NCS000259_MONITORING INFO_20200922

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
DOC TYPE
❑ FINAL PERMIT
154 MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ rZoZDC t22
YYYYMMDD

.r
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME AkzoNobel Surface Chemistry LLC COUNTY Rowan
PERSON COLLECTING SAMPLE(S) LVynWhIte PHONE NO. [phone]
CERTIFIED LABORATORY(S) Prism Laboratories Inc. Lab# 377G`���/
Lab # 402
ED
AUG 17 2018 SIGNATURE
GNAT REOF ON PAGE 2TTEE OR DESIGNEE
Part A: Specific Monitoring Requirements CENTRAL FILES
r ION
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m L
m
m
SIU
SW-1
07/30/2018
0.2
0.020
<0.00050
0.40
7.2
SW-2
07/30/2018
0.2
<0.00050
0.0017
1.1
7.3
SW-3
07/30/2018
0.2
< 0.00050
< 0.00050
1.3
6.8
SW-4
07/30/2018
No Flow
No Flow
No Flow
No Flow
No Flow
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorine Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
at Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
mg1l
m I
unit
al/mo
Form S WU-247, last revised 2121201
Pagel of 2

STORM EVENT CHARACTERISTICS:
Date 07/30/2018
Total Event Precipitation (inches): 0.2
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
b/i6/1F
(Signature of Permittee) (Date)
Form SWU-247, last revised 2121201
Page 2 of 2

n. \
D Full -Service Analytical &
aP R I M Environmental Solutions
n! LMBOIUTOFIE$ INC
Akzo Nobel
David Simons
485 Cedar Springs Road
Salisbury, NC 28147
NC Certification No. 402
NC Drinking Water Cart No. 37735
SC Certification No. 99012
Project: Stormwater
Lab Submittal Date:08/01/2018
Prism Work Order: 8080022
Case Narrative
08/09/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Terri W. Cole
Project Manager
Data Qualifiers Key Reference
Reviewed By Terri W. Cole
Project Manager
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: 704I629-6364 - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 Of 9

/*E,)'R
I S M I Fun -Service al Sol do Environmental Solutions
i
Sample Receipt Summary
08/09/2018
Prism Work Order: 8080022
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
SW-1
8080022-01
Water
07/30/18 14:15
SW-2
8080022-02
Water
07/30/18 14:22
SW-3
8080022-03
Water
07/30/18 14:31
Samples were received in good condition at 2.6 degrees C unless otherwise noted.
Date/Time Received
08/01/18 17:15
08/01/18 17:15
08/01/18 17:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]-Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 2 of 9

P R I S M I Full -Service Analytical 4
Environmental Solutions
�l�.ewrawes roe
Summary of Detections
08/09/2018
Prism Work Order: 8080022
Prism ID
Client ID
Parameter
Method
Result
Units
8080022-01
SW-1
Nitrate/Nitrite as N
'SM4500-NO3 F
0.40
mg/L
8080022-01
SW-1
1,2-Dichloroelhane
'8260B
0.020
mg/L
8080022-02
SW-2
Nitrate/Nitrite as N
'SM4500-NO3 F
1.1
mg/L
8080022-02
SW-2
Toluene
'8260B
0.0017
mg/L
8080022-03
SW-3
Nitrate/Nitrite as N
'SM4500-NO3 F
1.3
mg/L
B
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3o 99

Laboratory Report
`- � %� Pull-aarvice Analytical 8
Jn I
rL� J' V I Environmental solutions
I
7r.eoe..owea,aa
08/09/2018
Akzo Nobel
Project: Stormwater
Client Sample ID: SW-1
Attn: David Simons
Prism Sample ID: 8080022-01
485 Cedar Springs Road
Prism Work Order: 8080022
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: 07/30/18 14:15
Time Submitted: 08/01/18 17:15
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Dateliime ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.40
mg/L
0.10 0.033
1 'SM4500-1403 F 818118 14:17 BMS Pill
Volatile Organic Compounds by GCIMS
1,2-Dichloroethane 0.020
11
0.00050 0.000066
1 '8260B 818118 17:03 KDM P81-10129
Toluene BRL
mg/L
0.00050 0,000044
1 `8260B 8/8118 1703 KDM P81-10129
Surrogate
Recovery Control Limits
4-Bromoguorobenzene
86 % 80-124
Dibromofluoromelhane
85 % 75-129
Toluened8
75 % 77-123 SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 4 of 9

Laboratory Report
/
iP,R l M
S.�,renm..r., 6e,enon,al&
FWServiceal Solutions
08/09/2018
Akzo Nobel
Project: Stormwater
Client Sample ID: SW-2
Attn: David Simons
Prism Sample ID: 8080022-02
485 Cedar Springs Road
Prism Work Order: 8080022
Salisbury, INC 28147
Sample Matrix: Water
Time Collected: 07/30/18 14:22
Time Submitted: 08/01/18 17:15
Parameter
Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
NitratelNitrite as N 1.1
mg/L
0.10 0.033
1 'SM4500-NO3 F 8/8118 14:17
BMS P8110114
Volatile Organic Compounds by GC/MS
1,2-Dichloroethane BRL
mg/L
0.00050 0.000066
1 '8260B B/B/18 17:28
KDM PBH0129
Toluene 0.0017
mg/L
0.00050 0.000044
1 '8260B 8/8/18 17:28
KDM P8110129
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene 83 % 80-124
Dibromo9uoromethane 84 % 75-129
Toluene-d6 77% 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0543
Phone: [phone]- Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 9

Laboratory Report
PRISM I y'lioService Analytical 8
Envlronmemal Solutions
0$/09/201$
�J.ma.'oaa...
Akzo Nobel
Project: Stormwater
Client Sample ID: SW-3
Attn: David Simons
Prism Sample ID: 8080022-03
485 Cedar Springs Road
Prism Work Order: 8080022
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: 07/30/18 14:31
Time Submitted: 08/01/18 17:15
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Nitrate/Nitrite as N
1.3
ri
0.10
0.033
1 'SM4500-NOS F 818/18 14:17 BMS P8H0114
Volatile Organic Compounds by GCIMS
1,2-Dichloroelhane
BRL
mg/L
0.00050
0.000066
1 '8260B 8/8/18 1754 KDM P8H0129
Toluene
BRL
mg/L
0.00050
0.000044
1 '8260B 8/8/18 1754 KDM PSH0129
Surrogate
Recovery Control Limits
4-BromoOuorobenzene
85 % 80-124
Dibromo8uoromethane
87 % 75-129
Toluene-d8
77 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 14001629-6364- Fax: [phone] Page 6 of 9

Full-SarviAnalytical
Environmenen tal Solutions
�—vluewuiwnes me
Akzo Nobel Project: Stormwater
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P81-10129 - 5030B
Reporting Spike
Result Limit Units Level
Level II QC Report
8/9/18
Prism Work Order: 8080022
Time Submitted: 8/1/2018 5:15:OOPM
Source %REC RPD
Result %REC Limits RPD Limit Notes
Blank (P8H0129-BLK1)
Prepared &
Analyzed:
08/08/18
1,2-Dichloroethene
BRL
0.00050
mg/L
Toluene
BRL
0.00050
mg/L
Surrogate: 4-Bromofluorobenzene
43.1
ug/L
50.00
86
80-124
Surrogate: Dibromofluoromethane
42.8
ug/L
5000
86
75-129
Surrogate: Toluene-d8
38.3
ug/L
50.00
77
77-123
LCS (P8H0129-BSI)
Prepared &
Analyzed:
08/08/18
1,2.Dichloroethane
0.0226
0.00050
mg/L
0.02000
113
68-131
Toluene
0,0245
0.00050
mg/L
0.02000
122
76-131
Surrogate: 4-Bromofluorobenzene
42.0
ug/L
5000
84
80-124
Surrogate: Dibromofluoromethane
42.4
ug/L
50.00
65
75-129
Surrogate: Toluene-0
374
ug/L
50.00
75
77-123 SR
LCS Dup (P8H0129-BSD1)
Prepared &
Analyzed:
08/08/18
1,2-Dichloroethene
0.0222
0.00050
mg/L
0.02000
ill
68-131 2 20
Toluene
0.0238
0.00050
mg/L
0.02000
119
76-131 3 20
Surrogate: 4-Bromofluorobenzene
42.0
U91L
50.00
84
60-124
Surrogate: Dibromofluoromethane
42.5
ug/L
50.00
65
75-129
Surrogate: Toluene-d8
38.0
ugA
50.00
76
77-123 SR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone]-Toll Free Number: l-800/629-6364- Fax: [phone] Page 7 of 9

Full -Service Analytical &
Ana),"Rism I Environmental Solutions
—rt.eoa.maca'.e
Akzo Nobel Project: Stormwater
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
General Chemistry Parameters - Quality Control
Level II QC Report
8/9/18
Prism Work Order: 8080022
Time Submitted: 8/1/2018 5:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8110114 - NO PREP
Blank (P81-10114-BLK1) Prepared & Analyzed: 08/08/18
Nitrate/Nitrite as N BRL 0.10 mg/L
LCS (P8H0114-BSI) Prepared & Analyzed: 08/08/18
Nitrate/Nitrite as N 0.985 0.10 mg/L 1.000 98 90-110
Prop Method: 6030E
Lab Number
8080022-01
6080022-02
8080022-03
Sample Extraction Data
Batch
Initial
Final
DateTme
PSH0129
10
mL
10 mL
08/08/18 9:54
P8H0129
10
mL
10 mL
08/08/18 9:54
P8H0129
10
mL
10 mL
08/08/18 9:54
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643
Phone: [phone]i364-Toll Free Number; l-8001529-6364- Fax: [phone] Page 8 of 9

PRISM
�.'r'-- ✓usowroRiw �rX
CHAIN OF CUSTODY RECORD
Full -Service Analytical &
Environmental Solutions PAGE-1 OFI_ QUOTE s TO ENSURE PROPER BILLING:
449 Springbrook Road • Charlotte. NC 26217
Phone [phone] • Fax: 7,0/�41525 09
Client Company Name: -
Report To/Contact Name: f - ++oe-
Reortp g yddress: 1 > S
`�arLrshL_7 At Z PI
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions andlor QC Requirements
Invoice To:
Address:
Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
Cr
CUSTODY SEALS INTACT?
CL
YES NO N/A Cr,i — — Orr
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used? _!
Phone&y7 —tj&a :3 Fax (Yes) (No): Purchase Order No.IBilling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Data 111 Day Cl2 Days ❑ 3 Days D 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF CBI_Other
9 Days ❑ Standard 10 days [a Rush Work Must Be
"Working Days" Pre -Approved
Sc OTHER
N/A
Site Location Name:
Samples received after 14:00 will be processed next business day.
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS It CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
P P -
NO
TIME
MATRIX
SAMPLE CONTAINER
YSIS REQUESTED
��qY
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
u(�}�,� J/ REMARKS
'TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATERER
TIVES
`/� oy, /
ID NO.
HOURS
SLUDGE)
SEE BELOW
�1
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Sampler's Signatur
I Sampled By (Print Name) (.tJ Affiliation k�
Upon relin 111Y9,11ris GRain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
subml n g to the Prism Proje
anger. There will be charges for any changes after analyses have been initialized.
•('B^'1 °ice"/ °p2 Additional Comments:
�
Site AnivalTime:
I I �-�'�rt�D �L
Time:
taim y: grratuw
R to 519wW.) o
Site Departure
(�
J
olNgw By, 1 - naWr
�/ t t
Rocorva r P/], La�ar"nalprlm BY OGG� -7
Field Tech Fee:
,./
7 ��� i .2-0
Mileage:
MaVad o ar, NOTE: ALL SAMPLE COOLERS SHOULD BE TAPEO S CUSTODY SEALS FOR TRANS NTATION TO THE LABORATORY. CDC GiOUP No.
�13
SAMPLES ARE No EPTEO AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. (� 0; r,/_ 2
d Ex CI la
O FeUPS D Harudro eretl - Field Service ❑ Em � - —(� Qi
NPDES: UST: G NDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: �j r r7 S
❑NC❑SC El NC ❑SC ❑ C ❑SC
❑NC ❑SC ❑NC ❑SC ❑NC❑SC ❑NC ❑SC ❑NC El SC ❑NC ❑SC /
n n ❑
❑ ❑ ___ --. ❑ ❑ ❑ _ ❑
*CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL =Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL

April 3, 2018
NCDENR — Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Certified Mail: Return Receipt Requested
Reference: Semi -Annual Permit Monitoring Report
Individual Stormwater Monitoring Permit
AkzoNobel Surface Chemistry LLC.
Permit No. NCS000259
RECEIVED
APR 0 4 2018
CENTRAL FILES
DWR SECTION
Attached are two copies of the AkzoNobel monitoring results for the period
of January I, 2018 to June 30, 2018 for our permit # NCS000259 for the
samples collected March 01, 2018. Any questions on this submittal you may
contact me at 704-642-6233.
Regards,
8:�-CU4
David Simons
HSES Manager
AkzoNobel Surface Chemistry, LLC, Salisbury, NC
Copy: William Teasdale AkzoNobel Surface Chemistry, LLC,
Salisbury, NC
Christopher Fleming AkzoNobel Surface Chemistry, LLC,
Salisbury, NC

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME AkzoNobel Surface Chemistry LLC COUNTY Rowan
PERSON COLLECTING SAMPLE(S) Lyyn White, Traci Sloop PHONE NO. 7( 04) 633-1731
CERTIFIED LABORATORY(S) Prism Laboratories Inc. Lab # 37735
Lab # 402
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PACE 2.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m L
m /L
m L
SIU
SW-1
03/01/2018
.35
0.020
<0.00050
0.52
6.92
SW-2
03/O1/2018
1
.35
0.0018
<0.00050
1.4
1 7.14
SW-3
03/01/2018
.35
0.0014
<0.00050
0.69
6.87
SW-4
03/01/2018
No Flow
No Flow
No Flow
No Flow
No Flow
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
No.
Date
Sample
Collected
150050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m /I
m /I
unit
gallmo
Form SWU-247, last revised 2121201
Pagel of 2

STORM EVENT CHARACTERISTICS:
Date 03/O1/2018
Total Event Precipitation (inches): .35
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
includingthepossibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
William Teasdale Site Operations Director
(Date)
Form SWU-247, last revised 2121201
Page 2 of 2

� Case Narrative
1 NC CertRcetion No. 402
ZZP' L I S Full -Service Analytical 8 NC Drinking Water Cart No. 37735 03/14/2018
Environmental Solutions SC Certifce6on No. 99012
OIAe09att1alR ING
Akzo Nobel Project: SW Samples
David Simons
485 Cedar Springs Road Lab Submittal Date: 03/02/2018
Salisbury, NC 28147 Prism Work Order: 8030059
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analylical report.
Respectfully,
PRISM LABORATORIES, INC.
sd-'M�Afflrdl
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Reviewed By Terri W. Cole
Project Manager
• Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: [phone]- Tall Free Number.. 1.8001629.6364-Fax: [phone] Page 1 oi9

GP R ISM I Fua-Serv�celcel a
£nvironment.1 el S.I 9olullane
uwunxuR me
Sample Receipt Summary
03/14/2018
Prism Work Order: 8030059
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
SW-1 8030059-01 Water 03/01/18 03/02/18
SW-2 8030059-02 Water 03/01/18 03/02/18
SW-3 8030059-03 Water 03/01/18 03/02/18
Samples were received in good condition at 2.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Leboratones, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, INC 28224-0543
Phone: [phone]- Toll Free Number.. l-0001529.6364-Fax: [phone] Page 2 of 9

AK�A`Q
'p\/p1Full-SoMce Rnalynml S
I S I tl, I Mironmentel solutions
v„a,e,a.re',
Summary of Detections
03/14/2018
Prism Work Order: 8030059
Prism ID
Client ID
Parameter
Method
Result
Units
8030059-01
SW-1
Nitrate/Nitrite as N
*SM4500-NO3 F
0.52
mg/L
8030059-01
SW-1
1,2-Dichloroethane
'8260B
0.020
mg/L
8030059-02
SW-2
Nitrate/Nitrite as N
•SM45o0-NO3 F
1.4
mg/L
8030059-02
SW-2
1,2-Dichloroethane
•8260B
otitis
mg/L
8030059-03
SW-3
Nitrate/Nitrite as N
'SM4500-NO3 F
0.69
mg/L
8030059-03
SW-3
1,2-Dichloroethane
'8260B
0.0014
mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number. 1.8001529-6364 - Fax: [phone]
Page 3 of 9

Laboratory Report
LE'bR�'Qg
ISM:
S{� i�I col-servms nnaryncel s 03/14/2018
��/� Envlronmentol 9olutlom
urwnawmxc
Akzo Nobel Project: SW Samples Client Sample ID: SW-1
Attn: David Simons Prism Sample ID: 8030059-01
485 Cedar Springs Road Prism Work Order: 8030059
,Salisbury, NC 28147 Sample Matrix: Water Time Collected: 03/01/18 07:10
Time Submitted: 03/02/18 17:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datefrime ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.52
mg/L
0.10
0.0024 1
'SM4500-NO3 F 319118 9:30
CLB
PeC0124
Volatile Organic Compounds by GC/MS
1,2.Dichlomethane 0.020
mg/L
0.00050
0.000066 1
'8260B 3I7118 21:08
KDM
P8C0108
Toluene BRL
mg/L
0,00050
0.000044 1
'8260B 3n118 21:08
KOM
PBC0108
Surrogate
Recovery
Control Limns
4-Bromonluorobenzene
101 %
80-124
Dibromolluoromethane
102 %
75129
Toluene-d8
98 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
"a Springbmok Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001629-63M - Fax: [phone]
Page 4 of 9

JE�P' 9emice Analytical a
'R ISM I Environmental eoluaans
..m Im t.
Laboratory Report
03/14/2018
Akzo Nobel
Project: SW Samples
Client Sample ID: SW-2
Attn: David Simons
Prism Sample ID: 8030059-02
485 Cedar Springs Road
Prism Work Order: 8030059
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: 03/01/18 07:15
Time Submitted: 03/02/18 17:30
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Nitrate/Nitrite as N
1.4 mg/L
0.10 0.0024
1 •SM4500-NO3 F 319118 9:30
CLB
PlIC0124
Volatile Organic Compounds by GC/MS
1,2-0Ichloroethane
0.018 mg/L
0.00050 0.000066
1 •82608 D17118 21:42
KDM
P8C0108
Toluene
BRL mg/L
0.00050 0.000044
1 •82608 Y7/18 21:42
KDM
P8C0108
surrogate
Reooyery
Control Limits
4-Bromofluorobenzene
100 %
80.124
Dibromo0uoromethane
103 %
75-129
Toluene -de
98 %
77423
This report should not be reproduced, except in its entirety, without the written consent of Prism Leboratones, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number..l-9001529.6364-Fax: [phone] Page 5 of 9

Laboratory Report
ZzK'rPL)'Q-IS�t A I Full -Santee al Sotucal a ' V I environmental Smmlom 0311412018
ume�,wmiec
Akzo Nobel Project: SW Samples
Client Sample ID: SW-3
Attn: David Simons
Prism Sample ID: 8030059-03
485 Cedar Springs Road
Prism Work Order: 8030059
Salisbury, NC 28147 Sample Matrix: Water
Time Collected: 03/01/18 07:15
Time Submitted: 03/02/18 17:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daterrime ID
General Chemistry Parameters
Nllmts/Nltdte as N 0.69 mg/L 0.10 0.0024 1 *SM4500-NO3 F 319118 9:30 CLB P8C0124
Volatile Organic Compounds by GC/MS
1,2.Dichloroethane 0.0014 mgll. 0.00050 0.000066 1 •82608 W/18 22:16 KDM PBC0108
Toluene BRL mg/L 0.00050 0.0000" 1 -8260B 3n1l8 22:16 KDM P8C0108
Surrogate Recovery Control Limits
4-Bmmofluombenzene 99 % 80-124
Dibmmofluommethane 103 % 75-129
Toluene-d8 97 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
"a Splingbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number. 1.8001529-6364- Fax: [phone]M09 Page 6 of 9

P`_ Environmental Solution
won.toa� i.c
Level II QC Report
3/14/18
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Volatile Organic Compounds by GC/MS - Quality Control
Reporting
Result Limit Units
Batch P8C0108 - 5030B
Prism Work Order: 8030059
Time Submitted: 3/2/2018 5:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (PBC0108-BLKt)
Prepared & Analyzed: 03/07/18
1,2-Dichloroethane
BRL
0.001150
mg/L
Toluene
BRL
0.00050
mg/L
Surrogate: 4-Bromofluorobenzene
49.8
ug/L
50.00 100
80-124
Surrogate: Dibromofluoromethane
49.9
u91L
50.00 100
75-129
Surrogate: Toluene-d8
49.5
ug/L
50.00 99
77-123
LCS (P8C0108-BS1)
Prepared & Analyzed: 03/07/18
1,2-Dichloroethane
0.0221
0.00050
mgtL
0.02000 ill
60-131
Toluene
0.0230
0.00050
mg/L
0.02000 115
76-131
Surrogate: 4-Bromofluorobenzene
50.5
ug/L
50.00 101
80-124
Surrogate: Dlbromofluoromethane
51.3
ug/L
5000 103
75-129
Surrogate: Toluene-0a
49.2
ugA
50.00 98
77-123
LCS Cup (P8C0108-BSD1)
Prepared & Analyzed: 03/07/18
1,2-Dichloroethane
0.0215
0.00050
m9/1-
0.02000 108
68-131 3 20
Toluene
0.0224
0,00050
mg/L
0.02000 112
76-131 3 20
Surrogate: 4-Bromofluorobenzene
49.6
ug/L
50.00 99
80-124
Surrogate: Dibmmofluomme/hane
50.7
ug/L
50.00 101
75-/29
Surrogate: Toluene-d8
49.2
u91L
50.00 98
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboretones, Inc.
449 Springbrook Road - P.O. Box 240543-Chadotte, NC 28224-0643
Phone: [phone] - Tall Free Number.l-0001529-6364- Fax: [phone] Page 7 of 9

A?-6\]R
1p\/p1 Pull-Servlca Analtloal a
ISM I Environmental Solutions
Level II QC Report
3114/18
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
General Chemistry Parameters - Quality Control
Prism Work Order: 8030059
Time Submitted: 3/2/2018 5:30:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8C0124 - NO PREP
Blank(PSC0124-BLK1) Prepared: 03/08/18 Analyzed: 03/09/18
Nitrate/Nitri e, as N BRL 0.10 mg/L
LCS(P8C0124-BSI) Prepared: 03/08/18 Analyzed: 03/09/18
Nitrate/Nitrite as 0.959 0.10 mg/L 1.000 96 90-110
Sample Extraction Data
Prep Method: 50308
Lab Number Batch Initial Final Daterlme
8030059-01 PSC0108 10 mL 10 mL 03/07/18 9:32
8030059-02 PBC0108 10 mL 10 mL 03/07/18 9:32
8030059-03 POCO108 10 mL 10 mL 03/07M8 9:32
This report should not be reprodumd, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spdngbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number...1-8g0/629-6364-Fax: [phone] Page 8 of 9

A
n Full -Service Analytical&
� PISM I
CHAINOF CUSTODY RECORD
(
NO N/A
Environmental Solutions
'., 1ABQnamwEa
PAGE—LOF1 CRIME 0 TO ENSURE PROPER 6ILLINGr _ (
Sempbs INTACT upon arrival?
/
lNC
Road •
/49 Sprone 2409
Project Name: _ Received ON WET ICE?
_
T
O
Ol
70Dreok
Fax:Charlotte,7041 25
Phone [phone]fi4 •Fax: 704152E-0a09
Short Hold Analysis: (Yes) (No) UST Pro1act: lees) (No) PROPER PRESERVATIVES indicated?
— —
or
Client Company Name: .p
P V
'Please ATTACH an Received WITHIN HOLDING TIMES?
y projeM e reporting (OC LEVEL I II III IV)
CUSTODY
—
m
provisions andlor QC Requirements SEALS INTACT?O-
e nts
Repoli TO/Contact Name:
Involve To: VOLATILES reed W/OUT HEADSPACE?
Reporting Address: 62ilar.�
PROPER CONTAINERS 4
Address: t
_
rD w Z j T
I TEMP: Therm ID: Obse1ed:3.
�Phon°C
dress: fe'L33 Fax (Yes)(No):
purchase Order NOJBilling Reference TO BE FILLED IN BY CLIENT/SAMPLING
PERSONNEL
Email
Email Address:
Requested Due Date O 1 Day 02 Days O 3 Days 0 4 Days 0 5 Days Certification: NELAC_ DOD_
FL_ NC_
EDD Type: PDR, Excel_Other
"WorkingDays' tii" Days O standard 10 days O R�AP��ust Be
Site Location Name:
Sc OTHER
Samples received after 14:00 will be processed next business day.
N/A
Site Location Physical Address:
Turnaround time is based on business days, excluding was ends and hellos Water Chlorinated: YES_ NO_
CES
(SEE RENDEREDERSE BYFOR TERNIS & CONDITIONS PRISM LABORATORIES, INC. TTOO CLIENT)
�SERVIL Sample Iced Upon Collection: YES_
NO_
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
h K -
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
BLUEDGE)
TNES
REMARKS
DNp
BELOW
��O�I�!L�L
07W0
w&e-
I3
L100•_4
Sw- I
pZWo
2S6
Sw- 2—
n7W5
_a(p,
_r5w-3
oJ-'
He, v
'K
10
Sw-3
2so
2451bq
Sampler's Signal ur Sampled By
-
(Print Name) n_ Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submittadjp4nfiting to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
eP ad SxJnatura)
Sy, (SgnaWra Darn N IllylHwrs Additional Comments:
Site Arrival Tlme:
Helm By: signs ) Hari ay: (sigre ) Dom W'� ' r� — Ij�?j
Site Departure Time:
eYrq Y: ISignaarol M Rooelved F. Laq� nos Date r )/lf'Z— )}N— Witt
T
Field Tech Fee:
_ ._ __
/ 3 -'Z-18 S 'T to iA/ 3 - pp ' ✓,r87
iueaye:
Mearod dSlirynunL NOTE:ALL SAMPLE COOLERBSNOUIERIF TAPED T
STODY SEALS OR R N THE IABOM RY. C mup No.
SAMPLES ARE NOT A PTED AND VERIFIED AGAMST COG
AGAINST
UNTIL RECEIVED THE UBORATO
UN
O Fed Fs O UPS O Fiend-detivved - m Frets Servim O OMer
NPOES: UST: GR U DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER;
❑NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC
❑NC ❑SC ❑NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC
1 1
❑ ❑ ❑ ❑ ___I
❑ ❑ ❑ ❑ ❑
'CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P= Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space)
ORIGINAL

AkzoNobel 485 Cedar Springs Road T+ 1 704 633 1731
Surface Chemistry Unit A F + 1 704 637 8912
Salisbury, NC 28147 www.akzonobel.com/sc
USA
October 2, 2017
NCDENR — Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Certified Mail: Return Receipt Requested
Reference: Semi -Annual Permit Monitoring Report
Individual Stormwater Monitoring Permit
AkzoNobel Surface Chemistry LLC.
Permit No. NCS000259
AkzoNobel
Tomorrow's Answers Today
CNT 3
Czp1l
CwR S��TipNs
Attached are two copies of the AkzoNobel monitoring results for the period
of July 1, 2017 to December 31, 2017 for our permit # NCS000259 for the
samples collected on September 12, 2017. Any questions on this submittal
you may contact me at 704-642-6233.
Regards,
David Simons
HSES Manager
AkzoNobel Surface Chemistry, LLC, Salisbury, NC
Copy: Brian Owen AkzoNobel Surface Chemistry, LLC, Salisbury,
NC

Permit Number NCS 000259
FACILITY NAME AkzoNobel Si
PERSON COLLECTING SAMP
CERTIFIED LABORATORY(S)
Lab # 402
Part A: Specific Monitoring Requirements
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
COUNTY Rowan
PHONE NO. [phone]
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m /L
m /L
m /L
SIU
SW-1
09/12/2017
1.1
0.0022
<0.00050
0.20
6.2
SW-2
09/12/2017 1
1.1
0.0045
<0.00050
0.36
7.2
SW-3
09/12/2017
1.1
0.0016
0.00091
0.25
6.8
SW-4
09/12/2017
1.1
<0.00050
<0.00050
<0.10
6.8
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m /I
mg/1
unit
Raumo
Form SWU-247, Iasi revised 2121201
Pagel of 2

STORM EVENT CHARACTERISTICS:
Date 09/12/2017
Total Event Precipitation (inches): 1.1
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
includigg the possibili!,hof fines and imprisonment for knowing violations."
of Permittee)
6Vg i/7
(Date)
Form SWU-247, last revised 2121201
Page 2 of 2

J
aPRISM
ft t% eoMroRiea we
Akzo Nobel
David Simons
485 Cedar Springs Road
Salisbury, NC 28147
INC Certification No. 402
Full -Service Analytical & NC Drinking Water Cent No. 37735
Environmental Solutions SC Certification No. 99012
Project: SW Samples
Lab Submittal Date: 09/13/2017
Prism Work Order: 7090196
Case Narrative
09122/2017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Terri W. Cole
Project Manager
Data Qualifiers Key Reference
Reviewed By Terri W. Cole
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: 1.8001629-6364 - Fax: [phone]
Page 1 of 10

:�P1 Full -Service Analytical 8
R I S M I Environmental Solutionso"r eea.,eae.1»
Sample Receipt Summary
09/22/2017
Prism Work Order: 7090196
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
SW-1
7090196-01
Water
09/12/17
09/13/17
SW-2
7090196-02
Water
09/12/17
09/13/17
SW-3
7090196-03
Water
09/12/17
09/13/17
SW-4
7090196-04
Water
09/12/17
09/13/17
Samples were received in good condition at 3.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 26224-0543
Phone: [phone] - Toll Free Number: 1-80016296364 - Fax: [phone] Page 2 of 10

mn015
I S M I FWb9ervlce al Solutio 4
Environmental Solutlona
ueon.rowu ixc
Summary of Detections
09/22/2017
Prism Work Order: 7090196
Prism ID
Client ID
Parameter
Method
Result
Units
7090196-01
SW-1
Nitrate/Nitrite as N
'SM4500-NO3 F
0.20
mg/L
7090196-01
SW-1
1,2-Dichloroethane
'6260B
0.0022
mg/L
7090196-02
SW-2
Nitrate/Nitrite as N
-SM4500-NO3 F
0.36
mg/L
7090196-02
SW-2
1,2-Dichloroethane
'8260B
0.0045
mg/L
7090196-03
SW-3
Nitrate/Nitrite as N
'SM4500-NO3 F
0.25
mg/L
7090196-03
SW-3
1,2-Dichloroethane
'6260B
0.0016
mg/L
7090196-03
SW-3
Toluene
'e260B
0.00091
mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0643
Phone: [phone] - Toll Free Number: 1-8001629.6364 - Fax: [phone]
Page 3 of 10

"�VuawuronenlrvcFWM1AnalyticalOPR ISM I envi
ronmental Solutio
ns
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147 Sample Matrix: Water
Laboratory Report
09/22/2017
Client Sample ID: SW-1
Prism Sample ID: 7090196-01
Prism Work Order: 7090196
Time Collected: 09/12/17 07:15
Time Submitted: 09/13/17 16:40
Parameter Result
Units
Report MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.20
mg/L
0.10 0.0024
1
'SM4600-NO3 F 9/16/17 8:37
CLB
P710205
Volatile Organic Compounds by GC/MS
1,2.Dichloroethane 0.0022
mg/L
0.00060 0.000066
1
'82608 9/15117 15:01
KDM
P710232
Toluene BRL
mg/L
0.00050 0000044
1
'8260B 9/15/17 1501
KDM
P710232
Surrogate
Recovery
Control Limits
4-Bmmofluorobenzene
102 %
80-124
Dibromofluoromethane
99 %
75-129
Toluene-d8
97 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: l-8001529-6364-Fax: [phone] Page 4 Df 10

�.\ Laboratory Report
PRISM I Full-ServiceEnvironmental
Analytical 8
Environmental Solutions 09/22/2017
�--y/wdurowr8 INC
Akzo Nobel Project: SW Samples Client Sample ID: SW-2
Attn: David Simons Prism Sample ID: 7090196-02
485 Cedar Springs Road Prism Work Order: 7090196
Salisbury, NC 28147 Sample Matrix: Water Time Collected: 09/12/17 07:19
Time Submitted: 09/13/17 16:40
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
NitratelNitrite as N 0.36
mg/L
0.10 0.0024 1
*SM4600-NO3 F 9/15/17 8:37
CLB
P710205
Volatile Organic Compounds by GC/MS
1,2-Dichloroethane 0.0046
ni
0.00060 0.000066 1
x8260e 9116117 15:27
KDM
P710232
Toluene BRL
mg/L
0.00050 0.000044 1
'8260B 9115117 15:27
KDM
P710232
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene 105 % 80-124
Dibromofluoromethane 99 % 75.129
Toluene-d8 99 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 5 of 10

1
� Full -Service Analylical8
llP'R I S M I Environmental Solutions
Akzo Nobel
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Parameter Result
Laboratory Report
09/22/2017
Project: SW Samples Client Sample ID: SW-3
Prism Sample ID: 7090196-03
Prism Work Order: 7090196
Sample Matrix: Water Time Collected: 09/12/17 07:20
Time Submitted: 09/13/17 16:40
Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
NitratoiNitdte as N 0.26
mg/L
0.10
0.0024
1
'SM4500-NO3 F 9116117 8:37
CLS
P710205
Volatile Organic Compounds by GC/MS
1,2.Dichloroethane 0.0016
mg/L
0.00050
0.000066
1
'826013 9/16/17 15:52
KDM
P710232
Toluene 0.00091
mg/L
0.00050
0.0000"
1
'826013 9116/17 15:62
KDM
P710232
surrogate
Rewvery
Control Limits
4-Bromofluorobenzene
102 %
80-124
Dibromofluoromethane
102 %
75129
Toluene-d8
97 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: 704IS296364 - Toll Free Number: 1.8001629-6364 - Fax: [phone] Page 6 of 10

P� a
Environmental Solutions
QptR I S M I Fun-Servloe al Solutions
�Jueauroxite sec
Laboratory Report
09/22/2017
Akzo Nobel Project: SW Samples
Client Sample ID: SW-4
Attn: David Simons
Prism Sample ID: 7090196-04
485 Cedar Springs Road
Prism Work Order: 7090196
Salisbury, NC 28147 Sample Matrix: Water
Time Collected: 09/12/17 07:25
Time Submitted: 09/13/17 16:40
Parameter
Result
Units
Report
MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
Nitrate/Nitrite as N
BRL
mg/L
0.10
0.0024
1
'SM4500-NO3 F 9/15/17 8:37 CLB
P710205
Volatile Organic Compounds by GC/MS
1,2-Dichloroethane
BRL
mg/L
0.00050
0.000066
1
*82606 9/15117 16:18 KDM
P710232
Toluene
BRL
mg/L
0.00050
0,000044
1
'8260B 9/15/17 16:18 KDM
P710232
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
80-124
Dibromofluoramelhane
100 %
75-129
Tolueri
99 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-8001629-6364-Fax: [phone] Page 7 Df 10

\ FulkService Analytical &
Environmental Solutions
Level II QC Report
9/22/17
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Volatile Organic Compounds by GC/MS - Quality Control
Reporting
Analyte Result Limit Units
Batch P710232 - 6030B
Prism Work Order: 7090196
Time Submitted: 9/13/2017 4:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P710232-BLK1)
Prepared &
Analyzed:
09/15/17
1,2-Dichloroethane
BRL
0.00050
mg/L
Toluene
BRL
0.00050
mg/L
Surrogate: 4-Bromofluorobenzene
49.7
ug/L
50.00
99
80-124
Surrogate: Dibromofluoromethane
48.5
ug/L
50.00
97
75-129
Surrogate: Toluene-d8
477
ug/L
5000
95
77-123
LCS (P710232-BSI)
Prepared &
Analyzed:
09/15/17
1,2-Dichloroethane
0.0210
0.00050
mg/L
0.02000
105
68-131
Toluene
0.0221
0.00050
mg/L
0.02000
110
76-131
Surrogate: 4-Bromolluorobenzene
50A
U91L
50.00
101
80-124
Surrogate: Dibromolluoromethane
49.4
U91L
$0.00
99
75.129
Surrogate: Toluene-d8
49.1
ug/L
50.00
98
77-123
LCS Dup (P710232-BSD1)
Prepared &
Analyzed:
09/15/17
1,2-Dichloroethane
0.0213
0.00050
mg/L
0.02000
107
68-131 2 20
Toluene
0.0221
0.00050
mg/L
0,02000
110
76-131 0.1 20
Surrogate: 4-Bromolluorobenzene
49.5
U91L
50.00
99
80-124
Surrogate: Dibromofluoromethane
49.2
ug/L
50.00
98
75129
Surrogate: Toluene-d8
48.5
ug/L
50.00
97
77423
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: 1-80015296364 - Fax: [phone] Page 8 of 10

P R I S M Full -Service Analytical 8
Environmental Solutions
An—'�b..awaoai.e i.c
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
General Chemistry Parameters - Quality Control
Level II QC Report
9/22117
Prism Work Order: 7090196
Time Submitted: 9/13/2017 4:40:00PM
Reporting Spike Source %REC RPD
Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P710205 - NO PREP
Blank (P710205-BLK1) Prepared: 09/14/17 Analyzed: 09/15/17
Nitrate/Nitrite as N BRL 0.10 mg/L
LCS (P710205-BS1) Prepared: 09/14/17 Analyzed: 09/15/17
Nitrate/Nitdte as N 1.02 0.10 mg/L 1.000 102 90-110
Prep Method: 5030E
Lab Number
7090196-01
7090196-02
7090196-03
7090196-04
Sample Extraction Data
Batch Initial Final DateTme
P710232
10
mL
10 mL
09/15/17 1023
P710232
10
mL
10 mL
09/15117 10.23
P710232
10
mL
10 mL
09/15/17 10:23
P710232
10
mL
10 mL
09/15/17 10:23
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 9 of 10

.:.:. .... ::::.: . ..
Full -Service Analytical A
Environmental Solutions
Jwm'_J=M��reBORATOSIE& INC
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] • Fax: [phone]f409
Client Company Name: 1`f«2c� a D2.r
Report To/Contact Name: ,:L
Re rting Address:
�:I �b-1.ter
CHAIN OF CUSTODY RECORD
PAGE-1 OF 1 QUOTE R TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
provisions and/or QC Requirements
Invoice To:
Atldress:
Phone—;21J n Z—bT_3'
Fax (Yes) (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date 1 Day ❑ 2 Days ❑ 3 Days O 4 Days ❑ 5 Days
Certification: NELAC_ DOD_
FL_ NC_
EDD Type: POF_Excel_Other
�❑
"Working Days" Y 6-9 Days O Standard 10 days ❑Ruh Work
dust BePre-
Sc OTHER
NIA
Site Location Name:
Samples received after 14:00 volt be processed next business day.
Turnaround time is based on business days, excluding weekends and holiday);,
Water Chlorinated: YES_ NO
Site Location Physical
Address:
(SEE REVERSE FOR TERMS a CONDITIONS REGARDING SERVICES ���
Sample Iced Upon Collection: YES
P P
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I
—
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
No .ITi ALYSIS REQUESTED
N
REMARKS
PRISM
LAB
•TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
+l' r
O C'
ID NO.
HOURS
SLUDGE)
SEE BELOW
,
G✓ I
d /7
DOah
SU�
sk
�i
_
01-
3
o72—o
5
L
x
03
//7Z0
`3da h
s�W
iC
03
!7/ 4-1d-72,
��
1
rBBjr�
�50y
�
1
Affiliation
Sampler's Signature
Sampled By (Print Name)
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in w ' '
he Prism Projec There will be cIiarges for any changes after analyses have been initialized. '
elinquls amre)
ece y: ignatura Deto Military/Hours additional Comments:
SIteARIV3l Time
(� ��r'l
SiteOeparturcTimeech
y: ( g Nre)
=Rfg!nq�hW
R - tl B . gnature)lb-
Feay:
(sgnature
Received For Prysmj b Dries I! Date 1 G I
r
Method of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT Vol S�UUSS ODY ..L.FOR TRANSPORTgnON TO TXE LABORATORY. CDC Group No.
THE LABORATORY.
JL4 ia•DG
SAMPLES
ARE N ACCEPTED AND VERIFIED
AGAINST COC=LRECENED AT t
701^4l yi
_ _
Fed Ex ❑ UPS ❑ Hand-defiNred
/hIkI�1•
m ❑ other . p
Ferve
NPDES: I UST:
G DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: N
❑NC❑SC ❑NC ❑SC NC OSC ZINC
1
❑SC ❑NC ❑SC ❑NC❑SC ❑NC ❑SC ❑NC El SC CI NC ❑SC
n n
❑ ❑
❑ ❑ ❑ O ❑
'CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS- 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME AkzoNobel Surface Chemistry LLC COUNTY Rowan
PERSON COLLECTING SAMPLE(S) Rick Evans Traci S loEIVED
op
PHONE NO. [phone]
CERTIFIED LABORATORY(S) Prism Laboratories Inc. Lab # 3773
PEC
Lab # 402 MAR 0 2 2017
SIGNATURE OF PERMITTEE OR DESIGNEE
Part A: Specific Monitoring Requirements CENTRAL FILES REQUIRED ON PAGE 2.DWR SECTION
Outfall
No.
Date
Sample
Collected
50050
Total
Flow ifa
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plusNO3
pH
mo/dd/ r
MG
inches
m /L
m /L
m /L
SIU
SW-1
02/15/2017
.28
0.037
<0.00050
0.28
6.40
SW-2
02/15/2017
.28
.0025
0.0019
.18
7.03
SW-3
02/15/2017
.28
<0.00050
0.00064
0.90
6.74
SW-4
02/15/2017
No Flow
No Flow
No Flow
No Flow
No Flow
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Act ivit Moni[orin Re uirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
a 1.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m /I
m /I
unit
gal/mo
Form SWU-247, last revised 2121201
Pagel of 2

��
.x
.
,..
_
..
;..
_
_
:.

STORM EVENT CHARACTERISTICS:
Date 02/15/2017
Total Event Precipitation (inches): .28
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Permittee)
0310! t201
(Date)
Form S WU-247, last revised 212120l
Page 2 of 2

QQUBOMToalE9 iXG
Akzo Nobel
David Simons
485 Cedar Springs Road
Salisbury, NC 28147
NC Certifiration No. 402
.Full -Service Analytical 8 NC Drinking Water Can No. 37735
Environmental Solutions SC Certification No, 99012
Project: SW Samples
Lab Submittal Date: 02/15/2017
Prism Work Order: 7020300
Case Narrative
02/27/2017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results. and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
0, AN � M a/ - I , E
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Reviewed By Terri W. Cole
Project Manager
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number.l-0001529-6364- Fax: [phone] Page 1 of 9

FW Analytical 6Rr�I SVI Environmental
Sotuiw®ixc
Sample Receipt Summary
02/27/2017
Prism Work Order: 7020300
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
SW-1 7020300-01 Water 02/15/17 02/15/17
SW-2 7020300-02 Water 02/15/17 02/15/17
SW-3 70203OG-03 Water 02/15/17 02/15/17
Samples were received in good condition at 0.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0643
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 2 of 9

i
LIu�I�.a I S M I Full Service Analyeul4
r Environmental Solutlona
Summary of Detections
02/27/2017
Prism Work Order: 7020300
Prism 10
Client ID
Parameter
Method
Result
Units
7020300-01
SW-1
Nitrate/Nitrite as N
'SM4500-NO3 F
0.28
mg/L
7020300-01
SW-1
1,2-Dichloroethane
'8260B
0.037
mg/L
7020300-02
SW-2
Nitrate/Nitrite as N
'SM4500-NO3 F
0.18
mg/L
7020300-02
SW-2
1,2-Dichloroethane
'8260B
0.0025
mg/L
7020300-02
SW-2
Toluene
'82608
0.0019
mg/L
7020300-03
SW-3
Nitrate/Nitrite as N
'SM4500-NO3 F
0.90
mg/L
7020300-03
SW-3
Toluene
'8260B
0.00064
mg/L
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 Spdngbmok Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1.8001529.6364 - Fax: [phone]
Page 3 Of 971

Fu. tical6LP-,RISM6vronmental Solutions
�wem.mwq�xc
Laboratory Report
02/27/2017
Akzo Nobel
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Project: SW Samples Client Sample ID: SW-1
Prism Sample ID: 7020300-01
Prism Work Order: 7020300
Sample Matrix: Water Time Collected: 02115/17 10:00
Time Submitted: 02/15/17 16:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daternme ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.28
mg/L
0.10 0.0024
1 'SM4500-NO3 F 2/22117 10:18
CLB P7130398
Volatile Organic Compounds by GC/MS
1,2-Dlchloroethane 0.037
mg/L
0.00060 0.000066
1 '8260B 2/22/17 19:13
KDM P780425
Toluene BRL
mg/L
0.00050 0.000044
1 '82608 2/22/17 19:13
KDM P780425
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
91 %
80-124
Dibromofluoromethane
90 %
75-129
Toluene-d6
88 %
77-123
This report should not be reproduced, except in its entirety, without the written consent or Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1.800/529-6364 - Fax: [phone] Page 4 of 9

LbL�QR-pVi
Fall-ServloaAnmlhlcal a
Laboratory Report
��
Environmental Solutions
02/27/2017
Akzo Nobel
Project: SW Samples
Client Sample ID: SW-2
Attm David Simons
Prism Sample ID: 7020300-02
485 Cedar Springs Road
Prism Work Order: 7020300
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: 02/15/17 10:05
Time Submitted: 02/15/17 16:20
Parameter
Result Units Report
MOIL Dilution Method Analysis Analyst Balch
Limit
Factor Dale/Time ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.18
mglL
0.10 0.0024
1 'SM4500-NO3 F 2/22117 10:18
CLB P780398
Volatile Organic Compounds by GC/MS
1,2-Dichlomethane 0.0025
mg/L
0.00050 0.000066
1 '82608 2/22/17 20:05
KOM P7150425
Toluene 0.0019
mg/L
0.00050 0.0000"
1 '8260B 2122117 20:05
KOM P7130425
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene 90 % 80-124
Dibromofluoromethane 89 % 75-129
Toluene -de 88 % 77-123
This report should not be reproduced, except in its entirely, without the written consent at Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1.8001529-6364 - Fax: [phone]
Page 5 of 9

lP R I S IVi I Fuvirorn loe Af W ludo a
J L� L EnNronmenfol aoluflone
umea 'ma
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147 Sample Matrix: Water
Laboratory Report
02/27/2017
Client Sample ID: SW-3
Prism Sample ID: 7020300-03
Prism Work Order: 7020300
Time Collected: 02/15/17 10:08
Time Submitted: 02/15/17 16:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.90
mg/L
0.10
0.0024
1 'SM4500-NO3 F 2122/17 10:18
CLB
P7B0398
Volatile Organic Compounds by GC/MS
1,2-Dichloroethane BRL
mg/L
0.00050
0.000066
1 '82606 2/22/17 20:57,
KDM
P7B0425
Toluene 0.00064
mg/L
0.00050
0.000044
1 '8260B 2/22117 20:57
KDM
P780425
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
91 %
80-124
Dibromofluoromethane
91 %
75-129
Toluene-08
89 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboralanes, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: IA001529-6364 - Fax: [phone] Page 6 of 9

\ 1
�P1 L- I `- n n I Full-Servim al Solutions
s
ru J'v' Enviranmontol 5olunana
..so
so
Level II QC Report
2/27117
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Volatile Organic Compounds by GC/MS - Quality Control
Reporting
Result Limit Units
Batch P7B0425-5030B•
Prism Work Order: 7020300
Time Submitted: 2/15/2017 4:20:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P7130425-131-1(1)
Prepared & Analyzed: 02/22/17
1,2-Dichloroeth2ne
BRL
0.00050
mg/ -
Toluene
BRL
0.00050
mg/L
Surrogate: 4-Bmmofluombenzene
44.1
ugh
50.00 88
80-124
Sumgate: Dibmmo8uoromethane
45.0
ugh
50.00 90
75-129
Surrogate: Toluene-o8
43.3
ugh
50.00 87
77-123
LCS (P7B0425-BS1)
Prepared & Analyzed: 02/22/17
1,2-Dichlaroethene
0.0198
0.00050
mg/L
0.02000 99
68-131
Toluene
0.0202
0.00050
mgtL
0.02000 101
76-131
Surrogate: 4-11romeBuombenzene
45.4
ugh
50.00 91
80-124
Surrogate: Dibromofluommethane
46.0
ugh
50.00 92
75-129
Surmgate: Toluene-d8
45.2
ug/L
5000 90
77-123
LCS Cup (P780425-BSD1)
Prepared & Analyzed: 02/22/17
1,2-Dichlcmethane
0.0193
0.00050
mg/L
0.02000 96
68-131 3 20
Toluene
0.0197
0.00050
mg/L
0.02000 98
76-131 2 20
Surrogate: 4-6romofluombenzene
44.8
ugh
50,00 90
80424
Surrogate: Dibmmo8uoromethane
4&2
ugtL
50.00 90
75-129
Surmgate: Toluene-d8
44.3
ugh
50.00 89
77-123
This report should not be reproduced, except in its entirety, without the wntten consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
'Phone: [phone] - Toll Free Number: 141001629-6364 - Fax: [phone]
Page 7 of 9

LOP,
I S M I Funironmea ArW tutu e
Environmental 9alutionx
u tic
Level II QC Report
2/27117
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
General Chemistry Parameters - Quality Control
Prism Work Order: 7020300
Time Submitted: 2/15/2017 4:20:0013M
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P780398 - NO PREP
Blank (P7B0398-BLK1) Prepared & Analyzed: 02/22/17
Nitrate/Nitrite as N BRL 0.10 mg/L
LCS (P7B0398-BS1) Prepared & Analyzed: 02/22/17
Nitrate/Nitfie as N 1.00 0.10 mg/L 1.000 100 90-110
Sample Extraction Data
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/rime
7020300-01
P780425
10 mL
10 mL
02/22/17 8:52
7020300-02
P7B0425
10 mL
10 mL
02/22t17 8:52
7020300-03
P7B0425
10 mL
10 mL
02/22/17 8:52
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 Sprfngbmok Road - P.O. Box 240543 -Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone]
Page 8 of 9

Li e
P3:ISM
'TuWRA10 Ea MG
Full -Service Analytical & CHAIN OF CUSTODY RECORD
Environmental Solutions PAGE L OF 4 QUOTE a TO ENSURE PROPER BILLING:
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone: [phone] • Fax: [phone]
Client Company Name: A /<Z U /y 0;R L: L
Report To/Contact Name: DAV 0 .S/ /A 0 A/ i
Reporting Address: 45'.S 1_'Z_Q J? :5n, R 114 45 l2n,
3AL/SA,JPv iC_ 2fi/-/7
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
`Please ATTACH any project specific reporting (OC LEVEL 1 II III IV)
provisions and/or OC Requirements
Invoice To:
Address:
1. „—,
Email (Yes) (No) Email Address
Purchase Order NoJBilling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
EDD Type: PDF✓✓Ezcel_Other
Requested Due Date rj ❑ El Day ❑ 2 Days 3 Days 4 Days ❑ 5 Days
Certification: NELAC_ USACE_
FL NC_
"Working Days" 301 Days ❑ Standard 10 days p Rush Work Must Be
_
Site Location Name:
A r
Samples received after 15:00 will be processed next business Prep oved
SC_ OTHER
N/A
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONOMONS REGARDING REND RED BY PRISM LABORATORIES INC. TO CLIENT)RWC� /
Sample Iced Upon Collection: YES
_ NO _
TIME
MATRIX
SAMPLE CONTAINER
f LYSES REQUESTED
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
/�-� 4r .
PRISM
'TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
v JY
REMARKS
LAB
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
�� 0 ,�U
10 NO.
1.5
—_P
5PP_ML-
�fz Lt%
1.7 1
WtL
i
t'
SyU- Z
/vps
l
SO q
—
—
G
s/peg
00/uL.
JJASPf
_
D'
Is
Sampler's Signature 4- %1 _ Sampled By
(Print Neil C v Affiliation 20 G
Upon relinquishing. this Chain of Custody is your authorization for
Priam to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be harges
for any changes after analyses have been initialized.
Ra'r'4° "a^Re) R
rasgea oate_/
Mllwy/ Additional Comments:
Sna Amvel:7lme f '
Rell Slgnawr _
y:(Sgnalurs) Data
8240 - Ri N
Ste Departure Time ".
Re s By: (51g c) - R
Prism laboratotles By:
I OUP. >G/`aF tl'
FBItlrTech F6e aa) y�r
Da
.N. ..t:..'........a..... _.
L jS /7
Dili
RE'tN�
Mileage 'r
McNod ai Shlpmenl: NOTE: ALLSAMPLE COOLERS SH ULO BE TAPED SHUr WRH CU ODY SEALS FOR TRANS RTATKIN TO THE LABORATORY. roue No.
SAMPLESARENOTA EKED AND VERIFIED AGAINST OOC U
L RECEIVED AT THE LABORATORY.
D Fed Es D UPS 7 HandEeOvewd f,.dsm FIeU Service D Olher
NPDES: UST: GR UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
UNC ❑SCIpNC ❑SC UNC ❑SC ❑NC ❑SC
❑NC ❑SC ❑NC pSC UNC ❑SC ❑NC ❑SC ❑NC ❑SC
❑ —_J ❑ U ❑ ___
❑ ❑ ❑ n n
_
_ - -
'CONTAINER TYPE CODES: A = Amber C = Clear G = Glass. P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

C-47
Glycotech
2271 Andrew Jackson Hwy, NE
PO Box 1956
Leland, N.C. 28451
910-371-2234
November 16, 2016
Central riles
RECEIVED
Division of Water Quality
l� �E®
1617 Mail Service Center
NOV 2 2 2016
Raleigh, N.C. 27699-1617
CENTRAL FILES
DWR SECTION
Subject: Fall 2016 Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc., under permit 4NCS000258 has performed the Fall qualitative
monitoring of the designated point source discharge Outfall 002. Under this permit,
Glycotech; Inc. is required to perform storm water sampling and subsequent analytical
testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD was
92 mg/L, versus the benchmark value of 120. The pH was 5.8, with a recorded Rain -gage
pH of 5.7, therefore the benchmark values of 6.0 to 9.0 do not apply (per the permit).
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
Billy King
General Man ger
Glycotech, Inc.
CC:
Gary Wooten — EHS Manager- Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS (DOG Z S O or
Certificate of Coverage Number: NCG /J�A
FACILITY NAME a LYCOT eco _TKC
PERSON COLLECTING SAMPLE(S) Y oe'f Ems!
CERTIFIEDLABORATORY(S) 671vyi2oCi4FM Lab#
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: ZG/�
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
/S COUNTY IC✓NSLLj/C/
PHONE NO. /O 37/-2Z34
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
• .
11WM.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes 1�no
(if yes, complete Part B)
Dart • Vehirla Ma ntnnan a Activity Mnnitnrinn Rrmdm reentc N/^^ A
R
Outfall
50050
00556
00530
00400
No.
Lmo/dd
Total Flow
(if applicable)
Total Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
a 1.
Total
Suspended
Solids
pH
New Motor Oil
Usage
MG
inches
mg/1
m /t
Units
al/mo
Form SWU-246, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date qL16
L116
Total Event Precipitation (inches): 2,41
Event Duration (hours): -44- (only if applicable —see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
-Mail Original and one copy to: -
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
111)41),(0
(Date
Form S W U-246, last revised 21212012
Page 2 of 2

NOV 2 2 2016
^n CENTRAL FILES
MCONEMR DWR SECTION
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: htro://Portal.ncdenr.or2/web/wci/ws/su/npdessw#tab-4
Permit No.: N/C/S7O/D/0/ 2/_S_7/
Facility Name: /J C LVV &-" Cu j 2
County: APotus co r ck
Inspector: a-ra
Date of Inspection: 9 / 19 t
or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Time of Inspection: a0 t 00 PAA
Total Event Precipitation (inches): 2 • `//
No. cl10-37/-
Was this a Representative Storm Event? (See information below) X Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By�� gnaq{re, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Perm4tee or Designee)
1. Outfall Description:
Outfall No. 002 A Structure ( ipe, ditch, etc.) Q 1TCt�
Receiving Stream: __ 4"1 f2A?b2 1Z tyCH CAP,-c Films l,10Z 8A S/Aj
Describe the industrial activities that occur within the outfall drainage area:
ORGA-,c C1.irnMtCAc M/�na�F�LTU(it11�T
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: TAKimi e- Rigowt l
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): NONE
Page I of 2
S W U-242-20120613

4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy: ������
/ I J 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
D 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is n�o� solids and 5 is extremely muddy:
is
( I ") 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes G
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may
be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-20120613

ANALYTICAL & CONSULTING CHEMISTS
Glycotech, Inc.
PO Box 1956
Leland NC 28451
Attention: Gary Wooten
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
environmentslchemists.com
Date of Report: Sep 28, 2016
Customer PO #: 7293
Customer ID:
Report #:
Project ID:
BIsIKYIIIII) E
2016-13531
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-32913 Site: Outfall 002 9/19/2016 8:00 PM Water Gary Wooten
Test Method Results Date Analyzed
COD SM 5220D 92 mg/L 09/23/2016
Comment: p�
Reviewed by: � 0 r� {Wll--�
Report #:: 2016-13531 Page 1 of 1

<�, x LN V IKUNMLN 1 AL 4,kJMN11b 1 bq ilvU 6602 Windmill Way
2 q Wilmington, NC 28405
Sample Collection and Chain of Custody Phone: [phone]
Fax [phone]
Client: G NYC Ck N 1 N L EMAIL: ELMS aQaol.com
Collected By G ACL, W c crrc— ti Report No: A, / :3 Sa/
m •= Infi wit. E Effluent, W -Well. aSi d -
PRESERVATION
6 � 8 � �
SamCollection pie Identification e a e cc c ANALYSIS REQDESTED
DATE TIIKE TEMP
0L TP/aLL_oO;Z 9 9 ib aooa ,4me ST C cti r. 32 /3 J tyPDEs CO (7
0.2 ppm or less)
Transfer
1.
2.
Temperature when
Delivered By:
Comments: _
UNATION : Samples for Ammonia, TKN, Cyanide, Phenol, and Bacteria must be dechlorinated
field at the time of collection. See reverie side for instructions.
Relinquished By:, Date/Time j Aecejvj By: Date/Time
Aved: , 'Accepted: V Reje a pie Requested:
Received B,y: Date: =y! Time:

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number'NCS 000259
FACILITY NAME AkzoNobel Surface Chemistry LLC
PERSON COLLECTING SAMPLE(S) Traci Sloop
CERTIFIED LABORATORY(S) Prism Laboratories Inc. Lab
Lab # 402
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
COUNTY Rowan
PHONE NO. [phone]
RECEIVED
SIGNATURE OF PERMITTEE OR DESIGNEE
NOV 0 1 2016 REQUIRED ON PAGE 2.
CENTRAL FILES
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m L
m /L
m /L
SIU
SW-1
10/07/2016
1.9
0.0020
<0.00050
0.62
7.01
SW-2
10/07/2016
1.9
0.0015
0.035
0.35
7.00
SW-3
10/07/2016
1.9
<0.00050
<0.00050
0.50
7.01
SW-4
10/07/2016
No Flow
No Flow
No Flow
No Flow
No Flow
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/'r
MG
inches
m /I
m I
unit
al/mo
Form SWU-247, last revised 2121201
Page] of 2

STORM EVENT CHARACTERISTICS:
Date 10/07/2016
Total Event Precipitation (inches): 1.9
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possi�ity of fines and imprisonment for knowing violations."
of
(D. te)
Form SWU-247, last revised 2121201
Page 2 of 2

AkzoNobel 485 Cedar Springs Road T+ 1 704 633 1731
Surface Chemistry Unit A F + 1 704 637 8912
Salisbury, INC 28147 w .akzonobel.com/sc
USA
AkzoNobel
Tomorrow's Answers Today
February 4, 2016
NCDENR — Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Certified Mail: Return Receipt Requested
52016
DWR rRALT��S
Reference: Semi -Annual Permit Monitoring Report
Individual Stormwater Monitoring Permit
AkzoNobel Surface Chemistry LLC.
Permit No. NCS000259
Attached are two copies of the AkzoNobel monitoring results for the period
of January 1, 2016 to June 30, 2016 for our permit # NCS000259 for the
samples collected January 15, 2016. Any questions on this submittal you
may contact me at 704-642-6203.
Regards,
David Simons
HSES Manager
AkzoNobel Surface Chemistry, LLC, Salisbury, NC
Copy: Brian Owen AkzoNobel Surface Chemistry, LLC, Salisbury,
NC
Christopher Fleming AkzoNobel Surface Chemistry, LLC,
Salisbury, NC

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME AkzoNobel Surface Chemistry LLC COUNTY Rowan
PERSON COLLECTING SAMPLE(S) Lvvn White, Traci Sloop PHONE NO. [phone]
CERTIFIED LABORATORY(S) Prism Laboratories Inc. Lab # 37735
Lab # 402
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements -
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m /L
m /L
m /L
SIU
SW-1
01/15/2016
.2
0.031
<0.00050
0.58
6.53
SW-2
01/15/2016
.2
<0.00050
0.0057
5.7
1 6.34
SW-3
01/IS/2016
.2
<0.00050
0.0012
0.30
6.76
SW-4
01/15/2016
No Flow
No Flow
No Flow
No Flow
No Flow
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m /I
m /I
unit
galtmo
-�r
Form SWU-247, last revised 2121201
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date O1/15/2016
Total Event Precipitation (inches): .2
Event Duration (hours): (only ifapplicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable— see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibiK of fines and imprisonment for knowing violations."
(Signature of
�9
(Dat )
Form SWU-247, last revised 2121201
Page 2 of 2

d§'E-'
hAppp nIS ,1 Full -Service Analytical&
' IEnvironmental Solutions
�DinmanroaNs, irc
Akzo Nobel
David Simons
485 Cedar Springs Road
Salisbury, NC 28147
NC Certificeuon No. 402
SC Certification No. 99012
NC Ddnkinq Water Cert No. 37735
VA Certmcadon No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: SW Samples
Lab Submittal Date: 01/18/2016
Prism Work Order: 6010289
Case Narrative
01 /27/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
0
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Reviewed By Terri W. Cole
Project Manager
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 29224-0543
Phone: [phone]- Toll Free Number.. 1-800/5294364 - Fax: [phone] E Page 1 of9

fice
FaGP RI S M I Environmental Solutions TW 11.
Sample Receipt Summary
01/27/2016
Prism Work Order: 6010289
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
SW-1 6010289-01 Water 01/15/16 01/18/16
SW-2 6010289-02 Water 01/15/16 01/18/16
SW-3 6010289-03 Water 01/15/16 01/18/16
Samples were received in good condition at 2.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its en0rety, without the written censent of Prism Laboratories, Inc.
449 Sprinpbruok Road - P.O. Box 240540 - Charlotte, NC 28224-0543
Phone: 7MIS29-6064 - Toll Free Number. 1.8001529E064 - Fax: [phone]
Page 2 of 9

Summary of Detections
PR
0 I S � %� III Fnvinon lce
l Solutions
ru 'V' Envlronmentel SoiWlona
,Ir La
ueoxnoneaixc
01/27/2016
Prism Work Order: 6010289
Prism ID Client ID
Parameter
Method Result Units
6010289-01 SW-1
Nitrate/Nitrite as N
'SM45o0-NO3 F 0.58 mg/L
6010289-01 SW-1
1,2-Dichloroethane
'8260B 0.031 mg/L
6010289-02 SW-2
Nitrate/Nitrite as N
'SM4500-NO3 F 5.7 mg/L
6010289-02 SW-2
Toluene
*82608 0.0057 mg/L
6010289-03 SW-3
Nitrate/Nitrite a6 N
'SM4500-NO3 F 0.30 mg/L
6010289-03 SW-3
Toluene
•8260B 0.0012 mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number...1-800/5296364- Fax: [phone] CPage3of9

Laboratory Report
IQ {� %� I PulSolutioaJ'
LE§P'=—,�"hp
V' Envlronmentel Solutions
u ixa
01/27/2016
Akzo Nobel
Project: SW Samples
Client Sample ID: SW-1
Attn: David Simons
Prism Sample ID: 6010289-01
485 Cedar Springs Road
Prism Work Order: 6010289
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: O1/15/16 13:20
Time Submitted: 01/18/16 17:20
Parameter Result
Units
Report MOIL
Dilution Method Analysis Analyst Batch
Limit
Factor Date7Time ID
General Chemistry Parameters
NltratelNltrite as N 0.58
mglL
0.10 0.0012
1 'SM4500-NO3 F 1121116 11:49 CLB PSA0306
Volatile Organic Compounds by GCIMS
1,2-Dichlomethane 0.031
mg/L
0.00050 0.000066
1 '82608 1126116 15:39 KDM P6A0390
Toluene BRL
nri
D.D0050 0.000D44
1 '8260B 4126/16 15:39 KDM P6A0390
Surrogate
Recovery Control Limits
4-Bromafluombenzene
98 % 80-124
Dibromofluoromethane
100 % 75-129
Toluene-d8
97 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OW
Phone: [phone] - Tall Free Number. 1-8001529-6364 - Fax: 7D4/525-0409 Page 4 of 9

GP R I S M I Full-9enrice Analytical 4
9nvhonmenrel Su ical A
Laboratory Report
01/2712016
Akzo Nobel
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Project: SW Samples Client Sample ID: SW-2
Prism Sample ID: 6010289-02
Prism Work Order: 6010289
Sample Matrix: Water Time Collected: 01/15/16 13:25
Time Submitted: 01 /18/16 17:20
Parameter Result Units Report MDL Dilution Method Anatysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Nitrate/Nltrlte as N 5.7 mg/L 2.0 0.024 20 *SM4500-NO3 F 1121/16 11:49 CLS P6A0306
Volatile Organic Compounds by GCIMS
1,2-Dichloroethene BRL mg/L 0.00050 0.000066 1 '8260B 1/26/16 16:13 KDM P6A0390
Toluene 0.0057 mg/L 0.00050 0.000044 1 •82608 1126/16 16:13 KDM P6A0390
Surrogate
Recovery
Control Limits
4-Bromoguombenzene
98 %
80-124
Dibromofluoromethane
98 %
75-129
Toluene-d8
97 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spdngbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] - To Free Number: 140015296364 - Fax: [phone] Page 5 of 9

Laboratory Report
I Q i� ii I rwi-service Amm�mo� n
�I]II J��/� Envlronmentel 5olutlom
imueowq ixC
01/27/2016
Akzo Nobel
Project: SW Samples
Client Sample ID: SW-3
Attn: David Simons
Prism Sample ID: 6010289-03
485 Cedar Springs Road
Prism Work Order: 6010289
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: 01/15/16 13:25
Time Submitted: 01/18/16 17:20
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Daterrime ID
General Chemistry Parameters
NltratelNltdte as N 0.30
mglL
0.10 0.0012
1 'SM4500-NO3 F 1121116 11:49 CLS P6A0306
Volatile Organic Compounds by GCIMS
1,2-Dichloroethane BRL
mg/L
0.00050 0.000066
1 '8260B 1/26/16 16:48 KOM P6A0390
Toluene 0.0012
mg/L
0.00050 0.0000"
1 '82608 1126/16 16:48 KDM P6A0390
surrogate
Recovery Control Limits
4-Bromofluorobenzene
98 % 80-124
Dibromofluoromethane
100 % 75-129
Toluene-d8
98 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 282244543 r
Phone: [phone] -Toll Free Number: 14100/529.6364 - Fax: [phone] Page 6 of 9

/A R I I� �I I Full -Service Analytical 6
ru ' V' Envlronmontal Solutions
Level II QC Report
1127/16
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P6A0390-5030B
Reporting
Result Limit Units
Prism Work Order: 6010289
Time Submitted: 1/18/2016 5:20:o0PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P6A0390-BLK1)
Prepared & Analyzed: 01/26/16
1,2-Dichloroethane
BRL
0,00050
mg/L
Toluene
BRL
0.00050
ni
Surrogate: 4-Bromofluorobenzene
49.6
ug'L
50.00 99
80-124
Surmgate: Dibmmolluommethene
49.4
ugA-
50,00 99
75-129
Sunugate: Toluene -de
48,8
ug/L
50,00 98
77-123
LCS (P6A0390-BS1)
Prepared & Analyzed: 01/26/16
1,2-Dichloroethane
0.0207
0.00050
mg/L
0.02000 104
68-131
Toluene
0.0207
0.00050
mg/L
0.02000 103
76-131
Surrogate: 4-Bromolluorobenzene
47.9
ugA
60.00 96
80-124
Surmgate: Dibromofluoromethane
50.9
ug/L
5000 102
75-129
Surmgate: Toluene-d8
48.3
ug/L
50.00 97
77-123
LCS Oup (P6A0390-BSD1)
Prepared & Analyzed: 01/26/16
1,2-Dichloroethane
0.0200
0.00050
mg/L
0.02000 100
68-131 3 20
Toluene
0.0198
0.00050
mg/L
0.02000 99
76-131 5 20
Surrogate: 4-Bromofluorobenzene
48.2
ug/L
50,00 96
80-124
Surrogate: Dibromofluoromethane
49.4
ug/L
50.00 99
75-129
Surrogate: Toluene-18
4&5
ugQ
50.00 97
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Labormones, Inc.
449 Spdngbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] r Page7of9

A
i a ' S p %� I E=1rc service Analy teal a
_ l-�monxme.�c Emlronmentel 9olWlana
Level II QC Report
1/27/16
Akzo Nobel Project: SW Samples Prism Work Order: 6010289
Attn: David Simons Time Submitted: 1/18/2016 5:20:OOPM
485 Cedar Springs Road
Salisbury, NC 28147
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analme Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6A0306 - NO PREP
Blank (KA0306.81-K7) Prepared 8 Analyzed: 01/21/16
Nitrate/Nitrite as BRL 0.10 mg/L
LCS (P6A0306-BS1) Prepared 8 Analyzed: 01/21/16
Nitrate/Nitrite as N 0.998 0.10 mg/L 1.000 100 90-110
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Initial Final Daternme
6010209-01 P6A0390 10 mL 10 mL 01/26/16 8:57
6010269-02 P6A0390 10 mL 10 mL 01/26/16 8:57
6010289-03 P6A0390 10 mL 10 mL 01/26/16 8:57
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spdngbrook Road - P.O. Box 240643 - Charlotte, NC 2822"563
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: 704152"409 Page 8 of 9

5
j CHAIN OF CUSTODY RE 0 D
ft n I C n Full -Service Analytical
yy, ki ism Environmental Solutionss PAGE OF L QUOTE A To ENSURE PROPER BILLING: gamplee INTAI
LAROPATORIEC INC 7o uuil'r1N n
449 Springbrook Road • Charlotte, NC 28217
Phone [phone]A •Fax: [phone]
Client Company Name:
Report To/Contact Name: I,17✓4 m.n�.ti
Reporting Address: ''i�:4 `- 5s
[ (74 1U.C.: d,$/q17
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
`Please ATTACH any project specific reporting (OC LEVEL 1 II III IV)
provisions and/or OC Requirements
Invoice To:
Address:
Phone: 2- Ar"37Fax (Yes) (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BYCLIENT/SAMPLING PERSONNEL
Email Address: � ��// _Other
EDD Type: PDF�Gcacel
Site Location Name:
Site Location Physical Address:
Requested Due Date O 1 ❑ 2 Days ❑ 3 Days El Days Cl5 Days
"Working Days O Standard 10 days O Rush Pro-Approvedrk Must Be
Days" 9
Samples recelved after 14:Do will be processed next business day.
Tumamund time is based on business days, excluding weekends and holidays.
(SEE REVERSE FOR TERMS 4 CONDITIONS REGARDINGSERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Certification: NELAC_ DOD_
SC OTHER
Water Chlorinated: YES_ NO_
Sample IcedU on Collection: YES_
P P
FL_ NC_
NIA
NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA.
TIVES
-k j,�P IN
Ly
y
.
SIB REQUESTED
REMARKS
PRISM
LAB
ID NO.
-TYPE
SEE BELOW
NO
SIZE
5 w-
I) $ I Le
11 zb
rp0 ai
50
x
OL
/ZJ
S li✓� 3
l�
I
Svr7.J>
�{2Se
3C
�
<< �L
Sampler's Signature
Sampled By (Print Name) _7igpS/.oci o Affiliation A 2. U / fz�w=
Upon relinquishing, s C of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
.
eliNd y: (s 9newra Re ¢ (s19Rawre a - Milttary/Roan gddhiona Comments:
�l o �zun
e nrpua . is W.) R i9nswre) Dare w
/! _ �o/Ar f A'i
RelirrWl y. (Siglelura) R ar Prism la ! V Dato �n � It-, �•�Il�fr�
Site Fvnval Time:
-site Depadure Tma
..:
Milea s <+
Meand of SNpmenT NOTE: ALL SAMPLE COOLERSSHOULO BETAPEDSHUT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. cup No.
SAMPLES ARE NDT A/CSEPTED AND VERIFlED AGAINST UNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ]UPS ❑ HaME JHered 4mm FMW ServN» Cloth
TER: I ATER: E.
❑ NC O SC I ElNC ❑ SC ❑ NC ❑ SC ❑ C ❑ SC ❑ NC ❑SCO NC ❑ SC El CERCLANC ❑ SC I O❑ NC F❑ SC El NC ❑ SC
❑ ❑ ❑ d ❑ ❑ ❑
'CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS D0009L or
Certificate of Coverage Number: NCG
FACILITY NAME ZI ock; Co arc
PERSON COLLECTING SAMPLES) E r erg
CERTIFIED LABORATORY(S) teak t�ti=.� Lab #�D—
Lab #
Part A: Specific Monitoring Requirements
ENV-0106
SAMPLES COLLECTED DURING CALENDAR YEAR: ?Z 16
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY 004_J
PH0. 0 Y' a. 5 O I 0I
(SIGNATU F PERMITTEE OR DESIGNEE)
By this sigt lure, I certify that this report is accurate
complete to the best of my knowledge.
-----------
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes no
(if yes, complete Part B)
Part R- Vehicle Maintenance Activity Monitoring Reouirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total Rainfall
Oil & Grease
Total
Suspended
Solids
pH
New Motor Oil
Usage
mo/dd/ r
MG
inches
m
m
Units
al/o
i✓
N
/i-
!✓ A —
Form SWU-246-112608
Page 1 of 2

ENV-0106
STORM EVENT CHARACTERISTICS:
Date I
Total ve t Precipitation
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my kno ge and belief, true, ccurate, and complete. I am aware that there are significant penalties for submitting false information,
includi the ossibilily of fine a d imprisonment for knowing violations."
64, 4?� 0/
(Signature of Permittee) (Date)
Form SWU-246-112608
Page 2 of 2

Lithium
January 27, 2016
Central Files
Division of Environmental Management
1617 Mail Service Center
Raleigh, NC 27699-1617
RF�'FIVF
RE: Semi -Annual Stormwater Discharge Summary Report (Ouffalls d4 and 00 A)
Rockwood Lithium Inc. FEB .0 5 2016
Kings Mountain, Cleveland County, INC CENTRAL FILESENC
Permit # NCS000096 EN SECTION
Registered Mail 7014 2120 0004 3692 6096 DWR
Dear Sir or Madam:
Please find attached a Semi -Annual Stormwater Discharge Ouffall (SDO) Monitoring Report for
the Rockwood Lithium Inc. facility located in Kings Mountain, North Carolina. This report was
prepared in accordance with the site's General Stormwater Permit effective on November 1,
2009 and covers the Monitoring Period of November 2015 through April 2016.
Please note that due to some problems with our sampling equipment, we were only able to
successfully collect samples from ouffalls 004 and 005A, and accordingly this report does not
include results from our other regulated ouffall (005B). Sampling of this outfall will be conducted
at a later date within the monitoring period, with a separate report to follow.
Based on the sampling results summarized herein, it appears that the site has met its
benchmark goals during the reporting period and will continue to implement appropriate best
management practices to maintain these goals.
Should you have any questions or need additional information related to this data, please
contact John Kuhn at 704-734-2708.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction
or supervision in accordance with a system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowin olations."
Christian M Iler
Site Director
Rockwood Lithium Inc.
348 Holiday Inn Drive
ARDellp �naCanparty Kings Mountain, NC 26086
�Y�^^�'W' �� Phone: [phone]
MYSC ROC www. rockwoodlithino.com

JOR ISM
QOIABORATORIEB, ING
Akzo Nobel
David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Full -Service Analytical &
Environmental Solutions
RECEIVED
NOV 01 2016
CENTRAL FILES
DWR SECTION
NC Certification No. 402
NC Drinking Water Cart No. 37735
SC Certification No. 99012
Project: SW Samples
Case Narrative
10/19/2016
N� abOaSS
Lab Submittal Date:10/11/2016
Prism Work Order: 6100219
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.,
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Terri W. Cole
Project Manager
Data Qualifiers Key Reference
Reviewed By Terri W. Cole
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: t-8001629.6364-Fax: [phone] I Pagel of9

7�
RFo�I-Service Analytical 4
I S M �P Environmental Solutions
,.eaa Rl,INC
Sample Receipt Summary
10/19/2016
Prism Work Order: 6100219
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
SW-1 6100219-01 Water 10/07/16 10/11/16
SW-2 6100219-02 Water 10/07/16 10/11/16
SW-3 6100219-03 Water 10/07/16 10/11/16
Samples were received in good condition at 4.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 2 of 9

P R
I S M
I Fuviron ice 3
al Solution
Environmental Solutions
7 towos
Summary of Detections
10/19/2016
Prism Work Order: 6100219
Prism ID
Client ID
Parameter
Method
Result
Units
6100219-01 '
SW-1
Nitrate/Nitrite as N
'SM4500-NO3 F
0.62
mg/L
6100219-01
SW-1
1,2-Dichloroethane
'6260B
0.0020
mg/L
6100219-02
SW-2
Nitrate/Nitrite as N
'SM4500-NO3 F
0.35
mg/L
6100219-02
SW-2
1,2-Dichloroethane
'8260B
0.0015
mg/L
6100219-02
SW-2
Toluene
'8260B
0.035
mg/L
6100219-03
SW-3
Nitrate/Nitrite as N
'SM4500-NO3 F
0.50
mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: i-8001629-6364-Fax: [phone] Page 3 of 9

��.
Laboratory Report
Sarvica d8
en.oemeelal Solutions
D/,9/2D,6ISM
Akzo Nobel Project: SW Samples
Client Sample ID: SW-1
Attn: David Simons
Prism Sample ID: 6100219-01
485 Cedar Springs Road
Prism Work Order: 6100219
Salisbury, NC 28147 Sample Matrix: Water
Time Collected: 10/07/16 16:00
Time Submitted: 10/11/16 12:44
Parameter Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.62
ri
0.10 0.0012
1 'SM4500-NO3 F 10/14/16 9:44
CLB PSJ0233
Volatile Organic Compounds by GC/MS
1,2-Dichloroethane 0.0020
ri
0.00050 0.000066
1 *82608 10/17/16 116:69
KDM P6J0297
Toluene BRL
mg/L
0.00050 0.000044
1 "8260B 10/17/16 1659
KDM P6J0297
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene 98 % 80-124
Dibromofluoromethane 100 % 75-129
Toluene-d8 99 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone]
Page 4 of 9

'i
Laboratory Report
�PL�tR I S M I on11-Service Analytical8
Evironmental Solutions
10/1 B/2U18
�Juvaurwuea ixc
Akzo Nobel Project: SW Samples
Client Sample ID: SW-2
Attn: David Simons
Prism Sample ID: 6100219-02
485 Cedar Springs Road
Prism Work Order: 6100219
Salisbury, NC 28147 Sample Matrix: Water
Time Collected: 10/07/16 16:10
Time Submitted: 10/11/16 12:41
Parameter Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Datelrime
ID
General Chemistry Parameters
Nitrate/Nitrite as N 0.35
mg/L
0.10
0.0012
1
'SM4600-NO3 F
10/14/16 9:44 CLB
P6J0213
Volatile Organic Compounds by GC/MS
1,2-Dichloroethane 0.0016
mg/L
0.00050
0.000066
1
'8260B
10117/16 17:33 KDM
P6J0297
Toluene 0.036
mg/L
0.00050
0.000044
1
'8260B
10117/16 17:33 KDM
P6J0297
Surrogate
Recovery Control Limits
4-Bromofluorobenzene 100 % 80-124
Dibromofluoromethane 99 % 75-129
Toluene-d8 98 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone]
Page 5 of 9

'
Laboratory Report
An:hAR-Ism I Enviro men Analytical AEnvironmental Solutions
1D/19/2D1B
aumn�rowrn a,c
Akzo Nobel
Project: SW Samples
Client Sample ID: SW-3
Attn: David Simons
Prism Sample ID: 6100219-03
485 Cedar Springs Road
Prism Work Order: 6100219
Salisbury, NC 28147
Sample Matrix: Water
Time Collected: 10/07/16 16:15
Time Submitted: 10/11/16 12:44
Parameter
Result
Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DalelTime ID
General Chemistry Parameters
NitratelNitrite as N
0.50
mg/L
0.10 0.0012
1 'SM4500-NO3 F 10/14/16 9:44 CLB P6J0233
Volatile Organic Compounds by GCIMS
1,2-Dichloroethane
BRL
mg/L
0.00050 0,000066
1 '8260B 10/17/16 1807 KDM P6J0297
Toluene
BRL
mg/L
0.00050 0.000044
1 '8260B 10/17/16 1807 KDM P6J0297
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
97 % 80-124
Dibromofluoromethane
100 % 75-129
Toluened8
100 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364-Fax: [phone] Page 6 of 9

Full -Service Analytical a
�P R I S M I Environmental Solutions
ouaoa..�.a�a�
Akzo Nobel Project: SW Samples
Attn: David Simons
485 Cedar Springs Road
Salisbury, NC 28147
Volatile Organic Compounds by OC/MS - Quality Control
Analyte
Batch
Reporting
Result Limit Units
Level 11 QC Report
10/19/16
Prism Work Order: 6100219
Time Submitted: 10/11/2016 12:44:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (PGJ0297-BLK1)
Prepared & Analyzed:
10/17/16
1,2-Dichloroelhane
BRL
0.00050
mg/L
Toluene
BRL
0,00050
mg/L
Surrogate: 4-Bmmotluorobenzene
49.5
u91L
50.00
99
80-124
Surrogate: Dibromolluoromethane
48.8
ug/L
saoo
98
75-129
Surrogate: Toluene-0
49.3
ug/L
5o00
99
77-123
LCS (P6J0297-BS1)
Prepared & Analyzed:
10/17/16
1,2-Dichloroelhane
0.0193
0.00050
mg/L
0.02000
96
68-131
Toluene
0.0210
0.00050
mg/L
0.02000
105
76-131
Surrogate: 4-Bromofluorobenzene
49.7
u9/L
50.00
99
80-124
Surrogate: Dibromolluoromethane
50.1
ug/L
5o.00
100
75-129
Surrogate: Toluene-d8
49.8
ug/L
50.00
100
77-123
LCS Dup (P6JO297-BSD1)
Prepared & Analyzed:
10/17/16
1,2-Dichloroethane
0.0195
0.00050
m9/L
0.02000
98
68-131 1 20
Toluene
0.0207
0,00050
mg/L
0.02000
104
76-131 2 20
Surrogate: 4-Bromolluorobenzene
48.8
u9/L
50.00
98
80-124
Surrogate: Dibromolluoromethane
49.2
ug/L
50,00
98
75-129
Surrogate: Toluene-d8
49.2
ug/L
5000
98
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/629.6364 - Fax: [phone] Page 7 of 9

UService Analytical &QPRISM EnIv,'uonal Solutions
p7ua�..wre>,.c
Level II QC Report
10/19/16
Akzo Nobel Project: SW Samples Prism Work Order: 6100219
Attn: David Simons Time Submitted: 10/11/2016 12:44:OOPM
485 Cedar Springs Road
Salisbury, NC 28147
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6JO233 - NO PREP
Blank (P6J0233-BLK1) Prepared & Analyzed: 10/14/16
Nitrate/Nitrite as BRL 0.10 mg/L
LCS (P6J0233-13SI) Prepared & Analyzed: 10/14/16
Nitrate/Nitrite as N 0.925 0.10 mg/L 1.000 92 90-110
Prep Method: 5030B
Lab Number
6100219-01
6100219-02
6100219-03
Sample Extraction Data
Batch
Initial
Final
Date/Time
P6J0297
10
mL
10 mL
10/17/16 10:33
P6J0297
10
mL
10 mL
10/17M6 1033
P6J0297
10
mL
10 mL
10/17/16 10:33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629.6364-Fax: [phone] P89B 8 Of 9

rA
CHAIN OF. CUSTODY RECORD
Full -Service Analytical &
p R� I S M
/�43310`"BORAIMES
— . .. .. ... .
'YES �NO NW M
Environmental Solutions PASS
It QUOTE 9 To ENSURE PROPER BILLING:
OF
', %Sarimples, INTACT,upon a
0
� INC
VV
',,,7R66eiv6d ON ETJCE?�T�
On
Project Name:
"g Springbrook Road -Charlotte, INC 28217 (NO)
Short Hold Analysis: (Yes) (No) UST Project: (Yes)
h
R PRESERVATIVES indi6tec!7�
Phone [phone] - Fax: [phone]
*Please ATTACH any project specific reporting (CC LEVEL 111111 IV)
Auk A14)1
I HOLDING I
M
Client Company Name: 7 provisions and/or QC Requirements
CUSTODY SEALS INTACT };
-4,
Report To/Contact Name: D,4LIIJ r6 ,Mm - Invoice To:
1 T, HEADSPACEv
Address: Ce. 1,7.,
Reporting Add Address:
OPER Use
Its a
Phone: -211/ �/-9121 -�"g ax(Yes)(No):— Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address" Requested Due Date 0 1 Day-- 0 2 Days EJ 3 Days Q 4 Days D 5 Days Certification: NELAC— DOD
FL NC
EDD Type: PDF,/ Ec01 �Othr_ 'Working Days" C1,49 Days 0 Standard 10 days L] Rush Work Must Be
Pre -Approved
SC_ OTHER
N/A_
Site Location Name: Samples received after 14:00 will be processed next business day. I
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— NO_
Site Location Physical Address:
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES_
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX
SAMPLE CONTAINER AYALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL,
PRESERVA- b�
TIVES
REMARKS
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
*TYPE NO. SIZE "0
ID NO.
HOURS SLUDGE)
SEE BELOW
ILI - /1- 16
1441e)
iil'
61A
3
J
-500�ls
1-17 5i'41
fi?
ttlile✓
AA
SOM is
Sampler's Signature Sampled By (Print Name) Affiliation 4k2c:> /oI­)043IF,
Upon relinquishing,,, this 0 ain of Custody is your authorization for
Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges
for any changes after analyses have been initialized.
Rei,W�I,ad BY: (SIgn-tors) ReesSlgnalure) Data I
WitarlHoeS Ad itional Comments:
RGkrl
Site Arrival Time;
re
eem,.artgw. t.,greaun, Reosved UY: (Nguato DaleSite
DepaTtLreTune:,'
Ralln signstur-T R eived For usm Laboratories By:
Field Tech Fee:
Mileage:
mathoa m Shipment: PI ALL COOLERS SHOULD HE TAPED 5 T
VWr
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST C
DY SEALS FOR TRANSPORTATION LABORATORY. urC Group No. P
To I.No
T.L. RECEIVEDATT�ELABORATORY.
�3 5'
LcR, Swak-
3 Fed Ex 0 UPS U Hanaalivered 0 Pdarn HrAce Fled SeU Offie NPDES, UST:LANDFILL
GROUNDWATER: DRINKING WATER. SOLID WASTE:
CNC6SC O4C aSC LNC USC ENC ESC
I
IRC�AICERCLA IDTH1E
ENC QSC �CCSCU NC El El NC U SC SLJ2
`CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL.

i.
Permit Number: NCS 006 Z 5 B
Certificate of Coverage Number: NCG_
or
STORMWATER DISCHARGE OUTFALL(SDO)
MONITORING REPORT
FACILITY NAME G(Y(oTECH T.-tC
PERSON COLLECTING SAMPLE(S)
CERTIFIED LABORATORV(S)FAl✓tF2O CJE.rI Lab#
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 20I S
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.
COUNTY B2 OAIJ W i CA
PHONE NO. (q/D) 3 -
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
-----------
-----------
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes xno
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitorine Requirements
Outfall
Date
50050
00556
00530
00400
No.
Sample
Collected
Total Flow
(if applicable)
Total Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G!I'PH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor Oil
Usage
mo/dd/ r
MG
inches
m I
mg/1
Units
al/mo
Form S W U-246, lust revised 2/2/2012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date 111631/S
Total Event Precioitation (inches): 2.32
Event Duration (hours): N ,d (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable— see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Scrvicc Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permr ee)
(Date)
Form S W U-246, last revised 21212012
Page 2 of 2

Cie-7
Glycotech
2271 Andrew Jackson Hwy, NE
PO Box 1956
Leland, N.C. 28451
910-371-2234
December 21, 2015
ATTENTION: Central Files REeEIVED
Division of Water Quality DEC 2 9 2015
1617 Mail Service Center
Raleigh, N.C. 27699-1617 CENTRAL FILES
DWR SECTION
Subject: Fall Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc., under permit #NCS000258 has performed the Fall 2015
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, Glycotech, Inc. is required to perform storm water sampling and subsequent
analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD was
83 mg/L, versus the benchmark value of 120 mg/L. The pH was 5.1, with a recorded
Rain -gage pH of 5.0, therefore the benchmark values of 6.0 to 9.0 do not apply (per the
permit).
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
Wayne Duff
Plant Manager
Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

,w r
NC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://I)orial.ncdenr.org/web/wq/ws/su/nT)dessw#tab-4
Permit No.: N/C/S/0/0/0/ 2/$/ Ff/ or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Facility Name: GLttol6et4 + -Uc -
County: Bt2"AJAwirrm Phone No.
Inspector: G
Date of Inspection: 1-1I/M r
Time of Inspection: U900
Total Event Precipitation (inches): Z . 3 Z
Rto- 3i 1 — Z234
Was this it Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signatu wj certify that ttlis report is accurate and complete to the best of my knowledge:
(Signature of Pernidee or Designee)
1. Outfall Description:
Outfall No. 00 i. Structure (pipe, ditch, etc.) lit?Z<i
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
CHEi+'l/C,tit_ tmllAtuFACTu2r1JG
2. Color: Describe the color of the disch!Ha ;e using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: fANA/t C 132oc,)AJ
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): NO Alf
Page I of 2
S W U-242-20120613

4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
11 O 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no s�oliids and 5 is the surface covered with floating solids:
no
� 1 J 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where l is no solids and 5 is extremely muddy:
1 J 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
). Is there evidence of erosion or deposition at the outfall? Yes No
1(). Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may
be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
swu-242s0120613

e I virochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Glycotech, Inc.
Date of Report:
Nov 19, 2015
PO Box 1956
Customer PO #:
6515
Leland NC 28451
Customer ID:
09060025
Attention: Gary Wooten
Report#:
2015-14902
Project ID:
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
15-35413 Site: Outfall 002 11/312015 9:00AM Water Gary Wooten
Test Method Results Date Analyzed
COD SM5220o 83mg/L 11/13/2015
Comment: (�^ r�
Reviewed by: �"I�.I��k OK YQ VJ
1.
Report#.: 2015-14902 Page 1 of 1

L` 1\ 111\V1'4iVu+lI Aa� �.aaa:u.uvi v, �.. �. --__ ....._--- ...y
Wilmington, NC 28405
Sample Collection and Chain of Cuatodv Phone: (9I0) 392.0223
Fax [phone]
]lent G �Y c o A EMAIL: E
.. A.., n _. Rennrt Nne 1 S
m ="M Uent. w Tffsu.%.�■
PRESERVATION
Q Collection
Sam: pie Identification o ANALYSISREQIIESTED
DATE TIME TEMP
ll3IS baoo ST c P COD NPDES
Culwfc:a �bffA�� 35`}Ij (3 G G
n C P
: bamp:
time of
for
Phenol, and Bacteria must be
Transfer Relinquished y:. Date/Time Received By: Date/Time
i.Ok.,cv 1 ok
2.
Temperature when Received: Accepted: / Resample Requ t
Delivered By: Received By: Date; 11 q Time:
Comments: PC 'tr GS 1 5 DR < Z Qe r, Qr ro o N :cr'

Permit Number NCS 000259
FACILITY NAME Akzo Nobel Surfacc
PERSON COLLECTING SAMPLE(S)
CERTIFIED LABORATORY(S) Pac[
Part A: Specific Monitoring Requirements
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days f�
the date the facility receives the sampling results from the laboratory.)
COUNTY Rowan
PHONE NO. (LO4) 633-1731
# 12
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m L
m
m L
SIU
SW-1
07/29/15
.15
.000991
.00026
0.89
6.02
SW-2
07/29/15
.15
.00077J
.00026
2.1
16.20
SW-3
07/29/15
.15
.00025J
.0226
1.6
6.30
SW-4
07/29/15
No Flow
No Flow
No Flow
No Flow
No Flow
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirement%
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
m /I
unit
gavmo
Form SWU-247, last revised 2121201
Page I

a i
'ot
of ..
QJ. ..
_
_ #.� s
;#._r�. a.n
• .. t : _ ..

STORM EVENT CHARACTERISTICS:
Date 07/29/15
Total Event Precipitation (inches): .13
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Alm: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of
Ia-,,1
(Da e)
Form SWU-247, last revised 2121201
Page 2 of 2

3
r.
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' t
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T .
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y C

AkzoNobel 485 Cedar Springs Road T + 1 704 633 1731
Surface Chemistry Unit A F + 1 704 637 8912
Salisbury, NC 28147 w .akzonobel.com/sc
USA
August 17, 2015
NCDENR — Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Certified Mail: Return Receipt Requested
Reference: Semi -Annual Permit Monitoring Report
Individual Stormwater Monitoring Permit
AkzoNobel Surface Chemistry LLC.
Permit No. NCS000259
AkzoNobel
Tomorrow's Answers Today
RECEIVED
AUG 2 8 2015
CENTRAL FILES
DWR SECTION
Attached are two copies of the AkzoNobel monitoring results for the period of July 1,
2015 to December 31, 2015 for our permit # NCS000259 for the samples collected
July29, 2015. Any questions on this submittal you may contact me at 704-642-6203.
Regards,
David Simons
HSES Manager
AkzoNobel Surface Chemistry, LLC, Salisbury, NC
Copy: Brian Owen AkzoNobel Surface Chemistry, LLC, Salisbury, NC
David Simons AkzoNobel Surface Chemistry, LLC, Salisbury, NC

IceAnallytical'
inmpacelabswm
August 06, 2015
David Simons
Akzo Nobel
485 Cedar Springs Rd.
Salisbury, NC 28147
RE: Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
Dear David Simons:
Pace Analytical Services, Inc.
9800 NSncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 29, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
\,�, C ,-- Cc.r,r �Ly
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
cc: Chris Fleming
Leonard White, Akzo Nobel
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

(�15'ceAnalytical'
w psce,lab&=
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
Charlotte Certification We
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky LIST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)8759092
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certiflcation #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Paw Analytical Services, Inc.. Page 2 of 13

55c'eAnalyficale
eee.Pcelabscan
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
Lab IDSample ID
92260960001 SW #1
92260960002 SW #2
92260960003 SW #3
Pace Ana"cal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Water
07/2711519:50
0729/1516:45
Water
0712711519:55
07/29/1516:45
Water
0712711519:55
07/29/1516:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 3 of 13

Pace Analytical Services, Inc.
aceAnalytical s 9800Hunesvil e, NC 28078
..pacelaftcrom
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SW SAMPLING 0729/15
92260960
Analytts
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92260960001
SW#1
EPA 8260
CAH
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92260960002
SW #2
EPA 8260
CAH
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92260960003
SW #3
EPA 8260
CAH
5
PASI-C
EPA 353.2
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 13

aceAnalytical e
s wpircelab&=
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
Sample: SW #1
Parameters
8260 MSV Low Level
1,2-Dichloroethane
Toluene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene -dB (S)
353.2 Nitrogen, N021NO3 pros
Nitrogen; NO2 plus NO3
Pace AnahNcal Services, Inc.
9800KinceyAve. Suite 100
Huntersville, NC 28078
(704)8759092
ANALYTICAL RESULTS
Lab ID: 92260960001 Collected: 07127115 19:50 Received: 07/29/1516,45 Matrix: Water
Results Units PQL
Analytical Method: EPA 8260
0.991
ug/L 1.0
<0.26
ug/L 1.0
105
% 70-130
96
% 70-130
99
% 70-130
Analytical
Method: EPA 353.2
0.89
mg/L 0.020
MDL DF Prepared Analyzed CAS No. Qual
0.24
1
07/31/15 00:46
107-06-2
0.26
1
07/31/15 00:46
108-88-3
1
07/31/15 00:46
460-004
1
07/31/15 00:46
17060-07-0
1
07/3l/1500:46
2037-26-5
0.010
1
08/05/15 08:57
Sampler SW #2 Lab ID: 92260960002 Collected: 0712711519:55 Received: 0712911516:45 Matfx: Water
Parameters
Results
Units PQL
8260 MSV Low Level
Analytical
Method: EPA 8260
1,2-Dichloroethane
0.77J
ug/L 1.0
Toluene
<0.26
ug/L 1.0
Surrogates
4-Bromofluorobenzene (S)
111
% 70-130
1,2-Dichloroethane-04 (S)
108
% 70-130
Toluene-d8 (S)
100
% 70-130
353.2 Nitrogen, NO2/1403 pres.
Analytical
Method: EPA 353.2
Nitrogen, NO2 plus NO3
2.1
mg/L 0.020
MDL DF Prepared Analyzed CAB No. Qual
0.24
1
08/06/15 11:31
107-06-2
0.26
1
08/05/15 11:31
108-88-3
1
08/05/15 11:31
460-004
1
08/05/15 11:31
17060-07-0
1
08/05/15 11:31
2037-26-5
0,010
1
08/05/15 09:00
Sample: SW #3 Lab ID: 92260960003 Collected: 07127115 19:55 Received: 07/29/15 16:45 Matrix: Water
Parameters
8260 MSV Low Level
1,2-Dichloroethane
Toluene
Surrogates
4-8romofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene -dB (S)
353.2 Nitrogen, NO2/NO3 pres
Nitrogen, NO2 plus NO3
Date: 08/06/2015 03:49 PM
Results Units PQL
MDL
DF
Prepared Analyzed
CAS No. Qua]
Analytical Method: EPA 8260
0.26,11 ug/L 1.0
0.24
1
07131/1513:52
107-06-2
22.6 ug/L 1.0
0.26
1
07/31/15 13:52
108-88-3
108 a/ 70-130
1
07/3111513:52
460-004
103 % 70-130
1
07/31/15 13:52
17060-07-0
100 % 70-130
1
07/31/15 13:52
2037-26-5
Analytical Method: EPA 353.2
1.6 mg/L 0.020
0.010
1
08/05/15 09:04
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of PaceAnalytical Services, Inc..
Page 5 of 13

aceAnalj4ical e
ewwpacelabs.00m
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntemville, NC 28078
[phone]
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
OC Batch: MSV/32797
Analysis Method: EPA 8260
QC Batch Method: EPA 8260
Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92260960001
METHOD BLANK: 1522767
Matrix: Water
Associated Lab Samples: 92260960001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
1,2-Dichloroethane
ug/L
<0.24 1.0 07/30/15 18:21
Toluene
ug/L
<0.26 1.0 07/30/15 18:21
1,2-Dichloroethane-d4 (S)
%
94 70-130 07/30/15 18:21
4-Bromofluorobenzene (S)
%
97 70-130 07/30/15 18:21
Toluene-d8 (S)
%
99 70-130 07/30/15 18:21
LABORATORY CONTROL SAMPLE: 1522788
Spike LCS LCS % Rec
Parameter
Units
Conc. Result %Rec Limits Qualifiers
1,2-Dichloroethane
ug/L
50 42.4 85 70-130
Toluene
ug/L
50 48.0 96 70-130
1,2-Dichloroethane-d4 (S)
%
89 70-130
4-Bromofluorobenzene (S)
%
108 70-130
Toluened8 (S)
%
99 70-130
MATRIX SPIKE SAMPLE:
1522789
92260616001
Spike
MS MS
% Rec
Parameter
Units
Result
Conc.
Result % Rec
Limits Qualifiers
1,2-Dichloroethane
ug/L
NO
20
20.2 99
70-130
Toluene
ug/L
NO
20
22.7 112
70-155
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
97
70-13D
Toluened8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1522790
92260960001
Oup
Max
Parameter
Units
Result
Result
RPD RPD
Qualifiers
1,2-Dichloroethane
ug/L
0.991
1.0
30
Toluene
ug/L
<0.26
<0.26
30
1,2-Dichloroethane-d4 (S)
%
96
99
3
4-Bromofluorobenzene (S)
%
105
104
0
Toluened8 (S)
%
99
98
1
Results presented on this papa are In the unlb Indicated by the'Unbs' column except wham an aRemete unit la preser4ed to me right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/06/2015 03:49 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 13

aceAnalytical e
wmepacalab&corn
Project: SW SAMPLING 0729115
Pace Project No.: 92260960
QC Batch: MSV/32799
QC Batch Method: EPA 8260
Associated Lab Samples: 92260960003
METHOD BLANK: 1623192
Associated Lab Samples: 92260960003
Parameter
Units
1,2-Dichloroethane
ug/L
Toluene
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene'Ld8 (S)
%
QUALITY CONTROL DATA
Analysis Method: EPA 8260
Analysis Description: 8260 MSV Low Level
Matrix: Water
Blank Reporting
Result Limit
<0.24 1.0
<0.26 1.0
93 70-130
104 70-130
100 70-130
Analyzed
07131115 10:49
0761115 10:49
07/31/15 10:49
07131115 10:49
07/31/15 10:49
Qualifiers
Pace Analytical Services, Inc.
9800Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1523193
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
1,2-Dichloroethane
ug/L
50 45.3 91
70-130
Toluene
ug/L
50 50.0 100
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
107
70-130
Toluenet18 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
1523194
92261050003
Spike
MS MS
% Rec
Parameter
Units
Result
Conc.
Result %Rec
Limits Qualifiers
1,2-Dichloroethane
ug/L
ND
20
18.5 91
70-130
Toluene
ug/L
1.1
20
23.1 110
70-155
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
107
70-130
Toluene-d8(S)
%
100
70-130
SAMPLE DUPLICATE: 1525725
92261250005
Dup
Max
Parameter
Units
Result
Result
RPD RPD
Qualifiers
1,2-Dichloroethane
ug/L
NO
<0.24
30
Toluene
ug/L
NO
<0.26
30
1,2-Dichloroethane-d4 IS)
%
99
104
5
4-Bromofluorobenzene (S)
%
108
107
1
Toluene-d8 (S)
99
102
2
Resube presented on this page am In U,e units indicated by the'Unhs' column except wbem an aeereate unit b presented W the r10M of rim result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 03:49 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 13

laceAnallytical"
www.pscelabs.com
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
QC Batch: MSV/32853
QC Batch Method: EPA 8260
Associated Lab Samples: 92260960002
METHOD BLANK: 1526334
Associated Lab Samples: 92260960002
Parameter
Units
1,2-Dichloroethane
ug/L
Toluene
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LABORATORY CONTROL SAMPLE: 1526335
Parameter Units
1,2-Dichloroethane
ug/L
Toluene.
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
QUALITY CONTROL DATA
Analysis Method: EPA 8260
Analysis Description: 8260 MSV Low Level
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
<0.24
1.0
08/05/15 02:39
<0.26
1.0
08/05/15 02:39
101
70-130
08/05/15 02:39
99
70-130
08/05/15 02:39
99
70-130
08/05/15 02:39
Spike LCS LCS
Conc. Result % Rec
50 44A 89
50 50.2 100
98
111
99
Pace Analytical Services, Inc.
98001Gncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
% Rec
Limits Qualifiers
70-130
70-130
70-130
70-130
70-130
Results presented on this pago are in the units Indicated by the 'Units' column except when an ahemate unit Is presented to the right of Me moult
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 03:49 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 13

7;aceAnalyticalo
WewpM8laba.ONn
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
980010ncey Ave. Suite too
Huntersville, NC 28078
[phone]
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
QC Batch: WETA23989
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92260960001, 92260960002,
92260960003
METHOD BLANK: 1525930
Matrix: Water
Associated Lab Samples: 92260960001, 92260960002,
92260960003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
<0.010 0.020
08/05/1508:52
LABORATORY CONTROL SAMPLE: 1625931
Spike LCS
LCS %Rec
Parameter Units
Conc. Result
%Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L
2.5 2.3
94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1525932 1525933
MS MSD
92260827001
Spike Spike MS
MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result
Result %Rec %Rec
Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 2.3
2.5 2.5 4.6
4.5 91 86
75-125 3 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1525934 1525935
MS MSD
92260960001
Spike Spike MS
MSD MS MSD
% Rec Max
Parameter Units Result
Cana Conc. Result
Result %Rec %Rec
Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.89
2.5 2.5 3.3
3.1 95 90
75-125 4 10
Results pmaso ted on this page are In Me units bMluted by Me'Units' column except when an ahemam unh Is prevented to Me right or Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/06/2015 03:49 PM without the when consent of Pace Analytical Services, Inc..
Page 9 of 13

aceAnalytical a
a .pacelabs.=
QUALIFIERS
Project: SW SAMPLING 07/29/15
Pace Project No.: 92260960
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Wmtersville, NC 28078
[phone]
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
,U - Indicates the compound was analyzed for, but not detected.
Add preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
'A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
Date: 08/06/2015 03:49 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13

55'ceAnaifytical'
w pacalabs.=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Projects,
Pace Project No.:
SW SAMPLING 07/29/15
92260960
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92260960001
SW#1
EPA 8260
MSV/32797
92260960002
SW#2
EPA 8260
MSV/32853
92260960003
SW #3
EPA 8260
MSV/32799
92260960001
SW#1
EPA 353.2
WETA/23989
92260960002
SW#2
EPA 353.2
WETA/23989
92260960003
SW#3
EPA 353.2
WETA/23989
REPORT OF LABORATORY ANALYSIS
This report shall nor be reproduced, except in full,
Date: 08/06/2015 03:49 PM without the wnnen consent of Pace Analytical Services, Inc.. Page 11 of 13

Document Name: Document Revised: May 18, 2015
_� nceA>?yfical' Sample Condition Upon Receipt (SCUR) I Page 1 of 2"
Document Number: Issuing Authority:
r_nuo Po nn* __ Ac nw—
Client Name: kZo kk I Page 2 of 2 is for Internal Use Only
Courier: ❑Fed Ex ❑ UPS[] USPSQ� /Client❑ Commercial❑ ace OI er
Custody Sea[ on Cooler/Box Present: LX yes ❑ no Seals intact: Prdj Due;Daf �j
as ❑ no IS
,� Y .
Packing Material: ❑ Bubble VDp ❑ Bubble Bags ❑ None Other
Thermometer Used: IR Gun T1401 Type of Ice: Let' Blue None Samples on ice, cooling process has begun
Temp Correction Factor T1401 No Correction
CorrectedCoolerefreez: 'C
Temp should be above freezing to S°C
Biological Tissue is Frozen: Yes No )A
0
Comments:
Date and Initials of per;pn examining
contents:��'Y ,))
Chain of Custody Present:
9. ONO
❑NIA
1.
Chain of Custody Filled Out:
Yes ONO
❑N/A
2.
Chain of Custody Relinquished:
Yes ONO
❑NIA
3.
Sampler Name R Signature on COC:
es ONO
❑N/A
4.
Samples Arrived within Hold Time:
Yea ONO
❑N/A
5.
Short Hold Time Analysis <72hr :
Dyes 4.
❑N/A
6.
Rush Turn Around Time Requested:
Oyes No
❑NIA
7,
Sufficient Volume:
es ONO
ON/A
8.
Correct Containers Used:
-Pace Containers Used:
Yes ONO
Ye - ONO
❑N/A
❑N/A
g,
Containers Intact:
GKes ONO
DN/A
10.
Filtered volume received for Dissolved tests
,uses ONO
ONIA
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Malrix:
t "s ONO
tU
ON/A
12.
All containers needing preservation have been checked,
All containers needing preservation are found to be In
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, 0&G, WI-DRO (water)
yes ONO
ir7.is ONO
ie
es ONO
❑N/A
ON/A
13.
Samples checked for dechlorinalion:
Ryes ONO
❑N/A
14.
Heads ace in VOA Vials(>6mm):
es ONO
❑NIA
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Dyes ONO
Dyes ONO
r
14NIA
16.
Pace Trip Blank Lot #(if urchased:---------__.._..___.
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Datelrime:
Comments/ Resolution:
SCURF Review: CJ Date: r-l— � IJ WO# : 92260960
SRF Review: I LQ Date: (5
Note: Whenever there is a discrepancy affecting North Carolina compliance HIM
11111111111111111111
samples, a copy of this form will be sent to the North Carolina DEHNR 82280860
Certification Office ( is out of hold, incorrect preservative, out of temp,
Incorrect containers)
Page 12 of 13

CHAIN -OF -CUSTODY / Analytical Request Document o
/ eAnalytleal The Chait fCustoey is a LEGAL DOCUMENT. All relevant fieWs must to c mpletetl aauratey.
i
• wv.Pwbas.wm
Section A Section S Section C
Paso: / of
RequlreC Client Information: RequiroE Project Information: Ineoios Inormotion:
6
Company: �7
Report To:
AMn
/t /1(i� O
Aeere p qq
Copy To:
CM,aanY Name:
REGULATORY
AGENCY
tea'
r NPDES
r UST
i ; GROUNDWATER F DRINKING WATER
j RCRA i OTHER
Emad To:
Purtlaae Order No,
Paw 0.
flinfe m
Phone: ax:
Project Name:
Para P,
Site Location
STATEI
Roquostee Duo Data TAT:
Project Numa ..
Pau Pmtue a: Y'3�
✓C7
Requested
Analysis
Filtered
(YIN)
section Matrix COCas
Regahvecuem ulcmuaon NAralx r cMI
e
M
COLLECTED
Preservatives
9
DnMtirg Water Ow
Q
z
Wabr WT
(J
O
wastewater Ww
ProdtCt P
a
p
a
a
ST.T
cowas'rt
OUPCMe
j
4
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SoWSo4a SL
SAMPLE ID wpe OL
u
J
(A-Z0.91.) ter AR
w
w
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Samge IDs MUST BE UNIQUE Tasu TS
Order OT
p
¢
a
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w
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(�'•'(� /�
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TIME
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Pace Proiect No! Lab I.D.
a
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74Z/
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X
1
1X
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4sf
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X
X
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X
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7
1
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1
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1
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•DBY
ADDRIONAL COMMENTS
REj#QUISHEDBY1AFFlUXMN
DATE
TIME
ACCE I AF ON
DATE
TIME
SAMPLE CONDITIONS
Ncldlorce fh4AC!
7 �Cj
�q
a,7
:,<
I
AY 5ar=3
SAMPLER NAME AND SIGNATURE28
U
c
_°u°u
rj T°a Z'
H
E
SIGNATURE of SAMPLER:
l✓�
DATE Signed
(MMIDDmT: 7 Z7 ys
F-ALL-0-020nw.07, 15-May-2007

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days fron
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Akzo Nobel Surface Chemistry LLC COUNTY Rowan
PERSON COLLECTING SAMPLE(S) Lyyn White and Traci Sloop PHONE NO. [phone]
CERTIFIED LABORATORY(S) Pace Analytical Services. Inc.Lab # 37706
Lab # 12 O
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRE ON PACE 2.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m /L
m /L
m /L
SIU
SW-1
06/02/15
.13
.0268
.00026
.00042
6.20
SW-2
06/02/15
.13
.0034
.00026
.0012
6.33
J J
SW-3
06/02/15
.13
.00069J
.00068J
.00083
8.04
-EV
�FU�.
SW-4
06/02/15
No Flow
No Flow
No Flow
No Flow
No Flow
"� f/Q X
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m I
m l
unit
al/mo
Form SWU-247, last revised 2121201
Pagel of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date 06/02/15 Attn: Central Files
Total Event Precipitation (inches): .13 1617 Mail Service Center
Event Duration (hours): (only if applicable — see permit.) Raleigh, North Carolina 27699-1617
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable —see permit.)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge. nd belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility o es and imprisonment for knowing violations."
of
Form SWU-247, fast revised 2121201
Page 2 of 2

I don
aceAnalytical e
a .pacabbs.can
June 15, 2015
David Simons
Akzo Nobel
485 Cedar Springs Rd.
Salisbury, NC 28147
RE: Project: SW Samples 6/2
Pace Project No.: 92252696
Pace Analytical services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear David Simons:
Enclosed are the analytical results for sample(s) received by the laboratory on June 03, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
`
yx, C�, C Y, - �4.�c_
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
co: Chris Fleming
Leonard While, Akzo Nobel
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 16

ZeAnalyfical$
a»wpecalab:can
CERTIFICATIONS
Project: SW Samples 6/2
Pace Project No.: 92252696
Pace Ans"cal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersdlle, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
TNs report shall W be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 16

Pace Ana"cal Services, Inc.
aceAnalytical a 96001nceyAve. Suite 100
HuMersville, NC 26076
mvw.pealabscom
(764)8769092
SAMPLE SUMMARY
Project:
Pace Project No.:
SWSamples6/2
92252696
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92252696001
SW #1
Water
06/02/15 11:15
06/03/15 17:10
92252696002
SW #2
Water
06102115 11:22
06/03/15 17:10
92252696003
SW #3
Water
06/02/15 11:22
06/03/15 17:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 16

Pace Analytical Services, Inc.
te 100
aceAnalytical a 9�OHunersWl e, Cy Ave. 128078
e pacelabs.com
[phone]
SAMPLE ANALYTE COUNT
Project: SW Samples 6/2
Pace Project No.: 92252696
Lab ID
Sample ID
Method
Analysts
Analysts
Reported
Laboratory
92252696001
SIN#1
EPA 8260
GAW
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92252696002
SIN#2
EPA 8260
GAW
63
PASI-C
EPA 353.2
DMN
1
PASI-A
92262696003
SW #3
EPA 8260
GAW
63
PASI-C
EPA 353.2
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 16

aceAnalytical e
mmpacaabswm
Project: SW Samples 612
Pace Project No.: 92252696
Sample: SW #1
Parameters
Field Data
Collected Date
Collected Time
Field pH
8260 MSV Low Level
1,2-Dichloroethane
Toluene
Surrogates
4-BromoOuorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
363.2 Nitrogen, NO2IN03 pres
Nitrogen, NO2 plus NO3
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92252696001 Collected: 06/02/15 11:15 Received: 06/03/15 17:10 Matrix: Water
Results Units POL MDL DF Prepared Analyzed CAS No. Oual
Analytical Method
6112/15
1
06/02/15 11:15
11:15
1
06/02/15 11:15
6.2 Std. Units 0.10
0.10
1
06/02/15 11:15
Analytical Method: EPA 8260
26.8 ug/L 1.0
0.12
1
06/05/15 05:48
107-06-2
<0.26 ug/L 1.0
0.26
1
06/05/15 05:48
108-88-3-
96 % 70-130
1
06/05/15 05:48
460-00-4
99 % 70-130
1
06/05/15 05:48
17060-07-0
101 % 70-130
1
06/05/15 05:48
2037-26-5
Analytical Method: EPA 353.2
0.42 mg/L 0.020
0.010
1
06/09/1514:07
Sample: SW #2 Lab ID: 92252696002 Collected: 06/02/15 11:22 Received: 06103115 17:10 Matrix:Water
Parameters Results Units POL MDL DF Prepared Analyzed CAS No. Oual
Field Data
Collected Date
Collected Time
Field pH
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromod ichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromelhane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
Date: 06/15/2015 09:54 AM
Analytical Method
6/2/16
1
06/02/15 11:22
11:22
1
06/02/15 11:22
6.33
Sid. Units
0.10
0.10
1
06/02/15 11:22
Analytical
Method: EPA 8260
328
ug/L
25.0
10.0
1
06/05/15 06:05
67-64-1
<0.25
ug/L
1.0
0.25
1
06/05/15 06:05
7143-2
<0.30
ug/L
1.0
0.30
1
06/05/15 06:05
108-86-1
<0.17
ug/L
1.0
0.17
1
06/05/15 06:05
74-97-5
<0.18
ug/L
1.0
0.18
1
06/05/15 06:05
75-274
<0.26
ug/L
1.0
0.26
1
06/05/15 06:05
75-25-2
<0.29
ug/L
2.0
0.29
1
06/05/15 06:05
74-83-9
36.6
ug/L
5.0
0.96
1
06/05/15 06:05
78-93-3
<0.25
ug/L
1.0
0.25
1
06/05/15 06:05
56-23-5
<0.23
ug/L
1.0
0.23
1
06/05/15 06:05
108-90-7
<0.54
ug/L
1.0
0.54
1
06/05/15 06:05
75-00-3
<0.14
ug/L
1.0
0.14
1
06/05/15 06:05
67-66-3
<0.11
ug/L
1.0
0.11
1
06/05/15 06:05
74-87-3
<0.35
ug/L
1.0
0.35
1
06/05/15 06:05
9549-8
<0.31
ug/L
1.0
0.31
1
06/05/15 06:05
106434
<2.0
ug/L
2.0
2.0
1
06/05/15 06:05
96-12-8
<0.21
ug/L
1.0
0.21
1
06/05/15 06:05
12448-1
<0.27
ug/L
1.0
0.27
1
06/05/15 06:05
106-934
<0.21
ug/L
1.0
0.21
1
06/05/15 06:05
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wn8en consent of Pace Analytical Services, Inc..
Page 5 of 16

aceAnalytical.
w Pacola6Acan
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: SW Samples 6/2
Pace Project No.: 92252696
Sample: SW C2 Lab ID: 92252696002 Collected: 06102115 11:22 Received: 06/03/15 17:10 Matrix:Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
1,2-Dichlorobenzene
<0.30
ug/L
1.0
0.30
1
06/05/15 06:05
95-50-1
1,3-Dichlorobenzene
<0.24
ug/L
1.0
0.24
1
06/05/15 06:05
541-73-1
1,4-Dichlorobenzene
<0.33
ug/L
1.0
0.33
1
06/05/15 06:05
10646-7
Dichlorodifluoromethane
<0.21
ug/L
1.0
0.21
1
06/05/15 06:05
75-71-8
1,1-Dichlomethane
<0.32
ug/L
1.0
0.32
1
06/05/15 06:05
75-34-3
1,2-Dichloroethane
3.4
ug/L
1.0
0.12
1
06/05/15 06:05
107-06-2
1,1-Dichloroethene
<0.56
ug/L
1.0
0.56
1
06/05/15 06:05
75-35-4
cis-1,2-Dichloroethene
<0.19
ug/L
1.0
0.19
1
06/05/1506:05
156-59-2
trans-1,2-Dichloroethene
<0.49
ug/L
1.0
0.49
1
06/05/15 06:05
156-60-5
1,2-Dichloropropane
<0.27
ug/L
1.0
0.27
1
06/05/15 06:05
78-87-5
1,3-Dichloropropane
<0.28
ug/L
1.0
0.28
1
06/05/15 06:05
142-28-9
2,2-Dichloropropane
<0.13
ug/L
1.0
0.13
1
06/05115 06:05
594-20-7
1,1-Dichloropropane
<0.49
ug/L
1.0
0.49
1
06/0511506:05
563-58-6
cis-1,3-Dichloropropene
<0.13
ug/L
1.0
0.13
1
06/05/15 06:05
10061-01-5
trans-1,3-Dichloropropene
<0.26
ug/L
1.0
0.26
1
06/05/15 06:05
10061-02-6
Diisopropyl ether
<0.12
ug/L
1.0
0.12
1
06/05/15 06:05
108-20-3
Elhylbenzene
<0.30
ug/L
1.0
0.30
1
06105/15 06:05
100-41-4
Hexachloro-1,3-butadiene
<0.71
ug/L
1.0
0.71
1
06/0511506:05
87-08-3
2-Hexanone
<0.46
ug/L
5.0
0.46
1
06/05/15 06:05
591-78-6
p-Isopropyltoluene
<0.31
ug/L
1.0
0.31
1
06/05/15 06:05
99-87-6
Methylene Chloride
<0.97
ug/L
2.0
0.97
1
06/05/15 06:05
75-09-2
4-Methyl-2-pentanone(MISK)
0.44J
ug/L
5.0
0.33
1
06/05/15 06:05
108-10-1
Methyl-tert-butyl ether
<0.21
ug/L
1.0
0.21
1
06/05/15 06:05
1634-04-4
Naphthalene
<0.24
ug/L
1.0
0.24
1
06/05/15 06:05
91-20-3
Styrene
<0.26
ug/L
1.0
0.26
1
06/05/15 06:05
100.42-5
1,1,1,2-Tetrachloroethane
<0.33
ug/L
1.0
0.33
1
06/05/15 06:05
630-20-6
1,1,2,2-Tetrachloroethane
<0.40
ug/L
1.0
0.40
1
0610511506:05
79-34-5
Tetrachlomethene
<0.46
ug/L
1.0
0.46
1
06/05JI5 06:05
127-184
Toluene
<0.26
ug/L
1.0
0.26
1
06/05/15 06:05
108-88-3
1,2,3-Thchlorobenzene
<0.33
ug/L
1.0
0.33
1
0610511506:05
87-61-6
1,2,4-Trichlorobenzene
<0.35
ug/L
1.0
0.35
1
06/05/15 06:05
120-82-1
11,1-Trichloroethane
<0.48
ug/L
1.0
0.48
1
06105/1506:05
71-55-6
1,1,2-Trichloroethane
<0.29
ug/L
1.0
0.29
1
06/05/15 06:05
79-00-5
Trichloroethene
<0.47
ug/L
1.0
0.47
1
06/05/15 06:05
79-01-6
Trichlorofluoromethane
<0.20
ug/L
1.0
0.20
1
06/05/15 06:05
75-694
1,2,3-Trichloropropane
<0.41
ug/L
1.0
0.41
1
06/05/15 06:05
96-184
Vinyl acetate
<0.36
ug/L
2.0
0.35
1
06/05/15 06:05
108-054
Vinyl chloride
<0.62
ug/L
1.0
0.62
1
06/05/15 06:05
75-014
Xylene (Total)
<0.66
ug/L
2.0
0.66
1
06/05/15 06:05
1330-20-7
m&p-Xylene
<0.66
ug/L
2.0
0.66
1
06/05/15 06:05
179601-23-1
o-Xylene
<0.23
ug/L
1.0
0.23
1
06/05/15 06:05
9547-6
Surrogates
4-Bromofluorobenzene IS)
93
%
70-130
1
06/05/15 06:05
460-004
1,2-Dichloroethane-d4IS)
103
%
70-130
1
06/05/15 06:05
17060-07-0
Toluer4ed8 (S)
100
%
70-130
1
06/05/15 06:05
2037-26-5
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
Date: 06/15/2015 09:54 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 16

s
aceAnalytical
awrpecelabs.cw
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvills, NC 26078
(704)8759092
Project: SW Samples 6/2
Pace Project No.: 92252696
Sample: SW #2 Lab ID: 92252696002 Collected: 06/02/15 11:22 Received: 06/03/15 17:10 Matrix:Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3 1.2 mg/L 0.020 0.010 1 06/09/15 14:08
Sample: SW #3 Lab ID: 92252696003 Collected: 06/02/15 11:22 Received: 06/03/15 17:10 Matmx: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method
Collected Date
6/2115
1
06/02/16 11:22
Collected Time
11:22
1
06/02/15 11:22
Field pH
8.04
Std. Units
0.10
0.10
1
06/02/15 11:22
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
190
ug/L
25.0
10.0
1
06/05/15 00:21
67-64-1
Benzene
<0.25
ug/L
1.0
0.25
1
06/0511506:21
71-43-2
Bromobenzene
<0.30
ug/L
1.0
0.30
1
06/05/16 06:21
108-86-1
Bromochloromethane
<0.17
ug/L
1.0
0.17
1
06/05/15 06:21
74-97-5
Bromodichloromethane
<0.18
ug/L
1.0
0.18
1
06/05/15 06:21
75-27-4
Bromoform
<0.26
ug/L
1.0
0.26
1
06/05/15 06:21
75-25-2
Bromomethane
<0.29
ug/L
2.0
0.29
1
06/06/1606:21
74-83-9
2-Butanone(MEK)
67.4
ug/L
5.0
0.96
1
06105/1506:21
78-93-3
Carbon tetrachloride
<0.25
ug/L
1.0
0.25
1
06/05/15 06:21
56-23-5
Chlorobenzene
<0.23
ug/L
1.0
0.23
1
06/05/15 06:21
108-90-7
Chloroethane
<0.64
ug/L
1.0
0.54
1
06/05/15 06:21
75-00-3
Chloroform
<0.14
ug/L
1.0
0.14
1
06/05/15 06:21
67-66-3
Chloromethane
<0.11
ug/L
1.0
0.11
1
06/05/15 06:21
74-87-3
2-Chlorotoluene
<0.35
ug/L
1.0
0.35
1
06/05/15 06:21
9549-8
4-Chlorotoluene
<0.31
ug/L
1.0
0.31
1
06105/15 06:21
106434
1,2-Dibromo-3-chloropropane
<2.0
ug/L
2.0
2.0
1
0610511506:21
96-12-8
Dibromochloromethane
<0.21
ug/L
1.0
0.21
1
06/05/15 06:21
12448-1
1,2-Dibromoethane(EDB)
<0.27
ug/L
1.0
0.27
1
06105/1506:21
106-934
Dibromomethane
<0.21
ug/L
1.0
0.21
1
06/05/15 06:21
74-95-3
1,2-Dichlorobenzene
<0.30
ug/L
1.0
0.30
1
06/05/15 06:21
95-50-1
1,3-Dichlorobenzene
<0.24
ug/L
1.0
0.24
1
06105/1506:21
541-73-1
1,4-Dichlorobenzene
<0.33
ug/L
1.0
0.33
1
0610511506:21
10646-7
Dichlorodifluoromethane
<0.21
ug/L
1.0
0.21
1
06105/1506:21
75-71-8
i,t-Dichloroethane
<0.32
ug/L
1.0
0.32
1
- 06/05/15 06:21
75-34-3
1,2-Dichloroethane
0.690
ug/L
1.0
0.12
1
0610511506:21
107-06-2
1,1-Dichloroethene
<0.56
ug/L
1.0
0.56
1
06105/1506:21
75-354
cis-1,2-Dichloroethene
<0.19
ug/L
1.0
0.19
1
06/05/15 06:21
156-59-2
trans-1,2-Dichlooethene
<0.49
ug/L
1.0
0.49
1
06/05/15 06:21
156-60-5
1,2-Dichloropropane
<0.27
ug/L
1.0
0.27
1
06105/1506:21
78-87-5
1,3-Dichloropropane
<0.28
ug/L
1.0
0.28
1
06105/1506:21
142-28-9
2,2-Dichloropropane
<0.13
ug/L
1.0
0.13
1
06/05/15 06:21
594-20-7
1,1-Dichloropropane
<0.49
ug/L
1.0
0.49
1
06105/1506:21
563-56-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/15/2015 09:54 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 16

aceAnalytical a
wewpecela0.ccom
ANALYTICAL RESULTS
Project: SW Samples 6/2
Pace Project No.: 92252696
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW #3 Lab ID: 92262696003 Collected: 06/02/15 11:22 Received: 06/03/15 17:10 Matrix: Water
Parameters Results Units POL MDL DF Prepared Analyzed CAS No. Oual
8260 MSV Low Level Analytical Method: EPA 8260
cis-1,3-Dichloropropene
<0.13
ug/L
1.0
0.13
1
06/05/15 06:21
10061-01-5
trans-1,3-Dichloropropene
<0.26
ug/L
1.0
0.26
1
06/05/15 06:21
10061-02-6
Diisopropyl ether
<0.12
ug/L
1.0
0.12
1
06/05/15 06:21
108-20-3
Elhylbenzene
<0.30
ug/L
1.0
0.30
1
06/05/15 06:21
100414
Hexachloro-1,3-butadiene
<0.71
ug/L
1.0
0.71
1
06/05/15 06:21
87-68-3
2-Hexanone
<0.46
ug/L
5.0
0.46
1
0610511506:21
591-78-6
p-Isopropyltoluene
<0.31
ug/L
1.0
0.31
1
06/05/15 06:21
99-87-6
Methylene Chloride
<0.97
ug/L
2.0
0.97
1
06/05/15 06:21
75-09-2
4-Methyl-2-pentanone(MIBK)
<0.33
ug/L
5.0
0.33
1
06/05/15 06:21
108-10-1
Methyl-tert-butyl ether
0.28J
ug/L
1.0
0.21
1
06/05/15 06:21
1634-044
Naphthalene
<0.24
ug/L
1.0
0.24
1
0610511506:21
91-20-3
Styrene
<0.26
ug/L
1.0
0.26
1
06/05/15 06:21
10042-5
1,1,1,2-Tetrachloroethane
<0.33
ug/L
1.0
0.33
1
06105/1506:21
630-20-6
1,1,2,2-Tetrachloroethane
<0.40
ug/L
1.0
0.40
1
06/05/15 06:21
79-34-5
Tetrachloroethene
<0.46
ug/L
1.0
0.46
1
O6/05/15 66:21
127-184
Toluene
0.68J
ug/L
1.0
0.26
1
06/05/15 06:21
108-88-3
1,2,3-Trichlorobenzene
<0.33
ug/L
1.0
0.33
1
06/05/15 06:21
87.61-6
1,2,4-Trichlorobenzene
<0.36
ug/L
1.0
0.35
1
06/05/15 06:21
120-82-1
1,1,1-Trichloroethane
<0.48
ug/L
1.0
0.48
1
06/05/1506:21
71-55-6
1,1,2-Trichloroethane
<0.29
ug/L
1.0
0.29
1
06/0511506:21
79-00-5
Trchloroethene
<0.47
ug/L
1.0
0.47
1
06/05/15 06,21
79-01-6
Trichloro0uoromethane
<0.20
ug/L
1.0
0.20
1
06/05/15 06:21
75-694
1,2,3-Trichloropropane
<0.41
ug/L
1.0
0.41
1
06/05/15 06:21
96-184
Vinyl acetate
<0.35
ug/L
2.0
0.35
1
06/05/15 06:21
108-054
Vinyl chloride
<0.62
ug/L
1.0
0.62
1
06/05/15 06:21
75-014
Xylene (Total)
<0.66
ug/L
2.0
0.66
1
06/05/15 06:21
1330-20-7
m&p-Xylene
<0.66
ug/L
2.0
0.66
1
06/05/15 06:21
179601-23-1
o-Xylene
<0.23
ug/L
1.0
0.23
1
06/05/15 06:21
9547-6
Sunogafes
4-Bromo0uorobenzene (S)
93
%
70-130
1
06/05/15 06:21
460-004
1,2-Dichloroethane-d4 IS)
106
%
70-130
1
06/05/15 06:21
17060-07-0
Toluene-08IS)
103
%
70-130
1
0610511506:21
2037-26-5
353.2 Nitrogen, NO2IN03 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.83
mg/L
0.020
0.010
1
06/09/15 14:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/15/2015 09:54 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 16

(�15'ceAnalytical'
owwpacelabscom
QUALITY CONTROL DATA
Pace Analytical SerylCee, Inc.
98001oncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SW Samples 612
Pace Project No.:
92252696
QC Batch:
MSV/32004 Analysis Method: EPA 8260
QC Batch Method:
EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples:
92252696001, 92252696002, 92252696003
METHOD BLANK: 1475863 Matrix:
Associated Lab Samples: 92252696001, 92252696002, 92252696003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
<0.33
1.0
06/0511502:43
1,1,1-Trichloroethane
ug/L
<0.48
1.0
06105/1502:43
1,1,2,2-Tetrachloroethane
ug/L
<0.40
1.0
06105/1502:43
1,1,2-Trichloroethane
ug/L
<0.29
1.0
06/05/15 02:43
1,1-Dichloroethane
ug/L
<0.32
1.0
06/05/15 02:43
1,1-Dichloroethene
ug/L
<0.56
1.0
06/0511502:43
1,1-Dichloropropene
ug/L
<0.49
1.0
06/05/15 02:43
1,2,3-Thchlorobenzene
ug/L
<0.33
1.0
06/05/15 02:43
1,2,3-Trichloropropane
ug/L
<0.41
1.0
06105/1502:43
1,2,4-Trichlorobenzene
ug/L
<0.35
1.0
06/06/15 02:43
1,2-Dibromo-3-chloropropane
ug/L
<2.0
2.0
06/05/15 02:43
1,2-Dlbfomoethane(EDB)
ug/L
<0.27
1.0
06105/1502:43
1,2-Dichlorobenzene
ug/L
<0.30
1.0
06/05/15 02:43
1,2-Dichloroethane
ug/L
<0.12
1.0
06/05/15 02:43
1,2-Dichloropropane
ug/L
<0.27
1.0
06/05/15 02:43
1,3-Dichlorobenzene
ug/L
<0.24
1.0
0610511502:43
1,3-Dichloropropane
ug/L
<0.28
1.0
06/05/15 02:43
1,4-Dichlorobenzene
ug/L
<0.33
1.0
0610511502:43
2,2-Dichloropropane
ug/L
<0.13
1.0
06/05/15 02:43
2-Butanone (MEK)
ug/L
<0.96
5.0
06/05/15 02:43
2-Chlorotoluene
ug/L
<0.35
1.0
06/05/15 02:43
2-Hexanone
ug/L
<0.46
5.0
06/05/15 02:43
4-Chlorotoluene
ug/L
<0.31
1.0
06/05/15 02:43
4-Methyl-2-pentanone(MIBK)
ug/L
<0.33
5.0
06105/1502:43
Acetone
ug/L
<10.0
25.0
06/05/15 02:43
Benzene
ug/L
<0.25
1.0
06/05/15 02:43
Bromobenzene
ug/L
<0.30
1.0
06/06/15 02:43
Bromochloromethane
ug/L
<0.17
1.0
06/05/15 02:43
Bromodichloromethane
ug/L
<0.18
1.0
06/05/15 02:43
Bromofprm
ug/L
<0.26
1.0
06/05/15 02:43
Bromomethane
ug/L
<0.29
2.0
06/05/15 02:43
Carbon tetrachloride
ug/L
<0.25
1.0
06/05/15 02:43
Chlorobenzene
ug/L
<0.23
1.0
06/05115 02:43
Chloroethane
ug/L
<0.54
1.0
06/05/15 02:43
Chlorofomt
ugf-
<0.14
1.0
06/05/15 02:43
Chloromethane
ug/L
<0.11
1.0
06/05/15 02:43
cis-1,2-Dichloroethane
ug/L
<0.19
1.0
06/05/15 02:43
cis-1,3-Dichloropropene
ug/L
<0.13
1.0
0610511502:43
Dibromochloromethane
ug/L
<0.21
1.0
06/05/1502:43
Dibromomethane
uglL
<0.21
1.0
06/05/15 02:43
Dichlorodifluoromethane
ug/L
<0.21
1.0
06/05/15 02:43
Qualifiers
Results presented on this page am In the units Indicated by the 'Units" column except where an eliminate unit Is presented to the fight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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ZeAnalyficale
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QUALITY CONTROL DATA
Project: SW Samples 6/2
Pace Project No.: 92252696
METHOD BLANK: 1475863
Matrix:
Water
Associated Lab Samples: 92252696001,
92252696002, 92252696003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Diisopropyl ether
ug/L
<0.12
1.0
06/05/15 02:43
Ethylbenzene
ug/L
<0.30
1.0
06/05/15 02:43
Hexachloro-1,3-butadiene
ug/L
<0.71
1.0
06105/1502:43
m&p-Xylene
ug/L
<0.66
2.0
06/05/15 02:43
Methyl-tert-butyl ether
ug/L
<0.21
1.0
06/05/15 02:43
Methylene Chloride
ug/L
<0.97
2.0
06/05/15 02:43
Naphthalene
ug/L
0.25J
1.0
06/0611502:43
o-Xylene
ug/L
<0.23
1.0
06/05/15 02:43
p-Isopropyltoluene
ug/L
<0.31
1.0
06/05/15 02:43
Styrene
ug/L
<0.26
1.0
06/05/15 02:43
Tetrachloroethene
ug/L
<0.46
1.0
06/05/15 02:43
Toluene
ug/L
<0.26
1.0
06/05/15 02:43
trans-1,2-Dichloroethene
ug/L
<0.49
1.0
06/0511502:43
trans-1,3-Dichloropropene
ug/L
<0.26
1.0
06/05/15 02:43
Trichloroethene
ug/L
<0.47
1.0
06/06/15 02:43
Trichlorofluoromethane
ug/L
<0.20
1.0
06/05/15 02:43
Vinyl acetate
ug/L
<0.35
2.0
06/05/15 02:43
Vinyl chloride
ug/L
<0.62
1.0
06/05/15 02:43
Xylene (Total)
ug/L
<0.66
2.0
06/05/15 02:43
1,2-Dichloroethane-d4 (S)
%
103
70-130
06/05/15 02:43
4-Bromoguorobenzene (S)
%
98
70-130
06/05/15 02:43
Toluene-d8 (S)
%
101
70-130
06/05/15 02:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1475864
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.1
102
70-130
1, 1, 1 -Trichloroethane
ug/L
50
47.2
94
70-130
1, 1, 2,2-Tetrachloroetha ne
ug/L
50
49.6
99
70-130
1, 1, 2-Trichloroethane
ug/L
50
48.8
98
70-130
1,1-Dichloroethane
ug/L
50
48.3
97
70-130
1,1-Dichloroethene
ug/L
50
47.7
95
70-132
1,1-Dichloropropene
ug/L
50
52.2
104
70-130
1,2,3-Trcchlorobenzene
ug/L
50
50.5
101
70-135
1,2,3-Tiichloropropane
ug/L
50
52.1
104
70-130
1,24-Trcchlorobenzene
ug/L
50
55.0
110
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
51.0
102
70-130
1,2-Dibromoethane (EDB)
ug/L
50
51.8
104
70-130
1,2-Dichlorobenzene
ug/L
50
55.6
111
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
50.5
101
70-130
1,3-Dichlorobenzene
ug/L
50
53.1
106
70-130
1,3-Dichloropropane
ug/L
50
53.0
106
70-130
1,4-Dichlorobenzene
ug/L
50
52.4
105
70-130
Pace Analytical services, Inc.
9800 Riney Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Ra ults prasente l on this page are In the units Indicates by the'enlb" column except when, an aaemate unit is pmaentea to Me right or Me result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SW Samples 6/2
Pace Project No.: 92252696
LABORATORY CONTROL SAMPLE:
Parameter
1475864
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
45.0
90
58-145
2-Butanone (MEK)
ug/L
100
101
101
70-145
2-Chlorotoluene
ug/L
50
54.2
108
'70-130
2-Hexanone
ug/L
100
106
106
70-144
4-Chlorotoluene
ug/L
50
53.7
107
70-130
4-Methyl-2-pentanone (MIRK)
ug/L
100
103
103
,70-140
Acetone
ug/L
100
105
105
50-175
Benzene
ug/L
50
50.6
101
70-130
Bromobenzene
ug/L
50
53.4
107
70-130
Bromochloromethane
ug/L
50
50.3
101
70-130
Bromodichloromethane
ug/L
50
44.9
90
70-130
Bromofonn
ug/L
50
35.3
71
70-130
Bromomethane
ug/L
50
60.7
121
54-130
Carbon tetrachloride
ug/L
50
45.2
90
70-132
Chlorobenzene
ug/L
50
52.6
105
70-130
Chloroethane
ug/L
50
46.8
94
64-134
Chloroform
ug/L
50
46.6
93
70-130
Chloromethane
ug/L
50
54.9
110
64-130
cis-1,2-Dichlorcethene
ug/L
50
50.1
100
70-131
cis-1,3-Dichloropropene
ug/L
50
49.7
99
70-130
Dibromochloromethane
ug/L
50
43.4
87
70-130
Dibromomethane
ug/L
50
49.8
100
70-131
Dichlorodifluoromethane
ug/L
50
48.9
98
56-130
Diisopropyl ether
ug/L
50
50.0
100
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
Hexachloro-1,3-butadiene
ug/L
50
47.0
94
70-130
m&p-Xylene
ug/L
100
104
104
70-130
Methyl-tert-butyl ether
ug/L
50
45.2
90
70-130
Methylene Chloride
ug/L
50
56.7
113
63-130
Naphthalene
ug/L
50
53.0
106
70-138
o-Xylene
ug/L
50
51.2
102
70-130
p-Isopropyltoluene
ug/L
50
53.6
107
70-130
Styrene
ug/L
50
54.7
109
70-130
Tetrachloroethene
ug/L
50
50.7
101
70-130
Toluene
ug/L
50
50.0
100
70-130
trans-1,2-Dichloroethene
ug/L
50
48.2
96
70-130
trans-1,3-Dichloropropene
ug/L
50
49.5
99
70-132
Trichloroethene
ug/L
50
49.7
99
70-130
Trichlorofluoromethane
ug/L
50
46.9
94
62-133
Vinyl acetate
ug/L
100
107
107
66-157
Vinyl chloride
ug/L
50
49.5
99
50-150
Xylene (Total)
ug/L
150
155
103
70-130
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene(S)
%
102
70-130
Toluene-d8IS)
%
99
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Qualifiers
Results presented an this page am In the units indicated by the "Units- column except where an alternate une Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06115/2015 09,54 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 16

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QUALITY CONTROL DATA
Project: SW Samples 6/2
Pace Project No.: 92252696
QC Batch: WETA/23208 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92252696001, 92252696002, 92252696003
Pace Analytical Services, Inc.
980010ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1479274
Matrix:
Water
Associated Lab Samples: 92252696001, 92252696002, 92252696003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3
mg/L
<0.010
0.020
06/09/15 13:39
LABORATORY CONTROL SAMPLE:
1479275
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
%Rec Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/L
2.5
2.4
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1479276
1479277
MS
MSD
92252600007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD RPD Dust
Nitrogen, NO2 plus NO3
mg/L
1.4
2.5
2.5
3.6
3.5
88
87
75-125
1 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1479278
1479279
MS
MSD
92252600008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Nitrogen, NO2 plus NO3
mg/L
0.79
2.5
2.5
3.0
3.0
87
88
75-125
0 10
Results presented on this page am In the units Indicated by that 'UnW column except v m an eltemato unit W preserde4 to the right of the msvh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/15/2015 09:54 AM without the written consent of Pace Analytical Services, Inc..
Page 12 of 16

aceAnalXicala
e ..Pmbea.rorn
i
QUALIFIERS
Project: SW Samples 62
Pace Project No.: 92252696
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Ouantitabon Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Add preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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55?eAnalytical'
ewxpscmb&=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW Samples 612
Pace Project No.: 92252696
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8769092
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92252696001
SW #1
FLD/
92252696002
SW #2
FLD/
92252696003
SW #3
FLD/
92262696001
SW #1
EPA 8260
MSV/32004
92252696002
SW#2
EPA 8260
MSV/32004
92252696003
SW#3
EPA 8260
MSV/32004
92252696001
SW 91
EPA 353.2
WETA/23208
92252696002
SW#2
EPA 353.2
WETA/23208
92252696003
SIN#3
EPA 353.2
WETA/23208
Date: 06/1512015 09:54 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 14 of 16

Document Name:
aclmfkllyflcol'
Document Revised: May 18, GU1b
Pace Huntersville
Client Name: () V "/_L)
Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ Pac Other
p�E 0 lfD sfen tir .
Custody Seal on Cooler/Box Present: El yes no Seals Intact: Other —
yes ❑ no
Packing Material: ❑ Bubble VDp ❑ Bubble Bags None ❑ Other
Thermometer Used: IR Gun T1401 Type of Ice: W )Ilue None � Samples on ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooler Ternp.: 12 J C
Biological Tissue is Frozen: Yes No NIA
Date and Init g`pf p rs .exa INng_.-
1
)
contents:
Temp should be above freezing to WC
Comments:
Chain of Custody Present:
b ea ON,
ONIA
1.
Chain of Custody Filled Out:
E Wds1111,1.
ON/A
2.
Chain of Custody Relinquished:
DYes PNO
❑NIA
3.
Sampler Name & Signature on COC:
es No
ON/A
4.
Samples Arrived within Hold Time:
es ON,
❑NIA
5.
Short Hold Time Analysis <72hr :
DYes RNO
❑NIA
6.
Rush Turn Around Time Requested:
Dyes XNO
DN/A
7•
Sufficient Volume:
la es DNo
DN/A
8.
Correct Containers Used:
41 es ONO
DN/A
9.
-Pace Containers Used:
qX- No
ON/A
Containers Intact:
9 es ON,
DN/A
10.
Filtered volume received for Dissolved tests
Dye), ONO
NIA
11.
Sample Labels match COC:
11149 qVo
DN/A
12.
-Includes dateltimel10/Anal sis Matrix:
�I.
All containers needing preservation have been checked.
4Y-w ON,
DN/A
13.
All containers needing preservation are found to be In
�.v�s ONO
D WA
compliance with EPA recommendation.
exceptions: VOA, colilorm, TOC, O&G, W -DRO (water)
DYes ONO
Samples checked for dechiorination:
pea ONO
DwA
14.
Heads ace in VOA Vials >6mm :
DYes ONO
N/A
15.
Trip Blank Present:
Ores ONO
®NIA
, \NIA
16.
Trip Blank Custody Seals Present
Oyes ONO
Pace Trip Blank Lot# if urchased:--------._.------------
----
--- --- ------ ------- ---- - ----..____� ..--.----- -
Client Notification/ Resolution:
Person Contacted: Date/Time:
Comments/ Resolution:
Field Data Required? Y / N
SCURF Review: �) Date: 1 J-J /, Place label here
SRF Review: jDate: 16,l.. -. WO# : 92252696
Note: Whenever there Is a dlsaepancy affecting North Carolina compliance •s
samples, a copy of this form will be sent to the North Carolina DEHNR II'll�'lllllll I�III III
Certification Officee(Le out of hold, Incorrect preservative, out of temp,
Incorrect containers) _ 92252696
Page 15 of 16

/® CHAIN -OF -CUSTODY / Analytical Request Document o
The Chainof-Custoey is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
aceAnalytical'
ers+.aareDes.am d
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Section A Section B Section C
Pape: / of
Roquirod Client lnfohcation: Requirod Projed lMortnalion: Irnoi. lmarmatkm:
Company:
f IVI LV,
-LO B Report To: Adantpn;
J V
'
Ad e 4{ eti
Copy To:
Company Name:
REGULATORY AGENCY
ES
,.{
Address:
IF NPDES GROUNDWATER F DRINKING WATER
UST ^ RCRA r OTHER
mail To: PUmhase
Ord. No.:
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Site Location
STATE:
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Project Numpen
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DATE
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ACCEPTEDBYIAFFILIATION
DATE
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Permit Number: NCS 000 Z 5 O
Certificate of Coverage Number: NCG
or
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
FACILITY NAME GLytD-ITCA(
PERSON COLLECTING SAMPLE(S) ,4R
CERTIFIEDLABORATORV(S) ENV/RD F/Crn Lab#C?q
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2 O 1 S
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)�j]]u
0
COUNTY Saa.-ist✓rck
PHONENO. 9( /O ) . ZZ3V f_ 32 �
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
C�
-----------
-----------
-----------
-----------
-----------
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Xno
(if yes, complete Part B)
part R• Vnhirlo Ma ntannn a drfivity Mnnitnrino Renuirements
-...-_..._._....._.____._____.___.._
Outfall
Date
-
50050
00556
00530
00400
No.
Sample
Collected
Total Flow
(if applicable)
Total Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/fPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor Oil
Usage
mo/dd/vr
MG
inches
mg/1
m I
Units
gaumo
Form S W U-246, last revised 21212012
Page I of 2

STORM.EVENTCHARACTERISTICS:- -
Date 5 /D 115
Total Event Precipitation (inches):
Event Duration (hours):
4.qt
(only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and i/mprisonment for knowing violations."
/
(Signature of Perm' tee) (Date)
Form S W U-246, lust revised 21212012
Page 2 of 2

cit_7�
Glycotech REC EIVED
2271 Andrew Jackson Hwy, NE Jl1N 2 2 2015
PO Box 1956
Leland, N.C. 28451 CENTRAL FILES
910-371-2234 DWR SECTION
June 17, 2015
ATTENTION: Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Spring Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc., under permit 4NCS000258 has performed the Spring 2015
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, Glycotech, Inc. is required to perform storm water sampling and subsequent
analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD was
143 mg/L, versus the benchmark value of 120 mg/L. This is the first exceedence of COD
benchmark value. Tier I corrective action is being taken and recorded in the SWP3 Plan
per the permit requirements. The pl-1 was 5.1, with a recorded Rain -gage pH of 5.0,
therefore the benchmark values of 6.0 to 9.0 do not apply (per the permit).
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
Gary Wooten, CSM
�z4 k
EFIS Manager
Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

*4`&iA1 E
envi�r;�o,,chern
E
ANALYTICAL & CONSULTING CHEMISTS
Glycotech,Inc.
PO Box 1956
Leland NC
Attention: Gary Wooten
Lab ID Sample ID:
15-13725 Site: Outfall002
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710llowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: May 22, 2015
Customer PO #: 6012
28451 Customer ID: 09060025
Report #: 2015-05910
Project ID: Stormwater
Collect Date/Time Matrix Sampled by
5/10/2015 8:00 AM Water Client
Test Method Results Date Analyzed
COD
SM 5220D
Comment:
Reviewed by: &AA,0�Q, QQ 4WV`I.
143 mg/L 05/18/2015
Report #:: 2015-05910 Page 1 of 1

Analytical & Consulting Chemists
ENVIRONMENTAL
CHEMISTS,
OFFICE: 91 o-3 2-0223 FIAX ngton91 G-39244 45
INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
Info®environmentalchemists.com
COLLECTION AND CHAIN -OF CUSTODY
CLIENT: L CO frCId �OVC
PROJECT NAME: p 2 N 2Ut !r
REPORT NO: S� D J �IiD
ADDRESS: ZZ% / 2 %Jfe�fOd dW
CONTACT NAME: O E N
PO NO: (oO / 2—
(R4lu<o /VC UV,-1
REPORT TO: oaTF.
PHONE/FAX: q/6 -3 %I - Z Z3fe X37,
COPY TO: VJAvfjrs
email: . [uae en 09 /ycOfra4cnc - Ca A
Sampled Bv: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
d y
E
a
m n
E `0 7
o
_
= 7
= `o
U 6
m
c
8 E
G
¢
O W
m
g Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
i
i
z
a
o
i
xp
i
e
€
W
G
Gt yco�cH
OuTFAct, 002,
10 15
0800
IAMB
S?
C
P
Z
STbR.n w41�Z
IV?D 6-5 C O D
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
—E—
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Datelrime
Received By:
Daterrime
t.
2.
Temperature whe eceived• Accepted:
Delivered By: ��y R
< 2,n W < 2 "C TURNAROUND:

II4IPORANT NOTICE
C aralinaDivison of Water Qaatity (NCDWQ) is strictly enforcing EPA regol2tians far sample collection aodpreservation_
Client Must Provide the Following Information
1_ SAMPLE IDENTIFICATION (Cmtaiaer Asso iatedwith regaestedtesting)
2_ SAMPLE TYPE (Composite, Grab. Water, Sail. dta)
3. DATE COLLECTED
1. TIME COLLECTED
S. SAMPLE COLLECTOR
i. PRESERVATR)N(Imcrd"ugTmperahtremdpl3)
Te•perature Samples BHJSr be refrigerated arreeeived on ice between 2 and d•C_
Samplesreceivedwitbm two (2) bows ofcollationmast shawa downward trend_
Therefore; please retard temperature at coHecdon in space provided onmitecdon sheet
A two (2) haarlimt tu rbemirallypmwrve sample bypH adjostmentis allowed, except
formetals samples reported to the Gromdwater Sectionwkch coos- be acidified at the time efeolteetioo_
Cspliol<
These sample baffles may contain small amounts of avid or other corrosive and potentially 1 fd chemicals_Laborahnies are required to add
these chemicals for calm analyses in order
to comply with EPA preservationrequremeots Use eaireme ore when opening and handing
the botfles_ Hany chemical should get anyear skin or domes Bash lrbaallywithwater and seek medical attention_
DECffi.ORINATION INST3tIJCI1ONS
CAIMON: DO NOT NUXthiomifatewith add is buWebdnrecallstni= wonder as a vin&M rmctim wi pa=_
Derilnainatinw Samples that ReapireAdd Freservatiw
1_ Add 4 5 granules ofthiasuffate to abode with no and preservative_
2_ After mixing to dissolve the thiosulfalx, puurhalf of the sample into aboule containing acid
as apresavafive_ (AmmoniatT1 N)
3 _ Then moupletely fill both bottles with fresh sample_
'Arecmd of date ralechA time coUecWL sample collector, and nse orproper preservatives Lost be=aintained Eachmnple must desdyindicale The State ofWadh Carolina
cdtecfim site mat reeardhausmpRms- Rd NCAC 2H 0ZO5 (a)(i) M_
t�
`At any fine alaharatoryreceives mmpleswhichdo notmed sample collection. booing time, or presttvahmrequirments, the hilmatmymust nobfythe maple collector or
them and secure anaTh'be seeuedL The original ample maybe aoalyscdbot be resolarepmtdmust be qua riedwiththenature
of the idraetiun(s) and the laboratory must nu fy the Sate LabouLry abort the idractiae(4 The notificatim meet iodode a sbftmeot iodcmective aetisos taken t ,
preveni The pnbba for filon ample&- Rd NCAC 2H 0905 (a) () (Nl

Stormwater Discharge ®utfall (SD®)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: http://portal.ncdenr.or¢/web/wg/ws/su/nodessw#tab-4
Permit No.: N/C/5/ Ol0/ol2 /Sl Sl or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Facility Name: GIYGOTFCH XAIC
County: _
Inspector:
(i2v.usWICk Phone No. 371-7-2-3'r E>G 32
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): LI, 9�
Was this a Representative Storm Event? (See information below) [Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vmy).
A `Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signatyr;,)[ certify teat tlys report is accurate and complete to the best of my knowledge:
(Signature of Permitttee or Designee)
1. Outfall Description:
Outfall No. 0 2 nn StrucI r (pr e, ditch, etc.)
Receiving Stream: /-! I y�i �r, ,A RFF GE
Describe the industrJ}'1I activities that occur within the outfall drainage area:
(�rAEM I t 4t, inn w,4 F,4 e Tv2,N
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as
0.1
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /(ONE
Page 1 of 2
SWU-242-20120613

4. Clarity: Choose the number which best describes the charity of the discharge, where I is clear
and 5 is very cloudy:
O 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
1 G 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
S. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Mo IV E
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may
be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242-20120613

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Akzo Nobel Surface Chemistry LLC COUNTY Rowan
PERSON COLLECTING SAMPLE(S) Leonard White PHONE NO. [phone]
CERTIFIED LABORATORY(S) Pace Analytical Services, Inc.Lab # 37706
Lab # 12
SIGNATURE OF PERMITTEE OR DESIGNEE
REOUIRED ON PAGE 2.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 Ins NO3
pH
mo/dd/ r
MG
inches
m L
m L
m L
SIU
SW-1
11/17/2014
.3
0.0218
0.001
0.058
SW-2
11/17/2014
.3
0.001
0.014
0.002
*REC9RAM
SW-3
11/17/2014
.3
<0.001
0.022
0.071
DEC 2 3 am
SW-4
11/17/2014
No Flow
No Flow
No Flow
No Flow
No Flow
VMIN AL FII
ES
C
)N
*= Within Benchmark values
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
inches
m /I
m
unit
gaumo
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date 11/18/2014
Total Event Precipitation (inches): .3
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility.of fines and imprisonment for knowing violations."
re of Pei•mittee)
1 Rr
(Date
Form SWU-247, last revised 21212012
Page 2 of 2

aceAnalXical e
wwivpaceleba.mm
November 26, 2014
David Simons
Akzo Nobel
485 Cedar Springs Rd.
Salisbury, NC 28147
RE: Project: SW
Pace Project No.: 92226124
Dear David Simons:
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
`Sincerely,
CCwJ�OJ�—
Liamm Carrubba
[e-mail]
Project Manager
Enclosures
cc: Todd Barnhardt
Leonard White, Akzo Nobel
*149o
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 11

aceAnalytical
w 'P&C*Ucorn
Project: SW
Pace Project No.: 92226124
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florda/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
L'rn
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
uF^
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 11

Pace Analytical Services, Inc.
aceAnalytical ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
mwpamlabs.00m [phone]
SAMPLE SUMMARY
Project:
Pace Project No.:
SW
92226124
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92226124001
SW-1
Water
11/17/1410:35
11/18/1416:00
92226124002
SW-2
Water
11/17/1410:40
11/1811416:00
92226124003
SW-3
Water
1111711410:40
1111811416:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 11

aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Ana"cal Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project:
Pace Project No.:
SW
92226124
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92226124001
SW-1
EPA 8260
JDW7
5
PASI-C
EPA 353.2
DIAN
1
PASI-A
92226124002
SW-2
EPA 8260
JDW1
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92226124003
SW-3
EPA 8260
JDW7
5
PASI-C
EPA 353.2
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 11

aceAnalytical.
wwwoscelab&M
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW
Pace Project No.: 92226124
Sample: SW-1
Lab ID: 92226124001 Collected:
11/17/1410:35
Received:
11/18/1416:00 Matrix: Water
Parameters
Results Units POL
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
21.8 ug/L 1.0
0.12
1
11/19/14 18:36
107-06-2
Toluene
0.38.1 ug/L 1.0
0.26
1
11/19/14 18:36
108-88-3
Surrogates
4-Bromofluorobenzene (S)
106 % 70-130
1
11/19/14 18:36
460-00-4
1,2-Dichloroethane-d4 (S)
115 % 70-130
1
11/19/14 18:36
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
11/19/14 18:36
2037-26-5
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.58 mg/L 0.020
0.010
1
11/25/14 22:44
Sample: SW-2
Lab ID: 92226124002 Collected:
11/17/1410:40
Received:
11/18/1416:00 Matrix:Water
Parameters
Results Units PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
0.67.1 ug/L 1.0
0.12
1
11/19/14 19:07
107-06-2
Toluene
1.4 ug/L 1.0
0.26
1
11/19/14 19:07
108-88-3
Surrogates
4-Bromofluorobenzene (S)
105 % 70-130
1
11/19/14 19:07
460-00-4
1,2-Dichloroethane-d4 (S)
119 % 70-130
1
11/19/14 19:07
17060-07-0
Toluene-d8 (S)
97 % 70-130
1
11/19/14 19:07
2037-26-5
353.2 Nitrogen, N021NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
2.0 mg/L 0.020
0.010
1
11/25/14 22:45
Sample: SW-3
Lab ID: 92226124003 Collected:
11/1711410:40
Received: 11/18/1416:00 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
<0.12 ug/L 1.0
0.12
1
11/19/14 19:23
107-06-2
Toluene
2.2 ug/L 1.0
0.26
1
11/19/14 19:23
108-88-3
Surrogates
4-Bromofluorobenzene (S)
105 % 70-130
1
11/19/14 19:23
460-00-4
1,2-Dichloroethane-d4 (S)
116 % 70-130
1
11/19/14 19:23
17060-07-0
Toluene-d8(S)
99 % 70-130
1
11/19/14 19:23
2037-26-5
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.71 mg/L 0.020
0.010
1
11/25/14 22:48
Date: 11/26/2014 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 11

aceAnalytical
mmpace/aba.cwn
QUALITY CONTROL DATA
Project: SW
Pace Project No.: 92226124
QC Batch: MSV/29320 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92226124001, 92226124002, 92226124003
METHOD BLANK: 1333653
Matrix:
Water
Associated Lab Samples:
92226124001, 92226124002, 92226124003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,2-Dichloroethane
ug/L
<0.12
1.0
11/19/14
15:29
Toluene
ug/L
<0.26
1.0
11/19/14
15:29
1,2-Dichloroethane-d4 (S)
%
115
70-130
11/19/14
15:29
4-Bromofluorobenzene (S)
e/
105
70-130
'11/19/1415:29
Toluene-d8 (S)
%
98
70-130
11/19/14
15:29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1333654
Spike LCS
LCS
e/ Rec
'Parameter
Units
Conc. Result %Rec
Limits Qualifiers
1,2-Dichloroethane
ug/L
50
52.9
106
70-130
Toluene
ug/L
50
50.9
102
70-130
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
1333655
'' n
92224363013
Spike
MS
MS
%Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,2-Dichloroethane
ug/L
NO
20
20.8
104
70-130
Toluene
ug/L
NO
20
21.1
105
70-155
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromolluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
98
70-130
SAMPLE DUPLICATE: 1333656
92226055002
Cup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
1,2-Dichloroethane
ug/L
NO
<0.12
30
Toluene
ug/L
NO
<0.26
30
1,2-Dichloroethane-d4 (S)
%
117
117
0
4-Bromofluorobenzene (S)
%
104
105
1
Toluene-d8 (S)
%
98
98
0
Results presented on this page are In the units Indicated by the'UhrW column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11

6
aceAnalytical
..paa4ebaccm
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW
Pace Project No.: 92226124
QC Balch: WETA/21054
Analysis Method: EPA
353.2
QC Balch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92226124001, 92226124002,
92226124003
METHOD BLANK: 1338721
Matrix: Water
Associated Lab Samples: 92226124001, 92226124002,
92226124003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
<0.010 0.020
11/25/14 22:15
LABORATORY CONTROL SAMPLE: 1338722
Spike LCS
LCS %Rec
Parameter Units
Conc. Result
%Rec Limits Qualifiers
Nitrogen, N0Z plus NO3 - - mglL- - -
2:5- 2.5-
100 90-110
MATRIX SPIKE& MATRIX SPIKE DUPLICATE: 1338723 1338724
_
MS MSD
92226079004
Spike Spike MS
MSD MS MSD
e/ Rec Max
Parameter Units Result
Conc. Conc. Result
Result e/ Rec e/ Rec
Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.36
2.5 2.5 2.6
-2.6 91 90
75-125 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1338725 1338726
al:•�
MS MSD
92226079005
Spike Spike MS
MSD MS MSD
%Rec Max
Parameter Units Result
Conc. Conc. Result
Result e/ Rec %Rec
Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.41
2.5 2.5 2.7
2.7 91 91
75-125 0 10
Results presented on this page are In the units Indicated by the "Unm" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2014 04:10 PM without the written consent of Pace Analytical Services, Inc..
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aceAnalytical
v ..Pace/abs.com
QUALIFIERS
Project: SW
Pace Project No.: 92226124
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calwlate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC — Not Calculable. -
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each. analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES . t'
PASI-A PaceAnalytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Date: 11/26/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

aceAnalytical e
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW
Pace Project No.: 92226124
Lab ID Sample ID QC Batch Method QC Batch
92226124001
SW-1
EPA 8260
MSV/29320
92226124002
SW-2
EPA 8260
MSV/29320
92226124003
SW-3
EPA 8260
MSV/29320
92226124001
SW-1
EPA 353.2
WETA/21054
92226124002
SW-2
EPA 353.2
WETA121054
92226124003
SW-3
EPA 353.2
WETA121054
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Analytical Method Batch
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2014 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 11

' �'�cealaryflcal"
61
`a
Client Name: 9-r K- ­1 I
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ 'Commercial❑ 1!�R Other I'Mo
CustodySeaton CoolerlBox Present: El n/ ❑ no 'p
Y � Seals intact: El '
Packing Material: ❑ Bubble VQp ❑ Bubbldf[ a s ❑ None❑ Other
Thermometer Used: IR Gun T 40 Type of Ice( wgt Blue None Samples on Ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooler Temp.: .0
Biological Tissue Is Frozen: Yes No wA
Date and Initials of pars n examining
., contents: c,,
Temp should be above freezing to VC
Comments:
Chain of Custody Present:
des ONO
ON/A
1.
Chain of Custody Filled Out:
Yes ONO
ON/A
2.
Chain of Custody Relinquished:
- Y6` 01,10
❑NIA
3.
Sampler Name & Signature on COC:
Yes [IN,
❑NIA
4.
Samples Arrived within Hold Time:
Yes ONO
❑NIA
5.
Short Hold Time Analysis <72hr :
OYes tro 15141A
6.
Rush Turn Around Time Requested:
OYes lo'ON/A
7.
Sufficient Volume:
'OYes 'No
ON/A
8.
Cor'rect.Containers Used:
Yes ONO
ON/A
9.
-Pace Containers Used:
'ElYYeess ONO'
❑NIA
c+r
Containers Intact:
8'& ON.
❑NIA
10.
Filtered volume received for Dissolved tests
OYes ONO
1:20C
11
Sample Labels match COC:
SOY s Ono
ON/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservallon have been checked.
"ONO ❑No
❑N/A
13,
/
All containers needing preservation are found to be in
as ONo
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, wI-DRO (water)
OYes o
Samples checked for dechlorination:
Yes 6No
❑NIA
14,
Heads ace in VOA Vials >6mm :
OYes ONO
PINr
15.
Triptlank Present:
OYes ONO
Erh/A
16.
Trip Blank Custody Seals Present
Ores ONO
❑Nly.
Pace Trip Blank Lot # if purchased):
•/
Client Notification) Resolution: Field Data Required? Y I N
Person Contacted:
Comments/ Resolution:
Dale/Time:
SCURF Review: _(J/ Date: (•
SRF Review: Date: I I i 2v l y
Note: Whenever there Is a discrepancy affecting North Carolina complian
samples, a copy of this form will be sent to the N6th Carolina DEHNR
Certification Office ( Le out of hold, Incorrect preservative, out of temp,
Incorrect containers)
WO 92226124`_---
•IIIIIIIIIIIIIIIIIIIIII�
—
(if no label available)
Page 10 of 11

a
/, -ace Analytical
_ .w.nacelahs.mm
CHAIN -OF -CUSTODY / Analytical Request Document
The Clain-cfCusp ply is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
p
Pb9e: - -�- of
Section A .Section B -., i Sgction C �; I
Required Client Information: Requited Project Information: Invoice Information:
Company. I/ZD �1 /D (_,C r Rcpon To: Anention:
I� (V fl 1
1790068
Ad css: �Q -
Copy To:
Company Name:
REGULATORY AGENCY
-+ 3?•'i- VSLI-
Mon.:
F NPDES - T GROUND WATER DRINKING WATER
i UST RCRA OTHER
Email To: -
Purcnase Order No.:
Pam Duos
W....
Pmjpa Name:
Pam P'.
Location
Mmiaw,
.Site
STATE.,
Requested Out DatelTAT: Z6 (�
Project Number.
Papa `o'. r. 1 1-�
`
1
Requested Analysis Filtered (YIN)'
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Section D Matrix Codes
ftaqulmd Gbnl ln.'a'mation MATRIx r c DE
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2.
COLLECTED
Preservatives
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Sample lDs MUST BE UNIQUE Tosee TS
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ADDITIONAL COMMENTS.
RELINQUISHED BY I AFFILIATION
`DATE
TIME
ACCEPTEDBY/AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
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SAMPLER NAME AND SIGNATURE
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PRINT Name of SAMPLER:
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SIGNATURE o/SAMPLER:
DATE Signed
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(MMIDDIYY): 1
rn
�mpo�ai'rvo' oY v9mry mu imm Yw ae aaxGun9rrns.ve.-.'Payment mrmsam'roan,too:eGlmgas."".mr mvodms net poe w'. au pa'.
r -ALL-U-u[UreY.O (. 15-May-20 W

it
AkzoNobel
Surface Chemistry
485 Cedar Springs Road T+ 1 704 633 1731
Unit A F + 1 704 637 8912
Salisbury, NC 28147 w .akzonobel.com/sc
USA
AkzoNobel
Tomorrow's Answers Today
March 25, 2014
NCDENR — Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Certified Mail: Return Receipt Requested
Reference: Semi -Annual Permit Monitoring Report
Individual Stormwater Monitoring Permit
AkzoNobel Surface Chemistry LLC.
Permit No. NCS000259
Attached are two copies of the AkzoNobel monitoring results for Year 5- Period
2(sample 10) for our permit # NCS000259 for the samples collected March 7, 2014. Any
questions on this submittal you may contact me at 704-642-6203.
RECE'
Regards,
v�D
D APR 0 7 2014
Thom Andersen DWQ/BOG V
Waste Management Supervisor
AkzoNobel Surface Chemistry, LLC, Salisbury, NC
Copy: Brian Owens AkzoNobel Surface Chemistry, LLC, Salisbury, NC
David Simons AkzoNobel Surface Chemistry, LLC, Salisbury, NC

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000259 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Akzo Nobel Surface Chemistry LLC
PERSON COLLECTING SAMPLE(S) Chris Simon
CERTIFIED LABORATORY(S) Pace Analytical Services. Inc.Lab # 37706
COUNTY Rowan
PHONE NO. [phone]
Lab# 12
SIGNATURE OF PERMITTEE OR DESIGNEE
Part A: Specific Monitoring Requirements I REQUIRED ON PAGE 2.
Outfall
Date
50050
No.
Sample
Collected
Total
Flow if a
Total
Rainfall
1,2-
Dichloroethane
Toluene
Nitrogen
NO2 plus NO3
pH
mo/dd/ r
MG
inches
m /L
m /L
m /L
SIU
SW-1
03/07/2014
2.1
<0.001
<0.001
0.57
6.28
SW-2
03/07/2014
2.1
<0.001
0.054
0.18
16.93
SW-3
03/07/2014
2.1
<0.001
0.0016
0.17
6.62
SW-4
03/07/2014
2.1
<0.001
<0.001
.039
6.73
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitorino Remdrements
Outfall
No.
Date
Sample
Collected
150050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(ifappl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
JMG
inches
m /I
mg/1
unit
al/mo
Form SWU-247, last revised 21212012
Paget of2

STORM EVENT CHARACTERISTICS:
Date 03/07/2014
Total Event Precipitation (inches): 2.1
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belie', true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
includ)np, the possibility pif fines and imprisonment for knowing violations."
J31297 as 19—
(Date)
Form SWU-247, last revised 21212012
Page 2 of 2

aceAnalytical e
awwpscelabs.com
March 14, 2014
Mr. Thom Andersen
Akzo Nobel
485 Cedar Springs Road
Salisbury, NC 28147
RE: Project: 3/7/14 AKZO
Pace Project No.: 92192435
Pace Analytical Services, Inc.
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Andersen:
Enclosed are the analytical results for sample(s) received by the laboratory on March 07, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

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CERTIFICATIONS
Project: 3/7/14 AKZO
Pace Project No.: 92192435
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Dunking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE SUMMARY
Project: 3r7/14 AKZO
Pace Project No.: 92192435
Lab ID
Sample ID
Matrix
Date Collected
Data Received
92192435001
SW1
Water
03107/1410:40
0310711413:12
92192435002
SW2
Water
03107/1410:50
03/0711413:12
92192435003
SW3
Water
03/07/1410:50
03/07/1413*12
9219243SO04
SW4
Water
03107/1410:55
03/07/1413:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Hunlereville, NC 28078
[phone]
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aceAnalytical s
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 26078
[phone]
Project:3!7114 AKZO
Pace Project No.: 92192435
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92192435001
SW1
EPA 8260
MCK
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92192435002
SW2
EPA 8260
MCK
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92192435003
SW3
EPA 8260
MCK
5
PASI-C
EPA 353.2
DMN
1
PASI-A
92192435004
SW4
EPA 8260
MCK
5
PASI-C
EPA 353.2
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalylical e
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 317114 AKZO
Pace Project No.: 92192435
Sample: SW1
Lab ID: 92192435001
Collected:
03/07/14 10:40
Received:
03/07/14 13:12 Matrix: Water
Parameters
Results Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
<0.12 ug/L
1.0
0.12
1
03/12/14 05:48
107-06-2
Toluene
<0.26 ug/L
1.0
0.26
1
03/12/14 05:48
108-88-3
Surrogates
4-Bromofluorobenzene (S)
101 %
70-130
1
03/12/14 05:48
460-00-4
1,2-Dichloroethane-d4 (S)
89 %
70-130
1
03/12/14 05:48
17060-07-0
Toluene-d8(S)
98 %
70-130
1
03/12/14 05:48
2037-26-5
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.67 mg/L
0.020
0.020
1
03/11/14 18:32
Sample: SW2
Lab ID: 92192435002
Collected:
03/07/14 10:50
Received:
03/07/14 13:12 Matrix: Water
Parameters
Results Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
0.79.1 ug/L
1.0
0.12
1
03/12/14 06:04
107-06-2
Toluene
54.0 ug/L
1.0
0.26
1
03/12/14 06:04
108-88-3
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
03/12/14 06:04
460-004
1,2-Dichloroethane-d4 (S)
90 %
70-130
1
03/12/14 06:04
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
03/12/14 06:04
2037-26-5
353.2 Nitrogen, NO2/NO3 pros.
Analytical Method: EPA 353.2
Nitrogen,'NO2 plus NO3
0.18 mg/L
0.020
0.020
1
03/11/14 18:33
Sample: SW3
Lab ID: 92192435003 Collected:
03107/1410:50
Received: 03/0711413:12 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
<0.12 ug1L 1.0
0.12
1
03/12/14 06:20
107-06-2
Toluene
1.6 ug/L 1.0
0.26
1
03/12/14 06:20
108-88-3
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130
1
03/12/14 06:20
460-00-4
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
03/12/14 06:20
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
03/12/14 06:20
2037-26-5
363.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.17 mg/L 0.020
0.020
1
03/11/14 18:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 03/14/2014 11:22 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 13

aceAnalytical e
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 3/7/14 AKZO
Pace Project No.: 92192435
Sample:.SW4
Lab ID: 92192435004
Collected:
03/07/14 10:55
Received: 03/07/14 13:12 Matrix: Water
Parameters
Results Units
PQL
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
1,2-Dichloroethane
<0.12 ug/L
1.0
0.12
1
03/12/14 06:36
107-06-2
Toluene
<0.26 ug/L
1.0
0.26
1
03/12/14 06:36
108-88-3
Surrogates
4-BromoBuorobenzene (S)
100 %
70-130
1
03/12/14 06:36
460-00-4
1,2-Dichloroethane-d4 (S)
92 %
70-130
1
03/12/14 06:36
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
03/12/14 06:36
2037-26-5
353.2 Nitrogen, NO2IN03 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.039 mg/L
0.020
0.020
1
03/14/14 00:09
Mi
Date: 03/142014 11:22 AM
REPORT OF LABORATORY ANALYSIS
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aceAnalylical e
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 3/7/14 AKZO
Pace Project No.: 92192435
QC Batch: MSV/26053 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92192435001, 92192435002, 92192435003, 92192435004
METHOD BLANK: 1154673
Matrix:
Water
Associated Lab Samples:
92192435001, 92192435002, 92192435003, 92192435004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,2-Dichloroethane
ug/L
<0.12
1.0
03/12/14 04:15
Toluene
ug/L
<0.26
1.0
03/12/14 04:15
1,2-Dichloroethane-d4 (S)
%
90
70-130
03/12/14 04:15
4-Bromofluorobenzene (S)
%
101
70-130
03/12/14 04:15
Toluene-d8 (S)
%
98
70-130
03/12/14 04:15
LABORATORY CONTROL SAMPLE:
1154674
Parameter
Units
1,2-Dichloroethane
ug/L
Toluene
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Spike LCS LCS
Conc. Result % Rec
50 46.5 93
50 51.4 103
89
102
99
% Rec
Limits Qualifiers
70-130
70-130
70-130
70-130
70-130
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1154675
1154676
MS
MSD
92192618005 Spike
Spike
MS
MSD MS
MSD
% Rec Max
Parameter
Units Result Conic.
Conc.
Result
Result %Rec
%Rec
Limits RPD RPD Qual
Toluene
ug/L NO 50
50
51.1
54.3 102
109
70-155 6 30
1,2-Dichloroethane-d4 (S)
%
89
69
70-130
4-Bromofluorobenzene(S)
%
101
-103
70-130
Toluene-d8 (S)
%
98
98
70-130
Date: 03/14/2014 11:22 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 13

aceAnalytical.
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QUALITY CONTROL DATA
Project: 317/14 AKZO
Pace Project No.: 92192435
QC Batch: WETA/18321 Analysis Method: EPA 353.2
OC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92192435001, 92192435002, 92192435003
METHOD BLANK: 1154789 Matrix: Water
Associated Lab Samples: 92192435001, 92192435002, 92192435003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,,NO2 plus NO3 mg/L <0.020 0.020 03111/1418:01
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1154790
Spike LCS LCS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2.6 105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1154791 1154792
MS MSD
92192104002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conic. Conic. Result Result % Rec °% Rec Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.029 2.5 2.5 2.3 2.3 91 91 75-125 1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1154793 1154794
MS MSD
92192220001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 7.5 2.5 2.5 9.9 10 95 99 75-125 1 20
Date: 03/14/2014 11:22 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 13

aceAnalytical e
~Pscelabs.mxi
QUALITY CONTROL DATA
Project: 3/7/14 AKZO
Pace Project No.: 92192435
QC Batch: WETA/18351 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92192435004
METHOD BLANK: 1157246
Associated Lab Samples: 92192435004
Parameter Units
Nitrogen, NO2 plus NO3 mg/L
LABORATORY CONTROL SAMPLE: 1157247
i
Parameter Units
Nitrogen, NO2 plus NO3 mg/L
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
<0.020 0.020 03/14/14 00:07
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.6 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1157250 1157251
MS MSD
92192435004 Spike Spike MS MSD MS MSD %Rec Max
'Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.039 2.5 2.5 0.96 0.93 37 36 75-125 3 20 Mt
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1157252 1157253
MS MSD
. 92192851001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qua[
Nitrogen, NO2 plus NO3 mg/L 0.40 2.5 2.5 2.7 2.7 93 92 75-125 0 20
Date: 03/14/2014 11:22 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

aceAnalytical"
~..pecabbs.=
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 3f7I14 AKZO
Pace Project No.: 92192435
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL- Pace Reporting Limit.
RL— Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP- Sample Duplicate
RPD - Relative Percent Difference
NC.- Not Calculable.
SG - Silica Gel - Clean -Up
U Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE;QUALIFIERS
M1 , Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/142014 11:22 AM without the written consent of Pace analytical Services, Inc.. Page 10 of 13

aceAnalytical"
w pacelabsxwn
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 3!7/14 AKZO
Pace Project No.: 92192435
Lab ID Sample ID QC Batch Method QC Batch
92192435001
SW1
EPA 8260
MSV/26053
92192435002
SW2
EPA 8260
MSV/26053
92192435003
SW3
EPA 8260
MSV/26053
92192436004
SW4
EPA 8260
MSVI26053
92192436001
SW7
EPA 353.2
WETA/18321
92192435002
SW2
EPA 353.2
WETA/18321
92192435003
SW3
EPA 353.2
WETAI18321
92192435004 SW4 EPA 353.2 WETA118351
Analytical Method
Analytical
Batch
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/14/2014 11:22 AM without the when consent of Pace Analytical Services, Inc.. Page 11 of 13

e� Document Name: I Document Revised: uecemuet ia, �u is
%,,F3ceAr t19 rat` Sample Condition Upon Recei t. SCUR Pa e t of 2
Document Number.' Issuing Authority:
F-CHR-CS-03-rev.13 i Pace Huntersville.Quality Office
Client Name: NL.M A bird
Courier. O� Fed•Ex D UPSO uSPSO, Client0, commercial Pace Other 0 honal
Custody Seal onCoolerlBoxPresent: . 0 yes no Seals intact: Eli yes 0no Pro) Dlie:Date
6 666 Pro) Name
Packing Material,- 0 Bubble Wrap © Bubble Bags 0 None ❑ Other
i
Thermometer Used: IR Gun T1102 301� Type of Ice: ill Blue None L,u Samples on ice, cooling,process has beguni
r......, r.....,..w:..., o-..�... Tin!) Nn rinrrortinn T1 Zn Nn Cnrrartinn f
'G
Biological Tiis Frozen: Yes NO WA
g Tissue
Date and Initials of person examining
CorrectedCoolerTemp.: 7 c
contents:�lJe1'
Temp should be above fieezingto 6°C
Comments:
,Chain of Custody Present:
Yes ONO
ONIA
1.
Chain of Custody Filled Out:
es ONO
ONIA
2.
Chain of Custody eli�n ulsh—e :
' Yes ONO ONIA
T
Sampler Name & Signature on: COC:
Q,,rY`es ONO
ONIA
4,
Samples Arrived within Hold Time:
„dyes
❑N/A
5.
Short Hold Time Analysis (c72hr):
� ,,❑NNO
QYes no
y�
ONIA
6.
Rush Turn Around Time Requested:
Dyes PNO
ONIA
7.
Sufficient. Volumes
,,ores ONO
❑NIA
8.
Correct Containers Used:
plyes ONO
ONIA
9.
-Pace Containers Used:
wes. ONO
❑NIA.
Containersfntacl
OYes ONO
13 N/A
10:
Filtered volume received for Dissolved tests
❑Yes ONO
QN/A
11.
Sample Labels match COC:
Yes ❑No
❑NIA
'12.
-includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
k3Y`es El No
ONIA
13.
AW containers needing preservation are found to be in
es ONO
Yes
ONIA
compliance with EPA recommendation.
exceptions: VOA, colifbrm, TOC, 0&G, WI-DRO (water)
Yes ONO
Samples checked for dechlorination:
Q4 ONO
ON/A
'14.
Heads ace in VOA Vials (>6mm):
QGes ONO
ONIA
15.
Trip Blank Present:
❑Yes ONO
ONIA
16.
Trip Blank Custody Seals Present
❑Yes ONO
VNIA
Pace Trip Blank Lot # (if purchased):
Client Notification/Resolution:
Person Contacted: _
Comments/ Resolution:
Date/Time:
SCURF Review: Date: S 1
SRF Review: Date: I1 1
Note: Whenever there is a discrepancy affecting North Carolina compliance.
samples, a coi this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of ter
incorrect containers)
Field. Data Required? Y I N
Place label,here
W0#:921192435
, I7IIIIluI III u.ul. I
— 92192436,
_— Page 12 of 13

/ .P ceAt a tic l'
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CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant holds must be completed accurately.
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