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Home My WebLink AboutNCS000107_Discharge Monitoring Data for March 2021_20210826leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 05, 2021 Labarron McMillian LANXESS Corporation 520 Broome Rd Greensboro, NC 27406 RE: Project: Storm water Pace Project No.: 92528938 Dear Labarron McMillian: Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Franchellie Brewer, LANXESS Corporation REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Storm water Pace Project No.: 92528938 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Storm water Pace Project No.: 92528938 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92528938001 Outflow 1 SM 6200B SAS 4 PASI-C EPA 9040C SMK 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92528938002 Outflow 2 SM 6200B SAS 4 PASI-C EPA 9040C SMK 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92528938003 Travel Blank SM 6200B SAS 4 PASI-C PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Storm water Pace Project No.: 92528938 Sample: Outflow 1 Lab ID: 92528938001 Collected: 03/22/21 07:00 Received: 03/22/21 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte o-Xylene 6.2 ug/L 0.50 1 03/27/21 01:08 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 03/27/21 01:08 17060-07-0 4-Bromofluorobenzene (S) 91 % 70-130 1 03/27/21 01:08 460-00-4 Toluene-d8 (S) 99 % 70-130 1 03/27/21 01:08 2037-26-5 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.4 Std. Units 0.10 1 04/04/21 17:04 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 58.6 mg/L 25.0 1 04/03/21 02:53 04/03/21 07:33 Sample: Outflow 2 Lab ID: 92528938002 Collected: 03/22/21 07:00 Received: 03/22/21 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte o-Xylene 1.9 ug/L 0.50 1 03/27/21 01:26 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 03/27/21 01:26 17060-07-0 4-Bromofluorobenzene (S) 91 % 70-130 1 03/27/21 01:26 460-00-4 Toluene-d8 (S) 99 % 70-130 1 03/27/21 01:26 2037-26-5 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.8 Std. Units 0.10 1 04/04/21 17:10 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 30.6 mg/L 25.0 1 04/03/21 02:53 04/03/21 07:33 Sample: Travel Blank Lab ID: 92528938003 Collected: 03/22/21 00:00 Received: 03/22/21 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte o-Xylene 1.1 ug/L 0.50 1 03/27/2100:13 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 03/27/21 00:13 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Storm water Pace Project No.: 92528938 Sample: Travel Blank Lab ID: 92528938003 Collected: 03/22/21 00:00 Received: 03/22/21 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Surrogates 4-Bromofluorobenzene (S) 90 % 70-130 1 03/27/21 00:13 460-00-4 Toluene-d8 (S) 98 % 70-130 1 03/27/21 00:13 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Storm water Pace Project No.: 92528938 QC Batch: 609639 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200E MSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92528938001, 92528938002, 92528938003 METHOD BLANK: 3211059 Matrix: Water Associated Lab Samples: 92528938001, 92528938002, 92528938003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers o-Xylene ug/L ND 0.50 03/26/21 23:01 1,2-Dichloroethane-d4 (S) % 91 70-130 03/26/21 23:01 4-Bromofluorobenzene (S) % 93 70-130 03/26/21 23:01 Toluene-d8 (S) % 98 70-130 03/26/21 23:01 LABORATORY CONTROL SAMPLE: 3211060 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers o-Xylene ug/L 50 45.4 91 60-140 1,2-Dichloroethane-d4 (S) % 87 70-130 4-Bromofluorobenzene (S) % 96 70-130 Toluene-d8 (S) % 95 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211061 3211062 MS MSD 92528789006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual o-Xylene ug/L 1120 250 250 1400 1420 109 117 60-140 2 1,2-Dichloroethane-d4 (S) % 95 93 70-130 4-Bromofluorobenzene (S) % 97 97 70-130 Toluene-d8(S) % 96 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Storm water Pace Project No.: 92528938 QC Batch: 611320 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528938001, 92528938002 SAMPLE DUPLICATE: 3218500 92529967001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.8 7.6 2 D6,H3 SAMPLE DUPLICATE: 3218501 92530373002 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 12.0 12.0 0 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Storm water Pace Project No.: 92528938 QC Batch: 611269 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92528938001, 92528938002 METHOD BLANK: 3218410 Matrix: Water Associated Lab Samples: 92528938001, 92528938002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 04/03/21 07:32 LABORATORY CONTROL SAMPLE: 3218411 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 770 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3218412 3218413 MS MSD 92528935003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 37.6 100 100 140 140 103 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3218414 3218415 MS MSD 92529814001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 35.3 100 100 138 140 103 105 90-110 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Storm water Pace Project No.: 92528938 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/05/2021 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Storm water 92528938 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92528938001 Outflow 1 SM 6200E 609639 92528938002 Outflow 2 SM 6200E 609639 92528938003 Travel Blank SM 6200B 609639 92528938001 Outflow 1 EPA 9040C 611320 92528938002 Outflow 2 EPA 9040C 611320 92528938001 Outflow 1 SM 5220D-2011 611269 SM 5220D-2011 611294 92528938002 Outflow 2 SM 5220D-2011 611269 SM 5220D-2011 611294 Date: 04/05/2021 03:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 r3CBaf7ajytlCc�� Document No.'. Issuing Authority: P•CAR-CS-033-Rev.07 Pace Carolinas quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville f] Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑ Client Name: Courier: ❑Fed Ex ❑UPS ❑USPS ❑ Commercial [Pace ❑Other. Custody Seal Present? []Yes [2fNo Seals Intact? ❑Yes -Project# W4# : 92528938 []Client III 1111111111111111111 92528936 []No pate/tnitlals Person Examining Contents:�� Packing Material: ❑Bubble Wrap []Bubble Bags [None ❑ Other Biological Tissue Frozen? Thermometer, ZfNe[ ❑Niue ❑None []Yes ❑No ON/A ® iR Gun ID: �, Ui r I_� Type of Ice: Correction Factor: Cooler Temp: 1.7 Add/Subtract (°C) 0,0°C Temp should be above freezing to VC ❑Samples out of temp Criteria. Samples on ice, cooling process Cooler Temp Corrected (rC): I 7 has begun USDA Regulated Soil ([ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally, I —Iv— Mm including Flav%aii and Puerto Rico)? ❑Yes []NO C Comments/Dlscrepancy, Chain of Custody Present? MYes ❑No ❑tv/A 1. Samples Arrived within Hold Time? Mes ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes ®No ❑N/A 1 3. Rush Turn Around Time Requested? ❑Yea YNo ❑N/A 4. Sufficient volume? i$Yes []No ❑N/A S. Correct Containers Used? -Pace Containers Used? ®Yes (Yes ❑No []No []N/A ❑N/A 6. Containers Intact? Dissolved analysis Samples Field Filtered? Sample Labels Match COC? -Includes DateMme/ID/Analysis Matrix: ffYes ❑Yes MYes ❑No ❑No [—]No ❑N/A ®N/A []N/A 7. S. 9. Headspace in VOA Vials (>5.6mm)? ayes ❑No ❑N/A Trip Blank Present? Trip Blank Custody Seals Present? fffYes (Yes ❑No []No ❑N/A ❑N/A 11. COMMENTS/SAMPLE DISCREPANCY Fieid Data Required? ❑Yes ❑No !�0 a(�� P S k e) I r'r� n CC(:— - Project Manager SCURF Review; i]ate: Project Manager SRF Review: Date: Page 11 of 13 , ,.-PaceAnalyucai Document No.: F-CAR-CS-033-Rev.07 Issuing Authority: Pace Carolinas Quality Office `Check mark top half of box if pH and/or dechlorination is Project verified and within the acceptance range for preservation WOA : 92528938 samples. PM: MWB Due Date: 04/05/21 Exceptions: VOA, Cofiform, TOC, Oil and Grease, 0110/8015 (water) DOC, LLHg - CLIENT: 82—Lanxess "Bottom -half of-bo-rHs-te-list-number-o#-bottles --- --- - — -- u a, Z u z a E y Z 6, a 7aCVro 1 E , a d m a a z 2 Gl Ol a a mC 7vNC U a S E E o g > m N a d m m d NL7. y > r4 a m v V 2 0. G m O Z N„,• Z a E E u, o N Ln rV J, z e M a a m m a v 2 r: x IU 1 M Zy N m 1 E E ,n In N rN-1 N V a v a a m m u n Z 0 a mm n m = r-I w N L7 3 ¢ N v a 1. E u r•r i r+ L7 ¢ S m N n E A N m l7 ¢ N V 4 O V N E = rl ds a i7 a N v 2- V Q E a N yr rn [7 a ? FJ S z a C N 4 O a m L7 ¢ 4 \ Z O N MV Z p > > J `' a £ a c q 'T x I- a, m s Lo 0 C7 o > a Q \ ? O > s T L T s>> 4 Z Y mio V x d a Z ,� Y a m y - 0 I ¢ \ it ;e E ^ H != >n q Z ua @ E a N N m y Q rvZaV E ¢ M a, Z aaa Qm a > G L7 6 Z N rn �J E o la u, z 5 -0 N d ECEi Q J E a C, 0 J 2 I\N\J NN\3 4 N\ N\ ("\N\ A 6 7 8 li I 9 NN I I I h X 11 1 11 11 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preserrat'son adjustri Amount of Preservative added Lot 4 r' c r,, rsr� n nnanra sarnnlac a mov of thi< fnrrn wilt hygnttn the Nnrth rarnlinn QS UUF CPrt0Rcatlnn Office fi.e,__rr_ ni t ,err 9 ^ out of hold, incorrect preservative, out of temp, incorrect containers. Page 12 of 13 71 Tamp m c D GReceived a4 ica {Y Ni 0 m Custody m Saalatf Chula, O �1 $amplag Inlacl (YIN) ru o m ae v oI rn ♦ u a a ITEM N .v m n b to � 3 � nm 11 r �N g 5 b o $ GGG1ff �" t1 m_ m KQE S - a � k n m aln n 2 z o 7 4 MATRIX CODE {gee WGmogg m bnl $ SAMPLE TYPE (G.GRA6 C•COAIP) z i i1 s m 0 m r r m m' n '0 -n r� SAMPLE TEMP ATC7LLECTV4 3 y n m 93 tl OF CONTAINERS L� Unpreserved gg S g " �_ a H,50, = HNo, m 3 0 _ HCt ! m z �7 NaOH d A Na2S20, H o m Methanol ? 01her (J d K JAnalysls Test j YIN j 0 C z (n� m 1 J% m m 7 n x m n o 8 O V q Residual Chlorine [Y;N] N a v �i m --- � N a _ • 2-1r O o a o Page 13 of 13