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HomeMy WebLinkAboutWQ0004972_Monitoring - 09-2021_20211101Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * September Report Information WQ0004972 Forest Lakes Preserve ELS Year:* 2021 Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR Forest Lakes_September.pdf 1.62MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* Jessica.Mize@pacelabs.com Name of Submitter: * Jessica Mize Signature: jwd rA lip Date of submittal: 11/1/2021 This will be filled in automatically Initial Review Reviewer: Saunders, Erickson G Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Accepted Date: 11 /10/2021 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W 0004972 MONTH: September YEAR: 2021 AME: Forest Lakes Preserve ELS COUNTY: Davie -. I I •. ■ flMMIM t Da�ly Rate ONE 0 EM N ffimm INN l� �--��1����®®��i�i1®�■li�1Fa��11®■S�il�� MO M NM OM HEM ®IM=M ME ME EM HEM WM MEMM ME ME ME ME HEM mom==® ■�®®�®®®®®®®BEM HEM MW * Flows Estimated 9118 - 9130/21 (flow meter inoperable) Operator In Responsible Charge (ORQ: Glenn Price Check Box if ORC Has Changed: Certified Laboratories (1): Pace Analytical Serivices Grade: 11 Phone: 336-99 -2841 ORC Certification Number: 987931/20771 Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, 1 certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (512003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant ,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Flows estimated 9/18/21 - 9/30/21 flow meter inoperable "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Pennitee)* �'''r Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago. I1 60606 (Pennittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31 /21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN(Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W 004972 MONTH: September YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Loading (inches) _ (Volume Applied (gallons) x 0.1336 (wbie feetlgailony x 12 (inchesftot))! [Area Sprayed (acres) x 43.560 (square 1eeVaae) or = [Volume Applied (gallons) I [Area Sprayed (acres) x 27.152 (gallonslacreAnoh). Maximum Hourly Loading (inches) = Daily Loading (inCYies) i [Time irrigated (minutes)160 (minutewbouol Monthly Loading (inches) =Sum Di Daily Loading (inches) 12 Month Floating Total (inches) = Sum Df lhis month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (inchestmonth) / Number of days in the month (clays/month )I x 7 (dayslwesk) bid Irrigation Occur At This i Did lr�galicin Occur On This Field: No El Did lrffiigat!Dn Occur On This Fieid: YOE] NoJ2 i Fiald Number .14 jK93 2 13111• *Weather Cados: C�i PC -partly c[Gu4y, Cl-etaudy, R-rain, Sn-snow, SlAect Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Chcek Box if ORC Has Clanged: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center RALEIGH, NC 27699-1617 (SIGNATURE OF OPERATOR IN RESPONSIBLE CHE By this signature, I certify that this report is accurate and complete to the best of my knowledge. DENR Form NDAR-1 (512003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. C� 4. All buffer zones as specified in the permit were maintained during each application. `fir 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the C� limit(s) specified in the permit. If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Baron Neal MCDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized_Aent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago,11 60606 (Permittee Address) Field Services Director (Pace AnalZical Services) (Position or Title) 3/31/2021 (Permit Exp. Date) * If signed by other than the Penmittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). aceAnalytical www.pecolabs.com October 07, 2021 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lakes Pace Project No.: 92563393 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-09B1 Enclosed are the analytical results for sample(s) received by the laboratory on September 27, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNIlNELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie. knott@pacelabs.com 704-977-0981 Project Manager Enclosures IN - REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, B Page 1 of 16 aceAnalytical wrna7eeeEita.eam Project: Forest Lakes Pace Project No.: 92563393 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, INC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinkina Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North r:arnlinn r1rinkinn Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VrginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Page 2 of 16 aceAnalyiical wMnvpspis6s.eorn SAMPLE ANALYTE COUNT Project: Forest Lakes Pace Project No.: 92563393 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92563393001 Effluent SM 254OD-2011 AED 1 PASI-E EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 521OB-2011 DAW 1 PASI-E Colilert-18 AMI 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 350.1 Rev 2.0 1993 KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A PASI-A = Pace Analytical Services - Asheville PAS I-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 16 aceAnalytical. anr�patxltabt cote ANALYTICAL RESULTS Project: Forest Lakes Pace Project No.: 92563393 Pace Analytical Services, LLC 1377 South Park Drive Kernersviile, NC 27284 (704)977-0981 Sample: Effluent lab ID: 92563393001 Collected: 09/27/21 10:36 Received: 09/27/21 11:30 Matrix: water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 25400 Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids 11.5 mg/L 3.2 1 09/29/21 12:24 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Seances - Eden Nitrogen, Nitrate ND mg/L 0.040 1 09/27/21 17:05 14797-55-8 5210E BOD, 5 day EDN Analytical Method: SM 521OB-2011 Preparation Method: SM 521 OB-2011 Pace Analytical Services - Eden BOD, 5 day 39.2 mg/L 2.0 1 09/28/21 09:16 10/03/21 12:46 B1 Colllert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 09127/21 15:12 09/28/21 09:41 El Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 77.7 mg/L 0.62 1 10/07/21 17:33 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.01993 Pace Analytical Services -Asheville Nitrogen, Ammonia 68.5 mg/L 1.0 10 10/07/2111:31 766441-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 77.7 mg/L 5.0 10 10/05/21 20:50 10/06/21 05:28 7727-37-9 353.2 Nitrogen, NO2IN03 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 0.043 mg/L 0.040 1 10/06/21 13:53 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993 Pace Analytical Services -Asheville Phosphorus 10.7 mg/L 0.25 5 10/01/2117:33 1010112123:07 7723-14-0 Date: 10/07/2021 05:36 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 4 of 16 IceAnali(tical ttnr wtr prittlitizom Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 649848 QC Batch Method: SM 254OD-2011 Associated Lab Samples: 92563393001 QUALITY CONTROL DATA Analysis Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden METHOD BLANK: 3408250 Matrix: Water Associated Lab Samples: 92563393001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 09/29/21 12:19 Paco Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3408251 Spike LCS LCS ale Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 3408252 92563205001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 107 112 4 SAMPLE DUPLICATE: 3408253 92563413001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 116 126 8 Results presented on this page are In the units Indicated by the Vnits' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in foil, Date: 10/0712021 05:36 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 aceAnalytical 1tfliYrp.0010 QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 649555 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92563393001 METHOD BLANK: 3406693 Matrix: Water Associated Lab Samples: 92563393001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L NO 0.040 09/27/21 16:26 Pace Analytical Services, LLC 1377 South Park Drive Kernersvilie, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3406694 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.4 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3406695 3406696 MS MSD 92563399001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 1.4 1.5 1.5 2.8 2.6 92 91 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/07/2021 05:36 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 (�Ia'neAnab&cal Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 649608 QC Batch Method: SM 521OB-2011 Associated Lab Samples: 92563393001 METHOD BLANK: 3406879 Associated Lab Samples., 92563393001 Parameter BOD, 5 day QUALITY CONTROL DATA Analysis Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg1L ND 2.0 10103/2112:24 Pace Analytical Services, LLC 1377 South Park Drive Kentersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3406880 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 176 89 84.6-115.4 SAMPLE DUPLICATE: 3406882 92563442001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg1L 162 152 7 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/07/2021 05:36 PM without the written consent of Pace Analytical Services, I.I.C. Page 7 of 16 aeeAnaiytical t�rtrtlttaltb>teom QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 649549 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92563393001 SAMPLE DUPLICATE: 3406668 Parameter Fecal Coliforms 92563445001 Dup Units Result Result RPD Qualifiers MPN/100mL 17.3 15.8 9 Pace Analytical Services, Lt.0 1377 South Park Drive Kemorsville, NC 27284 (704)977-0981 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This retort shall not be reproduced, except in full, Date: 10/0712021 05:36 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 16 (�Ia'neAnal)dical Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 651320 QC Batch Method: EPA 350.1 Rev 2.01993 Associated Lab Samples: 92563393001 QUALITY CONTROL DATA Analysis Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville METHOD BLANK: 3415766 Matrix: Water Associated Lab Samples: 92563393001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 10/07/21 10:39 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3415767 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.9 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3415768 3415769 MS MSD 92564080001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 11.0 5 5 15.7 15.7 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3415770 3415771 MS MSD 92564086002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 41.8 5 5 46.6 47A 97 113 90-110 2 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit la presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/0712021 05:36 PM without the written consent of Pace Analytical Services, I.I.C. Page 9 of 16 C6Ai?d1J/ITCd�� rrtrM�patiNNrtDsesro QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 650926 Analysis Method: EPA 351.2 Rev 2.01993 QC Batch Method: EPA 351.2 Rev 2.01993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92563393001 METHOD BLANK: 3413579 Matrix: Water Associated Lab Samples: 92563393001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/06/21 04:25 LABORATORY CONTROL SAMPLE: 3413580 Parameter Nitrogen, Kjeldahl, Total Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers mg/L 10 10.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3413581 3413582 MS MSD 92563915005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 11.0 10.7 106 103 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presentod to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/07/2021 05:36 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 ceAnalytical to ttnrts�ul�bt.eaa QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92563393 QC Batch: 651055 Analysis Method: EPA 353.2 Rev 2.0 1993 OC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92563393001 METHOD BLANK: 3414354 Matrix: Water Associated Lab Samples: 92563393001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 10/06/21 13:28 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3414355 Spike LCS LCS % Rec Parameter Units Conc. Result %e Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3414356 3414357 MS MSD 92563993001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Nitrogen, NO2 plus NO3 mg/L NO 2.5 2.5 2.3 2.3 93 93 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3414358 MS MSD 92563993002 Spike Spike Parameter Units Result Conc. Conc. Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 3414359 MS MSD MS MSD % Rec Result Result % Rec % Rec Limits RPD Oval 2.3 2.3 93 92 90-110 1 Results presented an this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/0712021 05:36 PM without the written consent of Pace Analytical Services. LLC. Page 11 of 16 ceAnalytical www.pacdabs.com QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92563393 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie. NC 27284 (704)977-0981 QC Batch: 650327 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.01993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92563393001 METHOD BLANK: 3410866 Matrix: Water Associated Lab Samples: 92563393001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 10101/2122:22 LABORATORY CONTROL SAMPLE: 3410867 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3410868 3410869 MS MSD 92561769001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.2 2.5 2.5 3.7 3.7 102 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3410870 3410871 MS MSD 92562371001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cono- Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L NO 2.5 2.5 2.5 2.5 102 102 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/07/2021 05:36 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 Pace Analytical Services, LLC / m 1377 South Park Drive aCB�lk3/ICal Kemersville, NC 27284 1rwM.P"datimm (704)977-0981 QUALIFIERS Project: Forest Lakes Pace Project No.: 92563393 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1.2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS B1 Less than 1.0 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated for the dilution using the least amount of sample. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Date: 10/07/2021 05:36 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 16 ticeAnalytical MMw.Otpl�tq.t9[o QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lakes Pace Project No.: 92563393 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92563393001 Effluent SM 254OD-2011 649848 92563393001 Effluent EPA 353.2 Rev 2.01993 649555 92563393001 Effluent SM 521OB-2011 649608 SM 521OB-2011 649800 92563393001 Effluent Colilert-18 649549 Colilert-18 649550 92563393001 Effluent TKN+NO3+NO2 651544 Calculation 92563393001 Effluent EPA 350.1 Rev 2.01993 651320 92563393001 Effluent EPA 351.2 Rev 2.01993 650926 EPA 351.2 Rev 2.0 1993 651038 92563393001 Effluent EPA 353.2 Rev 2.0 1993 651055 92563393001 Effluent EPA 365.1 Rev 2.0 1993 650327 EPA 365.1 Rev 2.0 1993 650480 Date: 10/07/2021 05:36 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. LLC. Page 14 of 16 CHAIN -OF -CUSTODY Analytical Request Document f LAB USE ONLY- AfftxWoiicorder/Loginlai wo : 92563393 MIX Log -In $CPAITr?r'% u r - Chain -of -Custody Is a LEGAL DOCUMENT- Complete all relevent fields ALL SHADED AREAS Company: Forest lakes Billing information: Container Preservative T e •` 92563393 Address. .. . . � 2 g. _ Report To: Email To: •• Preservative Types: (1) nitric add, (2) sulfuric add, (3) hydrochloric add, (4) sadium hydro3dde,15) zinc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (C) ammonium hydroxide, (0) TSP, (U) Unpreserved, (0) Other (A) ascorbic add (a) ammonium sulfate, Copy To: Site Collection Info/Address: Analyses Lab profile ne: Customer Project Name/Number: State: County/City: Time Zone Collected: fmb saagile Race pt Cheekl iat t [ IPTI IMT( )CT [ )ET Custody-Soals Present/Intact Y N NA Custody signatures Present Y N NA Phone: Site/Facility ID u: Compliance Monitoring? EriJafi: [ Yes [ ]No Collector Signature Present Y N NA Battles Intact Y N NA Correct Bottlea Y N NA Collected B t): Purchase Order #: DW PWS ID #: Quote#' DWLocationCode: Z sufficient Volume Y H NA Samples Received on Ica Y N HA VOA Headspace Acceptable Y N NA Collette y ( gnature . Turnaround Date Required: Immediately ac on ce: [ IYes [ ]No N USDA'Requlated Soils Y N NA saiaples in Holding Time Y N NA Feld Filtered (if applicable): Ecamry#e Disposal: n. Rcsidunl Chlorine Present Y N NA ( ] Dispose as apprapr+a._ ; Return ( ] Same Day ( ] Nex: Day [ ] Yes [ ] No t+g Cl _stripa r I I Archive._ [ ] 2 Day [ ] 3 DaY [ ] 4 DaY [ 15 Day p !— ., sample - sample PH Acceptable- - YN NA pR Strips: l I Hold: (Expedite Charges Apply) r.j sulfide Present Y N NA bend Acetate SLrips r ' roa:r.c Cokta:• (Insc't #M Matri,')ox lJ.:6,w): Drinking Water (Old'1, Grot nd Water (GW), Wastewater (WW), t rro::i (Pi, 5+:11; 5.: ti.l : nl t0:.t, y.';i , nWP;, Air (AR), Ttssu (,). H,cwssay (B), Vapor (tit), Of -her (OT] '... U? r O ? ) J AII use ONLY ! _... —,-- --, �r nrp i oh : lies (ors # Of cn F- Z t J,ab Sample a ! Ct=nunto: # 0..':triY I C4mpoik, End R• l rdl, J_... 111 4lf� St3rt�.--' Cl Ctns { , ia"/j , t j - Ac '. Time Dat � T,ma i _ 3 V i� �t? i�Q3 i _... [ _ i4 � m !Z X.� ut /� Ehou4rs� Customer Remarks / Special Conditions / Possible Hazards: Type of ice Used: Wet Blue Dry None SHORT HOLDS PRESENT102 N N/A Lab Sample Temperature Info: Temp Blank d: Y N NA Packing Material Used. ' Lab Tracking qc �``y► Therm IDp Cooler l Temp•Upon Recef C Cooler 1 Therm Corr. Factor oc pies received via: Radchem sample(s) screened (sSOD cpmj:• _Y " N NA UPS Client Courer at Cooler 1Corrected Temp: oC Comments: Relinquished by/Compan Signature) Dat4'TIm ( Recely d by/Co any: (Signa re) Date/Time: 1 1� MTJL Table N: ro / Template: Reli uished by/Company- (Signature) Date/Time: Rece ve by/ ompany: (Signature)Acctnum: Date/Time: Trip Blank Received: V N NA _ v' Prelogin: ply: HCL McOH TSP Other Reli �uished by/Company: (Signature) Date/nme: Received by/Company: (Signature) Date/Time: __ _ Non Conformance(s)�Page: _ _ _PB: _��.YES � NO `_Vv of: