Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
NC0069841_Results from second Lab_20210721
Action History (UTC-05:00) Eastern Time (US & Canada) Submit by Anonymous User 7/21/2021 11:43:57 AM (Supplemental Submittal) Submit by Bennett, Tilman B 11/24/2021 9:44:39 AM (Supplemental Info Submittal) IN Reporting second Lab results here Bennett, Tilman B assigned the task to Bennett, Tilman B 11/24/2021 9:42 AM • The task was assigned to Thedford, Wren, Bennett, Tilman B 7/21/2021 11:44 AM Initial Review Information Updated ID#: * IMPORTANT: REVIEWER SHOULD VERIFY and revise here if necessary. NCO069841 How should this project be handled?* File Discard Information Submitted on 7/21/2021 Submitter Information Name: Alex Laytham Who is submitting the information? Email Address:* alex.laytham@unioncountync.gov Submittal Information The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through the eDMR system and should not be submitted here. Division staff will review all uploaded documents and will only maintain required information. Documents such as laboratory reports are not required to be submitted and will not be maintained in the system. Project Information: Please supply the permit number for this project. ...................................................................................................................................................................................................................................................................................................................................................................................................... Existing ID#* Permit Number NCO069841 Examples: NCxxxxxxx or NCGxxxxxx Facility Name: * Crooked Creek County: Union Please upload all files that need to be submited. * Click the upload button or drag and drop files here to attach document CC 6-1-2021.pdf 1.64MB CC 6-2-2021.pdf 1.47MB CC 6-3-2021.pdf 1.48MB CC 6-7-2021.pdf 1.47MB CC 6-8-2021.pdf 1.46MB CC 6-9-2021.pdf 1.48MB CC 6-14-2021.pdf 1.46MB CC 6-15-2021.pdf 1.46MB CC 6-16-2021.pdf 1.45MB CC 6-21-2021.pdf 1.48MB CC 6-22-2021.pdf 1.46MB CC 6-23-2021.pdf 1.97MB CC 6-28-2021.pdf 1.41 MB CC 6-29-2021.pdf 1.47MB CC 6-30-2021.pdf 1.54MB Only pdf files are accepted. Comments about the attachments: Samples were split between Charlotte Water lab and Statesville Analytical lab during the month of June to help ease into a transition of switching labs from Charlotte to Statesville. Attached are the Statesville lab results and Charlotte Waters was reported on the eDMR. * By checking the box and signing box below, I certify that: o I have given true, accurate, and complete information on this form; o I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act') o I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act'); o I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written signature; AND o I intend to electronically sign and submit the Supplemental Information form." Full Name: Alex Laytham Signature: Date Submitted: 07/21/2021 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/01/2021 Reported: 06/08/2021 For: Comments: Sample Number Parameter Sample ID Result 210601-36-01 Ammonia UCCC-Inf 29.34 210601-36-01 BOD UCCC-Inf 155 210601-36-01 TSS UCCC-Inf 212.7 210601-36-02 Ammonia UCCC-Eff 0.45 210601-36-02 BOD UCCC-Eff 2.36 210601-36-02 TSS UCCC-Eff <2.551 210601-36-03 Fecal Coliforms UCCC-Eff (LAB) 135.4 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/01/2021 CE mg/L SM521OB-2011 06/02/2021 CE mg/L SM2540D-2011 06/04/2021 CE mg/L SM4500NH3E-2011 06/01/2021 CE mg/L SM521OB-2011 06/02/2021 CE mg/L SM2540D-2011 06/04/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/01/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210601-36-01 Temp on Arrival: 4.4 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210601-36-02 Temp on Arrival: 4.4 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210601-36-03 Temp on Arrival: 4.4 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 g n 00 c7 n 0o> Fn z C! Cl f] f7 A f) A ? a 61 a -¢y¢yi 0 9 T ril T Z Z T T y' o, AL ft G w '� P,t g TJ �p Sampler Initials c N old Sample Begin Dale q g = � o z�1 Sample Begin Time a o `J �1 o e Sample End Date Tmm m T N Sample End Time a ° ° Date Samola CoYeued AlNO �S� AMOLV21 _ _ _ _ _ 9tll Sample Collected Nonnated System (YIN) -We Type (See Below) Alai., Type (See Belo of Containers M111 ACIDS RTHO-PHOSPHATE m ? � y C� D _ O ETALS RDNESS YANIDE " - r T n c N1 O 9 (i O IL & GREASE (HEM) ECAL COLIFORM c— m D Q J PO Box 228 ° Statesville, NC 28687 ° 704/872/4697 Page 3 of 4 n -i -i n 0 cu co co m i m e a 3 0. CD CD CD3 CD m 3 m 5' m �' 3 'x m C C a cm N O_ c� N Q m' O. (n' a m N CDD Q a o CA (n 3 3 `•ccr c. 3 5 3 N d yk 3 0 N 3 �. m m m cu �3 o � a `v a C CD ZY S C � 0 m a CD a N r cr Q 3 m m m 0 m m �� � Grab 3 3 3 3 D x sd 4t 3 m m m m c .�-.. N ' O lD m Z 0 2 Cl) m 0 0 O m W m - W 3 a 3 "a _ 'aH '... . O ;4.Q � Q CD 0 �• (C m a `C12 N cn rrl �• N Z R. r„ -n x N N a PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/14/2021 Reported: 06/21 /2021 For: Comments: Sample Number Parameter Sample ID Result 210614-26-01 Ammonia Nitrogen UCCC-INF 24.53 210614-26-01 BOD UCCC-INF 298 210614-26-01 TSS UCCC-INF 138.5 210614-26-02 Ammonia UCCC-EFF 0.11 210614-26-02 BOD UCCC-EFF 4.44 210614-26-02 TSS UCCC-EFF <2.674 210614-26-03 Fecal Coliforms UCCC-EFF 5.2 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3C-2011 06/15/2021 CE mg/L SM521OB-2011 06/14/2021 CE mg/L SM2540D-2011 06/18/2021 CE mg/L SM4500NH3E-2011 06/15/2021 CE mg/L SM521OB-2011 06/14/2021 CE mg/L SM2540D-2011 06/18/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/14/2021 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210614-26-01 Temp on Arrival: 3.1 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210614-26-02 Temp on Arrival: 3.1 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210614-26-03 Temp on Arrival: 3.1 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 NINE Fill ` �.m.......... .. . .m.......... =ME=..M.......... .... ..m.......... �.m.......... m1==.M.......... �.0©...©..... �.m.......... �i''.m........ �..........C. �.©...©...... �............ �............ �............ ..:©...©....... ..:............ ■M■■■MM■■■M■ �............ �............ �............ �..©...©..... - �............ pampo Domes oleo LABORATORY USE ONLY OWUPu3eldweg c LL _ wa Pu3 aidweg Z Z _ _ Z a E QW.juI6oGGjd Rs W W W ff aleO u6ag aldwe M r� — M' n _Cv_ Y o g$ € � F G W LL 2 LL 2 LL 2 LL LL LL 0 z tr 6 6 6 v c:f LY U o.3, W U O d < O y V > U > V > V > V > U > E E E , C g d E Ja t 6 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 @_)& 2 § /\g/ �■ » —2 w<P o \�k��� a + ` Gj®� © U - F § ° # 2 $ � ■ § o 3 § \ » L \ k _ CL k 2 \ / \ \ } U ) : ! 3 3 \ / )« k \ \ [ } # ( \ \ ( q � 2 2 E § § k @ Q P P / a I= � k E( [ # ƒ\ £ I cn , , j 3 k d ) [ k w \ \ \ ( / ( ( k71 k 7 2 J a= ) R 7= o a= § \ I \ \ \ i )\� } a) k a:v / / ° / / PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 Page 4y4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/15/2021 Reported: 06/25/2021 For: Comments: STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210615-26-01 Ammonia UCCC-INF 27.78 mg/L SM4500NH3E-2011 06/22/2021 CE 210615-26-01 BOD UCCC-INF 385 mg/L SM521OB-2011 06/16/2021 CE 210615-26-01 TSS UCCC-INF 374.3 mg/L SM2540D-2011 06/18/2021 CE 210615-26-02 Ammonia UCCC-EFF 0.22 mg/L SM4500NH3E-2011 06/22/2021 CE 210615-26-02 BOD UCCC-EFF <2 mg/L SM521OB-2011 06/16/2021 CE 210615-26-02 Fecal Coliforms UCCC-EFF 1.0 MPN/100 ml IDEXX Colilert 18 MPN 06/15/2021 CE 210615-26-02 TSS UCCC-EFF <2.732 mg/L SM2540D-2011 06/18/2021 CE Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210615-26-01 Temp on Arrival: 3.9 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210615-26-02 Temp on Arrival: 3.9 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 popmroo epun °'a 1=�- Grp-4 LABORATORY USE ONLY awil Pu3 91dweS fi 3 3 3 LL alga Pug aidweS _ i $ $ Z Y Z S 'o e41ui689 eMweS areau!BeG.jd—S S V G^ 1:z .j: C j7o� h $ e pRp ,,q�i slei,ul joldu2S c � O J LL LL LL LL LL LL LL LL LL > E E y 9Q 9a 6 qE y 2 7 fy y U U U U L) U U 0 V = E E y E 3 E ci LL a > > > w ui rii _ A B PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 N N N � b eo r„ 4 v .f. O O 4cu U E 0 N a U v � 3 ro o E O O O N E m c E L E c ro o 0 0 0 avi _m O N N N E '` `t \ E � yk n. a x m ro R U - cEa N ^� .d= G E E E E E 1- H F- rj X .a � J 3G o + E c m O m O Q p C7 L a m ¢ 00 1 o O 0 0 9 E E E E _ O. Q N O_ Q E E E E m w 0 cd cC j E E C F2 I ( a T U T N co m d � i ! I N 'O N 'C dl N C � •� C O O C rNii m v 0 O O a 6 > CT a L d N C U C U 41 CD a) a) E E o E F PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/16/2021 Reported: 06/30/2021 For: Comments: Sample Number Parameter Sample ID Result 210616-30-01 Ammonia UCCC-INF 29.12 210616-30-01 BOD UCCC-INF 272 210616-30-01 TSS UCCC-INF 162.7 210616-30-02 Ammonia UCCC-EFF 0.12 210616-30-02 BOD UCCC-EFF <2 210616-30-02 Fecal Coliforms UCCC-EFF <1 210616-30-02 TSS UCCC-EFF <2.717 210616-30-03 Total Solids UCCC-RAS 4824 210616-30-03 Total Volatile Solids UCCC-RAS 3336 210616-30-04 Total Solids UCCC-DIG 705 43788 210616-30-04 Total Volatile Solids UCCC-DIG 705 28032 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/22/2021 CE mg/L SM521OB-2011 06/17/2021 CE mg/L SM2540D-2011 06/18/2021 CE mg/L SM4500NH3E-2011 06/22/2021 CE mg/L SM521OB-2011 06/17/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/16/2021 CE mg/L SM2540D-2011 06/18/2021 CE mg/L SM2540B-1997 06/18/2021 MD mg/L SM2540G-2011 06/18/2021 MD mg/L SM2540B-1997 06/18/2021 MD mg/L SM254OG-2011 06/18/2021 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 Condition of Receipt Sample Number 210616-30-01 Temp on Arrival: 2.9 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210616-30-02 Temp on Arrival: 2.9 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210616-30-03 Temp on Arrival: 2.9 Parameter Schedule: Total Solids Received on Ice Parameter Schedule: Received on Ice Sample Number 210616-30-04 Temp on Arrival: 2.9 Parameter Schedule: Total Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 5 Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 5 �� C O a LY p N z y 0 � s3 V 0 U a W Of 0 O � WHOdIl001tl03 0 (W3H) 3SY389 V 11 U u O 301NVA Z MN0 SONOHdSOHd FN S. a E 00 ¢ SOC 9008 w (Zl <! y>1 Mks PMJI4W le Rd ae>IPR-Aiw 3s0 6Y EMU N K 10 LL chi �' HOE 6Osz m a EON 3NO s,euieryo0 )o r re •ores BeSI adAl,eurelua g W � � IrwNB �S) edAl epwe z 'A (NIA) we1SAS PelewoN De1�eIP0 eldweS aui1 U m v � ti 3 r� e a m a a 09Z 09Z U Q Z Z M E � i c? > � Q Pa1PeINo eldweS erea .� LABORATORY USE ONLY aw)1 Pu3 a)dwes w w ama Pu3 a)dweS � 1 \ Z Z Z Z O V c eW1 u16e8 epweS } i } u co rc V O z LL z � U ale0 u16eg eldureS �_. � E4 $ sle!pu1,eowes S Q L 1 v rCC F Ll` �Epy H } W W LL Z LL Z LL Z LL Ly LL W LL W N Vr C? d m E r C W o Q m U U U cJ U u U U U U U U U U U U LL U Q > > > > > > > > N U PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 5 u: (ask 2 c « 2 ® E § e ) ® 7 7 § § L 6 ^ 2 CD E ® § A ` E 5 / c ƒ . } / $ 3 } } \ k ) \ \ § LI t 2d k k \ [ } \ ( ( ( ƒ � "0 0 . � E E E E ( / E/ �\ I I a � E� \ / k ) / - . [ \ E E • § _ _ � ^ ( \ ( \ . . / E £ & 2cc § a) ID 7 ƒ o , r \ k } \ / / �/ cr } \ \ ) § / E § $ E b< o 0- aG = Cc I = Q P P o P PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 Page 5y5 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/21/2021 Reported: 06/28/2021 For: Comments: STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210621-06-01 Ammonia UCCC-INF 8.85 mg/L SM4500NH3E-2011 06/22/2021 CE 210621-06-01 BOD UCCC-INF 75.0 mg/L SM521OB-2011 06/21/2021 CE/WC 210621-06-01 Fecal Coliforms UCCC-INF <1 MPN/100 ml IDEXX Colilert 18 MPN 06/21/2021 WC 210621-06-01 TSS UCCC-INF 96 mg/L SM2540D-2011 06/25/2021 CE 210621-06-02 Ammonia UCCC-EFF 0.11 mg/L SM4500NH3E-2011 06/22/2021 CE 210621-06-02 BOD UCCC-EFF 4.38 mg/L SM521OB-2011 06/21/2021 CE/WC 210621-06-02 TSS UCCC-EFF 9.677 mg/L SM2540D-2011 06/25/2021 CE Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210621-06-01 Temp on Arrival: 5.9 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210621-06-02 Temp on Arrival: 5.9 pH on Arrival: <2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 3 a 3 3 3 f�'1 0 00n 0 0 9 0 9 n 9 3 � m A Z T m (Ryol N O 3 V m ° o m P ° °•�]7{{ T 1 m .11 O 2 fa` M _ Sampler Ineials ° _ e Begin Date a � _I a; c� n m .. 7 C _ s — T .. _ Y /y� '� Sample Begin rme m o o m y m y —' ^T v /� t/11 t _ _1 11_\ 1 O z a 0 0 0 v ample End Date o = � � m Ln , n n > :-% Ci N c Sample End Time Dble Samp a Collected AlN0 3sn AN51v-1 oevi \1 Y Sample Collected A *Wed System (YIN) z c m 0 y q m � m n 3 m � A m � ` 3 � 5 D y D 3 m y ^� Me Type (See Below) einer Type (See Belown; :aMahiers 1 Size (ml) 3 v )4 H �rF i203 USE ONLY-Indlege pH of ervee Swnple (<2;>12) 5 z S ATILE ACIDS TORUS z 'HATE 3 g 1 (HEM) PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 -I (� m CCD m 0 0 3 N O a co m m 3 m m 3 m m a C C w3 m O m n m N N y D_ (a a ClLm W Q. U) n. � s S. f�D O ID `CY CD "� M Ul fA CL O ? T c � 3 .. 3 3 3 3 0 ' 3 3 9 o a v v w w w w m m co co 3 od 3 � b N a a a �m <v 7 a r c 3 m m m m m " Grab C-R 3 3 3 3) a - 3 3 3 3 3 x m m m F I_ti I_N _ v N O O O A]y - - 3 a m 3 8 A m ? Q Q �v �• (D a cr CD 2 'n ti C � a z _• T a �o N N a PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/02/2021 Reported: 06/09/2021 For: Crooked Creek WWTP Comments: Sample Number Parameter Sample ID Result 210602-21-01 Ammonia UCCC-Inf 29.46 210602-21-01 BOD UCCC-Inf 331 210602-21-01 TSS UCCC-Inf 221.7 210602-21-02 Ammonia UCCC-Eff 0.34 210602-21-02 BOD UCCC-Eff <2 210602-21-02 TSS UCCC-Eff <2.512 210602-21-03 Fecal Coliforms UCCC-Eff (Lab) 99 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/08/2021 CE mg/L SM521OB-2011 06/03/2021 CE mg/L SM2540D-2011 06/04/2021 CE mg/L SM4500NH3E-2011 06/08/2021 CE mg/L SM521OB-2011 06/03/2021 CE mg/L SM2540D-2011 06/04/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/02/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210602-21-01 Temp on Arrival: 1.6 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210602-21-02 Temp on Arrival: 1.6 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210602-21-03 Temp on Arrival: 1.6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 S 0 N N N N A C.) 0 C) 0 in in Ca 0 n (i n O➢ P z — N �R m 0 c� n 0 A,z 0 0 C) ; m 7 z N a 3 a s 3 3 T T T T T T z T z T m o N a m n o —1 Sampler Irulials g o a e 1 & n 3 N Sample Begin Date n$ 0 R o -4-1 ' SNnple Beglll TYlle 3 _ n 0 0 0 Sample End Date n n n __V ° Sample End Time Dale San,pie coueaed AlN0 3sn Aiioiv2109v1 `^M1070 :j A i> " o�o 3 g? c i I?' 3.I > n n � s l" J C� G Time Sample Cdleclee z z z z z z CAlom ted Syst(YINI N z m 8 -I 0 I Iem C)D D O O 0 ample Type (See Below) �" v v v onlairler Type (See Below J ..• ..• .' of Containers 500 1000 1000 1500 250 250 IMle See (m) m y 3 8 x x one 3 1403' A n D X x 2SO4 0 3 � °' X m a0H g CI - - E. ` ti� a2S203 0. m LAB USE ONLY-Iedlute pN oy preu W Sample l,2.,12) Boos _ X 3OD5 s ^_ ! ? OD �1 Ir PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 St e0 3 e nƒ ƒ ƒ ƒ 3 3 0 > o_ \ ) } 2 2 2 § \ 3 \ / . #; ® $ ` _ ` 0 I 0 E�£ k 3 k E r` - 5 J s■ F } F / ! 3 5 3 3" e a' 0 2 E E E 0 $E � -0 C. 0 \� �) ( CD 41, �\ i c 2 2 CD2 CD $ _ ®— \ Cc 3 3 j �( 7 ] \ 3 / 2 2 2 2 ! E E E f ~ ƒ § ± k \ / ] K - 7 . $ ƒ G / i CF . - 2 CD` e c > \ CD _!�\ �w=zar2 > PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 94y4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/22/2021 Reported: 07/01 /2021 For: Comments: Sample Number Parameter Sample ID Result 210622-17-01 Ammonia UCCC-INF 20.38 210622-17-01 BOD UCCC-INF 253 210622-17-01 TSS UCCC-INF 6.904 210622-17-02 Ammonia UCCC-EFF <0.1 210622-17-02 BOD UCCC-EFF 2.89 210622-17-02 TSS UCCC-EFF 10.66 210622-17-03 Fecal Coliforms UCCC-EFF(LAB) <1 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/29/2021 CE mg/L SM521OB-2011 06/23/2021 CE mg/L SM2540D-2011 06/25/2021 CE mg/L SM4500NH3E-2011 06/29/2021 CE mg/L SM521OB-2011 06/23/2021 CE mg/L SM2540D-2011 06/25/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/22/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210622-17-01 Temp on Arrival: 3.6 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210622-17-02 Temp on Arrival: 3.6 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210622-17-03 Temp on Arrival: 3.6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 o = y m m n n n n n n 'o M O 0 m m !SP 8 3m 3 T T m = T T m y pg ll R 3etz s~ S T H Sampler Initials $ N 0 Sample Begin Date = $ it $p$ T Sample Begin Time 3 o c �., c 0 0 0 9 .Y Sample End Date g m •� .� � cj 7 J y Sample End Time s a n Q� iJ C � v V DaleSampieCollected AlNO3Sf1A2i01Vtl08M I,� zi g yJ '} Time Sample Collected4! ~ _ _ _ = 2 z Chlorinated System (YIN) C, i S S in g a� ID AD ADD O AD Sample Type (See Below) 3 nlamer Type (See Below m a ii — — — — — -• P of Containers m '1 500 1000 1000 500 250 250 lBoUe Size (mi) x x x x one NO3 W x x 12SO4 NaOH g co 3 3 K N A CI �° p 9 � ✓) 3 a2S203 � y LAB USE ONLY-Iedklb pN of wwwedSon& (<2;>12) Y a u BOOS 2_ D x x O05 a a l ................ PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 n -I =I n 77 ]J 1J SJ m CD CD 3w v c 3 y 0O = a CD CD 3 25 m m CD m' D N C = CD O m �. m Cl ID y 2 Co y a CD a to zr = = ry N l9 !fl CD CD c Q c' Q. 41 3 3 I rb 3 3 ro 3 i �+ @ �CD_ Imo_ h lit,I � UO O ;n 3 I I i CD .0 o N CD �l N p6 g 33" Zg p 7 3k N ID a r 6 `~ 0 3 3 3 3 3 3 CD CD CD CD N W Gb 3 3 33 X m s � a 3 3 �x 0 0 0 0 m m m m Ey m I� m N 3 o i CD N z v o 0 � 0 � y = m RL - 3 a = 3 o 0cn O A� O CL o CL s CD ti g 6> z G y A� J N (/1 Y �bM N Z e A A n ti N tJ PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/23/2021 Reported: 07/16/2021 For: Comments: STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 210623-15-01 Ammonia UCCC-Inf 22.06 mg/L SM4500NH3E-2011 06/29/2021 CE 210623-15-01 BOD UCCC-Inf 151 mg/L SM521OB-2011 06/24/2021 CE 210623-15-01 TSS UCCC-Inf 106 mg/L SM2540D-2011 06/25/2021 CE 210623-15-02 Ammonia UCCC-Eff <0.1 mg/L SM4500NH3E-2011 06/29/2021 CE 210623-15-02 BOD UCCC-Eff 2.31 mg/L SM521OB-2011 06/24/2021 CE 210623-15-02 Hardness UCCC-Eff 137 mg/L CaCO3 Calculation 07/08/2021 MD 210623-15-02 Nitrate/Nitrite UCCC-Eff 21.3 mg/L SM450OF-2011 06/30/2021 CL 210623-15-02 Silver UCCC-Eff <0.0005 mg/L EPA200.7 07/08/2021 MD 210623-15-02 T. Phosphorous UCCC-Eff 0.8 mg/L SM450OPE-2011 06/25/2021 CL 210623-15-02 TKN UCCC-Eff 2.13 mg/L SM4500NorgB-2011 07/02/2021 CE 210623-15-02 TSS UCCC-Eff 8.477 mg/L SM254OD-2011 06/25/2021 CE 210623-15-03 Total Solids UCCC-RAS 5188 mg/L SM2540B-1997 06/24/2021 WC 210623-15-03 Total Volatile Solids UCCC-RAS 3700 mg/L SM2540G-2011 06/25/2021 WC 210623-15-04 Total Solids UCCC-DIG 705 19964 mg/L SM254OB-1997 06/24/2021 WC 210623-15-04 Total Volatile Solids UCCC-DIG 705 11964 mg/L SM254OG-2011 06/25/2021 WC 210623-15-05 Fecal Coliforms UCCC-Eff(lab) <1 MPN/100 ml IDEXX Colilert 18 MPN 06/23/2021 WC Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 6 Condition of Receipt Sample Number 210623-15-01 Temp on Arrival: 1.0 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210623-15-02 Temp on Arrival: 1.0 pH on Arrival: <2 Parameter Schedule: Nitric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Hardness Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 6 pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210623-15-03 Temp on Arrival: 1.0 Parameter Schedule: Total Solids Received on Ice Sample Number 210623-15-04 Temp on Arrival: 1.0 Parameter Schedule: Total Solids Received on Ice Sample Number 210623-15-05 Temp on Arrival: 1.0 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 6 n _ y 3 = ' T 3 N 3 N 3 C (7 0 C 0 n S 0 C 0 0 C 0 cr C 0 O C 0 R C 0 C) C 0 n V n T C O D O n m a a m a V ~ v ~ V T T T T T T T T T T T T 2 T 2 T 2 T r m 0 N g S SP S J Tj Sampler Initials c1 c 3 ,T, iR � S $ _ Sample Begin DaleFr v✓ n O rA _ n' Q Sample Begin Time o e A o e; w w Sample End Date zo M m T Sample End Time L w ci c F w Date SampleCdecletl AlNO3Sf1A2101VbOBVI I - jTu*SampIeCG11weO n — Q s IF , D n z z z z z z z z z CNonnaled System(YM) g O 0 0 0 O 0 O AD D ample Type (See Below) 3 a .. n y v a "013 `0 `0 m � m onlainer Type (See Below o a A m ' 3 8 500 500 500 500 1000 1000 500 50 250 of Containers Er S¢e(M) x x x x ONE x x NO3 m x x x 2SO4 8 c a0H n n 3 m A CI n ' 3 a2S203 w e^ rc `- � -g r �I�S9 3 LAO USE ONLY -Indicate pH al Preened Sample l' 2:>12) rn Y 3 c^ OD5 n S $ S i� x x cc ACIDS G k _ x DNESS (#Hardness) 3 Z 11CYANIDE 9 O T n 0 IL & GREASE (HEM) ECAL COLIFORM O O M m % O w D C i m o J o N PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 6 m it w o Sampler lnYials g IT _ ps Sample Begin Date = $ Z .11 O N Sample Begin Tine 4 � g o Sample End Date P T T N N Sample End Time - m D w w DalesampeCouectea AINO38f1AMOIYMQBV! w g ci H d g 3 S $- m' 3 8 8 � g CTune Sample Cotlecled z 0 z z CNonnated System(YIN) G> Q Sainoe Type (See Beim) Wrier Type (See Below 9 of Containers �. 2X0 me Sae(m) XO ONE NO3 3 u d 25 D c m _� n H2SO4 NaOH g CI 2 R H 7 2 a a # S i ` § 3 a S203 o` v On LAa USEOWY-11 **PH.W vra.rvM s. l.t;>tYy U0D5 m JC 00 ACIDS M.........-.. 0. . - o MMMMMMMMMMMM MOMMOMMOMMOM MMMMMMMMMMMMa�� i MMMMMMMMMMMMIM MMMMMMMMMMMM MMMMMMMMMMMM 111111111,00 Hill 11 Is PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 6 n ID COED CD3 j CL Q CD lD CD 3 (D (D 3 CD 7' CD 7 53 N CS CD C ro a' � CD� CD_ fl. a VN C1 to C1 to yr (�j F ' n N (C M. CQ ID CD Q a CD 0 m ff cr w SD w w 3 3 ro 3 3 i a a 0 0 0 licJ• d � m� m Ow e V n CD zy �0 nJ J N O w ¢v N 7 v� Q m cr a 3 3 3 3 ro ro ro m N \. N K Grab Vi C amp. 5D ID 3 3 3 3 x �m 3 3 3 3 x CD m m Im N ai �3 i fA W rs Z 0 _ 0 0 o w w 3 a 3 3,,, , C LO O v O � m O CD O0 CD CL m w 0' CD CL � fn .. m ro o N N Ji O :n Z • � � R ' x r n r.a N PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 6 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/28/2021 Reported: 07/06/2021 For: Comments: Sample Number Parameter Sample ID Result 210628-03-01 Ammonia UCCC-INF 25.76 210628-03-01 BOD UCCC-INF 331 210628-03-01 TSS UCCC-INF 174.5 210628-03-02 Ammonia UCCC-EFF <0.1 210628-03-02 BOD UCCC-EFF 3.00 210628-03-02 TSS UCCC-EFF <2.660 210628-03-03 Fecal Coliforms UCCC-EFF(LAB) <1 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/29/2021 CE mg/L SM521OB-2011 06/28/2021 CE/LE mg/L SM2540D-2011 07/01/2021 LE/CE mg/L SM4500NH3E-2011 06/29/2021 CE mg/L SM521OB-2011 06/28/2021 CE/LE mg/L SM2540D-2011 07/01/2021 LE/CE MPN/100 ml IDEXX Colilert 18 MPN 06/28/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210628-03-01 Temp on Arrival: 2.4 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210628-03-02 Temp on Arrival: 2.4 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 A fA N N (n 41 0 0 0 o n r 0 On n m n m 9 z 9 z 9 z 3 m� i m 3 — m ° o m A 0 o `b Sampler Indials R T Q m s ggT i _ o g u o n9 o om .. N Sample Begin Dale a is N N N I\ O W W Sample Begin The 9 a oo � S � z T Y 0 Sample End Date o n Ntg T Sample End Time o kINO asn A80T"—c 9V1Q .■...o.°MMM MMM :.....ovvMMIM ME ME .........MINE ._.......MINE . MMMEMEMNow �E mom ■mom ■■mom ......MWIM ...... .: .........MIME .� .........MINE MMMMMMMMMMMIMi MMMMMMMMMMEM EMMMMMMEME.M""�■ PHOSPHORUS g 0 ME .....MM .......� • ......ME MINE EMMEEEEMEMEM� • MEMEMEEEEEINEE� r �1' PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 ƒ 0 2 ? / ƒ 01� , , O lu % o q » E g E m m o, ,, - q 2 - - E 2 a « } / S \ to 8 / - & (n ( ' F \ f \ . § cr r g g \ \ : a s a 3' » 2 E m E E k _ Ow ƒf I.. � I -� / ƒ ° 2[ C. CD 2/ \ 0 CD CD 2 » . QCorm. 3 ° 03 % / J 3 < , / 2 E { !� E E E ! / / ? 0 { ' f » 7 ] CD / E / 2 [ cl 9 — CD® = F CD CD k Qcr (\z} }\ 'n ®�§®'—f $�!(JG r /rn � a - m PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 94y4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/29/2021 Reported: 07/07/2021 For: Comments: Sample Number Parameter Sample ID Result 210629-15-01 Ammonia UCCC-INF 26.1 210629-15-01 BOD UCCC-INF 379 210629-15-01 TSS UCCC-INF 248.3 210629-15-02 Ammonia UCCC-EFF 0.34 210629-15-02 BOD UCCC-EFF <2 210629-15-02 TSS UCCC-EFF <2.732 210629-15-03 Fecal Coliforms UCCC-EFF(LAB) <1 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 07/06/2021 CE/MD mg/L SM521OB-2011 06/30/2021 CE mg/L SM2540D-2011 07/01/2021 LE/CE mg/L SM4500NH3E-2011 07/06/2021 CE/MD mg/L SM521OB-2011 06/30/2021 CE mg/L SM2540D-2011 07/01/2021 LE/CE MPN/100 ml IDEXX Colilert 18 MPN 06/29/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210629-15-01 Temp on Arrival: 2.2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210629-15-02 Temp on Arrival: 2.2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210629-15-03 Temp on Arrival: 2.2 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 a n {{ni1 ;llj C Chi Cn�) 2m T {�'1 11 nWSampleEndTime N o nafill .� p s g y n n C ; Dale • a mz• mN (V ^:: Time N on1 3 a o• cQ 3 z Qz �$ Z Zo O O "" d Date oTn tg md Time N N ate SampleConeaed AlNO3snAa01dNote 1 O D o N S O y 3 C a = 3 3 0 n u • c _ c> 3 _ �_ • 3 - .. A$ m m zv m 0 lnr O Time Sample Collected z z z z z z CNodnaled System (YIN) D D O D O O Type (See Below) a a a a a a onlainer Type (See Below of Containers m a z 3 B O 500 1000 1000 500 250 250 the Size(ml) 3 3 g" y n 3 3 y AN03 X x 2S01 a 80H • CA O 3 s a L a L = . � c m ? a2S203 m LAB IISEONLY-Yrdkale pH of INnrv�d sw (� 2:112) BOD5 ' - a D a o D g1 0r S R 3 S x x TSS SS J VOLATILE ACIDS `PLKALINMY x x kMMONLA 1 MATE -WRITE N Y - g li O z '� OTAL PHOSPHORUS THO-PHOSPHATE m ETALS G DNESS 5 ANIDE L IS GREASE (HEM) ECAL COLIFORM o � m z _ e 3 Q PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 9 e n 9 a n 2 fƒƒ 3? 3 0 2/ ) 2 ■ ) 2 § \ ƒ Z , = m = < = z ��� E(0 (& G g E 0 E J 5 £ ¢ 7 \ ¥ \ : . � § g 3 i E § 3 3 \ 3 ' E E E m /3 / 7 �)f 22 § ° CD { f3 CL \ e e e ) CD) ) ) 7 _w _ �> _P ) ) ) 2 k z f 3 2 E E E f - \ f 0 7 / / « \ \ R k - m 0 S } k § - ! ® J .. \ ' { n^�q $$; . gam}/// �{0rm PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 94y4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/30/2021 Reported: 07/16/2021 For: Comments: Sample Number Parameter Sample ID Result 210630-17-01 Ammonia UCCC-Inf 27.8 210630-17-01 BOD UCCC-Inf 283 210630-17-01 TSS UCCC-Inf 131.8 210630-17-02 Ammonia UCCC-Eff 0.22 210630-17-02 BOD UCCC-Eff <2 210630-17-02 Fecal Coliforms UCCC-Eff <1 210630-17-02 TSS UCCC-Eff <2.809 210630-17-03 Total Solids UCCC-RAS 5816 210630-17-03 Total Volatile Solids UCCC-RAS 4024 210630-17-04 Total Solids UCCC-DIG 705 23168 210630-17-04 Total Volatile Solids UCCC-DIG 705 14596 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 07/06/2021 CE/MD mg/L SM521OB-2011 07/01/2021 CE mg/L SM2540D-2011 07/01/2021 LE/CE mg/L SM4500NH3E-2011 07/06/2021 CE/MD mg/L SM521OB-2011 07/01/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/30/2021 WC mg/L SM2540D-2011 07/01/2021 LE/CE mg/L SM2540B-1997 07/01/2021 MD mg/L SM2540G-2011 07/01/2021 MD mg/L SM2540B-1997 07/01/2021 MD mg/L SM254OG-2011 07/01/2021 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210630-17-01 Temp on Arrival: 2.7 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210630-17-02 Temp on Arrival: 2.7 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210630-17-03 Temp on Arrival: 2.7 Parameter Schedule: Total Solids Received on Ice Sample Number 210630-17-04 Temp on Arrival: 2.7 Parameter Schedule: Total Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 n — V) 3 N = . d 3 . 9 lA 3 n n n n n n n n n n n n n n 0 n y s o> z" m m m z G m m m Z T Z Z T r; N ~ 3 v a 3 3 a N N T T m o O fb � T A R fl - - Tlito Sampler mina's g h - a q Er q y - on 3 - - Sample Begin Date $ of 3 S w w - N = w Semple Begin Time 4 n � � p 0 0 0 1 o Sample End Date a o a m T T tJ � Sample End Time _ N S ci — ? I I F -Z-" Date Sample wleded AlN0 3sn ANo1V? oevi Q g R y °' $ - J n C% E '- J z Z Z Z z I Z z Z 0 D 0 0 O 0 250 250 500 1000 1000 500 250 250 x x x x x x h1cinnated System (YIN) c m 0 q A o (Z'> 3 S _. u a iD � M v r m ample Type (See Below) `� onWiner Type (Sea below of Containers Ae Sae (od) DNE NO3 2SO4 aOH 4 a2S203 aB USE ONLY.-Indlala pH of wv.dS.mpl.(<2;>12) 30D5 105 UD $ FHO-PHOSPHATE PALS °3 (7 2 D IDNESS z OT C/) O HIDE & GREASE (HEM) AL COLIFORM M m 0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 C ; M Z a 9 d a a o l a m _ ',� r Samplerinitiels S y - r 0 a n 3 - 3 �o o _ Sampe Begin Dale F $ 0 c z z y N T Sample Begin Tune y+ 3 0 a o 0 0 0 0 8 ci Sample End Date o "s cci g Nm T \ \ n n Sample End Time A I f w DateS 'e Colleded AIN03sn kNoinceV1 x n z 0 T 0 C (n 0 0 O M m n 0 0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/03/2021 Reported: 06/11 /2021 For: Comments: Sample Number Parameter Sample ID Result 210603-14-01 Ammonia UCCC-Inf 13.89 210603-14-01 BOD UCCC-Inf 264 210603-14-01 TSS UCCC-Inf 114 210603-14-02 Ammonia UCCC-Eff 0.67 210603-14-02 BOD UCCC-Eff 2.94 210603-14-02 Nitrate/Nitrite UCCC-Eff 44.9 210603-14-02 T. Phosphorous UCCC-Eff 5.8 210603-14-02 TKN UCCC-Eff 0.78 210603-14-02 TSS UCCC-Eff <2.688 210603-14-03 Total Solids UCCC-RAS 7140 210603-14-03 Total Volatile Solids UCCC-RAS 5112 210603-14-04 Total Solids UCCC-DIG 705 43588 210603-14-04 Total Volatile Solids UCCC-DIG 705 29180 210603-14-05 Fecal Coliforms UCCC- Eff ( 1.0 LAB) Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/08/2021 CE mg/L SM521OB-2011 06/04/2021 CE mg/L SM2540D-2011 06/04/2021 CE mg/L SM4500NH3E-2011 06/08/2021 CE mg/L SM521OB-2011 06/04/2021 CE mg/L SM450OF-2011 06/10/2021 CL mg/L SM450OPE-2011 06/11/2021 CL mg/L SM4500NorgB-2011 06/10/2021 CL mg/L SM2540D-2011 06/04/2021 CE mg/L SM2540B-1997 06/04/2021 MD mg/L SM254OG-2011 06/04/2021 MD mg/L SM2540B-1997 06/04/2021 MD mg/L SM2540G-2011 06/04/2021 MD MPN/100 ml IDEXX Colilert 18 MPN 06/03/2021 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 Condition of Receipt Sample Number 210603-14-01 Temp on Arrival: 3.2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210603-14-02 Temp on Arrival: 3.2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice pH on Arrival: <2 Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210603-14-03 Temp on Arrival: 3.2 Parameter Schedule: Total Solids Received on Ice Sample Number 210603-14-04 Temp on Arrival: 3.2 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 5 Parameter Schedule: Total Solids Received on Ice Sample Number 210603-14-05 Temp on Arrival: 3.2 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 5 C n a n C n C 0 C 0 C l7 a n a 0 C O a T v a 0 3 y 93 y n 00 n 0 n T n � T 0 cn A O 0 0 y O (7 m V V D T T T T T O y 3 a i Sampler Initials m o o g m 4 G N CI vN r Sample Begm Date O Z T 2 T W w A ^ &G a mi Sample Begin Time C ` 4 o Sample End Date o m m a a n O w Sample End Time n Date Sampecdleaed 4ol AlNO3Sf1Ai111»-U N = ca N < D o o —1 CA C. 111 5 r y r r m Z N O a J. y yOy N < r PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 5 9 a 0 9 a 0 ƒ ( I ƒ ] 2 } (/ 3 0:± E 2 0 2 3 S g « R E o q/ o[ f \4 $} »£ = R ■ a o (a s f = & 5 E E = E 7 } a / / §. 3 3 3) a z 3 ] \ ] . - 2 E 7 J E E5 ( ( . � o C- 0 at 3§ 4{ i % { ` N \ } / 3 7 m m , , _ . P. ) j ] ] e 2 �{ } E E E 2 « « E E E - /\Ukj / / ( z o I Q @ ) 2 [ \> § ] \ k k k m Q a E f ; / 0 3 § # \ /nk\�>j A=�-arn ± A . PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 95y5 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/07/2021 Reported: 06/17/2021 For: Comments: Sample Number Parameter Sample ID Result 210607-15-01 Ammonia Nitrogen UCCC-Inf 25.06 210607-15-01 BOD UCCC-Inf 216 210607-15-01 TSS UCCC-Inf 215 210607-15-02 Ammonia Nitrogen UCCC-Eff <0.5 210607-15-02 BOD UCCC-Eff <2 210607-15-02 TSS UCCC-Eff <2.703 210607-15-03 Fecal Coliforms UCCC-Eff (LAB) <1 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3C-2011 06/15/2021 CE mg/L SM521OB-2011 06/07/2021 CE mg/L SM2540D-2011 06/11/2021 CE mg/L SM4500NH3C-2011 06/15/2021 CE mg/L SM521OB-2011 06/07/2021 CE mg/L SM2540D-2011 06/11/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/07/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210607-15-01 Temp on Arrival: 3.0 pH on Arrival: <2 Parameter Schedule: Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210607-15-02 Temp on Arrival: 3.0 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Sample Number 210607-15-03 Temp on Arrival: 3.0 Received on Ice Chemicals in containers, lab Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 0 c C.) c n c A N non x v m m in m y rtl � - `� Sampler Indials a3 S ag o- ple Begin jDale-.\ Sample Beget n c Z J O O ZZ `C; 7O S O _ Sample End Date m m Sample End Time t a v. AINO 3sn wlnoev1 MINN ■■■....v..... M ■■■..00..o.o WNW ■■v00■000 = ■■■.. I ...■■■©©..©© ■■■■■■■■■■■■'�■■ ■■■■■©■■.©... , ■■■■■■■■■■■■�= ON NM ■■■■■■■■■■■■ r (\\ '. .....NN ....... : • r ■■■■■■■■■■■■ rr - EN ■■■■■■■■■■.■� ■■■■■■©■■■©■� ■■■■■■■■■■■■� ■■■■■■■■■■■■� ON M OWN■■ TOTAL PHOSPHORUS z M RTHO-PHOSPHATE 3 .�\\ v v n D T METALS G RDNESS YANIDE IL & GREASE (HEM) C v ECAL COLIFORM M C) m � O � S s oK - rA PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 _I / 3 CD \ I7I O CD m CD Z CD CD �% ' CD 0 C N m3 3mCDOm O O O QM Q Cmi 7 N O 7 CCDD O (CD C. O. CO 7 N Q CO 7 U) A QQ (a CD a Q CA m a CD C N N 21 3 a 3 3 Q C a a a 3 3 3 3 v a � Q m sy iv [J m m m m c� �3 a <� m� T. m �m r �o9 �9 �� �Q a CD Q 0 N 3 C(D CD CD y Grab p. - £ 3 3 3 3 a m m m m w c a - y Z 0 3 I O 3 0 O O 3CL Bi Q ;3a CQ ED O CD iw*z O CD m n 1 CD b� \ J CO J d N N ]O PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/08/2021 Reported: 06/17/2021 For: Comments: Sample Number Parameter Sample ID Result 210608-24-01 Ammonia Nitrogen UCCC-Inf 26.10 210608-24-01 BOD UCCC-Inf 340 210608-24-01 TSS UCCC-Inf 311.1 210608-24-02 Ammonia Nitrogen UCCC-Eff <0.5 210608-24-02 BOD UCCC-Eff <2 210608-24-02 TSS UCCC-Eff <2.825 210608-24-03 Fecal Coliforms UCCC-Eff(LAB) <1 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3C-2011 06/15/2021 CE mg/L SM521OB-2011 06/09/2021 CE mg/L SM2540D-2011 06/11/2021 CE mg/L SM4500NH3C-2011 06/15/2021 CE mg/L SM521OB-2011 06/09/2021 CE mg/L SM2540D-2011 06/11/2021 CE MPN/100 ml IDEXX Colilert 18 MPN 06/08/2021 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210608-24-01 Temp on Arrival: <2 pH on Arrival: <2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210608-24-02 Temp on Arrival: <2 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Received on Ice Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Sample Number 210608-24-03 Temp on Arrival: <2 Received on Ice Chemicals in containers, lab Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 E I EI I E 3- a ' - - - � - , q ) � .. ! . _ ; _4 _. $ § E � \ x �.� m{ = � % ¥ / 7 _@� _ 6 S ® ) Sample End Date �e / e / amp .Bari. ^ 11 | _+wa_ t nKen22A2/ � 4 ) \ PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 93y4 e a o a a $ CD CD� A..:3 n)/ \\ 2 CL ƒ\ o 2 2 3 7 2 CD2 D 0 o@ R E \ } C £ \ � 5 2 5 ■ i a S \ / � \ � \ 0 ? / 2 E �2E U, ID f� / ID t>e,) \3 i \ N � 3 / ( / / ! ; m CD m _ # � � • � . }! 3 j § su 3 -n k CD \ 2 ■ ! & z o I 4 cn 93 0 ^ g / ) 2 0 \ f \ . y }cr/ (D } \ 3 \ cr \ 3 /P.2 § ;dA'®f PO Bo 2289 Statesville, NE 28687. 70 / 72 4697 94y4 Analytical Results Crooked Creek WWTP-Union County Government 500 N. Main Street Monroe, NC 28112 Receive Date: 06/09/2021 Reported: 07/16/2021 For: Crooked Creek WRF Comments: Sample Number Parameter Sample ID Result 210609-17-01 Ammonia UCCC-Inf 25.54 210609-17-01 BOD UCCC-Inf 290 210609-17-01 TSS UCCC-Inf 185.3 210609-17-02 Ammonia UCCC-Eff 0.11 210609-17-02 BOD UCCC-Eff <2 210609-17-02 TSS UCCC-Eff 3.191 210609-17-03 Total Solids UCCC-RAS 6876 210609-17-03 Total Volatile Solids UCCC-RAS 6684 210609-17-04 Total Solids UCCC-DIG 705 34638 210609-17-04 Total Volatile Solids UCCC-DIG 705 23936 210609-17-05 Fecal Coliforms UCCC-Eff (lab) <1 Respectfully submitted, Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 STATESVILLE ANALYTICAL Unit Method Analyzed Analyst mg/L SM4500NH3E-2011 06/15/2021 CE mg/L SM521OB-2011 06/10/2021 CE mg/L SM2540D-2011 06/11/2021 CE mg/L SM4500NH3E-2011 06/15/2021 CE mg/L SM521OB-2011 06/10/2021 CE mg/L SM2540D-2011 06/11/2021 CE mg/L SM2540B-1997 06/11/2021 WC mg/L SM2540G-2011 06/11/2021 WC mg/L SM2540B-1997 06/11/2021 WC mg/L SM2540G-2011 06/14/2021 WC MPN/100 ml IDEXX Colilert 18 MPN 06/09/2021 CL PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 210609-17-01 Temp on Arrival: 2.6 pH on Arrival: <2 Parameter Schedule: TSS Received on Ice Parameter Schedule: BOD Received on Ice Parameter Schedule: Sulfuric Acid Received on Ice Chemicals in containers, lab Sample Number 210609-17-02 Temp on Arrival: 2.6 pH on Arrival: <2 Parameter Schedule: BOD Received on Ice Parameter Schedule: TSS Parameter Schedule: Sulfuric Acid Sample Number 210609-17-03 Temp on Arrival: 2.6 Received on Ice Received on Ice Chemicals in containers, lab Parameter Schedule: Total Solids Received on Ice Sample Number 210609-17-04 Temp on Arrival: 2.6 Parameter Schedule: Total Solids Received on Ice Sample Number 210609-17-05 Temp on Arrival: 2.6 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 n N 3 N 'o N d 3 N 3 N 3 0 n 0 n A n A c7 CC] n 00 n c7 00➢ D (") 0 n rn z 2 T T 2 2 2 m N N a V v a N0 N T T T T T T m Go g M A n $ i \ Sampler Initials m 3 < r N Sample Begin Dale n =� o — � c -'j J Sample Begin Time a o UI R m 0 0 o r, N � ample End Date o z � z z z N T Q 0 m fic� Sample End Time v I a Date Sample Wlecled AIN0 3sn 48oiv i08d1 o 1 c> ~ Tme Sample Collected z z I Z Z z I z z z Chlonnated System(y/N) 0 0 1 D O O O O fJ ample Type (See Bel w) i v v T v ,nl,,,, Type (See Belo of Containers 250 250 500 1000 1000 1x000 00 250 250 ttleSize (m) m ' S x x x xx ONE NO3 4m a X 2qf ■■■■■■■■■.■■ • .- . :::ACC:©:::©:::• ............M N M CO) 1 0 m i cn An $ r r m 5 > dmz 0 D 5. a 0 Z A > N < D r V Ilia PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 —I i/ / m m m mNCDON 3 cn 3 Cy 0 O0 D aO l m 3 (D m CD m 3 m 07 N ro 3 CDCCDD 13 0 = N 0 m C m C1 CQ w 2 Co 0 CL ni C1 Oi O� - m In cp v m a CD a m d .. Q o 3 3 d 3 3 N 3 3 I1 o 0 o v o w w w w m CD m m t1`\ ` I zi m 3 v m m a ^' a 3 `< v a C C � 0 D Q m 0 y Z mCD r n p, c ^. 6 1 ' 0 N 3 m m m m — NJy Grab (� s m 3 3 3 3 > < 3 3 3 3 3 m m m m CD � c 0> - m m m 3 m Z / _ cn 0 0 0 w w - O y 7 Q o „ a O O Q CD 3 �' CL v o m m a. K n m a N FR < .. w i A W J y r N PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4