WQ0041666_Modification_20211222

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWrvnmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
Permit Number (IR) * WQ0041666
Applicant/Permittee EMA Resources, Inc.
Applicant/Permittee Address 755 Yadkinville Rd, Mocksville, NC 27028
Is the owner in BIMS? Yes • No Is the facility in BIMS? Yes No
Owner Type Organization
Facility Name EMA Resources Class A Residuals Program
County Davie
Fee Category Minor Fee Amount $245
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer
Complete App Date 12/22/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
.............................................................................
Name* Brent Collins
Email Address*
[e-mail]
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-399-3646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
Permit Number: * WQ0041666
Has Current Existing permit number
Applicant/Permittee *
EMA Resources, Inc.
Applicant/Permittee Address* 755 Yadkinville Rd, Mocksville, NC 27028
Facility Name* EMA Resources Class A Residuals Program
High -Rate Infiltration
Reclaimed Water
Residuals
Other
Please provide comments/notes on your current submittal below.
This permit modification is requesting to add the City of Durham - Brown WTP as a source on
EMA Resources Inc.'s Class A distribution permit. Check #30363 in the amount of $245 is
being mailed today along with this submittal confirmation.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Permit Modification - WQ0041666.pdf 24.07MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617

Signature
Submission Date 12/20/2021

—Resources, Inc.
Permit Modification
For
EMA Resources Inc. - WQ0041666
Distribution of Residual Solids
(503 Exempt)
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
December 20th, 2021
Phone [phone] — Fax [phone]
755 Yadkinville Road - Mocksville, NC 27028

MA
--Resources, Inc.
December 20th, 2021
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Modification — WQ0041666
To Whom it May Concern:
EMA Resources is submitting the included permit modification for the EMA Resources
Inc. — DCAR Permit WQ0041666. We are asking to have the City of Durham — Brown
WTP Facility added as a source to our distribution permit. A check for $245.00 is being
mailed today along with the submission confirmation.
If you have any questions concerning this modification, please contact Brent Collins —
Director of Technical Services
Respectfully,
e.,?‘"‘
Brent Collins
Director of Technical Services
[e-mail]
[phone]
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
S. DANIEL SMITH
Director
ERIK BLANKENSHIP — PRESIDENT
EMA RESOURCES, INC.
755 YADKINVILLE ROAD
MOCKSVILLE, NORTH CAROLINA 27028
Dear Mr. Blankenship:
NORTH CAROLINA
Environmental Quality
July 16, 2020
Subject: Permit No. WQ0041666
EMA Resources DCAR
Distribution of Class A
Residuals
Davie County
In accordance with your permit application request received May 5, 2020, we are forwarding
herewith Permit No. WQ0041666 dated July 16, 2020, to EMA Resources, Inc. for the operation of the
subject residuals management program.
This permit shall be effective from the date of issuance through January 31, 2027, and shall be
subject to the conditions and limitations as specified therein. The Permittee shall submit a renewal
application no later than August 4, 2026.
Please pay particular attention to the monitoring requirements listed in Attachment A. Failure to
establish an adequate system for collecting and maintaining the required operational information shall result
in future compliance problems.
If any parts, requirements, or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Erick Saunders at (919)
707-3659 or [e-mail].
Sincerely,
c
TS. Daniel Smith, Director
Division of Water Resources
cc: Duplin County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Roy Whitaker — EMA Resources, Inc. (Electronic Copy)
D_E
NUN fH (:Ai(1!INA
OepaNn.nla Ennlrpnmenlai Quality
North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 11617 Mail Service Center I Raleigh, North Carolina 27699-1617
919.707.9000

Mr. Erik Blankenship
July 16, 2020
Page 2 of 2
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
EMA Resources, Inc.
Davie County
FOR THE
operation of a residuals management program for EMA Resources, Inc. and consisting of the distribution
of Class A residuals generated by the approved facility listed in Attachment A, with no discharge of wastes
to surface waters, pursuant to the application received May 5, 2020, and in conformity with other supporting
data subsequently filed and approved by the Department of Environmental Quality and considered a part
of this permit. The disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 503.
This permit does not exempt the Permittee from complying with Federal Regulation 40 CFR Part 503.
This permit shall be effective from the date of issuance through January 31, 2027, and shall be subject to
the following conditions and limitations:
L SCHEDULES
1. The Permittee shall request renewal of this permit on Division -approved forms no later than August 4,
2026. [15A NCAC 02T .0105(b), 02T .0109]
II. PERFORMANCE STANDARDS
1. The Permittee shall maintain and operate the subject residuals management program so there is no
discharge to surface waters, nor any contravention of groundwater or surface water standards. In the
event the residuals management program fails to perform satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distributing residuals, take immediate corrective actions, and contact the Winston-Salem Regional
Office supervisor. [15A NCAC 02T .0108(b)(1)(A)]
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02T
.0108(b)(1)(A)]
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this permit. [15A NCAC 02T .1101]
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4. Pollutant concentrations in distributed residuals shall not exceed the following Ceiling Concentrations
or Monthly Average Concentrations, on a dry weight basis:
Parameter
Ceiling Concentration
Monthly Average
Concentration
(mg/kg)
(mg/kg)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
N/A
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T .1105(a), 02T .1105(c)]
5. Class A biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T
.1106(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1106(a), 02T .1106(d)]
6. Class A biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC
02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107(a), 02T .1107(c)]
7. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class A land application sites are as follows (all distances in feet):
Liquid Cake
Residuals Residuals'
i. Each private or public water supply source: 100 100
ii. Surface waters such as intermittent and perennial streams, perennial 100 25
waterbodies, and wetlands:
iii. Surface water diversions such as ephemeral streams, waterways, and 25 0
ditches:
iv. Groundwater lowering ditches where the bottom of the ditch 25 0
intersects the SHWT:
v. Each well with exception of monitoring wells: 100 100
vi. Bedrock outcrops: 25 0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported
and spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast
spreader or other equipment designed for handling solid materials) without leaving any
significant liquid fraction behind.
[15A NCAC 02T .1108(b)]
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8. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the determined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.php). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T .1109(a)(1)(K)]
9. Prior to distributing Class A residuals that have a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. The Permittee
shall notify third -party entities of the effects of a high SAR content residuals on their receiving sites.
[15A NCAC 02T .0108(b)(1)(A)]
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III. OPERATION AND MAINTENANCE REQUIREMENTS
1. The Permittee shall operate and maintain the residuals management program as a non -discharge system.
[15A NCAC 02T .1100]
2. The Permittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by whom the functions are to be
conducted;
b. Description of anticipated maintenance of facilities and equipment associated with the program;
c. Include provisions for safety measures, including restriction of access to sites and equipment;
d. Spill control provisions:
i. Response to upsets and bypasses including control, containment, and remediation; and
ii. Contact information for plant personnel, emergency responders, and regulatory agencies;
e. Detailed inspection procedures:
i. Names or titles of personnel responsible for conducting inspections;
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
iii. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed;
f. Detailed sampling and monitoring procedures:
i. Names or titles of personnel responsible for conducting sampling and monitoring;
ii. Description of monitoring procedures including parameters to be monitored; and
iii. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
[15A NCAC 02T .1110(a)]
3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T .0117, 08G .0204]
4. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying bulk Class A residuals. [15A NCAC 02T .1110(b)]
5. The Permittee shall ensure that spill control provisions are available when transporting or land applying
bulk Class A residuals. [15A NCAC 02T .1110(a)(4)]
6. Class A residuals may be staged at the land application site for up to 30 days for biological residuals
and 60 days for non -biological residuals. Class A residuals shall be stored or staged in a manner to
prevent runoff of leachate and other wastewaters generated. [15A NCAC 02T .1110(c), 02T .1110(d)]
7. Adequate measures shall be taken to prevent wind erosion and runoff from the bulk Class A residual
land application sites. [15A NCAC 02T .0108(b)(1)(A)]
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8. Bulk Class A residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event;
f. During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period;
If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated;
h. If the land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals;
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot;
j. If the vertical separation of the depth to bedrock and the depth of residuals application is less than
one foot;
k. If the application exceeds agronomic rates; or
1. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B .0212
or within the Critical Area of a WS-II pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-III or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NCAC 02B .0215, and .0216.
[15A NCAC 02T .1109(a)(1), 02T .1109(b)]
g-
9. The Permittee shall notify all third -party entities receiving bulk Class A residuals that land application
activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T
.1108(b) and 02T .1109(a)(1) (i.e., Conditions II.7.a. and III.8., respectively). [15A NCAC 02T
.1103(a)(4), 02T .1103(a)(5)]
10. Bagged or other container Class A residuals shall have an affixed label or an information sheet provided
to the person receiving the Class A residuals. The label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[15A NCAC 02T .1109(c)]
11. The Permittee shall not distribute bulk Class A residuals to any person or entity known to be applying
residuals contrary to the conditions of this permit. The Permittee shall report to the Winston-Salem
Regional Office any person or entity known to be applying residuals contrary to the conditions of this
permit. [15A NCAC 02T .0108(b)(1)(A)]
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IV. MONITORING AND REPORTING REQUIREMENTS
1. The Permittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [15A NCAC 02T .0108(c)]
2. The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses
(i.e., corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall be
performed at the frequency specified in Attachment A, and the Permittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall be specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Heptachlor (and its epoxide)
(0.008)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Hexachlorobenzene (0.13)
Toxaphene (0.5)
Chloroform (6.0)
Hexachlorobutadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
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3. The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Permittee shall maintain the results for a minimum of five years. Each analysis
shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T .1101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class A pathogen reduction
requirements in 15A NCAC 02T .1106(a), and one vector attraction reduction requirement in 15A
NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1106(a), 02T .1107(a), 02T .1111(c)]
5. Representative samples of residuals that are prepared for distribution shall be collected and analyzed.
[15A NCAC 02T .1111(a)]
6. The Permittee shall maintain records for all bulk Class A residual distribution events. These records
shall include the following:
a. Residuals source (as listed in Attachment A);
b. Date of distribution;
c. Name and address of residuals recipient;
d. Volume of residuals distributed to each recipient; and
e. Intended use of residuals.
[15A NCAC 02T .0108(c)]
7. One hard copy and one electronic copy of an annual report shall be submitted on or before March 1st
The annual report shall meet the requirements described in the Instructions for Residuals Application
Annual Reporting Forms. Instructions for reporting and annual report forms are available at
http://deq.nc. gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/non-
discharge-permitting-unit/reporting-forms, or can be obtained by contacting the Non -Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .1111(d)]
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8. Noncompliance Notification
The Permittee shall report to the Winston-Salem Regional Office, telephone number [phone],
within 24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
limitations.
d. Distribution of residuals abnormal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emergencies requiring reporting outside normal business hours shall call the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone]. All
noncompliance notifications shall file a written report to the Winston-Salem Regional Office within
five days of first knowledge of the occurrence, and this report shall outline the actions proposed or
taken to ensure the problem does not recur. [15A NCAC 02T .0108(b)(1)(A)]
V. INSPECTIONS
1. The Permittee shall perform inspections and maintenance to ensure proper operation of the Permittee's
storage and distribution facilities. [15A NCAC 02T .1110(f)]
2. The Permittee shall inspect the Permittee's residuals processing, storage, and transport facilities to
prevent malfunctions, facility deterioration, and operator errors that may result in discharges of wastes
to the environment, threats to human health, or public nuisances. The Permittee shall maintain an
inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be made available to the Division upon request.
[15A NCAC 02T .0108(b)(1)(A), 02T .1110(f)]
3. Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the distribution sites or facilities permitted herein at any
reasonable time for determining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the terms and conditions of this permit, and may collect
groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)]
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VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a
Division enforcement action. [G.S. 143-215.6A, 143-215.6B, 143-215.6C]
2. This permit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-215.1(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T .0105(n)]
4. The issuance of this permit does not exempt the Permittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [15A NCAC 02T .0105(c)(6)]
5. If the permitted residuals program change ownership, or the Permittee changes their name, the
Permittee shall submit a permit modification request on Division -approved forms. The Permittee shall
comply with all terms and conditions of this permit until the permit is transferred to the successor -
owner. [G.S.143-215.1(d3)]
6. This permit is subject to revocation or modification upon 60-day notice from the Division Director, in
whole or part for:
a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subchapter
02T;
b. obtaining a permit by misrepresentation or failure to disclose all relevant facts;
c. the Permittee's refusal to allow authorized Department employees upon presentation of credentials:
i. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
ii. to have access to any permit required documents and records;
iii. to inspect any monitoring equipment or method as required in this permit; or
iv. to sample any pollutants;
d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or
e. a Division determination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[15A NCAC 02T .0110]
WQ0041666 Version 1.0 Shell Version 200201 Page 9 of 10

7. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not
occur if any of the following apply:
a. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of
environmental crimes under G.S. 143-215.6B, or under Federal law that would otherwise be
prosecuted under G.S. 143-215.6B, and all appeals of this conviction have been abandoned or
exhausted.
b. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Permittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid an annual
fee.
[15A NCAC 02T .0120(b), 02T .0120(d)]
8. This permit shall not be renewed if the Permittee or any affiliation has not paid the required annual fee.
[15A NCAC 02T .0120(c)]
Permit issued this the 16th day of July 2020
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Daniel Smith, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0041666
WQ0041666 Version 1.0 Shell Version 200201 Page 10 of 10

ROY COOPER
Governor
DIONNE DELLI-GATTI
Secretary
S. DANIEL SMITH
Director
ERIK BLANKENSHIP — PRESIDENT
EMA RESOURCES, INC.
755 YADKINVILLE ROAD
MOCKSVILLE, NORTH CAROLINA 27028
Dear Mr. Blankenship:
NORTH CAROLINA
Environmental Quality
March 25, 2021
Subject: Permit No. WQ0041666
EMA Resources DCAR
Attachment A Certification
Davie County
In accordance with your permit major modification request received February 25, 2021, we are
forwarding herewith a modified Attachment A certified March 25, 2021, to EMA Resources, Inc. for the
subject residuals management program.
Modifications to the subject Attachment are as follows: Addition of the John J. Kime WTP (Permit
No. NC0087866) as a residuals source, with an approved dry tonnage of 1,035 dry tons/yr (DT/yr).
The modified Attachment A shall be effective from the date of certification until January 31,
2027 (i.e., expiration date of the current permit), shall void Attachment A of Permit No. WQ0041666
issued July 16, 2020, and shall be subject to the conditions and limitations as specified therein, as well as
those specified in the above -referenced permit. Please replace Attachment A of Permit No. WQ0041666
that was issued July 16, 2020 with the modified Attachment A. Please note that the Permittee shall
submit a renewal application no later than August 4, 2026.
If any parts, requirements or limitations contained in this certification are unacceptable, the
Permittee has the right to request an adjudicatory hearing upon written request within 30 days following
receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding.
If you need any additional information concerning this matter, please contact Erick Saunders at
[phone] or [e-mail].
cc: Davie County Health Department (Electronic Copy)
Randolph County Health Department (Electronic Copy)
Sincerely,
7-.,.,...
S. Daniel Smith, Director
Division of Water Resources
D_E
NORTH CAROLINA
Ifapa aM of Emlranmpulal Ouallry
---
North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 116I7 Mail Service Center I Raleigh, North Carolina 27699-1617
919.707.9000

Mr. Erik Blankenship
March 25, 2021
Page 2 of 2
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Brent Collins — EMA Resources, Inc. (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

ATTACHMENT A — APPROVED RESIDUAL SOURCES
EMA Resources, Inc.
Certification Date: March 25, 2021
Permit Number: WQ0041666 Version: 1.1
Owner
Facility Name
County
Permit
Number
Biological
Residuals
Maximum
Dry Tons
per Year 1
Monitoring
Frequency for
Non-hazardousz
Characteristics
Monitoring
Frequency for
Metals and
Nutrients
Monitoring
Frequency for
Pathogen &
Vector Attraction
Reductions 4, 5
Approved
Mineralization
Rate
Lear Corporation
Lear Corporation WWTP
Duplin
NC0002305
Yes
318
Annually
Annually
Annually
0.3
Piedmont Triad Regional
Water Authority
John F. Rime WTP
Randolph
NC0087866
No
1,035
Annually
See Table Below
-
0.4
Total
1,353
1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IV. 4.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Applied (metric tons)
Dry Tons Applied
(short tons per year)
Monitoring Frequency
(40 CFR 503 and 15A NCAC 02T
.1111(c))
< 290
< 319
Once per year (Annually)
> 290 to < 1,500
> 319 to < 1,650
Once per quarter (4 x Year)
>
1,500 to < 15,000
>
1,650 to < 16,500
Once per 60 days (6 x Year)
> 15,000
> 16,500
Once per month (12 x Year)
If no land application events occur during a required sampling period (e.g., no land application occur during an entire year when annual monitoring is required), then no sampling data is
required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to United States Environmental
Protection Agency (US EPA) may be required to make up the missed sampling. Contact the US EPA for additional information.
WQ0041666 Version 1.1 Attachment A
Page 1 of 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: EMA Resources Inc.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Erik Blankenship Title: President
Applicant's mailing address: 755 Yadkinville Rd
City: Mocksville State: NC Zip: 27028-
Telephone number: [phone] Email Address: erik.blankenship(a(emaresourcesinc.com
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip:
Telephone number: ( ) - Email Address:
3. Fee submitted: $245 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0041666
Date of most -recently issued permit: 7/16/2020
Date of most -recently certified Attachment A (if different than the permit): 3/25/2021
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Source Specific
City: State: Zip:
Coordinates: Latitude: _° _' " Longitude: _ _' "
Datum: Level of accuracy:
Method of measurement:
County where facility is located:
2. Facility contact (person familiar with residuals preparation):
Name: Title:
Mailing address:
City: State: Zip:
Telephone number: ( ) E-mail address:
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? ❑ Yes; ® No
If No, please specify delivery frequency and quantity of residual to be processed: Source Specific
4. Length of residuals storage at facility: Source Specific days (Note: the Division requires minimum 30 days storage in units that
are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); Residuals will be land applied by EMA Resources Inc. at agronomic rates
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
per 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: Source Specific dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: Source Specific dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Source Specific
6. Does the facility have a stormwater management plan? ❑ Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled. Source Specific
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
I, , attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
Yes ❑ No, Explain;
I,
Erik Blankenship President
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for EMA Resources Inc.
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Erikggarn Hfh1
Signature: Erik Blankenship l ID, LR1 43 EST)
Date: Dec 20, 2021
FORM: DCAR 06-16 Page 3 of 3

DCAR-06-1 6
Final Audit Report
2021-12-20
Created: 2021-12-20
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAbVJRt8nJ0XepUcZn7wbWCe-JPeW-BoOw
"DCAR-06-1 6" History
e Document created by Brent Collins ([e-mail])
2021-12-20 - 2:36:11 PM GMT- IP address: 24.88.129.34
Document emailed to Erik Blankenship ([e-mail]) for signature
2021-12-20 - 2:36:30 PM GMT
Email viewed by Erik Blankenship ([e-mail])
2021-12-20 - 2:42:04 PM GMT- IP address: 173.94.78.101
Document e-signed by Erik Blankenship ([e-mail])
Signature Date: 2021-12-20 - 2:43:20 PM GMT - Time Source: server- IP address: 173.94.78.101
Q Agreement completed.
2021-12-20 - 2:43:20 PM GMT
Ea Adobe Sign

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: EMA Resources Inc.
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
N
City of Durham
Brown WTP
Durham
PWS 03-32-010(A)
1500
1500
-
Piedmont Triad Regional
Water Authority
John F. Kime WTP
Randolph
NC0087866
1035
1035
-
Lear Corporation
Lear Corporation WWTP
Duplin
NC0002305
318
318
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16
Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Durham — Brown WTP
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Tom Lucas — WTP ORC
Complete mailing address: 101 City Hall Plaza
City: Durham
State: NC Zip: 27701-
Telephone number: [phone] E-mail address: [e-mail]
4. Facility physical address: 7297 Adams Fard Rd
City: Durham State: NC Zip: 27712-
Coordinates: Latitude: 36' 05' 29" Longitude: 78' 52' 21"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: MAP
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: • % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 30 MGD and facility average daily flow: 27.3 (both WTPs) MGD
8. Average amount of residuals being generated at this facility 1650 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Water treatment process
Type and volume of residuals storage (i.e., outside of residuals treatment units): Approximately '/2 acre covered storage pad
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit Environmental Labs and Date of analysis: 5/4/2020
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: Z yes E no. Flashpoint: >179 °F (> 140°F)
Passed reactivity test: • yes Eno. HCN: - mg/kg (<250) & H2S: I d mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page
2
of
5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 04/15/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<12.5
Cadmium
85
39
2.99
Copper
4,300
1,500
354
Lead
840
300
<7.5
Mercury
57
17
<0.074
Molybdenum
75
n/a
<6.25
Nickel
420
420
31.6
Selenium
100
100
<12.5
Zinc
7,500
2,800
76
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ >0but<25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page
3
of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 20 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 04/15/2020
Parameter
Result
(mg/kg)
Aluminum
9050
Ammonia -Nitrogen
1200
Calcium
<625
Magnesium
302
Nitrate -Nitrite Nitrogen
<23.8
pH (Standard Unit)
5.4
Phosphorus
815
Potassium
171
Sodium
<625
Total Kjeldahl Nitrogen
12,700
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.29
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 10 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1st) Year PAN
(mg/kg)
Five -Year
Maximum Adjusted PAN
(mg/kg)
Surface
1,774
2,464
Injection/Incorporation
2,374
3,064
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concem in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page
4
of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 115A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 115A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 115A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 115A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 115A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 115A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 115A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, In air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt - If Daily Cover Alternative is chosen in Item II.8. below 115A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 115A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 115A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 115A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 115A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 115A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 115A NCAC 02T.1107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 115A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 115A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 115A NCAC 02T.1107(a)(9)] - Injection.
❑ Alternative 10 115A NCAC 02T.1107(a)(10)1 - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover 115A NCAC 02T.1107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Standard Operating Procedure and Operation
and Maintenance Plan for Brown WTP Residuals
EMA Resources Inc. Permit
Land Application Program - WQ0041666
1. Purpose
a. Ensure the requirements of EMA Resources Inc. Permit# WQ0041666 are
met.
2. Personnel
a. The following is a list of personnel in order they are to be contacted when
information needs to be shared.
i. EMA Resources Inc.
1. David Ackley — Project Manager — 419-212-3699
2. Brent Collins — Director of Technical Services — 336-399-3646
3. Roy Whitaker — Director or Marketing — 336-909-1718
4. Mike Collins — Director of Operations — 336-399-6670
ii. City of Durham
1. Tom Lucas — WTP ORC — 919-560-4362 x35267
3. Operational Functions
a. The operational function of this project will involve trucking cake residuals
to agronomic sites. It is going to be spread at agronomic rates that are
determined using the Realistic Yield Expectations (RYE) as outlined in the
permit, the amount of other nutrient sources the landowner and operator
has applied, and the residuals nutrient and metal sample that is current for
that monitoring period. It is going to be spread with a cake applicator that
will use an auger and paddles to spread the material in such a way as to

achieve a consistent spread pattern. The material is going to be land
applied on fields that have a crop growing on them that are going to either
be grazed or cut for animal feed. Application rates will be reduced by 25%
on fields that are primarily used for grazing in accordance with USDA-NRCS
590. Grazed fields will be determined by the farmers and EMA project
managers.
4. Maintenance Schedule
a. EMA Resources Inc. will follow the maintenance schedule as recommended
by the EMA Resources Director of Operations (Mike Collins) for the
equipment necessary to complete the job.
5. Safety Measures
a. City of Durham -Brown WTP and EMA Resources Inc. believe in operating in
a safety conscious manner and all employees participate in safety training
that is designed to help employees recognize safety issues and take steps
to prevent accidents from occurring. In addition, EMA Resources employees
have the authority to stop operations if they think any aspect of the
operation is going to cause environmental or personal harm.
6. Spill Response Plan
a. In the unlikely event of a spill, the following action shall be taken
immediately.
i. Management of Spill Clean-up Activities: The EMA Resources
Project Manager shall take immediate charge and initiate clean-up
activities. EMA Resources labor and equipment is to be utilized. In
the event additional labor and equipment is required, assistance may
be requested from the City of Durham, The NC Department of
Transportation, and other private contractors as necessary.
ii. Halt the Source of the Spill: Such as a ruptured container or
damaged transport unit.
iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall
be used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The
Operations Manager or the person in charge on the spill site will
advise the clean-up personnel where to get the straw, lime, and other

items necessary to complete the clean-up operation. ie. local farmers,
farm supply centers, nurseries.
iv. Initial Clean -Up: Employ front-end loaders, vacuum equipment,
sludge application vehicles, and/or local septic tank service to
remove as much of the spilled material as possible. Straw and/or
sand should be scattered in the spill area to soak up the remaining
material. The straw and sand soaked material will be collected and
removed to a disposal area approved by representatives of the state
regulatory agency.
v. Final Clean -Up: Employ rotary brush sweeper if needed and apply
lime to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private
property, the clean-up will be completed to the satisfactory of the
property owner and state regulatory representatives. The ultimate
goal will be restore the spill area to its original condition if possible.
vi. Notification: As soon as possible after the spill occurs, the EMA
Resources Project Manager or designee will notify the City of Durham
and the EMA Resources main office. EMA Resources office staff are
then responsible for notifying other key EMA Resources personnel.
vii. Reporting: EMA Resources staff will notify the Raleigh Regional
office of NCDENR by telephone [phone] as soon as possible,
but not more than 24 hours after, or on the next working day
following the occurrence. The EMA Project Manager shall provide a
written report within 48 hours of the spill to the EMA Resources
Director of Technical Services and City of Durham staff. The report
shall list all relative information and actions taken. With the
assistance of EMA Resources personnel, and City of Durham
personnel, a written report will be filed with the Raleigh Regional
office within 5 days of the occurrence. For after-hours reporting, the
Division's emergency number shall be called to report all incidences
[phone].
7. Inspection Plan
a. Inspection for the land application of residuals will be conducted on a
minimum of a weekly basis at the land application site during land
application activities. The inspection frequency is based on the time frame

that it is going to take to complete the project and the amount of dry tons
to be land applied from this facility. The inspections will consist of
inspecting a current field that is being applied as well as inspecting random
fields that have been completed. Inspections will be conducted by David
Ackley — Project Manager. These inspections will consist of the following:
i. Verifying the application rates for each field that plan on receiving
material.
ii. Checking the calculated loads to ensure the correct amount of
residuals are being land applied.
iii. Ensure that all manned equipment has a copy of the permit and the
operation and maintenance plan.
iv. Ensure that the field has been flagged properly and that all buffers
are being adhered to.
v. Verify that the proper number of samples of the residuals have been
taken and that it meets the criteria for land application.
vi. The records will be kept in the EMA Resources project files in the
main office.
vii. EMA Resources and City of Durham staff will immediately inform the
other party if any of the following conditions are noted.
1. Any occurrence with the distribution program resulting in the
land application of significant amounts of material that is
abnormal in quantity or characteristics.
2. Any failure of the distribution system that results in the release
to surface waters.
3. Any time that self -monitoring indicates that the facility has
gone out of compliance with the permit.
4. Any process failure that results in the system not adequately
treating the residuals.
5. Any spill or discharge from a vehicle or piping system during
residuals transportation.
6. Any release that requires immediate reporting outside normal
business hours shall be called in by EMA Resources staff to
DENR at [phone]. This number is to be called in the
event of a release to surface waters or imminent failure of a

storage system when the event occurs outside of normal
business hours.
8. Sampling and Monitoring Plan
a. Sampling for this project consists of sampling the residuals prior to land
application occurring in order to ensure that the residuals are suitable for
land application.
b. The samples will be collected from the storage pad that holds the residuals
c. David Ackley, Brent Collins, Roy Whitaker or other designee will be
responsible for sample collection for nutrient and metal, TCLP, and soil
samples.
d. Nutrient, metal and TCLP sample aliquots will be collected randomly and
consist of at least 7 individual aliquots mixed together in order to get the
composite sample for these parameters.
e. The residuals will be sampled annually for TCLP including the RCIIs.
f. Metal and nutrient parameters will be collected and analyzed based on the
requested dry ton numbers in the permit application.
9. Environmental Impacts
a. The environmental impacts for residuals may be affected by this procedure.
b. This procedure helps assure that land application is conducted in a safe and
efficient manner while ensuring compliance with the laws and regulations
and to minimize exposure, negative environmental impacts and public
relation concerns.

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Property Boundary
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SCALE:
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DATE: 12-19-21
DRAWN BY: BC
' PROJECT NO:
` WQ0041666
AMA
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City of Durham - WTP
EMA Resources Inc.
FIGURE NO.
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C:\Users\letsg\Documents\ArcGIS\GIS Data\Durham\Maps\Plan

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DATE:
DRAWN BY:
PROJECT NO:
\ WQ0041666
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EMA Resources Inc.
FIGURE NO.
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C:\Users\letsg\Documents\ArcGIS\GIS Data\Durham\Maps\Plan

Program Information
1. Provide a narrative explaining the following:
a. How will the materials be handled and transported from where the residuals were
produced to where it will be treated?
The residuals are produced through non -biological water treatment processes at the
Brown WTP. See process flow. Liquid material from the Williams WTP is trucked to the
Brown WTP and comingled before being pressed using their belt filter press. Once the
residuals have been dewatered, they will be stored at the on -site pad. When the residuals
are ready to be land applied, they will be taken to agricultural sites by EMA Resources
and land applied at agronomic rates.
b. How will the residuals be processed/treated?
See Process flow diagram and narrative.
c. Where will the residuals be stored until processing?
The residuals will be stored at their approximately '/2 acre covered cake storage pad.
d. How will the fmal product be distributed?
The residuals will be delivered to local farmers via end clump trailers. Each load will be
off-loaded to a high flotation applicator for application on a receiver site (grassland or
row crop).

Brown WTP Marketability Statement
Residuals will be given to local farmers for crop production. EMA Resources Inc. will land apply the
material for the local farmers who have chosen to receive the product. Cake spreaders will be utilized
to spread the material in a consistent and even manner. The material will be applied to fields that have
a cover crop growing, either grass for hay production, pasture, or row crops. Agronomic rates will be
determined using the Realistic Yield Website through NC State.

EMA Resources Inc.
Land Application Permit WQ0041666
Label for Land Application
The residuals that are land applied are produced at the Brown WTP at: 1615 Infinity Road, Durham, NC
27712. Mr. Tom Lucas, Brown Water Treatment ORC is the preparer of the residuals and responsible for
the plant operations.
The residuals from the Brown WTP will be land applied at agronomic rates based on the Realistic Yield
Expectation rate for the fields and crops to be grown. The WTP residuals will not be applied to frozen,
snow covered or flooded fields. The fields will be flagged with the following buffers to help prevent
runoff from the applied fields.
Cake Residuals
Each private or public water supply source:
100
Surface waters such as intermittent and perennial streams, perennial
waterbodies, and wetlands:
25
Surface water diversions such as ephemeral streams, waterways, and
ditches:
0
Groundwater lowering ditches where the bottom of the ditch intersects
the SHWT:
0
Each well with exception of monitoring wells:
100
Bedrock outcrops:
0
Residuals produced by the Brown WTP will be applied to agricultural fields in bulk and will be land
applied according to this label as well as following all permit conditions listed in the land application
permit WQ0041666.
Adequate procedures will be followed to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.

BROWN WTP RESIDUALS FLOW PROCESS SCHEMATIC 2021
Backwash Clarifiers
Cake Storage Shed
Thickened Solids
Holding Tanks
Belt Press
Dewatering
Gravity Thickeners
Backwash
Eq Tanks
Settled
Solids Tanks

BROWN WTP RESIDUALS FLOW PROCESS SCHEMATIC 2021
Backwash from
Filters
Sludge from
Sedimentation
Basins
Backwash
Equalization
Basins
Filtrate goes to
Sanitary Sewer
Settled Solids
Basins
Backwash
Clarifiers
Filtrate goes to
Filtrate EQ
Tanks
Gravity
Thickeners
1
Belt Press
Dewatering
Clarified Water goes
back to Terminal
Reservoir
Thickened
Solids Holding
Tanks
Pressed Cake
goes to the
Cake Storage
Shed
Thickened
Sludge from
Williams
Cake is either
Land Applied or
Landfilled

Quantitative Justification for Residuals Production Rate
Facility:
City of Durham — Brown WTP
Requested Permitted Rate:
1500 dry tons/year
Justification:
We are requesting a permitted dry tonnage rate of 1500 dry tons of water plant
residuals. This number is based on past data from their previous contractor and an
expected increase in their production. This number includes the contributions from the
Williams WTP material that is comingled and pressed at the Brown WTP.

Sunnrit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TtCH 1OL.JCI S, € #C Cuyahoga Falls, Ohio 44223
Analytical Labaatorio , TEL: [phone] FAX: [phone]
JVebsite: httn://tvww.sellek-con
May 06, 2020
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Durham Brown
Dear Ryan Copeland:
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/24/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Order No.: 20041280
Quality control data is within Laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
.�rjyf..r�l/�s�jOpls
rr
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0€08, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-01-1-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada 0E1009232020.1, New
Hampshire 2996, New)ersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH200001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah 0H009232920-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 31

ENVIRONMENTAL TECHNOLOCWES,1
Analytical Laboratories
Sunmrit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://i'ww.setiek.coin
Case Narrative
WOiI: 20041280
Date: 5/6/2020
CLIENT: Synagro
Project: Durham Brown
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler
Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Comments for HGPrep {7470), Sample mb2-43232: 22.5 ml of KMnO4 added.
Original
Page 2of31

Analytical LaGoratorlofi
Suni,nit Environmental Technologies, In
3310 Win
NVltt0NtAENTALTEcHtvoL0CI! S, lhfG, Cuyahoga Falls, Ohio 442.
TEL: [phone] FAX: [phone]
Websiie: htlp://www,settek.co
Qualifiers and Acronyms
W O#: 20041280
Date:
5/6/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
11 The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
x The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS,
X The result was not confirmed when GC/MS Analysis was performed.
BIMB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+),
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
QC
MB
LCS
LCSD
QCS
DUP
MS
MSD
RPD
ICV
ICB
CCV
CCD
RLC
Dr
Not Detected
Quality Control
Method Blank
Laboratory Control Sample
Laboratory Control Sample Duplicate
Quality Control Sample
Duplicate
Matrix Spike
Matrix Spike Duplicate
Relative Percent Different
initial Calibration Verification
Initial Calibration Blank
Continuing Calibration Verification
Continuing Calibration Blank
Reporting Limit Check
Dilution Factor
RL
MDL
L01)
LOQ
PQL
CRQL
PL
RegLvl
MCL
MinCL
RA
RE
TIC
RT
CF
RF
Reporting Limit
Method Detection Limit
Level of Detection
Level of Quantitation
Practical Quantitation Limit
Contract Required Quantitation Limit
Permit Limit
Regulatory Limit
Maximum Contamination Limit
Minimum Compound Linnit
Reanalysis
Reextraction
Tentatively Identified Compound
Retention Time
Calibration Factor
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3of31

Suntan! Environmental Technologies, Inc.
3310 Win St.
E NVIfONME JTAL1!CH 1OL.0G11 S, SfYt Cuyahoga Falls, Ohio 44223
I niVyticaf Laboratori6,s TEL: [phone] FAX: [phone]
YVebsite: http:/hrww.seltek.conn
Workorder
Sample Summary
WO#: 20041280
06-May-20
CLIENT:
Pro j ect:
Synagro
Durham Brown
Lab SampleID Client Sample ID
20041280-001 Durham Brown WTP
Tag No Date Collected
4/23/2020 11:30:00 AM
Date Received
4/24/2020 10:10:00 AM
Matrix
Studgc
Page 4of31

Sunni! Environmental Technologies, Inc.
3310 Win Sr.
EHVIn4Nkl0N7AL tooHNOLClt40, MG, Cuyahoga Falls, Okla 44223
Analytical Laboratories 7EL: (330) 253-821! FAX: [phone]
We,site: hop:/Aswse.seack.com
DATES REPORT
wort: 200412S0
0644-20
Client: Synagro
Project: Durham Brown
Sample ill
Client San:pte ID
Collection Date Matrix
Test Nance Leaehate Date
Prep Date
Analysis Date
20041280-001 A Durham Drown WTP 4/2312020 11:30.00 AM Sludge Ignitability or Solids (SW-846: 1030)
Paint Filter Free Liquids Test (SW-846
pit (SW9045D)
Reactive Cyanide (901417.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides by 1/PA 83210
TCLP Mercury Analysis (SW 13I 1/7474/29/2020 2:00:00 PM
TCLP Metals Analysis (SIV 13 €1/6010 4/29/2020 2:00:00 PM
TCLP Metals Analysis (SW 1311 /6019 4/29/2020 2:00:00 PM
TCLP Pesticides Analysis (SW1311/8(4/29/2020 2:00:00 PM
TCLP Semi-Volatiles Analysis 4129/2020 2:00:00 PM
(SW 1311/8270)
TCI,P Volatiles Analysis
Page 5 of 31
4/29/2020 2:00:00 PM
5/1/2020 9:55:00 AM
4/30/2020 9:40:00 AM
4/30/2020 1:00:00 PM
4/30/2020 1:00:00 PM
4/29/2020 2:00:00 PM
511/2020 3:00:00 PM
4129/2020 8:30:00 AM
4/30/2020 10.07:00 AM
4/27/2020 9:09:00 AM
4/27/2020 9.09:00 AM
5/2/2020 6:32:00 AM
5/1/2020 1:07:00 PM
5/1/2020 2:49:45 PM
5/1/2020 I :31:46 PM
5/4/2620 7:27:00 PM
5/4/2020 3:38:00 PM
4/30/2020 1:09:00 PM
Original

Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TEctulmt,oGiCs, IIYO, Cuyahoga Falls, Ohio 44223
Analytical LaBorator/es TEL: [phone] FAX• [phone]
YVebsite: http://www.setlek.com
Analytical Report
(base report)
WO#: 20041280
Date Reported: 5/6/2020
CLIENT:
Matrix:
Lab ID:
Project:
Client Sample
Synagro
SLUDGE
20041280-00IA
Durham Brown
ID Durham Brown WTP
Tag Number:
Collection Date: 4/23/2020 1 1 :30:00 AM
Analyses
Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00200
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
ND
ND
NO
ND
ND
ND
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluoroblphenyl
Surr: p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
ND
85.6
85.2
72.7
116
86.1
123
mg/L
SW7470A SW7470A Analyst: MJM
SW6010D
5/1/2020 1:07:00 PM
Analyst: EAM
0.500 mg/L 1 5/1/2020 1:31:46 PM
5.00 mglL 1 5/1/2020 1:31:46 PM
0.100 mg1L 1 5/1/2020 1:31:46 PM
0.200 mg1L 1 5/1/2020 1:31:46 PM
0.500 mg/L 1 5/1/2020 1:31:46 PM
0.0500 mg/L 1 5/1/2020 1:31:46 PM
0.500 mg/L 1 5/1/2020 2:49:45 PM
SW8270 SW3510C Analyst: SFG
0.200 m9/L 2 5/4/2020 3:38:00 PM
0.500 mg/L 2 5/4/2020 3:38:00 PM
0.500 mg1L 2 5/4/2020 3:38:00 PM
0.100 mg/L 2 5/4/2020 3:38:00 PM
10.0 mg/L 2 5/4/2020 3:38:00 PM
0.0400 m0/L 2 5/4/2020 3:38:00 PM
0.100 mg/L 2 5/4/2020 3:38:00 PM
0.200 m0/L 2 5/4/2020 3:38:00 PM
0.200 mg1L 2 5/4/2020 3:38:00 PM
0.500 mg/L 2 5/4/2020 3:38:00 PM
0.500 mg/L 2 5/4/2020 3:38:00 PM
10 - 109 %Rec 2 5/4/2020 3:38:00 PM
10 - 109 %Rec 2 5/4/2020 3:38:00 PM
19 - 120 %Rec 2 5/4/2020 3:38:00 PM
10 - 120 %Rec 2 5/4/2020 3:38:00 PM
22 - 117 %Rec 2 5/4/2020 3:38:00 PM
34 - 116 S %Rec 2 5/4/2020 3:38:00 PM
Qualifiers:
B Analyte detected in the associated Method Blank
H Holding tines for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E
M
N
1'
R
U
Value above quantitation range
Manual Integration used to determine area response
Tentatively identified compounds
Second column confirmation exceeds
RPD outside accepted recovery limits
Samples with CalcVal <MDL
Original
Page 6 of 31

Summit Environmental Technologies, Inc.
3310 IVin St.
ON/Ma-AL TtcHot,0Gt5S, triC Cuyahoga Falls, Ohio 44223
Analytical Larsoratorie8- TEL: [phone] FAX: [phone]
WVebsite: hrtp://u'u'u.settek.cont
Analytical Report
(base report)
WO#: 20041280
Date Reported: 5/6/2020
CLIENT:
Matrix:
Lab ID:
Project:
Synagro
SLUDGE
20041280-001A
Durham Brown
Client Sample ID Durham Brown WTP
Tag Number:
Collection Date: 4/23/2020 11:30:00 AM
Analyses
Result RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epoxide
Methoxychlor
Surr: TCMX
Surr: DCB
TCLP HERBICIDES BY EPA 8321 B
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic aci
ND
ND
ND
ND
ND
ND
ND
19.6
18.2
ND
ND
105
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-B rom ofluorobenzene
Surr: Dibromofluoromethane
Surf: Toluene-d8
ND
ND
ND
ND
ND
ND
ND
NO
ND
ND
91.2
102
99.9
0.125 mg/L 5
0.250 mg/L 5
0.0125 mg/L 5
0.0125 mg/L 5
0.0125 mg/L 5
0.0125 mg/L 5
0.0125 d mg/L 5
10-119 %Rec 5
10-119 %Rec 5
0.500
0.500
70-130
SW8321A
mg/L
mg/L
%Rec
0.250 mg/L
0.250 mg/L
5.00 mg/L
0.250 mg/L
0.250 mg/L
2.50 mg/L
0.250 mg/L
0.250 mg/L
0.250 mg/L
0.100 mg/L
70-130 %Rec
70 - 130 %Rec
70-130 %Rec
SW8260
SW3510C Analyst: MES
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
5/4/2020 7:27:00 PM
SW1311 M Analyst: BJH
50 5/2/2020 6:32:00 AM
50 6/2/2020 6:32:00 AM
50 6/2/2020 6:32:00 AM
SW1311M Analyst: RMT
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
50 4/30/2020 1:09:00 PM
Qualifiers:
B
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Pennit Limit
Reporting Detection Limit
E Value above quantization range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with CaleVat < MDL
Original
Page 7 of 31

ElkiVllIONMEWAL TECI1NOLOri
AnalytIca1 Laboratories
tPIc
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX• [phone]
Website: http://www.settek.coda
Analytical Report
(base report)
WO#: 20041280
Date Reported: 5/6/2020
CLIENT:
Matrix:
Lab ID:
Project:
Synagro
SLUDGE
20041280-001 A
Durham Brown
Client Sample ID Durham Brown WTP
Tag Number:
Collection Date: 4/23/2020 11:30:00 AM
Analyses Result
RL Qual Units
DF Date Analyzed
RCI-SOLID-WI IGNITABILITY1030 SW9014
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND 0.490 mg/Kg
PAINT FILTER FREE LIQUIDS TEST (SW-846: 9095) SW9095
Free Liquid pass
RCI-SOLID-WI IGN1TABILITY1030 SW1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
pH
RCI-SOLID-WI IGNITABILITY1030
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive
non-flammable
6.1
ND 25.0
mmisec
1
1
Analyst: MS
4/27/2020 9:09:00 AM
Analyst: DHC
4/29/2020 8:30:00 AM
Analyst: AJT
5/1/2020 3:00:00 PM
SW9045D Analyst: DI -IC
s.u.©21.90 1 4/30/2020 10:07:00 AM
SW9034 Analyst: MS
mg/Kg
1 4/27/2020 9:09:00 AM
Qualifiers:
B
1-I
MC
ND
PI.
RL
Analyte detected in the associated Method Blank
Holding tunes for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with CalcVal < MDL
Original
Page 8of31

Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL ITCttfi3oL.4Glps, li C. Cuyahoga Falls, Ohio 44223
Analytical L.01.)0a'otor1eg TEL: [phone] FAX' [phone]
Website: hllp://w3vn'.settek.cont
Accreditation Program
Analytes Report
WO#: 20041280
06-May-20
Client: Synagro State: NW
Project: Durham Brown
Program Name: NC_WWSCM
Sample ID Matrix
'fest Name
Analyte Status
20041280-00IA
Sludge lgnitability of Solids (SW-846: 1030) lgnitability A
Sludge Paint Filter Free Liquids Test (SW-846: 9095) Free Liquid N
Sludge p11(SW9045D) Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive N
Sludge Reactive Sulfide (9034)/7.3.4:2 Sulfide, Reactive N
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis (SW 1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis (SW1311/6010) Barium A
Sludge TCLP Metals Analysis (SW 1311/6010) Cadmiutn A
Sludge "TCLP Metals Analysis (SW 1311/6010) Chromium A
Sludge TCLP Metals Analysis (SW 13 1 1/6010) Lead A
Sludge TCLP Metals Analysis (SW 1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Sludge TCLP Pesticides Analysis (SW 131 1/8081) Endrin A
Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis (SW 13I 1/8081) Heptachlor A
Sludge TCLP Pesticides Analysis (SW 1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis (SW 131 I/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis (SW 1311/8081) Toxaphcne A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5=frichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, 'fetal A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzetre A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis (SW 13 1 1/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Key Key.
NC WW SCM A Accredited
NC WW SCM N Not Accredited
Original #1.
Page 9of31

Summii Environmental Technologies, Inc.
3310 Win St.
tIONI/IENTAL TtClit OLOGIFS, INC Cuyahoga Falls, Ohio 44223
Analytkkat Laboratories Tories TEL: [phone] FAX: [phone]
Website: http://wwiv.settek.com
Accreditation Program
Analytes Report
WO#: 20041280
06-May-20
Client: Synagro State: NW
Project: Durham Brown
Program Name: NC WW SCM
Sample Ill Matrix
Test Name
Analyte Status
20041280-001 A
Sludge TCLP Sethi-Volatiles Analysis (SW 13 €1/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis t,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge 'TCLP Volatiles Analysis Carbon tetrachloride A
Sludge 'TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tctrachloroethene A
Sludge 'I'CLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original # l
Page 10 of 31

Summit hiurronnrenlal Technologies, Inc.
3310 Will St.
ENVIt7pNrAENTL tECfINpt,pts{l=5,
A Cn}YdrnS a Falls, Ohio 44223
3AC
Anafyticaf Laborardrtee TEL: [phone] FAX: [phone]
Ifehsire: hf/p:/Arunr.serrekcmu
QC SUMMARY REPORT
VOIk: 20041280
06-11lay-20
Client:
Project:
Synagro
Durham Brown
BatchID: 43209
Sample ID: MB-43209 SampType: MBLK TestCode: TCLP-VOC-M Units: mg1L Prep Date: 412912020 RunNo: 112431
Client ID: PBS Batch ID: 43209 TestNo: SW8260 SW1311M Analysis Date: 4/30/2020 SegNo: 2758003
Analyte
Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Quel
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachtoroethene
Trichtoreethene
Vinyl chloride
Burr: 4-B rom all uorobenzene
Surr: Dibromotuoromelhane
Surf Toluened8
ND 0.00500
ND 0.00500
ND 0,10D
ND 0.00500
ND 0.00500
ND 0.0500
ND 0.00500
ND 0.00500
ND 0.00500
NO 0.00200
48.0 50.00 97.2 70 130
50.1 50.00 100 70 130
50.2 50.00 100 70 130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
L Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 11 of 31
11 Holding times far preparation or anal}
MC Value is below Minimum Compound
PL Permit Limit
5 Spike Recovery outside accepted reco
Original

Sunrnrir En irotuaenln! Technologies, Int.
3310 i15n St.
6NVMOA€IAStd1ALYECI1H0LO0iES,140 Crr3nhuge lolls. Ohio 44223
0nnlyticsl Laboratart€s TEL: [phone] FAA': [phone]
IVebsae: h0p://www.seaek.carn
QC SUMMARY REPORT
WO#: 20041280
06-May-20
Client:
Project:
Synagro
Durham Brown
Balch1D: 43214
Sample ID: MB-43214
Client ID: PBS
Analyte
SampType: MBLK
Balch10: 43214
Result
TestCode: MO-TCLP-7(6 Units: mg/L Prep Dale: 413012020
TestNo; SW6010D SW3010A Analysis Date: 5/1l2020
RunNo: 112443
SegNo: 2759120
PQL SPK value SPK Ref Val %REC LowLireit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-43214
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 43214
Result
TestCode: Mti-TCLP-7(6 Units: mglL
Prep Date: 4/30/2020
TestNo: SW6010D SW3010A Analysis Date: 5/1/2020
RunNo: 112443
SegNo: 2759121
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Silver(Ag)
2.07
0.500
2.000
0
104
BO
120
Sample ID: 20041350-004AMS
Client ID: BatchQC
Analyte
SampType: MS
Batch ID: 43214
Result
TestCode: M11-TCLP-7(6 Units: mg1L
Prep Date: 4/38/2020
TestNo: SW6010D SW3010A Analysis Date: 5/112020
RunNo: 112443
SegNo: 2759928
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!
TCLP Silver(Ag)
1.72
0.500
2.000
0.001200
88.0
70
130
Sample ID: 20041350-004AMSD SampType: MSD
Client ID: BatchQC Batch ID: 43214
Analyte
Result
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/3012620
TestNo: 5W60100 SW301OA Analysis Dale: 511/2020
RunNo: 112443
SegNo: 2759929
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Silver(Ag)
1.73
0.500
2.000
0.041200
86.2
70
130
1.722
0.232
20
Qualifiers: B Analyte detected in the associated Method Blank
1 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding limes for preparation or anal)
M Manual Integration used to determine ores response MC Value is below Minimum Compound
P Second column confirmation eeceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reca
Page 12 of 31
Original

Stimuli Environmental Technologies. hie.
33101Vin Si.
ENVLRON MENTAL TECHNOLOGIES, MC Cuyahoga Falls, Ohio 44223
Analytical Laboretorlos 'i'L'i.: (330) 253-821i FAX: [phone]
frebsue: hllp::5vunv.sertekcom
QC SUMMARY REPORT
WO#: 20041280
06-A1ay-20
Client:
Project:
Synagro
Durham Brown
$atchlD: 43214
Sample ID: 20041360-004AMSD SampType: MSD
Client ID: BatchQC Batch ID: 43214
Analyte
Result
TeslCode: Mtl-TCLP-7(6 Units: mg1L Prep Date: 4/30/2020
TestNo: SW6010D SW3010A Analysis Date: 6/1/2020
RunNo: 112443
SegNo: 2766929
PQL SPK value SPK Ref Val %REC Loy/Limit Rightimit RPD Ref Val %RPD RPDLimit Qua1
Qualifiers: B Analyte defected in the associated Method Blank
I Analyte detected below quantifalion limits
ND Nat Detected
R RPD outside accepted recovery limits
E Value above quantilalion range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 31
Original

6NVIfiCitiM t1TAL izatiNOLt100ES, IN
Analytical Laborator/es
Summit Environmental Technologies, Lu.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: htio://www.setiek.com
QC SUMMARY REPORT
WW1: 20041280
06-Ma3'-20
Client:
Project:
Synagro
Durham Brown
BatchlB: 43218
Sample ID: MB-43218 SampType: MBLK TestCode: SVOC-BNA_T Units: mg1L Prep Date: 4/3012020 RunNo: 112439
Client ID: PBS Balch ID: 43218 TestNo: SW8270 SW3510C Analysis Dale: 5/1/2020 SegNo: 2758485
Analyte
Result PDL SPK value SPK Ref Val %REC Lowiimil HighLimit RPD Ref Val %RPD RPDLimit Dual
1,4-Dichlorobenzene
2, 4, 5-T r ich t o ro phe no I
2,4,6 Trichlorophenol
2,4-Dinilrotoluene
a -Cresol
Cresols, Total
Hexachloro-1,3-buladiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenoi
Pyridine
Surr: 2-Fluorophenol
Surr. Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2, 4,6-Tri hrom aphenoi
Sum 2-Fluarobiphenyl
Surr. p-Terphenyl-dl4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.100
0.250
0.250
0.0500
0.250
5.00
0.0200
0.0500
09 00
0.100
0.250
0.250
0.783 1,000 78.3 10 109
0.756 1.000 75.6 10 109
0.678 1.000 67.8 19 120
1.07 1.000 107 10 120
0.779 1.000 77.9 22 117
1.13 1.000 113 34 116
QC+
Qualifiers: 6 Analyle detected in the associated Method Blank
7 Analyte detected below quanti lotion limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine arca response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 14 of 31
H Holding limes for preparation or anal(
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

Srrnmut Environmental Technologies, Inc.
3310 Win Sr.
ENVINONi118NTAL TECH4F{1LOCi±=9. INC Cuyahoga Falls, 0lria 44223
Anslylfcal Laboratories TEL: [phone]! FAX: [phone]
fl ebsite: hlrn:dii'ar-seltek.cau
QC SUMMARY REPORT
WOO: 20041280
06-May-20
Client:
Project:
Synagro
Durham Brown
BateliID: 43218
Sample ID: LCS-43218
Client ID: LCSS
Analyte
SampType: LCS TestCode: SVOC-BNA_T Units: mgfL
Balch ID: 43218 TestNo: SW8270 SW3510C
Prep Date: 413012020
Analysis Dale: 51112020
RunNo: 112439
SegNo: 2758486
Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
i,4-Dichlorobenzene
2,4, 5 -T rich l oro ph a no l
2,4, 6-Trich lorophe nol
2,4-DinitrotoIuene
o-Cresol
Cresols, Total
Hoxachloro-1 ,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr. Nitrobenzene-d5
Surr: 2, 4, 6-Tri bro m op he not
Surr. 2-Flu o ro b ip he ny l
Sure p-Terphenyl-d14
0.426
0.809
0.796
0.818
0.637
ND
0.427
0.769
0.393
0.584
0.834
0.428
0.851
0.836
0,686
1.20
0.813
1.16
0,100
0.250
0.250
0.0500
0.250
5.00
0.0200
0.0500
0.100
0.100
0.250
0.250
0 8000
0,8000
0.8000
0.8000
0.6000
1.600
0.8000
0.8000
0.8000
0.8000
0.8000
0.8000
1.000
1.000
1.000
1.000
1.000
1.000
0
0
0
0
0
0
0
0
0
0
53.2
101
99.4
102
79.6
79.8
53.4
98.2
49.1
73.0
104
53.6
85.1
83.6
68.6
120
81.3
118
36.4
31.7
31.1
43.3
32.9
31.7
31.4
43.1
36.5
39.5
34
10
17.1
10
32.6
4.43
41.8
36,4
130
132
133
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
QC+
Qualifiers: H Analyte detected in the associated Method Blank
! Analyte detected below quantitation limits
ND Nat Defected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 15 of 31
H Holding times for preparation or analy
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

Summit Environmental Technologies, Inc,
3310 I6iu St.
ENVIRONMENTAL TOCHNOLQGiO.S, rriC Cuyahoga falls. Ohio 44223
Analytical Laboratories TEL [phone] FAX'. [phone]
it ebsite: lattr//www.settek.cam
w.sellekenm
QC SUMMARY REPORT
WO#: 20041280
06-May-211
Client:
Project:
Synagro
Durham Brown
BatchlD: 43218
Sample ID: 20041350-002AMS
Client ID: BatchQC
Analyte
SampType: MS
Batch ID: 43218
TesiCode: SVOC-BNA_T Units: rnglL
TestNo: SW8270 SW3510C
Prep Date: 4/3012020
Analysis Date: 5/1/2020
RunNo: 112439
SegNo: 2760532
Result PQL SPK vatue SPK Ref Val %REC LowLimit HighLimil RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene
2, 4, 5-Tri chlorophe nol
2,4, 6-T ri ch l oro ph en of
2,4-Dinitrotoluene
o-Cresol
Cresols, Total
Hexachloro-1, 3-butadiene
Hexachlorobenzene
Hexachlaroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr:2-Fluorophenol
Sure: Phenol-46
Sum Nitrobenzene-d5
Sur: 2, 4, 6-Tr i brom o ph en o f
Sun': 2-Fl u oro bi ph e n yl
Surr: p-Terphenyl-d14
0.558
0.900
0.921
0.914
0.755
ND
0.528
0.913
0.540
0.676
0.871
ND
0.930
0.946
0.797
1.34
0.938
1.28
0.200
0.500
0.500
0.100
0.500
10.0
0,0400
0.100
0.200
0.200
0.500
0.500
0.8000
0,8000
0.8000
0.8000
0.8000
1.600
0.8000
0.8000
0.8000
0.8000
0.8000
0.8000
1.000
1.000
1.000
1.000
1.000
1.000
0
0
0
0
0
0
0
0
0
0
0
0
69.7
113
115
114
94.4
93.0
66.0
114
67.5
84.6
109
61,8
93.0
94.6
79.7
134
93.8
128
33.8
28.7
12.8
20.4
10
10
29
33.7
32.8
20
10
10
3.39
5
14.5
19.5
34.4
8.86
126
144
153
155
148
148
126
134
132
158
176
130
130
130
154
130
130
156
m QC+
S
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
1: Value above quantitalion range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 16 of 31
11 lidding times For preparation or anal}
MC Value is below Minimum Compound
PE, Permit Limit
S Spike Recovery outside accepted reco
Original

6NYI80NMENTAL TEGHNOLOSII.S, I
Aaalyrtcal taboralorks
Suomi( environmental Technologies. Inc.
3310 Win Si.
Cuyahoga Falls, Ohio 41223
la: [phone] FAX: [phone]
1Vehsite: h1ip:/nrmir.settekcon
QC SUMMARY REPORT
WOO: 20041280
Qti-�Ur0'-20
CHciit:
Project:
Synagro
Durham Brown
falcliID: 43218
Sample ID: 20041350-082AMSD SampType: MSD TestCode: SVOC-BNA T Units: mg1L Prep Date: 413012620 RunNo: 112439
Client ID: BatchQC Batch ID: 43218 TestNo: SW8270 SW3510C Analysis Date: 5/112020 SegNe: 2760533
Analyte
Result
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RP Ref Val %RPD RPDLimil Dual
1,4-Dichlorobenzene
2,4,5 Trichlorophenol
2,4 6 Trichlarophenol
2,4-Dinkrotoluene
o-Cresol
Cresols, Total
Hexachloro-1,3-buladiene
Hexachlorobenzene
Hexacbloroethane
Nitrobenzene
Pentachlarophenol
Pyridine
Sun: 2-Fluorophenol
Surf: Phenol-d6
Sum Nilrobepzene-d5
Sum 2,4, 6-Tribrom ophenoi
Sum 2-Fluoroblphenyl
Surr p-Terphenyl-d14
0.476
0.807
0.799
0.855
0.672
ND
0.492
0.834
0.478
0.644
0.783
ND
0.871
0,881
0.742
1.25
0.846
1.18
0.200
0.500
4.500
0.100
0.500
10.0
0.0400
0.100
0.200
0.200
0.500
0.500
0,8000
0.8000
0.8000
0.8000
0.8000
1.600
0.8000
0.8000
0.8000
0.8000
0.8000
0.8000
1.000
1.000
1.000
1.000
1.000
1.000
0
0
0
0
0
0
0
0
0
0
0
0
59.4
101
99.9
107
84.0
83.0
61.5
104
59.8
80.6
97.9
48.0
87.1
88.1
74.2
125
84.6
118
33.8
28.7
12.8
20.4
10
10
29
33.7
32.8
20
10
10
3.39
10
14.5
19.5
34.4
8.86
126
144
153
155
148
148
126
134
132
158
176
130
130
130
154
130
130
156
0.5576
0.9004
0.9208
0.9140
0,7548
0
15.9
11.0
14.1
6.65
11.6
4
0.5280 7.06
0.9128 8.97 30
0.5400 12.1 30
0.6764 4.85 30
0.8708 10,6 30
0 0 30 m
0
0
0
0
0
0
30
30
30 mr1C+
30
30
30
30
Qualifiers: B Analyte detected in the associated Method Blank
! Analyte detected below quantitation iimits
NI) Not Detected
R RPD outside accepted recovery limits
B Value above quantitation range
M Manual Lrtegration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 17 of 31
H Holding limes for preparation or analy
MC Value is belowlulinimum Compound
FL Permit Limit
S Spike Recovery outside accepted reco
Original

Smumir Eneironnrenlal Technologies, Inc.
3310 Win Sr.
ENYIl1ONMTt{TAL 16C4444OLo0359, INC. Cuyvrhoga Falls, Ohio 44223
Analyilcal Lnfroratories TEL: [phone]PAX: [phone]
IVebsile: hllo:/hi,inv,seuek.com
QC SUMMARY REPORT
WO#: 20041280
06-Afay-20
Client:
Project:
Synagro
Durham Brown
Bateldi): 43232
Sample ID: MB-43232
Client ID: p1S
Analyte
SampType: MBLK
Batch ID: 43232
Result
TeslCode: HG_TCLP(74 Units: PPM Prep Dale: 51112020
TestNo: SW7470A SW7470A Analysis Date: 5/1/2020
RunNo: 112445
SeqNo: 2758965
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
ND
0, 00200
Sample ID: LCS-43232
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 43232
Result
TestCcde: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
Prep Dale: 5/1/2020
Analysis irate: 511/2020
RunNo: 112445
SeqNo: 2758967
PQL SPK value SPK Ref Val 1'REC LowLimit HighLimil RPD Ref Vat %RPD RPDLimit Qual
TCLP Mercury
0.00396
0.00200
0.00400
0
99.0
80
120
Sample ID: TCLP BLANK 4-30-2 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM
Client ID: PBS Batch ID: 43232
Analyte
Result
Prep Date: 5/1/2020
TestNo: SW7470A SW7470A Analysts Date: 5/112020
RunNo: 112445
SeqNo: 2758969
PQL SPK value SPK Ref Val %REC LowLimit HighLimil RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
ND
0.00200
Semple ID: 20041350-004AMS
Client ID: BatchQC
Analyte
SampType: MS
Batch ID: 43232
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
Prep Dale: 511/2020
Analysis Date: 5/1/2020
RunNo: 112445
SegNo: 2758994
PQL SPK value SPK Ref Val %REC LowLimit HighLimil RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
Qualifiers:
0.00514
0.00200
0.09400
0
128
75
125
5
B Analyte detected in the associated Method Blank
I Analyze detected below quantitaiion limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitalion range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Defection Limit
Page 18 of 31
H bolding times for preparation or anali
MC Value is below Minimum Compound
PL Permit Limit
5 Spike Recovery outside accepted reco
Original

Summit Envirrnonental Technologies, Inc.
3310 Win SI.
E8VIRONM6111ALICCNHOLOGI0S, INC Cuyahoga Taos, Ohio 44223
finalyffcaf Labornicrles TEL: [phone] FAX.: [phone]
IVebsite: hnn:/Srww.serlek.com
QC SUMMARY REPORT
WO#: 20041280
0b-AJny-20
Project:
Synagro
Durham Brown
13atchID: 43232
Sample ID: 20041350-004AM5
Client tD: BatchQC
Analyse
SampType: MS
Balch ID: 43232
Result
TestCode: HG_TCLP(74 Units: PPM Prep Date: 5f112020
TestNo: SW7470A SW7470A Analysis Date: 511/2020
RunNo: 112445
SegNo: 2759994
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Carat
Sample ID: 20041350-004AMSD SampType: MSD
Client ID: BatchQC
Analyse
Batch ID: 43232
Result
TestCode. HG_TCLP(74 Units: PPM
TestNo:5W7470A SW7470A
Prep Dale: 511/2020
Analysis Date: 5/1/2020
RunNo: 112445
SegNo: 2758998
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
0.00515
0.00200
0.00400
0
129
75
125
0.00514
0.194
20
S
Sample ID: TCLP BLANK 1 5-1- SampType: MHLK TestCode: HG_TCLP(74 Units: PPM
Client ID: PBS Batch ID: 43232
Analyte
Result
TestNo: SW7470A SW7470A
Prep Date: 511/2020
Analysis Date: 5/1/2020
RunNo: 112445
SegNo: 2759003
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
ND
0.00200
Sample ID: TCLP BLANK 2 5.1- SampType: MBLK
Client ID: PBS
Analyte
Batch ID: 43232
Result
TestCode: HG_TCLP(74 Units: PPM
Prep Dale: 5/1/2020
TestNo: SW7470A SW7470A Analysis Date: 5/1/2020
RunNo: 112445
SegNo: 2759005
PQL SPK value SPK Ref Vat %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
ND
0.00200
Qualifiers: B Analytc detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analy
J Analyte detected below quantitation limits M Manual Integration used to detemtine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reca
Page 19 of 31
Original

Simard Environmental Technologies, Inc.
3310 {Yin 5'f.
EM/InOinAEtttALTt(Hf1OLontEs, 3Nc Cuyahoga falls, Ohio 8/223
Analytical taboretori€s TEL: [phone] FAX: [phone]
Jleh.rile: h/Jp:/hnivtn.settek.cam
QC SUMMARY REPORT
WO#: 2004I280
06-3tfty-20
Client:
Project:
Synagro
Durham Brown
BatchlD: 43232
Sample ID: MB2-43232
Client ID: PBS
Analyte
SampType: MBLK
Batch ID. 43232
Result
TestCode: HG_TCLP(74 Units. PPM Prep Date: 511/202D
TestNo: SW7470A SW7470A Analysis Dale: 5/112020
RunNo: 112445
SeqNo: 2759012
PQL SPK value SPK Ref Val %REC LowLimit HighLirnit RPD Ref Val %RPD RPDLirnit Dual
TCLP Mercury
NO
0.00200
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected betoty quanlitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 20 of 31
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

S+nnmil Ern iromnental Technologies, Inc.
33113 {Yin Sl.
ENvrONhIENTAL TECHNOLOGIES, MC Cuyahoga Falls, Ohio -1223
tlnntytfcal Laboratories 7EL: [phone] FAX: [phone]
IVebsile: h1tp. iruor.sellek.cnur
QC SUMMARY REPORT
1V0#: 200,11280
06-Mny-20
Client:
Project:
Synagro
Durham Brown
BatcltlD: R112310
Sample ID: 20041280-001ADUP SampType: OUP
Client ID: Durham Brown WT Batch ID: R112310
Analyte
Result
TestCode: FreeLiquid S Units:
TestNo: 5W9095
Prep Date:
Analysis Date: 412912020
Runl+lo: 112310
SeqNo: 2753993
POL SPK value 5PK Ref Val %REC LowLimit HighLimil RPD Ref Val %RPD RPDLimit Dual
Free Liquid
pass
0
0
20
Qualifiers: 13 Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPIJ outside accepted recovery limits
E Value above quantitation range 1-I holding times for preparation or analy
M Manual Integration used to determine area response MC Value is below Iviinimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 31
Original

Sm mrll Environnrerrinl7echnologies, Gmc.
3310 Win St
ENV11101:1Mt_UTALLettnN040GIFS,?NC Cuyahoga Falls, Ohio 44223
linalyUcaf Lnboretor/en TEL: [phone] FAX: [phone]
Wehsile: htlo:Giruur.sellek.com
QC SUMMARY REPORT
`,VOI/: 2004/280
06-May-20
Client:
Project:
Synagro
Durham Brown
HatchlD: R112323
Sample ID: Blank
Client ID: PBW
Analyte
SampType: MBLK
Batch ID: R112323
Result
TestCode: Cyanide,Rea Units: mgfL
TestNo: SW9014
Prep Date:
Analysis Date: 4/27/2020
RunNo: 112323
SegNo: 2754426
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
ND
0.485
Sample ID: LCS
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R112323
Result
TestCode: Cyanide,Rea Units: mg/L
TestNo: 5W9014
Prep Dale:
Analysis Date: 4127/2020
RunNo: 112323
SegNo: 2754427
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Vat %RPD RPDLimit Qual
Cyanide, Reactive
9.44
0.495
10.00
0
94.4
85
115
Sample ID: RLCheck
Client ID: BatchQC
Analyte
SampType: RLC
Batch ID: R112323
Result
TestCode: Cyanide,Rea Units: mgfL
TestNo: SW9014
Prep Date:
Analysis Date: 4/27/2020
Runtio: 112323
SegNo: 2754429
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
ND
0.500
0.5000
0
81.0
55
135
Sample ID: 20041299-001AMS
Client ID: BatchQC
Analyte
SampType: MS
Batch ID: R112323
Result
TestCode: Cyanide,Rea Units: mg1L
TestNo: SW9014
Prep Date:
Analysis Date: 4/27/2020
RunNo: 112323
SegNo: 2764434
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
8.98
0.485
10.00
0
89.8
75
125
Qualifiers: B Analyte detected in the associated Method Blank
l Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery, limits
E Value above quantitation range
M Manual integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 22 of 31
H Holding times for preparation or aeal7
MC Value is below Minimum Compound
PL Permit Limit
5 Spike Recovery outside accepted reco
Original

Sauuxit Environmental Technologies; Inc.
3310 Win Sl.
EN0In6Nh1ENTAL TECt1HOLAGIES, INC CaJahoga Falls, Ohio 44223
Analytical Labnrate Ies TEL: [phone] FAX [phone]
lt'e6.,ile; hnp:.wuw.sellek.com
QC SUMMARY REPORT
WOO: 20041280
06-Afnp-20
Client:
Project:
Synagro
Durham Brown
Mehl"): R112323
Sample ID: 20041299.001AMS
Client in: BatchQC
Analyte
SampType: MS
Batch ID: R112323
Result
TestCode: Cyanlde,Ree Units: mgiL
TestNo: SW9014
Prep Date:
Analysis Date: 412712020
RunNo: 112323
SegNo: 2754434
PQL SPK value SPK Ref Val % REC LowLimit HighLimit RPD Ref Val %aRPD RPDLimit Qual
Sample ID: 20041299-001AMSD SampType: MSD
Client ID: BatchQC
Analyte
Batch ID: R112323
Result
TestCode: Cyanide,Rea Units: mg1L
TestNo: SW9014
Prep Date:
Analysis Date: 4127/2020
RunNo: 112323
SegNo: 2754435
PQL SPK value SPK Ref Val %REC LowLimit t-ighLimil RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.35
0.490
10.00
0
93.5
75
125
8.984
3.97
10
Qualifiers: B Analyte detected in the associated Method Blank
J Analyze detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range it Holding times for preparation or analy
M Manual integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds Pf, Permit Limit
RL Reporting Detection Limit 5 Spike Recovery outside accepted reco
Page 23 of 31
Original

Smooth' Environmental '!Technologies, lne.
3310 Win Si.
ENVIROLIMESTAL YEGHNOLOI?IFS, INC Cuyahoga Falls. Ohio 44223
�;..� Analyticaf LabOrataf1e 7FL: [phone] FAX. [phone]
Websile: hftwAvuvt.selrek.com
QC SUMMARY REPORT
wolf. 20041230
06-AMay-20
Client:
Project:
Synagro
Durham Brown
BatchID: R112336
Sample ID: MB-R112336
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: R112336
Result
TestCode: Sulftde,React Units: mg/Kg Prep Date:
TestNo: SW9034
Analysis Date: 4127/2020
RunNo: 112336
SegNo: 2755023
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!
Sulfide, Reactive
ND
25.0
Sample ID: LCS.R112336
Client ID: LCSS
Analyte
SampType: LCS
Balch ID: R112336
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
Prep Date:
Analysis Date: 412712020
RunNo: 112336
SegNo: 2765024
PCB_ SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!
Sulfide, Reactive
3120
25.0
3260
Qualifiers: 13 Analyte detected in the associated Method Blank
3 Analyte detected below gaantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0
95.1
85
E Value above quaatitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 24 of 31
115
H Holding times for preparation or anal]
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery, outside accepted reco
Original

Semmil Environmental Technologies, Inc,
3310 Win St.
EnVirlahthlartAL TECtltiohocriEo, €kC. Ceyahoga Falls, Ohio 44223
Analylca1 Laboralsj4en TEL: {330) 253-8211 FAX: [phone]
11'ehsile: hliv:/.i�u•u.aerfek.eau
QC SUMMARY REPORT
WO#: 2094/280
06-1 fay-20
Client:
Project:
Synagro
Durham Brown
BatcltlD: R112336
Sample ID: 20041299.001AMS
Client 1D: BatchQC
Analyte
SampType: MS
Batch ID: R112336
Result
TestCode: 5ulfide,Reacl Units: mgfL
TestNo: SW9034
Prep Date:
Analysis Dale: 4/27/2020
RunNo: 112336
SegNo: 2766029
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Dual
Sulfide, Reactive
3080
25.0
3280
0
93.9
75
125
Sample ID: 20041299-001AMSD SampType: MSD
Client ID: BatchQC Balch ID: R112336
Analyte
Result
TestCode: Sultide,React Units: mg1L
TestNo: SW9034
Prep Date:
Analysis Date: 4/2712020
Runlo: 112336
SeciNo: 2755030
PQL SPK value SPK Ref Val %REC LowLireit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive
3180
25.0
3280
0
97.0
75
125
3080
3.19
30
Qualifiers: B Analyte detected is the associated Method Blank
/ Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
F, Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 25 of 31
H Holding times for preparation or mall
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

Summit 1tnvtranmennr1 Technologies, Inc.
33401Vin S1.
ENViftONfdEN7AL 7tCNN0L0OI1S, tNC Cuyahoga Falls, Ohio 1.1223
Anafytical Lnbnratorles TEL: [phone] FAX: [phone]
IVe6srle: Into: //imic.,sellek.cnnr
QC SUMMARY REPORT
WO#; 20041280
O6-May-20
Client:
Project:
Synagro
Durham Brawn
BatclilD: R112377
Sample ID: LCS-R112377
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R112377
Result
TestCode: pH_DW(4500- Units: s.u.@21.9C Prep Dale:
TestNo: SW9045D
Analysis Date: 4/30/2020
RunNo: 112377
SegNo: 2756568
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0
99.6
98.6
101.4
Sample ID: 20041481-OO1ADUP SampType: DUP TestCode: pH_DW(4500- Units: s,u.@22.00 Prep Date:
Client ID: DatchQC Batch ID: R112377 TestNo: SW9045D
Analyte
Analysis Dale; 4/30/2020
RunNo: 112377
SegNo: 2756570
Result PQL SPK value SPK Ref Val %REC Lowlimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.8
7.8
0.4
5
Sample ID: PH 7 CHECK
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R112377
Result
TestCode: PH_DW(4500 Units: s.u.@21.9C Prep Date:
TestNo: SW9045D
Analysis Date: 4/30/2020
RunNo: 112377
SegNo: 2756616
PQL SPK value SPK Ref Val %REC LowLimit HighLimil RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0
100
98.6
101.4
Qualifiers: B Analyte detected in the associated Method Blank
f Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used 10 determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 26 of 31
H Holding limes for preparation or analy
MC Value is below Minimum Compound
PL Pennit Limit
S Spike Recovery Outside accepted rcco
Original

Sunnnh Environmental Technologies, Inc.
331011in Sr.
Et9VINONia0N1AL T 0 1NOL00i0.S, ING Crgnhaga Falls, Ohio 44223
Anrrlyffcal Laboraterles i1 L: (330)153-821I PLY: [phone]
IVehsrle: hilp:/Arirsrseriek.com
QC SUMMARY REPORT
WON: 20041280
06-dicey-20
Client:
Project:
Synagro
Durham Brown
BatchID: R112438
Sample ID: RLC
Client ID: BatchQC
Analyte
SampType: RLC
Batch ID: R112438
Result
TestCode: MII.CP_NPW Units: mg/L
TestNo: SW8010D
Prep Date:
Analysis Date: 5/i/2020
RunNo: 112438
SegNo: 2758335
PQL SPK value SPK Ref Val %REC LowLimiit HighLimit RPD Ref Val %RPD RPOLimil Qual
TCLP Arsenic(As)
TCLP Barium(Be)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
0.0207
ND
ND
ND
0.0425
0.0200
0.0200
0.90500
0.0200
0,0150
0.01600
0.02000
0.004000
0.01600
0.04000
0
0
0
0
0
129
98.9
99.1
102
106
70
70
70
70
70
130
130
130
130
130
Sample ID: RLC 2
Client ID: BatchQC
Analyte
SampType: RLC
Batch ID: R112438
Result
TestCode. Mil-ICP_NPW Units: mg1L Prep Date: RunNo: 112438
TestNo: SW60100 Analysis Date: 51112020 SegNo: 2758338
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Selenium(Se)
0.0388
0.0250
0.04000
0
97.0
70
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quareitation range H Holding times for preparation or anal)
1 Arsaiyte detected below quantitation limits M Manual integration used to determine area response MC Value is blow Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted recce
Page 27 of 31
Original

Smug( Euvironnrealal Technologies, Inc.
3310 Win SI.
Et4VIRONMENTAL TeettNat0Gi0S, IN a Cuyahoga Falls, Ohio 41223
An7fylfca! Labnre hrlee TEL: [phone] FAA: (330) 253-l189
iYehsile: htln:/,www..settekcom
QC SUMMARY REPORT
WOI: 20041280
06-May-20
Client:
Project:
Synagro
Durham Brown
Batelilf: Id112457
Sample ID: LCS-R112457
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: R112457
Result
TestCode: Ignitebility_S Units: mmisec Prep Date: RunNo: 112457
Analysis Date: 51112020 SegNo: 2769305
TestNo: SW1030
PQL SPK value SPK Ref Val %REC Lowlimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitabilily
7.96
7.240
0
110
70
130
Sample ID: 20041479•002ADUP SampType: DUP
Client ID: BatchQC Batch ID: R112457
Analyte
Result
TeslCode: Ignitability_S Units: mmisec
TestNo: SW1030
Prep Dale:
Analysis Date: 51112020
RunNo: 112457
SeqNo: 2759307
PQL SPK value SPK Ref Vat %REC LowLimil HighLimit RPD Ref Val %RPD RPDLimit Qual
lgnitabilily
non-flammable
0
0
20
Sample ID: 20041479-005ADUP SampType: DUP
Client ID: BatchQC Batch ID: R112457
Analyte
Result
TestCode: Ignitability_5 Units: mmisec
TesiNo: SW1030
Prep Date:
Analysis Date: 51112020
RunNo: 142457
SegNa: 2759309
PQL SPK value SPK Ref Val %REC Lowlimit HighLimit RPD Ref Val %RP() RPDLimit Quat
Ignitabilily
>2.2
O
0
20
Sample ID: 20041479-005ATRlP SampType: DUP
Client ID: BatchQC Batch ID: R112457
Analyte
Result
TestCode: Ignllability_S Units: mmisec
TestNo: SW1030
Prep Date:
Analysis Dale: 511/2020
RunNo: 112457
SegNo: 2759310
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitabilily
>2.2
O
0
20
Qualifiers: B Analyte detected in the associated Method Blank
3 Analyte detected below quanti lotion limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anaty
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RI, Reporting Detection Limit S Spif:e Recovery outside accepted reco
Page 28 of 31
Original

Snmwit Environmental Technologies, inc.
3310Win SI.
E1tVI0ONh10NTALTECHNOLOCTES, INC Cuyahoga Falls, Ohio 44223
Analytical taboralories iS7,: [phone] FAX• [phone]
Webviie; InttgGivww.seltekcom
QC SUMMARY REPORT
WW1: 20041280
06-Alay 20
Client:
Project:
Synagro
Durham Brown
Bat -chin: R112457
Sample ID: 20041479-005ATRIP SampType: DUP TestCode: lgnitabillty_S Units: mmisee Prep Dale:
Client ID: BatchQC Batch ID: R112457 TestNo: SW1030
Analyte
Result
Analysis Dale: 51112020
RunNo: 112457
SeqNo: 2759310
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID: 20041278-001ADUP SampType: DUP
Client ID: BatchOC
Analyte
Balch ID: R112457
Result
TestCode: Ignitability_S Units: mmisee
TeslNo: SW1030
Prep Date:
Analysis Date. 511/2020
RunNo: 112457
SeqNo: 2759312
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability
non -Flammable
0
0
20
Sample ID: 20041280-OOIADUP SampType: DUP TestCode: tgnitabili y_S Units: mmisee Prep Date:
Client ID: Durham Brown WT Batch ID: R112457 TestNo: SW1030
Analyte
Result
Analysis Date: 51112020
RunNo: 112457
SeqNo: 2750314
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
19nitability
non-iammable
0
a
20
Sample ID: 20041282-001ADUP SampType: DUP TestCode: Ignitabil-rty_S Units: mmisee Prep Date:
Client ID: BatchQC Batch ID: R112457 TestNo: SW1030
Analyte
Result
Analysis Date: 511/2020
RunNo: 112467
SeqNo: 2769316
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability
non -Flammable
0
0
20
Qualifiers: B Analyte detected in the associated Method Blank
f Analyte detected below quantization tirnits
ND Not Detected
R RPD outside accepted recovery limits
Ii Value above quantitatian range
M Manual Integration used to deterrnine area response
P Second colunur confirmation exceeds
RL Reporting Detection limit
Page 29 of 31
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

1,E 40 OE abed
DBPix Evaluation
MT
i tFti lF. 1le7.( 7:. L, F CCi.il<7t:ir..L.f. Zl14
Analysis Request / Chain of Custody
Beier In TiriFla and Csinefitians at rorxw. eltckcL.nl
Client rams
i'4 Cik�J{ ssi a Adi dr ?CA()
c;y ACLitS'iiiLLE st.INL.- zip2.L 1t cuy
Reprm To
COM Phone
Prniee. 14.alI✓y it 1i.r.
Prolnc+5i rAddrtar
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e u 17rr
PO Itjtinla Number
1'w'e I[I racltitr !b
Clkat Emil "Wilcox
Svmplcd By fprbl+:\'mroeerm+t Praetor Sljmanrry tyle'jariktes'Rccreditedan Regnkrealeuh:
Mat: j'L.r,?.. "arW.7 3--tOhio i'AP CI Obit LPA Vb. Cu
SO' II7_ �., (Lp .rV ❑ Drinking wont Compliance
FarDW -nob; results en Fie �rcparfed 1. omit late? NIL-, 1116rr Cnrapflaace SE.i.kSeute; Pna. xm}:
lab Fee murapptr ©V I__tN
Sump* Maki ID
Sample IdentN3cxtien
Dime
Calleritd
Collected
Grail Sample
iSoc„ J 0.TFP tt173 j74,
SL
aig
Ii1T�raLr t}a:v-. I fi:01. B I N
Page l of t
E
a.
5 la
Analytical Para meters and Methods Requested
X
use**
Relinquished by:
Rwr1i tpeCt t)
Silt
Received lit Summit 'y; Darr
I
Time
Received tw:
Time
V�V
Carrier(
Date
Time
Noma I Comments:
Zti0
Sufficient same pravi8sd to rue QC? I CoOter? .6 J1ti0
Rash -Reunited: Ilay(s)
Alasl he approved by 1.-ah Nlanattcr
Received Temp.:
oc
1. -0.3C f
Other Container.
tee Prewar?. SENOOMELTED
www.ammara.com

Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL ONM NTAL TcCHNdi3OGit S, iNC. Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.coin
Analytical Laboratoi3e
Sample Log -In Check List
Client Name: SYN-NC-27028
Work Order Number: 20041280
RcptNo: 1
Logged by: Jacqueline Rasile 4/2412020 10:10:00 AM
Completed By: Jacqueline Rasile 4/24/2020 2:34:37 PM
Reviewed By: Sara E. Kidd 4/24/2020 3:54:08 PM
1,��+r;,.•6tis.
xfom -E+dd
Chain of Custody
1. is Chain of Custody complete? Yes El
2. How was the sample delivered? UPS
Loa In
3. Coolers are present?
No ❑ Not Present ❑
Yes N❑ No ❑ NA ❑
4. Shipping containerlcooler in good condition? Yes ❑�/ No ❑
Custody seals intact on shipping containerlcooler? Yes ❑ No ❑ Not Present c3
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes 111 No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°G Yes El No ❑ NA ❑
7. Sample(s) in proper container(s)? Yes 0 No ❑
8. Sufficient sample volume for indicated test(s)? Yes V No ❑
g. Are samples (except VOA and ONG) properly preserved? Yes V No ❑
10. Was preservative added to bottles? Yes ❑ No 0
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials 0
12. Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes 0 No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes 0 No ❑
15, Is it clear what analyses were requested? Yes F1 No ❑
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17, Was client notified of all discrepancies with this order?
Yes © No ❑
Yes ❑
No ❑ NA V
Person Notified:
By Whom:
Regarding:
Client Instructions:
Date:
Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Dato
Signed By
1
1.4
Good
Not Present
Page 31 of 31

Waypoi nt.
ANALYTICAL
4/15/2020
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-097-0002
Project Description: Durham Brown
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalyticai.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/6/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information,
Sincerely,
Paw, r er
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Waypol nty
ANALYTICAL
Report Number: 20-097-0002
Client Project Description: Durham Brown
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 SM-4500-N113C WP MTN
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 9045D WP MTN
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 4500NO3F-2011 WP MTN
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 6010D WP MTN
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 SW-7471B WP MTN
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 SM-4500-NH3C-TKN WP MTN
70953 Durham Brown Solids 04/02/2020 08:40 04/06/2020 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypoint.
ANALYTICAL
46451
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypaintanalytical.com
Ryan Copeland
Project Durham Brown
Information :
Submitted By : Ryan Copeland
Report Number :20-097-0002 REPORT OF ANALYSIS
Report Date : 04/15/2020
Received : 04/06/2020
PAw'a ms &of/
Pauric McGroary
Agronomist
Lab No : 70953 Matrix: Solids
Sample ID : Durham Brown Sampled: 4/2/2020 8:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture 80.0 °70
Test Results Units
0.010
MQL
1 04/07/20 16:15 ADM SM-2540G
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen 1200 mg/Kg - dry 500 1 04/15/20 14:00 JP3 SM-4500-NH3C
Nitrate+Nitrite-N <23.8 mg/Kg - dry 23.8 1 04/13/20 14:02 7BD 4500NO3F-2011
Organic N 11500 mg/Kg - dry 1250 1 04/13/20 14:00 CALCULATION
pH 5.4 s.u. 1 04/13/20 05:39 3SL 9045D
Total Solids 20.0 % 0.010 1 04/07/20 16:15 ADM SM-2540G
Total Kjeldahl Nitrogen 12700 mg/Kg - dry 1250 1 04/13/20 14:00 JP] ;M-4500-NH3C-TKP
Phosphorus 815 mg/Kg - dry 125 5 04/09/20 12:03 KKM 6010D
Aluminum 9050 mg/Kg - dry 125 5 04/09/20 12:03 KKM 6010D
Arsenic <12.5 mg/Kg - dry 12.5 5 04/09/20 12:03 KKM 6010D
Calcium <625 mg/Kg - dry 625 5 04/09/20 12:36 KKM 6010D
Cadmium 2.99 mg/Kg - dry 2.50 5 04/09/20 12:03 KKM 6010D
Chromium 19.0 mg/Kg - dry 6.25 5 04/09/20 12:03 KKM 6010D
Copper 354 mg/Kg - dry 6,25 5 04/09/20 12:03 KKM 6010D
Iron 367000 mg/Kg - dry 250 10 04/09/20 12:08 KKM 6010D
Lead <7.50 mg/Kg - dry 7.50 5 04/09/20 12:03 KKM 6010D
Magnesium 302 mg/Kg - dry 125 5 04/09/20 12:03 KKM 6010D
Manganese 2580 mg/Kg - dry 12.5 5 04/09/20 12:03 KKM 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 7

Waypoi nt�,
ANALYTICAL
46451
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypotntanalytical.com
Ryan Copeland
Project Durham Brown
Information :
Submitted By : Ryan Copeland
Report Number :20-097-0002 REPORT OF ANALYSIS
Lab No : 70953
Sample ID : Durham Brown
Report Date : 04/15/2020
Received : 04/06/2020
Pik imc Gtr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 4/ 2/ 2020 8:40
Test Results Units MQL DE Date / Time By Analytical
Analyzed Method
Mercury <0.0740 mg/Kg - dry 0.0740 1 04/08/20 11:47 DDB SW-7471B
Molybdenum <6.25 mg/Kg - dry 6,25 5 04/09/20 12:03 KKM 60100
Nickel 31.6 mg/Kg - dry 6.25 5 04/09/20 12:03 KKM 6010D
Potassium 171 mg/Kg - dry 125 5 04/09/20 12:03 KKM 6010D
Selenium <12.5 mg/Kg - dry 12.5 5 04/09/20 12:03 KKM 6010D
Sodium <625 mg/Kg - dry 625 5 04/09/20 12:03 KKM 6010D
Zinc 76.0 mg/Kg - dry 31.3 5 04/09/20 12:03 KKM 6010D
Sulfur 5150 mg/Kg - dry 125 5 04/09/20 12:03 KKM 6010D
Qualifiers/
Definitions
DE Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 7

Waypoint.
ANALYTICAL.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Synagro Central LLC/ Durham
Project: Durham Brown
Lab Report Number: 20-097-0002
Date: 4/15/2020
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 70953 (Durham Brown)
QC Batch No: L486301/L485957
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 5 of 7

Waypoi nt.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypointa nalytica I,com
Shipment Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 20-097-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
• UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised?
▪ Yes 0 No
Number of coolers/boxes received I 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? • Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed
Samples in proper containers?
Sample containers intact?
Yes
• Yes
O No
O No
Yes 0No
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
• •
Yes
Yes
O No
O No
Cooler temperature in compliance?
• Yes 0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes O No
Water - Sample containers properly preserved 0 Yes
Water - VOA vials free of headspace 0 Yes
O No 0N/A
O No • N/A
Trip Blanks received with VOAs
0 Yes
O No • N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No • N/A
r High concentration container (48 hr) [ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) 7 Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature:
Brandi Watson
Date & Timo: 04/06/2020 10:31:50
Page 6 of 7

Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
SAMPLING LOG #
PROJECT MANAGER: gvilo C-okLANQ
ram: (a3b) MTN
1�i11IIIlII IIIIIIIIHIIlII 11 �111�111111 °Z
Synaaro Central LLCJ t?urham IQ:30:44
Durham Brown
u
CHAIN OF CUSTOM'
RECORD & ANALYSIS
RECORD
1 attest that the proper field sampling procedures
were used during the collection of these samples
g4Y41\1 CDPSIAAID
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAB # SAMPLE LD. LOCATION 'TYRE CONTAINERS DATE TIME PRESERVED SHIPPED
St./
OW
Relinquished by Sampler: Date Time
l 1ti CDP LA O `(J Jto I"1'11
. Time
Date Time
For NI Co
monitoring PurPoserk
Ike by: REMARKS:
bY:
PO #;
1 LD.
ANALYSIS HEQUESi"
SLI
SL2
NH4-N
NOrN
o re
Cd
Cr
NI
Pb
As
Hg
Se
pH
�aVbisostlle
Mo.
CI
NO-N
w
•
SLI; Total Aids (Moisture), Total Kjeidehl Ni ogen, Phosphorus, and Potassium
SLM Basic Test SLI plus Sulfur, Calcium, Magnesium, Scum, imn, Aluminum, Mom, Copper and Zinc
r
0
r