 0.17 mg/kg D.W. 0.021 0.075 EPA 7471 Pace -GB
05/08/21 WMC19/21006996 0.18 mg/kg D.W. 0.02 0.071 EPA 7471 Pace -GB
05/15/21 WMC20/21007343 0.14 mg/kg D.W. 0.02 0.07 EPA 7471 Pace -GB
05/22/21 WMC21/21008087 0.18 mg/kg D.W. 0.021 0.072 EPA 7471 Pace -GB
05/29/21 WMC22/21008532 0.19 mg/kg D.W. 0.022 0.075 EPA 7471 Pace -GB
06/05/21 WMC23/21009289 0.35 mg/kg D.W. 0.02 0.069 EPA 7471 Pace -GB
06/12/21 WMC24/21009604 0.22 mg/kg D.W. 0.021 0.074 EPA 7471 Pace -GB
06/19/21 WMC25/21010334 0.18 mg/kg D.W. 0.022 0.076 AX. EPA 7471 Pace -GB
06/26/21 WMC26/21010809 0.26 mg/kg D.W. 0.021 0.074 EPA 7471 Pace -GB
07/03/21 WMC27/21011518 0.31 mg/kg D.W. 0.021 0.074 AX. EPA 7471 Pace -GB
07/10/21 WMC28/21012257 0.2 mg/kg D.W. 0.019 0.068 EPA 7471 Pace -GB
07/17/21 WMC29/21012598 0.17 mg/kg D.W. 0.021 0.073 EPA 7471 Pace -GB
07/24/21 WMC30/21013393 0.27 mg/kg D.W. 0.021 0.075 AX. EPA 7471 Pace -GB
07/31/21 WMC31/21013754 0.17 mg/kg D.W. 0.022 0.076 EPA 7471 Pace -GB
08/07/21 WMC32/21014720 0.42 mg/kg D.W. 0.022 0.077 EPA 7471 Pace -GB
08/14/21 WMC33/21015332 0.27 mg/kg D.W. 0.018 0.064 EPA 7471 Pace -GB
08/21/21 WMC34/21016198 0.52 mg/kg D.W. 0.02 0.069 EPA 7471 Pace -GB
08/28/21 WMC35/21016442 0.33 mg/kg D.W. 0.019 0.066 EPA 7471 Pace -GB
09/04/21 WMC36/21017070 0.38 mg/kg D.W. 0.021 0.074 EPA 7471 Pace -GB
09/11/21 WMC37/21017714 0.31 mg/kg D.W. 0.021 0.075 EPA 7471 Pace -GB
09/18/21 WMC38/21018140 0.32 mg/kg D.W. 0.019 0.068 EPA 7471 Pace -GB
09/25/21 WMC39/21019025 0.23 mg/kg D.W. 0.021 0.074 EPA 7471 Pace -GB
10/02/21 WMC40/21019399 0.31 mg/kg D.W. 0.019 0.066 EPA 7471 Pace -GB
10/09/21 WMC41/21019807 0.21 mg/kg D.W. 0.019 0.065 EPA 7471 Pace -GB
10/23/21 WMC43/21021036 0.24 mg/kg D.W. 0.021 0.072 EPA 7471 Pace -GB
10/30/21 WMC44/21021576 0.26 mg/kg D.W. 0.022 0.079 EPA 7471 Pace -GB
11/06/21 WMC45/21022555 0.13 mg/kg D.W. 0.021 0.074 EPA 7471 Pace -GB
11/13/21 WMC46/21022746 0.25 mg/kg D.W. 0.02 0.071 EPA 7471 Pace -GB
11/20/21 WMC47/21023216 0.24 mg/kg D.W. 0.022 0.076 EPA 7471 Pace -GB
Page 107 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfdFL LI.EktERligilpIEW
Milorganite Weekly Composite
MERCURY by M. 7471 (sludge)
Sample Date Sample ID
Result LOD LOQ QA Flags na Ica e o
QC Batch
ID
11/27/21
WMC48/21023901
0.24 mg/kg D.W. 0.021
0.074
EPA 7471
Pace -GB
12/04/21
WMC49/21024741
0.24 mg/kg D.W. 0.023 0.082
EPA 7471
Pace -GB
12/11/21 WMC50/21025262
0.17 mg/kg D.W. 0.02 0.069
EPA 7471
Pace -GB
12/18/21 WMC51/21025623
0.25 mg/kg D.W. 0.02 0.07
EPA 7471 Pace -GB
12/25/21 WMC52/21026035
0.29 mg/kg D.W. 0.02 0.072
EPA 7471 Pace -GB
Avg Result: 0.24 mg/kg D.W. Min LOD: 0.018 mg/kg D.W.
NITRATE NITROGEN
Max Result: 0.52 mg/kg D.W. Max LOD: 0.023 mg/kg D.W.
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
W MCO2/21000596
< 0.01
0.01
WC PROC 32
Midwest
Laboratories
02/13/21
W MC07/21001740
< 0.01 % 0.01
03/13/21 WMC11/21003556
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
WC PROC 32 Midwest
Laboratories
04/10/21 WMC15/21005026
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
05/08/21 WMC19/21006996
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
06/12/21 WMC24/21009604
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
07/10/21 WMC28/21012257
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
08/07/21 WMC32/21014720
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
09/11/21 WMC37/21017714
< 0.01 % 0.01
10/09/21 W MC41 /21019807
WC PROC 32 Midwest
Laboratories
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
11/13/21 WMC46/21022746
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
12/11/21 WMC50/21025262
< 0.01 % 0.01
Avg Result: 0 % Min LOD: 0.01 0/0
WC PROC 32 Midwest
Laboratories
Max Result: 0.01 % Max LOD: 0.01 %
Page 108 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR (KiI iRWEEU
Milorganite Weekly Composite
NITROGEN-Total(Auto)
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o.
QC Batch
ID
01/09/21
W MCO2/21000596
6.6
0.01
02/13/21
W MC07/21001740
6.9 % 0.01
MWL WC PROC 55
Midwest
Laboratories
MWL WC PROC 55 Midwest
Laboratories
03/13/21 WMC11/21003556
6.9 % 0.01
MWL WC PROC 55 Midwest
Laboratories
04/10/21 WMC15/21005026
6.8 % 0.01
MWL WC PROC 55 Midwest
Laboratories
05/08/21 WMC19/21006996
6.6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
06/12/21 WMC24/21009604
6.2 % 0.01
MWL WC PROC 55 Midwest
Laboratories
07/10/21 WMC28/21012257
6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
08/07/21 WMC32/21014720
6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
09/11/21 WMC37/21017714
10/09/21 WMC41/21019807
5.7 % 0.01
MWL WC PROC 55 Midwest
Laboratories
6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
11/13/21 WMC46/21022746
6.5 % 0.01
MWL WC PROC 55 Midwest
Laboratories
12/11/21 WMC50/21025262
6.6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
Avg Result: 6.4 %
NITROGEN -Water Insoluble
Min LOD: 0.01 %
Max Result: 6.9 %
Max LOD: 0.01 %
amp e ' a e Sample ID Result LOD LOQ QA Flags Analytical Method
Lab
QC Batch
ID
01/09/21
W MCO2/21000596
5%
0.01
AOAC (16) 945.01
Midwest
Laboratories
02/13/21
W MC07/21001740
5.9 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
03/13/21 WMC11/21003556
5.3 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
04/10/21 WMC15/21005026
5.6 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
05/08/21 WMC19/21006996
5.4 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
06/12/21 WMC24/21009604
5%
0.01
AOAC (16) 945.01 Midwest
Laboratories
07/10/21 WMC28/21012257
4.7 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
08/07/21 WMC32/21014720
09/11/21 WMC37/21017714
10/09/21 WMC41/21019807
5.1 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
4.7 % 0.01
4.8 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
AOAC (16) 945.01 Midwest
Laboratories
11/13/21 WMC46/21022746
5%
0.01
AOAC (16) 945.01 Midwest
Laboratories
12/11/21 WMC50/21025262
5.5 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
Avg Result: 5.2 % Min LOD: 0.01 %
Max Result: 5.9 % Max LOD: 0.01 %
Page 109 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL CLER+fR ix•1lE HERE
Milorganite Weekly Composite
pH -Solids
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/02/21
W MC01 /21000078
6.25 Stnd. Units
0.1
SW846: 9045D
MMSD
01/09/21
W MCO2/21000596
6.18 Stnd. Units 0.1
SW846: 9045D
MMSD
01/16/21 WMC03/21000799
6.17 Stnd. Units 0.1
SW846: 9045D MMSD
01/23/21 WMC04/21001061 6.18 Stnd. Units 0.1
SW846: 9045D MMSD
01/30/21 WMC05/21001319 6.12 Stnd. Units 0.1
SW846: 9045D MMSD
02/06/21 WMC06/21001491 6.25 Stnd. Units 0.1
SW846: 9045D MMSD
02/13/21 WMC07/21001740 6 Stnd. Units 0.1
SW846: 9045D MMSD
02/20/21 WMC08/21002074 5.91 Stnd. Units 0.1
SW846: 9045D MMSD
02/27/21 WMC09/21002480 5.89 Stnd. Units 0.1 SW846: 9045D MMSD
03/06/21 WMC10/21002860 5.97 Stnd. Units 0.1 SW846: 9045D MMSD
03/13/21 WMC11/21003556 5.95 Stnd. Units 0.1 SW846: 9045D MMSD
03/20/21 WMC12/21004095 5.99 Stnd. Units 0.1 SW846: 9045D MMSD
03/27/21 WMC13/21004287 5.99 Stnd. Units 0.1 SW846: 9045D MMSD
04/03/21 WMC14/21004661 6.04 Stnd. Units 0.1 SW846: 9045D MMSD
04/10/21 WMC15/21005026 6.14 Stnd. Units 0.1 SW846: 9045D MMSD
04/17/21 WMC16/21005483 6.21 Stnd. Units 0.1 SW846: 9045D MMSD
04/24/21 WMC17/21006274 6.23 Stnd. Units 0.1 SW846: 9045D MMSD
05/01/21 WMC18/21006444 6.2 Stnd. Units 0.1 SW846: 9045D MMSD
05/08/21 WMC19/21006996 6.18 Stnd. Units 0.1 SW846: 9045D MMSD
05/15/21 WMC20/21007343 6.18 Stnd. Units 0.1 SW846: 9045D MMSD
05/22/21 WMC21/21008087 6.39 Stnd. Units 0.1 SW846: 9045D MMSD
05/29/21 WMC22/21008532 6.4 Stnd. Units 0.1 SW846: 9045D MMSD
06/05/21 WMC23/21009289 6.49 Stnd. Units 0.1 SW846: 9045D MMSD
06/12/21 WMC24/21009604 6.39 Stnd. Units 0.1 SW846: 9045D MMSD
06/19/21 WMC25/21010334 6.32 Stnd. Units 0.1 SW846: 9045D MMSD
06/26/21 WMC26/21010809 6.38 Stnd. Units 0.1 SW846: 9045D MMSD
07/03/21 WMC27/21011518 6.34 Stnd. Units 0.1 SW846: 9045D MMSD
07/10/21 WMC28/21012257 6.37 Stnd. Units 0.1 SW846: 9045D MMSD
07/17/21 WMC29/21012598 6.32 Stnd. Units 0.1 SW846: 9045D MMSD
07/24/21 WMC30/21013393 6.35 Stnd. Units 0.1 SW846: 9045D MMSD
07/31/21 WMC31/21013754 6.34 Stnd. Units 0.1 SW846: 9045D MMSD
08/07/21 WMC32/21014720 6.36 Stnd. Units 0.1 SW846: 9045D MMSD
08/14/21 WMC33/21015332 6.38 Stnd. Units 0.1
SW846: 9045D
MMSD 149911-1
08/21/21 WMC34/21016198 6.52 Stnd. Units 0.1
SW846: 9045D
MMSD 149911-1
08/28/21 WMC35/21016442 6.46 Stnd. Units 0.1
SW846: 9045D
MMSD 149911-1
09/04/21 WMC36/21017070 6.45 Stnd. Units 0.1
SW846: 9045D
MMSD 149911-1
09/11/21 WMC37/21017714 6.46 Stnd. Units 0.1
SW846: 9045D
MMSD 149911-1
09/18/21 WMC38/21018140 6.33 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
09/25/21 WMC39/21019025 6.38 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
10/02/21 WMC40/21019399 6.32 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
10/09/21 WMC41/21019807 6.31 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
10/23/21 WMC43/21021036 6.17 Stnd. Units 0.1 SW846: 9045D MMSD 150952-1
10/30/21 WMC44/21021576 6.16 Stnd. Units 0.1 SW846: 9045D MMSD 150952-1
11/06/21 WMC45/21022555 6.31 Stnd. Units 0.1 SW846: 9045D MMSD 150952-1
11/13/21 WMC46/21022746 6.29 Stnd. Units 0.1
SW846: 9045D
MMSD 151251-1
11/20/21 WMC47/21023216 6.29 Stnd. Units 0.1
SW846: 9045D
MMSD 151251-1
Page 110 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FP fLER+fR ix�lE HERE
Milorganite Weekly Composite
pH -Solids
Sample Date Sample ID
Result
LOD LOQ QA Flags na Ica e o
QC Batch
ID
11/27/21
WMC48/21023901
6.35 Stnd. Units
0.1
SW846: 9045D
MMSD
151251-1
12/04/21
WMC49/21024741
6.26 Stnd. Units 0.1
SW846: 9045D
MMSD 151929-1
12/11/21 WMC50/21025262
6.17 Stnd. Units 0.1
SW846: 9045D
MMSD 151929-1
12/18/21 WMC51/21025623 6.23 Stnd. Units 0.1
12/25/21 WMC52/21026035 6.22 Stnd. Units 0.1
Avg Result: 6.2 Stnd. Units Min LOD: 0.1 Stnd. Units
PHOSPHORUS ICP Dry wt.
SW846: 9045D
MMSD 151929-1
SW846: 9045D
MMSD 151929-1
Max Result: 6.52 Stnd. Units Max LOD: 0.1 Stnd. Units
Sample Dat- Sample ID
Result
LOD LOQ QA Flags
Analytical Method Lab
QC Batch
ID
09/11/21
WMC37/21017714
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
150517-1
10/09/21
W MC41 /21019807
28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151576-1
11/13/21 WMC46/21022746
28000 mg/kg D.W. 23 89 S5.
SW846: 6010C
MMSD 151576-1
12/11/21 WMC50/21025262 29000 mg/kg D.W. 23 89
Avg Result: 28000 mg/kg D.W. Min LOD: 23 mg/kg D.W.
SW846: 6010C
MMSD 151576-1
Max Result: 30000 mg/kg D.W. Max LOD: 24 mg/kg D.W.
Page 111 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEll FL CLER+fR ix�l4[iINERE
Milorganite Weekly Composite
Solids (% Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/02/21
W MC01 /21000078
6.2
0.1
SM 2540 G (1997)
MMSD
01/16/21
W MC03/21000799
6% 0.1
SM 2540 G (1997) MMSD
01/23/21 WMC04/21001061
6.1 % 0.1
SM 2540 G (1997) MMSD
01/30/21 WMC05/21001319
5.7 % 0.1
SM 2540 G (1997) MMSD
02/06/21 WMC06/21001491
5.9 % 0.1
SM 2540 G (1997) MMSD
02/13/21 WMC07/21001740 4.8 % 0.1
SM 2540 G (1997) MMSD
02/20/21 WMC08/21002074 5.2 % 0.1
SM 2540 G (1997) MMSD
02/27/21 WMC09/21002480 5.5 % 0.1
SM 2540 G (1997) MMSD
03/06/21 WMC10/21002860 4.5 % 0.1 SM 2540 G (1997) MMSD
03/13/21 WMC11/21003556
5%
0.1
SM 2540 G (1997) MMSD
03/20/21 WMC12/21004095 4.8 % 0.1 SM 2540 G (1997) MMSD
03/27/21 WMC13/21004287 5.2 % 0.1 SM 2540 G (1997) MMSD
04/03/21 WMC14/21004661 5.5 % 0.1 SM 2540 G (1997) MMSD
04/10/21 WMC15/21005026 5.7 % 0.1 SM 2540 G (1997) MMSD
04/17/21 WMC16/21005483 5.4 % 0.1 SM 2540 G (1997) MMSD
04/24/21 WMC17/21006274 5.3 % 0.1 SM 2540 G (1997) MMSD
05/01/21 WMC18/21006444 4.5 % 0.1 SM 2540 G (1997) MMSD
05/08/21 WMC19/21006996 4.9 % 0.1 SM 2540 G (1997) MMSD
05/15/21 WMC20/21007343 5.1 % 0.1 SM 2540 G (1997) MMSD
05/22/21 WMC21/21008087
5.6 % 0.1
SM 2540 G (1997) MMSD
05/29/21 WMC22/21008532 5 % 0.1 SM 2540 G (1997) MMSD
06/05/21 WMC23/21009289 5 % 0.1 SM 2540 G (1997) MMSD
06/12/21 WMC24/21009604 5.2 % 0.1 SM 2540 G (1997) MMSD
06/19/21 WMC25/21010334
5.6 % 0.1
SM 2540 G (1997) MMSD
06/26/21 WMC26/21010809
5.3 % 0.1
SM 2540 G (1997) MMSD
07/03/21 WMC27/21011518 5.4 % 0.1 SM 2540 G (1997) MMSD
07/10/21 WMC28/21012257 4.7 % 0.1 SM 2540 G (1997) MMSD
07/17/21 WMC29/21012598 4.3 % 0.1 SM 2540 G (1997) MMSD
07/24/21 WMC30/21013393 5.1 % 0.1 SM 2540 G (1997) MMSD
07/31/21 WMC31/21013754 4.7 % 0.1 SM 2540 G (1997) MMSD
08/07/21 WMC32/21014720 5 % 0.1 SM 2540 G (1997) MMSD
08/14/21 WMC33/21015332 4.6 % 0.1 SM 2540 G (1997) MMSD
08/21/21 WMC34/21016198
3.6 % 0.1
SM 2540 G (1997) MMSD
08/28/21 WMC35/21016442 4.8 % 0.1 SM 2540 G (1997) MMSD
09/04/21 WMC36/21017070 4.6 % 0.1 SM 2540 G (1997) MMSD
09/11/21 WMC37/21017714 5.4 % 0.1 SM 2540 G (1997) MMSD 149896-1
09/18/21 WMC38/21018140 5.3 % 0.1 SM 2540 G (1997) MMSD 150039-1
09/25/21 WMC39/21019025 4.8 % 0.1
SM 2540 G (1997)
MMSD 150169-1
10/02/21 WMC40/21019399 4.2 % 0.1 SM 2540 G (1997) MMSD 150294-1
10/09/21 WMC41/21019807 4.6 % 0.1
SM 2540 G (1997)
MMSD 150419-1
10/23/21 WMC43/21021036 4.1 % 0.1 SM 2540 G (1997) MMSD 150673-1
10/30/21 WMC44/21021576 4.8 % 0.1 SM 2540 G (1997) MMSD 150796-1
11/06/21 WMC45/21022555 4.9 % 0.1 SM 2540 G (1997) MMSD 150902-1
11/13/21 WMC46/21022746 6 % 0.1 S5. SM 2540 G (1997) MMSD
11/20/21 WMC47/21023216 5.5 % 0.1
SM 2540 G (1997)
MMSD 151138-1
11/27/21 WMC48/21023901 6.2 % 0.1
SM 2540 G (1997)
MMSD 151230-1
Page 112 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEfd FL fLER+fR ixilE HERE
Milorganite Weekly Composite
Solids (0 Moisture)
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o.
QC Batch
ID
12/04/21
WMC49/21024741
5.3
0.1
SM 2540 G (1997)
MMSD
151365-1
12/11/21
WMC50/21025262
6% 0.1
SM 2540 G (1997)
MMSD 151485-1
12/18/21 WMC51/21025623
5.7 % 0.1
SM 2540 G (1997)
MMSD 151597-1
12/25/21 W MC52/21026035
6.6 % 0.1
SM 2540 G (1997)
MMSD 151706-1
Min LOD: 0.1 %
Solids (% Volatile)
Max LOD: 0.1 0/0
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
W MCO2/21000596
73 % 0.1 S5. SM 2540 G (1997)
MMSD
02/13/21
W MC07/21001740
74 % 0.1 S5. SM 2540 G (1997) MMSD
03/13/21 WMC11/21003556
75 % 0.1
SM 2540 G (1997) MMSD
04/10/21 WMC15/21005026
74% 0.1
SM 2540 G (1997) MMSD
05/08/21 WMC19/21006996
74% 0.1
SM 2540 G (1997) MMSD
06/12/21 WMC24/21009604 71 % 0.1
SM 2540 G (1997) MMSD
07/10/21 WMC28/21012257
69 % 0.1
SM 2540 G (1997) MMSD
08/07/21 WMC32/21014720
69 % 0.1
SM 2540 G (1997) MMSD
09/11/21 WMC37/21017714
68% 0.1
SM 2540 G (1997) MMSD 149895-1
10/09/21 WMC41/21019807 70 0/0 0.1
SM 2540 G (1997) MMSD 150420-1
11/13/21 WMC46/21022746
72 % 0.1
SM 2540 G (1997)
MMSD 151005-1
12/11/21 WMC50/21025262
73 % 0.1
SM 2540 G (1997)
MMSD 151486-1
Avg Result: 72 %
Solids (% Total)
Min LOD: 0.1 %
Max Result: 75 0/0
Max LOD: 0.1 %
Sample Dat= Sample ID Result LOD LOQ QA Flags
Analytical Method
Lab
QC Batch
ID
01/09/21
W MCO2/21000596
94 % 0.1 55. SM 2540 G (1997)
MMSD
02/13/21
W MC07/21001740
95 % 0.1 55. SM 2540 G (1997)
MMSD
Avg Result: 94 %
Phosphorus - Water Extractable
Min LOD: 0.1 0/0
Max Result: 98 0/0
Max LOD: 0.1 0/0
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
W MCO2/21000596
0.015 % of Total P
0
WDNR Guidance
MMSD
02/13/21
W MC07/21001740
0.017%ofTotalP 0
WDNR Guidance
MMSD
03/13/21 WMC11/21003556
0.018%ofTotalP 0
WDNR Guidance MMSD
04/10/21 WMC15/21005026 0.016 % of Total P 0
WDNR Guidance MMSD
05/08/21 WMC19/21006996 0.019 % of Total P 0
WDNR Guidance MMSD
06/12/21 WMC24/21009604 0.017 % of Total P 0
WDNR Guidance MMSD
07/10/21 WMC28/21012257 0.013 % of Total P 0
WDNR Guidance MMSD
08/07/21 WMC32/21014720 0.01 % of Total P 0
WDNR Guidance MMSD
09/11/21 WMC37/21017714 0.017 % of Total P 0 WDNR Guidance MMSD
10/09/21 WMC41/21019807 0.011 % of Total P 0 WDNR Guidance MMSD
11/13/21 WMC46/21022746 0.014 % of Total P 0 WDNR Guidance MMSD
12/11/21 WMC50/21025262 0.018 % of Total P 0 WDNR Guidance MMSD
Avg Result: 0.015 % of Total P Min LOD: 0 % of Total P
Max Result: 0.019 % of Total P Max LOD: 0 % of Total P
SYS/rptlMiloMonthlyDW 10/21/21 tj
Page 113 of 121
Printed: 1/13/2214:24

MMSD
PIRNEfd FP CEER+fR ix�l4[iIHERE
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Page 114 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tl Printed: 1/13/22 14:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARRIEfd FL CLER+fR ix�lE HERE
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
Sample Date Sample ID
Result
LOD LOQ QA Flags na Ica e o
QC Batch
ID
01/05/21
21000710
19 MPN/g TS
0.2
EPA 1680
MMSD
01/12/21
21001371
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
01/19/21 21001822
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
01/26/21 21002195
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
02/02/21 21002507
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
02/09/21 21002800
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
02/16/21 21003494
0.21 MPN/g TS 0.19
EPA 1680 MMSD
02/23/21 21003853
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/02/21 21004350
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/09/21 21004569
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/16/21 21004992
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/23/21 21005822
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/30/21 21006155
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
04/13/21 21006930
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
04/20/21 21007414 < 0.2 MPN/g TS 0.2
EPA 1680 MMSD
04/27/21 21008161
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/04/21 21008583
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/11/21 21009267
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/18/21 21009703
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/25/21 21010237
< 0.18 MPN/g TS 0.18
EPA 1680 MMSD
06/01/21 21010778 < 1.9 MPN/g TS 1.9
AO. EPA 1680 MMSD
06/08/21 21011270
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
06/22/21 21012528
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
06/29/21 21013172
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/06/21 21013781
< 0.19 MPN/g TS 0.19
Q2.
EPA 1680 MMSD
07/13/21 21014462
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/20/21 21015226
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/27/21 21015938
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/03/21 21016520 1.9 MPN/g TS 1.9
EPA 1680 MMSD
08/10/21 21017148
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/24/21 21018406
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/31/21 21018961
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
09/07/21 21019296 140 MPN/g TS 1.9
EPA 1680 MMSD
09/14/21 21019839
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150008-1
09/21/21 21020475
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150137-1
09/28/21 21021002
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150249-1
10/20/21 21022830
< 0.18 MPN/g TS 0.18
EPA 1680
MMSD 150687-1
10/26/21 21023248
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150774-1
11/09/21 21024070
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150983-1
11/16/21 21024363
14 MPN/g TS 0.19
EPA 1680
MMSD 151105-1
11/23/21 21024720
< 0.2 MPN/g TS 0.2
EPA 1680
MMSD 151250-1
11/30/21 21025009
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151323-1
12/07/21 21025371
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151459-1
12/14/21 21025593
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151598-1
12/21/21 21026062
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151713-1
12/28/21 21026149
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151781-1
Page 115 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PIRNEE CLER+fR ix�l4[iIHERE
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
Sample Date Sample ID Result LOD LOQ QA Flags
e o
QC Batch
ID
Min LOD: 0.18 MPN/g TS
Max LOD: 1.9 MPN/g TS
Page 116 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/22 14:24

MMSD
PARNEfd FP CLER+fR ix�l4[iINERE
Solids (% Total)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Outfall 006) PRODUCTION
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/05/21
21000710
91%
0.1
SM 2540 G (1997)
MMSD
01/12/21
21001371
94% 0.1
SM 2540 G (1997) MMSD
01/19/21 21001822
94% 0.1
SM 2540 G (1997) MMSD
01/26/21 21002195
93% 0.1
SM 2540 G (1997) MMSD
02/02/21 21002507
95% 0.1
SM 2540 G (1997) MMSD
02/09/21 21002800
95% 0.1
SM 2540 G (1997) MMSD
02/16/21 21003494
94% 0.1
SM 2540 G (1997) MMSD
02/23/21 21003853 96 % 0.1
SM 2540 G (1997) MMSD
03/02/21 21004350 96 % 0.1 SM 2540 G (1997) MMSD
03/09/21 21004569 94 % 0.1 SM 2540 G (1997) MMSD
03/16/21 21004992
96 % 0.1
SM 2540 G (1997) MMSD
03/23/21 21005822
96% 0.1
SM 2540 G (1997) MMSD
03/30/21 21006155 94 % 0.1 SM 2540 G (1997) MMSD
04/13/21 21006930
95 % 0.1
SM 2540 G (1997) MMSD
04/20/21 21007414 91 % 0.1 SM 2540 G (1997) MMSD
04/27/21 21008161
96 % 0.1
SM 2540 G (1997) MMSD
05/04/21 21008583 95 % 0.1 SM 2540 G (1997) MMSD
05/11/21 21009267 94 % 0.1 SM 2540 G (1997) MMSD
05/18/21 21009703 94 % 0.1 SM 2540 G (1997) MMSD
05/25/21 21010237 97 % 0.1 SM 2540 G (1997) MMSD
06/01/21 21010778
96 % 0.1
SM 2540 G (1997) MMSD
06/08/21 21011270
96% 0.1
SM 2540 G (1997) MMSD
06/22/21 21012528 95 % 0.1 SM 2540 G (1997) MMSD
06/29/21 21013172
96% 0.1
SM 2540 G (1997) MMSD
07/06/21 21013781
95 % 0.1
SM 2540 G (1997) MMSD
07/13/21 21014462 96 % 0.1 SM 2540 G (1997) MMSD
07/20/21 21015226 95 % 0.1 SM 2540 G (1997) MMSD
07/27/21 21015938
96% 0.1
SM 2540 G (1997) MMSD
08/03/21 21016520
96% 0.1
SM 2540 G (1997) MMSD
08/10/21 21017148 96 % 0.1 SM 2540 G (1997) MMSD
08/24/21 21018406
96% 0.1
SM 2540 G (1997) MMSD
08/31/21 21018961
96% 0.1
SM 2540 G (1997) MMSD
09/07/21 21019296
96% 0.1
SM 2540 G (1997) MMSD
09/14/21 21019839 96 % 0.1
SM 2540 G (1997)
MMSD 149919-1
09/21/21 21020475 95 % 0.1 SM 2540 G (1997) MMSD 150073-1
09/28/21 21021002 96 % 0.1 SM 2540 G (1997) MMSD 150186-1
10/20/21 21022830 98 % 0.1 SM 2540 G (1997) MMSD 150588-1
10/26/21 21023248 97 % 0.1 SM 2540 G (1997) MMSD 150695-1
11/09/21 21024070 95 % 0.1 SM 2540 G (1997) MMSD 150928-1
11/16/21 21024363 95 % 0.1
SM 2540 G (1997)
MMSD 151030-1
11/23/21 21024720 90 % 0.1 SM 2540 G (1997) MMSD 151161-1
11/30/21 21025009 96 % 0.1 SM 2540 G (1997) MMSD 151264-1
12/07/21 21025371 93 % 0.1
SM 2540 G (1997)
MMSD 151388-1
12/14/21 21025593 95 % 0.1
SM 2540 G (1997)
MMSD 151514-1
12/21/21 21026062 94 % 0.1
SM 2540 G (1997)
MMSD 151632-1
12/28/21 21026149 94 % 0.1
SM 2540 G (1997)
MMSD 151708-1
Page 117 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PAR11181 FP CLER+fR ix�lE HERE
Milorganite (Outfall 006) PRODUCTION
Solids (% Total)
Sample Date Sample ID
Result LOD LOQ QA Flags ' e o
QC Batch
ID
Avg Result: 95 %
FECAL COLIFORM SLUDGE
Min LOD: 0.1 "/o
Max Result: 98 0/0
Max LOD: 0.1 %
Milorganite (Outfall 009) BAGGING
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/05/21
02/09/21
03/09/21
21000712
21002802
21004571
1.4 MPN/g TS
0.19
EPA 1680
MMSD
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
04/13/21 21006932
1.1 MPN/g TS 0.19
EPA 1680 MMSD
05/11/21 21009269
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
06/08/21 21011272
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
07/13/21 21014464
2.1 MPN/g TS 1.9 Q2. EPA 1680
MMSD
08/17/21 21017789
14 MPN/g TS 0.19
EPA 1680
MMSD
08/24/21 21018407
0.47 MPN/g TS 0.19
EPA 1680
MMSD
09/14/21 21019841
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150008-1
10/26/21 21023250
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150774-1
11/09/21 21024074
< 1.9 MPN/g TS 1.9
EPA 1680
MMSD 150983-1
12/14/21 21025597
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151598-1
Min LOD: 0.19 MPN/g TS
Solids (0 Total)
Max LOD: 1.9 MPN/g TS
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/05/21
21000712
95
0.1
SM 2540 G (1997)
MMSD
02/09/21
21002802
94% 0.1
SM 2540 G (1997) MMSD
03/09/21 21004571
95 % 0.1
SM 2540 G (1997) MMSD
04/13/21 21006932
94% 0.1
SM 2540 G (1997) MMSD
05/11/21 21009269
95% 0.1
SM 2540 G (1997) MMSD
06/08/21 21011272
95% 0.1
SM 2540 G (1997) MMSD
07/13/21 21014464
94% 0.1
SM 2540 G (1997) MMSD
08/17/21 21017789
95 % 0.1
SM 2540 G (1997) MMSD
08/24/21 21018407
95 % 0.1
SM 2540 G (1997) MMSD
09/14/21 21019841
95% 0.1
SM 2540 G (1997)
MMSD 149919-1
10/26/21 21023250
96 % 0.1
SM 2540 G (1997) MMSD 150695-1
11/09/21 21024074
95% 0.1
SM 2540 G (1997) MMSD 150928-1
12/14/21 21025597
96 % 0.1 SM 2540 G (1997) MMSD 151514-1
Avg Result: 95 0/0
Min LOD: 0.1 0/0
Max Result: 98 % Max LOD: 0.1 %
Page 118 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

faR111Efd ft � LIEktERKilolEllf
FECAL COLIFORM SLUDGE
01/05/21 21000711
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Outfall 008) SHIPPING
QC Batch
ID
2.1 MPN/g TS 1.9
EPA 1680 MMSD
02/09/21 21002801
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
03/09/21 21004570
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
04/13/21 21006931
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/11/21 21009268
< 0.19 MPN/g TS 0.19
Q3.
EPA 1680 MMSD
06/08/21 21011271
1.4 MPN/g TS 0.19
EPA 1680 MMSD
07/13/21 21014463
0.47 MPN/g TS 0.19
EPA 1680 MMSD
08/10/21 21017149
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
09/21/21 21020476
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150137-1
10/26/21 21023249
1.1 MPN/g TS 0.19
EPA 1680
MMSD 150774-1
11/09/21 21024073
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150983-1
12/14/21 21025595
< 0.19 MPN/g TS 0.19
EPA 1680
Min LOD: 0.19 MPN/g TS
Solids (% Total)
MMSD 151598-1
Max LOD: 1.9 MPN/g TS
Sample Date Sample ID
Result
LOD LOQ QA Flags
Analytical Method Lab
QC Batch
ID
01/05/21
21000711
95
0.1
SM 2540 G (1997)
MMSD
02/09/21
21002801
94% 0.1
SM 2540 G (1997) MMSD
03/09/21 21004570
95 % 0.1
SM 2540 G (1997) MMSD
04/13/21 21006931
94 % 0.1
SM 2540 G (1997) MMSD
05/11/21 21009268
06/08/21 21011271
07/13/21 21014463
95% 0.1
SM 2540 G (1997) MMSD
95% 0.1
SM 2540 G (1997) MMSD
96% 0.1
SM 2540 G (1997) MMSD
08/10/21 21017149
96% 0.1
SM 2540 G (1997) MMSD
09/21/21 21020476 95 0/0 0.1
SM 2540 G (1997) MMSD 150073-1
10/26/21 21023249
96% 0.1
SM 2540 G (1997) MMSD 150695-1
11/09/21 21024073
96% 0.1
SM 2540 G (1997) MMSD 150928-1
12/14/21 21025595 95 0/0 0.1
SM 2540 G (1997)
MMSD 151514-1
Avg Result: 95 % Min LOD: 0.1 0/0
Max Result: 98 % Max LOD: 0.1 0/0
Page 119 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARNEE FL LI.EktERKilolEllf
Milorganite (Spring Valley) BAGGING
FECAL COLIFORM SLUDGE
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Metho.
QC Batch
ID
01/26/21
21002185
0.21 MPN/g TS
0.19
EPA 1680
MMSD
03/09/21
21004562
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
04/13/21 21006927
4.9 MPN/g TS 0.19
EPA 1680
MMSD
05/11/21 21009233
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
06/08/21 21011242
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/13/21 21014418
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/10/21 21017140
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
09/14/21 21019846
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150008-1
10/26/21 21023242
< 1.9 MPN/g TS 1.9
EPA 1680
MMSD 150774-1
12/07/21 21025357
12/14/21 21025590
Solids (% Total)
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151459-1
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151598-1
Min LOD: 0.19 MPN/g TS
Max LOD: 1.9 MPN/g TS
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/26/21
21002185
94 %
0.1
SM 2540 G (1997)
MMSD
03/09/21
21004562
95% 0.1
SM 2540 G (1997) MMSD
04/13/21 21006927
95% 0.1
SM 2540 G (1997) MMSD
05/11/21 21009233
95 % 0.1
SM 2540 G (1997) MMSD
06/08/21 21011242
95 % 0.1
SM 2540 G (1997) MMSD
07/13/21 21014418
08/10/21 21017140
09/14/21 21019846
95% 0.1
SM 2540 G (1997) MMSD
96% 0.1
SM 2540 G (1997) MMSD
95% 0.1
SM 2540 G (1997)
MMSD 149919-1
10/26/21 21023242
96 % 0.1
SM 2540 G (1997) MMSD 150695-1
12/07/21 21025357
95% 0.1
SM 2540 G (1997)
MMSD 151388-1
12/14/21 21025590
96 % 0.1 SM 2540 G (1997) MMSD 151514-1
Avg Result: 95 %
Min LOD: 0.1 "/o
Max Result: 98 % Max LOD: 0.1 %
Page 120 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

Annual Milorganite Report DW
January 1 to December 31, 2021
E' 1111Efd Hit CLEifR (11'0114.1101W
Flag Descriptions
AO Other -- Flag requires additional explanation.
IS Insufficient sample volume for analysis.
AX Qualified data - see contract laboratory report.
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits.
Di Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed beyond holding time.
] Estimated concentration above the adjusted method detection limit
and below the adjusted Limit of Quantification.
LA Not analyzed - laboratory accident.
M1 Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data (Water Quality only).
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5
S6
Reading was not confirmed by a constant weight measurement.
Dried solid residue yield outside of method specifications (<2.5mg
or >200mg).
SD Supplemental details provided (Water Quality only).
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
T5 GGA BOD was above method acceptance criteria.
T6 Sample supersaturated with dissolved oxygen for BOD analysis.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 121 of 121
SYS/rptlMiloMonthlyDW 10/21/21 tj Printed: 1/13/2214:24

�!�MMSD
PARTNERS FOR A CLEANER ENVIRONMENT
January 13, 2022
TO:
FROM:
COPY:
SUBJECT:
Memorandum
Tom Nowicki and Steve Unger
Zach Vogel
Laboratory Project Manager
S. Mertens, A. Sotomayor, E. Guyant, K. Walden, E. Stroik, P. Bechler, Lab File
2021 Annual Milorganite PCB Report
Attached is the Annual PCB Milorganite report for the year 2021. Daily Milorganite samples are 24-hour
composite samples, representative of a full day of production. All analyses were performed by Pace Analytical
Services, Inc. in Green Bay, WI (Wisconsin Certification #: 405132750). Full laboratory results are available upon
request.
There was no Milorganite production on the following dates:
• May 24, 2021
• May 31, 2021
• June 15 through June 17, 2021
• August 29, 2021
• October 5, 2021
• October 9 through October 18, 2021
Data/Report Review By:
I-13.2 2z
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PrR_1M7 DrR_17SA PrR_1771 DrR_17Q7 PrR_1'MR DrR_17F,n PrR_1MF. Tntal PrR Arnrinrc
1/1/21 < 32 32 < 32 < 32 < 32 < 32 < 32 32
1/2/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
1/3/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
1/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/5/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/6/21 < 32 36 < 32 < 32 < 32 < 32 < 32 36
1/7/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
1/8/21 < 32 41 < 32 < 32 < 32 < 32 < 32 41
1/9/21 < 33 47 < 33 < 33 < 33 < 33 < 33 47
1/10/21 < 33 40 < 33 < 33 < 33 < 33 < 33 40
1/11/21 < 32 42 < 32 < 32 < 32 < 32 < 32 42
1/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/16/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
1/17/21 < 33 34 < 33 < 33 < 33 < 33 < 33 34
1/18/21 < 33 35 < 33 < 33 < 33 < 33 < 33 35
1/19/21 < 33 39 < 33 < 33 < 33 < 33 < 33 39
1/20/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/22/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/23/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/24/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/25/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/26/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/29/21 < 32 40 < 32 < 32 < 32 < 32 < 32 40
1/30/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
1/31/21 < 33 45 < 33 < 33 < 33 < 33 < 33 45
2/1/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
2/2/21 < 32 40 < 32 < 32 < 32 < 32 < 32 40
2/3/21 < 32 36 < 32 < 32 < 32 < 32 < 32 36
2/4/21 < 32 41 < 32 < 32 < 32 < 32 < 32 41
2/5/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39
2/6/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
2/7/21 <31 41 <31 <31 <31 <31 <31 41
2/8/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/10/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/12/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
2/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/16/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/17/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PrR_1M7 DrR_17SA PrR_1771 DrR_17Q7 PrR_1'MR DrR_17F,11 PrR_1niA Tntal PrR Arnrinrc
2/18/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
2/19/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/20/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/22/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/25/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
2/26/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/8/21 < 32 40 < 32 < 32 < 32 < 32 < 32 40
3/9/21 < 32 36 < 32 < 32 < 32 < 32 < 32 36
3/10/21 < 32 32 < 32 < 32 < 32 < 32 < 32 32
3/11/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
3/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/16/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
3/17/21 < 32 49 < 32 < 32 < 32 < 32 < 32 49
3/18/21 < 32 36 < 32 < 32 < 32 < 32 < 32 36
3/19/21 < 32 53 < 32 < 32 < 32 < 32 < 32 53
3/20/21 < 32 54 < 32 < 32 < 32 < 32 < 32 54
3/21/21 < 32 50 < 32 < 32 < 32 < 32 < 32 50
3/22/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
3/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/25/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
3/26/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
3/27/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
3/28/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
3/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/30/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/31/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PrR_1M7 DrR_17SA PrR_1771 D('R_1747 PrR_1'MR DrR_17F,f1 PrR_1niA Tntal PrR Arnrinrc
4/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/8/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/10/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/13/21 < 32 42 < 32 < 32 < 32 < 32 < 32 42
4/14/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
4/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/16/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/17/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/18/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
4/19/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
4/20/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
4/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/22/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/25/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/26/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/30/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/8/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/10/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
5/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/16/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/17/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
5/18/21 < 32 < 32 < 32 < 32 < 32 55 < 32 55
5/19/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
5/20/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
5/21/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
5/22/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
5/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/25/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PrR_1M7 DrR_17SA PrR_1771 DrR_17Q7 PrR_1'MR DrR_17F,11 PrR_1niA Tntal PrR Arnrinrc
5/26/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/30/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/8/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
6/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/10/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/13/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
6/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/18/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/19/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/20/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/22/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/25/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
6/26/21 < 33 48 < 33 < 33 < 33 < 33 < 33 48
6/27/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
6/28/21 < 32 40 < 32 < 32 < 32 36 < 32 75
6/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/30/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
7/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/2/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
7/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/6/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
7/7/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39
7/8/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
7/9/21 41 37 < 32 < 32 < 32 < 32 < 32 78
7/10/21 39 34 < 32 < 32 < 32 < 32 < 32 73
7/11/21 40 34 < 32 < 32 < 32 < 32 < 32 74
7/12/21 36 43 < 32 < 32 < 32 < 32 < 32 79
7/13/21 41 34 < 32 < 32 < 32 < 32 < 32 74
7/14/21 60 37 < 32 < 32 < 32 < 32 < 32 97
7/15/21 51 42 < 32 < 32 < 32 < 32 < 32 92
7/16/21 45 35 < 32 < 32 < 32 < 32 < 32 80

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016 Total PCB Aroclor,
7/17/21 49 39 < 32 < 32 < 32 < 32 < 32 88
7/18/21 58 38 < 32 < 32 < 32 < 32 < 32 96
7/19/21 67 47 < 32 < 32 < 32 < 32 < 32 110
7/20/21 79 73 < 32 < 32 < 32 < 32 < 32 150
7/21/21 80 59 < 32 < 32 < 32 < 32 < 32 140
7/22/21 86 55 < 32 < 32 < 32 < 32 < 32 140
7/23/21 71 49 < 32 < 32 < 32 < 32 < 32 120
7/24/21 88 54 < 32 < 32 < 32 < 32 < 32 140
7/25/21 96 56 < 32 < 32 < 32 < 32 < 32 150
7/26/21 100 52 < 32 < 32 < 32 < 32 < 32 160
7/27/21 96 56 < 32 < 32 < 32 < 32 < 32 150
7/28/21 100 64 < 32 < 32 < 32 < 32 < 32 170
7/29/21 100 56 < 32 < 32 < 32 < 32 < 32 160
7/30/21 93 56 < 32 < 32 < 32 < 32 < 32 150
7/31/21 120 59 < 32 < 32 < 32 < 32 < 32 180
8/1/21 93 54 < 32 < 32 < 32 < 32 < 32 150
8/2/21 120 74 < 32 < 32 < 32 < 32 < 32 190
8/3/21 110 54 < 32 < 32 < 32 < 32 < 32 160
8/4/21 110 53 < 32 < 32 < 32 < 32 < 32 160
8/5/21 110 58 < 32 < 32 < 32 < 32 < 32 160
8/6/21 100 50 < 32 < 32 < 32 < 32 < 32 150
8/7/21 110 49 < 32 < 32 < 32 < 32 < 32 160
8/8/21 92 44 < 32 < 32 < 32 < 32 < 32 140
8/9/21 120 72 < 32 < 32 < 32 < 32 < 32 190
8/10/21 97 64 < 32 < 32 < 32 < 32 < 32 160
8/11/21 120 80 < 32 < 32 < 32 33 < 32 230
8/12/21 110 100 < 32 < 32 < 32 < 32 < 32 220
8/13/21 99 70 < 32 < 32 < 32 < 32 < 32 170
8/14/21 86 70 < 31 < 31 < 31 < 31 < 31 160
8/15/21 85 71 < 31 < 31 < 31 < 31 < 31 160
8/16/21 95 60 < 31 < 31 < 31 < 31 < 31 160
8/17/21 82 59 < 31 < 31 < 31 < 31 < 31 140
8/18/21 73 72 < 31 < 31 < 31 35 < 31 180
8/19/21 70 62 < 32 < 32 < 32 34 < 32 160
8/20/21 120 68 < 32 < 32 < 32 < 32 < 32 190
8/21/21 120 80 < 32 < 32 < 32 < 32 < 32 200
8/22/21 130 84 < 32 < 32 < 32 < 32 < 32 220
8/23/21 130 92 < 32 < 32 < 32 < 32 < 32 220
8/24/21 140 110 < 32 < 32 < 32 44 < 32 300
8/25/21 120 93 < 32 < 32 < 32 < 32 < 32 220
8/26/21 110 82 < 32 < 32 < 32 < 32 < 32 190
8/27/21 100 94 < 32 < 32 < 32 < 32 < 32 200
8/28/21 100 100 < 32 < 32 < 32 < 32 < 32 200
8/30/21 89 51 < 32 < 32 < 32 35 < 32 180
8/31/21 57 61 < 32 < 32 < 32 < 32 < 32 120
9/1/21 77 84 < 32 < 32 < 32 < 32 < 32 160
9/2/21 61 65 < 32 < 32 < 32 < 32 < 32 130
9/3/21 65 61 < 32 < 32 < 32 < 32 < 32 130

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016 Total PCB Aroclor,
9/4/21 55 69 < 32 < 32 < 32 < 32 < 32 120
9/5/21 52 60 < 32 < 32 < 32 < 32 < 32 110
9/6/21 57 60 < 32 < 32 < 32 < 32 < 32 120
9/7/21 87 71 < 32 < 32 < 32 < 32 < 32 160
9/8/21 88 88 < 32 < 32 < 32 < 32 < 32 180
9/9/21 82 68 < 32 < 32 < 32 < 32 < 32 150
9/10/21 59 57 < 32 < 32 < 32 < 32 < 32 120
9/11/21 53 58 < 32 < 32 < 32 < 32 < 32 110
9/12/21 46 54 < 32 < 32 < 32 < 32 < 32 100
9/13/21 40 53 < 32 < 32 < 32 < 32 < 32 93
9/14/21 45 55 < 32 < 32 < 32 < 32 < 32 100
9/15/21 32 48 < 32 < 32 < 32 < 32 < 32 80
9/16/21 88 78 < 32 < 32 < 32 < 32 < 32 170
9/17/21 51 52 < 33 < 33 < 33 < 33 < 33 100
9/18/21 52 55 < 32 < 32 < 32 < 32 < 32 110
9/19/21 36 55 < 32 < 32 < 32 < 32 < 32 91
9/20/21 60 70 < 32 < 32 < 32 < 32 < 32 130
9/21/21 79 61 < 32 < 32 < 32 < 32 < 32 140
9/22/21 57 48 < 32 < 32 < 32 < 32 < 32 100
9/23/21 57 65 < 32 < 32 < 32 < 32 < 32 120
9/24/21 61 75 < 32 < 32 < 32 < 32 < 32 140
9/25/21 54 71 < 32 < 32 < 32 < 32 < 32 120
9/26/21 79 100 < 56 < 56 < 56 < 56 < 56 180
9/27/21 56 70 < 32 < 32 < 32 < 32 < 32 130
9/28/21 56 69 < 32 < 32 < 32 < 32 < 32 120
9/29/21 58 69 < 32 < 32 < 32 < 32 < 32 130
9/30/21 53 71 < 32 < 32 < 32 < 32 < 32 120
10/1/21 38 50 < 32 < 32 < 32 < 32 < 32 88
10/2/21 37 52 < 32 < 32 < 32 < 32 < 32 89
10/3/21 63 86 < 32 < 32 < 32 < 32 < 32 150
10/4/21 79 98 < 32 < 32 < 32 < 32 < 32 180
10/6/21 46 82 < 32 < 32 < 32 32 < 32 160
10/7/21 43 74 < 32 < 32 < 32 < 32 < 32 120
10/8/21 50 71 < 31 < 31 < 31 < 31 < 31 120
10/19/21 <31 38 <31 <31 <31 <31 <31 38
10/20/21 49 42 < 32 < 32 < 32 < 32 < 32 91
10/21/21 < 32 40 < 32 < 32 < 32 < 32 < 32 40
10/22/21 32 38 < 32 < 32 < 32 < 32 < 32 70
10/23/21 < 32 42 < 32 < 32 < 32 < 32 < 32 42
10/24/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
10/25/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
10/26/21 34 44 < 32 < 32 < 32 < 32 < 32 78
10/27/21 < 32 35 < 32 < 32 < 32 < 32 < 32 35
10/28/21 < 32 32 < 32 < 32 < 32 < 32 < 32 32
10/29/21 41 36 < 32 < 32 < 32 42 < 32 120
10/30/21 41 40 < 32 < 32 < 32 48 < 32 130
10/31/21 44 43 < 32 < 32 < 32 46 < 32 130
11/1/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PrR_1M7 DrR_17SA PrR_1771 DrR_17Q7 PrR_1'MR DrR_17F,n PrR_1niA Tntal PrR Arnrinrc
11/2/21 < 33 55 < 33 < 33 < 33 < 33 < 33 55
11/3/21 < 32 56 < 32 < 32 < 32 < 32 < 32 56
11/4/21 < 32 53 < 32 < 32 < 32 < 32 < 32 53
11/5/21 < 32 47 < 32 < 32 < 32 < 32 < 32 47
11/6/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
11/7/21 < 32 52 < 32 < 32 < 32 < 32 < 32 52
11/8/21 33 44 < 32 < 32 < 32 < 32 < 32 77
11/9/21 < 32 43 < 32 < 32 < 32 < 32 < 32 43
11/10/21 < 33 59 < 33 < 33 < 33 < 33 < 33 59
11/11/21 < 33 65 < 33 < 33 < 33 < 33 < 33 65
11/12/21 < 32 57 < 32 < 32 < 32 < 32 < 32 57
11/13/21 < 32 61 < 32 < 32 < 32 < 32 < 32 61
11/14/21 < 32 55 < 32 < 32 < 32 < 32 < 32 55
11/15/21 < 32 35 < 32 < 32 < 32 < 32 < 32 35
11/16/21 < 32 47 < 32 < 32 < 32 < 32 < 32 47
11/17/21 < 32 85 < 32 < 32 < 32 < 32 < 32 85
11/18/21 < 32 58 < 32 < 32 < 32 < 32 < 32 58
11/19/21 38 65 < 32 < 32 < 32 < 32 < 32 100
11/20/21 < 32 63 < 32 < 32 < 32 < 32 < 32 63
11/21/21 < 32 57 < 32 < 32 < 32 < 32 < 32 57
11/22/21 < 33 56 < 33 < 33 < 33 < 33 < 33 56
11/23/21 < 33 49 < 33 < 33 < 33 < 33 < 33 49
11/24/21 < 32 47 < 32 < 32 < 32 < 32 < 32 47
11/25/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
11/26/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
11/27/21 < 33 41 < 33 < 33 < 33 < 33 < 33 41
11/28/21 < 32 48 < 32 < 32 < 32 < 32 < 32 48
11/29/21 < 32 49 < 32 < 32 < 32 < 32 < 32 49
11/30/21 < 32 47 < 32 < 32 < 32 < 32 < 32 47
12/1/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
12/2/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
12/3/21 < 32 48 < 32 < 32 < 32 < 32 < 32 48
12/4/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
12/5/21 < 33 45 < 33 < 33 < 33 < 33 < 33 45
12/6/21 < 32 50 < 32 < 32 < 32 < 32 < 32 50
12/7/21 < 33 43 < 33 < 33 < 33 < 33 < 33 43
12/8/21 < 32 43 < 32 < 32 < 32 < 32 < 32 43
12/9/21 < 33 36 < 33 < 33 < 33 < 33 < 33 36
12/10/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39
12/11/21 < 32 35 < 32 < 32 < 32 < 32 < 32 35
12/12/21 <31 40 <31 <31 <31 <31 <31 40
12/13/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
12/14/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
12/15/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
12/16/21 < 32 48 < 32 < 32 < 32 < 32 < 32 48
12/17/21 < 32 50 < 32 < 32 < 32 < 32 < 32 50
12/18/21 < 32 48 < 32 < 32 < 32 < 32 < 32 48
12/19/21 < 33 41 < 33 < 33 < 33 < 33 < 33 41

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016 Total PCB Aroclor,
12/20/21 35 45 < 33 < 33 < 33 < 33 < 33 80
12/21/21 34 36 < 33 < 33 < 33 < 33 < 33 71
12/22/21 36 34 < 33 < 33 < 33 < 33 < 33 70
12/23/21 < 33 58 < 33 < 33 < 33 < 33 < 33 58
12/24/21 < 33 50 < 33 < 33 < 33 < 33 < 33 50
12/25/21 < 33 53 < 33 < 33 < 33 < 33 < 33 53
12/26/21 < 33 50 < 33 < 33 < 33 < 33 < 33 50
12/27/21 < 32 48 < 32 < 32 < 32 < 32 < 32 48
12/28/21 < 32 35 < 32 < 32 < 32 < 32 < 32 35
12/29/21 < 33 41 < 33 < 33 < 33 < 33 < 33 41
12/30/21 < 32 38 < 32 < 32 < 32 < 32 < 32 38
12/31/21 < 32 42 < 32 < 32 < 32 < 32 < 32 42
'Samples analyzed by Pace Analytical Services, Green Bay, Wisconsin (WI Certification #405132750) by EPA 8082. All
results reported on a dry weight basis.

flMK5D
PAIRS FDh 0.111111110
964
3/20/21
Sample Data
SU
Site Coda
WMC12
Cwtomer ID
Milorganite Priority Pollutants: Spring 2021
Milo. Priority Pollutant Sample
21004580
LIMS Number
OpSID Test Name Reported Value
MDL
LOQ
Flags Analysis Date Method
Lab
S
1253
1315 1,2-Diphenylhydrazine Dry wt
1234 2,4,6-Trl hlorophenol Dry wt.
1,2,4-Trichlorobenzene Dry wt.
< 1200 ug/kg D.W.
< 960 ug/kg D.W.
< 1700 ug/kg D.W.
1200
17000
3/26/21 8270D
960 17000
1700 8600
3/26/21 8270D
Test America B 3
Test America B 3
3/26/21 8270D
Test America B 3
1226 2,4-Dichiorophenol Dry wt < 910 ug/kg D.W. 910 8600
3/26/21 8270D
1227 2,4-Dimethylphenol Dry wt. < 2100 ug/kg D.W. 2100 8600
1229 2,4-Dinitrophenol Dry wt < 40000 ug/kg D.W. 40000 84000
1252 2,4-Dinitrotoluene Dry wt. < 1800 ug/kg D.W. 1800 8600
3/26/21 8270D
Test America B 3
Test America B 3
3/26/21 8270D
Test America B 3
1317 2,6-Dlnitrotoluene Dry Wt. < 1000 ug/kg D.W. 1000 8600
3/26/21 8270D
3/26/21 8270D
1249 2-Chloronaphthalene Dry wt. < 1400 ug/kg D.W. 1400 8600
1225 2-Chlorophenot Dry wt.
Test America B 3
Test America B 3
3/26/21 8270D
Test America B 3
< 1600 ug/kg D.W. 1600 17000
3/26/21 8270D
Test America B 3
1230 2-Nitraphenol Dry wt
1324 3,3.-DIchlorobenzidine Dry wt
1260 4,4-DDD Dry wt
< 2400 ug/kg D.W.
< 10000 ug/kg D.W.
2400 8600
10000 17000
3/26/21 8270D
Test America B 3
3/26/21 8270D
< 6.7 ug/kg D.W. 6.7
35
3/29/21 8081E
Test America B 3
Test America B 3
1259 4,4-DDE Dry wt.
< 7.3 ug/kg D.W, 7.3
35
3/29/21 80818
1258 4,4-DDT Dry wt
< 8.1 ug/kg D.W. 8.1
35
Test America B 3
3/29/21 80818
1228
1247
1250
1231
1254
1235
1318
1304
4,6-Dlnibo-o-Cresol Dry wt < 8600 ug/kg D.W.
8600 17000
4-Bromopherryl Phenyl Ether Dry wt < 1200 ug/kg D.W. 1200 8600
4-Chloro-phenyl-phenyl ether Dry wt< 1100 ug/kg D.W. 1100 8600
4-Nitrophenol Dry wt. < 6000 ug/kg D.W.
Test America B 3
3/26/21 8270D
3/26/21 8270D
3/26/21 8270D
6000 17000
A-BHC-Alpha Dry wt. < 6.2 ug/kg D.W. 6.2 35
Acenaphthene Dry wt. < 1300 ug/kg D.W. 1300 8600
Acenaphthylene Dry wt
Aldrin Dry wt.
< 1100 ug/kg D.W.
< 8.5 ug/kg D.W.
524 ALUMINUM ICP Dry wt.
1236 Anthraoene Dry wt.
545
525
1255
1237
1238
1239
1240
1241
1242
528
1256
1243
1244
1245
1246
526
3200 mg/kg D.W.
< 2100 ug/kg D.W.
3/26/21 8270D
3/29/21 8081B
3/26/21 8270D
1100
8.5
4.4
8600
35
10
3/26/21 8270D
3/29/21 80818
Test America B 3
Test America 8 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
AX.
4/6/21 6010C
2100 8600
ANTIMONY ICP Dry wt
< 0.4 mg/kg D.W. 0.4 15
ARSENIC ICP Dry wt
3 mg/kg D.W. 0.4 2
B-BHC-Bela Dry wt
Benzldine Dry WL
Benzo(a)Anthracene Dry wt.
Benzo(a)Pyrene Dry wt.
< 6.2 ug/kg D.W. 6.2 35
3/26/21 8270D
Test America B 3
Test America B 3
4/6/21 6010C
Test America B 3
4/6/21 6010C
Test America B 3
3/29/21 80818
< 110000 ug/kg D.W. 110000 250000
3/26/21 8270D
< 860 ug/kg D.W. 860 8600
< 1300 ug/kg D.W. 1300 8600
Benzo(b)Fluoranthene Dry Wt.
< 1400 ug/kg D.W. 1400 8600
3/26/21 8270D
3/26/21 8270D
3/26/21 8270D
Benzo(g,h,i)Perylene Dry wt. < 910 ug/kg D.W.
910 8600
Benzo(k)Ruaranthene Dry wt < 1100 ug/kg D.W.
1100 8600
BERYLLIUM ICP Dry Wt. 0.063 mg/kg D.W.
BHC-Delta Dry wt. < 6.4 ug/kg D.W.
81s(2-Chloroethoxy)Methane Dry wt < 1800 ug/kg D.W.
0.028
6.4
1800
0.2
35
8600
3/26/21 8270D
3/26/21 8270D
4/6/21 6010C
Test America B 3
Test America 8 3
Bls(2-Cribroethyl)Ether Dry Wt. < 1100 ug/kg D.W. 1100 8600
3/29/21 8081E
3/26/21 8270D
Bis(2-Chlorolsopropyl)Ether Dry wt. < 1700 ug/kg D.W.
Bls(2-Ethythexyl)Phthatate Dry wt. 7800 ug/kg D.W.
BORON ICP Dry wt. 14 mg/kg D.W.
1700 8600
3/26/21 8270D
3/26/21 8270D
2900 8600
0.19
1248 Butyl Benzyl Phthalate Dry wt.
530 CADMIUM ICP Dry wt.
529 CALCIUM ICP Dry wt
SYS6pt5Genartc3 411/14 #
2
< 1400 ug/kg D.W. 1400 8600
< 0.03 mg/kg D.W. 0.03 0.2
I
3/26/21 8270D
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
Test America B 3
Test America B 3
14000 mg/kg D.W. 3.3
50
4/6/21 6010C
Test America B 3
Test America B 3
Test America 8 3
3/26/21 8270D
Test America B 3
M.
4/6/21 6010C
Test America B 3
4/6/21 6010C
Test America B 3
Page 1 of 4
Prhied: Mal 12:45

�MMSD
iiallal IOU CUM MOW
Milorganite Priority Pollutants: Spring 2021
1305 CNordane Dry wt. < 77 ug/kg D.W. 77 350 3/29/21 8081E
532 CHROMIUM ICP Dry wt. 210 mg/kg D.W. 0.2 0.5 4/6/21 6010C
1251 Chrysene Dry wt. < 1900 ug/kg D.W. 1900 8600 3/26/21 8270D
531 COBALT ICP Dry wt. 2.5 mg/kg D.W. 0.05 0.5 4/6/21 6010C
533 COPPER ICP Dry wt. 180 mg/kg Q.W. 0.21 1 4/6/21 6010C
263 Cyanide - Total (solids) 4.4 mg/kg D.W. 0.45 0.94 3/30/21 90126
1325 Dibenzo(a,h)Anthracene Dry wt. < 1500 ug/kg D,W. 1500 8600 3/26/21 8270D
1306 Diekirin Dry wt. < 8.3 ug/kg D.W. 8.3 35 3/29/21 8081E
1314 Diethyl Phthalate Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D
1328 Dimethyl Phthalate Dry wt. < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D
1320 Di-n-Butyfphthalate Dry wt. < 1500 ug/kg D.W. 1500 8600 3/26/21 8270D
1323 Di-n-octyl phthalate Dry wt. 2100 ug/kg D.W. 1000 8600 ] 3/26/21 8270D
1261 Endosulfan alpha Dry wt. < 6.6 ug/kg D.W. 6.6 35 3/29/21 808113
1262 Endosulfan beta Dry wt. < 6.2 ug/kg D.W. 6.2 35 3/29/21 80818
Test America B -
Test America B
Test America B I
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B
Test America B
Test America 8
Test America 8
wiwlwlw
Test America 8 3
Test America B 3
Test America B 3
1263 Endosulfan Sulfate Dry wt. < 6.5 ug/kg D.W. 6.5 35 3/29/21 8081E Test America B 3
1265 Endrin Aldehyde Dry wt. < 8.8 ug/kg D.W. 8.8 35 3/29/21 80818 Test America 8 3
1264 Endrfn Dry wt. < 6.9 ug/kg D.W. 6.9 35 3/29/21 80818 Test America B 3
1321 Fluoranthene Dry wt. < 910 ug/kg D.W. 910 8600 3/26/21 8270D Test America 8 3
1316 Fluorene Dry wt. < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D Test America B 3
1266 Heptachlor Dry wt. < 7.5 ug/kg D.W. 7.5 35 3/29/21 8081B Test America B 3
1267 Heptachtarepoxide Dry cat. < 8.9 ug/kg D.W. 8.9 35 3/29/21 80816 Test America B 3
1330 Hexachlorobenzene Dry wt. < 1200 ug/kg D.W. 1200 8600 3/26/21 8270D Test America B 3
1327 Hexachlorobutadiene Dry wt. < 1300 ug/kg D.W. 1300 8600 3/26/21 8270D Test America B 3
1308 Hexachlorocyclopentadlene Dry wt. < 1200 ug/kg D.W. 1200 8600 3/26/21 8270D Test America B 3
1329 Hexachloroethane Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
1326 Indeno(1,2,3-cd)Pyrene Dry Wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
534 IRON ICP Dry wt. 34000 mg/kg D.W. 3.5 10 4/6/21 6010C Test America B 3
1311 Isophorone Dry wt. < 1800 ug/kg D.W. 1800 8600 3/26/21 8270D Test America B 3
544 LEAD ICP Dry wt. 17 mg/kg DN. 0.24 1 4/6/21 6010C Test America B 3
538 _ MAGNESIUM ICP Dry wt. 3600 mg/kg D.W. 0.93 20 AX. 4/6/21 6010C Test America B 3
539 MANGANESE ICP Dry wt. 890 mg/kg D.W. 0.032 0.2 AX. 4/6/21 6010C Test America B 3
428 MERCURY by M. 7471(sludge) 0.12 mg/kg D.W. 0.015 0.038 AX. 3/25/21 74718 Test America B 3
540 MOLYBDENUM ICP Dry wt. 7.2 mg/kg D.W. 0.13 1 4/6/21 6010C Test America 8 3
1312 Naphthalene Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
542 NICKEL ICP Dry wt. 20 mg/kg D.W. 0.23 5 4/6/21 6010C Test America B 3
1310 Nitrobenzene Dry wt. < 960 ug/kg D.W. 960 8600 3/26/21 8270D Test America B 3
1307 N-Nltrosodlmethylamine Dry wt. < 3900 ug/kg D.W. 3900 17000 3/26/21 _ _ 8270D Test America B 3
1309 N-Nitrosodl-n-propylamine Dry wt. < 1500 ug/kg DN. 1500 8600 3/26/21 8270D Test America B 3
1313 N-Nitrosodiphenylamfne Dry wt. < 7000 ug/kg D.W. 7000 8600 3/26/21 8270D Test America B 3
678 PCB-1016 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
674 PCe-1221 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
675 PCB-1232 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
672 PCB-1242 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
676 PCB-1248 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
673 PCB-1254 < 0.22 mg/kg D.W. 0.22 0.47 3/28/21 8082A Test America B 3
677 PCB-1260 < 0.22 mg/kg D.W. 0.22 0.47 3/28/21 8082A Test America B 3
1224 p-Chloro-m-Cresol Dry wt. < 2100 ug/kg D.W. 2100 8600 3/26/21 8270D Test America B 3
1232 Pentachlorophenol Dry wt. < 8600 ug/kg D.W. 8600 17000 3/26/21 8270D Test America B 3
1319 Phenanthrene Dry Wt. < 1300 ug/kg D.W. 1300 8600 3/26/21 8270D Test America B 3
1233 Phenol Dry wt. < 1300 ug/kg D.W. 1300 8600 3/26/21 8270D Test America B 3
Page 2 of 4
SYSJrpI5Generk3 4/11f14 6 Printed• 7i9/21 12;15

IHMSD
MIMS InAQHn NEM
Milorganite Priority Pollutants: Spring 2021
543 PHOSPHORUS ICP Dry wt. 15000 mg/kg D.W. 140 360 AX, 4/6/21 SM 4500 P E Test America B 3
536 POTASSIUM ICP Dry wt. 3200 mg/kg D.W. 20 30 AX. 4/6121 6010C Test America B 3
1322 Pyrene Dry wt < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D Test America B 3
546 SELENIUM ICP Dry wt. 5.7 mg/kg D.W. 0.4 4 4/6/21 6010C Test America B 3
523 SILVER ICP Dry wt. 1,8 mg/kg D.W. 0.2 0.6 4/6/21 6010C Test America B 3
541 SODIUM ICP Dry wt. 1300 mg/kg D.W. 13 140 4/6/21 6010C Test America B 3
550 THALLIUM ICP Dry wt. < 0.3 mg/kg D.W. 0.3 6 4/6/21 6010C Test America B 3
697 Total PCB Arodors < 0.22 mg/kg D.W. 0.22 0.47 3/28/21 8082A Test America B 3
1268 Toxaphene Dry wt. < 200 ug/kg D.W. 200 350 3/29/21 8081B Test America B 3
1257 Y-BHC-Gamma(Undane) Dry wt. < 6.4 ug/kg D.W. 6.4 35 3/29/21 80818 Test America B 3
260 mg/kg D.W. 0.64 2 4/6/21 6010C Test America B 3
552
ZINC ICP Dry wt.
3/22121
Sample Date
SU
21004581
UMS Number
OpSID Test Name Reported Value r.1LIL. I I r. Analysis Date Method I ,111 b
1341 1,1,1-Trichloroethane Dry wt. < 27 ug/kg D.W. 27 99 3/27/21 8260C Test America 8 3
1350 1,1,2,2-Tet adttoroethane Dry wt < 16 ug/kg D.W. 16 99 3/27/21 8260C Test America B 3
1348 1,1,2-Trk hloroetlwne Dry wt < 21 ug/kg D.W. 21 99 3/27/21 8260C Test America B 3
1338 1,1-Dichbroethane Dry wt. < 31 ug/kg DN. 31 99 3/27/21 8260C Test America B 3
1336 1,1-Dichbroethyiene Dry wt. < 34 ug/kg D.W. 34 99 3/27/21 8260C Test America B 3
1355 1,2-Dlchlorobenzene Dry Wt. < 25 ug/kg D.W. 25 99 3/27/21 8260C Test America B 3
1340 1,2-Didibroeihane Dry wt. < 40 ug/kg D.W. 40 99 3/27/21 8260C Test America B 3
1222 1,2-Dichloropropane Dry wt. < 16 ug/kg D, W. 16 99 3/27/21 8260C Test America B 3
1356 1,3-Dichlorobenzene Dry Wt < 26 ug/kg D.W. 26 99 3/27/21 8260C Test America B 3
1357 1,4-Dlchlorobenzene Dry Wt < 14 ug/kg D.W. 14 99 3/27/21 8260C Test America B 3
Site Code
Customer ID
1337 2-Chloroetlrylvinyl Ether Dry wt. < 32 ug/kg D.W. 32 490 3/27/21 8260C Test America B 3
1334 Acrolein Dry wt < 200 ug/kg D.W. 200 490 3/27/21 8260C Test America/3 3
1335 Aaybnlirlle Dry wt. < 250 ug/kg D.W. 250 490 3/27/21 8260C Test America 8 3
1346 Benzene Dry wt. < 19 ug/kg D.W. 19 99 3/27/21 8260C Test America B 3
1343 Bromodlchloromethane Dry wt < 20 ug/kg D.W. 20 99 3/27/21 8260C Test America B 3
1219 8romcform Dry wt < 49 ug/kg D.W. 49 99 3/27/21 8260C Test America B 3
1342 Carbon Tetrachloride Dry wt < 25 ug/kg D.W. 25 99 3/27/21 8260C Test America B 3
1352 Chlorobenzene Dry wt. < 13 ug/kg D.W. 13 99 3/27/21 8260C Test America B 3
1220 Chloroethane Dry wt. < 21 ug/kg D.W. 21 99 3/27/21 8260C Test America B 3
1339 Chloroform Dry wt. < 68 ug/kg D.W. 68 99 3/27/21 8260C Test America B 3
1344 cis-1,3-Dichloropropene Dry wt. < 24 ug/kg D.W. 24 99 3/27/21 8260C Test America B 3
1347 Dibromochloromethane Dry wt. < 48 ug/kg D.W. 48 99 - 3/27/21 8260C Test America B 3
1353 Ethyibenzene Dry wt. < 29 ug/kg O.W. 29 99 3/27/21 8260C Test America B 3
1331 Methyl Bromide Dry wt. < 22 ug/kg D.W. 22 99 3/27/21 8260C Test America 8 3
1354 Methyl Chloride dry wt. < 24 ug/kg D.W. 24 99 3/27/21 8260C Test America B 3
1333 Methylene Chloride Dry wt. < 20 ug/kg D.W. 20 99 3/27/21 8260C Test America B 3
1349 Tetrachloroethylene Dry wt < 13 ug/kg D.W. 13 99 3/27/21 8260C Test America B 3
1351 Toluene Dry wt 120 ug/kg D.W. 26 99 3/27/21 8260C Test America B 3
1221 Trans-1,2-Dichbroethyiene Dry wt < 23 ug/kg D.W. 23 99 3/27/21 8260C Test America B 3
1223 Trans-1,3-Dichbropropene Dry wt < 9.7 ug/kg D.W. 9.7 99 3/27/21 8260C Test America B 3
1345 Trichloroethytene Dry wt. < 27 ug/kg D.W. 27 99 3/27/21 8260C Test America B 3
1332 Vinyl Chloride Dry wt
SYSApt5Generie3 Ui 1/14
< 33 ug/kg D.W. 33 99 3/27/21 8260C Test America B 3
Page 3014
Printed.: 7.9121 12:45

Milorganite Priority Pollutants: Spring 2021
IIADM la HIM Of111 filt10
** The MDL for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
*** The LOQ for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
Column S: Test Status. Not Started=8, Intermediate=7, Final-3, Analyst Approved 12, Not Reportable=15.
Fls&Des erleions
AO Other — Hag requires additional explanation.
AX Qualified data • see contract laboratory report.
B3 Target analyte detected In method blank > 10% of sample
concentration. - -
B7 LC'S recovery was above control limits.
Be LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits.
Di Duplicate precision control rmlt was exceeded.
02 Matrix spike precision control limit was exceeded. _
03 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not Mow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected. _
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time- _
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed beyond holding time.
SYShpf5Generic3 4/1 //14 f
137
IS Insufficient sample volume for analysis.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit.
LA Not analyzed - laboratory accident.
Mi Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies . unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements.
M7
M9
NR
NU
P2
02
Q
RT
S5
SD
T3
T4
T5
Ti
:re
T9
Microbiology sample received without adequate headspace.
Target organism detected in associated method blank.
Not usable data (Water Quality only.
Not usable Data.
Sample received with Improper or inadequate chemical preservation.
Matrix spike recovery for this sample was above control limits.
3 Matrix spike recovery for this sample was below control limits_
Sampletemperature upon receipt exceeded regulatory or project
requirements.
Reading was not confirmed by a constant weight measurement
Supplemental details provided (Water Quality only).
The SOD dilution water D.O. depletion was > 0.2 mg/L.
GGA BOD was below method acceptance criteria.
GGA BOD was above method acceptance criteria.
The BOD dilution water D.O. Increase was > 0.2 mg/L.
Sample matrix did not allow adtlustin9 sample pH for BOD.
Sample Is outside of the prescribed method temperature range.
Pepa4of4
Printed- 7/9/2i 1245

S
PNIMOICLIR1Fit Mt
964
9/11/21
Sample Date
SU
Site Code
WMC37
Customer ID
Milorganite Priority Pollutant: Fall 2021
September 5 to 11, 2021
Milo. Priority Pollutant Sample
21019080
LIMS Number
OpSID Test Name
Reported Value
MDL LOQ Flags Analysis Date Method
Lab S
1253 1,2,4-Trichlorobenzene Dry wt.
1315 1,2-DIphenyfhydrazine Dry wt.
1234 2,4,6•Trichbrophenol Dry wt.
< 250 ug/kg D.W.
< 200 ug/kg D.W.
250
3500
200 3500
< 360 ug/kg D.W. 360 1800
1226 2,4-Dichlorophenol Dry wt.
1227 2,4-Dimethyiphenol Dry wt.
1229 2,4-Dinitrophenol Dry wt.
< 190 ug/kg D.W. 190 1800
< 430 ug/kg D.W.
< 8200 ug/kg D.W.
430 1800
8200 17000
9/21/21
8270D
9/21/21 82700
9/21/21 8270D
1252 2,4-Dinitrotoluene Dry wt.
< 370 ug/kg D.W. 370 1800
1317 2,6-Dinftrotoluene Dry wt.
< 210 ug/kg D.W. 210 1800
1249 2-Chicronaphthalene Dry wt.
< 290 ug/kg D.W. 290 1800
1225 2-Cribrophenol Dry wt.
1230 2-Nltrophenol Dry wt.
1324 3,3'-Dlchlorobenzldlne Dry wt.
< 330 ug/kg D.W.
< 500 ug/kg D.W.
330 3500
500 1800
< 2100 ug/kg D.W. 2100 3500
1260 4,4-DDD Dry wt
1259 4,4-DDE Dry wt
1258 4,4-DOT Dry cat
< 6.6 ug/kg D.W. 6.6
34
< 7.2 ug/kg D.W. 7.2 34
< 8 ug/kg D.W. 8 34
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/20/21 8081B
9/20/21 8081E
9/20/21 80818
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
1228 4,6-Dinitro-o-Cresol Dry wt < 1800 ug/kg D.W.
1247 4-Bromophenyt Phenyl Ether Dry wt < 250 ug/kg D.W.
1250 4 Chloro-phenyl-phenyl ether Dry wt < 220 ug/kg D.W.
1231 4-Nltrophenol Dry wt. < 1200 ug/kg D.W.
1800 3500
250 1800
9/21/21 8270D
9/21/21 8270D
220 1800
9/21/21 8270D
1200 3500
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
9/21/21 8270D
Test America B 3
1254
1235
1318
1304
524
A BHC-Alpha Dry cat.
Acenaphthene Dry wt.
Acenaphthylene Dry wt
Aldrin Dry wt
ALUMINUM ICP Dry wt
1236 Anthracene Dry wt.
< 6.2 ug/kg D.W.
< 260 ug/kg D.W.
< 230 ug/kg D.W.
6.2 34
260 1800
230 1800
< 8.4 ug/kg D.W.
6500 mg/kg D.W.
< 440 ug/kg D.W.
545 ANTIMONY ICP Dry wt.
8.4 34
4.6 10
440 1800
< 0.42 mg/kg D.W. 0.42
16
525 ARSENIC 1CP Dry wt.
4.9 mg/kg D.W. 0.42 2.1
1255 B-BHC-Beta Dry wt.
1237 Benzidlne Dry wt.
< 6.2 ug/kg D.W. 6.2 34
< 22000 ug/kg D.W. 22000 53000
9/20/21 8081E
9/21/21 8270D
9/21/21 8270D
9/20/21 8081E
9/23/21 6010C
9/21/21 8270D
9/21/21 6010C
9/21/21 6010C
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
9/20/21 8081B
9/21/21 8270D
Test America B 3
Test America B 3
1238 Benzo(a)Anttvacene Dry wt
1239 Benzo(a)Pyrene Dry wt.
< 180 ug/kg D.W. 180 1800
< 260 ug/kg D.W. 260 1800
9/21/21 8270D
1240 Benzo(b)Fluoranthene Dry wt.
1241 Benzo(g,h,f)Perylene Dry wt.
1242 Benzo(k)Fluoranthene Dry wt.
528 BERYLLIUM ICP Dry wt.
1256 BHC Delta Dry wt
600 ug/kg D.W. 280 1800
< 190 ug/kg D.W. 190 1800
< 230 ug/kg D.W.
0.15 mg/kg D.W.
< 6.4 ug/kg D.W.
230 1800
0.029 0.21
6.4 34
3
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
3
9/21/21 6010C
9/20/21 80818
1243 8ls(2-Chbroethaxy)Methane Dry wt.
1244 Bls(2-Chioroethyl)Ethher Dry wt.
1245 Bls(2-Chlorolsopropyl)Ether Dry wt.
1246 Bls(2-Ethythexyl)Phthalate Dry wt.
526 BORON ICP Dry cat.
< 380 ug/kg D.W.
< 230 ug/kg D.W.
< 360 ug/kg D.W.
6300 ug/kg D.W.
380 1800
9/21/21 8270D
Test America B 3
Test America B 3
Test America B 3
230 1800
9/21/21 8270D
Test America B 3
Test America B 3
Test America B 3
360 1800
610 1800
21 mg/kg D.W. 0.2
2.1
9/21/21
9/21/21
9/21/21
8270D
8270D
6010C
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
1248 Butyl Benzyl Phthalate Dry wt.
530 CADMIUM ICP Dry wt
529 CALCIUM ICP Dry wt.
SYShpl5Generk3 4/11114 0
< 290 ug/kg D.W. 290 1800
0.74 mg/kg D.W. 0.031 0.21
9/21/21 8270D
9/21/21 6010C
24000 mg/kg D.W. 3.5 52 AX. 9/21/21 6010C
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Page 1 o13
Printed: 11/24r21 14:22

NMSD
PIATNEAS 1011 CLEIMII Eyli1E191811
Milorganite Priority Pollutant: Fall 2021
September 5 to 11, 2021
1305 Chlordane Dry wt. < 76 ug/kg D.W. 76 340 9/20/21 8081E Test America B 3
532 CHROMIUM ICP Dry wt. 260 mg/kg D.W. 0.21 0.52 9/21/21 6010C Test America B 3
1251 Chrysene Dry wt. < 400 ug/kg D.W. 400 1800 9/21/21 8270D Test America B 3
531 COBALT ICP Dry wt 4.1 mg/kg D.W. 0.052 0.52 9/21/21 6010C Test America B 3
533 COPPER ICP Dry wt 240 mg/kg D.W. 0.22 1 9/21/21 6010C Test America B 3
263 Cyanide - Total (solids) < 2.3 mg/kg D.W. 2.3 4.7 9/16/21 90128 Test America B 3
1325 Dibenzo(a,h)Anthracene Dry wt. < 320 ug/kg D.W. 320 1800 9/21/21 8270D Test America B 3
1306 Dieldrin Dry wt. < 8.2 ug/kg D.W. 8.2 34 9/20/21 8081E Test America B 3
1314 Diethyl Phthalate Dry wt. < 230 ug/kg D.W. 230 1800 9/21/21 8270D Test America B 3
1328 Dlmethyl Phthalate Dry wt. < 210 ug/kg D.W. 210 1800 9/21/21 8270D Test America B 3
1320 Di-n-Butylphthalate Dry wt. < 300 ug/kg D.W. 300 1800 9/21/21 8270D Test America B 3
1323 Dl-n-octyl phthalate Dry wt. < 210 ug/kg D.W. 210 1800 9/21/21 8270D Test America B 3
1261 Endosulfan alpha Dry wt. < 6.6 ug/kg D.W. 6.6 34 9/20/21 80818 Test America B 3
1262 Endosulfan beta Dry wt. < 6.2 ug/kg D.W. 6.2 34 9/20/21 80818 Test America B 3
1263 Endosulfan Sulfate Dry wt. 23 ug/kg D.W. 6.4 34 3 _ 9/20/21 8081E Test America B 3
1265 Endrin Aldehyde Dry wt. < 8.7 ug/kg D.W. 8.7 34 9/20/21 8081E Test America B 3
1264 Endrin Dry wt. < 6.8 ug/kg D.W. 6.8 34 9/20/21 80816 Test America B 3
1321 Fluoranthene Dry wt. 640 ug/kg D.W. 190 1800 3 9/21/21 8270D Test America B 3
1316 Fluorene Dry wt. < 210 ug/kg D.W. 210 1800 9/21/21 8270D Test America B 3
1266 Heptachlor Dry wt. < 7.4 ug/kg D.W. - 7.4 34 9/20/21 8081B Test America 8 3
1267 Heptachlorepoxide Dry wt. < 8.8 ug/kg D.W. 8.8 34 9/20/21 8081E Test America B 3
1330 Hexachlorobenzene Dry wt. < 240 ug/kg D.W. 240 1800 9/21/21 8270D Test America B 3
1327 Hexachlorobutadlene Dry wt. < 260 ug/kg D.W. 260 1800 9/21/21 8270D Test America B 3
1308 Hexadrlorocydopentadlene Dry wt < 240 ug/kg D.W. 240 1800 9/21/21 8270D Test America B 3
1329 Hexachloroethane Dry wt < 230 ug/kg D.W. 230 1800 9/21/21 8270D Test America B 3
1326 lndeno(1,2,3-cd)Pyrene Dry Wt. < 220 ug/kg D.W. 220 1800 9/21/21 8270D Test America B 3
534 IRON ICP Dry wt. 42000 mg/kg D.W. 3.7 10 9/21/21 6010C Test America B 3
1311 Isaphorone Dry wt. < 380 ug/kg D.W. 380 1800 9/21/21 8270D Test America B 3
544 LEAD ICP Dry wt. 51 mg/kg D.W. 0.25 1 9/21/21 6010C Test America B 3
538 MAGNESIUM ICP Dry wt. 8600 mg/kg D.W. 0.97 21 9/21/21 6010C Test America B 3
539 MANGANESE ICP Dry wt. 1200 mg/kg D.W. 0.033 0.21 9/21/21 6010C Test America B 3
428 MERCURY by M. 7471 (sludge) 0.28 mg/kg D.W. 0.0048 0.021 9/20/21 7471B Test America B 3
540 MOLYBDENUM ICP Dry wt. 11 mg/kg D.W. 0.14 1 9/21/21 6010C Test America B 3
1312 Naphthalene Dry wt. < 230 ug/kg D.W. 230 1800 9/21/21 8270D Test America B 3
542 NICKEL ICP Dry wt. 29 mg/kg D.W. 0.24 5.2 9/21/21 6010C Test America B 3
1310 Nitrobenzene Dry wt. < 200 ug/kg D.W. 200 1800 9/21/21 8270D Test America B 3
1307 N-Nltrosodimet ylamine Dry wt. < 760 ug/kg D.W. 760 3500 9/21/21 8270D Test America B 3
1309 N-Nltrosodi-n-propylamine Dry wt. < 300 ug/kg D.W. 300 1800 9/21/21 8270D Test America B 3
1313 N-Nitrosodiphenylamine Dry wt. < 1400 ug/kg D.W. 1400 1800 9/21/21 8270D Test America B 3
678 PCB-1016 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
674 PCB-1221 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
675 PCB-1232 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
672 PCB-1242 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
676 PCB-1248 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
673 PCB-1254 < 0.098 mg/kg D.W. 0.098 0.21 9/16/21 8082A Test America B 3
677 PC8-1260 < 0.098 mg/kg D.W. 0.098 0.21 9/16/21 8082A Test America B 3
1224 p- hloro-m-Cresol Dry wt. < 440 ug/kg D.W. 440 1800 9/21/21 8270D Test America B 3
1232 Pentadrlorophenol Dry wt. < 1800 ug/kg D.W. 1800 3500 9/21/21 8270D Test America B 3
1319 Phenanthrene Dry wt. < 260 ug/kg D.W. 260 1800 9/21/21 8270D Test America B 3
1233 Phenol Dry wt < 270 ug/kg D.W. 270 1800 9/21/21 8270D Test America B 3
SYS✓rpt5Genedc3 4/11/14 U
Page 2 of 3
Printed: 11/24 21 14.22

&MMSD
tiifill 311A MIDI IDIOM
Milorganite Priority Pollutant: Fall 2021
September 5 to 11, 2021
543 PHOSPHORUS ICP Dry wt. 23000 mg/kg D.W. 150 360
536 POTASSIUM ICP Dry wt.
3200 mg/kg D.W. 21 31
1322 Pyrene Dry wt
546 SELENIUM ICP Dry wt.
530 ug/kg D.W. 210 1800
9/21/21 SM 4500 P E
9/21/21 6010C
] 9/21/21 8270D
2.4 mg/kg D.W. 0.42 4.2
523 SILVER ICP Dry wt 2.3 mg/kg D.W. 0.21 0.63
] 9/21/21 6010C
9/21/21 6010C
Test America S 3
Test America B 3
541 SODIUM ICP Dry wt
1500 mg/kg D.W. 14 150
1187 Solids for dry weight determination (T 95 %
Ink friar
1187 Solids for dry weight determination (r 94 %
550 THALLIUM ICP Dry wt
AX. 9/21/21 6010C
Test America B 3
Test America B 3
Test America B 3
Test America B 3
9/23/21 Moisture Test America B 3
9/21/21 Moisture Test America B 3
< 0.31 mg/kg D.W. 0.31 6.3
9/21/21 6010C Test America B 3
697 Total PCB Arodors < 0.098 mg/kg D.W. 0.098 0.21
1268 Toxaphene Dry wt < 200 ug/kg D.W. 200 340
9/16/21 8082A Test America B 3
9/20/21 80818 Test America B 3
1257 Y-BHC-Gamma(Undane) Dry wt. < 6.3 ug/kg D.W. 6.3 34
552 ZINC ICP Dry wt 510 mg/kg D.W. 0.67 2.1
** The MDL for this test is the lowest level of predsion shown, example: 4.1 would be "0.1".
*** The LOQ for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test
9/20/21 8081E Test America B 3
9/21/21 6010C Test America B 3
Column S: Test Status. Not Started=8, Intermediate=7, Rnal=3, AnalystApproved=12, Not Reportable=15.
107
Grp Descriptions
AO
AX
B3
B7
B8
B9
Di
D2
D3
Other — Flag requires additional explanation.
Qualified data - see contract laboratory report,
Target analyte detected in method blank > 10% of sample
concentration.
LCS recovery was above control limits. _
LCS recover was below control limits.
Low Level CO/ recovery was outside of method aolaptance limits.
Duplicate precision control limit was exceeded.
Matrix spike precision control limit was exceeded.
Sample Is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the anaty%.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received peat holding time.
H3 Analysis performed beyond holdirritime.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holdifl time.
MS Analysis performed be rm holding time.
SYShpt5Genark3 Ui 1/r1 a
IS Insufficient sample volume for anaim.
7 Estimated concentration above the adjusted method detection limit
and below the adtusted reporting limit
u Not arrpl d - laboratory accident
141 Too numerous to count
M2 Sample Incubation ppifod outside method requirement
M3 Spreading colonies - unable to determine result.
M4 Results are an alp .duration due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adeo uate 7oeadspace.
M9 Target organism detected in associated method blank.
NR Not usable data QVtraterlll)rp,
NU Not usable Data.
P2 Sample received with borrow or inadequate chemical preeervaltpn.
Q2 Matrix spike riTallY for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or Project
regidrement5.
S5 Reading was not confirmed try a constant weight measurement
56 Dried solid residue yield outside of method spedfiwtlor>s (<2.5mg
or >2000gJ.
SD Supplemental details prodded (Water QwNly cr .
13 The BOD diulon water D.O. dlpletipn was > 0.2 mg/L.
T4 GGA BOD was below method aoeeptance criteria.
T3 GGA BOD was above method acceptance criteria.
T6 Sample supersaturated with dissolved oxlgen for BOD analyda.
T7 The BOD dilution water D.O. increase was > 0.2 wok.
TO Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the mooted method temperature fence.
Page 3of3
Pentad: 11/24/21 14:22

MM5D
(MI5 I1i11 Cllh i milig1110r
964
9113/21
Sample Date
SU
Site Code
Milorganite Priority Pollutant: Fall 2021
September 13, 2021
Customer ID
Milo. Priority Pollutant Sample
21O19081
LIMS Number
OpSID Test Name Reported Value MDL i O .I Analysis Date Method Lab S
1341 1,1,1-Trichioroethane Dry wt.
< 23 ug/kg D.W. 23
1350 1,1,2,2-Tetrachloroethane Dry wt. < 13 ug/kg D.W. 13
1348 1,1,2-Trichloroethane Dry wt. < 17 ug/kg D.W. 17 82
1338 1,1-Dichloroethane Dry wt. < 25 ug/kg D.W. 25 82
1336 1,1-Dichloroethylene Dry wt. < 29 ug/kg D.W. 29 82
1355 1,2-Dichlorobenzene Dry Wt. < 21 ug/kg D.W. 21 82
1340 1,2-Dithloroethane Dry wt. < 34 ug/kg D.W. 34 82
—
1222 1,2-Dichloropropane Dry wt. < 13 ug/kg D.W. 13 82
82
9/22/21
82
8260C
9/22/21 8260C
9/22/21 8260C
9/22/21 8260C
9/22/21
9/22/21
9/22/21
9/22/21
8260C
8260C
8260C
8260C
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
1356 1,3-Dichlorobenzene Dry Wt < 22 ug/kg D.W. 22 82 9/22/21 8260C Test America B 3
1357 1,4-Dichlorobenzene Dry Wt. < 12 ug/kg D.W. 12 82 9/22/21 8260C Test America B 3
1337 2-Chloroethylvinyl Ether Dry wt. < 26 ug/kg D.W. 26 410 9/22/21 8260C Test America B 3
1334 Acroleln Dry wt. < 170 ug/kg D.W. 170 410 _ 9/22/21 8260C Test America B 3
1335 Acrylonibile Dry wt < 210 ug/kg D.W. 210 410 9/22/21 8260C Test America B 3
1346 Benzene Dry wt. < 16 ug/kg D.W. 16 82 9/22/21 8260C Test America B 3
1343 Brom odichlorornethane Dry wt. < 16 ug/kg D.W. 16 82 9/22/21 8260C Test America B 3
1219 Bromoform Dry wt. < 41 ug/kg D.W. 41 82 9/22/21 8260C Test America B 3
1342 Carbon Tetrachloride Dry wt. < 21 ug/kg D.W. 21 82 9/22/21 8260C Test America B 3
1352 Chlorabenzene Dry wt. < 11 ug/kg D.W. 11 82 9/22/21 8260C Test America B 3
1220 Chloroethane Dry wt. < 17 ug/kg D.W. 17 82 9/22/21 8260C Test America B 3
1339 Chloroform Dry wt. < 57 ug/kg D.W. 57 82 9/22/21 8260C Test America B 3
1344 cis-1,3-DIchloropropene Dry wt. < 20 ug/kg D.W. 20 82 9/22/21 8260C Test America B 3
1347 Dibromochloromethane Dry wt. < 40 ug/kg D.W. 40 82 9/22/21 8260C Test America B 3
1353 Ethylbenzene Dry wt. < 24 ug/kg D.W. 24 82 9/22/21 8260C Test America B 3
1331 Methyl Bromide Dry wt. < 18 ug/kg D.W. 18 82 9/22/21 8260C Test America B 3
1354 Methyl Chloride dry wt. < 20 ug/kg D.W. 20 82 9/22/21 8260C Test America B 3
1333 Methylene Chloride Dry wt. < 16 ug/kg D.W. 16 82 9/22/21 8260C Test America B 3
1187 Solids for dry weight determination (T 95 % .. "• 9/15/21 Moisture Test America B 3
1349 Tetrachioroethylene Dry wt. < 11 ug/kg D.W. 11 82 9/22/21 8260C Test America B 3
1351 Toluene Dry wt. 120 ug/kg D.W. 22 82 9/22/21 8260C Test America B 3
1221 Trans-1,2-Dirhloroethylene Dry wt. < 19 ug/kg D,W. 19 82 9/22/21 8260C Test America B 3
1223 Trans-1,3-Didiloropropene Dry wt. < 8.1 ug/kg D,W. 8.1 82 9/22/21 8260C Test America B 3
1345 Trlchioroethylene Dry wt. < 23 ug/kg D.W. 23 82 9/22/21 8260C Test America B 3
- 1332 Vinyl Chbride Dry wt. < 28 ug/kg D.W. 28 82 9/22/21 8260C Test America B 3
Pagel of 2
SYS/rpt5Oenadc3 4/11/14 Ir Prided: 1124121 1418

641MSD
oJRTK(Rf fDta I-JJ ti15 lliiM
Milorganite Priority Pollutant: Fall 2021
September 13, 2021
** The MDL for this test Is the lowest level of predsion shown, example: 4.1 would be "0.1".
*** The LOQ for this test Is the lowest level of predsion shown, example: 4.1 would be'0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
Column S: Test Status. Not Started=8, Intermediate=7, final=3, Analyst Approved=12, Not Reportable=15.
33
flog De1rL11iotlesis
AO Other -- Hag requires additional explanation.
AX Qualified data - see contract laboratory report
B3 Target analyte detected in method blank > 10% of sample
concentration.
87 LCS recovery was above control limits. _ Mi
B8 LCS recovery was below control limits. M2ian
B9 Low Level CCV recovery was outside of method acc gt limits. M3
D1 Duplicate precision control limit was exceeded.
D2 Matrixljlike precision control limit was exceeded. M5
D3 Sample is heterogeneous. Sample homogeneity could not be readily.
achieved using routine laboratory practices. M7
D4 Sample matrix Interferences did not allow completing the anaiids.
D5 The reported result Is an estimate because the concentration of
HEM in this sample exceeded the madmum allowed in the method
for the sample volume collected.
H1 Sample was received part holding time.
H3 Analyes performed he'arnd holding time. -
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past hoicks time.
H5 Analysis performed beyond holding time.
SYS. pt5Lienerfe3 4/11/14 Q
M9
NR
NU
P2
Q2
Q3
RT
55
S6
SD
T3
T4
TS
TS
IS Insufficient sample volume for analyss.
3 Estimated concentration above the adjusted method detection limit
and below the 'gusted reporting limit.
LA Not analyzed - laboratory accident.
Too numerous to count.rs 5padir colonies - unable to determine result.
M4 Results are an affroodmation due to speeding colonies.
Incubator/water bath temperature was outside method
requirements.
Sample incubation perVod outside method requirement.
Microbiology sample received without adequate heidSpeCe.
Target organism detected in associated method blank.
Not usable data (Water Quality only).
Not usable Data.
Sample received with Improper or Inadequate chemical preservation.
Matrix Spike rent'. eiy for this sarrple was above control limits.
Matrix spike recovery for this sample was below control limits.
Sample temperature upon receipt exceeded regulatory or project
requirements.
Reading was not confirmed by a constant weight measurement
Dried solid residue yield outside of method spec location (<2.5mg
or >200m .
Ship .lemental details provided (Water Quality of r).
The GOD dilution water D.O. depletion was > 0.2 melt.
GGA GOD was below method acceptance criteria._
GGA GOD was above method ore nce criteria.
Sample supersaturated with dissoWed oxygen for GOD anal
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow add sample pH for GOD.
T9 Sample Is outside of the prescribed method temperature rattle.
Pap 2of2
Printed: 1124121 14:26

Milorganite Dioxin Toxic Equivalent Concentrations 2021
Measured Concentration (pg/g or ppt)
Factor
CAS
Congener
1/9/2021
2/13/2021
3/13/2021
4/10/2021
5/8/2021
6/12/2021
7/10/2021
8/7/2021
9/11/2021
10/9/2021
11/13/2021
12/11/2021,
EPA
Maine
1746-01-6
2,3,7,8- Tetrachlorodibenzo-p-dioxin
0
0
6.8
0
0
0
0
0
0
0
0
0
1.0
1.0
40321-76-4
1,2,3,7,8- Pentachlorodibenzo-p-dioxin
0
0
0
0
0
0
0
0
0
0
0
0
1.0
0.5
39227-28-6
1,2,3,4,7,8- Hexachlorodibenzo-p-dioxin
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
57663-85-7
1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin
0
0
0.0
0
0
0
10
7.4
13
6.3
0
0
0.1
0.1
19408-74-3
1,2,3,7,8,9- Hexachlorodibenzo-p-dioxin
0
6.2
0.0
0.0
0.0
0
7.3
0.0
8.5
0
0
0
0.1
0.1
35822-46-9
1,2,3,4,6,7,8- Heptachlorodibenzo-p-dioxin
75
62
59
58
85
84
180
210
240
140
120
79
0.01
0.01
3268-87-9
1,2,3,4,6,7,8,9- Octachlorodibenzo-p-dioxin
660
550
540
560
780
840
1600
1600
2400
1400
1300
880
0.0001
0.001
51207-31-9
2,3,7,8- Tetrachlorodibenzofuran
0.0
3.8
4.4
1.7
1.1
1.4
1.6
1.2
1.5
2.0
2.0
2.0
0.1
0.1
57117-41-6
1,2,3,7,8- Pentachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.05
0.05
57117-31-4
2,3,4,7,8- Pentachlorodibenzofuran
0
7.0
9
0
0
0
0
0
0
5.5
0
0
0.5
0.5
70648-26-9
1,2,3,4,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
57117-44-9
1,2,3,6,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
7
0
0
0
0.1
0.1
72918-21-9
1,2,3,7,8,9- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
60851-34-5
2,3,4,6,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
6.8
0
0
0
0.1
0.1
67562-39-4
1,2,3,4,6,7,8- Heptachlorodibenzofuran
31
20
18
22
34
31
78
47
110
48
37
26
0.01
0.01
55673-89-7
1,2,3,4,7,8,9- Heptachlorodibenzofuran
0
0
0
0
0
0
0
0
6.6
0
0
0
0.01
0.01
39001-02-0
1,2,3,4,6,7,8,9- Octachlorodibenzofuran
42
27
34
39
51
43
140
75
200
86
97
57
0.0001
0.001
32598-13-3
3,3',4,4'- Tetrachlorobiphenyl
232
141
192
184
182
163
338
993
673
414
450
365
0.0001
0.0005
70362-50-4
3,4,4',5- Tetrachlorobiphenyl
0
0
0
0
0
0
0
52
0
0
0
0
0.0001
57465-28-8
3,3',4,4',5- Pentachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
32598-14-4
2,3,3',4,4'- Pentachlorobiphenyl
1230
940
1090
1020
1130
945
1560
1920
2280
1670
1970
1560
0.0001
0.0001
31508-00-6
2,3',4,4',5- Pentachlorobiphenyl
3030
1870
2510
2290
2350
2280
3850
4890
4940
3540
4460
3500
0.0001
0.0001
65510-44-3
2',3,4,4',5- Pentachlorobiphenyl
0
225
0
59
0
0
71
169
103
0
78
79
0.0001
0.0001
74472-37-0
2,3,4,4',5- Pentachlorobiphenyl
0
0
65.1
60.7
51.2
60.1
89
109
131
0
114
97
0.0005
0.0005
32774-16-6
3,3',4,4',5,5'- Hexachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.01
0.01
38380-08-4
2,3,3',4,4',5-Hexachlorobiphenyl
571
415
423
375
433
440
679
954
964
805
766
613
0.0005
0.0005
69782-90-7
2,3,3',4,4',5'- Hexachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.0005
0.0005
52663-72-6
2,3',4,4',5,5'-Hexachlorobiphenyl
191
124
152
120
146
154
280
298
328
250
244
201
0.00001
0.00001
39635-31-9
2,3,3',4,4',5,5'- Heptachlorobiphenyl
69
59
53
55
54.7
69.2
181
132
147
104
87
83
0.0001
0.0001
35065-30-6
2,2',3,3',4,4',5-Heptachlorobiphenyl
1430
1100
878
853
634
1150
1780
1990
2270
1970
1760
1460
0.0001
35065-29-3
2,2',3,4,4',5,5'-Heptachlorobiphenyl
1430
2650
2350
2230
1580
2640
4190
4800
5080
3940
4220
3160
0.0001
Total EPA Toxic Equivalent (TEQ)
1.9
5.9
13.0
1.6
2.0
2.0
5.6
4.9
8.9
6.6
3.1
2.3
Total Maine Toxic Equivalent (TEQ)
2.9
6.9
14.0
2.5
3.0
3.2
7.9
7.5
12.2
8.7
5.1
3.7
"0" means that the concentration was less than the level of detection