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HomeMy WebLinkAboutWQ0023306_Residual Annual Report 2021_20220118Non -Discharge Branch Upload/Submittal Form NORTH CAROLINA En.anmemfal Qualify Version 2 - Revised June 23, 2020 Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number (IR) * WQ0023306 Applicant/Permittee City of New Bern Email Notifications Does this need review by the hydrogeologist?* Yes No Regional Office CO Reviewer Admin Reviewer Washington January 19, 2022 NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Reference: NEW BERN NORTH CAROLINA Everything comes together here Department of Public Utilities Wastewater Treatment Plant 307 Glenburnie Drive New Bern, NC 28560-2816 2021 Land Application Annual Report City of New Bern CLASS A RESIDUALS Permit Number WQ0023306 The City of New Bern is submitting all monitoring and reporting requirements as specified in the above referenced permit for its land application program for Sewage Sludge. The city has managed and compiled the submitted data. The city produced approximately 5274 dried tons of sludge during 2021, which met the CIass A Sewage Sludge criteria. The city hauled to the Craven County Solid Waste Management Authority to be used for ground cover. The report includes form ACF, form DMSDF, form RSSF, form MFLSF, Lab Sheets, and form PVRF 2T. If any further information is required, please contact Tony Hawkins at (252) 693-7555. Sincerely, Tony Hawkins Treatment Plants Manager Enclosures Cc: File ANNUAL LAND. APPLICATION CERTIFICATION FORM WQ Permit#: WQ0023306 County: Facility Name (as shown on permit): Land Application Operator: Craven Year: 202I City of New Bern Tony Hawkins Phone: (252) 639-7555 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permit: 1 Total number of fields utilized for land application during the year: I Total amount of dry tons applied during the year for all application sites: 5,274 Total number of acres utilizes for Iand application during the year: Craven county land field Part B - Annual Compiance Statement: Facility was compliant during calendar year (including but not limited to items 1-13 below) issued by the Division of Water Resources.❑ Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 2021 with all conditions of the land application permit 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the pen -nit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permif were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Tony Hawkins Plant Manager Permittee Name a d Title (type or print) Date Signature of Permittee Date Signature of Preparer* Signature of Land Applier (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) Date CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0023306 FACILITY NAME: City of New Bern PHONE: (252) 639-7555 COUNTY: Craven OPERATOR: Tony Hawkins FACILITY TYPE (please check one): v❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes 0 No ❑ -IP- If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bullring Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January land field 30 lime 503 512 February land field 35 lime 477 487 March land field 35 Iime 492 498 April Did not haul 0 lime 0 0 May land field 32 lime 483 486 June land field 36 lime 489 498 , July land field 36 lime 476 487 August land field 36 lime 438 449 September land field 35 lime 347 350 October land field 36 Iime 501 507 November land field 35 lime 509 515 December land field 36 lime 481 485 Total from FORM DMSDF (sup) Totals: Annual (dry tons): 382 5196 5274 .... . .... . . . . . . . .. . . 0 Amendment(s) used: 382 Bulking Agent(s) used: lime DMSDF (Sapp) * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form 0 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 6/4.'1 1^\ ignature of Permittee 1-4cl 2Z Date **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Signature of Preparer** (if different from Permittee) Date DENR FORM DMSDF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0023306 Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data City of New Bern 23306 City of New Bern Laboratory: 1) Environment 1 2) 3) 4) 5) Parameter (mg/kg) Ceiling Conc. Limit Sample or Composite Date 1/19 2/4 3/17 4/7 5/13 6/2 7/20 814 918 10/7 11/3 12/2 Percent Solids (%) NA 36.58 32.94 42.39 . 37.42 33.62 28.91 Arsenic 75 4.7 3 6 7.3 6 4.2 2.6 <2.5 3.5 <2.5 <2.5 <2.5 Cadmium 85 <0.5 <0.5 0.52 0.61 0.52 0.59 0.65 <0.5 1.5 0.66 <5.0 <0.5 Copper 4,300 96 53 143 297 237 241 158 143 399 205 167 111 Chromium NA 8 5 11 11 12 13 11 11 33 19 16 12 Lead 840 5 2.9 6.3 7.5 5.3 7 7.4 6.8 16 11 6.2 4.1 Mercury 57 0.15 0.11 0.16 0.14 0.22 0.37 0.49 0.3 0.4 0.3 0.21 0.27 Molybdenum 75 <5.0 <5.0 <5.0 5 <5.0 <5.0 <5.0 <5.0 9 6 <5.0 <5.0 Nickel 420 <5.0 <5.0 <5.0 5 <5.0 6 6 5 17 8 8 5 Selenium 100 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Zinc 7,500 230 109 277 291 267 352 286 276 742 368 363 216 Total Phosphorus NA c12960 c6229 c9529 c10290 c16340 c11120 c10660 c10250 c36110 c958.8 c16950 c11040 TKN NA c26650 c3761 c19250 c24290 c12490 c27490 c9265 c15920 c57280 c20390 c18200 c30690 Ammonia -Nitrogen NA c42.82 c37.92 c92.78 c72.88 c98.96 c58.54 c64.50 c135.5 c2386 c78.80 c126 c135.2 Nitrate and Nitrite - NA c63.73 e61.88 c49.88 c42.93 c103 c123 c143.9 c96.65 c17.92 c71.81 c108 c27.84 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the indiv d.ua1 permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submit ing false information, including the possibility of fines and imprisonment for knowing violations." k Sigrfature of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of New Bern Total Dry Tons Applied (Annual): Permit #: WQ0023306 Cation Exchange Capacity (non 503 only): Operator: Tony Hawkins Owner: City of New Bern Predominant Soil Series: Acres Used: nla Acres Permitted: Site #: land field Field #: 5274.00 Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent #): Sample or Com- posite Date Li] 2 3/17/21 4 5 I 5/13/21 ,_tj 6/2/21 7_ 8 110 1 11 1 12 1/19/21 2/4/21 4/7/21 7/20/21 8/4/21 9/8/21 10/7/21 11/3/21 12/2/21 % Solids 36.58 32.94 42.39 37.42 33.62 28.91 Arsenic 4.7 3 6. 7.3 6 4.2 2.6 <2.5 3.5 <2.5 <2.5 <2.5 Cadmium <0.05 <0.5 0.52 0.61 0.52 0.59 0.65 <0.5 1.5 0.66 <5.0 <5.0 Copper 96 53 143 297 237 241 158 143 399 205 167 111 Chromium 8 5 11 11 12 13 11 11 33 19 16 12 Lead 5 2.9 6.3 7.5 5.3 7 7.4 6.8 16 11 6.2 4.1 Mercury 0.15 0.11 0.16 0.14 0.22 0.37 0.49 0.3 0.4 0.3 0.21 0.27 Mo1yb- denum <5.0 <5.0 <5.0 5 <5.0 <5.0 <5.0 <5.0 9 6 <5.0 <5.0 Nickel <5.0 <5.0 <5.0 5 <5.0 6 6 5 17 8 8 5 Selenium <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Zinc 230 109 277 291 267 352 286 276 724 368 363 216 Total Phos- phorus c12960 c6229 c9529 c10290 c16340 c11120 c10660 c10250 c361100 c958.8 c16950 c11040 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total ': DT/Ac./ App. Event U U_ 1 6 u 9 'IA 11 12 o x - Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### 0.000 ###### ###### ###### ###### Cadmium ###### ###ff## 0.000 0.000 0.000 0.000 0.000 ###### 0.000 0.000 ###### ###### ###### Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb denum ###### ###### ###### 0.000 ###### 0.000 0.000 ###### ###### ###### ###### ###### ###### Nickel ###### ###### ###### 0.000 ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Selenium ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Total Phos- phorus ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### ###### "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowin vioIat; ns". -z Signature of Land Applier Date DENR FORM MFLSF (12/2006) EIN[1113©DEUR 1111 QENDITNEatgcI 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 �iyokt,Ai* .tint- tx:.o , PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 01/19/21 DATE REPORTED : 01/22/21 tO REVIEWED BY: e/ /L,� Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % 33.08 41,10 35.94 36.61 36.17 01/19/21 JMS 2540G11 Fecal Coliform (MPN), /gram Solids < 1,8 < 1.8 < 1.8 < 1.8 <1.8 01/19/21 JMS 9221E-06 wriramung 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 dicupgrOgd CITY OF NEW BERN (BIOSOLIDS) ATTN: TONX HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 01/19/21 DATE REPORTED : 01/22/21 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % Fecal Coliform (MPN), /gram Solids C 1.8 <1.8 01/19/21 JMS 9221E-06 36.12 36.34 01/19/21 JMS 2540G-11 udaQ®totti 1t Rum] ©Ma{ 114 OAKMONT DRIVE OREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 2661 01/29/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 4.7 01/28/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 311196 01/29/21 LFJ EPA200.7 Cadmium (dry wt, basis), mg/kg <0.5 02/02/21 MTM 3113B-04 Copper (dry wt. basis), mg/kg 96 01/29/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 8 01/29/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 5.0 02/01/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/lcg 3607 01/29/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0,15 01/27/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg <5.0 01/29/21 LFJ EPA200.7 - Potassium (dry wt. basis), mg/kg 3405 01/29/21 LFJ EPA200.7 Selenium (dry wt, basis), mg/kg <5.0 02/01/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 01/29/21 LFJ EPA200,7 Sodium (dry wt. basis), mg/kg <1250 01/29/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 230 01/29/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 31.5 01/20/21 KITS 4500CNE-11 TKN (dry wt.), rng/kg c 26650 01/22/21 TLH 351.2 R2-93 Ammonia Nitrogen (dry wt.),mglkg c 42.82 01/21/21 ICES 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 12960 01/22/21 ICES 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 63.73 01/21/21 DTI, 353.2 R2-93 Plant Available Nitrogen, mg/kg 13389 01/27/21 MAO Molybdenum (dry wt. basis), mg/kg <5.0 01/29/21 LFJ EPA200.7 PHONE (252) 756-6208 FAX (252) 756-0633 ID*: 214 DATE COLLECTED: 01/1.9/21 DATE REPORTED : 02/03/21 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification For this analytical, procedure. /77--Q 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 2191 02/09/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 3.0 02/10/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 388919 02/09/21 LFJ EPA200.7 Cadmium (dry wt. basis), rug/kg <0.5 02/12/21 MTM 311313-04 Copper (dry wt. basis), mg/kg 53 02/09/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 5 02/09/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 2,9 02/11/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 4048 02/09/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.11 02/23/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg <5.0 02/09/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 2296 02/09/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 02/10/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 02/09/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 02/09/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 109 02/09/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 24.11 02/08/2I I(DS 4500CNE-11 TICN (dry wt.), mg/kg c 3761 02/11/21 KES 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 37.92 02/10/21 TLH 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 6229 02/11/21 TLI-1 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 61.88 02/10/21 DTL 353.2 R2-93 Plant Available Nitrogen, mg/kg 1570 02/20/21 MAO Molybdenum (dry wt. basis), mg/kg < 5.0 02/09/21 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater ID. 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 02/04/21 DATE REPORTED : 02/25/21 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. FE-MrcnnorR Drinking Water ID1 37715 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 knorpcxraNid CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PHONE (252) 756-6208 FAX (252) 756-0633 ID# 214 A DATE COLLECTED: 03/17/21 DATE REPORTED : 03/22/21 REVIEWED BY: Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin -FM Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % Fecal Cotifortn (MPH /grans Solids <1.8 < 1.8 < 1.8 < 1.8 < 1.8 03/17/21 KDS 9221E-06 31.94 32.24 31.52 37.31 35.13 03/17/21 KDS 2540E-11 Ammo 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 -LoQpo gbd CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking Water ID: 37715 PHONE (252) 758-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 03/17/21 DATE REPORTED : 03/22/21 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % Fecal Coliform (MPN), /gram Solids <1.8 <1.8 03/17/21 KDS 9221E-06 29.54 32.96 03/17/21 KDS 2540G-11 WIQoEDBEa �o D011COInOPiglaa{ 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TON.' HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Alnmimum, (dry wt, basis), mg/kg 4489 04/01/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 6.0 04/05/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 280925 04/01/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0,52 04/01/21 MTM 311313-04 Copper (dry wt. basis), mg/kg 143 04/01/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 11 04/01/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 6,3 04/01/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 3311 04/01/21 LFJ EPA200.7 Mercury (dry wt, basis), mg/kg 0.16 04/05/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg <5.0 04/01/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 3803 04/01/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 03/31/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 04/01/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 04/01/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 277 04/01/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 47.95 03/29/21 KDS 4500CNE-11 TKN (dry wt.), mg/kg c 19250 03/23/21 ICES 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 92.78 03/24/21 DTL 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 9529 03/23/21 TLH 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 49.88 03/23/21 DTL 353.2 R2-93 Plant Available Nitrogen, mg/kg 7759 04/02/21 MAO Molybdenum (dry wt. basis), mg/kg <5.0 04/01/21 LFJ EPA200.7 Drirss i"4.; '`t s° - , Wastewater ID, 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 03/17/21 DATE REPORTED : 04/08/21 REVIEWED BX: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. E too pma o 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWICXNS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 3671 04/14/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 7,3 04/19/21 MTM 3113E-04 Calcium (dry wt. basis), mg/kg 264826 04/14/21 LEI EPA200.7 Cadmium (dry wt. basis), mg/kg 0.61 04/16/21 MTM 3113B-04 Copper (dry wt. basis), mg/kg 297 04/28/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),nig/kg 11 04/14/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 7.5 04/15/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 3484 04/14/21 LFJ EPA200.7 Mercury (dry ►vt. basis), mg/kg 0.14 04/27/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 5 04/14/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 4142 04/15/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 04/20/21 MTM 3113E-04 Silver (dry wt. basis), mg/kg <2.5 04/14/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 04/15/21 LFJ EPA200.7 Zinc (dry wt, basis), mg/kg 291 04/14/21 LF,1 EPA200.7 Total Cyanide (dry weight), mg/kg 36.76 04/12/21 KDS 4500CNE-11 TKN (dry wt.), mg/kg c 24290 04/14/21 TLH 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 72.88 04/14/21 DTL 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 10290 04/14/21 KES 365.4-74 Nitrate -Nitrite (dry wt.), tug/kg c 42.93 04/14/21 DTL 353.2 R2-93 Plant Available Nitrogen, mg/kg 9766 04/15/21 MAO Molybdenum (dry wt. basis), mg/kg 5 04/14/21 LFJ EPA200.7 Drinking Water ID; 37715 Wastewater ID: 117 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 04/07/21 DATE REPORTED : 04/29/21 REVIEWED BY: e Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. LINIIMEHOH ijItc1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWINS P.O. BOX 1129 NEW BERN, NC 28563 DrinkEng Wator ID. Wastewater 1Dr PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 05/13/21 DATE REPORTED : 05/20/21 REVIEWED BY: Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin -FM Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, Fecal Coliform (MPN), /gram Solids <1.8 < 1.8 < 1.8 <1.8 < 1,8 05/13/21 BLV 9221E-06 37.30 47.36 39.72 45.94 42.44 05/17/21 BLV 2540G-11 0 � ITCREITi c 1t Ala hgErpomhd Drinking Water ID' 37715 W©atewater ID: 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 ID#: 214 A DATE COLLECTED: 05/13/21 DATE REPORTED : 05/20/21 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % Fecal ColiWorm (MPN), /gram Solids <1.8 < 1.8 05/13/21 BLV 9221E-06 41.43 42.56 05/17/21 BLV 2540G-11 aW1h3Callng lg hENINDTEND6 -r 7U 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 3057 05/19/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 6.0 05/21/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 263600 05/19/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0.52 05/19/21 MTM 3113E-04 Copper (dry wt. basis), mg/kg 237 05/19/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 12 05/19/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 5.3 05/20/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 3384 05/I9/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.22 05/27/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg <5.0 05/19/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 3617 05/19/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 05/19/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 05/19/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg < 1250 05/19/21 LF,T EPA200.7 Zinc (dry wt. basis), mg/kg 267 05/19/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 65.37 05/17/21 KDS 4500CNE-11 '1'KN (dry wt.), mg/kg c 12490 05/18/21 KES 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 98.96 05/19/21 KES 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 16340 05/18/21 TLH 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 103.0 05/19/21 DTL 353.2 R2-93 Plant Available Nitrogen, mg/kg 5109 05/30/21 MAO Molybdenum (dry wt. basis), mg/kg <5.0 05/19/21 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 05/13/21 DATE REPORTED : 06/01/21 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. EATCD Drinking Water SD: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 ID#: 214 DATE COLLECTED: 06/02/21 DATE REPORTED : 07/01/21 REVIEWED BY: Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 3891 06/25/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 4.2 06/24/21 MTM 3I13B-04 Calcium (dry wt. basis), mglkg 245246 06/25/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0.59 06/24/21 MTM 3113B-04 Copper (dry wt. basis), mg/kg 241 06/25/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 13 06/25/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 7.0 06/25/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 4899 06/25/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.37 06/21/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 6 06/25/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 3109 06/25/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 06/25/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 06/25/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg < 1250 06/25/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 352 06/25/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 112.5 06/09/21 KDS 4500CNE-11 TKN (dry wt.), mglkg c 27490 06/15/21 TLH 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 58.54 06/09/21 DTI, 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 11120 06/15/21 KES 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 123.0 06/09/21 KES 353.2 R2-93 Plant Available Nitrogen, mg/kg 11125 06/22/21 MAO Molybdenum (dry wt. basis), mg/kg <5.0 06/25/21 LFJ EPA200.7 c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. doQ©[UM llg Locoymb4 11111111"--- 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 07/20/21 DATE REPORTED : 07/23/21 RLVIEWED BY Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % 37.15 36.95 37.00 40.64 35.53 07/20/21 JMS 2540G-.11 Fecal Coliform (MPN), /gram Solids <1.8 < 1.8 < 1.8 < 1.8 < 1.8 07/20/21 KDS 9221E-06 l� El-mcgpmegd Drinking Water ID: 37,15 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 ID#: 214 A DATE COLLECTED: 07/20/21 DATE REPORTED : 07/23/21 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % 38.27 36.44 07/20/21 JMS 2540G-11 Fecal Coliform (MPN), /gram Solids <1.8 <1.8 07/20/21 KDS 9221E-06 Euhinonift ki©CRAITEad yu Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOI,IDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 3335 08/04/21 MTM EPA200.7 Arsenic (dry wt. basis), mg/kg 2,6 08/04/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 283233 08/04/21 MTM EPA200.7 Cadmium (dry wt. basis), mg/kg 0.65 08/03/21 MTM 3113E-04 Copper (dry wt. basis), mg/kg 158 08/04/21 MTM EPA200.7 Chromium, T.(dry wt. hasis),mg/kg 11 08/04/21 MTM EPA200.7 Lead (dry weight basis), mg/kg 7.4 08/03/21 MTM 3113E-04 Magnesium (dry wt. basis), mg/kg 4160 08/04/21 MTM EPA200.7 Mercury (dry wt. basis), mg/kg 0.49 08/02/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 6 08/04/2I MTM EPA200.7 Potassium (dry wt. basis), mg/kg 2253 08/04/21 MTM EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 08/04/21 MTM 3113B-04 Silver (dry wt, basis), mg/kg < 2.5 08/04/21 MTM EPA200.7 Sodium (dry wt. basis), mg/kg < 1250 08/04/21 MTM EPA200.7 Zinc (dry wt, basis), mg/kg 286 08/04/21 MTM EPA200.7 Total Cyanide (dry weight), mg/kg 50.9 07/27/21 KDS 4500CNE-11 TKN (dry wt.), mg/kg c 9265 07/22/21 DTL 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 64.50 07/23/21 HMM 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 10660 07/22/21 KES 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 143.9 07/22/21 HNLM 353.2 R2-93 Plant Available Nitrogen, mg/kg 3856 07/30/21 MAO Molybdenum (dry wt. basis), mg/kg < 5.0 08/04/21 MTM EPA200.7 ID#: 214 DATE COLLECTED: 07/20/21 DATE REPORTED : 08/05/21 REVIEWED BY : c Uncertified data, DWR does not offer non -aqueous certification for this analytical procedure. It 17 ©©Qp©Q©� r Drinking Water ID; 37715 Wastewater ID: 1G 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 3173 08/17/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 08/17/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 308776 08/17/21 LFJ EPA200.7 Cadmium (dry wt. basis), rug/kg <0.5 08/18/21 MTM 3113E-04 Copper (dry wt. basis), mg/kg 143 08/17/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 11 08/17/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 6.8 08/18/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 4172 08/17/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.30 08/24/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 5 08/17/21 LFJ EPA200.7 , Potassium (dry wt. basis), mg/kg 2122 08/17/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 08/17/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 08/17/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 08/17/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 276 08/17/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 31.1 08/11/21 KDS 4500CNE-11 TKN (dry wt.), mg/kg c 15920 08/12/21 KES 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 135.5 08/11/21 KES 350.I R2-93 Phosphorus, T. (dry wt.), mg/kg c 10250 08/10/21 KES 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 96.65 08/17/21 KES 353.2 R2-93 Plant Available Nitrogen, mg/kg 6478 08/28/21 MAO Molybdenum (dry wt. basis), mg/kg < 5.0 08/17/21 LFJ EPA200.7 ID#: 214 DATE COLLECTED: 08/04/21 DATE REPORTED : 08/30/21 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. ERAMIIIIgn ill dr©OrpErffigd Drinking Water ID: 37715 Wastewater ID; 16 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 ID# : 214 A DATE COLLECTED: 09/08/21 DATE REPORTED : 09/15/21 REVIEWED BY: Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % 26.53 34.21 36.03 29.80 31.25 09/10/21 JMS 2540G-15 Fecal Coliform (MPN), /gram Solids < 1.8 < 1.8 < 1.8 < 1.8 < 1.8 09/08/21 JMS 9221E-14 I[T1 I]namparOod Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 Total Solids, CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.D. BOX 1129 NEW BERN, NC 28563 ID#: 214 A DATE COLLECTED: 09/08/21 DATE REPORTED : 09/15/21 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Bashi-FC#7 Date Analyst Code 40.83 36.71 09/10/21 JMS 2540G-15 Fecal Coliform (MPN), /gram Solids <1.8 <1.8 09/08/21 JMS 9221E-14 ��i]dOQO IdEg'R higNparagd Drinking Water ID: 3/315 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW KERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 8608 09/15/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 3.5 09/16/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 35392 09/15/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 1.5 09/16/21 MTM 3113B-04 Copper (dry wt. basis), mg/kg 399 09/15/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 33 09/15/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 16 09/16/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 4742 09/15/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.40 09/15/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 17 09/15/21 LFJ EPA200.7 . Potassium (dry wt. basis), mg/kg 4427 09/15/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 09/15/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg 4 09/15/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg 2295 09/15/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 742 09/15/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 45.5 09/21/21 HMM 4S00CNE-16 TKN (dry wt.), mg/kg c 57280 09/16/21 KES 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 2386 09/14/21 KES 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 36110 09/14/21 BMD 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 17.92 09/21/21 TRJ 353.2 R2-93 Plant Available Nitrogen, mg/kg 23169 09/29/21 MAO Molybdenum (dry wt. basis), mg/kg 9 09/15/21 LFJ EPA200.7 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 09/08/21 DATE REPORTED : 09/30/21 REVIEWED BY: v c Uncertified data. ❑WR does not offer non -aqueous certification for this analytical procedure. m9ikiicuum CoQ ©ITM' Drinking Seater ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 4783 10/21/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 10/27/21 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 232835 10/21/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0.66 11/03/21 MTM 3113B-04 Copper (dry wt. basis), mg/kg 205 10/2I/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 19 10/21/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 11 11/09/21 MTM 3113E-04 Magnesium (dry wt. basis), mg/kg 4532 10/21/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.30 10/27/21 MTM EPA747IB Nickel (dry wt. basis), mg/kg 8 10/21/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 2828 10/21/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 11/10/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 10/21/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 10/21/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 368 10/21/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 44.8 10/18/2I HMM 4500CNE-16 TKN (dry wt.), mg/kg c 20390 10/12/21 BMD 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 78.80 10/11/21 KES 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 958.8 10/12/21 TRJ 365.4-74 Nitrate+Nitrite (dry wt.), mg/kg c 71.81 10/12/21 KES 353.2 R2-93 Plant Available Nitrogen, mg/kg 8236 10/25/21 MAO Molybdenum (dry wt. basis), mg/kg 6 10/21/21 LFJ EPA200.7 ID#: 214 DATE COLLECTED: 10/07/21 DATE REPORTED : 11/11/21 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. EldfrEtEg IA L fl oQroT R Drinking Water ID; 37715 Waatewater ID: 10 114 OAKMONT DRIVE PHONE (252) 755-6208 GREENVILLE, N C. 27858 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 28563 ID#: 214 A DATE COLLECTED: 11/03/21 DATE REPORTED : 11/09/21 REVIEWED BY: ✓�� Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin -WO Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % 30.91 31.11 29.04 27.01 26.86 11/04/21 BLV 2540G-15 Fecal Coliform (MPN), /gram Solids <1.8 <1.8 <1.8 <1.8 < 1.8 11/03/21 JMS 9221E-14 whr©EngEl u Elogualegd. Drinking Water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.D. BOX 1129 NEW BERN, NC 28563 ID#: 214 A DATE COLLECTED: 11/03/21 DATE REPORTED : 11/09/21 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % 28.00 29.47 11/04/21 BLV 2540G-15 Fecal Coliform (MPN), /gram Solids <1.8 <1.8 11/03/21 JMS 9221E-14 Enos©R©cal ilg lincgiurbd• 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (SIOSOLIDS) ATTN: TONY HAWICINS P.O. BOX 1129 NEW BERN, NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 3810 11/17/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 11/17/21 MTM 3113E-04 Calcium (dry wt, basis), mg/kg 256929 11/17/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg <0.5 11/16/21 MTM 3113E-04 Copper (dry wt. basis), mg/kg 167 11/17/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 16 11/17/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 6.2 11/15/21 MTM 311313-04 Magnesium (dry wt. basis), mg/kg 4525 11/17/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.21 11/23/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 8 11/17/21 LFJ EPA200.7 - Potassium (dry wt. basis), mg/kg 2862 11/17/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 11/16/21 MTM 3113E-04 Silver (dry wt. basis), mg/kg 3 11/17/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 11/17/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 363 11/17/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 94.36 11/12/21 HUM 4500CNE-16 TEN (dry wt.), mg/kg c 18200 11/10/21 BMD 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 126.0 11/08/21 BMD 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 16950 11/08/21 TRJ 365.4-74 Nitrate+Nitrite (dry wt.), mg/kg c 108.0 11/08/21 TRJ 353.2 R2-93 Plant Available Nitrogen, mg/kg 7401 12/20/21 MAO Molybdenum (dry wt. basis), mg/kg <5.0 11/17/21 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater ID: 10 l'I IUfdL (2:2) /;1(i 6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 11/03/21 DATE REPORTED : 12/20/21 REVIEWED BY: ✓ ✓J c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure, cahOEIII ¶a [IMCCEp©Fabd mast orator ZDJ. au 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN, NC 26563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 2866 12/20/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 12/22/21 MTM 3113E-04 Calcium (dry wt. basis), mg/kg 304318 12/20/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg <0,5 12/22/21 MTM 3I13B-04 Copper (dry wt. basis), mg/kg 111 12/20/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 12 12/20/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 4.1 12/21/21 MTM 3113E-04 Magnesium (dry wt. basis), mg/kg 4516 12/20/21 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.27 12/22/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 5 12/20/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 3954 12/20/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 12/22/21 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 12/20/21 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg 1270 12/20/21 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 216 12/20/21 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 61.36 12/13/2I HMM 4500CNE-16 TKN (dry wt.), mg/kg c 30690 12/07/21 TRJ 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 135.2 12/08/21 BMD 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 11040 12/07/21 BMD 365.4-74 Nitrate+Nitrite (dry wt.), mg/kg c 27.84 12/07/21 ICES 353.2 R2-93 Plant Available Nitrogen, mg/kg 12317 01/02/22 MAO Molybdenum (dry wt. basis), mg/kg <5.0 12/20/21 LFJ EPA200.7 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 12/02/21 DATE REPORTED : 01/05/22 REVIEWED BY: e Uncertified data. DWR dose not offer non -aqueous certification for this analytical procedure. I .i-tc`n art i-i=tSi'.ut7. by SGS Nor,) Technical Report for Environment 1, Inc City of New Bern (Biosoilds); New Bern, NC 214A SGS Job Number: FA87897 Sampling Date: 08/05/21 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 abrown@environmentlinc.com ATTN: Ann Brown Total number of pages in report: ..4 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. e-Hitedeopy Z.0 , tF.?tPYtfi3iY.:'d Report Norm Farmer Technical Director Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • lei: 407-425-6700 • fax: 407-425-0707 .S 1 o 4 Serdous; Table of Contents 4 Section1Sample Summary 3 Section Z:Summary oYHits 3:�~-~-~^...-^..-..^.~_...~.~._^^......'~..'.'...~,~~.^^......~..~~..~.~' - ��I� I��87897'l� HOLDING BASIN (RA) " IlO�I�T0G]9A�I�[(�/�) ' ~' l% Sookno4; Misc. Forms 13 4,1: Cham' of Custody 2or14 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA87897 City of New Bern (Biosoilds); New Bern, NC Project No: 214A Sample Collected Matrix Number Date Time By Received Code Type Client Sample ID This report con Organics ND tilts! reported as ND = Not detected Tlie following applies::'. = Not detected above the MDL FA87897-1 08/05/21 10:15 LS 08/07/21 SO Soil FA87897-1L 08/05/21 10:15 LS 08/07/21 SO Soil HOLDING BASIN (RA) HOLDING BASIN (RA) Soil samples reported on a dry weight basis unless otherwise indicated on result page. SGS Summary of Hits Job Number: FA87897 Account: Environment 1, Inc Project: City of New Bern (Biosoilds); New Bern, NC Collected: 08/05/21 Page 1 of 1 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA87897-1 HOLDING BASIN (RA) Corrosivity as pH a Ignitability (Flashpoint) b > 200 12.2 FA87897-1L HOLDING BASIN (RA) Lead (a) 20mis added to log for pH. (b) Not ignitable. su SW846 CHAP7 Deg. F SW846 1010A MOD 0.055 0.050 mg/1 SW846 6010D SGS Sample Results Report of Analysis S S Ot14 r-Ari7a27 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: HOLDING BASIN (RA) Lab Sample ID: FA87897-1 Matrix: SO - Soil Project: City of New Bern (Biosoilds); New Bern, NC Date Sampled: 08/05/21 Date Received: 08/07/21 Percent Solids: 45.0 General Chemistry An alvte Currosivity as pH a Cyanide Reactivity Ignitability (Flashpoint) 6 Solids, Percent Sulfide Reactivity (a) 20m1s added to log for pH. (b) Not ignitable. Result RL Units DF Analyzed By Method 12.2 su 1 08/14/21 14:17 JB 3.3 3.3 mg/kg I 08/17/21 12:04 AC > 200 Deg. F 1 08/11/21 10:18 KSA 45 % 1 08/12/21 10:36 HH < 110 110 mg/kg 1 08/12/21 13:50 IC SW846 CHAP7 SW846 CHAP7 SW846 1010A MOD SM19 2540G SW846 CHAP7 RL = Reporting Limit m of 14 F,Ala 18 8: SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: HOLDING BASIN (RA) Lab Sample ID: FA87897-1L Matrix: SO - Soil Method: Project: SW846 8260E SW846 1311 City of New Bern (Biosoilds); New Bern, NC Date Sampled: 08/05/21 Date Received: 08/07/21 Percent Solids: 45,0 File ID Run #1 C0150417.D 10 08/17/21 03:46 SO 08/12/21 13:30 OP86798 VC6067 Run #2 DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 Run #2 Purge Volume 5.0 mi VOA TCLP List CAS No. Compound TCLP Leachate method SW846 1311 Result I4W# MCL RL MDL Units Q 71-43-2 Benzene ND D018 0.50 0.010 0.0031 mg/1. 78-93-3 2-Butanone (MEK) ND D035 200 0.050 0.020 mg/I 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene ND D021 100 0.010 0.0020 mg/1 67-66-3 Chloroform ND D022 6.0 0.010 0.0030 mg/1 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 0.0026 mg/1 107-06-2 L2-Dichloroethane ND D028 0.50 0.010 0,0031 mg/1 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 0.0032 mg/1 127-18-4 Tetrachloroethylene ND D039 0.70 0.010 0.0022 mg/1 79-01-6 Trichloroethylene ND D040 0.50 0.010 0.0035 mg/1 75-01-4 Vinyl Chloride ND D043 0.20 0.010 0.0041 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99% 83-118% 17060-07-0 1,2-Dichloroethane-D4 101% 79-125% 2037-26-5 Toluene-D8 99% 85-112% 460-00-4 4-Browofluorobenzene 100% 83-118% ND = Not detected MDL = Method Detection Limit .1 — Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound _.., ..SGS 7 of 14 rA,w7fl97 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: Lab Sample ID: Matrix: Method: Project: HOLDING BASIN (RA) FA87897-1L SO - Soil SW846 8270D SW846 3510C City of New Bern (Biosoilds); New Bern, NC Date Sampled: 08/05/21 Date Received: 08/07/21 Percent Solids: 45.0 Run #1 Run #2 File ID 6F10557.D DF 1 Analyzed By Prep Date Prep Batch Analytical Batch 08/16/21 16:30 JB 08/14/21 07:30 OP86828 S6F394 Run #1 Run #2 Initial Volume Final Volume 100 mi 1.0 ml ABN TCLP List CAS No. Compound 95-48-7 87-86-5 95-95-4 88-06-2 106-46-7 121-14-2 118-74-1 87-68-3 67-72-1 98-95-3 110-86-1 2-Methylpbenol 3&4-Methylphenol Pentachlorophenol 2, 4, 5-Trichtorophenol 2, 4, 6-Trichloraophenol 1,4-Dichlorobenzene 2, 4-Dinitrotoluene Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Nitrobenzene Pyridine CAS No. Surrogate Recoveries 367-12-4 4165-62-2 118-79-6 4165-60-0 321-60-8 1718-51-0 2-Fluorophenol Phenol-d5 2,4, 6-Trihromophenol Nitrobenzene-d5 2-Fluorobiphenyl Terphenyl-d14 TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q ND D023 200 0.050 0.0056 mg/I ND D024 200 0.050 0.0098 mg/1 ND D037 100 0.25 0.050 mg/1 ND D041 400 0.050 0.0074 mg/I ND D042 2.0 0.050 0.0075 mg/I ND D027 7.5 0.050 0.0050 mg/1 ND D030 0.13 0.050 0.0081 mg/1 ND D032 0.13 0.050 0.0069 mg/l ND D033 0.50 0.050 0.0050 mg/1 ND D034 3.0 0.050 0.016 mg/I ND D036 2.0 0.050 0.0093 mg/1 ND D038 5.0 0.10 0.020 mg/1 Run# 1 Run# 2 Limits 31% 14-67% 22% 10-50% 72% 33-118% 68% 42-108% 70% 40-106% 72% 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E — Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: HOLDING BASIN (RA) Lab Sample ID: FA87897-1L Matrix: SO - Soil Method: SW846 8151A SW846 3510C Project: City of New Bern (Biosoilds); New Bern, NC Date Sampled: 08/05/21 Date Received: 08/07/21 Percent Solids: 45.0 File ID DF Run #1 CC076511.D 1 Run #2 Analyzed By Prep Date Prep Batch Analytical Batch 08/16/21 17:38 NJ 08/14/21 11:00 OP86830 GCC1903 Run #1 Run #2 Initial Volume Final Volume 10.0 ml 5.0 ml Herbicide TCLP List CAS No. Compound TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q 94-75-7 2,4-4) ND D016 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) ND D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 61% 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method plank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound bG 9 of14 FA 7.997 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: HOLDING BASIN (RA) Lab Sample ID: FA87897-IL Matrix: SO - Soil Method: SW846 8081B SW846 3510C Project: City of New Bern (Biosoilds); New Bern, NC Date Sampled: 08/05/21 Date Received: 08/07/21 Percent Solids: 45.0 File ID DF Run #1 ST154697.D 1 Rim #2 Analyzed By Prep Date Prep Batch Analytical Batch 08/16/21 17:01 W11 08/14/21 09:00 OP86829 GST3755 Run #1 Run #2 Initial Volume Final Volume 100 ml 5.0 ml Pesticide TCLP List CAS No. Compound TCLP Leachate method SW846 1311. Result HW# MCI RL MDL Units Q 58-89-9 gamma-BHC (Lindane) a ND D013 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin a ND D012 0.020 0.00020 0.000021 mg/I 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide a ND : D031 0.0080 0.00010 0.000020 mg/I 72-43-5 Methoxychlor ND . D014 10 0.00020 0.000050 mg/1 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits - 877-09-8 Tetrachloro-m-xylene 93% 42-127% 2051-24-3 Decachlorobiphenyl 53% 27-127% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit .1 = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E — Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10of`<,4 FAn7aa7 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: HOLDING BASIN (RA) Lab Sample ID: FA87897-1L Date Sampled: 08/05/21 Matrix: SO - Soil Date Received: 08/07/21 Percent Solids: 45.0 Project: City of New Bern (Biosoilds); New Bern, NC Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/I 1 08/16/21 08/16/21 LM SW846 6010D 2 SW846 3010A 3 Barium < 2.0 D005 100 2.0 mg/I 1 08/16/21 08/16/21 LM SW846 6010D 2 SW846 3010A 3 Cadmium < 0.050 D006 1.0 0.050 mg/1 1 08/16/21 08/16/21 LM 5W896 6010D 2 SW846 3010A 3 Chromium < 0.10 D007 5.0 0.10 mg/1 1 08/16/21 08/16/21 LM SWS96 6010D 2 SW846 3010A 3 Lead 0.055 D008 5.0 0.050 mg/1 1 08/16/21 08/16/21 LM SW846 60100 2 SW846 3010A 3 Mercury < 0.0050 D009 0.20 0.0050 mg/1 1 08/16/21 08/16/21 iC SW846 7470A 1 SW846 7470A 4 Seleniurn < 0.10 D010 1.0 0.10 mg/1 1 08/16/21 08/16/21 LM SW846 6010D 2 SW846 3010A 3 Silver < 0.10 D011 5.0 0.10 mg/1 1 08/16/21 08/16/21 LM SW896 6010D 2 SW846 3010A 3 (1) Instrument QC Batch: MA17944 (2) Instrument QC Batch: MA17946 (3) Prep QC Batch: MP39393 (4) Prep QC Batch: MP39395 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) 11of14 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of New Bern WQ Permit Number: WQ0023306 WWTP Name: City of New Bern WWTP Monitoring Period: From 1/1/2021 NPDES Number: To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt_ A (time/temp) 0 Alt B (Alk Treatment) ■ Alt. C (Prior Testing)❑ Alt_D (No Prior Test) ❑ Process to Further Reduce Pathogengs 7. If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost • Heat Drying ■ Heat Treatment 0 Thermophilic ❑ _ Beta Ray • Gamma Ray 0 Pasteurization CI Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens • If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying • Composting • Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen DensityNumber gExcee- of deuces Frequency of Analysis Sample Type Analytical Tech - nigue Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN <1.8 1.8 <1.8 MPN 7 bi monthl) grab n/a CFU I000 rnpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal conform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) • Alt. 4 (Spec. 02 uptake) ■ Alt. 5 (14-Day Aerobic) ■ Alt. 6 (Alk. Stabilization 0 Alt 7 (Drying - Stable) 151 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ■ Alt. 10 (Incorporation) • No vector attraction reduction alternatives were. performed 0 CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tony Hawkins / Manager Preparer Name and itle (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006)