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HomeMy WebLinkAboutNCG030124_DMR_202103083/3/2021 Submission Completed G Stormwater NPDES Permit Data Monitoring Report NC Department of Environmental Quality F wtlI mUROQL�rv�ry (DMR) Upload Received MAR 0 8 20111 Winston-Salem Regional Office Permit and Facility Information: f le.ue enter the permit number and other details for this upload, __.............__.._. _.... __.........._.... IMPORTANT. Until the eDMR system is implemented for DEMLR Stormwater Program permits, an original signed hardcopy of the DMR MUST be mailed to the address in your permit, in addition to this electronic upload. Fields marked with a red asterisk are required. Permit Number* Enter COC or Individual Permit Number (NOT General Permit number with all 0's) NCG030124 Must begin with NCS or NCG Facility Name: * Wieland Copper Products, LLC County: * Stokes After uploading here, the original signed hardcopy must be mailed to: DEQ Winston-Salem Regional Office Attn: DEMLR Stormwater Program 450 West Hanes Mill Road Suite 300 Winston-Salem, NC 27105 Further contact details at https://deq.nc.gov/contact/regional-offices/winston- Salem Monitoring Period Information: Monitoring Period What is the YEAR of the sample date(s)? Year:* 2021 Multiple DMRs from sampling periods within the same year can be uploaded together, but please upload different years with a new submittal form. hUps://edocs.deq.nc.gov/Forms/Form/Submit 1/2 3/3/2021 Submission Completed Also, copies of the lab results and qualitative (visual) monitoring should NOT be submitted unless specifically requested by DEQ staff. Only upload the completed and signed DMR forms. DMR Upload* Click the upload button or drag and drop files here to attach document. Stormwater Report First QTR 2021.pdf 2AMB Only PDFs are accepted. Comments: WCP is in Tier 1 for TSS for Outfall 001. My investigation of the area revealed that the demolition crew is using the dirt and gravel road and driving on it with heavy trucks and equipment. The demolition of the old equipment should be completed within a month or so. We will replace the gravel once the work has been completed. * By checking the box and signing box below, I certify that: o I have given true, accurate, and complete information on this form; o I agree that submission of this Data Monitoring Report (DMR) upload form is a "transaction" subject to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act"); o I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act"); o I understand that an electronic signature on this upload form has the same legal effect and can be enforced in the same way as a written signature; AND o I intend to electronically sign and submit this DMR upload form. Full Name:* Tony Ryan Sprinkle Name of person submitting this form Email Address: * tony.spdnkle@wieland.com Phone Number: * 336-445-4526 Signature: * Date: * 03/03/2021 https://edocs.deq.nc.gov/Forms/Form/Submit 2/2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS NCG030124 FACILITY NAME Wieland Copper Products, LLC PERSON COLLECTING SAMPLE(S) Clifford Cain CERTIFIED LABORATORY(S) Pace Analytical -Eden Lab # 633 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2021 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Stokes PHON 6 445 4526 SIGNATURE OF PERMITTEE OR DESIGNEE REOUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow ifs Total Rainfall TSS Total CU Lead Oil &Grease Total Zinc PH mo/ddtvr MG inches mA m/I m/I m/1 m/l 001 2/11/21 0.534 1.00 155 1.23 0.0098 9.1 0.0829 6.7 002 2/11/21 0.099 1.00 9 0.176 ND ND 0.039 6.7 003 1 2/11/21 1 0.192 1 1.00 1 47 1.64 1 ND ND 1 0.134 6.8 004 2/11/21 0.309 1.00 20 0.750 ND ND 0.067 6.8 005 2/11/21 0.347 1.00 52 0.708 ND ND 0.057 6.6 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Qyes Ono (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/PPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m /l MCA unit al/mo N/A Form SWU-247, last revised 611212015 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 2/11/21 Total Event Precipitation (inches): 1.00 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable— see permit.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." K gVLG /)O2it (Sig ermittee) (Date) Form SWU-247, last revised 611212015 Page 2 of 2 Footnotes: 1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes For purposes of this permit the definitions of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facilities sub*t to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.1 1; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode my tube manufacture use the definition found in 40 CFR 469.31). Facilities that develop a solvent management plan to be incorporated into the Stotmwater Pollution Prevention Plan may make a request to DWQ that monitoring of total toxic organics be waived The solvent management plan shall include a list of the total toxic organic compounds used; the method of disposal used instead of dumping, such as reclamation, contract hauling, or incineration; and the procedures for assuring that toxic organics do not routinely spill or leak into the stonnwater. For those facilities allowed such a waiver, the discharger shag include the following signed certification statement on the discharge monitoring report. "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stonnwater or areas which are exposed to rainfall w stonnwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the solvent management plan included in the Stormwater Pollution Prevention Plan" " 1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those perfom directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.' (Date) Form MR-03 Page 2 of 2 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this jarrn, please visit hnp://Dorlal-ncdenr.or-'web,'%vq/ws/su/nr)dessw*tab-4 Permit No.: N/C Facility Name: County: Inspector: Date or Inspection: Time of Inspection: Total Event Precipitation (inches): or Certificate of Covera,N/C/G &2-,�,O Phone No. 00 AGh-'S Was this a "Representative Storm Event" as defined by the permit? (See infor tion below.) es ❑ No Please verb whether Qualitative honitoring must be performed during a "representative storm event or "measureable storm event" (requirements vary, depending on the permit.) Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measurable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measumble storm event must h able to document that a shorter approval from the local DWQ Regional Office. By this swu-tu-ozotos is accurate and complete to the best of my knowledge: I.Outfall Description 170�- Outfall No. eig1 Structure (pipe, ditch, etc.) ' Receiving Stream: t Describe the industrial activities that occur within the outfall drainage area: a v 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Q0 A- _ j AICk-L 3.Odor: Describe any distinct colors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,etc.) A i _. _ n 4: Clarity: Chose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 2 D 4 5 5. Floating Solids: Choose the number which best describes the amount of foating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (,No-' 8. is there an oil sheen in the stormwater discharge? Yes CN9) 9. Is there any evidence of errosion or deposition at the outfall? Yes N 10.Other Obvious indicators ofStormwater Pollution: List and describe: 1\ _0 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or errosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit htmlloortal nedenr ore`viceb'wvq'ws'su'npdessvv-tab 4 Permit No.: N,C or Certificate of Covera,N,'C/G V,>of 9�`) Facility Name: County: ,� k P S Phone No. Inspector. Date of Inspection. _ �/ ,�/ Time of Inspection: /tilt•] Total Event Precipitation (inches): I - 0 v i kic h- S Was this a "Representative Storm Event" as defined by the permit? (See informs ' n below.) es ❑ No Please verb whether Oualitative Slonitoring must be perforated daring a "representative storm evert or "measureable storm event" (requirements vary, depending on the permit.) Qua!i=ive monitoring requirements van'. Most permits require qualitative moni Loring to be perforated during a "representative storm event" or during a "measurable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches or rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A sin_ele storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must h able to document that a shorter approval from the local DWQ Regional Office. this or swu-t+:-0e0705 that this report is accurate and complete to the best or my knowledge: 1. Vuttall Description Outfall No. DQ Structure (pipe, ditch, etc.) Iri Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: � 2. Color: Describe the color of the discharge using basic colors (red, bro r'l- 3. 4: Clarity: Chose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: I 4 5 S. Floating Solids: Choose the number which best describes the amount of foating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: I 4 5 7. Is there anv foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes N 9. is there any evidence of errosion or deposition at the outfall? Yes 'CN 9) 10. Other Obvious Indicators of Stormwater Pollution: List and describe: Note: Low clarity, high solids, and,'or the presence of foam, oil sheen, or errosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. StorniNvater Discharge Outfall (SDO) Qualitative Monitoring Report For gnidanwe ort.filli)W nut this form. please visit h :: ,'portal ncdenr or"'vveb'wn'vvs'su npdessvv-tab 4 Permit No.: N'C or Certificate ofCoveralN.'CiG D-aQla`, Facility Name: County: ��,,;tkV�.. Phone No. Inspector: _ Date of lnspection: Time of Inspection: Total Event Precipitation (inches): I - C) ^ 1 RC h.-,5 Was this a "Representative Storm Event" as defined by the permit? (See information below.) es ❑ No Please ver fi whether Qualitative ,i(oniioritg nurse be perforated dewing a "representative stor•ne event or "measureable storm event" (requirements vmy, depending rat the permit.) 2ua!i;a:ive muni:oring:equiremens van. %lost permits require representative stone event" or durin_ a "measurable storm event. refer to these definitions, if applicable. dilative munitoring to be performed during a However. some permits do not have this requirement. .A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 da}'s) in which no storm event measuring greater than 0.1 inches has occurred A sin_flle storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must h to document that a shorter oval from the local DW'Q Regional Office. By thi igna ce . that this report is accurate and complete to the best of my knowledge; swims au.oimns 1. Vutfall Description Outfall No. OD Structure (pipe, ditch, etc.) ' Receirina Stream: Describe the industrial activities that occur within the outfall drainage area: ?. Color: Describe the color of the discharge using basic colors (red. br ��n, blue, etc.) and tint (light, medium. dark) as descriptors: M.,)k,/ _ I ; � -.L- _ 3. Odor: Describe any distinct colors that the discharge may have (i.e., smells strongl. of oil, weak chlorine odor,etc.) 11— n 4: Clarity: Chose the number which best describes the clarity of the discharge, where I is clear and 5 is ven• cloudy: 3 '/ 3 4 5 l.� 5. Floatina Solids: Choose the number which best describes the amount of foating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 ' 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 2 ; 4 5 7. Is there any foam in the stormwater discharge? yes ONO 8. Is there an oil sheen in the stormwater discharge? yes N 9. Is there any evidence of errosion or deposition at the outfall? Yes /Nn 10. Other Obvious Indicators of Stormwater Pollution: List and describe: Note: Low clarity, high solids, and,or the presence of foam, oil sheen, or errosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Storniwater Discharge Outfall (SDO) Qualitative Monitoring Report For gzihknee on filling out this form, please visit htm: "eortal.nedenr om,v%eb'ua'ws'su'nmdessv0 tab 4 Permit No.: N'C or Certificate orCov'era,N.•C/G olaL, Facility Name: I:j7P('UJn , P,,vA.r�-L. County Inspector: _ Date of Inspection: Time of Inspection: Phone No. Total Event Precipitation (inches): _ C) L7 Was this a "Representative Storm Event" as defined by the permit? (See inI ation below.) 7es ❑ No Please ver fv whether Qualitative •i,lonitoring ours[ be performed during a "representative storm event or "measureable slornt event" (requirements vary. depending on the penuit.) Qualitatve mnci:orine rcqui:emen;s �nr:. %lost permits require qualitative monitoring Lobe performed during a "representative storm event" or during a "measurable storm event." However. some permits do not have this requirement. Please refer to these definitions. if applicable. .A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must h able to document that a shorter approval from the local DW'Q Regional Office. that this report is accurate and complete to the best army knowledge: SWU4424 a7a5 1.Outtall Description Outfall No. coq Structure (pipe, ditch. etc.) Reeeivin_ Stream: Describe the industrial activities that occur within the outfall drainage aria: 2. Color: Describe the color of the discharge using basic colors (red, b o%%n, blue, etc.) and tint (light, medium. dark) as descriptors: /�.; rkd . 1 � 3. Odor: Describe apv distinct colors that the discharge may have (i.e., smells strong=1-, of oil, iA —.� weak chlorine odor,etc.) � 4: Clarity: Chose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: l 4 5 S. Floating Solids: Choose the number which best describes the amount of foating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2 4 5 7. is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes fNq 9. Is there any evidence of errosion or deposition at the outfall? Yes N 10. Other Obvious Indicators of Stormwater Pollution: List and describe: Note: Low clarity, high solids, andf'or the presence of foam, oil sheen, or errosion;deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form. please visit hM2"Portal ncdenr or"'web'wP'tvs'su'nodessw=tab 4 Permit No.: N;C or Certificate of CoverarN.'C!G 301 aq Facilitv name: ),J'Q A C L)3n? % P,,A �. r Countv ,� I 1 Phone No. Inspector: Date of Inspection: _/ t Time of Inspection: Total Event Precipitation (inches): I v o d I VtC+_07 Was this a "Representative Storm Event" as defined by the permit? (See information below.) es ❑ No Please verb, it hether Qualitative .Monitoring must be performed during a "representative storm event or "measureahle storm event" (requirements vary. depending on the permit.) hive monitoring rcquir=cros vac; . %lost permits require qualitative monitoring to be performed during a Tentative storm event" or during a "measurable slomi event." However, some permits do not have this requirement. refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the pennitted site outl'all. The previous measurable storm event must h to document that a shorter aval from the local DWO Regional Office. B^ this sigethat this report is accurate and complete to the best of my knowledge: swuu-2424320705 1. Vutfall Description Outfall No. no5 Structure (pipe, ditch. etc.) Receirine Stream: Describe the industrial activities that occur within the outfall drainage area: ?. Color: Describe the color of the discharge using basic colors (red, bro�%n. blue. etc.) and tint (light, medium. dark) as descriptors: , 3. Odor: Describe any distinct colors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,etc.) ►. 1 e% . _ 4: Clarity: Chose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 2 03 4 5 S. Floatiincy Solids: Choose the number which best describes the amount of foating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 ? 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 ? 0 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes Nd 9. Is there any evidence of errosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe: Note: Low clarity, high solids, and,'or the presence of foam, oil sheen, or errosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. P ceAnalytical www.pacelahsxom February 24, 2021 Tony Sprinkle 3990 US 311 Hwy North Pine Hall. NC 27042 RE: Project: Wieland Copper Pace Project No.: 92521915 Dear Tony Sprinkle: Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 Enclosed are the analytical results for sample(s) received by the laboratory on February 12, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Eden • Pace Analytical Services - Kemersville, NC If you have any questions concerning this report, please feel free to contact me. Stephanie Knott stephanie.knott@pacelabs.com 336-996-2841 Project Manager Enclosures cc: Cliff Cain Accounts Payable, Wieland Copper Products LLC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, I.I.C. Page 1 of 15 (�Ia'ucrlea.Analytical WmPacelabs.cara CERTIFICATIONS Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-998-2841 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersvllle, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Flodda/NELAP Certification #: E87648 South Carolina Certification #: 99030001 North Carolina Drinking Water Certification #: 37712 Vrginia/VELAP Certification #: 460222 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Vlrginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalyical www.pacelabs.com SAMPLE ANALYTE COUNT Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical services, LLC 106 Short St. Kemersviile, NC 27284 336-998-2841 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92521915001 002 SM 2540D-2011 AFJ 1 PASI-E EPA 1664E WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A AF 6 PASI-KR 92521916002 001 SM 2540D-2011 AFJ 1 PASI-E EPA 1664B WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH 1 3 PASI-A AF 6 PASI-KR 92521915003 003 SM 2640D-2011 AFJ 1 PASI-E EPA 1664B WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH 1 3 PASI-A AF 6 PASI-KR 92521915004 004 SM 2540D-2011 AFJ 1 PASI-E EPA 1664B WAM 1 PASI-C EPA 200.7 Rev 4.41994 SH1 3 PASI-A AF 6 PASI-KR 92521915005 005 SM 2540D-2011 AFJ 1 PASI-E EPA1664B WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A AF 6 PASI-KR PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-E = Pace Analytical Services - Eden PASI-KR = Pace Analytical Services - Kemersville, NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 15 aceAnalytical l rrww.pacaiaba.com 1 ANALYTICAL RESULTS Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Sample: 001 Parameters Lab ID: 92521915002 Collected: 02/11/21 14:52 Results Units Report Limit DF Received: 02/12/21 10:30 Matrix: Water Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids 155 mg/L 16.7 1 02/15/21 16:32 1664 SGT HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons 9.1 mg/L 5.0 1 02/22/21 10:37 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 1230 ug/L 5.0 1 02/17/21 01:43 02117/2122:22 7440-50-8 Lead 9.8 ug/L 5.0 1 02/17/21 01:43 02/1712122:22 7439-92-1 Zinc 82.9 ug/L 10.0 1 02/17/21 01:43 02/17/2122:22 7440-66-6 Field Data Kernersville Analytical Method: Pace Analytical Services - Kemersville, NC Performed by Pace 1 02/11/21 14:52 Collected By Cllfford 1 02/11/21 14:52 Cain Collected Date 02/11/2021 1 02/11/21 14:52 Collected Time 1452 1 02/11/21 14:52 pH 6.7 Std. Units 1 02/11/21 14:62 Temperature 8 deg C 1 02/11/21 14:52 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 (�Ia'ucvAnalytical www.pacelabo.com ANALYTICAL RESULTS Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-906-2841 Sample: 002 Lab ID: 92621915001 Collected: 02/11/21 14:44 Received: 02/12/21 10:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 26400 Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 9.0 mg/L 2.8 1 02/15/21 16:31 1664 SGT HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/22/21 10:37 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 176 ug/L 5.0 1 02/17/21 01:43 02/17/21 22:19 7440-50-8 Lead ND ug/L 5.0 1 02/17/21 01:43 02/17/21 22:19 7439-92-1 Zinc 39.4 ug/L 10.0 1 02/17/21 01:43 02/17/21 22:19 7440-66-6 Field Data Kernersville Analytical Method: Pace Analytical Services - Kemersville, NC Performed by Pace 1 02/11/21 14:44 Collected By Clifford 1 02/11/21 14:44 Cain Collected Date 02/11/2021 1 02/11/21 14:44 Collected Time 14" 1 02/11/21 14:44 pH 6.7 Std. Units 1 02/11/21 14:44 Temperature 8 deg C 1 02/11/21 14:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalyfical www.pacatabstall ANALYTICAL RESULTS Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 108 Short St. Kemersville, NC 27284 336-998-2841 Sample: 003 Lab ID: 92521916003 Collected: 02/11/21 15:00 Received: 02/12/21 10:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 47.1 mg/L 5.2 1 02/15/21 16:32 1664 SGT HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/22/21 10:37 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 1640 ug/L 5.0 1 02/19/21 02:30 02/19/21 15:41 7440-50-8 Lead ND ug/L 6.0 1 02/19/2102:30 02/19/2115:41 7439-92-1 Zinc 134 ug/L 10.0 1 02/19/21 02:30 02/19/21 15:41 7440-66-6 Field Data Kernersville Analytical Method: Pace Analytical Services - Kemersville, NC Performed by Pace 1 02/11/21 15:00 Collected By Clifford 1 02/11/21 15:00 Cain Collected Date 02111/2021 1 02/11/21 15:00 Collected Time 1500 1 02/11/21 15:00 pH 6.8 Std. Units 1 02/11/21 15:00 Temperature 9 deg C 1 02/11/21 15:00 REPORT OF LABORATORY ANALYSIS This report shatl not be reproduced, except in fell, Date: 02/24/2021 02:24 PM without the wd ton consent of Pace Analytical Services, LLC. Page 6 of 15 aceAnalytical www.p:cetabs.ccm ANALYTICAL RESULTS Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-998-2841 Sample: 004 Parameters Lab ID: 92521916004 Collected: 02/11/21 15:05 Results Units Report Limit DF Received: 02/12/21 10:30 Matrix: Water Prepared Analyzed CAS No. Qual 25400 Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 20.4 mg/L 3.0 1 02/15/21 16:32 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/22/21 10:37 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper 760 ug/L 5.0 1 02/19/21 02:30 02/19/21 15:44 7440-50-8 Lead ND ug/L 5.0 1 02/19/2102:30 02/19/21 15:44 7439-92-1 Zinc 67.2 ug/L 10.0 1 02/19/21 02:30 02/19/21 15:44 7440-66-6 Field Data Kerneravllle Analytical Method: Pace Analytical Services - Kerersville, NC Performed by Pace 1 02/11/21 15:05 Collected By Clifford 1 02/11/21 15:05 Cain Collected Date 02/1112021 1 02/11/21 16:05 Collected Time 1606 1 02/11/21 15:06 pH 6.8 Std. Units 1 02/11/21 15:06 Temperature 8 deg C 1 02/11/21 15:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 (�Ia'ceAnalytical www.pacelabs.ccrs ANALYTICAL RESULTS Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 Sample: 005 Parameters Lab ID: 92521916006 Collected: 02/11/21 15:11 Results Units Report Limit DF Received: 02/12/21 10:30 Matrix: Water Prepared Analyzed CAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 52.3 mg/L 7.1 1 02/15/21 16:32 1664 SGT HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/22/21 10:37 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper 708 ug/L 5.0 1 02/19/21 02:30 02/19/21 15:48 7440-50-8 Lead ND ug/L 5.0 1 02/19/2102:30 02/19/21 15:48 7439-92-1 Zinc 57.4 ug/L 10.0 1 02/19/21 02:30 02/19/21 16:48 7440-66-6 Field Data Kernersville Analytical Method: Pace Analytical Services - Kemersville, NC Performed by Pace 1 02/11/21 15:11 Collected By Clifford 1 02/11/21 15:11 Cain Collected Date 02/11/2021 1 02/11/21 15:11 Collected Time 1511 1 02/11/21 15:11 pH 6.6 Std. Units 1 02/11/21 15:11 Temperature 8 deg C 1 02/11/21 15:11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 15 aceAnalytical rrwnw.pacalabs.com QUALITY CONTROL DATA Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 QC Batch: 599922 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92521915001, 92521915002, 92521915003, 92521915004, 92521915005 METHOD BLANK: 3162599 Matrix: Water Associated Lab Samples: 92521915001, 92521915002, 92521915003, 92521915004, 92521915005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02/15/21 16:28 LABORATORY CONTROL SAMPLE: 3162600 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 260 104 90-110 SAMPLE DUPLICATE: 3162601 92521783004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 56.0 76.2 31 D6 SAMPLE DUPLICATE: 3162602 92521916005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 52.3 59.1 12 Results presented on this page arc in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 aceArialylcal www pacelabs.eeta 1 QUALITY CONTROL DATA Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 QC Batch: 601591 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92521915001, 92521915002, 92521915003, 92521915004, 92521915005 METHOD BLANK: 3170085 Matrix: Water Associated Lab Samples: 92521915001, 92521915002, 92521915003, 92521915004, 92521915005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 02/22/21 10:37 LABORATORY CONTROL SAMPLE: 3170086 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 16.5 82 64-132 MATRIX SPIKE SAMPLE: 3170087 92522076001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 7.0 14 64-132 M1 Results presented on this page are In the units Indicated by the "Unite" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 a %Mnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 short St. Kernersville, NC 27284 336-996-2841 QC Batch: 600513 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.41994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92521915001, 92521915002 METHOD BLANK: 3165276 Matrix: Water Associated Lab Samples: 92521916001, 92521915002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 02/17/2120:58 Lead ug/L ND 5.0 02/17/2120:58 Zinc ug/L ND 10.0 02/17/2120:58 LABORATORY CONTROL SAMPLE: 3165277 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 530 106 85-115 Lead ug/L 500 495 99 85-115 Zinc ug/L 500 477 95 86-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3165278 3165279 MS MSD 92520977001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 0.036 500 500 564 583 105 109 70-130 3 mg/L Lead ug/L ND 500 500 501 518 100 103 70-130 3 Zinc ug/L 0.22 500 500 703 727 96 101 70-130 3 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3165280 3165281 MS MSD 92521347001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 29.4 500 500 567 672 108 109 70-130 1 Lead ug/L ND 500 500 488 490 98 98 70-130 0 Zinc ug/L 415 500 500 912 924 99 102 70-130 1 Results presented on this page are In the units Indicated by the "UnW column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 la'Cl ive A na ly Aca / www.pacalabs.ccrn QUALITY CONTROL DATA Project: Wieland Copper Pace Project No.: 92521915 Pace Analytical Services, LLC 106 Short St Kennersvilie, NC 27284 336-998-2841 QC Batch: 601143 Analysis Method: EPA 200.7 Rev 4.41994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92521915003, 92521915004, 92521915005 METHOD BLANK: 3166278 Matrix: Water Associated Lab Samples: 92521915003, 92521915004, 92521915005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 02/19/2115:12 Lead ug/L ND 5.0 02119/2115:12 Zinc ug/L ND 10.0 02119/2115:12 LABORATORY CONTROL SAMPLE: 3168279 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 523 105 85-115 Lead ug/L 500 487 97 85-115 Zinc ug/L 500 458 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3168280 3168281 MS MSD 92521339001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 0.087 500 500 645 638 112 110 70-130 1 mg/L Lead ug/L ND 500 500 505 498 100 99 70-130 1 Zinc ug/L 0.11 500 500 581 577 94 93 70-130 1 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3168282 3168283 MS MSD 92522136001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 8.5 500 500 554 530 109 104 70-130 4 Lead ug/L ND 500 600 518 489 104 98 70-130 6 Zinc ug/L 70.2 500 500 570 542 100 94 70-130 5 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15 aceAnalytical www.pacelabs.com QUALIFIERS Project: Wieland Copper Pace Project No.: 92521915 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 338-985-2841 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte In a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chlorcethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2021 02:24 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 16 aceAnalytical www.pacelabs.ccra Project: Wieland Copper Pace Project No.: 92521915 Lab ID 92521915001 92621915002 92521916003 92521915004 92621916005 92521916001 92621916002 92521915003 92521916004 92521915005 92621915001 92521916002 92521915003 92521915004 92621916005 92621915001 92621915002 92521916003 92621915004 92521915005 Pace Ana"cal Services, LLC 106 Short Sc Kemersville, NC 27284 336-998-2841 QUALITY CONTROL DATA CROSS REFERENCE TABLE Sample ID QC Batch Method QC Batch Analytical Method 002 SM 2540D-2011 599922 001 SM 2540D-2011 599922 003 SM 2540D-2011 599922 004 SM 2540D-2011 599922 006 SM 2540D-2011 599922 002 EPA 1664E 601591 001 EPA 1664B 601591 003 EPA 1664B 601691 004 EPA 1664E 601591 005 EPA 1664B 601591 002 001 003 004 006 002 001 003 004 006 Date: 02/24/2021 02:24 PM Analytical Batch EPA 200.7 Rev 4.4 1994 600513 EPA 200.7 Rev 4.41994 600545 EPA 200.7 Rev 4.4 1994 600513 EPA 200.7 Rev 4.4 1994 600545 EPA 200.7 Rev 4.4 1994 601143 EPA 200.7 Rev 4.4 1994 601181 EPA 200.7 Rev 4.4 1994 601143 EPA 200.7 Rev 4.4 1994 601181 EPA 200.7 Rev 4.4 1994 601143 EPA 200.7 Rev 4.4 1994 601181 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 15 CHAIN -OF -CUSTODY Analytical Request Document F ceAnalytical Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevant fields LAB USE ONLY- Affix Workorder/Login Label I Here or List Pace Workorder Number or A-- - • •mHcr Here 6 �0# 92521915 ALL SHADED Container Preserva[ieT d 111111111111111111 I III 92521915 • • Preservative Types: (1) nitric acid, (2) sulfuric.. (6) methanol, (7) sodium bisulfate, Iel sodium thiosulfate, (9) hexane, (A) au.u, 11.1.,..., (C) ammonium hydroxide, IDI 75P, ILI Unpreserved, (0) Other Company: s n L Billing Information: Address: Report To: Email To: Copy To: Site Collection Info/Address: Analyses Lab Proflle/Line: Customer Project Name/Number: Pt Ll� State: County/City: Time Zone Collected: l [ I PT ( ] MT ( I CT I JET J4 g � y G n' ltJ tab sample RecPIPL cheeki,1; Custody Seale Present/Inteet Y N NA Custody Signatures Present Y N NA Collector Signature Present Y N NA Bottles Intact Y N NA Correct Bottles Y N NA Sufficient Volume Y N NA Samples Received on Ice Y N NA VOA - Heedspace Acceptable Y N NA USDA Regulated Soils Y N NA Samples in Holding Time Y N NA Plsstulp chlorine ereaent Y N NA Cl 9t[ipe: Sample pH Acceptable Y N NA a: Strl H P P Sulfide Present V N NA Lead Acetate strips: - LAB Use ONLY: Lob Sample k I Comments; Phone: Email: Site/Facilitf ID k: Compliance Monitoring? es I INo C011g�pted riot)' / Purchase Order p: Quote B: DINPWS ID k: DIN Location Code:ta CO ¢(t B igoatUr )' / ` Qi•- Turnaround Date Required: Imme iat2 ate on [e: e5 ( INo Sample posal: I I Dispose as appropriate I I Return Archlve [ 1 - [ eHoltl: Rush: [ ] Same Day I I Next Day 2 Da ] 3 Da 4 Da 5 Da [ ] Y ] Y I ] Y [ ] Y (Expedite Charges Apply) Field Filtered (if applicable): I ] Yes [ ] No Analysis: 'Matrix Codes (insert in Matrix box below): Drinking Water(DW), Ground Water(GW), Wastewater(WW), Product (P), Soil/Solid (SQ, Oil (OL), Wipe (WP), Air (AR), Tissue ITS), Bioassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix • Comp/ Grab Collected (or Composite Start) Composite End Res O ¢of Clans Date Time Date Time - _ JJYY t 3 TCVl21 !7 W -a. Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: Wet Blue Dry None SHORT HOLDS PRESENT (.72 hours): Y N N/A Lab Sample Temperature Info: Temp Blank Received: Y N NA Therm IDk: Cooler 1 Temp Upon Receipt:la.0 Cooler 1 Therm Corr. Factor: O oC Cooler L Corrected Temp:— T-_oC Comments: Packing Material Used: Lab Tracking N: ^ O O L 4 o O Radchem sampte(s) screened(4500 cpm): Y N NA Samples received via: FEDEA UPS Client Courier Pace Courier Relin hP4 by/Company: (Si gture) �Nti Date�me: LC a'f Y�V lT i�a'f( 1 A Receiv d by/Comps : (Signature) Date/Time: IC.t �1�� MTIL LAB USE ONLY Table tl: Acctnum: Relinquishe /Company: (Signature) DateRm : Received by/Company: (Signature) Datelfime: Template: Prelogm: P Tri Blank Received. Y N NA HCL McOH TSP Other Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM: PB: Non Conformance(s): YES / NO Page: Of: