WQ0016247_Modification_20211214

Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
Permit Number (IR) * WQ0016247
Applicant/Permittee Synagro Central, LLC
Applicant/Permittee Address 284 Boger Rd. Mocksville NC 27028
Is the owner in BIMS? Yes No Is the facility in BIMS? Yes No
Owner Type
Facility Name
County
Fee Category
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Organization
Synagro Western Piedmont Class B Residuals Program
Alexander
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $395
Complete App Date 12/14/2021
Below list any additional email address that need notification about a new project.
... ... ..
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Synagro Central LLC
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3364034324
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number: * WQ0016247
Has Current Existing permit number
Applicant/Permittee* Synagro Central, LLC
Applicant/Permittee Address* 284 Boger Rd. Mocksville NC 27028
Facility Name* Synagro Western Piedmont Class B Residuals Program
Please provide comments/notes on your current submittal below.
Modification to add additional source. Check sent via UPS. Tracking number: 1Z 51 F 78W 01
00991391
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
WO0016247 Dec 2021 Mod.pdf 19.57MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature

Submission Date 12/13/2021

SYNAGRO
December 7, 2021
N.C. Deparlinent of Environment and Natural Resources
Division of Water Resources
Water Quality Permitting Section — Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
ATTENTION: Mr. Nathaniel Thornburg
REFERENCE: APPLICATION FOR MODIFICATION OF PERMIT 4
WQ0016247
S'YNAGRO CENTRAL, LLC
Dear Mr, Thornburg:
Synagro Central LLC is submitting this application to modifiy the referenced residuals land
application permit.
The following modifications are requested:
1. Addition ofPittshcro WW'1'11 as an approved source.
Enclosed is a check for $395.00 to cover the fee associated with a major perinit m od I Fi cat i on.
This application package should contain all the information necessary to completc the
rearrested modification of Synagm's land application permit. However, if you require
additional information or have further questions, please contact ire at [phone] or
rroth ,,lsynagro.eorn_ Thank you in advance for the timely and efficient review of this renewal
application.
Sincerely,
ltoberl N. Roth
284 Boger Road, Mocksville, NC 27028 • Phone' [phone] . Fax: [phone]

Statc of North Carolina
DWR
Department of Environmental Quality
Division of water lizesonrces
Division of Water Resources RESIDUALS SOURCECER'I'LFICATION
INSTRUC'HONS FOR FORM) RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and eheeking the provided boxes will help produce a quicker review time and reciuce the amount of additional
information requested. Failure to submit x11 of the required items will lead to additional processing and review time for the
permit application. [Unless otherwise noted, the Anglicant shall submit Oise original and two copies of the nnnlication ahhrl
sutitlyrting documentation
1"Or wore h2fornwfio►r, visit the ]Prater Quafily flerraaitlrng Secdon's Non-Dischai Te Peordelhw /.'parr
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, cr disposal in accordance with 1 SA NCAC 02T . I 100, Do not submit this certification for review without
n mrrespanding npplicalioa form (FORM: RLAP 11-15, FORM: DCAR 11-15, ar FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Rcsiduals Source Certification (FORA: RSC 11-15):
Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthari=d content changes to this fond, If necessary for clarity or due to space restrictions, attachments to the
applicaticn may be made, as long as the aftachanents are numbered to correspond to the section and item to which they refer.
® For new or renmed permits, submit a separate certification far each source facility.
® For modified permits, submit a separate certification for only those facilities IIIat are affected by the proposed inodificadon.
Complete tlhe residuals soul-ce facility summary page. List all new, renewed, or modified faoliIitles.
S. Residuals Source -Generating Facility Informatiohh:
® For each source facility, attach the fallowing:
Vicinity map -A vicinity map that shows the location of the facility and meets all of the criteria in the "Man Guidance for
Residuals Land Applicad" Permits",
Process flow diagrain and/or narrative - A detailed narrative and/or process flow diagram that describes haw the residuals
art to be generated, treated, processed, and scored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in item t, $.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling paints, sampling frequency, sample type, as well as the Division-ertified laboratory to be used, in addition,
eirsure, that the plan dr;tails how the fAcility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to he land applied, distributed, andfor disposed.
C. Residuals Quality information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requimments.
For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS POP, FORM: RSC 06-16 Pagc l of l

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DWR
Division of Water Resources
State of North Carolina
Depai-tnient: ol'Environ mentaI Quality
Division of Water Resources
RESI DUALS SOURCE CERTIFICATION
FORM: RSC 06-14
1. RES]DUokLS SOURCE -GENERATING FACI1,ITY 11NFOItMAT10N (See Instructian B.):
I . Facility Name: Town of Pittsbom, Wastewatel'i-mattnerit Plant
2. Facility permit holder is: ❑ federal, ❑ State, 0 Local Government, or ❑ Private.
Facility permit issued by: 0 Div. of rater Resouives, ❑ Div, of Environmental I Icalth,
or ❑ Other (explain: _),
3. facility contact person and title: Jamie McLaurin: Wastewater Plant Saper€ntertdent
Complete mailing address: P.O. Box 759
City: Pittsboro Slate: l,�C 2ip: 27312
Telephone nwiibrr: (2L9) 200-8927 E-mail address: jmclauriA [e-mail]
4. Facility physical addresm 495 Small St
City: Pittsboro Stale: NC Zip: 27312-
Coordinates: Latitude: 35° 42`52" Longitude: 7r 10' 12"
Datum: Man Level afaccuracy; Secoml
Melted of measurement: Map
5. Purpose ofthe facility:
® treatment of municipal wastewater, ❑ treatinent of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
Q ireatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: °/a industraI an d % domestic)
❑ other (explain:_).
G, Does the facility have an approved pretreatment pr❑grans: Yes ❑ No
7, Fac€Illy permitted{design flow:.75 MGD and facility average daily flow:.575 MGD
S. Average amount of residuals being generated at this facility 12G.,£ dry tons per year.
9. Specify the fo€lowing regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatmcol: Aerobically digested liquid, 145,000 total zallons
Type and volume of residuals storage (i.e., outside of residuals treatment units): Two basins, 145,000 total gallons
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1, Specify if residuals are regulated under:
19 40 CFR Part 503 or ❑ 40 CFR furl 257.
Note: Only residuals that are generated during domcsticlmunicipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if res€duals are defined under 15A NCAC 02T..1 1_02 16 as:
Biological ❑ Nan -Biological
Note! Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that 11tilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed Elm sysleims).
FORM: RSC 06- 1G Page i of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit Environmental Technologies, Inc. and Date of analysis: 1/25/2021
Passed corrosivity test: M yes R no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes E] no. Flashpoint: >140 °F (> 140°F)
Passed reactivity test: Eyes ❑no. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
Ong/1)
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., ns applicable) to denlonstrate that the residuals do not
violate the ceiling concentrations for meials regulated under I5A \NCAC WT .1105,
a. Tar DiSfribrrriarrl wed A»nireadon. Fill [v the following table with the rmitS Of thV IateSt ailafySCS (i,C., on it dry weight
basis) far the following ill claI parameters;
Laboratory; Pace Anal tical Services LLC and Date of analysis: 01/1IJ2021
PAvArneter
Ceiling
Concentration Limits
(CY,L sri & cfasso)
(nrgi)W
Monthly Average
Concentration Limits
(aelss A only)
(Prg/kr)
Result
(+"949)
Arsenic
75
41
4.7
Cadmium
a5
39
AID
Copper
4,300
1,30D
150
Lead
940
300
11
Mercury
57
17
2.0
Molybdenum
75
n/a
3.9
Nickel
420
420
20
Selenium
100
100
5.8
zi ne,
7,500
2, $oo
400
b, For Surface D%snasul Unk f ayrdfifi): Fill in the following table with the results of the latest analyses (i.e., on a diy weight
basis] for the following metal parameters:
Laboratory; And Date o f an alys is:
DiStance frxynl DiSpoSal
Unit to Boundary to
CluseSi Fr6pL'Pty Lille
0-1e1s, check avre)
Arsenic
(irrglkg)
Chromium
(iwlkg)
Nickel
(rr►g.`kg)
❑ > 0 but c 25
30
200
210
❑ � 25 but c 50
34
220
240
❑ 2 50 but < 75
39
260
27-0
❑ Z: 75 but < 100
46
300
320
❑ 100 but < 125
53
360
390
❑ 125
62
450
420
Resull (Wglkg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 4.77 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 01/13/2021
Parameter
Result
(nrg/l(g)
Aluminum
43000
Ammonia -Nitrogen
14000
Calcium
9600
Magnesium
3400
Nitrate -Nitrite Nitrogen
25
pH (Standard Unit)
6.9
Phosphorus
22000
Potassium
3000
Sodium
1600
Total ICjeldahl Nitrogen
74000
c. Using the results listed in Item Il. 5b. above, calculate the sodium adsorption ration (SAR): 078
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): M default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (Ise) Year PAN
Five -Year
Maximum Adjusted PAN
0110(g)
(mg/hg)
Surface
25025
36703
Injection/Incorporation
32025
43730
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A
FORM: RSC 06-16 Page 4 of 5

7. Pathaten Reduction': Per 15A NCAC 02T. 1106, specify how residuals will meet the pathogen reduction requiraments:
a. For DtslribidinrtlCand Aopllea#orn oI'G7rrss A or EauhialoW.,
❑ A Fecal col iform density that is demonstrated to be less than 1,000 lh FN Per gram Df [Dial dry solids,
or
❑ A salmone!!a s;jx density that is demonstration to be less than 3 MPNi per 4 grams of total dry solids.
AND one ofthe followings (except for nu n-biological residuals):
❑ Alternative 1 [1SA NCAC 02T.1106(b)(3)(A)] - Time}Tcrnperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] -Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.1 106(b)(3)(C)] -Prior Testing For Enteric Viruslviable Helaninth Ova.
0 Alternstiva 4 [15A NCAC 02T. 1106(b)(3)(D)] -No Prior Testing For Enteric VirusMable I-Ici minth Ova.
❑ Alternative 5 [ 15A NCAC 02T.1 106(b)(3)(E),(K)] -Process to Furlher Reduce Pathogens (PFRP).
spccify one; ❑ composting, ❑ heat drying, ❑ heal treatment,
❑ therniophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. Fur i:altd A r alicfrlirfrr n Class l;:
Alternative I [ ISA NCAC 02T.1106(c)(I)] -Fecal Cofiform Density Dew oil stration.
❑ Alternative 2 [ 15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobia digestion, © air dryianaerohic digestion,
❑ composting, Or ❑ lime stabilization.
c. For Sip rface Disposaf:
❑ Select One of the Class A or Equivalent Pathogen Reduction Aherrmadves in Item 11. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in item 11. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in [tern 11.8. below [ 15A NICAC 02T. [ 106(a)(2.)].
❑ Nat Applicable - Nun-Blologieal Residuals with NO Domestic Wastewater Contribution.
8, Vector Attraction Reduction (VAR); per 16A NCAC 02T.1107, specify how residuals will ineet the VAR requirements:
X Alternative 1 115A NCAC 02TJ 107(a)(1)] -38% Volatile Solids Reduction (Aerobic/Anaerobic Digestionl)-
❑ Alternative 2 [15A NCAC 02T.1 107(a)(2}] - 40-Day Bench Seale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Beach Scale Test (Aerobic Digestion).
Alternative 4 [ 15A NCAC 02T.1107(a)(4)] -Specific c Oxygen Uptake [fate Test (Aerobic Digestion).
❑ Altcrnativc5 [1.5A NCAC 02T,1107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [ 15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T. 1107(aX7)] - Dying of Stabilized Residuals.
❑ Altimnative 8 [15A NCAC 02T. 1107(a)(8)) - ❑tying ofUnstrib iIized Residuals.
® Alternative 9 [15A NCAC 02T.1 107(a)(9)] - injection.
® A.Itcrnative 10 [1SA NCAC 02T.1 107(a)(10)] - Incorporation.
© Alternative for Surface Disposal Units Only - SoiUOther Material Cover [ 15A NCAC 021'.1107(b)(2)1.
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For aniinal pro atssing residuals, only alternatives 9 or 10 in ay be chosen due to the nuisance corid [Iions that typically
occur when thew residuals are applied and left on the land surFace.
FORM: RSC 06-16 Page 5 of 5

OPERATIONS AND MAINTENANCE PLAN
SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0016247 (Synagro Western Piedmont RLAP)
Inspection Plan
Inspections will be conducted on a weekly basis at the land application site during activities of the project. Inspection
frequency is based on the time frame to complete the project and the amount of dry tons to be land applied from the
facility. In all cases, fields shall be inspected during application or within 48 hours following application. The inspections
will consist of inspecting a current field that is being applied as well as inspecting random fields that have been completed.
These inspections will consist of:
1. Verifying that the "Pre -Operations Check List" has been completed and signed by both operational and technical
staff.
2. Checking the calculated loads to insure the correct amount of residuals are being land applied.
3. Insuring that all manned equipment has a copy of the spill control plan, the permit, and the operations and
maintenance plan.
4. Insuring that the field has been flagged properly and that all buffers are being adhered to.
S. Insuring that the "Crop and Landowner Verification" form has been filled out.
6. Verifying that the residuals have been adequately sampled to confirm compliance.
The records will be kept in the project files in the respective office for the project. The Permittee or Inspector shall report
by telephone to the NCDENR/DWR Mooresville Regional Office at 704-663-1699, as soon as possible, but no later than 24
hours after, or the next working day, following the occurrence or first knowledge of the occurrence of the following.
• Any occurrence with the distribution program resulting in the land application of significant amounts of
material that is abnormal in quantity or characteristics.
• Any failure of the distribution system that results in the release of material to surface waters.
• Any time that self -monitoring information indicates that the facility has gone out of compliance with the
permit.
• Any process failure that results in the system not adequately treating the residuals.
• Any spill or discharge from a vehicle or piping system during residuals transportation.
Any release that requires immediate reporting outside of normal business hours shall be called in to DENR at 800-662-
7956, 800-858-0368, or 919-733-3300. These numbers are to be called in the event of a release to surface waters or
imminent failure of a storage system when the event occurs outside of normal business hours. Within 5 days of the first
notice of an occurrence, a written response in the form of a letter shall be sent to DENR outlining the actions taken or
purposed actions taken to ensure that the problem does not recur.
Persons responsible for inspections on this project are as follows:
Robert N. Roth, Technical Services Manager or his designee

OPERATIONS AND MAINTENANCE PLAN
SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0016247
Sampling Plan
Sampling for this project consists of sampling the residuals prior to each land application event. The chart at
the bottom of Attachment A provides a listing of required sampling, based on the dry tonnage applied from
each individual WWTP. Based on the recent dry tonnage applied, each plant will need to be sampled either
once or four times per year.
The residuals shall be sampled annually for the following: (Regulatory level in milligrams per liter in parentheses.)
Arsenic (5.0)
1, 4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1, 2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2, 4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachlorethane (3.0)
2,4,5-Trichlorophenol (400.0)
M-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
204,5 TP ( Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl Chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
The residuals will also be sampled based on the chart below for the following constituents
Dry Tons Generated
(short tons per year)
Monitoring Frequency
(Established in 40 CFR 503 and 15A NCAC 02T.1111)
<319
1 time per year
=>319-<1,650
1 per Quarter (4 times per year)
=>1,650-<16,500
1 every 60 days (6 times per year)
=>16,500
1 every month (12 times per year)
Aluminum
Ammonia -Nitrogen
Arsenic
Cadmium
Calcium
Copper
Lead
Sodium Adsorption Ratio (SAR)
Magnesium
Mercury
Molybdenum
Nickel
Nitrate -Nitrite Nitrogen
Phosphorous
Potassium
pH
Plant Available Nitrogen (calculation)
Selenium
Sodium
Total Solids
Total Kjeldahl Nitrogen
Zinc
In order to meet pathogen requirements, the material from each plant will be sampled for fecal coliform density. The
means to verify vector attraction reduction monitoring requirements will vary based on each plant. The samples that will
be pulled for the TCLP, nutrient and metals sample, and fecal coliform density will be taken from the storage areas of each
plant. In contrast, for the City of Statesville's WWTPs and Clariant's WWTP, the samples will be taken prior to belt -
pressing the residuals as directed by testing requirements. Samples collected for nutrients/metals analysis and TCLP/RCI
will be composite samples. The following people are responsible for sampling:
Robert N Roth, Technical Services Manager or his designee.

OPERATIONS AND MAINTENANCE PLAN
SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0016247 (Synagro Western Piedmont)
Operational Functions
The operation function of this project is going to involve land application of either liquid or dewatered residuals. Liquid
material will be either be mixed in a basin or with a lagoon mixer prior to loading of tankers. Dewatered cake material
will be loaded into end dump trailers at the plant and transported to the field. Once at the field, dewatered cake will be
dumped and loaded into cake spreaders and liquid materials will be offloaded to liquid applicators. Both liquid and cake
material is going to be spread at agronomic rates that are determined by the nutrient and metal sample that is current
for that monitoring period. Liquid material will be spread with a liquid applicator that will use pressure to spread the
material in such a way to achieve a consistent spread pattern. Cake material will be applied with side discharge
spreaders. The material is going to be land applied on fields that are in normal agricultural row crop production or grass
land.
Safety Measures
Synagro believes in operating in a safety conscious manner and has all employees participate in quarterly online safety
course that are designed to help its employees recognize safety issues and take steps to prevent accidents from
occurring. In addition, all Synagro employees have the authority to stop operations if they think any aspect of the
operation is going to cause environmental or personal harm.
Maintenance Schedule
Synagro will follow the maintenance schedule as recommended by the Synagro fleet manager for the equipment
necessary to complete the job.

SPILL RESPONSE PLAN
PROJECT: SYNAGRO WESTERN PIEDMONT PERMIT W00016247
IN THE UNLIKELY EVENT OF A SPILL THE FOLLOWING ACTIONS SHALL BE TAKEN
IMMEDIATELY:
1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES:
The Synagro Operations Manager shall take immediate charge and initiate clean-up activities. Synagro labor and
equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the
NC Department of Transportation, and other private contractors as necessary.
2. HALT THE SOURCE OF THE SPILL:
Such as a ruptured container or damaged transport unit.
3. CONTAIN THE SPILL:
Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The Synagro Operations Manager or the person in charge on the
spill site will advise the clean-up personnel where to get the straw, time, and other items necessary to complete the clean-
up operation, i.e., local farmers, farm supply centers, nurseries, etc.
4. CLEAN-UP:
Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as
much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining
material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by
representatives of the state regulatory agency.
5. FINAL CLEAN-UP:
Employ rotary brush sweeper if needed and apply time to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction
of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original
condition if possible.
6. NOTIFICATION:
As soon as possible after the spill occurs, the Synagro Operations Manager or assistant will notify the Synagro Central
office, and they will then be responsible for notifying other key Synagro personnel. The Synagro Mocksville office can be
reached at 336-790-1610. Using the provided extensions, calls are forwarded to the appropriate staff.
7. REPORTING:
Synagro Central personnel will notify the Mooresville Regional office at [phone] as soon as possible, but not more
than 24 hours after, or on the next working day following the occurrence. The Operations Manager shall provide a written
report within 48 hours of the spill to the Technical Services Director. The report shall list all relative information and
actions taken. Synagro Central personnel will file a written report to the Mooresville Regional office of the NCDENR
within 5 days of the occurrence. For after hours reporting the Division's emergency number shall be called to report all
incidences (1-800-858-0368) or (919-733-3300).

State of Nortli Carolina
DWR
Department of Cnvironinental Qttality
Division of Water Resottrous
Division of Water Resaurces 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
iNSTRUCTIOiriS MR FORK, RLAP 06-16 & SIO PPORTING DOCUMENTATION
Plense use the following iusiructiotts as si cheeldist in order to ensure nil required items are subiuitted. Adherence to these
instructions and cltr.cicing fire providcd boxes will help produce a tluicl(er review time 216d 1°Cducc the amount of additional
inrorninlioia reguegful. Failure to submit all of ilie required items will lead to additional proces%ing and review lime i`or the
permit application. Unless utherwise noted the A pIicaul shall submit one orl.inaf and two copies of the apulwatinn and
sn1)1rnrtinL) docuirlcntstion
for y1ore ij oi-weition, visit the b atur Quality Per ntPring Section's )Von -Discharge PerM;WfirS _I.I.nh
Gupierml — This application is for ircatinent, storage, ti-dnsport, nndlor land application of Class R residuals (inay include residuals that
are generated from a water treatment plant or other type facilities) on Ilia proposed ar currently approved laird application sitc(s) under
15A NCAC 02T .1100.
Unless otherwise srvted, the Applicant shall saibiriit oale original and two copies of the npplication and mipporting documentation listed
below.
A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Appkition Packages):
® Submit the compictcd 4tid appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) Win. Please
do not snake any unati thori zed content changes to this form. if necessary for clarity or due to space restrictions, attachments to
the application may be inada, m long as the Atacliinents are numbered to correspond to the section and itein to which they
refer.
* `Hie Applicant's Certification on Page 5 of this form shall be signed 1t1 accoid$ncewith 15A NCAC 02T .0IDG(b). An alternate
person inay be designated as the signing official if ti delegation letter is provided from a person who in Calls the criteria in 15A
NCAC 02T .Q 10
® if this project is for a modification of an existing permit, submit one copy of the existing pet' nit.
Please submit this application foma at least 1&0 day prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed racillty(ies) for application packages involving new or changes to treatment and storage units.
B. Applicatlon Fee (New and Major Modification Application Packages)
Submit a check, money order or electronic Funds transfer made payable to: Nortli Carolina Department of Envirvalut ial
Quality (NCI)EQ).
Facility Cixssiiicatioly
Neer permit
Major (land ate permitted for i'�! 300 acres) I $1,310
Major Modification i
S395
Minor (land are permitted for < 300 acres) $91 D � $245 _
i - A major modification shall he clef ined as any permit modification that; increases the gene rating facility's residuals dry tonnuge;
adds additional land application areas not previously approved for that particular prograin [including transferring of field(s) from
one program to another]; adds additional residuals sources; or iw lodes the addition of now treatment or storage units/processes not
previously permitted, There is no Fee for minor modifications to a permit.
C, Cover Letter (All Application Pazkaps)
0 List ell items included in the application package, as well as a brief description of the requested permitting action.
D. Env ironill enial Assessments (May be Regtaired —See 15A NCAC IC .0300
Submit a copy of the Findings of No Significant Impact (FONSI) or Divirontnental impact Statement (BIS). AIso, inclride
information on any lnitigating factors) from the Environmental Assessmoitt (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public. funds and/or lands are used for
the construction of the sriirject facilities.
wSTRUCTIONS FOR FORM: RLAP 06-16 Page I of 3

Es opei•ntioir anti Mnintenance Plan (New tlnd Renewal Application Packages)
ror Modification Application, if there are any changes to the existing plan, suk>nil Rn updated O&M }clan,
Submit the O&M Plmi in accordance with 15A.L4CACO2T.1 I I and include at a ininimum:
® operational functions; describe the Opel-allon of the program to show whtit uperations are necessary for the progru'rs to
function and by whom the functions are to be conducted.
❑ {titainteasance schedules; inay include equipment calibration, nlnintenance ofsigm, etc.
Safety measures; may include safely lrainhig program, manuals, signs, ete.
Spill response plan; includltlg control, i:oatainment, renlediation,-,mergency contact infonnatimi, etc.
Inspection plan induding the Following information;
Names anti titles of personnel responsible for conducting the inspections.
Frequency and location of inspections, including those to be conducted by the ORC, and p1wedures to 85sure that tile,
selected looation(s) and inspection frequency are representative of the residual$ management prograrn,
® ❑ctailed description ofinspection proceduMs including record kcepingand actions tube talcen by the itlspcctor in the event
that noncompliance is observed.
Sainpl ing arld monitoring plan including the following information;
® Names atld titles of personnel responsible for conducting the saneplir1g and Innnitoring.
detailed dESGdption orinonitorllig procedures including parameters to be rnoniturcd.
® Sampling frequency and procedures to ussum, that mpresentative samples am being collected, Fluctuation in temperature,
flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event The
sampling plan shall account far any foreseen nuctuations in residuats quality and indicate the most limiting tunes for
residuals to ineet pathogen and vector attraction reduction requirements (e.g. Facilities that land apply multiple times per
year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is inost
likely to be negatively affected by cold temperatures.
THE FOLLOWING ADDITIONAL ITEMS G to M ARE REQUIRED FOR DEDICATED PROGRAM ONLY.
F. Peograln Determinatirut
❑ Dedicated residuals land application programs are Hues in which land application sites meet the criteria in 15A NCAC 02T
,I 102 12 . Specifically, a residuals land applications program is designated as dedicated if any of the following M'e appiicabie
❑ Any land application site certified for the residuats land application ptogrant That receives residuals at rates or frequencies
greater than agrorroinic rates.
❑ Any land application site e:cAMW for the residuals land application prograrn that is used primarily for residuals disposal,
and agricultural crop production is of secondary importance,
❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation
facilities or irrigation facilities fed through a fixed supply system.
❑ Please contact the Nan -Discharge Permitting Unit if you seed any assistance in determining whether your residuals program
Falls under the dedicated program def"rnitions.
G. 11'1'ow'a111 Information
❑ Provide tin explttnaliun or wily a dedicated system is required instead of a conventional non -dedicated systwu.
L] Provide an explanation of the dedicated system and its operation,
H. Detalie d Site Maps (AlI Naw or Modification Application Packages)
❑ Submit three (3) set5 of standard size plans and two (2) sets of t I" by i 7" plans (electronic format is acceptable - Adobe PDF
only). For Modifications, submit plans specific to the modification(s) Only.
❑ Plans must include the following minimum items:
❑ A general tocation map, a viciiiity map and a topographic neap with contours not exceeding 10 feet or25%ofthe total site
relief and showing all facility related structures and fences within the land application area.
❑ The Location of all wells (including usage and construction details if available), streams (cphetnecal, intermittent, and
perennial}, springs, lakes, ponds, and other surface drainage features within 500 feet cif the land appticadbil site(s).
❑ Delineation of the review and compliance boundaries
0 Setbacks as required by 15A NCAC 02T .1 103
0 Site property boundaries w0hi 500 Feet or all waste treatment, storage, and disposal site(s).
❑ A snap showing the entire irrigatiou area with an overlay ❑f the suitable irrigation area depicted by the soil scientist's
evaluation. The irrigation plans shall show each noxzlelerniiter and {wetted area (whets applicable). Clearly label spray
irrigation zones as they will be operated.
❑ flans must depi❑t a completed design and not be labeled with pieiinunary phrases (e.g., rOR REVIEW 01; LY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plaits. However, t11e plans play be Iabeled with
the phrase: FINAL DES 10N � NOT RELEAS 41) rOR CONSTRUCTION
INSTRUCTIONS FOR FORM: RLAP 06-1 G Page 2 of 3

J.
K,
L.
M.
Project >E yninatlon and Remivers Ito MRnrtgcment Plan (AIINcw Application I'ooliages oi-Moditications that include new sites)
❑ Submit €i project MILlalivn and n receiver site inanagtMeIIt plan (if al)p5icab1e) with recommendations coil Cecil in€, cover Crops
and their ability to atcepl the propowd appiIca[ ion rates.
Hydrogenlogic Report (All New Application Packages ar Modifications Involving increasing the total design capflcity)
❑ Submit a delalled hydrogeologlo evaluation in w=xinnce svith 15A NCAC 02T .1 1.04 d 4 and e4trtrnt Division Policy
available at. lttt :liwww.netvater.er Rules Policies and Re uWionsl. The document shall be sighed, sealed and direst by a
qualified pcofessimiaL
Engiuccring Drsign Documents (All New or Modification Application Packages with fixed irrigation facilities or irrig6tion
fucilities fed through fixed supply system)
❑ Submit engineering design doetnnenls that. have been signed, sealed, and dated by a NC licensed Professional Fjigineer andlor
Professional Land Surveyor in accordance with 15A NCAC 02T. I 104(d)f2l. For Modifications, submit an upduted site orals
specific to the tncdlfication(s) only.
❑ The design docrrtneals must iinelWe the following minimum items:
❑ Enginccri11g plans for the facility and equiptncut exccpt thw previously permitted unless they are directly tied into tile new
units or are critical to die undwstandhig afthe complete process:
❑ Specirications describing materials to he used, method of construction, and means for ensuring quality and integrity of the
finished product including leaking testing; and
❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic pivlile, total dynamic head
curve analysis for each pump, and irrigation design.
❑ Soil mapping units shown on all dispwal sites.
Water Iialauce (Ail New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities ar
irrigation tocII Itias fod through fixed supply systems}
❑ Submit a completed and accurate water balance in accci-dance with I SA NCAC 02T ,1 104(dX5 and curreflt Division Policy
available at: fit, tip•flwww ncwater.arVRu1es_Policies and RtgulatianslI
Property Ownership Documentation (All New or Modification Application Packages involving new andlor relocated Ireatment
or irrigation components)
❑ Pnopetty ownership documentation shall consist of one of the fallowing:
❑ Legal documentation of ownership (i.e., G I S, deed or article of incorporation), or
❑ Written notarized intent to purchase agreement sighed by both parties wish a plat or s4rrvey map, or
❑ An easeltrent running with the land speoif utdly indicating the intended rise of the property and meeting the regk0rements of
15A NCAC 021.0107 , or
❑ A written notarized lease agreement siglied by both patties, indicating the intended Use of the properly, as well as a plat ar
survey map.
ONE ORIGINAL AND TWO COPIES OF TH E COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SL1ATA, RE 9ENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION Olt WATER RE, $011 RC>'S
WATER QUALITY PERMIT'i NG SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAILS1;i VICE CENTER
RALEIGH, N0R'I H CAROLINA 27699-1617
TELEPHONE NUMBER, [phone]
By Courict•lanecial Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
VAX NUMBER: [phone]
iNsTRUCTIONS FOR FOKM; RLAP 06-16 Page 3 of

Stale of Notrtlt Carolina
DWR
DeparIment of CnvironmentaI Quality
Division of Water Resources
Division of Water Itesntlrces 15A NCAC t11T A 100 — RESIDUA" LAND APPLICATION PROGRAM
fORli4'1: RLAi' 06-16
1. APPLICANT INFORMA TIOM
1. Applicant's mine: SYnugru Central. LLC
Applicant type. ❑ individual N Corporation ❑ General Partnership ❑ Privately -owned Public Utility
❑ FederaI ❑ State ❑ Municipal ❑ County
Sign€tture authority's name per 15A NCAC 02T .010G.: Robeil N. Roth Title' Technical Services Mannor
Applicant's mailing address: 284 Barer Rd.
City, Mocksyd State: ]1 C Zip: 028-
Telephone number: (336) -1610 Email Address: rrath Q sYnagrv.Cbm
2. Consultant's name: NJA License Nikrnber (for P.E.):
Affiliation. ❑ On Staff ❑ Retained (Firin:
Consultant's snailing address:
City. State: _
Zip:
Telephone number: (-) =
Email A.ddr=;
3, Agronomist's name: N/A
License Number:
Affiliation: ❑ NIA ❑ On Stuff
❑ Retained {Firm; )
Agrancinist's smiling address:
City: ! state'
Zip: ,.
Telephone number: (_)
Email Atl vss:
4. Sail Scientist's names Chrlstopller Murl'aY License Number; 1284
Affiliation: ❑ N/A ❑ On Staff
0 Retained (Firm: Piedmont Environmental Associates)
Soil Scientist's mailing address: 5401 Thacker Duii;v Rd.
City: Grqqnsbor_n State: NC
Zip; 27406-
Telephone number; 3( 3G) 215-8820
Email Address: ,
5. Fee submitted: 395.00 (See lastmetion B)
II. PERMIT INFORMATION:
l , Appkatloli is f81 (check all that apply): ❑ new, 9 modified, ❑ renewed permit
2. 1f this appiication is being submitted to renew or modify an existing permit, provide the following:
Permit utunber: WO0016247
Date aFinast-recently issued permit: 11/ 712017
Dote of inost-recently cet'tified Attachment A (irdifferent than the permit); 1 I15/21
pate of most -recently certified Attachinent B (if different than the peltnit)i l 115/21
FORM: RLAP06-16 Page I of

i11. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 284 Boger Rd.
City: Mocksville State: NC Zip: 27028
Coordinates: Latitude: 350 58' 27" Longitude: 80. 30' 07"
Datum: NAD 84 Level of accuracy: Second
Method of measurement: MAP
2. County where residuals land application program is headquartered: Davie
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Robert N. Roth
Synagro, LLC
1001672
Back -Up ORC
Adam Brigman
Synagro,LLC
1006653
Additional Back -Up
ORCs
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test:
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen SunnnarV: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 13466.6 dry tons per year.
PAN
Pounds of PAN per Dry Ton
Pounds of PAN per Year
(Weighted Average)
Surface
Incorporation
Surface
Incorporation
or Injection
or Injection
First -Year
50.05
64.05
672,902
861,127
Five -Year Maximum Adjusted
73.46
87.46
987,646
1,175,871
b. Land Application Site Use StunmarV: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
431.05
Hay
1158.68
Pasture
1274.62
Twat:
2896.7
Methods
Surface
2864.35
Incorporation or Injection
Total:
2864.35
FORM: RLAP 06-16 Page 2 of 5

c. Resltlrrrrls Land Agpiieediou Srrnulserr ip: Determine the ill i11imttm acreage required to Ian apply the residuals Its ctiri-entiy
certified and 1)mpased for certilicat!on assuming the scenarios Iisted in (he foilow ing tabie:
Assumed
Acres Required Using
Acres Required Using
Application Me
First -Year PAN Concetltratiuns
Five -Year Maximum Adjusted FAIL!
0& Pl-Nlar yr)
Caneentratious
Sus -face
iecurporatlon or
Sut'raee
Incorporation ❑r
Injection
[ejection
13458.0
17222.5
19752.9
23517.4
50
t 00
6729.0
8611.3
9876.5
117583
L 0
4486.0
5744.8
6584.3
7839.1
200
3364.5
4305.6
4938.2
5879.4
G, if applicahle, provide a plait and a solledtlle to resolve any known issues that would prevent laud application of the proposed
msiduats due to the Violation of Noj1h Carolina Adnllnlsh'Ative Cede (e.g• not enough storage, not enough land, vectorreduciion
pfactices not in place, etc.):
T. Specify type of residuals program (See Instruction lr): 0 Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals progs^am contains any land applicatiorlsitt(s) thatreceives residuals at rates ar firquenciiesgreaterthan agronomic
rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural strap
production is ofsecondary importance, explain;
Residuals pvograrn contains any land application site(s) that receives residuals t1irough fixed iffigatian facilities or irrigation
facilities fed through a fixed supply system, explain;
1V, RF,$IDUAI S SOURCE ]INFORMATION; (Required for all now, renewed, or modified residuals source)
Colnpfete and Slibmit the following Rcsid uals Source Cerlljicalion and all associated documentation.
w Wh
TA
Residuals Source
Certification
V. LAND APPLICATION 5lTLE INFORMATION- (Re u[red for all new, renewed, or modified land appiicatierr site)
Complete and submit the following Lanci rlpplrcalia)a Site Cer•rrfica0ion and all associated documentation.
Land Applit*atlort Slice
Cerklfkndun, doc
FORM: CLAP 06-16 I'age 3 of 5

Note. Ile= V1. AppIionble to Dedicated Program with Excel ire if<11ic3�, syslcu� as�ly.
V1. DESIGN INFORMATION FOR FIXED IRRI ATION SVS EM
1. Theirrigation system is: ❑ Spray ❑ Drip
2. Dispasal system is: ❑ existing ❑ proposed.
3. Minimum depth to mean seasonal high wat,ertable (5HWT) within irrigation sites(s) per Soil Scientist's Evaluation; feet
below gmund surface. RuIm 15A NCAC 02T .0505{n) mquires at least one -fast verlical separation bet}Veen 2HWT and grom)d
surface.
4, Are there any arlifi6al dMiitage or water 1novement struvAtires within 200 feet of any irrigation area?
Lj Yes or D No if Yes, please explain if the sail scientist report addresses artificial structures and please indicate if
structures are to be maintained or mod iHed: .
5. Loading rates recommended by tl7e Soil Scientist Evaluation:
Soil Series
Pields within Soil Aron
Recommended
Loading Rate
iidh�•
Recommended
Loading Rate
in! ,'
G. Design loading rates are equal or less than the loading rates recoirtmended by Soil Scientist?
❑ Yes or n No if No, explain why 15A NCAC 02T .0505(n) is not met:
7. Nan -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field I Zorte
Design Aden
ft'
Number of
N❑zzlcs
I ]trxhnulti Application
hate allonsllu
Design Annual 1loadiitg
Rate allonsl r
Total
Spray Irrigation Design Element
Plant Slice(
I�umhei-
Specification
Ptti a Number
diameter aFnoa..ales
ft
wetted area of nozzles
ftl
Nozzle capacity
gp�n
Nomle manufacturer I model
1
Elevation of highest iroazle
ft
rO RW RLAP 06-16 page 4 of5

Applicant's Certifienliou (signiilt; nudtorlty huts( bo in carnpli>lorc with t5A NCAC 02T .Otttl):
The applicant orany affillak: has oat lacen cunvicted ol'an environmental crime, has not abandoned a wastewater facility without proper
closturc, (toes not have im outstanding civil penalty where. all appeals have Been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Ruic 15A NCAC 02T ,9105•
N Yes ❑ 'No, Explain;
I, RobertN. Roth hnical Service Man.;;get
(Signature Authority's Name —PLEASE PRINT) (Title)
attest that this application for Synagro Cenwal, LLC
(Facility Name)
has bt to reviewed by the and is accurate and complete to the best of ray knowledge. I understand (hurt the Division of Water Resources
(nay not conduct a technical review of this program and approval does not constitute a variance to nny rules or statutes 4inless specifically
granted in the perm it, Further, any dischm'ge of reAdu0.15 to slit face wafers or tilt% land will t'emi t in an immcdiate enfai'vem4 nt action,
which may include civil penalties, injunctive relief, andfor criminal proseetttion, l will make no claim against the division of Water
Resources should a condition of this permit be violated. 1 also understand that if all trquired parts of'this application are not completed
and that if all required supporting information and attachments are not included, this appiicatian puckage will be returned to isle as
ineomp lt:te.
Note: In accordance with North Carolina General Statutes §143-215.6A and §1.43-215.C13, any Person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of'a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties tip to $25,UOU liar violation.
Sig�iaittre: date:
FORM. RLAP 06-16 Page 5 of 5

Quantitative Justification for Residuals Production
The Town of Pittsboro WWTP is currently permitted for 318 dry tons per year of land
applied biosolids. There is no request at this time to change this amount. Based on the
average daily flows of 575,000 gallons per day, 318 dry tons per year should be sufficient
for any increase in volumes.
Total Dry Tons = gallons of residuals x % solids x 8.34 lbs/gallon
2,000 lbs/ton
= 575,000 gallons x 0.048 x 8.34 lbs/gallon
2,000 lbs/ton
= 115 dry tons

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UA
ti ChDJIIA� . 6
Site: Town of Pittsboro (all 16calions appmx1mals) I inch = 7,500 fe,?l

Residuals Sampling Plan
Town of Pittsboro
Wastewater Treatment Plant
Nutrients and Metals Analysis
Sampling Point: Basin
Sampling Frequency: Annually
Sample Type: Composite
Lab: Waypoint Analytical
Pathogen
Vector
TCLP
Sampling Point: Basin
Sampling Frequency: Annually
Sample Type: Grab, Fecal Testing
Lab: Cameron Testing
Sampling Point: Basin
Sampling Frequency: Annually
Sample Type: Grab, 30 Day Bench
Lab: Cameron Testing
Sampling Point: Basin
Sampling Frequency: Annually
Sample Type: Composite
Lab: Summit Environmental Technologies, Inc

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MY IRO14Meri7AL IVCHNOLOi211:5. INC
Ana1yncai cabore4crw
January 25, 2021
Chris Wynne
Synagro
284 Boger Rd.
MocksviIIe, NC 27MA
TEL:
FAX:
RE: Pittshoro W\ TP
Dear Chris Wynne.
SJrururir Envirroalurerrrrrl 7'ecfuro�oxied. fW.
J310 lyhr A
C'WYPAcVe marts. Ohio 44223
TEL [phone] FAA: (3317) 253-4439
frebsire_ krre.Jlu,�tir..sPtr¢krarl
Order Ma.: 2 t Q 10279
Summit Environmental Technologies, Inc. received l sampic(s) an 11712021 for the
analyses presented in the following report.
There were no problems with the arlalyticial events associated with this report unless noted
in the Case Narrative.
Quality contruI data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to Call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 89-0735, CRIIPor111a 2M, Colarada, CGunkdicul I11-I.01%. Florida iaEiX' EMMS6, Idaiw 01 IMEL, I Ilirtiois 204061, Ind1FnA C-OH-13, 1Cmsas
L•193d7, Kcnoxky (Usdergmund Slump Tnnk)3. Ka KM4 90MG. belwy1nnd 339. MirliWn 99U. Mimic" 1780279. Nevada 0H0392320204, New
Hhm*i rc 299,6, New Imey OI 1006, New Yo-rk 11777, Nor11r CutAina 39703 and 631. Norsk Dakala F-20I, Ohio DW, Chic) YAP CL0052, Okiahmna
2019-ISS, Onmoo ON200001, Parmsylvania 0J 1, RIIvde 1sbild L,%ona317, %awh Carolir 9AI6001, Texmx 71047M446-19-16, UtatiOF100923202412,
Virginia VF.I.Ap 10391,1Yea Virginia 9957C
Paga 1 of 36

.F{l+ijliiif 1:ll1'iFY711JJ1OFJlai iCC�f11UiUg7P.S� MC. Case Narrative
SUMMITE NVjncmmFNTAtTLCHNOLOCIII S, INC Cooyahaga Falk 0hfa44223 WOO: 2101K79
APTalytkaUlborefori TEL [phone] FAX [phone]
IVet�wg�J+rro.Il���r�r..serreh.sae� Dale: 112512421
CLIENT: 5ynagre
Project: P111sbvro WWTP
WorkOrder Narrative:
21010279: This rcpart in its entirety consists of the following documents: Cover Letter, Case narrative,
Analyticai Results, QC Suminary Report, Applicable Accreditation Information, Chain -of Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain (he Summit
Environmental Technologies, Inc., Work Order Number assigned to this report,
SllrnmIt Env ironmentaI Technologies, Inc., holds the accreditatiunslcertificativas listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Deport" For accredited analytcs list.
The information contained in this analytical report is (lie sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditicns. Summit Environmental 'Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry Weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of (lie requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
21010279-001a CYANIDE,REACTIVE-S(9014): Below detection limit data was reported based on
Total Cyanide Below Detection Limit
21010279-001 a TCLP-SVOC-CPest(808113). Bracketing CCV's exhibit high recoveries for Heptachlor
and Methoxychlor; sample is N.I. for these analytes.
Analytical Sequence QC Imes:
LCS-47303 TCLP-S V OC -C Pest(8 08 113): Possible high bias For Heptachlor and McthoxychIor due tc
high recoveries in bravkuting CCV's.
MB-47303 TCLP-SV0C-CPest(808 1 B). High recover-y(ies) in the CCV indicate high bias. Data
deemed acceptable as no target analytes were observed in the field saniple(s).
Original
Page 2 of 36

mmlir
3'xrawrAwronurenralTechnologies, lit Qualifiers and Acronyms
su3310 fttl
ENVY a"MEtiTikL ur—H NUi.og19S. INN CiQwhoga Falls, ONe 442; WCll: 210111279
Analyrlcnl tAbor&tares TEL: (3M) 253-Ott PAY- 030);S340
lYebsile: Dale: 11251202 L
These commonly used Qnalifiers and Acronyms may or may not be present in this report.
Qualifiers
1.1 The: rrrmpound tivos annlyved for but was lint detected.
1 "['he reported vnluc Ligreater than the Method Detection Liinit but less then the Retorting Limit.
I the hold lime for sample pieltaralion andlor analysis was exceeded.
D The result is reported from a dilution,
E The restilI exceeded the I inear t angc of the r alihrat-son a is estimated due In interference.
NICI The result is below the Minimum Gampottnd Limit,
* The result exceeds the Regulatory Limit or Maximum {:ontaminaiion Umil.
rn Manual integration was used to determine the area response.
d Manual integmtx}n in which peak was deleted
N The result is presumplive based an a Mass Spectral library seamh assuming a 1;1 icsponsc.
P The sucond column confirmation cxcvcded 25°lu difference.
C The result has been confirmed by GUMS.
X The ivsull was rtot confirmed kvincn GC/MS An;rlysis vas performed.
13 MB+ The analyte was detected in the associated blank,
G The ICB ur CCB contained reportable amotints of analyte_
QC-4 The CCV recovery failed low (-) or
R1QDR The Rl'l) was outside ofaccepled recovery limits,
QL-1+ The LCS or LCSD recovery railed low (-) orb igh (t],
QLR The LCS11.C:S❑ RPI] %was outside of accepted recovery limits.
QM.I+ 'rho MS or MSD recovery railed law (-) cr high (+).
QMR The MSIMSD RPD was outside of accepted recovery limits.
QV,l+ The 1C:V recovery failed lose (-) oT high (+),
S The spike result was onside of accepted recovery limits.
z Deviation; A devintion from lber method was ryerformed; Plcasv wfcr io tlu Cwc Nar ralirc rut
addirional information
Atemnyms
IYD
Not bd=ted
RL
Rcporling Limil
QC
Quid gy Control
141DL
Method Detection limit
MR
Method Blank
LOD
Level of Detectifln
LC5
L9b(IFUlary Control Sample
LCIQ
Level oFQkrSntdal ion
LCSI)
Laboratory CoiflnA Samp1q;Duplicatt
PQL
Practical Qualil i to t ion 1_4nit
QCS
Quality Control sample
CRQL
Contrae[ Required Quaniitalian Limit
DUP
Dupiicaw
Pl,
Nrmit Limit
MIS
Matrix Spike
RegLA
Regulatary Limit
W3D
Matrix Spike Duplicate
MCL
MaxirmkniContamination Limit
RPD
Relalivo Percent Differeal
MinCL
Wtinu rnCompouud Limit
1CV
IQiatCol ibretinn VcriFin tion
RA
Reanalysis
lC6
Inilini Calibration Blank
RE
Reexiraction
C.C:V
Continuing Cal ibrntlon Verification
TIC
Tentatively ldcneiFled {'arrlpnmrd
CCU
Continuing Calibration Blank
R71
Ralanlion Time
RLC:
Rapvrling L'unit Clocuk.
CF
Calibiatioll Factor
DIF
Dilullon Factor
KFN
Rcspanse racier
This list of Qualifiers and Acrmiyms reflects the mast commonly utilized Qualifiers and Acronyrs far reporting.
11lrol a refer to the Analytical Notes in flee Case NFL rrative for any Qualifiers or Acronyms that do not appear in this
list or for additional ilrforination regak-diug tltc use of these Qualifiers on reported data,
Original
Page 3 of 36

��� 5rnrmpir Crlrr1vorrrscufrrf 7'ecbojolagies, hrc.
3310 will &
ENVIn014MENTAL T0WN8LOC. i23, WC CayahW Falls, Qfdo 44223
,4nafrthuf Labanateol" TEL. [phone]V 0 FAX, (3311)) 253-4 39
1Febsire; hrrn:lhwvir.serre�.eoxt
CICIENT: Synagro
Project: PiWboro WWTP
LabSantpldll Client Sample11)
21010279 001 Piusbaro WW I P I OY
Tag No Date Collected
1102021 10.30:00 APA
Wo rkord er
Sample Summary
wok 21010279
aS-fan-21
Date Received hlalrix
IiW2021 10.15:00AM 5ludgc
Page 4 of 36

co
a
a�

SUMMIT idummif Enviogy iarNAf Technologies, hre• Analytical Report
3�iaklw&.
ENVIAONM t! WAL Ift;tir O L OWES, lta[: Cyr}vrhogn FrOs. 012io 44223 (tow TCliorrj
Analylkcaf i-nbomlaroE TF.L: (310) 253421 f PkK (330) 253.44A9 WON: 21010279
Wchsire: hnz?.11wrrw..sefrc✓F_cam Dam Reporled: 1125/2021
CLIENT:
5ynagro
Mfllrix.
SLUDGE
Lab ID:
2101.0279-001 A
Project:
Pittsburo WWT"P
Client Simple ID Pittsburg WWTP TCLP
Tag INmnher:
C;alleetion Date: I/W2021 10:30:00 AM
Analyses Result
RL Qual
Units
bF
Date Analyzed
TCLP METALS, VOC, RNA, PFST, HERB-5CLID
SVV7470A
SW7470A Analyst. ERA
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
N❑
0.00200
mgiL
1
V1612021 12:01:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SWi311f5O10)
TCLP Amenic(As)
NO
0,500
m91L
1
1119i2021 11:03:49 AM
TCLPBadurn(Ba)
Nl]
5.K
"&
1
1 M Si2021 11:03:49 AM
TCLPCadmium(Cd)
ND
(}.1DO
mgiL
1
1MW202111;03.49AM
TCLP Chram1um(C;�
ND
6.20a
mgiL
1
111 Si2021 11:03:49 AM
TCLP Lead(Pb)
NB
0.500
mg1L
1
1i1812021 11;03:49 AM
TCLP SeleNum(Sa)
ND
0.0500
mg1L
1
Ill 812021 11.,03:49 AM
TCLP Silver(Ag)
NO
0.500
mnll,
1
V1812021 11:d3;49 AM
TCLP METALS, VOC, DNA, PEST, HERB -SOLID
SW8270
SW3510C Analyst: SFD
TCLP S EMI-VOLATI LES ANALYSIS (SW131118270)
1,4-01chlorobenzene
Na
0.200
mg&
2
Ill 512 D21 6:30: 00 ?M
2,4,5-TrlChlcrophenol
NO
0500
rng1L
2
111512D21 6:30:00 PM
2,4.6-Trichlmphenol
NO
0.500
mgiL
2
Vi5120216:30:00 PM
2,4-Din0otoluene
NO
0.100
mg1L.
2
111512021 6,30:00 PM
Cresols, Total
ND
10-0
mgiL
2
ill5120215:30:00 FIM
Hexachloro-15-buladlene
ND
0.0400
mg&
2
111512021 0,10,DO PM
Hexachlorobenzene
NO
0.100
mgiL
2
1f1512021 619010 PPA
Hmachloroethane
ND
0.200
mg1L
2
1115120216:30:00 PM
Nitrobenzene
ND
0.200
mgk
2
1 ill &20216:30:00 PM
Peniachlarophenal
ND
0.500
mgiL
2
11192021 6:30:00 PM
Pyridine
ND
0-SDO
mgiL
2
Ill5f2021 6:30:00 PM
Slur: 2-Pluaraphenoi
72.6
10 - 157 m
%Rec
2
1115/2021 610:00 PM
5urc Phenokc!6
75.4
10 - 189
%Rec
2
1i1512021 6,30:04 PM
5urr: Nitrobenzene-d5
81.7
32.1 - 130
%Rec
2
IllW2021 6;30:OD PM
Sum 2,4,6-Tf vomophenol
95.3
45.4 - 100
%Rec
2
1115/2021 6,30:00 PM
Sum 2-Fluarobiphenyl
79.1
35.7 - 130
%Rec
2
1115=21 6:30,00 PM
Serf: p-Terphenyl-d 14
120
74.7 - 145
%Rec
2
111512021 a:30:00 PM
Quallfiers: 6
Analyte detecled in the associaled Method Blank
6
Value above quaniitatiun,ungc
H
Holding times for preparation orarmlysitrcxceeded
M
Manual intcgreiionused lodelemrinc urea response
MC
Valm is tielow Minimum Compound Limit.
N
-1-matively idemified cnmPortnds
ND
Not Detected
P
Stcaiwl column confirmation ==Ms
PL
Permit t,imh
R
RP[] outside accepted recovery Iiinirs Original
KL
Iteparling Dctccuun Limit
U
Samples wrilli CalcYal < MDL
Page 6 of 36

��,�_ Snrurrllr Ertritarrj��e,a1a1 Tecl+r�vragres. {rrc,
33101vin 5r.
EP1VACNMeNTAL=Hmal..o ms.iw CrqWoogtrfafhs Obw44223
Ilnalytreattaborararres 70(330) 233-3ai1 FAX- 030)-M-44as
WaRvile: kno.lfn,brr "irek.cam
CLIENT:
Synagro
matrix:
SLUDGE
Lab CD:
21010279-001A
Project:
Pittsboro WWTP
Client SampLe I Pittsboro W WTP TCLP
Analy5f5
Analytical Report
(bast report)
WON: 2010279
10279
Dale ReporleLL 1{2512021
Tag Number;
C'nll�vtign Dare- 41412021 10:10:00 All+{
Result RI. Qual tlttitw D
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SVV1311=01)
Chlordane, totat
ND
Texaphene
ND
Endrin
Na
gamma-DIC
ND
Heptachlor
ND
Heptachlor epoxide
Na
Melhoxychlor
NI7
Sum TCMX
68.3
Surr: DCB
83.8
TCLP HERBICIDES BY EPA 8321E
2.4-D ND
2.4,54P ND
Surr 2,4-1}ichlatvphenylacelic aci Ice
TCLP METALS, VOC, RNA, PEST, HERB -SOLID
TCLP VOLATIL♦=S ANALYSIS
1,1-Qichloroethene
ND
1,2-Dichlowethane
ND
MEK
ND
Renaene
ND
Carbon letrachlarlde
ND
Chlarobenzene
ND
Chloroform
ND
Telrachloroelhene
ND
Triehlamihene
ND
Vinyl chloride
ND
Surr; 4-13ramo#luambe:nzana
68.5
Stirr: ❑Ibrnmptlummelhane
103
Sum- Toluene d8
102
Date Analyzed
SW8061 SVV3510C Analyst CSS
0.0250
m9il.
1
111912021 1:19.00 PM
0.0500
mgiL
1
111912421 1.16-60 P.M
0.00250
mgrL
1
1YIW2021 1-.18:00 PM
4-00250
mg1L
1
10 900211,18,00 PM
0.00250
QC+ mgrL
1
111 WN21 1:18:00 PM
0.00250
mg1L
1
IM9120211:18:00PM
0,00250
QC+ mglk
1
V1512021 VI&D0 PM
10 - 111a
%Rec
1
1)1912021 1:15;00 PM
10 -118
%Rec
1
11TW2021 1:18:00 PM
SW8321 SW1311 M Analyst: JPG
0,500 mg(L 50 112V2021 7:09:00 PM
4.5i}0 mgrL 30 1r2212021 7:06:00 PM
70 -130 %Rec 50 1=12021 7:08:00 PM
SVV8280 SW13111111 Analyst: SL,V
0.254
rrlglL
54
111W2D21 2:50:00 PM
0.250
mgrL
50
111812021 2-.60:00 PM
5.00
mg1L
50
1118(2021 2,50:00 PM
0-250
mgrL
5fl
1I18I2021 2.50.00 PM
0.250
mg1L
50
11IM021 2:50:00 PM
2.50
mglL
Sa
1IIW021 2,50,0) PM
0.250
r11gIL
50
1I1&2021 2:59:00 PM
0.250
mglL
50
111812021 2:50,DO PM
0.250
mg)L
50
liIW2021 2:50:00 PM
0.100
mg&
50
117812021 2:50:00 PM
70 - 130
%Rec
50
1/1812021 2:50:00 PM
70 - 130
%Rec
56
111BIZO21 2:50:00 PM
70 - 130
%Rec
5o
1M&2021 2:60:00 PM
Qnalifivrs: 13 ArmlyM detecled in the assaciaied Mathnd RIan Ir
H Holding times Far preparation or analysis. cxDccdcd
MC Value is bclmv t~+ilnimum Compound Limit.
NO NaL Detected
PE. Permit Limit
RL Reporting Detection Limit
E Vakm above quantitation range
M Manual InttWinion Used to dclenainc area rc3ponm
N Ttkltatively idenlificd compowids
P Second column r-DOLrmalian exceeds
R RPDotalsidoacceptedrecoverylilnils Original
U Samples with ClskVal <MDL
Page 7 of 36

5rwrndf Evvirrrrrrrreirfal Technairrgies, krc. Analytical Report
summlir 3310 if"M Sr.
ENvMONME46MAL 7MINOl{ MF3, rNC Clcmhoga Polls. 067 44.03 (hagC rt Ixsrtl
AmldyffcalLaboralvrW 7JiL: (3301 251.821i FAX. [phone] WO#: 2100279
FV*&o�v ❑alu Reporled: 11217421
CLIENT;
Syna$ra
Mrltrk:
SLUDGE
Lab ID:
21010279-091 A
Project:
Pittsbora WWTP
Client Sample ID Pittsboro W WTP TCLP
Tag ]Number:
Collection Date: 1!6l2021 10:30:00 AM
Analyses, Result
RL QuAl units DF
Date Analyzed
RCI
SW9014
Analyst JAP
REACTIVE CYANIDE (901417,3.3.2)-SOLID
Cyanide, ReaetNe NC-)
0.840 mg)Kg 1
111912021 11:15:00 AM
IGNiTAGILITY OF SOLIDS (SW.a46: 1030)
SW1030
Analyst: SEE
IgnilablMy nonflammable
mrmisec 1
111312G21 11:15:56 AM
IiCI
SW90450
Analyst: DHC
PH (SW3046D)
PH 6A
s.tu.Q19.2C 1
116/2021 11MG4 00 AM
RCI
SW9054
Analyst; JAP
REACTIVE SULFIDE (9034)17.3,4.2
Sulfide, Reactive ND
25.0 mglKg 1
1119M21
Qnatlifrers: B
Amlyle detected In the ascucialed Method Blank
11
Holding limes for preparation orallalysiscxceedcd
MC
Valuc isbclowMinknum Compound I.hnit.
ND
Not ❑otecled
lIL
Perntit 1 imir
RL
Repotting Detooiw Limit
E VAlue abowc quantitation range
M ]Manual lnlegraMn Used tD deteviiine Dma reswise
N Tcntadvely identified compounds
P Smund colunm conf rnlalioA er curls
R RPD outside ameplcd recovery lnnits Original
U Samples with CaloVal � MD1_
Page 8 of 36

startharFolwommwirar Wwnkgkx, hw,
Accreditation Program
' 11-
331f11F'i,�Sr.
Anal fes Report
ENIVII0111AENTlyILUCHNO) OCIFS.1kC
Cu}whUgaa!SUMM'4ifN,Qilk.?44223
AnMyGeal taboralunfis
TEL: [phone] FAX: [phone]
w0 is 21111OZ79
ffebarra:lrr Iltnr ..ra? cnrrr
2_'�Jrr11-21
Client:
Synagm
State: NW
Project.-
Pittsboro WWTP
1'ragram NAme: NC_WW—SCM
saul,ple 11) Matrix
'rest Nome
AmIlp•tr
Status
21010279-001A Sludge
IgnirnhilityofSol ids{SW 946: ID30)
Igr:itabiliry
A
Sludge
pE (SW9045D)
Hydrogai Ion (PH)
A
Sluc*
RewiveCyanide(401417.3.3.2)-Sd[d
Cyanide, Rwiive
N
Sludge
RcactivcSuIfidc(9034y7.3.4.2
5ulfide,Reactive
IN
sludge
'I CLP Herbicides by EPA 8321 B
2,4,5-TP
A
sludge
TCLP Herbicides by EPA 02113
2,4-D
A
sludge
TCLP Mercury Analysis (S W 1311f7470)
Mercury
A
sludge
TCLP Metals Anatysis(SW1311/6010)
Amenit
A
sludge
TCLP MCIAS Aralysis (S W 131116010)
Barium
A
sludge
TCLPMcWsAnalysis(5Wt311161)10)
Cadmium
A
Sludge
TCLP MatalsAmlysis(SW1311fb010)
Cltrurriiurrl
A
Sludge
'IrLP Metals Analysis (SW131 116010)
Lead
A
Sludge
TCIY Metal Analysis (SW I31 11601U)
Selimium
A
$1odgle
TCLP Metals Analysis (SW 131116010)
Silver
A
Sludge
TCLP Rem icides Analysis (SIN 1311l8Q81)
Chlordane, IcW
A
Sludge
TCLP Pesticides Analysis(SW131118081)
Endrin
A
Sludge
TCLPPestinidt4Analysis (SW 131118081)
gamma-BlIC
A
Sludge
TCLF Pesticides Analysis (SW 1311 A08 13
Hcptwhlor
A
5hrdV
TCLP Pe5tioides Analysis (5W 13i If8081)
HeplAahlgr epoxide
A
Sludgc
TCLPPesticidesAnalysis (5W13111908 1)
McthoxyChlor
A
Sludge
TCLP I'eseiskips. Analysis(SW 1311(9081)
Toxaphcne
A
Sill*
TC"Serrri-VolalilesAna lysis(SW 131tNMI)
1,4-Dichlorohen7cnn
A
Sludge
TCLPSemi -Volaiiies Analysis {SW 131118270)
2,4,5-'frichlaroghcnol
A
Sludge
TCLP Seam-Volatiles Analysis (SW 131113270)
2,4,4-Trichlurophcnol
A
sludge
TCI.lsSem!-Volall Ics Aralysis (SW1311 IM)
2,4-❑initrotoluere
A
Sludge
TCLP Semi-Volatilcs Analysis (SW13111827D)
€ resols,1,ola1
A
Sludge
TCLPSemi-Volalilm,Analysis (SW1311r8270)
Flexauhlorcibcnzme
A
Sludge
'it LI'Semi-VolaSdcs AnairIs (SW131 11$270)
Hexachlomhutodicne
A
Sludge
TCLP Semi -VolatilesAnalysis (SW 111118270)
11a" hlaraelhaanr
A
Sludge
TCLP Semi-Valatilt Analysis (SW 131 5f8270)
hrilrobennne
A
Sludge
TCLP Semi -Vol ntiles Analysis (SW 131 I19270)
Pentachluruphenul
A
sludge
TCLPSemi-Volatil" Analysis(SW131119 274)
Pyridine
A
Key
Key
NC WW 5CM A Accredited
KC WW SCf1 N N4l Accrediled
0P11}illal #I
Page 9 of 36

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summlySunni! Enrironmenlal %'echn 1[s, Inc.
3310310 fVin SI.
ENVIRONMENTAL' ECHN0i_QQ1FS, Mr Cityahoga Falls, Ohio 44223 Sample Log -In Check List
Analytical Laboraforles DEL: [phone] FAX: [phone]
ftlebsile: hlryr//minj,.sellek.com
Client Name: SYN-NC-27028 Work Order Number: 21010279 RcptNo: 1
Logged by: Christina N. Jager
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
1/7/2021 10:15:00 AM
1/8/2021 9:49:01 AM
1/8/2021 12:42:20 PM
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ElNot Present El2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes W No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present W
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes d❑ No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑
7, Sample(s) in proper container(s)?
Yes
❑d
No ❑
8, Sufficient sample volume for indicated test(s)?
Yes
©
No ❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No ❑
10. Was preservative added to bottles?
Yes
❑
No W NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
❑d
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
0
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA
Person Notified: Date: r
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C I Condition I Seal Intact I Seal No Seal Date I Signed By
1 15.2 1 Goodl Not Present
Page 36 of 36

aceAnalytical 0
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Pittsboro WWTP
Lot Number:WA07005
Date Completed: 0 1 /26/2021
01/26/2021 5:04 PM
Approved and released by:
Project Manager II: Lucas Odom
pC
r , -�
AN
ANSI Nelbntl AttreEihUoa Baud
q'
A C C R E D I T E D
_wizzamn__
TESTINGLABONATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WA07005
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of these samples was 3 times the standard procedure amount per
PM's request. The LOQ has been adjusted accordingly.
TKN
Matrix prevented in -range sample testing mass. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:WA07005-001
Description: Pittsboro WWTP Matrix: Solid
Date Sampled:01/06/2021 % Solids: 4.77 01/07/2021 2316
Date Received:01107/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 01/07/2021 2316 AAB
78812
1 350.1
(Ammonia - N ) 350.1
25 01/08/2021 1100 DRD
78739
1
(Nitrate - N ) 9056A
1 01/08/2021 1943 AMR
79020
1
(Nitrite - N ) 9056A
1 01/08/2021 1943 AMR
79022
2
(Phosphorus) 365.1
25 01/18/2021 1835 DMA
01/13/2021 2032 79352
1
(Soil pH meas) 9045D
1 01/08/2021 2219 AAB
78948
2 351.4
(TKN) 351.2
5 01/21/2021 1229 DMA
01/19/2021 1952 79979
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4.77
%
1
Ammonia - N (gas diffusion)
350.1
14000
520
270
mg/kg
1
Nitrate - N (soluble)
9056A
25
10
2.1
mg/kg
1
Nitrite - N (soluble)
9056A
ND
4.2
2.1
mg/kg
1
Phosphorus
7723-14-0 365.1
22000
2600
520
mg/kg
2
Soil pH measured in water @ 18 ° C
9045D
6.9
su
1
TKN
351.2
74000
2600
2600
mg/kg
2
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 01/13/2021 1451 JAB2
01/13/2021 0455 79069
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
2.0
1.6
0.39
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 01/13/2021 1312 KSH2
01/12/2021 0520 78979
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
43000
130
50
mg/kg
1
Arsenic
7440-38-2 601OD
4.7 J
5.0
1.7
mg/kg
1
Cadmium
7440-43-9 601OD
ND
1.7
0.42
mg/kg
1
Calcium
7440-70-2 6010D
9600
1700
210
mg/kg
1
Chromium
7440-47-3 6010D
25
3.3
0.84
mg/kg
1
Copper
7440-50-8 6010D
150
3.3
1.5
mg/kg
1
Iron
7439-89-6 601OD
15000
33
15
mg/kg
1
Lead
7439-92-1 6010D
11
3.3
1.5
mg/kg
1
Magnesium
7439-95-4 6010D
3400
1700
210
mg/kg
1
Manganese
7439-96-5 6010D
860
5.0
2.0
mg/kg
1
Molybdenum
7439-98-7 6010D
3.9 J
13
3.3
mg/kg
1
Nickel
7440-02-0 6010D
20
13
3.5
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the
calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result
< LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WA07005-001
Description: Pittsboro WWTP Matrix: Solid
Date Sampled:01/06/2021 % Solids: 4.77 01/07/2021 2316
)ate Received:01/07/2021
ICP-AES
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst
601OD 1 01/13/2021 1312 KSH2
Prep Date Batch
01/12/2021 0520 78979
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 601OD
3000
1700
210
mg/kg
1
Selenium
7782-49-2 6010D
5.8 J
6.7
2.7
mg/kg
1
Sodium
7440-23-5 6010D
1600 J
1700
210
mg/kg
1
Zinc
7440-66-6 601OD
400
17
4.2
mg/kg
1
LOQ = Limit of Quanlitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
ed
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
[phone] Fax [phone] www.pacelabs.com
Page 6 of
70
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III

PACE ANALYTICAL SERVICES, LLC
Samples Receipt; Cheddist (SRQ (MEObit1C•15) kevised:9/29/2020
PaceAl+a+�ttcw�f Issuing Authority: Pace CND' - WCOL jape i at 1
Sample Receipt: Checklist (SRC)
client: SYNA4Rt3 Coole4.111st.,eeted by;+dot(,: KSG 1 OV0712021 Lut 8: WA07005
Means of receipt:
Yes ✓ No
Yes No
D face C;liew. ✓ Ul'S P'cdLx Other;
1. Mere.. custody seals present on the cooler?
vl N.4 2, l: custody seals were prossant, were Ilicy intact told unbroken?.
n1d Strip ID: 10, Chorine Strip ID: NA Tested by: NA
Original temperature, up(m receipt f Drrivtxl (C�.wm,,leti) tentpertrllirn ttptm receipt Mo1[d Simp-Cup ID: 20-973
2.7 42.7 ^C KA f NA °C NA /NA ftC NA (NA n[;
MGtho l; ❑Tt mpuntuce Cilart lc 04uainht Liulltet llt Gun ID: S tit (iun Correction i'etalor, 0 "(
Ialethod ofcoalal t: C Wet Ice El Ice Pacts © My Ice El None
kas
Na
�hlA
3. If tentpet,iztre of at:y cooler axceeded G OTC; t3s Eamit ct Ivtt nager Notified?
PM was i\otificd by: phone I cmad r fuce-to-face (circle one).
J Yes
=No
LJNA
4, is the commercial. courlcr's ecking slip attached to this fomt7
Yes
,+ Yes
t No
❑No
5, Were, proper custody procedures (relinquishedlreceived) follmved?
G. Were. raTT[e 1Ds listed on the COC?
J YestNo
r. Wcrc sample IDs listed on all sampe contziners?
Yea
8. Was collection date S. Liuta listed on thti cor,?
Yes
4. War. collection dear �k, time listed on a'.1 s,wipte container?
,/ Yes
10, Did all container label information (iD., (Mie, time) agree with the COC?
1 l . Were tests to Lie perrouned tilted an .lie COO
Yes
Yes
[ No
12. Dill all sampl4l mriytz in thu proper contninCrs for each tact arc or in good condition
(unbroken, lids on; etc.)"
Y-;s
No
13. Was ad1tviatt VAmp"O voluntl' nyailablO
14, Wore till sntttples received within!/2 the lioldir gtime or 48 hours, whichcvcrcomcs first?
J YCs
Nei
Yes
No
15. Were, any samples, 'onluincrs missingf"ccss (circle ona) stunples Not listed gn COC?
Yes
[:]No
DNA
lei, For VDA and RSK-175 samples, were bi,bbIcs prescnt f"lea-size" ('ii"n: fimin in ilitsmcter)
m any of the VOA vials?
Yo
No
WNA
IT Wvry till DKOfmcta[s'nutricntsartt lcs received at a P11 of< ? ,...
Yes
No
1tJNA
18. Wctc till cyanide: sampIcs received at a PH > 12 and Su fido Samples receivers at a old > 9?
® Yes
❑No
�iVA
1% NVort all app tea a NH3,1'Klr. cyanide+tt;renolfb� , ltfit?$.; {- t),;n:gj),} samp'.es free o
Imidual chlorine?
® Yes
❑ No
E]NA
"_ �tiere client (ix, ruqucsted dilutions, WFOO,U) desip,,lntlops, etc...}
correctly trnnscr3b A tro n the COC into the crnnnient section in i M)'IS?
Yes
d N0
21_ Wtis the yiott: numh(-r li icd on the container label? If $S, UotC (F NA
8nniple Preservalion (Muse baGUtttpIotgd fortmy sample(&) iticorrectty pregervcd of with hcadslxice.)
SattMple(s) :A _ ?verc received inc6i'mal} ln'eserved aarl wrm ttdjtlstcd accoMina
ir. Sample receiving with NA niL o6ckele one:1.12SQ4, I-INO3, HCI, NuOI•I using.SR of MA
Time: of pmervatioc NA _. If more. Yhait otie pmst;rvulivc is n4cded, phase note in the commo.ji I'Sbelow
Samples) NA
were ttccived with bubbles'-,b nim in diameter,
Samples(s) lei weer rmcivc d with 1 ItC -, 0.5 mg/L. ([17919 is no) and were
;Adjusted accordingly in sanmpIc mcciving with sodium thiosolfate (NR;SyO;) w'th Shealy 1D., NA
SR barcode latze.s applied by; KSCavlmi Clata: OIA17r7.0.t '
Coot mcnts:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Cameron Testing Services, Inc. Laboratory Report
2101-032 -01
-02
-03
-04
-05
-06
-07
2101-032
-01
-02
-03
-04
-05
-06
-07
3ludot Gr Fee. Coliform-S
Geomean
Bludge CA TS M
NC DENR #654
NC PHHS #37799
US EPA #NC01 918
2101-032 DW Cent # 37799
Yes
J. Cameron 01106/21
75500
cruto
18900 01/06121 RL
76700
uuig
19200
56800
GFUIO
18900
95300
GFUtg
19100
37900
crft
19000
225000
CFWa
18700
134000
CM9
19100
86400
5,30%
0,01 01106121 RL
5,21%
O.Oi
6.28%
O'Ot
5,25%
0.01
5.27%
601
5,33%
0,01
6,23%
001
Report
Review OLO
Project limajo Date
9222D - MF
2540 G -TS
219 S. Stcele Str, 919.209-4240'
SanfoM NC 27330 CMQft4Mier4jPtcsling,wm

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