Landfill Site 50-02

North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary
lulu1 t 1 UI. 1
August 19, 1987
Ronald H. Levine, M.D., M.P.H.
State Health Director
TO: Perry Nelson, Chief Ground -Water Section
Division of Environmental Management
FR(ft Paula Byrd, Solid Waste Unit
Solid & Hazardous Waste Management Branch
SUBJECT: Analytical results from 'no smn+� sotihtyliart fi`11j Solid Waste
Facility #50-02. [7 11 s boao s �YQ
Per the MQA dated June 4, 1987 between IMCD and EM, enclosed are copies
of recent analytical results from the above referenced facility that may
indicate contravention or potential contravention of ground -water standards.
If any additional information is required please advise.
PDB/mj/6369pg5
cc: Wayne Hooper Jackson Co. Manager
Jim Patterson
Julian Foscue
Michael Babuin �\ 9
�I (No
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LOCArroN ON C3ACK 7

N. C. Department of Human Resources State Laboratory of Public Health
Division of Health Services SAMPLE ANALYSES REQUEST P. O. Box 28047
306 N. Wilmington Street
I Raleigh, 27611
Site Number00Co.
O 0(9 0 O 0000 9- Field Sample Number
Name of Site Jac kso n l LF Site Location 00 I J I I r 5 h0 f ci Pd.
Collected By B� rd i I U, 1 1 ID# 20 , 52 Date Collected / as i 7 Time S
Type of Sample:
Environmental Concentrate
Groundwater (1) Solid (5) '' i.,".'i�F}�y '2'? i
'.'..tH
Surface Water (2) Liquid (6)
Soil (3) Sludge (7) SEP � 198T
Other (4) Other (8) f ii�' ' WbW �-;;n�
iN0R(;ANi(:('.HRA.11C'rRV 'itchil,IJIILs
Extractables
Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
— Arsenic
—Barium
—Cadmium
—Chromium
— Lead
—Mercury
—Selenium?
—Silver
=
—.pT.4tc fi: �'N `
_Barium
_'= 'Cadmium cA,
Chloride ,� r�,t
'
Chromium `
,Copper �
oride It
— ,.�'nf;JOUS�Ps�,
_ Silver
—Sulfates
—Zinc
—Ph
—Conductivity
—TDS
r+ g 6® E2 3
U f fv I
— Manganese
—
—
—Mercury
— Nitrate .
—Selenium {e—
lc
c.�e
--- •D,.f' H--a
Abb `RnoLn�al flfficfl
—
—
�.
ORGANIC CHEMISTRY
Parameter Results mg/1
iP&T:GC/MS
Acid:B/N Ext.
— TOX
Parameter Results mg/1
— EDB
—PCB's
— Petroleum
Parameter Results mg/I
— Methoxychlor
—Toxaphene
— 2,4-D
—
— Endrin
— 2A5-TP (silvex)
—
— Lindane
MH;itOBIOLOGy RADIOCHEMISTRY
Parameter
Parameter Results PCi/1
— (MF) Coliform Colonies/100mis
—(MPN) Coliform Colonies/100mis
— Gross Alpha
—Gross Beta
Date Receivec
Date Extracte
Reported By
DHS 3191 (Revi,
Solid and Hazardous Waste (R,. ie , 7/A7)
Date Reported — _ 7- . k "rf 7
Date Analyzed BT f-2 -J 7 644 r(n -�'J 77 t
rJ
Lab Number
-17-470/Z2-2-' 76/zz3-

N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: _Generator _Transporter _Treatment Facility
_Storage Facility _Disposal Facility ✓ Landfill
Other:
Company's Name �G n ry �� r, AC}} Telephone {
Address
Collector's Name Teleph n
signature' Kai
Dale Sampled-Ti
rype of Process Generating Waste
Field Information
'icid Sample No. CID to
;hairs of Possession:
signature 2s 4 a3
title inclusive—
ncl sive dates
signature title inclusive dates
Signature title
inclusive dates
esults reported
signature title
date
istructions: Complete all applicable information including signatures, and submit
with analvsis request forms. I

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST., RALEIGH. N.C. 21611
ORGAN C CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID
EXTRACTABLES
LAB NO
O AZ.
O
FIELD M
L/
Z
COMPOUND
N-nitrosodimeth lamine
TYPE
UNITS
09V1 /k
/ /k
/1 /k4/1/k
/1 /k
/1 /k
bis 2-chloroeth 1 ether
2-chlorophenol
henol
1 3-dichlor nzene
1 4-dichlorobenzene
1 2-dichlorobenzene
bis 2-chloroi 1 ether
hexachloroethane
N--nitroso-di-n lamine
nitrobenzene
isophorone
2--nit henol
2 4-dimeth 1 phenol
bis 2-chloroethox methane
2 4-dichlo henol
1 2 4-trichlorobenzene
naphthalene
hexachlorobutadiene
R;'rr,, _r'-
4-chloro-nn-cresol
hexachlorocycl tadiene
2 4 6-trichlo henol
SAP
t
2-chloronaphthalene
acenaphthylene
M
t„
dimeth 1 Phthalate
1
2 6-dinitrotoluene
acenaphthene
14,z
2 4--dinit henol
I(
_
2 4-dinitrotoluene
4--nit 1
10
-0
ryy
V�
Ego
fluorene .
O
t
inoo
4-chlorcPhenylphenylether
D
diethyl Phthalate
Wun Wpte
$ecd0n
4 6-dinitro-o-cresol
y,
�gpgi
di hen lamine
5
k
azobenzene
4-bruwPhenylphenylether .
/ a
hexachlorobenzene
/a
Pentachlorophenol
henanthrene
anthracene
dibut 1 Phthalate
fIuoranthene
rnDL
J - Estimated value. U�y/�
K - Actual value is known to be Mess than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but not detected. The number
NA - Not analyzed.
1/ - Tentative identification.
g/ - On NRDC List of Priority Pollutants.
is the Minimum Detection Limit.
N.C. Divi.6.ion o6 Heaeth Se uiae6
DHS 3068-0 (4186 Laboaatohy)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON. ST.. RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID
EXTRACTABLES
LAB NO
Z
D/
FIELD #
COMPOUND
TYPE
/
UNITS
/1 /k
/1 /k
/1 /k
/1 /k
/1 /k
/1 /k
rene
p
benzidine
TP
butyl benz 1 phthalate
benz a anthracene
0
chrysene
3 3-dichlorobenzidine
bis 2-eth lhex 1 hthalate
a
di-n-oct 1 phthalate
e
i
benzo b f1uoran thene
benzo k fluoranthene
benzo(a)pyrene
indeno(1 2 3-cd rene
dibenzo a h anthracene
benzo h i lene
aniline
benzoic acid
S�
benzyl alcohol
4-chloroan i 1 i ne
dibenzofuran
2-meth 1 hthalene
2-meth 1 henol
4-meth 1 henol
2-nitroaniline
2
3-nitroaniline
4-nitroaniline
n
2 4 5-trichlo henol
S
Af
C
FIG
--RAI
FA ) Vo U
4 V
1 {
191itl
WL
_
C
J - Estimated value. / W -
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but not detected. The number is the Minimum Detection Limit.=7'-J�y
NA - Not analyzed. _
1/ - Tentative identification.
R/ - On NROC List of Priority Pollutants.
N.C. D.iv.i.a.ion ob Heaf-th. Sehvicu
DHS 3068-0 (4186 Labaxatoty)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST., RALEIGH. N.C. 27611
ORGANIC CHEMICAL ANALYSIS
PORGEABLE COMPOl1NDS
LAB NO
70 P-3
FIELD 0
COMPOUND
TYPE
1
l
UNITS
/1 /k
/1 /k
/1 /k
/1 ljglkq
PVT /k
/1 /k
chloromethane
o
bronomethane
/ O
dichlorodifluora ethane
2d
vinyl chloride
v
chlorcethane
/
met ,lene ch or.t
trichlorofluoranethane
�2p
ethene 1 l-dichloro
S
ethane 1 l-dichloro-
1 2-trans-dichloroethene
chloroform
ethane 1 2-dichloro-
ethane 1 1 1-trichloro-
cartantetrachloride
branodichloronethane
Propane.1 2-dichloro-
1 3-trans-dichlo
trichlorneth lene
chlorodibromarethane
benzene -
ethane 1 1 2-trichloro-
1 3-"cis-dichla
2-chloroeth 1 vinyl ether
J a
I'i`r, •tom
y
t
branoform
S
ethane 1 1 2 2-tetrachloro-
ethenetetrachloro-
!
S
toluene
chlorobenzene
ftnI1141
NIP" L."
eth lbenzene
acetone
o
l L
2-butanone
carbondisulfide
2-hexanone
o
s
4-meth 1-2 ntanone
styrene
'JIM
vinyl acetate
/c
• v
x lens (hmtal
pmutxlY
11T
U
J
- Estimated value.
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but not detected. The number is the Minimum Detection Limit.
NA - Not analyzed.
l/ - Tentative identification"
2 - On HROC 5tst of Priority Pollutants.
N.C. Division of Health Services
DHS 3068-0 (4/86 Laboratory)

i
N. C. Department of Human Resources
Division of Health Services
ALYSES REQUEST
State Laboratory of Public. Health
P. O. Box 28047
306 K Wilmington Street
Raleigh 27611
Site Number 0 0 0 0 0 0 O1 ' 2 ;,_®r J / 1r//
"" ` " i �t ` U Field Sample Numberh t0f o1 (`1 / n
Name of Site Ja C KSun iO�i �+ r Site Location�J�4 �I i YX71 0 Kc�
a
Collected By _Iu r J I f n i r I r Date Collected — a Time ! 1 ' 30
Type of Sample:
Environmental
—L' Groundwater (1)
;Surfa«'Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
iUr'1D!_ A UTl� nvca arc .-., v
Comments
SECTION
Extractables
Total 11pLEIGH.
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
— Arsenic
/L_ Arsenic e O , o
Silver 0'
—Barium
Ekr NOW
L/ Sulfates 5
—Cadmium,
✓ Cadmium � �O- do 5`
� Zinc fo �_6-
- Chromium
Chloride
Ph 2-
-Lead
Chromium o' 01
_�:L
Conductivity
— Mercury
✓ Copper f(kt>
TDS
_Selenium
_!L Fluoride
_TOC
MAO
t—
Lead_
�/
''JJ
_
- -
z •:..
Mercury !D J06OR
G/sots
IQ1[wLrt..:r
—Seleolum <nr aoS'
'-
',:."..JVWiV. . ... - vl!',2u 1:1H[iANtl'a]HHMrSr'RV '_ - ,;...,gal::
Parameter - f Resultstng/V
Parameter -- Result mg/1'
Parameter. Results mg/1-.'.
— P&T:GC/MS
Acid.B/N Ext.
—TOX
—
— EDB
— PCB's
— Petroleum
_ Endrin
— Lindane
— Methoxychlor
— Tgxaphene
_ 2,4-D
— 2,4,5-TP (silvex)
—
Paramete3:ei.c..;,'
4
4V 1l\1
3 : • ,..
Parameter Results PCi/1"`
—(MF) Colifor &lomcs/lOOmis .
a Gross Alpha
—(MPN) Collform Colonies/100m1s
Beta
—Gross
_
JUN g 18 I
—_
Date Received
Date Extracted
Reported By
Date Reported 7/67
N
Date Analyzed
Lab Number rS4
DHS 3191 (Revised 7/85)
Solid and Hetardous Waste (Review 7/871

9
N. Department of Human Resources t• to Laboratory of Public Health
Division of Health Services SAMPLE ANALYSES RE Q EST _
.., P. O. \yBox 28047 90O ilT 306 N. Wilmington Street
RAleigh,276t1
Site Number 0 0 0 o 00 0 0 o a Field Sample Number
Name of Site Jae k sGYA Ov. . L r-7 Site Location
Collected By l Y d (Ail/ I IDN,561 7 Date Collected cZ - R
f Time
Type of Sample:
Environmental
—)L Groundwater (1)
Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
TWnR(:A VU' f'14FU7_,Zr'R V
Exttactables
-- - Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
—Arsenic
—Bami
cadmium
—Chromium
—�?d:.:
_lvleicuty
Selenium
";' Silveir
—
Arsenic 4. tl,.of
/ Barium G Ot /
Cadtriitun
Chloride [Nit/Frregc�
✓ Chromium ���/
Copper
L Ruori 6 1
Iron
fry-c"ZMHilgenese. rc++.. /✓`oti:�3f'J
1/ Silver
LSulfates
ZiricOt
/ Ph
✓ Conductivity. 36• w
TDS 02
TOC
r _-'r.C:•
Nitratex:
Selenium fO�00S � •,
4b.
V. _.':. :I -. 1s:3;dr.:.!:.R+P`:•rc.:n( IKIANII' CHFMEI-PRV,-:.raa.,..., :. d:, .}�..,.:: :..:.. ate:
Parariietec; - :.,..-.Rmuho mVl,"'::.-
--.Parameter s;' :..:. Results m�/1
Parameteri..Results mg/1
— P&T:GC/MS
—Acid:B/N Ext.
—TOX
—
— EDB
—PCB's
—Petroleum I{
— Endrin
— Lindane
—Methoxychlor
— Toxaphene
�4.,v E ""'9s
— 2,4,5-TP (silva
—
_
JdJ�'
LV IUM IKIt 31 A K i v D A TrI'1levrl e.o.nw
Parameter
--evyt•t
Parameter ' Roronaii{iilta P�i/1
— (MF), Coliform Colonies/ I0omIs
—(MPN) Coliform Colonies/100mis
_ Gross Alpha 1
—Gross Beta `
Date Received
Date Extracted
Reported By
Date Reported /
i
Date Analyzed
Lab Number ()()CS 65 AF 24 84
DHS 3191 (Revixd 7/85)
Solid and Hasardo. Waste (Review 7/87)

GROUND WATER DIVISION
OFFICE OF WATER AND AIR RESOURCES
DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES
RECORD OF GROUND WATER POLLUTION SOURCE
RECOR
TOWN:
LOCATION (SKETCH ON BACK:
OWNER(S) OF FACILITY OR INSTALLATION:
TYPE SOURCE: LAND FILL, LAGOON, ETC
CHARACTER AND QUANTITY OF POLLUTANTS:
DESCRIPTION OF FACI^LIITY (SKETCH ON BACK):
/
HYDROGEOLOGIC CONDITIONS AT SITE:Q
Oq 5 rn
a7 a`J D. PERMIT NO.
UNTY : �C1`c "C:5-n
POLLUTION CONFIRMED BY ANALYSIS? DATE ANALYST:
MONITORING FACILITIES INSTALLED:
SAMPLING SCHEDULE:
NEAREST STREAM:
NEAREST WATER SUPPLY WELL:
ANALYSES AND OTHER DATA AVAILABLE:
REMARKS: 3S7,-7ZO F131700
ISTANCE
ISTANCE
FORM GW-46

I
COL1tirc'i'i i