WQ0024003_Monitoring - 11-2021_20211230

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
WQ0024003
Harvey Point Defense Facility
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
G W-59
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2021
Upload Document*
NDMR Upload Nov. 2021.pdf 1.77MB
PDF Only
GW-59 Upload Nov. 2021.pdf 6.04MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-7, NDAR-2, NDMLR, GW-59).
[e-mail]
Dustin Brent Combs
xrxf cG�wAf,
12/30/2021
This will be filled in automatically

Reviewer: Zhong, Vivien
Is the project number correct?* WQ0024003
Is the monitoring report accepted?* Yes No
Regional Office* Washington
Accepted Date:
1 /5/2022

I ORM NDIVIR 03 12 NON -DISCHARGE MONITORING REPORT (NDMR) Page - I n1 ,�
Pormlt No.: W00024003
Facility Name: Harvey Point Defense Facility
County: Perquimans
Month: November
Year 11021
PPI: 001
I'arametm Code 1-
U
O
Flow Measuring Point: [ Itn(luent [�]Eftluent [ No nowgeaerated
00050 00310 00940 31616 00610 00620
A
LL 0 Z
U
Parameter Monitoring Point: ❑Influent Effluent
❑Groundwato
Iuwrunq
I I'allf,,„" WA l
00400
00665
70295
00530
00600
00625
00630
o
i
FN
0
a
15
°
��o
ASo
d
ao
In�
n
°¢E
Z
YIy
Z
d
_
Z z]
24-hr
hrs
GPD
mg/L
mg/L
91100 mi-
mg/L
mg/L
su
mg/L
mg1L
mg/L
mglL
mg/L
mg/L
1
07.30
4
6,198
7.26
2
5,878
7.83
3
0/:30
4
7,070
7.37
4
08:00
4
7,286
7.22
5
07:30
_
4
5,192
2
<1
<0.2
44.3
7.6
4.52
5.2
44.3
<0-5
44.3
6
11:00
2
2,939
7
2,603
_
8
6,818
7.04
9
07:00
4
10,190
7.6
10
07:30
4
9,358
7.44
11
12:00
2
6,158
7.39
12
7,092
7.21
13
3,328
14
10:45
2
2,182
15
07:30
4
7,198
7.55
16
07:30
_
4
6,752
7.49
17 07:30 4
18 07:30 4
19 0130 4
20 I() 30 1
21
22
23 0/ all I
24 01 t11 I
21, lu 41, I
76
Jtt IY'I 'YI
2'I I Y, 111 1
An W W I
At
Av,,.,'r
Dailymamilllun
I I,Itly Mlnhnuni
nn,llllull 1Y1n•
MmOhly Avt1 I hntl
I I„Ily I lino
n„I .t,. I 1 u,11a, m, y
9,198
7.47
_
+14.uI
44 Ill
14 %0
7,298
7.45
7,202
7A
1,224
-
-
--
II',Ii
4,976
I.1',8
:I, 1 1?
2,R40
di6
I.'4
".1%4
f1,?/t1
1p.004
11f,190
G12 4
7.43
7.41
7,43
-
7.47
7.82
-
-
7.54
7.5
2.00
200
200
1.00
0.00
44.30
4.52
4.52 -
4 !r2
n
A)
Al
44,10
4430
44 3u
1.00
0.20
44.30
7.83
1.00
0.20
44-30
7.04
�IN,, o,ln!
.14,100
1 0 d it luuun
I:I:IE,
:to
Mnl lthly
Grab
Grab
Grab
Grah
Grab
1;I'li,
moral l dy
Otab
--
3 x Yoru
I.Y,11
M, ,nll dy
200
15
-
fi 9
3 x Year
Monthly
Monthly
Monthly
5 x Week

I ORM NI Wk u.f I NON -DISCHARGE MONITORING REPORT (NDMR) Page 2 of
5.Il l>Ilnil I'arson(s) Certified Laboratories
Name: 11u ,lln C mtlfs Name: Environmental Chemists Inc.
Name: Name:
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? Qcomphant ❑Non Compliiaud
If the 1aclllly c, non c ompllnnl, please explain in the space below the reason(s) the facility was not in compliance Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORc: Dustin B.Combs
Permittee: Harvey Point Defense Testing Activity
Certification No.: 1003645
signing Official: Geoffrey A. Chandler
Grade: III Phone Number: 252-562-2684
Signing Official's Title. Public Works Manager
i
Has the ORC changed since the previous NDMR? Coves ONo
Phone Number: 252-426-4250 Permit Expiration: 3/31/2023
Signature Date
Signature Date
Hy lhe; signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORK NDAI2-1 08 11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page � of .A
Permit No.: W00024003
Facility Name: Harvey Paint Defense Testing Activity WWTP
County: Perquiman5
Month: November
Year: 2021
Field Name:
1
Field Name:
2
Field Name:
3
Field Name:
4
Did irrigation occur
-
Area (acres):
1.46
Area (acres):
1.14
Area (acres):
1.38
Area (acres):
1.29
at this facility?
Cover Crop:Cover
Crop:
P�
Cover Crop;
P�
Cover Crop:
P:
klv!, 1 INO
Hourly Rate (in):
0.5
Hourly Rate (in):
0.5
Hourly Rate (in):
0.5
Hourly Rate (in):
0.5
Annual Rate (in):
57.2
Annual Rate (in):
57.2
Annual Rate (in):
57.2
Annual Rate (in):
57.2
Weather
Freeboard
Field Irrigated?
❑� YES []NO
Feld Irrigated?
❑YES ONO
Field Irrigated?
❑YES []NO
Field Irrigated?
DYFS LINO
a
❑
O
O
t
L
E
a)amm
°
'U
a
m
dIG)
o
-
W
w
m
CL
5. a
r
LO
v
0 CL
7
a
4
L
tm
v
❑ _
E 0)
O
Ew
%O
M
J
aD'a
O
7
LM
rn
-a
`9
J
E rn
ED a
oU
J
m'a
�EG°7
O .
a
Em
F- °
or
},
00
J
E M
E�zs
Ko
O
J
a, o
Ea •-
O CL
7 Q
a
yCE
m-
•
rn
C
OM
•1
E rn
aC
K o O
J
°F
in
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
C
47
0
0
0
0.00
0,00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
2
C
51
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
3
PC
44
0
6,566
100
0.17
0.10
6,566
100
0.21
0.13
6,566
100
0.18
0.11
0
0
0.00
0.00
4
CL
47
0.35
5,000
75
0.13
0.10
5,000
75
0.16
0.13
5.000
75
0.13
0.11
0
0
0.00
0.00
5
C
39
0
3.5
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
6
CL
59
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0,00
0
0
0.00
0.00
7
CL
56
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
8
C
49
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
9
C
40
0
4,700
75
0.12
0.09
4,700
75
0.15
0.12
4,700
75
0.13
0.10
0
0
0.00
0,00
10
t;
41
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
a00
11
{;
69
0
3 `r
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
12
CL
62
0.25
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0,00
0.00
0
0
0.00
0.00
13
C
63
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0,00
0.00
0
0
0.00
0.00
14
C
52
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0,00
0.00
0
0
0.00
0.00
15
C
41
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
16
C
39
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
17
C
50
0
4,325
60
0.11
0.11
4,325
60
0.14
0,14
4,325
60
0.12
0.12
4,325
60
0.12
0.12
18
C
55
0
4,175
60
0.11
0.11
4,175
60
0.13
0.13
4,175
60
0,11
0.11
4.175
60
0.12
0.12
19
C
44
0
3.5
3.850
60
0.10
0.10
3,850
60
0.12
0.12
3,850
60
0.10
0.10
3,850
60
0.11
0.11
20
C
47
0
0
0
0.00
0.00
0
0
0,00
0.00
0
0
0.00
0.00
0
0
0.00
0,00
21
C
44
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
D
0
0.00
0.00
22
C
56
0.35
0
0
0,00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
23
C
32
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
24
C
32
0
5,350
75
0.13
0.11
5,350
75
0.17
0.14
5,350
75
0.14
0.11
5,350
75
0.15
0.12
251
C
49
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0,00
26
CL
43
0.13
3.5
0
0
0.00
0.00
0
0
0"00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
27
C
40
0
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
28
C
45
0
0
0
0.00
0,00
0
0
0.00
0.00
0
0
0.00
0.00
0
0
0.00
0.00
29
C
38
0
0
0
0.00
O.DO
0
0
0.00
0.00
0
0
o.OD
D.DO
D
0
0.00
0.00
30
C
30
0
3,375
50
0.09
0.09
3,375
50
011
0.11
3,375
50
0.09
0.09
3,375
50
0.10
0.10
31
Monthly Loading:
12 Month Floating Total (in):
37,341
0,94
37,341
1.21
37,341
1.0D
21,075
0.60
20.16
25.80
21.31
20.60

FORM 1 1 Oa I I NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 1�_ of ,--2--
Did the application rates exceed the limits in Attachment B of your permit?
❑' Compliant ❑Non -Compliant
Were adequate measures taken to prevent effluent ponding in or runoff from the sites? ❑r Compliant ❑Non -Compliant
Was a suitable vegetative cover maintained on all sites as specified in your permit? ❑Compliant ❑Non -Compliant
Were all setbacks listed in your permit maintained for every application to each permitted site? ❑Compliant ❑Non -Compliant
Were all freeboards maintained in accordance with the specified freeboard heights in your permit? OCompliant ❑Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Uperalor in Responsible Charge (ORC) Certification
I (mc: Dustin B. Combs
Certification No.: 1007989
Grade: SI Phone Number: 252-562-2684
Has the ORC changed since the previous NDAR-1? ❑ve5 ONo
4.-
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
Perm ittee Certification
Permittee:
Harvey Point Defense Testing Activity
Signing Official: Geoffrey A. Chandler
Signing Official's Title: Public Works Manager
Phone Number: 252-426-4250 Permit Exp.
3/31 /23
Signature Date
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please PrinrCleanyorType
PERMIT Number: WQ0024003 Expiration Date: 3/31/2023
Facility Name: Harvey Point Defense Testing
Activity
Non -Discharge X UIC
NPDES Other
Permil Name (if different):
Facility Address: 2835 Harvey Point Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Hertford is"') N.C. 27944 County Perquimans
lc (slate;
(: ip)
❑X Spray Field ❑ Remediation:
Contact Person: Dustin Combs
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:MW #2
No. of wells to be sampled: 3
❑ Water Source Heat Pump ❑ Other:
from Perm![)
SAMPLING INFORMATION
If WELL
WELL Id NUMBER (from Permit): MW#2
Date sample collected: 11/5/2021
FIELD ANALYSES:
WAS
Well Depth: 20 f#.
Well Diameter: 2 in.
pH 0040o: 6.77 units Temp. 00010: 14.9 °C
DRY at
Depth to Water Level 82546:8 ft. below measuring point Screened Interval: 2 ft.
to 20 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 4 ft. above land surface
Relative M.P. Elevation:
ft, Odor 00085: None
check
Volume of water pumpedlbailed before sampling:
5
gallons
Appearance Light Tan
here:❑
Samples for metals were collected unfiltered: ❑
YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/512021-1111512021
Laboratory Name: Environmental Chemists Inc. Certification No. #94
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD oo335
mg1L
Nitrite (NO2) as N 00645 <0.02
mglL Pb - Lead o1o51 ug1L
Coliform: MF Fecal 31616 <1
1100mL
Nitrate (NO3) as N 00620 0.03
mglL Zn - Zinc 01092 mg1L
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665 0-64
mglL
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg1L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 7030c 3-4
mg/L
Al - Aluminum ol1o5
mg1L
pH (Lab) 00403
units
Ba - Barium 01007
ug1L
TOO 00680 12.8
mg1L
Ca - Calcium 00916
mg1L
Chloride 00940 138
mglL
Cd - Cadmium 01027
ug1L
Arsenic 01002
uglL
Chromium: Total 01034
ug1L
Grease and Oils 00552
mglL
Cu - Copper 01042
mglL ORGANICS: (by GC, OC1MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug1L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg1L
Hg - Mercury 7190o
uglL Lab Report Attached? ❑■ Yes (1) ❑A No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mglL VOC 78732 method #
Total Ammonia 00610 1.5
mglL
Mg - Magnesium 00927
mglL method #
(Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug1L , method #
TKN as N 00625
mg1L
Ni - Nickel 01067
uglL method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs: mglL VOC Removal%
Geoffrey A. Chandler Public Works Manager HPDTA
Permitlee (or Authorized Agent) Name and Title - Please print or type
wv-ny nev.ziZucU

SUBMIT FORM ON YELLOW PAPER ONLY
�..a
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
;
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0024003 Expiration Date: 3/31/2023
Facility Name: Harvey Point Defense Testing
Activity
Non -Discharge X UIC
Permit Name (if different):
NPDES Other
Facility Address: 2835 Harvey Point Rd_
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Hertford """`''} N.G. 27944 County Perquimans
v' (state}
(zip)
1❑ Spray Field ❑ Remediation:
Contact Person: Dustin Combs
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:MW #3
No. of wells to be sampled:
3
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#3
Date sample collected: 11/5/2021 FIELD ANALYSES:
WAS
Well Depth: 20 ft.
Well Diameter: 2
in. pH 00400: 7,70 units Temp. 00010: 16.4 °C
DRY at
Depth to Water Level 82546:9 ft. below measuring point Screened Interval: 2
ft, to 20 ft. Spec. Cond. 00094: µMhos
�
time of
sampling,
Measuring Point is 4 ft. above land surface
Relative M.P. Elevation:
ft. Odor o0085; None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan
here:❑
'; :iml Iles for metals were collected unfiltered: ❑
YES
❑ NO and field acidified: ❑ YES
❑ NO
I AHORATORY INFORMATION
I );dtr !.ample analyzed: ll/5/2021--11/15/2021
Laboratory Name: Environmental Chemists Inc. Certification No. #94
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335
rriglL
Nitrite (NO2) as N 00615 0.15
mg/L Pb - Lead 01n51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/1
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.76
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1710
mg/L
Al - Aluminum of lo5
mg/L
pH (Lab) 00403
units
Ba - Barium 011107
ug/L
TOG 0068o 29.1
mg/L
Ca - Calcium 00916
ni
Chloride 0094o 693
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method M ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ■❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732 method #
Total Ammonia oo610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg1L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Geoffrey A. Chandler Public Works Manager HPDTA
Permitlee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.212010

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
.. `
gIVISION OF WATER auALITYaNFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NO 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please PnntClearly orType
PERMIT Number: WQ0024003 Expiration Date: 3/31/2023
Facility Name: Harvey Point Defense Testing Activity
Non -Discharge X UIC
NPDES Other
Permit Name (if different):
Facility Address: 2835 Harvey Point Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Hertford I} N.C. 27944 County Perquimans
�ivr tsiate}
(ern)
❑M Spray Field ❑ Remediation:
Contact I'ersnll: Dustin Combs
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Wall Location/Site Name:MW #1
No. of wells to be sampled: 3
❑ Water Source Heat Pump ❑ Other:
from Permit}
SAMI'I ING INFORMATION
If WELL
WI I I ID NUMBER (from Permit): MW#1
Date sample collected: 11/5/2021
FIELD ANALYSES:
WAS
Wcll Depth: 20 ft.
Well Diameter: 2 in.
pH 00400: 6.62 units Temp. 00010: 15.2 °C
DRY at
11+10h In Water I evel 82546:10 ft. below measuring point Screened Interval: 2 ft.
to 20
ft. Spec. Cond. 00094: µMhos
time of
sampling,
M1.. ir,urincl Point is 4 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 0008& None
check
V+,Iruno of water pumped/bailed before sampling:
5
gallons
Appearance Light Tan
here:
❑
nrlldof, for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
I ABORATORY INFORMATION
1 hdr• r:nrnpIv amdyred:111512021-11115/2021
Laboratory Name: Environmental
Chemists Inc. Certification No. #94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00336
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01c51 ug/L
Colikwrm MF Fecal mm6 s1
/100mL
Nitrate (NO3) as N 00620 0,02
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 2.37
mg/L
(Nu(e: Use MPN melhod for highly lurbA samples}
Orthophosphate 70507
mg1L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 7030o 233
mg/L
Al - Aluminum o11os
mg/L
pH (Lab) 00403
units
Be - Barium 01007
ug/L
TOG 00680 32.8
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 87
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug1L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Capper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑A No (0)
Specific Conductance 00095
pMhos
K - Potassium oag37
mg/L
VOC 78732: method #
Total Ammonia 00610 1.8
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _ _ mg/L Effluent Total VOCs: , / mg/L VOC Removal%
1 J ,' !
Geoffrey A. Chandler Public Works Manager HPDTA j1�;,, 12/21/2021
Permittee (or Authorized Agent) Name and Tile -Please print or type Si, aFure of Per ttee (ol Authorized AqehS) (Date)
GW-59 Rev.212010

G«--59A COMPLIANCE REPORT PORN1
(Submit one euc-h m4mirorh . _
Permit # WCk-C-AC,6 )
1 Enter date monitoring results were due. 1 3O Al Will this monitoring report (GW-59 and GW-59A)
YES
be submitted after the established due date?
2 Was any required information missing on the GRV-59 report forms.,
YES
v0
IF the answer to question I or 2 is "YES", list in the space cr ce e 7 rr the well identification number(s) and
i
explain the problems encountered in obtaining the requirec a. _...
3
Are any of the monitor wells in need of repair or maintenance ldamaged casing, unlocked or missing cap, missing
'YES \D
identification plate, area overgrown, etc.)? If the answer is -Fes ••.:;onracr the Regional Offrce.for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
\O
If the answer to question 4 is "NO" skip to section B.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the s provided below:
`�ac,+efe
r� y�
Mvb— 1`�i^� ✓ �� 7 C` ill`71.�riL�'S�l-flL,*jc',1►iC'-hC',
Rrgx-v'-�1 r jig 7D"1 :17iG
Cl�}crf�ia�-i�`13 C►�1uc��.^r�►-hi�'�<l� l 1
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section B.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years)•
Miw1 3 JoIC, )151j21
TDFJ 3C>10
Are the monitoring wells listed in section 5 located at or beyond the review boundary? 1-ES jKlO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIA TELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located, contact the Regional Office,
7
Is the permittee implementing previously approved actions required by the Division involving this YFS
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided belosi.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subiect the permittee to a Notice of Violation,
fines, and/or penalties.
S
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report k( omplianc Rep 1+t GW-59AI true to the best knowledge.
is and complete of my
" �--� 7 17 i ' - z 1
I
ign tore mitten (or Autho ' e Agent) Date
Gv►-59A 12181200;

e] vi Iochem
ANAL'+TiCAL & CONSULTING CHEMISTS
Harvey Point Defense Testing Activity
2835 Harvey Point Road
Hertford NC 27944
Attention: Dustin Combs
Lab ID Sample ID:
21-49264 Site: MW-1
Test
Ammonia Nitrogen
Total Dissolved Solids (TDS)
Total Phosphorus
Total Organic Carbon (TOC)
1, 1. 1,2-Tetrachloroethane
1, 1, 1 -Trichioroethane
1,1,2, 2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-DicNoroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichioropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1.2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trim ethyl benzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1.4-Dichlorobenzene
2.2-Dichloropropane
2-Chlorotoluene
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392,0223 Lab • 910.392.4424 Fat
710 13owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info u environmentalchemists.com
Method
Date of Report: Nov 17, 2021
Customer PO #:
Customer ID: 10030007
Report #: 2021-19688
Project ID: Monitoring Wells
Collect Date/Time Matrix
11/5/2021 8:15 AM Water
EPA 350,1, Rev 20 1993
SM 2540 C-2015
SM 4500 P (F-H)-2011
SM 5310 9-2014
SM 6200 C-2011
SM 0200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-20f 1
SM 5200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 8200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 5200 C-2011
SM 6200 C-2011
SM 6200 C-2011
SM 6200 C-2011
Results
Sampled by
Dustin Combs
Date Analyzed
1.8mg/l_
11/11/2021
233 mg/L
11/09/2021
2.37 mg/L
11 /12/2021
32.8 mg/L
11/11/2021
< 0.50 µg/L
11/6/2021
< 0.50 µg/L
11/6/2021
< 0.50 µg/L
11/6/2021
< 0,50 µg/L
11/6/2021
< 0.50 µg/L
11/6/2021
* 0.50 pg/L
11/6/2021
< 0.50µg/L
11/6/2021
< 0.50 µg/L
11/6/2021
< 0.50 µg/L
11/6/2021
< 0.50 µg/L
11/6/2021
< 0.50pg/L
11/6/2021
< 0.50 µglL
11/6/2021
* 0.50 µg/L
1116/202'.
< 0.50 µg/L
11/6/202'
* 0,50 ug/L
I1/6/2C2'
* 0.50 µg/L
11 /6, 2K2'
* 0.50 µg/L
1'.'6 2�2'
< 0.50 pg/L
, 5 K2-
* 0.50 µg/L
= 2:21
* 0.50µg/L
.2--2'
< 0,50 pg/L
".6,2�2'
* 0.50 µg/L
111612021
Report #:: 2021.19688 Page 1 of 9

Eenvir,ochemn]
ANALYTICAL &. CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910,392.4424 Fax
710 Bowsertown (toad, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
info Cenvironmen[alchemists.com
Harvey Point Defense Testing Activity
Date of Report: Nov 17, 2021
2835 Harvey Point Road
Customer PO #:
Hertford NC
27944
Customer ID: 10030007
Attention: Dustin Combs
Report #: 2021-19688
Project ID: Monitoring Wells
4-Chlorotoluene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Benzene
SM 6200 c-2011
< 0,50 pg/L
11/6/2021
Bromobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Bromochloromethane
SM 6200 C-2011
< 0.5C pg/L
11 /612021
Bromodichloromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Bromoform
SM 6200 C-2011
< 0.50 pg1L
11 /6/2021
Bromomethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Carbon tetrachloride
SM 6200 C-2011
< 0.50 pg/L
111612021
Chlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Chloroethane
SM 6200 C-2011
< 0.50 pg/L
11 /612021
Chloroform
SM 6200 C-2011
< 0,50 pg/L
11/6/2021
Chloromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
cis-1,2-Dichloroethene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
cis- 1,3-Dichloropropene
SM62DOC-2011
<0.50pg/L
11/6/2021
Dibromochloromethane
SM 5200 C-2011
< 0.50 pg/L
11/6/2021
Dibromomethane
SM 6200 C-2011
< 0.50 pg/L
11 /612021
Dichlorodifluoromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Ethylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Hexachlorobutadiene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
lsopropylbenzene
SM 62oo C-2011
< 0.50 pg/L
11/6/2021
M+P Xylene
SM 6200 C-2011
< 1.00 pg/L
11/6/2021
Methylene chloride
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Naphthalene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
n-Butylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
n-Propylbenzene
SM 6200 C-2o11
< 0.50 pg/L
11/6/2021
ortho-Xylene
SM 62co C-2011
< 0.50 pg/L
11 /612021
p-Isopropyltaluene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
sec-Butylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Styrene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
tert-Butylbenzene
SM6200C-2011
< 0,50pg/L
11/6/2021
Report #:: 2021-196a6
Page 2 of 9

ANALYTICAL 8 CONSULTING CHEMISTS
Harvey Point Defense Testing Activity
2835 Harvey Point Road
Hertford NC 27944
Attention: Dustin Combs
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, IBC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 17, 2021
Customer PO #:
Customer ID: 10030007
Report #: 2021-19688
Project ID: Monitoring Wells
Tetrachloroethene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Toluene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Trans- 1,2-Dichloroethene
SM 6200 C-2011
< 0 50 {ig/L
11/6/2021
Trans-1,3-dichloropropene
SMfi200C-2011
<0,50pg/L
11/6I2021
Trich loroethene
SM 6200 C-2011
< 0.50 pg/L
11 /612021
Trichlorofluoromethane
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
Vinyl chloride
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
Fecal Coliform
SM9222DMF
<1 Colonies/100mL
11/05/2021
Chloride
SM4500 C] E-2011
87mg/L
11/08/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev, 2.0, 1993
< 0.02 mg/L
11/05/2021
Nitrate+ N itrite-N itrogen
EPA 353.2, Rev, 2.0, 1993
0.02 mg/L
11/09/2021
Nitrate Nitrogen
Subtraction Method
0.02 mg/L
11/15/2021
Reoc.rt #, 2021-186a9 Page 3 of 9

envirochem
r
ANALYTICAL & CONSULTING CHEMISTS
Harvey Point Defense Testing Activity
2835 Harvey Point Road
Hertford NC 27944
Attention: Dustin Combs
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 913,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.3702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910-347.5843 Lab/Fax
infoCaenvironmentalcnernists.com
Date of Report: Nov 17, 2021
Customer PO #:
Customer ID: 10030007
Report #: 2021-19688
Project ID: Monitoring Wells
Lab ID Sample ID;
Collect Date/Time
Matrix Sampled by
21-49265 Site: MW-2
11/5/2021 8:30 AM
Water Dustin
Combs
Test
Method
Results
Date Analyzed
Ammonia Nitrogen
EPA 35o.1, Rev. 2.0,1993
1.5 mg/L
11/11/2021
Total Dissolved Solids (TDS)
SM 2540 C-2015
304 mg/L
11 /09/2021
Totai Phosphorus
SM 4500 P (F-H)-2011
0.64 mg/L
11/12/2021
Total Organic Carbon (TOC)
SM 5310 8-2014
12.8 mg/L
11/12/2021
1.1,1,2-Tetrachloroethane
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
1,1.1-Trichloroethane
SM 6200 C-2011
< 0.50 pg/L
11 /612021
1.1,2,2-Tetrachloroethane
SM6200C-2o11
<0.50pg/L
11/6/2021
1,1,2-Trichloroethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,1-Dichloroethane
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
1, 1 -Dichloroethene
SM 6200 c-2011
< 0. 50 pg/L
11 /612021
1,1-Dichloropropene
SM 620a c-2011
< 0.50 pg/L
11/6/2021
1,2,3-Trichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2,3-Trichloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2,4-Trichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2,4-Trimethylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2-Dibromo-3-Chloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2-Dibromoethane
SM 6200 C-2011
< 0,50 pg/L
11/6/2021
1,2-Dichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2-Dichloroethane
SM 52CO C-2011
< 0.50 pg/L
11/6/2021
1,2-Dichloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,3,5-Trimethylbenzene
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
1,3-Dichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11 /612021
1,3-Dichloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,4-Dichlorobenzene
SM620o C-2011
< 0.50 pg/L
11 /612021
2,2-Dichloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
2-Chlorotoluene
SM 6200 C-2011
< 0.50 pg/L
1102021
Report#:: 2021-19688
Page 4 of

:env--roche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, \C 25405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Nianteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville,',C 28540 • 910.347.5843 Lab/Fax
[e-mail]
Harvey Point Defense Testing Activity
Date of Report: Nov 17, 2021
2835 Harvey Point Road
Customer PO #;
Hertford NC
27944
Customer ID: 10030007
Attention: Dustin Combs
Report #: 2021-19688
Project ID: Monitoring Wells
4-Chlorotoluene
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
Benzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Bromobenzene
SM 6200 C-2011
< 0.50 pg/L
11 /612021
Bromochloromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Bromodichloromethane
SM 6200 C-2a11
< 0.50 pg/L
11/6/2021
Bromoform
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Brornomethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Carbon tetrachloride
SM6200C-2011
< 0.50pg/L
11/6/2021
Chlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Chloroethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Chloroform
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Chloromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
cis- 1,2-Dichloroethene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
cis-1,3-Dichloropropene
SM6200C-2011
<0,50pg/L
11/6/2021
Dibromochloromethane
SM 62ao C-2011
< 0.50 pg/L
11/6/2021
Dibromomethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Dichlorodifluoromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Ethylbenzene
SM 6200 C-2011
< 0,50 pg/L
11/6/2021
Hexachlorobutadiene
SM 0200 C-2o11
< 0.50 pg/L
11/6/2021
isopropyl benzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
M*P Xylene
SM 6200 c-2011
< 1.00 pg/L
111612021
Methylene chloride
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Naphthalene
SM 6200 C-2011
< 0.50 pglL
11/6/2021
n-Butylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
n-Propylbenzene
SM 5200 C-2011
< 0.50 pg/L
1116/2021
ortho-Xylene
SM 6200 C-2011
< D.50 pg/L
11/6/2021
p-Isopropyltoluene
SM 6200 0-2011
< 0.50 pg/L
11/6/2024
sec-Butyi benzene
SM 6200 C-2011
< 0.50 pg1L
11/6/2021
Styrene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
tert-Butylbenzene
SM 6200 C.2011
< 0.50 pg/L
11/6/2021
Report 1e:: 2021-19666
Page 5 of 9

Environmental Chemists, Inc.
1 : to 6602 Windmill Way, Wilmington, NC 28405 ' 910,392.0223 Lab • 910.392.4424 Fax
710 $owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Harvey Point Defense Testing Activity
Date of Report: Nov 17, 2021
2835 Harvey Point Road
Customer PO #:
Hertford NC
27944
Customer ID: 10030007
Attention: Dustin Combs
Report #: 2021-19688
Project ID: Monitoring Wells
Tetrachloroethene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Toluene
SM 5200 C-2011
< 0.50 Pg/L
11/6/2021
Trans-1,2-Dichloroethene
SM62COC-2011
<0.50wgIL
11/6/2021
-pans-1,3-dichloropropene
SM6200C-2011
< 0.50ug/L
11/6/2021
"-icy !croethene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Tr;cr: crofluoromethane
SM6200C-2011
< 0.50ug/L
11/6/2021
V;^yi cnioride
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Fecal Coliform
SM 9222D MF
<1 Colonies/100mL
11/05/2021
Chloride
SM45000IE-2011
138mg/L
11/08/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0. 1993
<0.02mg/L
11/05/2021
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.03 mg/L
11/09/2021
Nitrate Nitrogen
Subtraction Method
0.03 mg/L
11/15/2021
ReportX: 2021.19668 Page 6 of 9

Eviroehem
ANALYTICAL $ CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowser town Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5543 Lab/Fax
[e-mail]
Harvey Point Defense Testing Activity
Date of Report: Nov 17, 2021
2835 Harvey Point Road
Customer PO #:
Hertford NC
27944
Customer ID: 10030007
Attention: Dustin Combs
Report #: 2021-19588
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
21-49266 Site: MW-3
11/5/2021
8:45 AM Water Dustin Combs
Test
Method
Results
Date Analyzed
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
< 0.2rng1L
11/11/2021
Total Dissolved Solids (TDS)
SM 2540 C-2015
1710 mg/L
11/09/2021
Total Phosphorus
SM 4500 P (F-H)-2011
0.76mg/L
11/12/2021
Total Organic Carbon (TOC)
SM5310B-2014
29.1 mg/L
11/12/2021
1, 1, 1,2-Tetrachloroethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1, 1, 1 -Trichloroetha ne
SM 6200 C-2011
< 0.50 pg/L
111612021
1,1,2,2-Tetrachloroethane
SM62000-2011
<0,50pg/L
11/6/2021
1,1, 2-Trick loroethane
SM 5200 C-2011
< 0, 50 pg/L
11/6/2021
1,1-Dichloroethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1, 1 -Dichloroethene
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
1,1-Dichloropropane
5M 9200 C-2011
< 0.50 pg/L
11/6/2021
1, 2, 3-Trichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11 /612021
1, 2, 3-Trichlo ropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2,4-Trichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11 /612021
1,2,4-Trimethylbenzene
SM6200C-2011
<0.50pg/L
11/6/2021
1,2-Dibromo-3-Chloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2-Dibromoethane
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
1,2-Dichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1,2-Dichloroethane
SM 6200 C-2011
< 0.50 pg/L
11 /612021
1,2-Dichloropropane
SM 6200 C-2011
< 0.60 pg/L
11/6/2021
1,3, 5-Trimethylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
1, 3-D ich loro benzene
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
1,3-Dichloropropane
sM6200c-2011
<0.50pg/L
11/6/2021
1,4-Dichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
2,2-Dichloropropane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
2-Chlorotoluene
SM 6200 C-2011
< 0.50 pg/L
11/6/2024
Report #:: 2021-19688
Page 7 of 9

Environmental Chemists, Inc.
t 6602 Windmill Way, Wilmington, NC 28405 ' K0.392.0223 Lab " 910.392.4424 Fax
:v
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS info laenvirormentalchemists.com
Harvey Point Defense Testing Activity
Date of Report: Nov 17, 2021
2835 Harvey Point Road
Customer PO #:
Hertford NC
27944
Customer ID: 10030007
Attention: Dustin Combs
Report#: 2021-1968B
Project ID: Monitoring Wells
4-Chiorotoluene
SM 6200C-2011
< 0.50 pg/L
11/6/2021
Benzene
SM 6200 c-2011
< 0.50 pg/L
11/6/2021
Bromobenzene
SM 6200 C-2011
< 0.50 {ig/L
11/6/2021
Bromochloromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Bromodichloromethane
SM6200C-2011
0.97pg/L
11/6/2021
Bromoform
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Bro m om etha n e
SM 6200 C-2011
< 0, 50 pg/L
11/6/2021
Carbon, tetrachloride
SM6200C-2011
< 0.50 pg/L
11/6/2021
Chlorobenzene
SM6200C-2011
< 0.50 pg/L
11/6/2021
Chloroethane
SM 6200 C-2011
< 0,50 pg/L
11/6/2021
Chloroform
SM 6200 C-2011
53.8 pg/L
11/6/2021
Chloromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
cis-1,2-Dichloroethene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
cis- 1,3-Dichloropropene
SM62000-2011
< 0,50 pg/L
11/6/2021
Dibromochloromethane
SM6200C-2011
0,75 pg/L
11/6/2021
Dibromomethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Dichlorodifluoromethane
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Ethylbenzene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Hexachlorobutadiene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
lsopropylbenzene
SM620OC-2011
< 0,50 pg/L
11/6/2021
M+P Xylene
SM 6200 C-2011
< 1.00 pg/L
11/612021
Methylene chloride
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
Naphthalene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
n-Butytbenzene
SM 5200 C-2011
< 0.50 pg/L
11/6/2021
n-Propyibenzene
5M6200C-2011
< 0.50pg/L
11/6/2021
ortho-Xylene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
p-Iscpropyitoluene
SM 6200 C-2011
< 0.50 pg1L
11/6/2021
sec-Buty`benzene
SM 6200 C•2011
< 0.50 pg/L
11/6/2021
Styrene
SM 6200 C-2011
< 0.50 pg/L
11/6/2021
tert-Butylbenzene
SM6200C-2011
< 0.50pg/L
11/6/2021
Repor; #:: 2021.19666 Page 8 of 9

[enviroehem,]n
ANALYTICAL & CONSULTING CHEMISTS
Harvey Point Defense Testing Activity
2835 Harvey Point Road
Hertford NC 27944
Attention: Dustin Combs
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, IBC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info(a environmentalchemists.com
Date of Report: Nov 17, 2021
Customer PO #:
Customer ID: 10030007
Report #: 2021-19688
Project ID: Monitoring Wells
Tetrachloroethene
SM 52o0 C-2011
< 0-50 pgIL
11/6/2021
Toluene
SM 6200 C-2011
25.0 pg/L
11/6/2021
Trans- l,2-Dichloroethene
SM6200C-2011
<0.50pg/L
11/6/2021
Trans-1,3-dichloropropene
SM6200C-2a11
<0.50pg/L
11/6/2021
Trichloroethene
SM 6200 C-2011
< 0.50 pg/L
11/612021
Trichlorofl uo ro m eth a ne
SM 6200 C-2o11
< 0.50 pg/ L
11/6/2021
Vinyl chloride
5M 6200 C-2011
< 0.50 Wg/L
11/6/2021
Feml Coliform
SM9222DMF
<1 Colonies1100mL
11/05/2021
Chloride
SM4500 CI E-2o11
693 mg/L
11/08/2021
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA353.2, Rev. 2.0, 1993 0.15 mg/L 11/05/2021
Nitrate+Nitrite-Nitrogen EPA353.2. Rev. 2.0. 1993 0.12 mg/L 11/09/2021
Nitrate Nitrogen Subtraction Method <0.02mg/L 11/15/2021
Comment:
Reviewed by:
Report #:: 2021-19688 Page 9 of 9

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
-�' - u Date: S 21 Report Number: 2021.-
cf sample: ECHEM Pickup Client Delivery © UPS ❑ FedEx ❑ Other
❑ YES ❑ NO
N/A —Ti.
Were custody seats present on the cooler?
YES 112 NO 11 If custody seals were present, were they intact/unbroken?
0^g.na'te--perature upon receipt t °C Corrected temperature upon receipt
terrnerature taken: ❑ Temperature Blank K Against Bottles
C. n D. T;^omas Traceable 5/N 192511657 IR Gun Correction Factor °C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
`."r I ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES 10 NO
5. Were sample 1D's listed on the COC?
'" =5 Cl NO
6. Were samples ID's listed on sample containers?
L� ❑ N0
7. Were collection date and time listed on the COC?
s NO
8. Were tests to be performed listed on the COC?
NO
9. Did samples arrive in proper containers for each test?
=5 NO
10. Did samples arrive in good condition for each test?
1 NNCl Ill
Was ;ApnF+Atw carnnIp t,nlrwna �„ 0-4hla)'
=� ❑ NO
12. Were samples received within proper holding time for requested tests?
•.5
© NO
13. Were acid preserved samples received at a pH of <2?
DES
❑ NO
14. Were cyanide samples received at a pH >12?
r- E5
❑ NO
15. Were sulfide samples received at a pH >9?
ES
© NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
Y E5
❑ NO jig.
Were orthophosphate samples filtered in the field within 15 minutes?
' T�)-/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
*' Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
I
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
❑otify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 284C5 • 910.392.G223 Lab • 910.3��' y
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab F .
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 91C 347.58. -3 F.
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Harvey Point Defense Testing Activity Date of Report: Dec 15, 2021
2835 Harvey Point Road Customer PO #:
Hertford NC 27944 Customer ID: 10030007
Attention: Dustin Combs Report #: 2021-21395
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53641 Site: MW-3 12/3/2021 9,00 AM Water Dustin Combs
Test Method Results Date Analyzed
1,1,1,2-Tetrachloroethane
SM6200C-2011
< 0,50pg/L
12/8/2021
1,1,1-Trichlaroethane
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
1,1,2,2-Tetrachloroethane
SM6200C-2011
<0.50pg/L
12/8/2021
1,1,2-Trichloroethane
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
1,1-Dichloroethane
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
1 1-Dichloroethene
SM 6200 C•2011
< 0.50 pg/L
12/8/2021
1. 1 -Dichloropropene
SM e20C C-2011
< 0,50 pg/L
12/8/2021
1 2.3-Thchlorobenzene
SM 6200 c-2011
< 0,50 pg/L
12/8/2021
1.2.3-Trichloropropane
SM 620o c-2011
< 0,50 pg/L
12/8/2021
' 2.4-Trichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
1218/2021
1 2,4-Trimethyl benzene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
1,2-Dibromo-3-Chloropropane
SM6200C-2011
<0.50pg/L
12/8/2021
1,2-Dibromoethane
SM 6200 c-2011
< 0, 50 pg/L
12/8/2021
1,2-Dichlorobenzene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
12-Dichloroethane
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
1,2-Dichloropropane
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
1,3,5-Trimethylbenzene
SM 6200 c-201 i
< 0,50 pg/L
12/8/2021
1,3-Dichlorobenzene
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
1,3-Dichloropropane
SM 5200 c-2o11
< 0.50 pg/L
12/8/2021
1,4-Dichlorobenzene
SM 6200 c-2011
< 0, 50 pg/L
12/8/2021
2,2-Dichloropropane
SM 620o C-2011
< 0.50 pg/L
12/8/2021
2-Chlorotoluene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
4-Chlorotoluene
SM 6200 c-2011
< 0,50 pg/L
12/8/2021
Benzene
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
Bromobenzene
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
Bromochloromethane
SM 6200 C-2011
< 0.50 pg1L
12/8/2021
Report # 2021-21395 Page 1 of 3

Environmental Chemists, Inc.
envirochem
6602 ��indmili
' , ; , �;:: ,irgton, NC 2640 • 910.392.0223 Lab • 9i0=°=
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702
Lab/Fa•
4
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.34738.13 Lai
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Harvey Point Defense Testing Activity
Date of Report: Dec 15, 2021
2835 Harvey Point Road
Customer PO #:
Hertford NC 27944
Customer ID: 10030007
Attention: Dustin Combs
Report#: 2021-21395
Project ID: Monitoring Wells
Bromodichloromethane
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Bromoform
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Bromomethane
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Carbon tetrachloride
SM62000-eon
< 0.50pg/L
12/8/2021
Chlorobenzene
SM 6200 C-2011
< 0 50 pg/L
121812021
Chlorcethane
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
Chloroform
SM 6200 C-2011
83,2 pg/L
12/8/2021
Chloromethane
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
cis-1,2-Dichloroethene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
cis-1.3-Dichloropropene
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
Dibromochloromethane
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
DVomomethane
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
Dichlorodifluoromethane
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
Ethylbenzene
SM 6209 C-2011
< 0.50 pg/L
12/8/2021
Hexachlorobutadiene
SM e200 C-2011
< 0.50 pg/L
12/812021
Isopropylbenzene
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
M+P Xylene
SM 6200 C-2011
< 1.00 pg/L
12/8/2021
Methylene chloride
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Naphthalene
SM 6200 c-2011
< 0.50 pg/L
12/8/2021
n-Butylbenzene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
n-Propylbenzene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
ortho-Xyfene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
p-Isopropyltoluene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
sec-Butylbenzene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Styrene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
tert-Butylbenzene
SM 6200 C-2011
< 0.50 pg/L
12/8/202 1
Tetrachloroethene
SM 6200 C-2011
< 0.50 pg/L
12/8/202'
Toluene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Trans-1,2-Dichloroethene
SM 6200 C-2011
< 0.50 pg/L
12/8/2021
Trans-1,3-dichloropropene
SM 6200 C-2011
< 0,50 pg/L
12/8/2021
Report # : 2021-21395
Page 2 of 3

Environmental Chemists, Inc.
v
ANALYTICAL & CONSULTING CHEMISTS
Harvey Point Defense Testing Activity
2835 Harvey Point Road
Hertford NC 27944
Attention: Dustin Combs
Date of Report: Dec 15, 2021
Customer PO #:
Customer ID: 10030007
Report #: 2021-21395
Project 1D: Monitoring Wells
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/8/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/8/2021
Vinyl chloride SM6200C-2011 < 0.50Ng/L 12/8/2021
Comment:
Reviewed by:�
Report 4 2021-21395 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: H-6" ,� �Date. 2 3 �4 Report Number:— _ 2/21- 2-1 9 S
Receipt of sample: ECHEM Pickup K Client Delivery 0 UPS ❑ FeclEx ❑ Other ❑
❑ YES ❑ NO N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun fD: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 5°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES C NO 5. Were sample la's listed on the COC?
YES !❑ NO 6, Were samples lD's listed on sample containers?
=5 ❑ NO 7. Were collection date and time listed on the COC?
NO 8. Were tests to be performed fisted on the COC?
9 Did samples arrive in proper containers for each test?
C 10. Did samples arrive in good condition for each test?
_ — tibias adequate sample volume available?'
1 :2. Were samples received within proper holding time for requested tests?
"4O ' 13. Were acid preserved samples received at a pH of <2?
-- — `y0 14. Were cyanide samples received at a pH >12?
- , NO#17.
Were sulfide samples received at a pH >9?
== ❑ NO Were NH3/TKN/Phenol received at a chlorine residua! of <0.5 m/1 ? **
=5 ❑ NO Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/t_?
-- El NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
' -- , c at ies are ph checked at time of analysis and recorded on the benchsheet.
;a samples are checked far Chlorine at time of analysis and recorded on the benchsheet.
jSa—pie Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
- • a -fling (circle one): H2SO4 HNO3 HCI NaOH
�.—= of preservation: If more than one preservative is needed, notate in comments below
`act °y customer service immediately for incorrectiy preserved samples. obtain a new sample or
tie state lab if directed to analyzed by the customer. who was notified, date and time:
Ualatiles Sample(s) were received with headspace
COMMENTS:
°C
DOC. QA.002 Rev 1