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Home My WebLink AboutNCG060409_DMR_20210513NC Department of Environmental Quality NCDEQ Division of Energy, Mineral and Land Resources Received Stormwater Discharge Monitoring Report (DMR) Form for NCG060000 MAY 13 2021 Food and Kindred Winston-Salem Chck here f Re io Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG06 0409 Person Collecting Samples: Parker Cliatt Facility Name: Amazon.com Services LLC - GS01 Laboratory Name: Eurofins Test America Facility County: Guilford Laboratory Cert. No.: 269 Discharge during this period: ✓❑ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes Q No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR 0 Yes ❑ No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall001 Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class WS N/A Date Sample Collected MM/DD/YYYY 4/24/2021 46529 24-Hour Rainfall in inches 0.3 C0530 TSS in mg/L (100 or 50") 5.4 00400 1 pH in standard units (6.0-9.0) 7.44 00556 Oil & Grease in mg/L (30) 1.9 31616 Fecal Coliform per 100 ml of N/A freshwater (if required) (1000) 61211 Enterococci per 100 ml of saltwater N/A (if required) (500) Chemical Oxygen Demand in mg/L 00340 (120) 17 Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month I N/A 00552 1 Non -Polar Oil & Grease in mg/L (15) N/A r outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false informajlor i4cluding the possibility of fines and imprisonment for knowing violations." or Delegated Authorized Individual n Date Email Address vvvijayk@amazon.com Phone Number (484) 252-1748 urofins Environment Testing America ANALYTICAL REPORT Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel:(912)354-7858 Laboratory Job ID: 680-198096-1 Client Project/Site: Storm Water - Amazon Warehouses (GS01) For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by: 5/4/2021 8:33:52 AM Lauren Evans, Project Manager 1 (615)301-5034 Lauren.Evans@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters. exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. w Y Definitions/Glossary Client: ERM-West Job ID: 680-198096-1 w Project/Site: Storm Water - Amazon Warehouses (GS01) Qualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. o Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFI- Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) DII Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) I Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MOL Method Quanlitatlon Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 2 of 13 5/4/2021 Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (GSO1) Job ID: 680-198096-1 Lab Sample ID Client Sample ID Matrix Collected Received Asset ID 680-198096-1 GS01_Sample Point 01_20210424 Water 04/24/21 16:42 04/27/21 09:55 Eurofins TestAmerica, Savannah Page 3 of 13 5/4/2021 Case Narrative Client: ERM-West Job ID: 680-198096-1 Project/Site: Storm Water - Amazon Warehouses (GS01) Job ID: 680-198096-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job Narrative 680-198096-1 Comments No additional comments. Receipt The sample was received on 4/27/2021 9:55 AM. Unless otherwise noted below, the sample arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 2.40 C. General Chemistry Methods SM 254OD: The sample duplicate precision for the following sample associated with analytical batch 680-666128 was outside control limits: (680-198102-C-1 DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD) precision met acceptance criteria. Methods 410.4: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 666299 were outside control limits. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits. Methods 1664A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 680-666593. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 13 5/4/2021 Client Sample Results Client: ERM-West Job ID: 680-198096-1 Project/Site: Storm Water - Amazon Warehouses (GS01) Client Sample ID: GS01_Sam ple_Point_01_20210424 Lab Sample ID: 680-198096-1 Date Collected: 04/24121 16:42 Matrix: Water Date Received: 04/27/21 09:55 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac HEM (Oil 8 Grease) 1.9 1 4.8 1.3 mg/L 04/30/21 08:23 04/30/21 10:34 1 Total Suspended Solids 5.4 2.5 2.5 mg/L 04/27/21 14:14 1 Chemical Oxygen Demand 17 10 5.0 mg/L 04/28/21 13:10 1 Eurofins TestAmerica, Savannah Page 5 of 13 5/4/2021 QC Sample Results Client: ERM-West Job ID: 680-198096-1 Project/Site: Storm Water - Amazon Warehouses (GS01) Method: 1664A - HEM and SGT-HEM Lab Sample ID: MB 680-66659311-A Matrix: Water Analysis Batch: 666656 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 666593 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ,- HEM (Oil & Grease) <1.4 5.0 1.4 mg/L 04/30/21 08:23 04/30/21 10:34 1 Lab Sample ID: LCS 680-666593/2-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 666656 Prep Batch: 666593 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits HEM (Oil & Grease) 40.0 34.80 mg/L 87 78-114 Lab Sample ID: LCSD 680-666693/3-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 666656 Prep Batch: 666593 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit HEM (Oil & Grease) 40.0 34.00 mg/L 85 78 -114 2 18 Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-1050C) Lab Sample ID: MB 680-666128/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 666128 Analyte Total Suspended Solids Lab Sample ID: LCS 680-666128/2 Matrix: Water Analysis Batch: 666128 Analyte Total Suspended Solids Lab Sample ID: LCSD 680-666128/3 Matrix: Water Analysis Batch: 666128 MB MB Result Qualifier RL MDL Unit <2.5 2.5 2.5 mg/L Spike LCS LCS Added Result Qualifier 951 906 D Prepared Analyzed Dil Fac 04/27/21 14:14 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec. Unit D %Rec Limits mgll 95 80 -120 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 932 mg/L 98 80- 120 3 25 Method: 410.4-1993 R2.0 - COD Lab Sample ID: MB 680-666299/3 Matrix: Water Analysis Batch: 666299 Client Sample ID: Method Blank Prep Type: Total/NA MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 04/28/21 13:10 1 Eurofins TestAmerica, Savannah Page 6 of 13 5/4/2021 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (GS01) Method: 410.4-1993 R2.0 - COD (Continued) Lab Sample ID: LCS 680-666299/4 Matrix: Water Analysis Batch: 666299 Analyte chemical Oxygen Demand tt1771�A:i:ItSl�i:itkI:t31 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 50.7 mg/L 101 90 -110 Eurofins TestAmerica, Savannah Page 7 of 13 5/4/2021 QC Association Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (GS01) General Chemistry Analysis Batch: 666128 Job ID: 680-198096-1 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-198096-1 GSOt_Sample_Polnt_01_20210424 TotaVNA Water 2540 D-2011 MB 680-666128/1 Method Blank Total/NA Water 2540 D-2011 LCS 680-666128/2 Lab Control Sample TotaUNA Water 2540 D-2011 LCSD 680-66612813 Lab Control Sample Dup Total/NA Water 2540 D-2011 Analysis Batch: 666299 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-198096-1 GS01_Sample_Point_01_2021 G424 Total/NA Water 410.4-1993 R2.0 MB 680-666299/3 Method Blank Total/NA Water 410.4-1993 R2.0 LCS 680-666299/4 Lab Control Sample Total/NA Water 410.4-1993 R2.0 Prep Batch: 666593 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-198096-1 GS01_Sample_Point _01_20210424 TbtaVNA Watar 1664A MB 680-666593/1-A Method Blank TotaUNA Water 1664A LCS 680-666593/2-A Lab Control Sample TotaUNA Water 1664A LCSD 680-66659313-A Lab Control Sample Dup Total/NA Water 1664A Analysis Batch: 666656 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-198096-1 GSOt_Sample_Point_01 _20210424 Total/NA Water 1664A 666593 MB 680-666593/1-A Method Blank Total/NA Water 1664A 666593 LCS 680-666593/2-A Lab Control Sample Total/NA Water 1664A 666593 LCSD 680-66659313-A Lab Control Sample Dup Total/NA Water 1664A 666593 Eurofins TestAmerica, Savannah Page 8 of 13 5/4/2021 Lab Chronicle Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (GS01) Job ID:680-198096-1 Client Sample ID: GS01_Sample_Point_01_20210424 Lab Sample ID: 680-198096-1 Date Collected: 04124/21 16:42 Matrix: Water Date Received: 04/27/21 09:55 Batch Batch oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664A 525 mL 500 mL 666593 04/30/21 08:23 JAS TAL SAV Total/NA Analysis 1664A 1 666656 0413012110:34 JAS TAL SAV Instrument ID: NoEquip TotaVNA Analysis 2540 D-2011 1 1000 mL 1000 mL 666128 04/27/21 14:14 PG TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 410.4-1993 R2.0 1 2 mL 2 mL 666299 04/28/21 13:10 MCL TAL SAV Instrument ID: SPC7 Laboratory References: TAL SAV = Eurofins TestAmenca, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah a Page 9 of 13 5/4/2021 Accreditation/Certification Summary Client: ERM-West Job ID: 680-198096-1 Project/Site: Storm Water - Amazon Warehouses (GSO1) Laboratory: Eurofins TestAmerica, Savannah The accredllations/certiflcations listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina(WW/SW) State 269 12-31-21 0 Eurofins TestAmerica, Savannah Page 10 of 13 5/412021 Method Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses (GS01) Job ID: 680-198096-1 Method Method Description Protocol Laboratory 1664A HEM and SGT-HEM 2540 D-2011 Total Suspended Solids (Dried at 103-105°C) 410.4-1993 R2.0 COD 1664A HEM and SGT-HEM (Aqueous) 1664A TAL SAV SM TAL SAV MCAWW TAL SAV 1664A TAL SAV Protocol References: 1664A = EPA-821-98-002 MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 In Eurofins TestAmerica, Savannah Page 11 of 13 5/4/2021 A N 0 N J Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah. GA 31404 Phone (9121 354-7858 Fax (912) 352.0165 Chain of Custody Record -, �,.`�r."" v�eurofins Env,ron—tnl *�.. anwn<a Client lnfomlation samo yil (_-�. .� PMne 3i`7 Lae PM Evans LaurenR _ E-Mao lauren.Evans@Eurohnset com Cane, p.c.'N rvdsl Sblt al O"g COCw 240-78217.31058 Pp Page of _ _ clt'CCMaeI Doug Wade cmm�anr ERM-West ew,m Analysis Requested Ammse 1920 Man Street Sure 300 out DAI. lt,..tta _ Z 8 u ro v 1Z 2 u L m € o ~ fr s g u d e Praaervailon Codes: Ha.ne A.NCL V-9 NaOr� Nuone C ZnA 1.1e O ASW02 D NT: AM P NaiOeS E 101rIS04 0, Na2503 r-IAtoH R. Na2s'ro3 d An,cnm• 5. H2s0e H-AT,. PM ` TSPn Irryp . to U PcelOnt J dWater V MCAA K EOTA W a01 t S L EDA Z 0.1 ienenp, Olnar, Gry IMIIe TAT Ae4oeatM l4aya): $tape. ZV CA. 92614 Complunat Projlct 4 Yn 4 No Pnorc 443-812-M14-60'ei) Po. Purchase Order Requested EmYi doug wade@eTm.corn WO• Pmleat Name Storm Water - Amazon Warehouses ( ) N'w t 24024260 S.le rD 1 SSOWa Sample Identification Sample Date Sample Time Sample Type (C=c P. G= rab) Matnxe (o� .. n.1'.,A— Spacial Instructions/Note: Preservation Code: >QN S S 1 7- I y I I IIIIIIIIIIIIIIIII �,9e�n lllllllllllllllllllllllll A Chain of Custotl IIIIIIIIIII�IIIII Y -- -- -- Possible Hazard Identification C71 Nor.Hazard =Flammahte (-�Skrn Irnlant U Poason B Unknown n Radiol ,cal Sample Disposal ( A fee may be assessed it samples are retained longer than 1 month) U Helum ro Chant n Dt5905o/ By Lao E7 Archrve For Months Delh rrable Requested I. h. III IV. Other (specdy) Special Instruct onsfOC Requirements Empty Kd Relinquished by Ddle Time k4troa t! sno� •_� Nehmusnen er mmmme Comoanr Recmvee Dalen, a Li en,npnY Rl�mm:nn4 Oy / DdldTt a 11 ri 5z eomwny Reuivea eY _ Datert� Y' 1 I y i7 Dam Y Rei•rqunMa Ur Dateni eomwnY Rtct�re4 ey Daferttmt eemoanv Custody Seals Intact b Yes .1 No Custody Seal No Coder iemperalurenl' ene Oeier Banes ,� 3 ./. LJ V er n l 11'IT Login Sample Receipt Checklist Client: ERM-West Job Number: 680-198096-1 Login Number: 198096 List Number:1 Creator: Sims, Robert D Question List Source: Eurofins TestAmerica, Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a surrey NIA meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. NIA There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins TestAmerica, Savannah Page 13 of 13 5/4/2021