NCS000509_MONITORING INFO_20180301

--------STORMWATER"DIVISION-CODING-SHEET- -
PERMIT NO.
NCS ©w 5 D9
DOC TYPE
❑ FINAL PERMIT
MONITORING INFO
APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
03 D�
YYYYM M D D

Permit Number NCS 000509
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACMITYNAME TriEstAoGroup Inc Greenville NC RECEIVED
PERSON COLLECTING SAMPLE(S) Ipff From
CERTIFIED LABORATORY(S) Test America LabA
Lab �j A �/ A A 2018
CENTRAL FILES
Part A: Specific Monitoring Requirements DWR SECTION
COUNTY Pitt
PHONE NO. (800 1 637-9466
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
RainfallS
Solids
CO Demand
Oil & Grease
Hexane
Methyl Bromide
Chloropicrin
mo/dd/ r
MG
inches
m /L
m /L
m /L
m /L
u /L
u /L
N-001
12/20/17
0.25
17
75
3.9
ND
ND
ND
N-002
1 0/17
0.25
80
170
4
ND
ND
NO
N-003
12/20/17
0.25
150
150
8.9
ND
ND
ND
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes `� no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitorina Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
unit
al/mo
Form SWU-247-062310
Page I of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000509
FACILITY NAME TriEst Ag,Group, Inc Greenville NC
PERSON COLLECTING SAMPLE(S) .iaff From
CERTIFIED LABORATORY(S) Test America Lab #
Lab #
Part A: Speck Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Pitt
PHONE NO. Ciloo 637-9466
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the (rest of my knowledge.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow ff a
Total
Rainfall
odium Methyidithio
Formaldehyde
Nitrate + Nitrite - N
Total Phosphorus
pH
mo/dd/ r
MG
inches
u /L
m /L
m /L
m /L
Standard Units
N-001
12/20/17
0.25
ND
0.038
0.46
0.12
6.8
N-002
12120117
0.25
ND
0.11
1.6
0.24
7.3
N-003
12/20/17
0.25
ND
0.05
0.67
0.31
7.9
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes ',no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitorine Requirements
Outfau
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/PPH
(Method 1664
SGT-HEM), if
a 1.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
unit
aVmo
Form SWU-247-062310
Page I of 2

"
.
_
, � �.
.r
..

AA
STORM EVENT CHARACTERISTICS:
Date 12/20/17
Total Event Precipitation (inches): 0.25
Event Duration (hours): .75 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(� k / / 2/18/18
(Signature of Permit ) (Date)
Form SWU-247-062310
Page 2 of 2

I

Ricky L. Keck
Manager, Environmental, Health & Safety -
THEstt"
Ag Group; ,Inc.
F.ebruary'22, 2618
CERTIFIED MAIL -RETURN RECEIPT REQUESTED
Division of Water Quality .
Attn: Central Files
CORPORATE OFFICE 1617 Mail Service Center .
Raleigh, NC 27699-1617
P.O. Box 448 -
Greenville, NC 27835 - - -
252.758.4263 - -
800.637.9466-
•f 252.758.2767 RE: STORMWATER DISCHARGE OUTFALL"(SDO) MONITORING; _
REPORT.
REGIONAL OFFICES"
To Whom It May Concern:
3500 NC Highway 133
.Rocky Point. NC 28457 Enclosed is the SDO for the. second semester 2017 for our Greenville facility.
910.675.9409 There were two slight exceedances ofTSS and COD at Outfalls N-002 and 003. '
800.533.9789 - - .
f 9i0.6o23106 We are conducting;additional sampling to'determine if this was.an anomaly.
We are 'still awaiting the new SW Permit and were wondering when it might be
P.O. Box 965
Tifton, GA 31793 available.
229.382.7272.-
800.872.0644 Should you require further information' regarding this submittal please.do not
f 2D.382.9375. hesitate ,to contact me at [phone].
.7610 US HWY 41-N Sincerely, -
Palmetto, FL 34221 - - - -
941.722.5587 -
800 726.5215.
CVKe_ck,04310 National Guard Drive.
e -
Plant City, FL 33563 Mgr., Environmental; Health &Safety
813.752.4244 -
800.832.5982' -
f 813.754.8095
- RLK: 06-18
www.TriEstAg.com enc.
cc: File
,

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000509 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME TriEst Ag Group, Inc Greenville NC REC IVED COUNTY Pitt
PERSON COLLECTING SAMPLE(S) .toff From CFp 2 5 2� �% PHONE NO. ( Bn0 1 637-9466
CERTIFIED LABORATORY(S) Test America Lab #
Lab # Cr=h rrrRAL FILES (SIGNATURE OF PERMITTEE OR DESIGNEE)
DWR SECTION By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
S Solids
CO Demand
Oil & Grease
Hexane
Methyl Bromide
Chloropicrin
mo/dd/ r
MG
inches
m /L
m /L
m /L
m /L
u /L
u /L
N-001
6/5/17
0.3
7
31
1.9
ND
ND
ND
N-002
I117
0.3
18
54
ND
ND
ND
ND
N-003
6/5/17
0.3
21
82
2.1
ND
ND
ND
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes `( no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
unit
al/mo
Form SWU-247-062310
Page 1 of 2

I

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000509
FACILITY NAME TdEst Ag Group. Inc. Greenville, NC
PERSON COLLECTING SAMPLE(S) .Taff Frnm
CERTIFIED LABORATORY(S) Test America Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Pitt
PHONE NO. eoo 637-9466
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow(if a
Total
Rainfall
Sodium MethAdithio
Formaldehyde
Nitrate + Nitrite - N
Total Phosphorus
p H
mo/dd/ r
MG
inches
u /L
m /L
m /L
m /L
Standard Units
N-001
6/5/17
0.3
ND
0.081
0.31
ND
6.9
N-002
7
0.3
ND
0.083
0.35
0.05
7.4
N-003
6/5/17
0.3
0.015
0.088
0.38
0.047
6.9
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes *(no
(if yes, complete Par B)
Part B: Vehicle Maintenance Ac ivity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/IPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
unit
galtmo,
Form SWU-247-062310
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date 6/5/17
Total Event Precipitation (inches): 0.3
Event Duration (hours): 1.5 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility tTrncs-and imprisonment for knowing violations."
I9/18/17
(Signature of Permitt ) (Date)
Form SWU-247-062310
Page 2 of 2

' Ricky L. Keck -
'., , Manager, Environmental, Health & Safety - -
TriEstt"
Ag Group, Inc.
September 15, 2017
CERTIFIED MAIL -RETURN RECEIPT REQUESTED -
Division of Water Quality
Attn: Central Files
eORPORATE OFFICE 1617 Mail Service Center
P.O. Box 448
Raleigh, NC 27699-1617 � - �
Greenville, NC 27835 - -
252.758.4263 -
.. 800.637.9466
f 252.758.12767 RE: STORMWATER.DISCHARGE OUTFALL (SDO) MONITORING.;
REPORT %
REGIONAL OFFICES'
To Whom It May Concer-n;.. _
3500 NC Highway 133
Rocky Point, NC z8457 Enclosed is the SDO for the first semester 2017 for our Greenville facility. There
- 0..99
800.533533.978789 ' were no exceedances at.any of the three outfaIIS.
- .. _ -
f 910.602.3106 We are still, awaiting'the new SW.Permit and were wondering when'it might be
available..
.P.O. Box 965
Tifton, GA 31793 - -
229.382.7272 Should you require further information, regarding this submittal please do not
800.872.0644 : hesitate to contact me at [phone].
f 229382.9375 -
Sincerely,
761 O US HWY 41-N
Palmetto. FL 34221 -
941.722.5587 - -
.800.726.5215 ,
f 941.729.2814 - - -
RicRicK ck
4310 National Guard Drive
Mgr., Environmental, Health & Safety
. -
Plant City, FL.33563. - - -
813.752.4244
806.832.5982
f 813.754.8095 RLIC: 100-17
enc.':
www.Tr7EstAg.com _ -
cc: File
. CA

1-1
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000509
FACILITY NAME TriEst Ag Group, Inc. Greenville, NC
PERSON COLLECTING SAMPLE(S) .30 ,n g k-! c
CERTIFIEDLABORATORY(S) Test Amec%da Lab#�35
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 26 t y e
(This monitoring report shall be received by the Division no later than 30 a s from
the date the facility receives the sampling results from the laboratory.)
COUNTY Pitt
;i PHONE NO. (B00) 637-9468 rn
$ r' 7 r
( NAT F PERMITTEE OR D GNE )
y this signature, I certify that this report is accurate
complete to the best of my knowledge.
—►l Jt
I Ott
----------
----------
----------
----------
----------
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes `I no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
MAR 0 5 2015
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appi.)
Non -polar
O&G/fPH
(Method 16"
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New otOENR -
Oil U 401 8
mo/dd/ r
MG
inches
nWA
mgfl
unit
al/mo
Form SWU-247-062310
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Dale 12 1 M a y
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable - see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable - see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center i6iL
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
�t �7 z Fvr Ir,Gst Ag GrooLY01- Z4dsll5
( ature of P ittee) (Date)
d5a-759-1/a63
Form SWU-247-062310
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
V
Permit Number NCS 000509 SAMPLES COLLECTED DURING CALENDAR YEAR: V
(This monitoring report shall be received by the Division no later than 3 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME TriEst Ag Group Inc Greenv Ile. NC COUNTY Pitt
PERSON COLLECTING SAMPLE(S) John g i i io PHONE NO. aoo 637-9466
CERTIFIEDLABORATORY(S) TestAmer,ca Lab# 7 * fvr ine,TAgCWL.rf
Lab # (SIGNAL PURMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
odium Methyldithio
Formaldehyde
Nitrate + Nitrite - N
Total Phosphorus
pH
mo/dd/ r
MG
inches .
u /L
millL
m /L
m /L
Standard Units
N-001
t i V
0.4
N D
0. 029
N D
N D
7.51
N-002
i r
aj
tvD
NO
NO
0.035
, 54
N-003
0,U
N
01017
0.39
0.0837,30
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes `( no
(if yes, complete Part B)
Part B: Vehicle Maintenance Ac ivity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/PPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
m
unit
al/mo
Form SWU-247-062310
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date I2- 2`1 11 O,
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
-Fvr lnFSl G(ojp ,Inc. 2 i 's
r)lnature of P� nittee) (Date)
Form SWU-247-062310
Page 2 of 2

Fs* A,5
STORM WATER DISCHARGE INSPECTION / MONITORING / SAMPLING FORM
Greenville, NC Branch
Semi -Annual Inspections: I" Semester 2"d Semester
(Visual examination t Z 2! y
of the storm water Date
discharged from the
outfall)
Inspector's Initials
Stormwater Discharge OOutfall (SDO)
N-001 d" N-002 ❑ N-003 ❑
Criteria for Inspection: Obvious indicators of storm water pollution such as color, odor, clarity,
floating solids, suspended solids, foam, oil sheen, erosion or deposition at the outfall.
Directions for collecting sample: Samples shall be collected within the first 30 minutes (or as
soon thereafter as practical, but not to exceed one hour) of when the runoff begins discharging
from a storm event that is greater than 0.1 inches in magnitude. Samples may be collected in
clear glass jars (mason) for observation. No analysis is required.
If no rain occurs during a given semester, make note on this form below.
Make comments regarding the water quality below:
I" Semester
2"d Semester ccleac no CAD( -
Additional Comments: /I
d erm � OOSn �t

STORM WATER DISCHARGE INSPECTION / MONITORING / SAMPLING FORM
Greenville, NC Branch
Semi -Annual Inspections: I" Semester 2"d Semester
(Visual examination
of the storm water Date
discharged from the
outfall)
Inspector's Initials
Stormwater Discharge Outfall (SDO)
N-001 ❑ N-002 m/ N-003 ❑
Criteria for Inspection: Obvious indicators of storm water pollution such as color, odor, clarity,
floating solids, suspended solids, foam, oil sheen, erosion or deposition at the outfall.
Directions for collecting sample: Samples shall be collected within the first 30 minutes (or as
soon thereafter as practical, but not to exceed one hour) of when the runoff begins discharging
from a storm event that is greater than 0.1 inches in magnitude. Samples may be collected in
clear glass jars (mason) for observation. No analysis is required.
If no rain occurs during a given semester, make note on this form below.
Make comments regarding the water quality below:
I" Semester
2"d Semester clear' nu Uc�or
Additional Comments:
Part oosoi

STORM WATER DISCHARGE INSPECTION I MONITORING / SAMPLING FORM
Greenville, NC Branch
Semi -Annual Inspections:
(Visual examination
of the storm water
discharged from the
outfal l)
Ist Semester 2"d Semester
Stormwater Discharge Outfall (SDO)
12-24/c(
Date
Inspector's Initial
N-001 ❑ N-002 ❑ N-003 [R'
Criteria for Inspection: Obvious indicators of storm water pollution such as color, odor, clarity,
floating solids, suspended solids, foam, oil sheen, erosion or deposition at the outfall.
Directions for collecting sample: Samples shall be collected within the first 30 minutes (or as
soon thereafter as practical, but not to exceed one hour) of when the runoff begins discharging
from a storm event that is greater than 0.1 inches in magnitude. Samples may be collected in
clear glass jars (mason) for observation. No analysis is required.
If no rain occurs during a given semester, make note on this form below.
Make comments regarding the water quality below:
I" Semester
2"d Semester Clear, l o acloc,
Additional Comments:
91

RECEIVED
FEB 18 2014
STORMWATER DISCHARGE OUTFALL (SDO) CENTRAL FILE MONITORING REPORT
DWQ/BOG
Permit Number NCS>000509a SAMPLES COLLECTED DURING CALENDAR YEAR: 2014
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME TriEst Act Group Inc Greenville NC
PERSON COLLECTING SAMPLE(S) A I H ricnn
CERTIFIED LABORATORY(S) Test America Lab # E87358
Lab #
Part A: Specific Monitoring Requirements
COUNTY Pitt
PHONE NO. (_a00_) 637-9466
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow (if a.)
Total
Rainfall
S Solids
CO Demand
Oil & Grease
Hexane
Methyl Bromide
Chloropicrin
mo/dd/yr
MG
inches
m /L
m /L
m /L
m /L
u /L
u /L
N-001
1/14/2014
0.6
Not Detected
9.1
Not Detected
Not Detected
Not Detected
Not detected
N-002
1/14/2014
0.6
11
22
3.3
Not Detected
Not Detected
0.26
N-003
1/14/2014
0.6
Not Detected
27
Not Detected
Not Detected
Not Detected
Not Detected
M L.
, /L
lfn. Ntel Idt6�
m�p u L
O�mu®� e
!(Rol`<-+N,trtc-nl
lo'foL P (m /c
N-ool
ND
o,ogy
0-obli
6•ZS
N-0o
N0
NO2
00
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes 0, no
(if yes, complete Pan B)
Part B: Vehicle Maintenance Activity Monitorine Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
a 1.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
m
unit
al/mo
Form SWU-247-062310
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date i 4 1
Total Event Precipitation (inches): 0• (D
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
/ / ' / 6 {ur Tiu�o't` Q 5 mitt-, 2
(Signs of Permttt (Date)
Form SWU-247-062310
Page 2 of 2

ARA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Mr. Ricky L. Keck
I lendrix and Dail, Inc.
POI3 648
Greenville, North Carolina 27835
Dear Mr. Keck:
William G. Ross, Jr., Secretary
Alan W. Klimek, P.E., Director
RECEIVED
August 6, 2004 AUG 13 2004
DWQ-WARD
Subject: NPDES General Permit Application
Application Number NCS000509
Individual Stormwater Permit
Pitt County
The Division of Water Quality's Stormwater Permitting Unit hereby acknowledges receipt of your application for an
NPDES individual stormwater discharge permit on July 23, 2004. Your submittal has been assigned the application
number shown above.
The submitted package contained EPA Form I General, EPA Form 2F NPDES, a site plan, laboratory analytical
results of stormwater sampling, and the application processing fee.
Please be aware that the Division's Washington Regional Office, copied below, will be asked to comment on the
draft permit prior to final action by the Division.
You should be aware that the review process generally takes 90 days from the date your complete submittal is
received. This 90-day process may be extended if additional information is required.
If you have any questions, please contact me at [phone], extension 584
Sincere y,
Ken Pickle
Permit Writer
cc: Washington Regional Office
Stormwater Permitting Unit
Central Files
1617 Mail Service Center, Raleigh, North Carolina 27699.1617 T�iOne 7., 1
512 N. Salisbury St., Raleigh, North Carolina 27604 1 � orth Carolina.
Phone: [phone]/ FAX: [phone] / Internet: h2o.enr.state.nc.us
An Equal Opportunity/Affirmative Action Employer- 50 % Recycled/10% Post Consumer Paper Naturally

HENDRIX AND DAIL, INC.
CORPORATE OFFICE
HENDRIX AND DAIL, INC.
P.O. BOX 648
GREENVILLE, NC 27835
800-637-9466
HOLLISTER OFFICE
P.O. BOX 1327
HOLLISTER, CA 95024
408-637-0195
TIFTON OFFICE
P.O. BOX 965
TIFTON, GA31793
800-872-0644
FRANKFORT OFFICE
2150 COMMERCIAL DR.
FRANKFORT, KY40601
800-999-1262
PALMETTO OFFICE
7610 US HWY 41 NORTH
PALMETTO, FL 34221 .
800-726-5215
Ricky L Keck .,.....,,:,,,..,::..:,n..—i•.
Manager, Environmental, Health & Safety-
CF_RTIFIED AL41L-RETURN RECEIPT
July 19, 2004
D
JUL 2 3 2004
NCDENR OEi;R - W41ER OUALIC
POIHT SOURCE BRANCH
SW & General Permits Unit
1617 Mail Service Center "
Raleigh, NC 27699-1617 1.-11- " ..
RE: NOI FOR STORMWATER DISCHARGES
To Whom It May Concern:
I have enclosed the EPA Form I General and Form 2F NPDES for our facility
located at 1101 Industrial Blvd.', in Greenville. I have also included a recent
stormwater analysis of our SW discharge and a check in the amount of $715.00
to cover the application cost.
Should you require further information regarding this submittal please do not
hesitate to contact me at [phone].
Sincerely,
&KL)
Ricky L. Keck,
Mgr., Environmental, Health & Safety
RLK:51/04
enc.
cc: File

Inn-rn areas are Wecea - - -- - -
'us. ENVIRowM ewrwL PworecnpN we ENcv -. ',
REVERSE
1• 9PA I.D. NUMBER
FORM
GENERAL INFORMATION
v p Consolidated Pcrmitt Program
1 as��/�
F�
GENERAL INSTRUCTIONS ,
GENERAL (Read the -General 7nstructioni'
before Yarn e 1
LABEL
if a preprinnad:.label,has been provided, affix`
1. EPA I.D. NUM R \ -
-
itin the designated space. Review the inform-i;
ation carefully: if any of it is Incorrect, cross.`
Ill- FACILITY NAME
through it and enter the cprrect data in the
appropriate fill=in area below. Also, if any of.
\
the preprinted data is absent (the area to the,'
FACILITY -
V.
- -
left of the tabor space lists the information
that should appeed.'please provide it in the.
MAILING ADDRESS\�\PLEASE PLACE LABEL IN
THIS SPACE'
proper filltirr area(s/.:below. If the label .is.
complete and correct, you need not Complete.',
,.�
\
Items 1, III; V, and .VI !except VI-B which
;
\
must be completed .rGgarrll¢ssl. Complete, all
FACTl�ITYoN
.V 1.
items if not label has.been provided. Refer tq,,,
the instructions for detailed : item. doscnp-."
wcAn
:bons and for -ihe legal:. authorizations .antler'
which thisdata s; collected. :>:.,
It. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit: application forma to the EPA. If you answer 'yes" to any
submit this form and the supplemental form listed in the
parenthesis following the question. Mark "W'.. in the box jn the third column
questions, you must
if the supplemental form is attached. if you answer "no",to-eafh iiuestion, you need not suhmit any of -these forms. You may answer 7no (f your acti6ity
Section C the.itti ructions. Sea alto,
Section Bill the instructions for definitions`of bold faced terms.
is excluded from permit requirements; we of
h,
A,-M .
SPECIFIC QUESTIONSsis
.'aPECIPIC-OU ESTIONS y
e^cwen
A. 'Is this fadnty a publicly owned 'treatment. world
E. Does cewill This facility fe/drer existing or proposed),-
.''include o'eonce tratadaldlnal feeding oparetlon`or.:
x
'which results in a discharge to waters of.the U.S.?
x
..;aquatic animal production facility which results W, e
(FORM 2A) .' .. ...
•
' dischargeas to watof the U.S.? I FORM 28)
,.
C. Is this o aedrty w ¢ current y rasa is m, Ise aryes
to of the U.S. other than' those oeunbed in
X"In
s t n a pmpq _ cl Ity of er an more described
A ar Ba(sdml which will rewlt cob d-edwrga to-:..
x'
A waters
or auovez FORM 2C)
wate.eeif thisU 7 (FORM 2D)
'�
F. Do you oi:wiif-you infect at this facility _)ndustrml or:
E. Does or will this facility treat, store, or dispose of
X
- municipal effluent below the lowermost stratum con -
hazardous wastes? (FORM3)
taming, wfthi,n one ::quarter. mile of.tha-well rare_:
..
underprpurid,iources'ofdrinkingwater➢tFORM41
'
,.
o you or wi you inject at this aal ry any p ace
H. Do you or w1U you injeiT at thli Iac11Ry tlulds for spa-',
water or other fluids which are brought to the surface
natural
'C1a1 P 1zKlt mining of zulfur Gy'the Ftasch,
'
'
in connection with conventional oil or gas. Pro--
x
;,<ar.�� solptipn miftng'6( minerals Insttd eorlbus
duction, inject fluids used for enhanced recovery of,
tlpn of fosstl7uel or,racovlry of gwthermel anerg`yT
-oil or natural ,gas,'or, inject fluids to storage of liquid
teDRMal.u� aM„'
S t Is acI ry vprdpoted statntrlaty source which R
Is t n 80 Ity a pr statronety fO1ItCa Whit n'.
the '18 wteporks{istedhl Fhe :
one or the 28 industrial otegorm tlstad In the .n,-;
structions and Whlch',Win; potentially :emitx100 tons.
X
tJOT,.orw of Itlduftrul
<^,?instrucuons -ell,E<which Rnll IxnsntRlly �tnlht 250 tolrs ..
4
/`
.
Ypar year -of;.any a r;pollutant regulated underc-ha
t per y®r of Bny gV pol(utant rLqula[ed under the Cl rtz
-Clean Air -Ace and kiay"affect or 6e brat d to an-
r..Alr Aet arld,fisv eNee�br 6e Coated (n'i attain nt
`<?%�aa7'{FDTi ;51: zi `_-!Y`Y.+ `i.�-+Y: `s.KIO-'�
.,:bttainmentarae? IF6RM'51 V 1'.•.+,�'T."XI.* :.
aN.a
e _
_ I. x,_
-�.-.
.III: NAME OF FACICITV
-t>A�
SNIP �fJ•DRI�C AtJ t7 tiIz-
k.�i11+
IV. FACILITY CONTACT' ~
• .1 •. '.. A.'H AME'Q TITLE (IN}..'/rear a(f t%1.
_ 11r.8 PHONE Iaredcnrte d o ;;yy r
•'(•1 S +
o
z R� Cr 1� Kam= c yc i✓ ti S ,AAtJA C>E
2 g 0
V. FACILITY MAILING ADDRESS
A. STREET OR P.O. BOX!`,%-
s O }3
B. CITY OR TOWN
QSTATE O•ZIP CODE
VL FACILITY LOCATION
A. STREET. ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
5
a. ccUNTY NAME
S
•'
C. CITY OR TOWN r: -N -.}ti�� `.
9
LTATE
^•
:! ,Xle coo E?
r. COUNTY O
; tg A
//'•]a
Z. % O ,J 'l
1•
r%�y,�g�
t)
EPA Form 3510-1 (8-90) ^ , rt ZA o U
�1 t5r60
CONTINUE ON
V I. 6. l-

VNI Iry UC r"UNI ITI
VII. SIC CODES (d-digit.'in order of priority) '
A. FIRST
q (tDeeill'I '7
(Specify)AG
C.�%
C.HEt-4.( f.faLs
" G. TNIRO � � �D. FOURTH
ltpecifly (Specify/
7
Vill`OPERATOR INFORMATION
A.NAME_ t ':. e... •, •.. ,.: ... ., ."
B. Is the llama listed it,
'. heal V I I I -A else, the
8
N � c-� UR�x A� � n �Ai � (t � L
OWMf7', .'. ..'T'- u
YES O NO'
.. _ .. ...
Ea ..
C. STMTVS OF OPERATOR (Enter the appropriate left,, i"10 the answer ilOJ: IJ .mtilrr", Specify.
a (oN'a I.de
'...;:
FEDERAL PUBLIC (other than federal or stare)
P
ltpecifl'i
`
A
8do
ty3%
S STATE - ...' O• OTHER(weeffyl
a
_ •.z�
'.P •PRIVATE
N
u - ,•
' 1 : "'-[. STREET OR P.O. BOX
.. F.'CITY OR TOWN - - "`G.STAT
NI zwcooei1XANDIAN-LAND
U the lac,tny Ioested on Indian Iandsr
s.
GR E-F' `IC:
N
Z7 g 3 AYES NO 0.t
Ella
l Sr }.,'.. ly'.1l�
.:a
X. EXISTING ENVIRONMENTAL PERMITS
" A.'NPOES (DUchaeges to Surface Water)
D. PSO (Air EnliAions from Prtir)vwd Source) 'sib
'•
a. Ule (Underground Injection of.Fluidl)
- "E: OTNER.(speeify)
(specify)
G. RGRA (Hazardous WESfesf
- E:OTHER (rp[fifv/ T ` - n%
e (rpeuifr) -
9
R
9
X1. MAP
Attach tO this`ippltcaiiori.a topogriPhic map Di the area extending to at least one mile beyond property Italod�rles The (napinu `;hi.
'tlI•e OUt11ne of .the-faahtythe Iocatlai of eachyofits lexlstingatM proposed Intake and/dlsdlargstructtlrps eadi of Its tlaar�ousjwa
treatment storage tqr disposal facihtles arW teach 4✓e{I where it tn)eets ftuitk tmdercp"` h, and a all rings inters artd-d lie wryiLa`c
water bodiesin. thefnlaparea See lnstructl0[IetOr,pecls�requlrementa
XII::NATUREOr• U$INES rpm--.41irt/dfrtRP lion
ezl+\ k-DE.5 -Fc7R CDt�rAP2C�A� APPLt�1tDr�
XIII. CERTIFICATION Tree fnrtruedons)-
I certify under penalty of law that 1 have persona/ty examined and amYamiliar'with the intormatrori submitted m thrs epp/rcauon an`d aft
attachments and that'based on my inquiry of'those persons immediately rasporislble, foiobtainirg 6& infomraation'coniained in the, '
application, I believe that the information is true, accurate and comp/eta. I am aware that there are slgnificarYtpenalties fwsubmftt+ng "
false information, including the possibility of fine and imprisonment.
A. NAME 6 OFFICIALTITLE,(typeorprintf
EI-S7
URE GDATE SIGNED
Ricky .ke-je- E Ns NfaN�>✓ro
COMMENTS FOR OFFICIAL USE ONLY.
1w 9;P
j
EPA Form 3510.1 (8-90)

EPA 0 Neff leer . PVV ftM Allen i of Form 1) FaM Approved. OMB No. 2040.OM
Pke aiMIer tune in the unshaded areas ordv - Approval axplres "192
Fenn
N DM
YyeGdrgtoa, DO2D460 �� .
EPA Application
q {rater
saharces Associated with Industrial Activity
Paperwork Paduollon Act Notice
PAft roportLq burden for tide appBallm Isestimated SoamnW MA hours pardon, Including tiro for rsvbwkhg Inffiucti
Ui�ons
Saud .GXWnp damea seamen, g"IV and rrlakhteer ining the data needed, uct am'reidawig }he coiIectia In at Mrmation:
... cnnrrhente roDemanD tlo, burden.aatkrha0a, ahoy other eager; a this Ddlectonh a khlonifetbru, « ealiens for improving thisform, including .
suggestion kh may Inrneaea or reduce this burden to: Chief, Monnatbn Policy Branch; PMea U.& Environmental Protection jancy, 401
-` IL!KYVatlllrom. DC2D4W or Director, Ottoe of I bmuffi n aria Regub+M MUFO: Otis of Management and Budget Mahington, DC
I.
Fa each oultall, listihe lot hide and lowltude of Ite lobetorh tdtmrAoffidisthe AMM of the raaiN
A. Outf a lhrmber
00
B. Latitude
C. Lawfulde
D. Receiving Water .
name
v
1?
7-1
O
C>R _ 5WAMP CAOP,l—
tj0Z
3
3
- -)
O
7
N- 003
3S
is
-�
zo
Z.
II.lm rovemerft
A Are you now required by arty Federal Sate, or local authority to meat any ImpbrnmaatWn schedule for In consbuctlon, upgmdinp «
operation a wastewater trsetrnerd equpmeM «q�to� or rely other amlronmeMel prop which zany afloat the diedmrges desertbed
In Ads appeoatorh7 This Indudes, but Is not I rna to, penMt condition, admtnbtratlw traMorcemaM orders, enforcement oanpliena
schedule letters, sdpuletloro, curt orders, and grant ban aondMes
1. IdemiBaton of Cowildo o.
-Agree Re. -
2. Affected OuNeTh
3. Brist pesompow of
4. Final
Own nonce Date
number.
wawa source of diac herne
0. You rosy, attach additional dheste desaiMnp arhy additional water pollution nor other environmental projects which ussy atac your
dbdhaa"9) you now hews under way or which you pith. 6dioals whether each program to now under way or planned, and Indicate your
er'Ahai Of road mhWuka for construction.
III. Me DmIrmae Ma
Attedh a site map tapog (w bdtatinp the outiko a areas served by doe outat(s) covered In the eppllcaticn M e
topbgrepldo map Is amvallabb) d rngg to feoaty IndufihQ each a He fihmks and dladh#gs ; the draboags area of each storm
water ouMaa; paved areas and bhdldirga rdthln t e drainage area each storm water Dolton, each known past or present areas used for outdoor
storage or disposal of dgro icem materials, each mdatkg structural ehorN, measure to rsdua pdiutam in storm waor nrhoM, materbh baaing
and access grew. areas where psstddey herbicides, sDt conditioners and fertilizers are applied; each of Its hazardous waste beabnem,
storage or disposal units Urhruding each area not required to have a RCRA perndt which b used for aooumulaft hazardous waste under 40
CFR AW 34); each well where aWtls kom to facility are Injected haMerground; spdnga, end other surface water bodies which receive storm
water disclueraes, from the facliftv.
EPA Form 3510-21F (Rev. 1-02) - - Page 1 a 3 - Continue on Page 2

8
�
-
m
�
J
a
s
s
Js
kgo
AL
Q
y
o N
Ila
.ar
f
2 2 1
'R
CrD
fill
Z
�
to

. FPA m Number (eopyaom rmm l orrmm l)
Continued from Pane 2
A,B,G & D: $oe Insbudkro before prooaedinp. Complete one eel of tebles for each outfail. Annotate to outlell number In the space provided.
Tables 111144, VI and MI -Care Inchded on separate shaft numbered MI l and VIF2
E: Polendal discharges not covered by analysis - is any tops pollutant listed in table 2F-2, 2F-3 or 2Fd, a substance or a component of a substance
which you currency use or manufacture as an Intermediate or final Product or byproduct? .
Yes afl such polAdants below No to Section no
Do you have say Knowledge or reason to believe tat any biological teat for acute or chronic toolcty has been made on my of your di cltarg" or
on a recelving water In relation to your dlacrerps widdn the fast 3 years? .
Yes Mer a9 such pWhjtnnts beAN4 No to Seedon
IX Contract Ana
Were of are analysis reported in ham VII performed by a wand laboratory or cansulft rem? .
eaa"Y
V� I Yes (at to name, .It end iskphaw Wival nueMer d, and poflutanfa :❑ No (go to Section Jp
lam''
A. Nam
& Address
C. Area Cods & Phone No.
D. Pollutants Analymed
5cosp- J TnE�
Rd.
813 88S ")y2�
" �nwsc
C0
LA80&AT0 R1 ES I 1 -
Sv,hTt 100
TSS f H
TAhpr1 FL
TKO. l P
33 LR
82 Ca o
of law this document and all atlachmero were prepared under my dkoctfol or
I under penallythat
.
sf�slon Jn accordance tMtll a system designed to assure that qualified personnel property gather and evaluate
the kdOrpnffifon submitted. Based on my hfqulty d tine person or persons who manage fhe system or those persons
diroody responslb)e for go the /Namadon, (he Irdomadon submitted Is, to the best of my knowledge and
I that there signb7cant for submitting false hdbmwdbr4
belle[, but and C�ete Bm aware are penalties
includingfhea possWityof Hine andkilpdsonmentfor (mow)ngiblatfons.
0. Name & OMdd Tltls (dpe orprOtQ
B. Ares (bde and PIxm No.
�1 (deck. EHS I'�r'AGE2
if'vo�2:l. S'L15
G
D. Date Signed
(s -0
EPA Form 3510-2F (Rev. 1-92) Pape 3 of 3

EPA ID rwmber &oPyt=n Ram 1 of Form 1)
Form Approved. OMB No. 2Da0o085
Approvd ezphee 53182
n
• 1 '10..
1. � Ic'• • C'� I'•
EPAForm3510-21F-(Rev. 1.04 - Page V6.1 - -- -' _ ___' --- - Continue on Heverae

Continued from the Front
Part C - Nda Wde� adwwn fd feq buIn Tobi a. Co 2F- one 18bb tol a ll oloom of have season to believe Is preeeM. See the InsCwYbna tw '
Pdluterd
CAS Nanber
(Ravailable)
Mm&num Volume
Qraluds uMls)
pie Values
Wwfuds un"
Number
of
soam
Ewnb
Sampled
Sources of FblMrtante
T
1pN
FlowAweiphted
Conl calls,
. firab S pb
Ta �Du�ring
MBu1be
. qvw-*Mad
CorrrpoNb
Pet D - Provide dab for the None evendsl which resulted
in the maximum velum for the flow welchlad
1.
Dab of
Storm
Evert
2
Duration
of Storm Evert
mlrwba
&
Total rNMa2
durYtp Nam evarrt
Inctin
A
Number d Itoura between
u � ant erW of previaia
rtgestaebb rein evmrl
5.
Mmdmum flow rate dudng
min event
(gapona nu0s ar
Wte
&
Total flow from
rein event
or urdfa
G•tv�I
SY
).2
�2
3 pSP„
Z000JA)
f. Provide a desal of the matlwd of flow ntaemxementofeadmab.
V(SUA(, C--3'ffl•MATE
EPA Fofm 9510.2E (PAY- 1-02) . t-qp vl�

F-
12 3 4 7 8
R Ra.{tian note Date Sgmn ChackW
To aanara avez —�
I
A yeMyNN, A
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terra tltr simar xyde MAtefaeice
Legend
DBWWW W CheckaaM Mpwad M-dib F"e Date &ale
F }y svnnvaer RLK RLK RLK71laW GVFadliH 7/73004 ww Srale F
ear. Drainage Plan
H&D, Inc. EM.
0 1/1
1 2 3 6 7 8

STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Analytical Report
For: Mr. Rick Keck
Hendrix and Dail
7610 U.S. Hwy 41 North
Palmetto, FL 34221
CC:
Order Number:B423238
SDG Number:
Client Project ID:
Project: Greenvi11e,NC
Report Date:07/09/2004
Sampled By:Client
Sample Received Date:06/30/2004
Requisition Number:
Purchase Order:
[e-mail]
The test results in this report meet all NELAP requirements for parameters for which
accreditation is required or available. Any exceptions to NELAP requirements are noted in
this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the
written approval of the laboratory.
Page 1 of 10

STL, -
STL Tampa
6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Order: B423238
Date Received: 06/30/2004
Client Sanple ID
Greenville, Outfall (9p0
Sample Summary
Client: Hendrix and Dail
Project: Greenville,NC
Lab Sample ID Matrix
B423238*1 Liquid
Date Sampled
06/28/2004 06:00
Page 2 of 10

STL
STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Analytical Data Report
Lab Sample ID Description Matrix Date Received Date Sampled SDGV
23238-1 Greenville, Outfall (SW) Liquid 06/30/04 06/28/04 06:00
Lab Sample IDs
parameter Units 23238-1
Volatiles by GC/MS (8260)
Bromomethane (Methyl bromide)
ug/l
0.66U
trans-1,3-Dichloropropene
ug/l
0.14U
Surrogate - Toluene-d8 *
%
116 %
Surrogate -
4-Bromofluorobenzene *
%
108 %
Surrogate -
Dibromofluoromethane *
%
108 %
Analysis Date
07/06/04
Analysis Time
14:35
Oil & Grease (Hexane Extractable Material)(1664) (1664)
Oil & Grease (Hexane
Extractable Material)(1664)
mg/l
0.73U
Prep Date
07/06/04
Analysis Date
07/06/04
Analysis Time
15:00
Biochemical Oxygen Demand (5 Day)
(405.1/5210B)
Biochemical Oxygen Demand (5
Day)
mg/l
2.OU
Analysis Date
06/30/04
Analysis Time
16:25
Page 3 of 10

STL
STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Analytical Data Repot
Lab Sample M Description
23238-1 Greenville, Outfall (SW)
Lab Sample Ms
Parameter Units 23238-1
Suspended Solids (160.2)
Suspended Solids mg/l S.OU
Analysis Date 07/02/04
Analysis Time 10:30
PH (150.1)
pH
units
7.1
Analysis Date
06/30/04
Analysis Time
13:30
Chemical Oxygen Demand (SM5220C)
Chemical Oxygen Demand
mg/l
20U
Prep Date
07/01/04
Analysis Date
07/02/04
Analysis Time
10:34
Total Kjeldahl Nitrogen-N
(351.3)
Total Kjeldahl Nitrogen-N
eg/l
1.3
Analysis Date
07/06/04
Analysis Time
10:00
Phosphorus, Total (365.2)
Phosphorus, Total
mg/1
0.056I
Analysis Date
07/01/04
Analysis Time
20:00
Matrix Date Received Date Sampled SDGI
Liquid 06/30/04 06/28/04 06:00
Page 4 of 10

SrTL
STL Tampa 6712 Benjamin
Road, Suite 100 - Tampa FL 33634
Telephone:[phone] Fax:(813)
885-7049
Analytical Data Report
Lab Sample ID Description
Matrix Date Reoeived Date Sanpled SDG#
23238-2 Method Blank
Liquid 06/30/04
23238-3 Accuracy Mec)
Liquid 06/30/04
23238-4 LCS Accuracy Control Limit
(%O
Liquid 06/30/04
23238-5 Precision (%iPD)
Liquid 06/30/04
23238-6 LCS Precision Control
Limit (Advisory) %iPD
Liquid 06/30/04
Lab Sample 3Ds
Parameter hits
23238-2
23238-3
23238-4
23238-5
23Z38-6
Volatiles by GC/MS (8260)
Bromomethane (Methyl bromide) ug/l
0.66U
trans-1,3-Dichloropropene ug/1
O.14U
Surrogate - Toluene-d8 * %
110 %
102/106 %
77-122 %
Surrogate -
4-Bramofluorobenzene * %
102 %
100/102 %
74-126 %
Surrogate -
Dibromofluoromethane * %
98 %
96/98 %
70-130 %
Benzene %
94 %
62-135 %
0 %
<16 %
Toluene %
105 %
68-131 %
1.9 %
<33 %
Analysis Date
07/06/04
07/06/04
07/06/04
Analysis Time
11:59
Oil & Grease (Hexane Extractable Material)(1664) (1664)
Oil & Grease (Hexane
Extractable Material)(1664) mg/l
O.73U
97 %
78-114 %
2.1 %
<18 %
Prep Date
07/06/04
07/06/04
07/06/04
Analysis Date
07/06/04
07/06/04
07/06/04
Analysis Time
15:00
Biochemical Oxygen Demand (5 Day) (405.1/5210B)
Biochemical Oxygen Demand (5
Day) mg/l
2.OU
90 %
85-115 %
2.8 %
<30 %
Analysis Date
06/30/04
06/30/04
06/30/04
Analysis Time
16:25
Page 5 of 10

STL
-
STL Tampa 6712 Benjamin Road, Suite 100 -
Tampa FL 33634
Telephone:[phone]
Fax:(813)
885-7049
Analytical Data Report
Lab Sample ID Desmiptian
Matrix Date Received Date Sampled
-9"
23238-2 Method Blank
Liquid 06/30/04
23238-3 Accuracy Stec)
Liquid 06/30/04
23238-4 LCS Accuracy Control Limit M
Liquid 06/30/04
23238-5 Precision (%2PD)
Liquid 06/30/04
23238-6 LCS Precision Control Limit (Advisory) %2PD
Liquid 06/30/04
Lab Sample II2s
Parameter Units
23238-2
Z3238-3
Z3238-4
23238-S 23238-6
Suspended Solids (160.2)
Suspended Solids mg/l
S.Ou
99 %
80-120 %
6.1 % <25
%
Analysis Date
07/02/04
07/02/04
07/02/04
Analysis Time
10:30
PH (150.1)
PH units
6.0
107 %
63-158 %
0.67 % <40
%
Analysis Date
06/30/04
06/30/04
06/30/04
Analysis Time
13:30
Chemical Oxygen Demand (SM5220C)
Chemical Oxygen Demand mg/l
20U
105 %
80-120 %
3.8 % <40
%
Prep Date
07/01/04
07/01/04
07/01/04
Analysis Date
07/02/04
07/02/04
07/02/04
Analysis Time
10:34
Total Kjeldahl Nitrogen-N (351.3)
Total Kjeldahl Nitrogen-N mg/l
0.44U
100 %
75-125 %
1.1 % <40
%
Analysis Date
07/06/04
07/06/04
07/06/04
Analysis Time
10:00
Page 6 of 10

SrTL
STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Analytical Data Report
Lab Sample ID Description
23238-2 Method Blank
23238-3 Accuracy Qaiec)
23238-4 LCS Accuracy Control Limit (%i)
23238-5 Precision MPD)
23238-6 LCS Precision Control Limit (Advisory) %tPD
Lab Sample )Ds
Parameter Units 23238-2 23238-3
Phosphorus, Total (365.2)
Phosphorus, Total mg/l 0.017U 99 %
Analysis Date 07/O1/04 07/01/04
Analysis Time 20:00
Page 7 of 10
Mhtmx Date Received Date Sampled SDG#
Liquid
06/30/04
Liquid
06/30/04
Liquid
06/30/04
Liquid
06/30/04
Liquid
06/30/04
23238-4 23238-5
23238-6
60-140 % 0 % <40 %
07/01/04

STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Analytical Data Report
Lab Sample ID Descr-iption Matrix Date Reoeived Date Sampled SDG#
23238-7 Practical Quantitation Limit (PQL) Liquid 06/30/04 -
23238-8 Method Detection Limit (POL) Liquid 06/30/04
Lab Sample IN
Parameter- Units 23238-7 23238-8
Volatiles by CC/MS (8260)
Bromomethane (Methyl bromide)
ug/l
1.0
0.66
trans-1,3-Dichloropropene
ug/1
1.0
0.14
Oil & Grease (Hexane Extractable Material)(1664) (1664)
Oil & Grease (Hexane
Extractable Material)(1664)
mg/l
5.0
0.73
Biochemical Oxygen Demand
(5 Day)
(405.1/5210B)
Biochemical Oxygen Demand (5
Day)
mg/l
2.0
2.0
Suspended Solids (160.2)
Suspended Solids
mg/l
5.0
5.0
Chemical Oxygen Demand (SM5220C)
Chemical Oxygen Demand
mg/l
20
20
Total Kjeldahl Nitrogen-N
(351.3)
Total Kjeldahl Nitrogen-N
mg/l
0.50
0.44
Page 8 of 10

STL,
STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Analytical Data Report
Lab Sample ID Description Matrix Date Received Date Sampled SDGN
23238-7 Practical Quantitation Limit (PQL) Liquid 06/30/04
23238-8 Method Detection Limit (bDL) Liquid 06/30/04
Lab Sample Ms
Parameter Wits 23238-7 23238-8
Phosphorus, Total (365.2)
Phosphorus, Total mg/l 0.10 0.017
Page 9 of 10

STL
STL Tampa 6712 Benjamin Road, Suite 100 - Tampa FL 33634 Telephone:[phone] Fax:[phone]
Order Number: 9423238
Method: EPA 600/4-79-020,SW-846,FDEP,Federal Register, Standard Method
DOH Certification NE84282
I e The reported value is between the laboratory method detection
limit and the laboratory practical quantitation limit.
U e Indicates that the compound was analyzed for but not detected.
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL project manager
who signed this test report.
The estimated uncertainty associated with these reported results is
available upon request.
Page 10 of 10

Serial Number 05371
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
' STL 8Lf2�Z3�
®f STL Tampa Website: w .stl-inc.com
6712 Benjamin Road, Suite 100 Phone: [phone]
Tampa, FL33634 Fax:[phone]
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Phone:
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