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HomeMy WebLinkAboutNC0085359_Results from Second Lab_20210722Action History (UTC-05:00) Eastern Time (US & Canada) Submit by Anonymous User 7/22/2021 2:43:38 PM (Supplemental Submittal) Submit by Bennett, Tilman B 11/24/2021 10:01:08 AM (Supplemental Info Submittal) * Second Lab Results Bennett, Tilman B assigned the task to Bennett, Tilman B 11/24/2021 10:00 AM • The task was assigned to Thedford, Wren, Bennett, Tilman B 7/22/2021 2:44 PM Initial Review Information Updated ID#: * IMPORTANT: REVIEWER SHOULD VERIFY and revise here if necessary. NCO085359 How should this project be handled?* File Discard Information Submitted on 7/22/2021 Submitter Information Name: Jonathan Jordan Who is submitting the information? Email Address:* jonathan.jordan@unioncountync.gov Submittal Information The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through the eDMR system and should not be submitted here. Division staff will review all uploaded documents and will only maintain required information. Documents such as laboratory reports are not required to be submitted and will not be maintained in the system. Project Information: Please supply the permit number for this project. ...................................................................................................................................................................................................................................................................................................................................................................................................... Existing ID#* Permit Number NCO085359 Examples: NCxxxxxxx or NCGxxxxxx Facility Name: * Twelve Mile Water Reclamation Facility County: Union Please upload all files that need to be submited. * Click the upload button or drag and drop files here to attach document 210601-37.pdf 1.99MB 210602-20.pdf 1.75MB 210603-13.pdf 1.84MB 210604-12.pdf 1.85MB 210607-14.pdf 1.86MB 210608-23.pdf 1.84MB 210609-16.pdf 1.96MB 210610-15.pdf 1.95MB 210614-27.pdf 1.72MB 210615-28.pdf 1.83MB 210616-29.pdf 1.94MB 210617-14.pdf 1.74MB 210618-07. pdf 1.67M B 210621-05 (1).pdf 1.95MB 210622-16.pdf 1.95MB 210623-14.pdf 1.73MB 210624-09. pdf 1.65M B 210625-01. pdf 1.96M B 210628-02. pdf 1.68M B 210629-14.pdf 1.95MB 210630-16.pdf 1.97MB Only pdf files are accepted. Comments about the attachments: Laboratory results from Statesville Analytical * By checking the box and signing box below, I certify that: o I have given true, accurate, and complete information on this form; o I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act') • I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act'); • I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written signature; AND o I intend to electronically sign and submit the Supplemental Information form." Full Name: Jonathan Jordan Signature: Date Submitted: 07/22/2021 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/01/2021 Reported:06/21/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210601-37-01 Ammonia UC12-Eff 0.34 mg/L SM4500NH3E-2011 06/01/2021 CE 210601-37-01 BOD UC12-Eff 4.79 mg/L SM5210B-2011 06/02/2021 CE 210601-37-01 Carbonaceous BOD UC12-Eff 2.47 mg/L SM5210B-2011 06/02/2021 CJE 210601-37-01 TSS UC12-Eff 2.935 mg/L SM2540D-2011 06/04/2021 CE 210601-37-02 Ammonia UC12-Inf 35.39 mg/L SM4500NH3E-2011 06/01/2021 CE 210601-37-02 BOD UC12-Inf 139 mg/L SM5210B-2011 06/02/2021 CE 210601-37-02 Carbonaceous BOD UC12-Inf 219 mg/L SM5210B-2011 06/02/2021 CJE 210601-37-02 T. Phosphorous UC12-Inf 2.1 mg/L SM4500PE-2011 06/03/2021 MD 210601-37-02 TSS UC12-Inf 228.3 mg/L SM2540D-2011 06/04/2021 CE 210601-37-03 TSS UC12-MLSS 3570 mg/L SM2540D-2011 06/04/2021 CE 210601-37-04 Total Solids UC12-BFP1- CAKE 176914 mg/L SM2540B-1997 06/02/2021 MD 210601-37-05 Total Solids UC12#3 DIG 23408 mg/L SM2540B-1997 06/02/2021 MD 210601-37-05 Total Volatile Solids UC12#3 DIG 14960 mg/L SM2540G-2011 06/02/2021 MD 210601-37-06 Fecal Coliforms UC12-Eff (LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/01/2021 WC 210601-37-07 Hardness UC12CB (LAB)96.2 mg/L CaCO3 Calculation 06/16/2021 MD 210601-37-07 Nitrate/Nitrite UC12CB (LAB)5.6 mg/L SM4500F-2011 06/10/2021 CL 210601-37-07 T. Phosphorous UC12CB (LAB)1.2 mg/L SM4500PE-2011 06/03/2021 MD 210601-37-07 TKN UC12CB (LAB)7.62 mg/L SM4500NorgB-2011 06/10/2021 CL 210601-37-08 Hardness UC12CB2(LAB)89.8 mg/L CaCO3 Calculation 06/16/2021 MD 210601-37-08 Nitrate/Nitrite UC12CB2(LAB)6.5 mg/L SM4500F-2011 06/10/2021 CL 210601-37-08 T. Phosphorous UC12CB2(LAB)0.3 mg/L SM4500PE-2011 06/03/2021 MD 210601-37-08 TKN UC12CB2(LAB)2.24 mg/L SM4500NorgB-2011 06/10/2021 CL Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 8 Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210601-37-04 Total Volatile Solids UC12-BFP1- CAKE 144416 mg/L SM2540G-2011 06/02/2021 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 8 Condition of Receipt Sample Number 210601-37-01 Temp on Arrival:3.3 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210601-37-02 Temp on Arrival:3.3 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210601-37-03 Temp on Arrival:3.3 Parameter Schedule: TSS Received on Ice Sample Number 210601-37-04 Temp on Arrival:3.3 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 8 Parameter Schedule: Total Solids Received on Ice Sample Number 210601-37-05 Temp on Arrival:3.3 Parameter Schedule: Total Solids Received on Ice Sample Number 210601-37-06 Temp on Arrival:3.3 Parameter Schedule: Sodium Thiosulfate Received on Ice Sample Number 210601-37-07 Temp on Arrival:3.3 pH on Arrival: <2 Parameter Schedule: Hardness Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210601-37-08 Temp on Arrival:3.3 pH on Arrival: <2 Parameter Schedule: Hardness Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 8 pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 8 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 8 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 7 of 8 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 8 of 8 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/02/2021 Reported:06/21/2021 For:12 Mile WWTP Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210602-20-01 Ammonia UC12-Eff <0.1 mg/L SM4500NH3E-2011 06/08/2021 CE 210602-20-01 BOD UC12-Eff 3.97 mg/L SM5210B-2011 06/03/2021 CE 210602-20-01 Carbonaceous BOD UC12-Eff 3.64 mg/L SM5210B-2011 06/03/2021 CE 210602-20-01 TSS UC12-Eff 2.762 mg/L SM2540D-2011 06/04/2021 CE 210602-20-02 Ammonia UC12-Inf 39.76 mg/L SM4500NH3E-2011 06/08/2021 CE 210602-20-02 BOD UC12-Inf 334 mg/L SM5210B-2011 06/03/2021 CE 210602-20-02 Carbonaceous BOD UC12-Inf 347 mg/L SM5210B-2011 06/03/2021 CE 210602-20-02 T. Phosphorous UC12-Inf 2.2 mg/L SM4500PE-2011 06/03/2021 MD 210602-20-02 TSS UC12-Inf 228.3 mg/L SM2540D-2011 06/04/2021 CE 210602-20-03 TSS UC12-MLSS 3600 mg/L SM2540D-2011 06/04/2021 CE 210602-20-04 Total Solids UC12- BFP1CAKE 170265 mg/L SM2540B-1997 06/02/2021 MD 210602-20-04 Total Volatile Solids UC12- BFP1CAKE 140261 mg/L SM2540G-2011 06/02/2021 MD 210602-20-05 Total Solids UC12-#3DIG 22456 mg/L SM2540B-1997 06/02/2021 MD 210602-20-05 Total Volatile Solids UC12-#3DIG 14284 mg/L SM2540G-2011 06/02/2021 MD 210602-20-06 Hardness UC12-CA 57.3 mg/L CaCO3 Calculation 06/16/2021 MD 210602-20-06 Nitrate/Nitrite UC12-CA 0.2 mg/L SM4500F-2011 06/10/2021 CL 210602-20-06 T. Phosphorous UC12-CA 0.2 mg/L SM4500PE-2011 06/03/2021 MD 210602-20-06 TKN UC12-CA 1.46 mg/L SM4500NorgB-2011 06/10/2021 CL 210602-20-07 Fecal Coliforms UC12-Eff (Lab)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/02/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210602-20-01 Temp on Arrival:2.7 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210602-20-02 Temp on Arrival:2.7 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210602-20-03 Temp on Arrival:2.7 Parameter Schedule: TSS Received on Ice Sample Number 210602-20-04 Temp on Arrival:2.7 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210602-20-05 Temp on Arrival:2.7 Parameter Schedule: Total Solids Received on Ice Sample Number 210602-20-06 Temp on Arrival:2.7 pH on Arrival: <2 Parameter Schedule: Hardness Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210602-20-07 Temp on Arrival:2.7 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/03/2021 Reported:06/21/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210603-13-01 Ammonia UC12-Eff 0.22 mg/L SM4500NH3E-2011 06/08/2021 CE 210603-13-01 BOD UC12-Eff 3.41 mg/L SM5210B-2011 06/04/2021 CE 210603-13-01 Carbonaceous BOD UC12-Eff 4.07 mg/L SM5210B-2011 06/03/2021 CE 210603-13-01 Nitrate/Nitrite UC12-Eff 9.3 mg/L SM4500F-2011 06/10/2021 CL 210603-13-01 T. Phosphorous UC12-Eff 0.2 mg/L SM4500PE-2011 06/11/2021 CL 210603-13-01 TKN UC12-Eff 2.35 mg/L SM4500NorgB-2011 06/10/2021 CL 210603-13-01 TSS UC12-Eff 14.11 mg/L SM2540D-2011 06/04/2021 CE 210603-13-02 Ammonia UC12-Inf 34.94 mg/L SM4500NH3E-2011 06/08/2021 CE 210603-13-02 BOD UC12-Inf 268 mg/L SM5210B-2011 06/04/2021 CE 210603-13-02 Carbonaceous BOD UC12-Inf 361 mg/L SM5210B-2011 06/03/2021 CE 210603-13-02 T. Phosphorous UC12-Inf 7.2 mg/L SM4500PE-2011 06/11/2021 CL 210603-13-02 TSS UC12-Inf 250.8 mg/L SM2540D-2011 06/04/2021 CE 210603-13-03 TSS UC12-MLSS 3640 mg/L SM2540D-2011 06/04/2021 CE 210603-13-04 Fecal Coliforms UC12-Eff (LAB)4.1 MPN/100 ml IDEXX Colilert 18 MPN 06/03/2021 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210603-13-01 Temp on Arrival:1.3 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210603-13-02 Temp on Arrival:1.3 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210603-13-03 Temp on Arrival:1.3 Parameter Schedule: TSS Received on Ice Sample Number 210603-13-04 Temp on Arrival:1.3 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/04/2021 Reported:06/21/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210604-12-01 Ammonia UC12-Eff 0.22 mg/L SM4500NH3E-2011 06/08/2021 CE 210604-12-01 BOD UC12-Eff 3.46 mg/L SM5210B-2011 06/04/2021 CE 210604-12-01 Carbonaceous BOD UC12-Eff 2.62 mg/L SM5210B-2011 06/04/2021 CE 210604-12-01 TSS UC12-Eff 5.217 mg/L SM2540D-2011 06/04/2021 CE 210604-12-02 Ammonia UC12-Inf 36.18 mg/L SM4500NH3E-2011 06/08/2021 CE 210604-12-02 BOD UC12-Inf 275 mg/L SM5210B-2011 06/04/2021 CE 210604-12-02 Carbonaceous BOD UC12-Inf 202 mg/L SM5210B-2011 06/04/2021 CE 210604-12-02 T. Phosphorous UC12-Inf 6 mg/L SM4500PE-2011 06/11/2021 CL 210604-12-02 TSS UC12-Inf 175 mg/L SM2540D-2011 06/04/2021 CE 210604-12-03 TSS UC12-MLSS 4110 mg/L SM2540D-2011 06/04/2021 CE 210604-12-04 Total Solids UC12-BFP1- CAKE 156684 mg/L SM2540B-1997 06/04/2021 MD 210604-12-04 Total Volatile Solids UC12-BFP1- CAKE 128921 mg/L SM2540G-2011 06/04/2021 MD 210604-12-05 Total Solids UC12-#3DIG 20704 mg/L SM2540B-1997 06/04/2021 MD 210604-12-05 Total Volatile Solids UC12-#3DIG 12712 mg/L SM2540G-2011 06/04/2021 MD 210604-12-06 Fecal Coliforms UC12-Eff(Lab)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/04/2021 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210604-12-01 Temp on Arrival:4.4 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Received on Ice Sample Number 210604-12-02 Temp on Arrival:4.4 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Received on Ice Sample Number 210604-12-03 Temp on Arrival:4.4 Parameter Schedule: TSS Received on Ice Sample Number 210604-12-04 Temp on Arrival:4.4 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210604-12-05 Temp on Arrival:4.4 Parameter Schedule: Total Solids Received on Ice Sample Number 210604-12-06 Temp on Arrival:4.4 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/07/2021 Reported:06/21/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210607-14-01 Ammonia Nitrogen UC12-Eff 0.42 mg/L SM4500NH3C-2011 06/15/2021 CE 210607-14-01 BOD UC12-Eff 4.34 mg/L SM5210B-2011 06/07/2021 CE 210607-14-01 Carbonaceous BOD UC12-Eff 2.30 mg/L SM5210B-2011 06/07/2021 CE 210607-14-01 TSS UC12-Eff 4.828 mg/L SM2540D-2011 06/11/2021 CE 210607-14-02 Ammonia Nitrogen UC12-Inf 32.62 mg/L SM4500NH3C-2011 06/15/2021 CE 210607-14-02 BOD UC12-Inf 236 mg/L SM5210B-2011 06/07/2021 CE 210607-14-02 Carbonaceous BOD UC12-Inf 145 mg/L SM5210B-2011 06/07/2021 CE 210607-14-02 T. Phosphorous UC12-Inf 5.5 mg/L SM4500PE-2011 06/11/2021 CL 210607-14-02 TSS UC12-Inf 105.3 mg/L SM2540D-2011 06/11/2021 CE 210607-14-03 TSS UC12-MLSS 2230 mg/L SM2540D-2011 06/11/2021 CE 210607-14-04 Total Solids UC12-BFP2 CAKE 150217 mg/L SM2540B-1997 06/07/2021 MD 210607-14-04 Total Volatile Solids UC12-BFP2 CAKE 122539 mg/L SM2540G-2011 06/08/2021 MD 210607-14-05 Total Solids UC12-#3 DIG 20960 mg/L SM2540B-1997 06/07/2021 MD 210607-14-05 Total Volatile Solids UC12-#3 DIG 12700 mg/L SM2540G-2011 06/08/2021 MD 210607-14-06 Total Solids UC12 GBT- TWAS 65669 mg/L SM2540B-1997 06/07/2021 MD 210607-14-06 Total Volatile Solids UC12 GBT- TWAS 53514 mg/L SM2540G-2011 06/08/2021 MD 210607-14-07 Fecal Coliforms UC12-Eff (LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/07/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210607-14-01 Temp on Arrival:6.0 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210607-14-02 Temp on Arrival:6.0 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210607-14-03 Temp on Arrival:6.0 Parameter Schedule: TSS Received on Ice Sample Number 210607-14-04 Temp on Arrival:6.0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Received on Ice Parameter Schedule: Total Solids Received on Ice Sample Number 210607-14-05 Temp on Arrival:6.0 Parameter Schedule: Received on Ice Parameter Schedule: Total Solids Received on Ice Sample Number 210607-14-06 Temp on Arrival:6.0 Parameter Schedule: Received on Ice Parameter Schedule: Total Solids Received on Ice Sample Number 210607-14-07 Temp on Arrival:6.0 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/08/2021 Reported:06/17/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210608-23-01 Ammonia Nitrogen UC12-Eff <0.5 mg/L SM4500NH3C-2011 06/15/2021 CE 210608-23-01 BOD UC12-Eff 3.12 mg/L SM5210B-2011 06/09/2021 CE 210608-23-01 Carbonaceous BOD UC12-Eff <2 mg/L SM5210B-2011 06/09/2021 CE 210608-23-01 TSS UC12-Eff 3.616 mg/L SM2540D-2011 06/11/2021 CE 210608-23-02 Ammonia Nitrogen UC12-INF 31.02 mg/L SM4500NH3C-2011 06/15/2021 CE 210608-23-02 BOD UC12-INF 324 mg/L SM5210B-2011 06/09/2021 CE 210608-23-02 Carbonaceous BOD UC12-INF 144 mg/L SM5210B-2011 06/09/2021 CE 210608-23-02 T. Phosphorous UC12-INF 6.2 mg/L SM4500PE-2011 06/11/2021 CL 210608-23-02 TSS UC12-INF 198.2 mg/L SM2540D-2011 06/11/2021 CE 210608-23-03 TSS UC12-MLSS 3340 mg/L SM2540D-2011 06/11/2021 CE 210608-23-04 Fecal Coliforms UC12-Eff (LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/08/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210608-23-01 Temp on Arrival:2.4 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210608-23-02 Temp on Arrival:2.4 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210608-23-03 Temp on Arrival:2.4 Parameter Schedule: TSS Received on Ice Sample Number 210608-23-04 Temp on Arrival:2.4 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/09/2021 Reported:06/21/2021 For:12 Mile WRF Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210609-16-01 Ammonia UC12-Eff 0.22 mg/L SM4500NH3E-2011 06/15/2021 CE 210609-16-01 BOD UC12-Eff 3.50 mg/L SM5210B-2011 06/10/2021 CE 210609-16-01 Carbonaceous BOD UC12-Eff <2 mg/L SM5210B-2011 06/10/2021 CE 210609-16-01 TSS UC12-Eff 4.581 mg/L SM2540D-2011 06/11/2021 CE 210609-16-02 Ammonia UC12-Inf 28.78 mg/L SM4500NH3E-2011 06/15/2021 CE 210609-16-02 BOD UC12-Inf 273 mg/L SM5210B-2011 06/10/2021 CE 210609-16-02 Carbonaceous BOD UC12-Inf 489 mg/L SM5210B-2011 06/10/2021 CE 210609-16-02 T. Phosphorous UC12-Inf 6.5 mg/L SM4500PE-2011 06/11/2021 CL 210609-16-02 TSS UC12-Inf 173.8 mg/L SM2540D-2011 06/11/2021 CE 210609-16-03 TSS UC12-MLSS 3350 mg/L SM2540D-2011 06/11/2021 CE 210609-16-04 Total Solids UC12-BFP2- Cake 152233 mg/L SM2540B-1997 06/11/2021 WC 210609-16-05 Total Solids UC12-#3DIG 18024 mg/L SM2540B-1997 06/11/2021 WC 210609-16-05 Total Volatile Solids UC12-#3DIG 12632 mg/L SM2540G-2011 06/11/2021 WC 210609-16-06 Fecal Coliforms UC12-Eff (lab)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/09/2021 CL Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210609-16-01 Temp on Arrival:1.0 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210609-16-02 Temp on Arrival:1.0 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210609-16-03 Temp on Arrival:1.0 Parameter Schedule: TSS Received on Ice Sample Number 210609-16-04 Temp on Arrival:1.0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210609-16-05 Temp on Arrival:1.0 Parameter Schedule: Total Solids Received on Ice Sample Number 210609-16-06 Temp on Arrival:1.0 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/10/2021 Reported:06/21/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210610-15-01 Ammonia Nitrogen UC12-Eff <0.5 mg/L SM4500NH3C-2011 06/15/2021 CE 210610-15-01 BOD UC12-Eff 3.35 mg/L SM5210B-2011 06/11/2021 CE 210610-15-01 Carbonaceous BOD UC12-Eff <2 mg/L SM5210B-2011 06/11/2021 CE 210610-15-01 TSS UC12-Eff 4.382 mg/L SM2540D-2011 06/11/2021 CE 210610-15-02 Ammonia Nitrogen UC12-Inf 31.14 mg/L SM4500NH3C-2011 06/15/2021 CE 210610-15-02 BOD UC12-Inf 229 mg/L SM5210B-2011 06/11/2021 CE 210610-15-02 Carbonaceous BOD UC12-Inf 125 mg/L SM5210B-2011 06/11/2021 CE 210610-15-02 T. Phosphorous UC12-Inf 5.8 mg/L SM4500PE-2011 06/11/2021 CL 210610-15-02 TSS UC12-Inf 182.5 mg/L SM2540D-2011 06/11/2021 CE 210610-15-03 TSS UC12-MLSS 3270 mg/L SM2540D-2011 06/11/2021 CE 210610-15-04 Fecal Coliforms UC12-Eff (LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/10/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210610-15-01 Temp on Arrival:3.0 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210610-15-02 Temp on Arrival:3.0 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210610-15-03 Temp on Arrival:3.0 Parameter Schedule: TSS Received on Ice Sample Number 210610-15-04 Temp on Arrival:3.0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/14/2021 Reported:06/30/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210614-27-01 Ammonia UC-12 EFF 0.56 mg/L SM4500NH3E-2011 06/15/2021 CE 210614-27-01 BOD UC-12 EFF 5.77 mg/L SM5210B-2011 06/14/2021 CE 210614-27-01 Carbonaceous BOD UC-12 EFF 5.13 mg/L SM5210B-2011 06/14/2021 CE 210614-27-01 TSS UC-12 EFF <2.778 mg/L SM2540D-2011 06/18/2021 CE 210614-27-02 Ammonia Nitrogen UC-12 INF 33.38 mg/L SM4500NH3C-2011 06/15/2021 CE 210614-27-02 BOD UC-12 INF 261 mg/L SM5210B-2011 06/14/2021 CE 210614-27-02 Carbonaceous BOD UC-12 INF 226 mg/L SM5210B-2011 06/14/2021 CE 210614-27-02 T. Phosphorous UC-12 INF 1.9 mg/L SM4500PE-2011 06/21/2021 MD 210614-27-02 TSS UC-12 INF 82 mg/L SM2540D-2011 06/18/2021 CE 210614-27-03 TSS UC-12 MLSS 2870 mg/L SM2540D-2011 06/18/2021 CE 210614-27-04 Total Solids UC-12 BFP1-CK 165700 mg/L SM2540B-1997 06/16/2021 MD 210614-27-05 Total Solids UC-12 #3 DIG 18970 mg/L SM2540B-1997 06/16/2021 MD 210614-27-05 Total Volatile Solids UC-12 #3 DIG 11680 mg/L SM2540G-2011 06/16/2021 MD 210614-27-06 Fecal Coliforms UC-12 EFF 5.2 MPN/100 ml IDEXX Colilert 18 MPN 06/14/2021 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210614-27-01 Temp on Arrival:3.8 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210614-27-02 Temp on Arrival:3.8 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210614-27-03 Temp on Arrival:3.8 Parameter Schedule: TSS Received on Ice Sample Number 210614-27-04 Temp on Arrival:3.8 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210614-27-05 Temp on Arrival:3.8 Parameter Schedule: Received on Ice Parameter Schedule: Total Solids Received on Ice Sample Number 210614-27-06 Temp on Arrival:3.8 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/15/2021 Reported:06/25/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210615-28-01 Ammonia UC-12-EFF <0.1 mg/L SM4500NH3E-2011 06/22/2021 CE 210615-28-01 BOD UC-12-EFF 3.36 mg/L SM5210B-2011 06/16/2021 CE 210615-28-01 Carbonaceous BOD UC-12-EFF 3.45 mg/L SM5210B-2011 06/16/2021 CE 210615-28-01 Fecal Coliforms UC-12-EFF 1.0 MPN/100 ml IDEXX Colilert 18 MPN 06/15/2021 CE 210615-28-01 TSS UC-12-EFF <2.874 mg/L SM2540D-2011 06/18/2021 CE 210615-28-02 Ammonia UC-12 INF 32.59 mg/L SM4500NH3E-2011 06/22/2021 CE 210615-28-02 BOD UC-12 INF 348 mg/L SM5210B-2011 06/16/2021 CE 210615-28-02 Carbonaceous BOD UC-12 INF 361 mg/L SM5210B-2011 06/16/2021 CE 210615-28-02 T. Phosphorous UC-12 INF 2 mg/L SM4500PE-2011 06/21/2021 MD 210615-28-02 TSS UC-12 INF 168.3 mg/L SM2540D-2011 06/18/2021 CE 210615-28-03 MLSS UC-12 MLSS 3100 mg/L SM2540G 06/18/2021 CE Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210615-28-01 Temp on Arrival:3.9 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210615-28-02 Temp on Arrival:3.9 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210615-28-03 Temp on Arrival:3.9 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: MLSS Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/16/2021 Reported:06/30/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210616-29-01 Ammonia UC-12EFF <0.1 mg/L SM4500NH3E-2011 06/22/2021 CE 210616-29-01 BOD UC-12EFF 3.03 mg/L SM5210B-2011 06/17/2021 CE 210616-29-01 Carbonaceous BOD UC-12EFF <2 mg/L SM5210B-2011 06/17/2021 CE 210616-29-01 Fecal Coliforms UC-12EFF 3 MPN/100 ml IDEXX Colilert 18 MPN 06/16/2021 CE 210616-29-01 TSS UC-12EFF 3.529 mg/L SM2540D-2011 06/18/2021 CE 210616-29-02 Ammonia UC-12-INF 34.38 mg/L SM4500NH3E-2011 06/22/2021 CE 210616-29-02 BOD UC-12-INF 262 mg/L SM5210B-2011 06/17/2021 CE 210616-29-02 Carbonaceous BOD UC-12-INF 252 mg/L SM5210B-2011 06/17/2021 CE 210616-29-02 T. Phosphorous UC-12-INF 2.2 mg/L SM4500PE-2011 06/21/2021 MD 210616-29-02 TSS UC-12-INF 210.9 mg/L SM2540D-2011 06/18/2021 CE 210616-29-03 TSS UC-12-MLSS 2980 mg/L SM2540D-2011 06/18/2021 CE 210616-29-04 Total Solids UC12-BFP1-CK 157443 mg/L SM2540B-1997 06/18/2021 MD 210616-29-05 Total Solids UC12-#3 DIG 18264 mg/L SM2540B-1997 06/18/2021 MD 210616-29-05 Total Volatile Solids UC12-#3 DIG 10700 mg/L SM2540G-2011 06/18/2021 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210616-29-01 Temp on Arrival:3.2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210616-29-02 Temp on Arrival:3.2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210616-29-03 Temp on Arrival:3.2 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: TSS Received on Ice Sample Number 210616-29-04 Temp on Arrival:3.2 Parameter Schedule: Total Solids Received on Ice Sample Number 210616-29-05 Temp on Arrival:3.2 Parameter Schedule: Total Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/17/2021 Reported:06/25/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210617-14-01 Ammonia UC12-EFF <0.1 mg/L SM4500NH3E-2011 06/22/2021 CE 210617-14-01 BOD UC12-EFF 3.78 mg/L SM5210B-2011 06/18/2021 CE 210617-14-01 Carbonaceous BOD UC12-EFF 2.41 mg/L SM5210B-2011 6/18/2116:30 CE 210617-14-01 Fecal Coliforms UC12-EFF 2.0 MPN/100 ml IDEXX Colilert 18 MPN 06/17/2021 CE 210617-14-01 TSS UC12-EFF 3.743 mg/L SM2540D-2011 06/18/2021 CE 210617-14-02 Ammonia UC-12-INF 32.70 mg/L SM4500NH3E-2011 06/22/2021 CE 210617-14-02 BOD UC-12-INF 332 mg/L SM5210B-2011 06/18/2021 CE 210617-14-02 Carbonaceous BOD UC-12-INF 217 mg/L SM5210B-2011 6/18/2116:30 CE 210617-14-02 T. Phosphorous UC-12-INF 2.1 mg/L SM4500PE-2011 06/21/2021 MD 210617-14-02 TSS UC-12-INF 198.6 mg/L SM2540D-2011 06/18/2021 CE 210617-14-03 TSS UC12-MLSS 2627 mg/L SM2540D-2011 06/18/2021 CE Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 Condition of Receipt Sample Number 210617-14-01 Temp on Arrival:3.9 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210617-14-02 Temp on Arrival:3.9 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210617-14-03 Temp on Arrival:3.9 Parameter Schedule: TSS Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 5 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/18/2021 Reported:06/30/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210618-07-01 Ammonia UC-12 EFF 0.11 mg/L SM4500NH3E-2011 06/22/2021 CE 210618-07-01 BOD UC-12 EFF 4.92 mg/L SM5210B-2011 06/18/2021 CE 210618-07-01 Carbonaceous BOD UC-12 EFF 3.89 mg/L SM5210B-2011 6/18/2116:30 CE 210618-07-01 Fecal Coliforms UC-12 EFF 1.0 MPN/100 ml IDEXX Colilert 18 MPN 06/18/2021 MD 210618-07-01 TSS UC-12 EFF 6.353 mg/L SM2540D-2011 06/18/2021 CE 210618-07-02 Ammonia UC-12 INF 35.95 mg/L SM4500NH3E-2011 06/22/2021 CE 210618-07-02 BOD UC-12 INF 285 mg/L SM5210B-2011 06/18/2021 CE 210618-07-02 Carbonaceous BOD UC-12 INF 177 mg/L SM5210B-2011 6/18/2116:30 CE 210618-07-02 T. Phosphorous UC-12 INF 2.5 mg/L SM4500PE-2011 06/21/2021 MD 210618-07-02 TSS UC-12 INF 220 mg/L SM2540D-2011 06/18/2021 CE 210618-07-03 TSS UC12-MLSS 3170 mg/L SM2540D-2011 06/18/2021 CE 210618-07-04 Total Solids UC12-BFP1-CK 161829 mg/L SM2540B-1997 06/18/2021 MD 210618-07-05 Total Solids UC12-#3DIG 17212 mg/L SM2540B-1997 06/18/2021 MD 210618-07-05 Total Volatile Solids UC12-#3DIG 10560 mg/L SM2540G-2011 06/18/2021 MD Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210618-07-01 Temp on Arrival:3.2 Parameter Schedule: Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210618-07-02 Temp on Arrival:3.2 Parameter Schedule: BOD Received on Ice Parameter Schedule: Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210618-07-03 Temp on Arrival:3.2 Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/21/2021 Reported:06/28/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210621-05-01 Ammonia UC-12-EFF 0.22 mg/L SM4500NH3E-2011 06/22/2021 CE 210621-05-01 BOD UC-12-EFF 5.80 mg/L SM5210B-2011 06/21/2021 CE/WC 210621-05-01 Carbonaceous BOD UC-12-EFF 3.48 mg/L SM5210B-2011 06/21/2021 CE 210621-05-01 Fecal Coliforms UC-12-EFF 9 MPN/100 ml IDEXX Colilert 18 MPN 06/21/2021 WC 210621-05-01 TSS UC-12-EFF <2.874 mg/L SM2540D-2011 06/25/2021 CE 210621-05-02 Ammonia UC-12-INF 18.82 mg/L SM4500NH3E-2011 06/22/2021 CE 210621-05-02 BOD UC-12-INF 175 mg/L SM5210B-2011 06/21/2021 CE/WC 210621-05-02 Carbonaceous BOD UC-12-INF 133 mg/L SM5210B-2011 06/21/2021 CE 210621-05-02 T. Phosphorous UC-12-INF 1.4 mg/L SM4500PE-2011 06/25/2021 CL 210621-05-02 TSS UC-12-INF 126.2 mg/L SM2540D-2011 06/25/2021 CE 210621-05-03 TSS UC-12 MLSS 2870 mg/L SM2540D-2011 06/25/2021 CE Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210621-05-01 Temp on Arrival:5.6 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210621-05-02 Temp on Arrival:5.6 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210621-05-03 Temp on Arrival:5.6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: TSS Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/22/2021 Reported:07/02/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210622-16-01 Ammonia UC12-EFF <0.1 mg/L SM4500NH3E-2011 06/29/2021 CE 210622-16-01 BOD UC12-EFF 5.58 mg/L SM5210B-2011 06/23/2021 CE 210622-16-01 Carbonaceous BOD UC12-EFF 2.44 mg/L SM5210B-2011 06/23/2021 CE 210622-16-01 TSS UC12-EFF <2.778 mg/L SM2540D-2011 06/25/2021 CE 210622-16-02 Ammonia UC12-INF 21.28 mg/L SM4500NH3E-2011 06/29/2021 CE 210622-16-02 BOD UC12-INF 331 mg/L SM5210B-2011 06/23/2021 CE 210622-16-02 Carbonaceous BOD UC12-INF 178 mg/L SM5210B-2011 06/23/2021 CE 210622-16-02 T. Phosphorous UC12-INF 1.7 mg/L SM4500PE-2011 06/25/2021 CL 210622-16-02 TSS UC12-INF 52.5 mg/L SM2540D-2011 06/25/2021 CE 210622-16-03 TSS UC12-MLSS 4960 mg/L SM2540D-2011 06/25/2021 CE 210622-16-04 Total Solids UC12-BFP1- CAKE 164939 mg/L SM2540B-1997 06/24/2021 WC 210622-16-05 Total Solids UC12#3 DIG 15108 mg/L SM2540B-1997 06/24/2021 WC 210622-16-05 Total Volatile Solids UC12#3 DIG 8812 mg/L SM2540G-2011 06/24/2021 WC 210622-16-06 Fecal Coliforms UC12 EFF (LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/22/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210622-16-01 Temp on Arrival:3.1 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210622-16-02 Temp on Arrival:3.1 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210622-16-03 Temp on Arrival:3.1 Parameter Schedule: TSS Received on Ice Sample Number 210622-16-04 Temp on Arrival:3.1 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210622-16-05 Temp on Arrival:3.1 Parameter Schedule: Received on Ice Parameter Schedule: Total Solids Received on Ice Sample Number 210622-16-06 Temp on Arrival:3.1 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/23/2021 Reported:07/02/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210623-14-01 Ammonia UC12-Eff <0.1 mg/L SM4500NH3E-2011 06/29/2021 CE 210623-14-01 BOD UC12-Eff 2.90 mg/L SM5210B-2011 06/24/2021 CE 210623-14-01 Carbonaceous BOD UC12-Eff 2.37 mg/L SM5210B-2011 06/24/2021 CE 210623-14-01 TSS UC12-Eff <2.747 mg/L SM2540D-2011 06/25/2021 CE 210623-14-02 Ammonia UC12-Inf 25.31 mg/L SM4500NH3E-2011 06/29/2021 CE 210623-14-02 BOD UC12-Inf 231 mg/L SM5210B-2011 06/24/2021 CE 210623-14-02 Carbonaceous BOD UC12-Inf 185 mg/L SM5210B-2011 06/24/2021 CE 210623-14-02 T. Phosphorous UC12-Inf 1.5 mg/L SM4500PE-2011 06/25/2021 CL 210623-14-02 TSS UC12-Inf 137.3 mg/L SM2540D-2011 06/25/2021 CE 210623-14-03 TSS UC12-MLSS 3390 mg/L SM2540D-2011 06/25/2021 CE 210623-14-04 Total Solids UC12-BFP1- CAKE 30927 mg/L SM2540B-1997 06/24/2021 WC 210623-14-05 Total Solids UC12-#3DIG 14136 mg/L SM2540B-1997 06/24/2021 WC 210623-14-05 Total Volatile Solids UC12-#3DIG 8796 mg/L SM2540G-2011 06/25/2021 WC 210623-14-06 Fecal Coliforms UC12-Eff(lab)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/23/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210623-14-01 Temp on Arrival:2.0 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210623-14-02 Temp on Arrival:2.0 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210623-14-03 Temp on Arrival:2.0 Parameter Schedule: TSS Received on Ice Sample Number 210623-14-04 Temp on Arrival:2.0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210623-14-05 Temp on Arrival:2.0 Parameter Schedule: Total Solids Received on Ice Sample Number 210623-14-06 Temp on Arrival:2.0 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/24/2021 Reported:07/01/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210624-09-01 Ammonia UC12 EFF <0.1 mg/L SM4500NH3E-2011 06/29/2021 CE 210624-09-01 BOD UC12 EFF 2.26 mg/L SM5210B-2011 06/25/2021 CE 210624-09-01 Carbonaceous BOD UC12 EFF <2 mg/L SM5210B-2011 06/25/2021 CE 210624-09-01 T. Phosphorous UC12 EFF 0.16 mg/L SM4500PE-2011 06/25/2021 CL 210624-09-01 TSS UC12 EFF 4.859 mg/L SM2540D-2011 06/25/2021 CE 210624-09-02 Ammonia UC12 INF 26.77 mg/L SM4500NH3E-2011 06/29/2021 CE 210624-09-02 BOD UC12 INF 218 mg/L SM5210B-2011 06/25/2021 CE 210624-09-02 Carbonaceous BOD UC12 INF 179 mg/L SM5210B-2011 06/25/2021 CE 210624-09-02 T. Phosphorous UC12 INF 1.5 mg/L SM4500PE-2011 06/25/2021 CL 210624-09-02 TSS UC12 INF 170.6 mg/L SM2540D-2011 06/25/2021 CE 210624-09-03 TSS UC12MLSS 3310 mg/L SM2540D-2011 06/25/2021 CE 210624-09-04 Fecal Coliforms UC12EFF(LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/24/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210624-09-01 Temp on Arrival:3.2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210624-09-02 Temp on Arrival:3.2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210624-09-03 Temp on Arrival:3.2 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: TSS Received on Ice Sample Number 210624-09-04 Temp on Arrival:3.2 pH on Arrival: <2 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/25/2021 Reported:07/02/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210625-01-01 Ammonia UC12-EFF <0.1 mg/L SM4500NH3E-2011 06/29/2021 CE 210625-01-01 BOD UC12-EFF 2.21 mg/L SM5210B-2011 06/25/2021 CE 210625-01-01 Carbonaceous BOD UC12-EFF <2 mg/L SM5210B-2011 06/25/2021 CE 210625-01-01 TSS UC12-EFF 3 mg/L SM2540D-2011 06/25/2021 CE 210625-01-02 Ammonia UC12-INF 28.9 mg/L SM4500NH3E-2011 06/29/2021 CE 210625-01-02 BOD UC12-INF 221 mg/L SM5210B-2011 06/25/2021 CE 210625-01-02 Carbonaceous BOD UC12-INF 200 mg/L SM5210B-2011 06/25/2021 CE 210625-01-02 T. Phosphorous UC12-INF 1.25 mg/L SM4500PE-2011 06/25/2021 CL 210625-01-02 TSS UC12-INF 195.3 mg/L SM2540D-2011 06/25/2021 CE 210625-01-03 TSS UC12-MLSS 3340 mg/L SM2540D-2011 06/25/2021 CE 210625-01-04 Total Solids UC12-BFP1 CAKE 166318 mg/L SM2540B-1997 06/25/2021 CL 210625-01-05 Total Solids UC12-#3 DIG 14890 mg/L SM2540B-1997 06/25/2021 CL 210625-01-05 Total Volatile Solids UC12-#3 DIG 8843 mg/L SM2540G-2011 06/28/2021 CL 210625-01-06 Fecal Coliforms UC12-EFF(LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/25/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210625-01-01 Temp on Arrival:3.8 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210625-01-02 Temp on Arrival:3.8 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210625-01-03 Temp on Arrival:3.8 Parameter Schedule: TSS Received on Ice Sample Number 210625-01-04 Temp on Arrival:3.8 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Total Solids Received on Ice Sample Number 210625-01-05 Temp on Arrival:3.8 Parameter Schedule: Total Solids Received on Ice Parameter Schedule: Sodium Hydroxide Received on Ice Chemicals in containers, lab Sample Number 210625-01-06 Temp on Arrival:3.8 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/28/2021 Reported:07/07/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210628-02-01 Ammonia UC12-EFF 0.22 mg/L SM4500NH3E-2011 06/29/2021 CE 210628-02-01 BOD UC12-EFF 3.75 mg/L SM5210B-2011 06/28/2021 CE/LE 210628-02-01 Carbonaceous BOD UC12-EFF <2 mg/L SM5210B-2011 06/28/2021 CE/LE 210628-02-01 T. Phosphorous UC12-EFF <0.1 mg/L SM4500PE-2011 07/02/2021 CL 210628-02-01 TSS UC12-EFF <2.778 mg/L SM2540D-2011 07/01/2021 LE/CE 210628-02-02 Ammonia UC12-INF 30.13 mg/L SM4500NH3E-2011 06/29/2021 CE 210628-02-02 BOD UC12-INF 188 mg/L SM5210B-2011 06/28/2021 CE/LE 210628-02-02 Carbonaceous BOD UC12-INF 135 mg/L SM5210B-2011 06/28/2021 CE/LE 210628-02-02 T. Phosphorous UC12-INF 1.5 mg/L SM4500PE-2011 07/02/2021 CL 210628-02-02 TSS UC12-INF 63 mg/L SM2540D-2011 07/01/2021 LE/CE 210628-02-03 TSS UC12-MLSS 2268 mg/L SM2540D-2011 07/01/2021 LE/CE 210628-02-04 Total Solids UC12-GBT1- TWAS 64875 mg/L SM2540B-1997 07/01/2021 MD 210628-02-04 Total Volatile Solids UC12-GBT1- TWAS 23840 mg/L SM2540G-2011 07/01/2021 MD 210628-02-05 Total Solids UC12 #3 DIG 17832 mg/L SM2540B-1997 07/01/2021 MD 210628-02-05 Total Volatile Solids UC12 #3 DIG 11120 mg/L SM2540G-2011 07/01/2021 MD 210628-02-06 Fecal Coliforms UC12-EFF(LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/28/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/29/2021 Reported:07/07/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210629-14-01 Ammonia UC12-EFF 0.11 mg/L SM4500NH3E-2011 07/06/2021 CE/MD 210629-14-01 BOD UC12-EFF 2.34 mg/L SM5210B-2011 06/30/2021 CE 210629-14-01 Carbonaceous BOD UC12-EFF <2 mg/L SM5210B-2011 06/30/2021 CE 210629-14-01 TSS UC12-EFF <2.841 mg/L SM2540D-2011 07/01/2021 LE/CE 210629-14-02 Ammonia UC12-INF 33.6 mg/L SM4500NH3E-2011 07/06/2021 CE/MD 210629-14-02 BOD UC12-INF 331 mg/L SM5210B-2011 06/30/2021 CE 210629-14-02 Carbonaceous BOD UC12-INF 241 mg/L SM5210B-2011 06/30/2021 CE 210629-14-02 T. Phosphorous UC12-INF 1.95 mg/L SM4500PE-2011 07/02/2021 CL 210629-14-02 TSS UC12-INF 140 mg/L SM2540D-2011 07/01/2021 LE/CE 210629-14-03 TSS UC12-MLSS 2420 mg/L SM2540D-2011 07/01/2021 LE/CE 210629-14-04 Fecal Coliforms UC12-EFF(LAB)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/29/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 Condition of Receipt Sample Number 210629-14-01 Temp on Arrival:3.6 Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210629-14-02 Temp on Arrival:3.6 Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210629-14-03 Temp on Arrival:3.6 Parameter Schedule: TSS Received on Ice Sample Number 210629-14-04 Temp on Arrival:3.6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 5 12 Mile WRF-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date:06/30/2021 Reported:07/07/2021 For: Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210630-16-01 Ammonia UC12-Eff <0.1 mg/L SM4500NH3E-2011 07/06/2021 CE/MD 210630-16-01 BOD UC12-Eff 3.27 mg/L SM5210B-2011 07/01/2021 CE 210630-16-01 Carbonaceous BOD UC12-Eff 2.26 mg/L SM5210B-2011 07/01/2021 CE 210630-16-01 TSS UC12-Eff <2.747 mg/L SM2540D-2011 07/01/2021 LE/CE 210630-16-02 Ammonia UC12-Inf 31.7 mg/L SM4500NH3E-2011 07/06/2021 CE/MD 210630-16-02 BOD UC12-Inf 293 mg/L SM5210B-2011 07/01/2021 CE 210630-16-02 Carbonaceous BOD UC12-Inf 266 mg/L SM5210B-2011 07/01/2021 CE 210630-16-02 T. Phosphorous UC12-Inf 2.1 mg/L SM4500PE-2011 07/02/2021 CL 210630-16-02 TSS UC12-Inf 178.3 mg/L SM2540D-2011 07/01/2021 LE/CE 210630-16-03 TSS UC12-MLSS 2187 mg/L SM2540D-2011 07/01/2021 LE/CE 210630-16-04 Fecal Coliforms UC12-Eff(lab)<1 MPN/100 ml IDEXX Colilert 18 MPN 06/30/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210630-16-01 Temp on Arrival:2.4 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210630-16-02 Temp on Arrival:2.4 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Carbonaceous BOD Received on Ice Sample Number 210630-16-03 Temp on Arrival:2.4 Parameter Schedule: TSS Received on Ice Sample Number 210630-16-04 Temp on Arrival:2.4 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6