NCG030557_2021 DMR_20211006

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office -
Certificate of Coverage No. NCG03 030557
Person Collecting Samples: Tim Fernandez
Facility Name: Kidde Aerospace and Defense
Laboratory Name: Microbac Laboratories
Facility County: Wilson
Laboratory Cert. No.: 11
Discharge during this period:
Yes
C
No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?U Yes MNo
If so, which Tier (I, Il, or Ill)? 1
A copy of this DMR has been uploaded electronically via http5!//edocs.deg.nc.gov/Forms/SW-DMR UYes UNo
Date Uploaded: 10/6121
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
Outfall 1
Outfall2
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
C
C
N/A
Date Sample Collected MM/DD/YYYY
9/1/21
9/1121
46529
24-Hour Rainfall in inches
.3
.3
C0530
TSS in mg/L (100 or 50*)
50.5
18.9
pH in standard units (6.0-9.0 FW,
00400
6.8-8.5 SW)
6.5
7.0
Copper, total recoverable in mg/L
01119
(0.010 FW, 0.0058 SW)
0.0219
<0.00200
Lead, total recoverable in mg/ L
0105i
(0.075 FW, 0.22 5W)
0.031
<0.020
zinc, total recoverable in mg/ L (0.126
01094
FW, 0.095 SW)
0.269
0.009
Chemical Oxygen Demand (COD) in
00340
mg/L (120)
119
42.7
00552
Non -Polar Oil & Grease in mg/L (15)
<5.00
<5.00
* Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) 5W (Saltwater)
Notes (optional): r'ejbr jou 7,: —Jea /,;s
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee or
Authorized Individual
Date
Email Address Phone Number

�MICROBAC@
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Project Description
Stormwater Sample
For:
Mr. Tim Fernandez
Kidde Aerospace & Defence, Inc
4200 Airport Drive NW
Wilson, NC 27896
Administration
Brittany Smith
Tuesday, September 28, 2021
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions. comments, or require further
assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are
reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported
on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be
reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the
samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com
Page 1 of 10

Revised Report: Amended - See
Case Narrative.
Kidde Aerospace & Defence, Inc
Mr Tim Fernandez
4200 Airport Drive NW
Wilson NC 27896
Case Narrative
Report amended due to client adding COD
Sample Summary Report
Samnie Name
Outfall #1, grab
Outfali #2, grab
6>MICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Laboratory ID Client Matrix
K110154-01 Stormwater
K110154-02 Stormwater
Project Name: Stormwater Sample
Project 1 PO Number 201528352
Received. 09/02/2021
Reported: 09/28/2021
Sample Type Sample Begin Sample Taken
Grab 09/01/21 1147
Grab 09101 /21 11.37
Lab Received
09/02/21 13:30
09/02/21 13:30
Page 2 of 10

Analytical Testing Parameters
Client Sample ID: Outfall aM 1, grab
Sample Matrix: Slormwaler
Lab Sample ID: K11015 ,01
Metals Total by ICPMS
EPA 200.8, Rv. 5.4 (1994)
Copper
�qMICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Collected By: Fernandez
Collection Date: 09/01/2021 11 47
Analyses Performed by: Microbac Laboratories Inc, Marietta, OH
Result RL Units DF Note Prepared Analyzed Analyst
0.0219 000200 mg1L 1
Analyses Performed by. Microbac Laboratories, Inc. - Fayetteville
Inorganics Total Result RL Units DF Note
EPA 1664E
Oil & Grease (SGT-HEM)
SM 2540 D-2011
Total Suspended Solids
SM 6220 D-2011
COD, Total
Metals Total by ICP
Metals AqueouslEPA 200.7, Rv. 4.4 (1994)
Lead
Zinc
09110121 0619 09110/21 1319 JYH
Prepared Analyzed Analyst
<5 00
5.00
mg/L
1
B26 09/09/21 1134
09/09/21 1134
713M
50.5
13.2
mg1L
5
09/07/21 1125
KNIN
119
10.0
mg1L
1
09/28/21 1005
09128/21 1207
TXN
Result
RL
Units
DF
Note Prepared
Analyzed
Analyst
0.031
0 020
mg1L
1
09108121 1343
0108121 1343
TBM
0.269
0 005
mg1L
1
09108121 1343
0l08121 1343
TBM
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 3 of 10

(5>MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Client Sample ID: Outfall #2, grab
Sample Matrix: Slormwater
Collected By:
Fernandez
Lab Sample ID: K110154-02
Collection Date: 09/01/2021 11.37
Analyses Performed by.
Microbac Laboratories
Inc, - Marietta. OH
Metals Total by ICPMS
Result
RL
Units
OF
Note
Prepared
Analyzed
Analyst
EPA 200.8, Rv. 5.4 (1994)
Copper
-;0.00200
0.00200
mg1L
1
J
09/10121 0619
09110/21 1115
JYH
Analyses Performed by.
M crobac Laboratories, Inc -
Fayetteville
Inorganics Total
Result
RL
Units
OF
Note
Prepared
Analyzed
Analyst
EPA 1664E
f)d & Grease (SGT-HEMa
<5 0(1
500
mg/L
1
B25
09/09/21 1134
09M121 1134
TOM
SM 2540 0-2011
Total Suspended Solids
18.9
943
mglL
4
09M7W 1125
KMN
SM 5220 0-2011
COD. Total
42.7
100
mglL
1
09128/21 1005
09/28/21 1207
TXN
Metals Total by ICP
Result
RL
Units
OF
Note
Prepared
Analyzed
Analyst
Metals AqueouslEPA 200.7, Rv. 4.4 (1994)
Lead
cC.002C.
0.020
mg+l-
1
09/08/21 1347
09/08/21 1347
TOM
Zinc
0.009
0.005
mg?L
1
09/08/21 1347
09/08/21 1347
T13M
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 19110.864.11920 p I www,microbac.com Page 4 of 10

(5)MICROBAC'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Batch Log Summary
Method Bach LADOEatory ID Q12ent I Source ID
EPA 200 8, Rv 5 4 (1994) 13110476 8110476-BLK1
B 110476-BS i
K110154 02
Outfall #2, grab
B110476-SRL1
M110546-01
K110154-01
Outfall #1, grab
Method Batch Laboratory ID
Client/ SourceID____._
SM 2540 D-2011 KI10309 K110309-BS1
K110154-01
Outfall #1, grab
K110154--02
Outfall #2, grab
K110309-BLK1
K110309-DUP1 K110017-01
Method Batch Laboratory ID
Client! Source ID
EPA 200.7. Rv. 4.4 (1994) K110721 K110721-SRMI
KI10721 •CCVI
K110721 •CCB1
K110721-BS1
K 110721-BS2
K110721-BLK1
K110154-01
Outfall #1, grab
K110154-01
Outfali #1, grab
K110154-02
Outfall #2, grab
K110154-02
Outfall #2, grab
K110721-DUP1
K110138-01
K110721-MS I
K110138-01
K110721-MS01
K110138-01
KI10721-CCV2
K110721-CCB2
K110721-CCV3
K110721-CCB3
KH 0721-CCV4
K 110721-CCB4
K110721-SRM2
____Method Batch_
Laboratory_ID
_ Client Source _ID_
EPA 1664E KI10725
K110725-DUP1
K110154-01
K110725-BLK1
K110154-02
Outfall #2, grab
K110725-BSI
K110725-MSI
K110154-02
K110154-01
Outfall #1, grab
Method _ _. ..__ _ Batch
Laboratory ID
Client I Source ID
SM 5220 D-2011 KI12804
K110154-02
Outfall #2. grab
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 10

6)MICROBAC'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
SM 5220 D-2011 KI12804 K112804-CCV2
K 112804-CCV I
K112804 BLK2
K112804 BLK1
K112804-DUPI K110026-01
K112804-DUP2 K110062-01
K112804 BS1
K112804 MS1 K110026-01
K112804-MS2 K110062-01
K110154-01 Outfall #1, grab
K112804 CCV3
Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville
Spike Source %REC RPD
Inorganics Total Result RL Units Level Result %aREC Limits RPD Limit Notes
Batch K110309 - Wet Chem Aqueous - SM 2540 D-2011
PBW01 (KI10309-BLK1) Prepared &Analyzed: 09/07/2021
Total Suspended Solids <2 50 250 mg1L
LCSW01 (KI10309-B$l) Prepared & Analyzed: 09/07/2021
Total Suspended Solids 964 250 mg1L 994 97 95-105
Reactor #1 D (KI10309-DUPI) Source: K110017-01 Prepared & Analyzed: 09/07/2021
Total Suspended Solids 5280 2.50 mg1L 5280 0 10
Batch K110725 - Wet Chem Aqueous - EPA 1664B
Blank (KII0725-BLKI)
Prepared & Analyzed: 0910912021
Oil & Grease (SGT-HEM)
<5.00
5.00
mg/L
LCS (KI10725-BSI)
Prepared & Analyzed: 09/09/2021
Oil & Grease (SGT-HEM)
21.2
5.00
mg1L 64-114
Duplicate (KI10725-DUPI)
Source: K110154-01
Prepared & Analyzed: 09/09/2021
Oil & Grease (SGT-HEM)
<5.00
500
mg1L 3.08 48 200
Matrix Spike (Ki10725-MS1)
Source: K110164-02
Prepared & Analyzed: 09/09/2021
Oil & Grease (SGT-HEM)
35.5
500
mg1L ND 64-132
Batch KI12804 -Wet Chem Aqueous - SM 5220 D-2011
PBW01 (K112804-BLKI)
Prepared & Analyzed: 09/2812021
COO, Total
<10.0 10.0
mg1L
PBW02 (K112804-BLK2)
Prepared & Ana yzed: 09/28/2021
COD, Total
<10 0 10.0
mg1L
LCSW01 (K112804.BS1)
Prepared & Analyzed: 09/28/2021
COD, Total
507 10.0
mglL 500 101 95-105
Effluent, compositeD (KI12804-DUP1)
Source: K110026-01
Prepared & Analyzed: 09/28/2021
COD, Total
66.7 10.0
mg1L 73.7
10 20
Final Effluent, compositeD (KI12804-DUP2)
Source: K110062-01
Prepared & Analyzed: 09/28/2021
COD, Total
777 10.0
mg1L 79.7
3 20
Microbac Laboratories, Inc.
2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 6 of 10

*MICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Spike Source
%REC
RPD
Inorganics Total
Result
RL
Units Level Result %REC
Limits
RPD Limit Notes
Batch KI12804 - Wet Chem Aqueous - SM 5220 D-2011
Effluent, compositeS (KI12804-MS1)
Source: K110026-01
Prepared & Analyzed 0912812021
COD, Total
102
10.0
mg1L 25.0 73.7 112
80-120
Final Effluent, compositeS (KI I 2804-MS2)
Source: K110062-01
Prepared & Analyzed 09/28/2021
COD, Total
997
10.0
mglL 25.0 79.7 80
80-120
Spike Source
%REC
RPD
Metals Total by ICP
Result
RL
Units Level Result %REC
Limits
RPD Limit Notes
Batch Kill 0721 - Metals Aqueous - EPA 200.7, Rv. 4.4 (1994)
Blank (KI10721-BLKI)
Prepared & Analyzed 09/08/2021
Lead
<0.040
0.040
mg1L
Zinc
<0.010
0 010
mg1L
LCS (KI10721-BSI)
Prepared &Analyzed: 09/08/2021
Lead
0.229
0 040
mg1L 0.248 92
85 115
Zinc
0.241
0 010
mg1L 0.248 97
85 115
LCS (KII0721-BS2)
Prepared & Analyzed: 0910812021
Lead
0.231
0 040
mglL 0.248 93
85-115
Zinc
0.248
0.010
mg1L 0.248 100
85-115
Duplicate (KI10721 -DU P1)
Source: K110138-01
Prepared & Analyzed. 09/08/2021
Lead
<0.020
0.020
mg1L ND
20
Zinc
0.131
0.005
mglL 0.125
5 20
Matrix Spike (KII0721-MS1)
Source: K110138-01
Prepared & Analyzed: 0910812021
Lead
0.230
0 020
mglL 0 248 ND 93
70-130
Zinc
0.390
0 005
mglL 0.248 0,125 106
70-130
Matrix Spike Dup (KI10721-MSD1)
Source: K110138-01
Prepared & Analyzed: 09/08/2021
Lead
0.231
0 020
mglL 0.248 ND 93
70-130
0.4 30
Zinc
0.379
0 005
mglL 0.248 0,125 102
70-130
3 30
Reference (KI10721SRM1)
Prepared & Analyzed: 09/08/2021
Lead
0.978
mg1L 1.00 98
95-105
Zinc
1.01
mg+L 1.00 i01
95-105
Reference (KI10721-SRM2)
Prepared & Analyzed: 09/08/2021
Lead
0.930
mg1L 1.00 93
95-105
Zinc
0.989
mg1L 100 99
95-105
Batch Quality Control Summary: Microbac Laboratories Inc.,
- Marietta, off
Spike Source
%REC
RPD
Metals Total by ICPMS
Result MDL
RL
units Level Result %REC
Limits
RPD Limit Notes
Batch B110476 - 200.8 W - EPA 200.8, Rv. 5.4 (1994)
Blank (B110476-BLKI)
Prepared & Analyzed: 09/10/2021
Copper
<0.00100 0.00100
0.00200
mg1L
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 10

6)MICROBAC'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K110154
Metals Total by ICPMS Result MDL RL
Batch B110476 - 200.8 W - EPA 200.8, Rv. 5.4 (1994)
Spike Source %REC RPD
Units Level Result %REC Limits RPD Limit Notes
LCS (13V0476-13SI) Prepared &Analyzed: 09/1012021
Copper 0 164 000100 0 00200 mg1L 0.160 102 85-115
Definitions
B25:
J:
MDL:
mglL:
RL:
RPD:
<1 Liter of sample analyzed
The result is an esl�mated quantity. The assoc-ated numerical value is the approximate concentrat,on of the analyte
in the sample.
Minimum Detection Limit
Milligrams per Liter
Reporting Limit
Relative Percent Difference
Cooler Receipt Log
Cooler ID: Default Cooler
Cooler Inspection Checklist
ice Present or not required?
Custody seals intact or not required
COC includes customer information?
Sample collector identified on COG?
Correct type of Containers Received
Containers Intact?
Enough sample volume for indicated tests received?
Samples arrived within hold time?
Chemical preservations checked or not required?
VOA vials have zero headspace, or not recd ?
Project Requested Certifications)
Microbac Laboratories Inc., Marietta. OH
583
Microbac Laboratories. Inc. - Fayetteville
11
Report Comments
Temp: 2.1 °C
Yes
Shipping containers sealed or not required?
Yes
Yes
Chain of Custody (COC) Present?
Yes
Yes
Relinquished and received signature on COC?
Yes
Yes
Sample type identified on COC?
Yes
Yes
Correct number of containers 'isled on COC?
Yes
Yes
COC includes requested analyses?
Yes
Yes
Sample labels match COG (Name, Date & Time?)
Yes
Yes
Correct preservatives on COG or not required')
Yes
Yes
Preservation checks meet method requirements?
Yes
Yes
NC Dept of the Environment and Natural Resources
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received rn proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying doruments, represents onty the
sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith
present and an authorized signature is included The services were provided under and Administration
subject to Microbac's standard terms and conditions whkh can be located and Reported 0912812021 19 18
! d �►r b d
rev ewe at_ ttys:J mrcr0 ac.comisrrR_BFrltemis-eorrWtruhs}.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 10

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