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Home My WebLink AboutNC0021962_625 Scan_20210721Action History (UTC-05:00) Eastern Time (US & Canada) Submit by Anonymous User 7/21/2021 1:17:40 PM (Supplemental Submittal) Submit by Bennett, Tilman B 11/24/2021 9:57:58 AM (Supplemental Info Submittal) IN Lab Results for 625 Scan Bennett, Tilman B assigned the task to Bennett, Tilman B 11/24/2021 9:56 AM • The task was assigned to Thedford, Wren, Bennett, Tilman B 7/21/2021 1:17 PM Initial Review Information Updated ID#: * IMPORTANT: REVIEWER SHOULD VERIFY and revise here if necessary. NCO021962 How should this project be handled?* File Discard Information Submitted on 7/21/2021 Submitter Information Name: James Utke Who is submitting the information? Email Address:* jutke@citgo.com Submittal Information The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through the eDMR system and should not be submitted here. Division staff will review all uploaded documents and will only maintain required information. Documents such as laboratory reports are not required to be submitted and will not be maintained in the system. Project Information: Please supply the permit number for this project. ...................................................................................................................................................................................................................................................................................................................................................................................................... Existing ID#* Permit Number NCO021962 Examples: NCxxxxxxx or NCGxxxxxx Facility Name: * CITGO Petroleum Corporation County: Mecklenburg Please upload all files that need to be submited.* Click the upload button or drag and drop files here to attach document NPDES625June2021.pdf 7.16MB Only pdf files are accepted. Comments about the attachments: 625 Compound Scan Submittal. June 2021. * By checking the box and signing box below, I certify that: o I have given true, accurate, and complete information on this form; a I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act) a I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act'); a I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written signature; AND o I intend to electronically sign and submit the Supplemental Information form." Full Name: James Earl Utke Signature: r,A1V65W4O6& Date Submitted: 07/21/2021 ow ace na>Iytical ANALYTICAL REPORT / June 24, 2021 I CITGO-Charlotte, NC Sample Delivery Group: L1366918 Samples Received: 06/16/2021 Project Number: SEMIANN Description: Treated stormwater Report To: Mr. Jim Utke 7600 Mount Holly Road Charlotte, NC 28214 Entire Report Reviewed By: U Reagan Johnson Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 a d , ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provide , and as the samples are received. r- r F a , , x 77 N )UNT: PROJECT: SDG: ATE/TIME: PAG_z. arlotte, NC SEMIANN L1366918 0 24/2117:08 or13 TABLE OF CONTENTS or [p�Cover Page Tc: Table ofContents 2 � Ss: Sample Summary 3 Cn:Case Narrative 4 ' Sr: Sample Results S LJOUTFALL0O1 L1366918f] 5 []c Quality Control Summary 7 Semi Volatile O�an��om�u�s��1 7 l � ` - ��^ -- -_- . '- G|:Glossary ofTerms 11 L__ J A174ccnydheions&Locations 12 / Sc: Sample Chain ofCustody 0 — - �Ccouwr peoJscr sma PAGE OUTFALL 001 L1366918-01 WW . w SAMPLE SUMMARY :Ile.ted by RobD:iham C ;Ixtc :1:0t : o��;l ;-_I�; t: ;r✓.>-�:�:, Method Batch Dilution Preparation Analysis Aiiolyst Loa111011 date/time date/time Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1690S63 1 06/21/21 15:11 06/22/2116:27 Mlvl bit 1::6rt. l N f C-I f i ACCOUNT: PROJECT. SDG: ATE/TIME: PAGE: CIT 0-Charlotte, NC SEMIANN L1366918 0 /24/2117.08 Y CASE NARRATIVE II sample aliquots were received at the correct temperature, in the proper containe ppropriate preservatives, and within method specified holding times, unless qualifiE 1e report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for envil ave been corrected for the dilution factor used in the analysis. All Method and Batc re within established criteria except where addressed in this case narrative, a non-( r properly qualified within the sample results. By my digital signature below, I affirm nowledge, all problems/anomalies observed by the laboratory as having the potent uality of the data have been identified by the laboratory, and no information or data nowingly withheld that would affect the quality of the data. eagan Johnson oject Manager with the or notated within nmental samples Quality Control nformance form the best of my I to affect the ave been ACCOUNT: PROJECT: SOG'. IO-Charlotte, NC SEMIANN L1366918 IME: PAGE: 17:08 4 ) "', OUTFALL 0�01 Collected date/tim : 06t15/21 09:00 SAMPLE RESULTS - 01 L1366918 Semi Volatile Analyte - . Acenaphthene Acenaphthylene Anihiacene Benzidine Benzo(a)anthracene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(g,h,i)perylene Benzo(a)pyrene B is(2-chloroethyl)et h 2-Chloronaphthalene Chiysene Dibenz(a,h),inthiacene 3,3-Dichlorobenzidine 2,4-Dinitrotoluene 2,6-Dinitrotoluene 1,2-Diphenylhydrazine Fluoranthene Fluorene Hexachloiobenzene Hexachloro-1.3-butadie Hexachloroethane. Isophorone, Naphthalene Nitrooenzene n-Nitrosodiph Phenanthrene Senzylbutyl phthalate Bis(2-othylhexyl)phthala Di-n-butyl phthalate Diethyl phthalate Dimethyi phthalate Di-n-octyl phthalate Pyrene 1,2 n-Tnchlorobenzene 4-Chlofo-3-met hylphen( 2-Chlorophenol 2,4-Dichiorophenol 2,4-Dimethylphenol 2A-Dmitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenof Phenol 2,4,6-Trichlorophenol (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl Drganic Compounds (GC/MS) by Method 625.1 Result Oualifier MDL RDL Dilution Analysis Batch mg/I mg/I mg/I date/time U 0.0000886 0.00100 1 06/22/202116:27 WG16905 3 U 0.0000921 0.00100 1 06/22/202116:27 WG16905 U 0.0000804 0.00100 1 06/22/202116:27 WG16905 U J3 J4 0.00374 0.0100 1 06/22/202116:27 WG16905 U 0.000199 0.00100 1 06/22/202116:27 WG1690563 U 0.000130 0.00100 1 06/221202116:27 WG1690563 U 0,000120 0.00100 1 06/22/202116:27 WG169056 U 0.000121 0.00100 1 06/22/202116:27 WG169056 U 0.0000381 0.00100 1 06/221202116:27 WG169056 me U 0.000116 0.0100 1 06/22/202116:27 WG169056 U 0.000137 0.0100 1 06/22/202116:27 WG169056 pane) U 0.000210 0.0100 1 06/22/202116:27 WG169056 ther U 0.0000877 0.0100 1 06/22/202116:27 WG169056 U 0.0000648 0.00100 1 06/221202116:27 WG169056 they U 0.0000926 0.0100 1 06/22/202116:27 WG169056 U 0.000130 0.00100 1 06122/202116:27 WG169056 U 0.0000644 0.00100 1 06/22/202116:27 WG169056 U 0.000212 0.0100 1 06/22/202116:27 WG169056 U 0.0000983 0.0100 1 06/22/202116:27 WG169056 U 0.000250 0.0100 1 06/22/202116:27 WG169056 U 0.000105 0.0100 1 06/22/202116:27 WG169056 U 0.000102 0.00100 1 061221202116:27 WG169056 U 0.0000844 0.00100 1 06/22/202116:27 WG169056 U 0.0000755 0.00100 1 06122/202116:27 WG169056 e U 0.0000968 0.0100 1 06/22/202116:27 WG169056 ene U 0.0000598 0.0100 1 06/22/202116:27 WG169056 U 0.000127 0.0100 1 06/22/202116:27 WG169056 U 0.000279 0.00100 1 06/22/202116:27 WG169056 U 0.000143 0.0100 1 06/22/202116:27 WG169056 U 0.000159 0.00100 1 06/22/202116:27 WG169056 U 0.000297 0.0100 1 06/22/202116:27 WG169056 U 0.000998 0.0100 1 06/22/202116:27 WG169056 U 0.00237 0.0100 1 06/22/202116:27 WG169056 ie U 0.000261 0.0100 1 061221202116:27 WG169056 U 0.000112 0.00100 1 06/22/202116:27 WG169056 U 0.000765 0,00300 1 06/22/202116:27 WG169056 e U 0.000895 0.00300 1 06/22/202116:27 WG169056 U 0.000453 0.00300 1 06/221202116:27 WG169056 U 0.000287 0.00300 1 06/22/202116:27 WG169056 U 0.000260 0.00300 1 06/22/202116:27 WG169056 U 0.000932 0.00300 1 06/22/202116:27 WG1690S6 U 0.000107 0.00100 1 06/22/202116:27 WG169056 U 0.0000698 0.0100 1 06/22/202116:27 WG169056 U 0.000131 0.0100 1 061221202116:27 WG169056 U 0.000133 0.0100 1 06/22/202116:27 WG169056 U 0.000102 0.0100 1 06/22/202116:27 WG169056 U 0.0000636 0.0100 1 06/22/202116:27 WG169056 of U 0.00112 0.0100 1 06/22/202116:27 WG169056 U 0.00593 0.0100 1 06/22/202116:27 WG169056 U 0.000117 0.0100 1 06/22/202116:27 WG169056 U 0.000143 0.0100 1 06/22/202116:27 WG169056 U 0.000313 0.0100 1 06/22/20211627 WG169056 U 0.00433 0.0100 1 06/22/202116:27 WG169056 U 0.000100 0.0100 1 061221202116:27 WG16905G 36.9 15.0-314 06/22/202116:27 WG169056 56.6 22.0.127 06/22/202116:27 WG169056 ACCOUNT: PROJECT. SDG: ATEITIME: PAGE. ;O-Charlotte, NC SEMIANN L1366918 0 /24/2117:08 5 of ,3 OUTFALL 001 SAMPLE RESULTS - 01 Collected dateltim . 06/15/21 09:00 L1366918 Semi Volatile rganic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/1 mg/I date I time (S) p-Telphenyl-M 53.8 29.0-141 061221202116:27 WG16f (S) Phenol-d5 12.0 8.00-424 061221202116:27 WG16S (S) 2-Fluorophenol 20.8 10.0-120 061221202116:27 MW (S)2,4,6-Tribromop' nol 53.1 10.0-153 0612Y202116:27 WG16S i L-,j CrI� a";.. ACCOUNT: PROJECT: SDG: ATE/TIME: PAGE: iO-Charlotte, NC SEMIANN L1366918 0 /24/2117:08 J 2 o G o O O o 0 0 o O o O O o o O O CJ O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O jr O O O O O O O O O O O O O O O O O O O O O O O O O O O O O I i. 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En F E Fu)l 4 E J m d D: Z UlI 0 U J G p O O 00 O O m � N N of O OO p 00-0 W h tn r� io P� ^ N �i rn GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sampl . ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampl ng Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbileviations and Definitions MDL Method Detection Limit, RDL Reported Detection Limit. Rec. Recovery, RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory C ntrol Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. S rrogates are not expected to be detected in all environmental media. u Not detected at the Reporting Limit (or MDL where applicable). Analyt The name of the particular compound or analysis performed. Some Analyses and Met ds will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or eight values differ from the Dilutioi standard, or if concentrations of analytes in the sample are higher than the highest limi laboratory can accurately report, the sample may be diluted for analysis. If a value diffe of concentration that the than 1 is result reported has already been corrected for this factor. ent used in this field, the Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target it analytes recovered or duplicated within these ranges. Qualifi This column provides a letter and/or number designation that corresponds to additiona information concerning the result r reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossa potentially a discussion of possible implications of the Qualifier in the Case Narrative if and Definitions page and ipplicable. The actual analytical final result (corrected for any sample specific characteristics) repoi Led for your sample. If there was Result no measurable result returned for a specific analyte, the result in this column may state (Below Detectable Levels). The information in the results column should always be accompanied 'ND" (Not Detected) or "BDL" by either MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest valu an that the laboratory could detect or report for this analyte. uncertainty (Radiochemistry) Confidence level of 2 sigma. ma. g Case Narrative A brief discussion about the included sample results, including a discussion of any non (Cn) observed either at sample receipt by the laboratory from the field or during the analytic onformances to protocol I process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample This is the document created in the field when your samples were initially collected. Thi Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is used to verify the time and is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratoryfor analysis. This section of your report will provide the results of all testing performed on your Samp es. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each s mple ID, including the dates and times of preparation and/or analysis. Qualifier J3 J4 Description The associated batch QC was outside the established quality control range for The associated batch QC was outside the established quality control range for PROJECT: SDG: C�ATE/TIME: PAGE NC SEMIANN L1366918 0 /24/2117:08 oi'J ACCREDITATIONS & LOCATIONS Dace AmIlytical National 12065 Lebanon ion Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TN002 California 2932 New Mexico TNO0003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R•140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky's KY90010 South Carolina 84004002 Kentucky 16 South Dakota n/a Louisiana A130792 Tennessee' ° 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas' LA60152 Maryland 324 Utah TN000032021-11 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2LA A21-A — ISO 1702 1461.01 AIHA-LAP,LLC EMLAP 789 A2LA— ISO 1702 5 1461.02 DOD F1461.01 Canada 1461.01 USDA 0-15-00234 EPA—Crypto TNO0003 Drinking Water ' Underground Storage Tanks 3 Aquatic Toxicity ° Chemical/Microbiological 5 Mold 'Wastewater n/a Accreditation not applicable Not all certificatilons held by the laboratory are applicable to the results reported in the attached report. Accreditation is my applicable to the test methods specified on each scope of accreditation held by Pace Analytical. PROJECT: SDG: ATE/TIME: PAGE NC SEMIANN L1366918 0 '24/2117:08 12 cf 1? 16M � � . . � � � � . �\ � ƒ� �� /;;�/ ./ �m �w ^ / � \ k �.\ \\�\ � ��}��\\ . I