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WI0700012_Monitoring (Report)_20210528 (2)
AJutrien. CERTIFIED MAIL May 28, 2021 NC Division of Water Resources - Groundwater Resources Section Attn: Michael Rogers 1636 Mail Service Center Raleigh, NC 27699 Subject: Injection Well Permit #WI0700012 February 2021— April 2021 PCS Phosphate Company, Inc.' Tank Farm Remedial Action System Beaufort Co. Please find the subject groundwater monitoring report attached. This includes the sampling and reporting requirements of the above referenced permit as well as the reporting requirements of the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7, b) MWTF1-CR, c) Form GW-59 for each of the fourteen withdrawal wells, d) piezometer level monitoring field sheet and e) the summary operational and maintenance report. Please do not hesitate to contact me at (252) 322-8283 if you have any questions regarding this information. Sincerely, C D. Daniel Winstead III Senior Environmental Engineer Nutrien 1Jg00 '1c ` 1 1530 NC Hwy 306 South, Aurora, NC USA 27806 nutrien.com 1 Effective January 1, 2018, PCS Phosphate Company, Inc. is an indirect subsidiary of Nutrien Ltd. PCS Phosphate Company, Inc. remains the legal operating entity and permittee. Attachments pc: 12-07-02 (w/ attachments) W.M Ponton (w/attachments) T.E. Herring (w/ attachments) J. A. Casey (w/ attachements) R. B. Lee (w/ attachments) 2 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESINGUNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (Strik&rora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (City) (Stale) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field rk Remediation: • Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: - (from Permit) SAMPLING INFORMATION FIELD ANALYSES: pH 00400: 6.6 units Temp. 00010: 24.0 °C If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): MWTF-1A Date sample collected: 04/20/21 Well Depth: 6.40 ft. Well Diameter: 2 in. Depth to Water Level 82546: 3.25 ft. below measuring point Screened Interval: 3.40 ft. to 5.40 ft. Spec. Cond. 00094: 921 µMhos Measuring Point is 3.86 ft. above land surface Relative M.P. Elevation: 14.35 ft. Odor oo0as: None Volume of water pumped/bailed before sampling: 2000 Milliters Appearance Clear here: Samples for metals were collected unfiltered: ■ YES IN NO '4 N/A Field acidified: M YES M NO !II N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 2.525 mg/L Other (Specify Compounds and Concentration Units): Fluoride = 0.50 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Dissolved Solids:Total 70300 440 mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 6.7 units Ba - Barium 01o07 N/A ug/L TOC 00680 6.1 mg/L Ca - Calcium 00916 N/A mg/L Chloride 00940 7.0 mg/L Cd - Cadmium 01027 N/A ug/L Arsenic o1002 N/A ug/L Chromium: Total 01034 N/A ug /L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron o1oa5 N/A ug1L Sulfate 00945 22.1 mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? • Yes (1) M No (0) VOC 7873 . method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia ooslo N/A mg/L Mg - Magnesium 00927 N/A mg/L , method # (Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total) Mn - Mananese 01055 N/A 9 ug/L . method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurateand complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and ,mprisonment for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 4 r Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY LABORATORY INFORMATION Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L /100mL Nitrate (NO3) as N o062o N/A mg/L /100mL Phosphorus: Total as P 00665 5.750 mg/L Orthophosphate 70507 N/A mg/L )issolved Solids:Total 70300 580 mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 5.7 units Ba - Barium o1007 N/A uglL TOC 0068o 6.7 mg/L Ca - Calcium oos16 N/A mg/L Chloride 00940 42.0 mg/L Cd - Cadmium 01027 N/A ug/L _ Arsenic 01002 N/A uglL Chromium: Total 01034 N/A ug/L 9 mg/L Cu - Copper 01042 N/A mg/L Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L Sulfate o0945 228.0 mg/L Hg - Mercury 71900 N/A ug/L Specific Conductance moss N/A µMhos K - Potassium 00937 N/A mg/L mg/L Mg - Magnesium cosy N/A mg/L Mn - Manganese 01055 N/A ug/L TKN as N o0625 N/A mg/L Ni - Nickel 01067 N/A ug/L Grease and Oils 00552 N/A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Mail original and 1 copy to: Please Print Clearly or Type Facility Name: PCS Phosphate Co., INC - Aurora Division Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (Strt rora, NC 27806 (City) Contact Person: (State) (Zip) Danny Winstead Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 :from Permit) DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon D Spray Field Remediation: ❑ Remediation: Infiltration Gallery ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump . ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): MWTF-1 B Well Depth: 13.5 ft. Depth to Water Level 82546:3.89 ft. below measuring point Measuring Point is 3.86 ft. above land surface Volume of water pumped/bailed before sampling: 2000 Samples for metals were collected unfiltered: D YES Date sample collected: 04/20/21 Well Diameter: 2 in. Screened Interval: 10.6 ft. Relative M.P. Elevation: 14.36 Milliters to 12.6 ft. ft. ❑ NO ®N/A Field acidified: in YES El NO V'I N/A FIELD ANALYSES: pH 00400: 5.7 units Temp. 00010: 24.0 Spec. Cond. 00094: 849 Odor 00085: None 0 µMhos Appearance Clear PCS Phosphate Co. / Environment 1,Inc Coliform: MF Fecal 31616 N/A Coliform: MF Total 31so4 N/A (Note: Use MPN method for highly turbid samples) Total Ammonia no610 N/A (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 If WELL WAS DRY at time of sampling, check here: Pb - Lead 01051 N/A CertificationNo. # 330 / # 10• Zn - Zinc 01092 N/A ug/L mg/L Other (Specify Compounds and Concentration Units): Fluoride = < 0.30 mg/I ORGANICS: (by GC, GC/MS; HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) No (0) VOC 7873 method # , method # , method # , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/k •-•'VOC.Removai% N/A 1 certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurateand complete, and that the laboratory analytical data was produced using apprevnd methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility rr fines and Imprisonment for knowing violatirc Signature of Permittee tor Authorized Agent) TA`ZrI ? i/ (Date) SUBMIT FORM ON YELLOW PAPER ONLY Specific Conductance 00095 N/A Total Ammonia 00610 N/A (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N o0625 N/A Grease and Oils 00552 N/A Chloride 00940 31.0 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION P, ease Print Clearly or Type Facility Name: PCS Phosphate Co., INC - Aurora Division Mail original and 1 copy to DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (Strrora, NC 27806 (City) Contact Person: (Slate) (Zip) Danny Winstead Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 ,from Permit PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery O Spray Field i!i Remediation: O Rotary Distributor ❑ Land Application of Sludge O Water Source Heat Pump 0 Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 42.5 ft. Depth to Water Level 82546: 9.85 Measuring Point is MWTF-1 CR ft. below measuring point 3..00 ft. above land surface Volume of water pumped/bailed before sampling: 2000 Samples for metals were collected unfiltered: ❑ YES Date sample collected: 04/20/21 Well Diameter: 2 in. Screened Interval: 40.5 ft. Relative M.P. Elevation: 14.54 Milliters ❑ NO ®N/A Field acidified: rl YES 0 NO LABORATORY INFORMATION Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A Coliform: MF Fecal 31616 N/A Coliform: MF Total 31504 N/A (Note: Use MPN method for highly turbid samples) ]issolved Solids:Total 70300 830 pH (Lab) 00403 6.6 mg/L units TOC 00680 9.2 mg/L mg/L Arsenic o1002 N/A ug/L mg/L Phenol 3273o N/A ug/L Sulfate 00945 149.0 mg/L µMhos mg/L mg/L For Remediation Systems Only (Attach Lab Reports): to 42.5 ft. ft. FIELD ANALYSES: pH 00400: 6.5 units Temp. mow: 24.9 °C Spec. Cond. 00094: 1461 Odor 00085: None Appearance 0 N/A PCS Phosphate Co. / Environment 1,Inc mg/L Nitrite (NO2) as N 00615 N/A mg/L /100mL Nitrate (NO3) as N 00620 N/A mg/L /100mL Phosphorus: Total as P 00665 30.250 mg/L Orthophosphate 70507 N/A mg/L Al - Aluminum 01105 N/A mg/L Ba - Barium 01007 N/A ug/L mg/L Cd - Cadmium 01027 N/A ug/L ug/L Cu - Copper o1042 N/A mg/L ug/L Hg - Mercury 7190o N/A ug/L K - Potassium 00937 N/A mg/L Ca - Calcium 00916 N/A Chromium: Total 01034 N/A Fe - Iron 01045 N/A Mg - Magnesium 00927 N/A Mn - Manganese 01055 66 Ni - Nickel 01067 N/A Influent Total VOCs: N/A mg/L mg/L ug/L uglL µMhos Clear Pb - Lead 01051 N/A Zn - Zinc 01092 NIA If WELL WAS DRY at time of sampling, check here:[ 1 Certification No. # 330 / # 10 ug/L mg/L Other (Specify Compounds and Concentration Units): Fluoride = < 0.30 mg/I ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 Yes (1) C I No (0) VOC 7873 Effluent Total VOCs: N/A , method # , method # , method # , method # mg/L VOC Removal% N/A I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and inaprisanment for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature or Permit -lee (or Authorized Ag (Date) SUBMIT FORM ON YELLOW PAPER ONLY William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 'Specific Conductance moss N/A Total Ammonia 00610 N/A (Ammonia Nitrogen; NHsas N; Ammonia Nitrogen, Total) TKN as N oos25 N/A Grease and Oils 00552 N/A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail original and 1 copy to: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-306 FACILITY INFORMATION Piaase Print Clearly or Type Facility Name: PCS Phosphate Co., INC - Aurora Division Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (Str t rora, NC 27806 (city) Contact Person: (State) Danny Winstead (Zip) Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 ,from Permit, PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other x TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Spray Field ❑ Rotary Distributor D Water Source Heat Pump ❑ Remediation: Infiltration Gallery IMM Remediation: ❑ Land Application of Sludge ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: N/A ft. WLCT Depth to Water Level 82546: N/A ft. below measuring point Measuring Point is N/A ft. above land surface Volume of water pumped/bailed before sampling: Continuous Samples for metals were collected unfiltered: D YES ❑ NO Date sample collected: 04/20/21 Well Diameter: N/A in. Screened Interval: N/A ft. Relative M.P. Elevation: N/A ft. Milliters ®N/A Field acidified: ri YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L /100mL /100mL Coliform: MF Fecal 31616 N/A Coliform: MF Total 31504 N/A (Note: Use MPN method for highly turbid samples) ]issolved Solids:Total 70300 590 mg/L pH (Lab) 00403 7.0 units TOC 00680 5.6 mg/L Chloride 0094o 49.0 mg/L Arsenic 01ooz N/A ug/L mg/L Phenol 32730 N/A ug/L Sulfate 00945 75.3 mg/L µMhos mg/L mg/L to N/A ft. N/A FIELD ANALYSES: pH 00400: 7.0 units Spec. Cond. 00094: 944 Temp. 00010: 21.1 °C Odor 00085: None Appearance PCS Phosphate Co. / Environment 1,Inc Nitrite (NO2) as N oos15 N/A Nitrate (NO3) as N 00620 N/A Phosphorus: Total as P 00665 0.020 Orthophosphate 70507 N/A Al - Aluminum 01105 N/A Ba - Barium 01007 N/A Ca - Calcium owls N/A Cd - Cadmium o1027 N/A Chromium: Total 01034 N/A Cu - Copper 01042 N/A Fe - Iron o1o45 N/A _ Hg - Mercury 7190o N/A K - Potassium 00937 N/A Mg - Magnesium 00927 N/A Mn - Manganese 01055 < 10.0 Ni - Nickel 01067 N/A mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L µMhos Clear Pb - Lead 01051 N/A Certification No. # 330 / # 10 Zn - Zinc 01092 NIA ug/L mg/L Other (Specify Compounds and Concentration Units): Fluoride = 0.53 mg/I ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) rt No (0) VOC 7873 method # method # method # method # If WELL WAS DRY at time of sampling, check here: For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is trueaccurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibII:ty of fines una imprisonment for knowing violations a4111101Mir \ Signature of Permittee (or Authorized Agent) S (Date) SUBMIT FORM ON YELLOW PAPER ONLY William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (strVirora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (City) (State) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field ' J Remediation: • Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: ,from Permit, SAMPLING INFORMATION _ FIELD ANALYSES: pH 00400: 6.8 units Temp. 00010: 22.2 °C If WELL WAS DRY at time of check WELL ID NUMBER (from Permit): CIW-7 Date sample collected: 04/20/21 Well Depth: 48.0 ft. Well Diameter: 4 in. 45.25 Depth to Water Level 82546: N/A ft. below measuringft. to P point Screened Interval: 31.0 ft. Spec. Cond. 00094: 862 µ Mhos MeasuringPoint is 3.33sampling, ft. above land surface Relative M.P. Elevation: N/A ft. Odor 00085: None Volume of water pumped/bailed before sampling: Continous gallons Appearance Clear here: Samples for metals were collected unfiltered: • YES ■ NO 6 IN/A Field acidified:. YES MI NO J N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 NIA mg/L Nitrite (NO2) as N 00615 N/A mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L uglL mg/L ug/L uglL mg/L mg/L uglL ug!L Pb - Lead (lost N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N ooszo N/A Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P oosss 0.147 Other (Specify Compounds and Concentration Units): Fluoride = 0.71 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A ]issolved Solids:Total 70300 551 mg/L Al - Aluminum 011os N/A pH (Lab) 00403 7.0 units Ba - Barium 01007 N/A TOC 00680 5.4 mg/L Ca - Calcium 00916 N/A Chloride 0094o 47.0 mg/L Cd - Cadmium o1027 N/A Arsenic o1o02 N/A ug!L Chromium: Total 01034 N/A Grease and Oils oo5s2 N/A mg/L Cu - Copper 01042 N/A ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A Sulfate oo94s 48.3 mg/L Hg - Mercury 71900 N/A Lab Report Attached? • Yes (1) ©■ No (0) VOC 7873 method # Specific Conductance o0o95 N/A µMhos K - Potassium 00937 N/A Total Ammonia ooslo N/A mg/L Mg - Magnesium 00927 N/A . method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese °toss < 10.0 , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify thatto the best of my knowledge and belief, the information submitted in this report is trueaccurateand complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the p•:rS t. ; ' r +' .a,r =;.:-••rnent for .00AWer Signs ure of Permtttee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY Specific Conductance 00095 N/A Total Ammonia 00610 N/A (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N 00625 N/A Grease and Oils 00552 N/A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION m'+ease Print Clearly or Type Facility Name: PCS Phosphate Co., INC - Aurora Division Permit Name (if different): Mail original and 1 copy to: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-308 Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (StrWt rora, NC 27806 (City) (State) (Zip) Contact Person: Danny Winstead Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 :from Permit. PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery D Spray Field Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge O Water Source Heat Pump 0 Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 55.0 ft. Depth to Water Level 82546: N/A CWW-1 ft. below measuring point Measuring Point is 2.25 ft. above land surface Volume of water pumped/bailed before sampling: 3000 Samples for metals were collected unfiltered: ❑ YES LABORATORY INFORMATION Date sample collected: 04/20/21 Well Diameter: 4 in. Screened Interval: 33.27 ft. to ft. Relative M.P. Elevation: 10.60 Milliters 0 NO I, IN/A Field acidified: II YES ❑ NO Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L /100mL /100mL Coliform: MF Fecal 31616 N/A Coliform: MF Total 31504 N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids:Total7o3oo 3000 mg/L pH (Lab) 00403 6.4 units TOC mom 4.9 mg/L Chloride 00940 452.0 mg/L Arsenic 01002 N/A ug/L mg/L Phenol 32730 N/A ug/L Sulfate 00945 778.0 mg/L µMhos mg/L mg/L 52.68 ft. (1 N/A FIELD ANALYSES: pH 00400: 6.30 units Temp. 00010: 20.7 °C Spec. Cond. 00094: 4360 Odor 00085: None µMhos Appearance Clear PCS Phosphate Co. / Environment 1,Inc Nitrite (NO2) as N 00615 N/A Nitrate (NO3) as N 00620 N/A Phosphorus: Total as P 00665 18.200 Orthophosphate 70507 N/A Al - Aluminum 01105 N/A Ba - Barium 01007 N/A Ca - Calcium 00916 N/A Cd - Cadmium 01027 N/A Chromium: Total 01034 N/A Cu - Copper 01042 N/A Fe - Iron 01045 N/A Hg - Mercury 71900 N/A K - Potassium 00937 N/A Mg - Magnesium 00927 N/A Mn - Manganese 01055 N/A Ni - Nickel 01067 N/A mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead 01051 N/A Certification No. # 330 / # 10 Zn - Zinc 01092 N/A ug/L mg/L Other (Specify Compounds and Concentration Units): Fluoride = < 0.30 mg/I. ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 Yes (1) AI No (0) VOC 7873 , method # , method # method # method # If WELL WAS DRY at time of sampling, check here: For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Permute (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY Specific Conductance 00095 N/A Total Ammonia 00610 N/A (Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total) TKN as N 00625 N/A Grease and Oils o0552 N/A Chloride 0094o N/A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Reese Print Clearly or Type Facility Name: PCS Phosphate Co., INC - Aurora Division Mail original and 1 copy to: Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (str rora, NC 27806 (City) (State) (Zip) Contact Person: Danny Winstead Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 nrom Pewit, DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-8074308 PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED D Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field [ri Remediation: D Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 52.15 ft. CWW-2 Date sample collected: N/A Depth to Water Level 82546: N/A ft. below measuring point Measuring Point is 3.0 ft. above land surface Volume of water pumped/bailed before sampling: N/A Well Diameter: 4 Screened Interval: 30.57 ft, Relative M.P. Elevation: 10.23 gallons in. to ft. 49.82 ft. Samples for metals were collected unfiltered: 0 YES 0 NO ®N/A Field acidified: El YES in NO 0 N/A LABORATORY INFORMATION Date sample analyzed: N/A Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A Coliform: MF Fecal 31616 N/A Coliform: MF Total 31504 N/A (Note: Use MPN method for highly turbid samples) )issolved Solids:Total 70300 N/A pH (Lab) 00403 N/A mg/L /100mL /100mL mg/L units TOC 0068o N/A mg/L mg/L Arsenic 01002 N/A ug/L mg/L Phenol 32730 N/A ug/L Sulfate 00945 N/A mg/L µMhos mg/L mg/L For Remediation Systems Only (Attach Lab Reports): FIELD ANALYSES: pH 00400: NIA units Temp. 00o10: N/A °C Spec. Cond. 00094: N/A Odor 00085: Appearance PCS Phosphate Co. / Environment 1,Inc Nitrite (NO2) as N 00615 N/A Nitrate (NO3) as N 00620 N/A Phosphorus: Total as P 00665 N/A Orthophosphate 70507 N/A mg/L mg/L mg/L mg/L Al - Aluminum 01105 N/A mg/L ug/L Ca - Calcium 00916 N/A mg/L Cd - Cadmium 01027 N/A ug/L Chromium: Total 01034 N/A ug/L Cu - Copper 01042 N/A mg/L ug/L ug/L K - Potassium 00937 N/A mg/L Ba - Barium 01007 N/A Fe - Iron 01045 N/A Hg - Mercury moo N/A Mg - Magnesium o0927 N/A Mn - Manganese 01055 N/A Ni - Nickel 01067 N/A Influent Total VOCs: N/A mg/L mg/L ug/L ug/L µMhos Pb - Lead 01051 N/A Zn - Zinc 01092 N/A Certification No. # 330 / # 10 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 Yes (1) IN No (0) VOC 7873 method # Effluent Total VOCs: N/A method # method # . method # If WELL WAS DRY at time of sampling, check here: mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. 1 am aware that there are significant penalties for submitting false information. including the possibility of fines , ,i! ,r-Tnsanment for knowing violations, William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Aloriv Signature of Permittee (or Authorized Agent) /Zg/ 2s2/ (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 Copy to: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807.6306 FACILITY INFORMATION Please Pnnt Cleaily or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (St HUrora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (City) (state) (zip) Contact Person: Danny Winstead - Telephone#: (252)-322-8283 • Spray Field ti] Remediation: • Rotary Distributor ■ Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: Sfrom Permit) SAMPLING INFORMATION FIELD ANALYSES: pH 00400: N/A units Temp. 000to: N/A °C I If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): CWW-3 Date sample collected: N/A Well Depth: 53.0 ft. Well Diameter: 4 in. Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 36.42 ft. to 50.6i ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 3.08 ft. above land surface Relative M.P. Elevation: 9.95 ft. Odor 000s5: Volume of water pumped/bailed before sampling: N/A gallons Appearance here: X Samples for metals were collected unfiltered: • YES • NO !A N/A Field acidified: A YES ■ NO '1 N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330/# 10 Date sample analyzed: N/A Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L 7issolved Solids:Total 7o30o N/A mg/L Al - Aluminum 01105 N/A mg/L _ pH (Lab) 00403 N/A units Ba - Barium 01007 N/A ug/L TOC o0680 N/A mg/L Ca - Calcium oos16 N/A mg/L Chloride 0094o N/A mg/L Cd - Cadmium 01027 N/A ug/L Arsenic at002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils o0552 N/A mg/L Cu - Copper o1042 N/A mg/L _ ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L Sulfate 00945 N/A mg/L Hg - Mercury 7190o N/A ug/L Lab Report Attached? • Yes (1) ill No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 0o937 N/A mg/L Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L , method # (Ammonia Nitrogen; NH,asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A ug/L _ , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify thatto the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are sic nificant penalties for submitting false information. including the possihiliiv r+ far !, a in 'n; ;r;sonment for known. violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 P27,4 Signa e of Permttee (or Authorized Agent) s/241/2p1) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 co'pt0: DEPARTMENT OF ENVIRONMETAL TWATERRESOURCES INFORMAION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1817 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (stt rora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (City) (State) (zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field Lai Remediation: • Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: ifrom Permit, SAMPLING INFORMATION FIELD ANALYSES: pH 00400: 6.6 units Temp. 00010: 27.6 °C If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): CWW-4 Date sample collected: 04/20/21 Well Depth: 53.0 ft, Well Diameter: 4 in. Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 41.67 ft. to 50.92 ft. Spec. Cond. 00094: 4737 µMhos Measuring Point is 2.75 ft. above land surface Relative M.P. Elevation: 10.73 ft. Odor 000ss: None Volume of water pumped/bailed before sampling: 3000 Milliters Appearance Clear here: Samples for metals were collected unfiltered: • YES • NO !►I N/A Field acidified: IA YES r NO 'I N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N o0s1s N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01o92 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 23.600 mg/L Other (Specify Compounds and Concentration Units): Fluoride = < 0.30 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L )issolved Solids:Total 70300 2900 mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 6.6 units Ba - Barium 01007 N/A ug/L TOC 0066o 4.3 mg/L Ca - Calcium 00916 N/A mg/L Chloride 0o940 555.0 mg/L Cd - Cadmium 01027 N/A ug/L Arsenic e1002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L g/ Sulfate 00945 813.0 mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? • Yes (1) ❑ No (0) VOC 7873 . method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L , method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A ug/L , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines ari•! is;,^.rnent for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Permittee (or Authorized Agent) 512�12o2( (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original to: COMPLIANCE REPORT FORM and 1 copy to: DEPARTMENT OF ENVIRONMENTALINFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1817 Phone: 919.807-8306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): _ NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (Stlerora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (city) (State) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field [il Remediation: • Rotary Distributor ■ Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump ■ Other: [from Permit) SAMPLING INFORMATION FIELD ANALYSES: pH 00400: N/A units Temp. 00010: N/A oC If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): CWW-5 _ Date sample collected: N/A _ Well Depth: 53.17 ft. Well Diameter: 4 in. Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 41.75 ft. to 51.06 ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 2.58 ft. above land surface Relative M.P. Elevation: 10.74 ft. Odor 00085: N/A - Volume of water pumped/bailed before sampling: N/A gallons Appearance N/A here: X Samples for metals were collected unfiltered: ■ YES ■ NO I7JN/A Field acidified: A YES MINO !1 N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: N/A Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A uglL Coliform: MF Fecal 31616 NIA /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L )issolved Solids:Total 70300 N/A mg/L Al - Aluminum o11os N/A mg/L pH (Lab) 00403 N/A units Ba - Barium 01007 N/A ug/L TOC o068o N/A mg/L Ca - Calcium 00916 N/A mg/L Chloride 0094o N/A mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 01o34 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper o1042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? • Yes (1) I No No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia o0610 N/A mg/L Mg - Magnesium o0927 N/A mg/L , method # (Ammonia Nitrogen; NH9as N; Ammonia Nitrogen, Total) Mn - Mananese 01055 N/A 9 ug/L , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the hest of my knowledge and belief, the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certifiecl laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for knowing violations. William M. Ponton, General Manager Perm ttee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Perm! ee (or Authorized Agent) X12V'201 2( (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail original and 1 copy t0: RESOURCES DEPARTMENT OF ENVIRONMENTALINFORMATION PROCESSING UNIT 1817 MAIL SERVICE CENTER, RALEIGH, NC 27699-1817 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC -Aurora Division Non -Discharge UIC X Permit Name (if different): _ NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (str§f/Jrora, NC 27806 County Beaufort ■ Lagoon • Remediation: Infiltration Gallery (city) (State) (zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 ■ Spray Field i Remediation: • Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 ■ Water Source Heat Pump • Other: from Permit _ SAMPLING INFORMATION 04/20/21 FIELD ANALYSES: pH 00400: 6.4 units Temp. 00o10: 28.3 °C If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): CWW-6 Date sample collected: Well Depth: 53.00 ft. Well Diameter: 4 in. Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 36.62 ft. to soma ft. Spec. Cond. 00094: 2294 µMhos Measuring Point is 2.92 ft. above land surface Relative M.P. Elevation: 9.92 ft. Odor 000s5: None Volume of water pumped/bailed before sampling: 3000 Milliters YES II NO Appearance Clear here: Samples for metals were collected unfiltered: ■ YES IN NO '4 N/A Field acidified: N J N/A LABORATORY INFORMATION PCS Phosphate Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: 04/20/21 to 05/11/21 Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 24.400 mg/L Other (Specify Compounds and Concentration Units): Fluoride = < 0.3 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L ]issolved Solids:Total 70300 1600 mg/L Al - Aluminum o1105 N/A mg/L pH (Lab) 00403 6.5 units Ba - Barium 01007 N/A ug/L TOC 0068o 8.2 mg/L Ca - Calcium oasis N/A mg/L Chloride 00940 54.0 mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron o1oa5 N/A ug/L Sulfate o09as 536.0 mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? ■ Yes (1) 0 No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L , method # (Ammonia Nitrogen; NH,asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A ug/L , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify thatto the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the poss;biF;y of fares and ,nprisonment for knowing vio'atlons. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Pennittee for Authorized Age T/Zx12 Z/ (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-306 FACILITY INFORMATION Please Print Clearly orType PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division - _ Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (str9 &ora, NC 27806 County Beaufort ■ Lagoon ■ Remediation: Infiltration Gallery (city) (Stale) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field i`' Remediation: ■ Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: _ from Permit SAMPLING INFORMATION FIELD ANALYSES: pH 00400: N/A units Temp. 00010: N/A °C If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): CWW-7 Date sample collected: N/A Well Depth: 53.00 ft. Well Diameter: 4 in. Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 36.58 ft. to 50_83 ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 1.25 ft. above land surface Relative M.P. Elevation: 9.95 ft. Odor 000ss: Volume of water pumped/bailed before sampling: N/A gallons Appearance here: X Samples for metals were collected unfiltered: • YES ■ NO p®N/A Field acidified: YES ■ NO !I N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 /4 10 Date sample analyzed: N/A Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD o0335 NIA mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A mg/L Other (Specify Compounds and Concentration Units): _ (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A _ mg/L Dissolved Solids:Total 70300 N/A mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 N/A units Ba - Barium 01007 N/A ug/L TOC 00680 N/A mg/L Ca - Calcium 00916 N/A mg/L Chloride 0094o N/A mg/L Cd - Cadmium 01027 N/A ug!L Arsenic 01002 N/A uglL Chromium: Total 01034 N/A uglL Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A uglL Fe - Iron 01045 N/A uglL Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A uglL Lab Report Attached? • Yes (1) (IA No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L , method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Mananese 01055 NIA g uglL , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A uglL , method # - For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false informationi including the possibility of nines and imprisonment for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Permittee (or Authorized Agent) �/Z ( IF2( (Date) SUBMIT FORM ON YELLOW PAPER ONLY Mail original GROUNDWATER QUALITY MONITORING: and 1 copy to: COMPLIANCE REPORT FORM DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC x Permit Name (if different): _ NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (str9t rora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (city) (State) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field !UI Remediation: ■ Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: from Permit' SAMPLING INFORMATION FIELD ANALYSES: pH 00400: N/A units Temp. 00010: N/A °C If WELL WAS DRY at time of II check WELL ID NUMBER (from Permit): SWW-1 Date sample collected: N/A Well Depth: 22.5 ft. Well Diameter: 4 in. 21.12 Depth to Water Level azsas: NIA ft. below measuring point Screened Interval 18.29 ft. to ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 1.52 ft. above land surface Relative M.P. Elevation: 10.70sampling, ft. Odor 00085: Volume of water pumped/bailed before sampling: N/A gallons Appearance here: X Samples for metals were collected unfiltered: ■ YES ■ NO ! 4 N/A Field acidified: A YES ■ NO %I N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 I # 10 Date sample analyzed: N/A Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L uglL uglL Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A (issolved Solids:Total 70300 N/A mg/L Al - Aluminum o11o5 N/A pH (Lab) 00403 N/A units Ba - Barium 01007 N/A TOC 00680 N/A mg/L Ca - Calcium 00916 N/A _ Chloride 00940 N/A mg/L Cd - Cadmium 01027 N/A Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A _ Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A Lab Report Attached? ■ Yes (1) L: No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A , method # (Ammonia Nitrogen; NH3as N: Ammonia Nitrogen, Total) Mn - Manganese moss N/A , method # TKN as N 00625 N/A nag/L Ni - Nickel 01067 N/A , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data vas produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the pese':.id ' tines arirt imprisonment for knowing violations William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Perrnittee (or Authorized Agent) s-l2 20z/ (Date) SUBMIT FORM ON YELLOW PAPER ONLY Specific Conductance 00095 N/A Grease and Oils 00552 N/A GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail original and 1 copy to: FACILITY INFORMATION 1'+ease Print Clearly or Type Facility Name: PCS Phosphate Co., INC - Aurora Division Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (Strora, NC 27806 (city) 'Contact Person: (State) Danny Winstead (Zip) Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 from Permit DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1817 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery D Spray Field Gwl Remediation: ❑ Rotary Distributor 0 Land Application of Sludge ❑ Water Source Heat Pump 0 Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 23.0 ft. Depth to Water Level 82546: N/A SWW-2 Date sample collected: N/A ft. below measuring point Measuring Point is 3.42 ft. above land surface Volume of water pumped/bailed before sampling: N/A Samples for metals were collected unfiltered: ❑ YES Well Diameter: 4 in. Screened Interval: 18.80 ft. Relative M.P. Elevation: 9.99 to 21.63 ft. ft. FIELD ANALYSES: pH 00400: NIA units Temp. motor N/A °C Spec. Cond. 00094: N/A µMhos Odor 00085: gallons Appearance ❑ NO ®N/A Field acidified: El YES 0 NO LABORATORY INFORMATION Date sample analyzed: N/A Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N o0615 N/A Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 0062o N/A N/A If WELL WAS DRY at time of sampling, check here: PCS Phosphate Co. / Environment 1,Inc Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids:Total 70300 N/A mg/L pH (Lab) 00403 N/A units TOC 00680 N/A _ mg/L Chloride cow N/A mg/L Arsenic oloo2 N/A ug/L mg/L Phenol 32730 N/A ug!L Sulfate 00945 N/A mg/L µMhos Total Ammonia 00610 N/A mg/L (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) TKN as N 00625 N/A mg/L Chromium: Total 01034 N/A mg/L mg/L mg/L Orthophosphate 70507 N/A mg/L Al - Aluminum 01105 N/A mg/L Ba - Barium 01007 N/A ug/L mg/L Cd - Cadmium 01027 N/A ug/L ug/L Cu - Copper o1042 N/A mg/L Fe - Iron o1045 N/A ug!L Hg - Mercury 71900 N/A ug/L K - Potassium 00937 N/A mg/L Ca - Calcium 00916 N/A Mg - Magnesium 00927 N/A Mn - Manganese 01055 N/A Ni - Nickel 01067 N/A mg/L ug/L uglL Pb - Lead 01051 N/A Certification No. # 330 / # 10 Zn - Zinc 01092 N/A ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, I-IPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) L No (0) VOC 7873 , method # , method # , method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for knowing violations. William M. Ponton, General Manager Ar', 41 .--- __ Permittee (or Authorized Agent) Name and Tille - Please print or type Sign- +re of Permittee (or Authorized Agent) GW-59 Rev. 05-02-2017 C/ 28'/ 2e 2-/ (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail original and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly orType PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED • Lagoon • Remediation: Infiltration Gallery • Spray Field ■❑ Remediation: 1530 Hwy 306 South (Str9ktl'rora, NC 27806 County Beaufort (city) (State) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Rotary Distributor IIILand Application of Sludge • Water Source Heat Pump • Other: Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 tfrom Permit) SAMPLING INFORMATION If WELL WAS DRY time sampling, check here: at of X WELL ID NUMBER (from Permit): SWW-3 Date sample collected: N/A FIELD ANALYSES: Well Depth: 24.5 ft. Well Diameter: 4 in. pH 00400: NIA units Temp. 00010: N/A oC Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 20.17 ft. to 23.0 ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 3.17 ft. above land surface Relative M.P. Elevation: 9.97 ft. Odor oaoss: Volume of water pumped/bailed before sampling: N/A gallons Appearance Samples for metals were collected unfiltered: ■ YES ■ NO n N/A Field acidified:. YES MI NO J N/A LABORATORY INFORMATION Date sample analyzed: N/A Laboratory Name: PCS Phosphate Co. / Environment 1,Inc Certification No. # 330 / # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coiiform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 NIA mg/L Coiiform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 N/A mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 N/A units Ba - Barium 01007 N/A ug/L TOC 0068o N/A mg/L Ca - Calcium oos16 N/A mg/L Chloride Mao N/A mg/L Cd - Cadmium 01027 N/A ug/L Arsenic o1002 N/A ug/L Chromium: Total o1o34 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L g/ (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A uglL Lab Report Attached? • Yes (1) N No (0) Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L VOC 7873 method # , Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L method # , (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Mananese 01055 N/A g ug/L , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A uglL method # , or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibilin •+i,_s inn „n ,ns ,ri-rent for k�now�in violations William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 rg ure of Permittee (or Authorized Agent) 3-f'S/ 29 ai (Date) SUBMIT FORM ON YELLOW PAPER ONLY William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Cleary or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): _ NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (Str4ff)t rora, NC 27806 County Beaufort ■ Lagoon • Remediation: Infiltration Gallery (City) (state) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field (I Remediation: • Rotary Distributor ■ Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: ;from Permit) SAMPLING INFORMATION _ FIELD ANALYSES: pH 0040o: N/A units Temp. 00o10: N/A oC If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): SWW-4 Date sample collected: N/A Well Depth: 25.0 ft. Well Diameter: 4 in. 23.33 Depth to Water Level 82546: N/A ft. below measuring point Screened Interval: 20.50 ft. to ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 3.42 ft. above land surface Relative M.P. Elevation: 10.73 ft. Odor oo08s: Volume of water pumped/bailed before sampling: N/A gallons Appearance here: X Samples for metals were collected unfiltered: ■ YES • NO '4 N/A Field acidified: la YES MI NO 54 N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: N/A Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L mg/L mg/L mg/L mg/L ug/L mg/L uglL uglL mg/L uglL uglL mg/L mg/L uglL uglL Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A dissolved Solids:Total 7030o N/A mg/L Al - Aluminum 01105 N/A pH (Lab) 00403 N/A units Ba - Barium o1o07 N/A TOC 00680 N/A mg/L Ca - Calcium 00916 N/A Chloride 0094o N/A mg/L Cd - Cadmium 01027 N/A Arsenic 01002 N/A ug/L Chromium: Total oio34 N/A Grease and Oils o0552 N/A mg/L Cu - Copper 01042 N/A ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A uglL Fe - Iron 01045 N/A Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A Lab Report Attached? • Yes (1) 1J No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A , method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Mananese 01055 N/A g _ , method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibiiit•r of fines and ',nprisonr ert 'r, k•+ :•rcj c:.a .,, AOriglir Signature of Per ndtee (or Authorized Agen (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail Original COMPLIANCE REPORT FORM and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-306 FACILITY INFORMATION Please Pnnt Cleady or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (strNarora, NC 27806 County Beaufort ■ Lagoon • Remediation: Infiltration Gallery (cry) (State) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field Cl Remediation: • Rotary Distributor ■ Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump ■ Other: (from Permit] SAMPLING INFORMATION FIELD ANALYSES: pH 00400: NIA units Temp. 00o10: N/A °C If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): SWW-5 Date sample collected: N/A Well Depth: 28.21 ft. Well Diameter: 4 in. Depth to Water Level 82546: N/A ft. below measuring27.21 p point Screened Interval: 24.83 ft. to ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 2.96 ft. above land surface Relative M.P. Elevation: 10.80 _ ft. Odor 00085: Volume of water pumped/bailed before sampling: N/A gallons Appearance here: X _ Samples for metals were collected unfiltered: ■ YES ■ NO !►I N/A Field acidified: a YES ■ NO .2 N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 / # 10 Date sample analyzed: NIA Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N 00620 N/A mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A mg/L _ Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Dissolved Solids:Total 7030o N/A mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 N/A units Ba - Barium 01007 N/A _ uglL TOC moo N/A mg/L Ca - Calcium 00916 N/A mg/L Chloride o094o N/A mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? ■ Yes (1) • No (0) VOC 7873 , method # Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L . method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Mananese D1055 N/A g ug/L . method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L . method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information including the possibility of tines and irnpriaonment for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Permittee (or Authorized Agent) J7 / 21P( (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION P+ease Print Clearly orType Facility Name: PCS Phosphate Co., INC - Aurora Division Mail original and 1 copy to: Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South (strrora, NC 27806 (City) Contact Person: (State) (Zip) Danny Winstead Well Location/Site Name: Tank Farm Remediation County Beaufort Telephone#: (252)-322-8283 No. of wells to be sampled: 18 from Permit. DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: W10700012 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field L>ri Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 29.5 ft, Depth to Water Level 82546: N/A SWW-7 ft. below measuring point Measuring Point is 3.0 ft. above land surface Volume of water pumped/bailed before sampling: NA Date sample collected: Well Diameter: Screened Interval: Relative M.P. Elevation: gallons N/A 4 in. 25.17 ft. 10.70 Samples for metals were collected unfiltered: ❑ YES ❑ NO ®N/A Field acidified: I1 YES LABORATORY INFORMATION Date sample analyzed: N/A Laboratory Name: _ PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A Coliform: MF Fecal 31616 N/A Coliform: MF Total 31504 N/A (Note: Use MPN method for highly turbid samples) :)issolved Solids:Total 70300 N/A pH (Lab) 00403 N/A TOC 00680 N/A Chloride 0osao N/A Arsenic o1002 N/A Grease and Oils 00552 N/A Phenol 32730 N/A Sulfate oo945 N/A Specific Conductance oo0s5 N/A Total Ammonia Dos10 N/A (Ammonia Nitrogen; NH9as N; Ammonia Nitrogen, Total) to 27.5 ft. ft. NO FIELD ANALYSES: pH 00400: NIA units Temp. 00010: N/A °C Spec. Cond. 00094: N/A µMhos Odor 00085: Appearance N/A PCS Phosphate Co. / Environment 1,Inc mg/L Nitrite (NO2) as N 00615 N/A mg/L /100mL Nitrate (NO3) as N 00620 N/A mg/L /100mL Phosphorus: Total as P 00665 N/A mg/L Orthophosphate 70507 N/A mg/L mg/L ug/L mg/L ug/L Chromium: Total 01034 N/A ug/L Cu - Copper 01042 N/A mg/L ug/L Hg - Mercury 71900 N/A ug/L K - Potassium 00937 N/A mg/L Mg - Magnesium 00927 N/A mg/L Mn - Manganese 01055 N/A ug/L Ni - Nickel 01067 N/A ug/L mg/L units mg/L mg/L ug/L mg/L ug/L mg/L µMhos mg/L TKN as N onus N/A mg/L Al - Aluminum o1105 N/A Ba - Barium 01007 N/A Ca - Calcium 00916 N/A Cd - Cadmium 01027 N/A Fe - Iron 01045 N/A Pb - Lead o1os1 N/A Zn - Zinc o1092 N/A Certification No. # 330 / # 10 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) •'.n1 No (0) VOC 7873 method # method # method # method # If WELL WAS DRY at time of sampling, check here:[ I For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is trueaccurateand complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knotting violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Ar' Signature of Perr tttee (or Authorized Agent) r/28' 2c2j (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Mail original COMPLIANCE REPORT FORM and 1 copy t0: DEPARTMENT OF ENVIRONMENTAL WATER RESOURCES INFORMATION PROCESSING UNIT 1817 MAIL SERVICE CENTER, RALEIGH, NC 27699-1817 Phone: 919-807-306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W10700012 Expiration Date: Facility Name: PCS Phosphate Co., INC - Aurora Division Non -Discharge UIC X Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South Aurora, NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED 1530 Hwy 306 South (strWarora, NC 27806 County Beaufort • Lagoon • Remediation: Infiltration Gallery (City) (State) (Zip) Contact Person: Danny Winstead Telephone#: (252)-322-8283 • Spray Field L1■ Remediation: • Rotary Distributor • Land Application of Sludge Well Location/Site Name: Tank Farm Remediation No. of wells to be sampled: 18 • Water Source Heat Pump • Other: (from Permits _ SAMPLING INFORMATION FIELD ANALYSES: pH 00400: N/A units Temp. 00010: N/A eC If WELL WAS DRY at time of sampling, check WELL ID NUMBER (from Permit): SWW-6 Date sample collected: NIA _ Well Depth: 26.0 ft. Well Diameter: 4 in. Depth to Water Level 82546: NIA ft. below measuring point Screened Interval: 22.25 ft. to 24.62 ft. Spec. Cond. 00094: N/A µMhos Measuring Point is 2.58 ft. above land surface Relative M.P. Elevation: 10.66 ft. Odor 000ss: Volume of water pumped/bailed before sampling: N/A gallons Appearance here: X Samples for metals were collected unfiltered: ■ YES • NO !►I N/A Field acidified: a YES MINO 'A N/A LABORATORY INFORMATION Co. / Environment 1,Inc Certification No. # 330 /# 10 Date sample analyzed: NIA Laboratory Name: PCS Phosphate PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N o0615 N/A mg/L Pb - Lead 01051 NIA ug/L Coliform: MF Fecal 31616 N/A /100mL Nitrate (NO3) as N o0620 N/A mg/L Zn - Zinc Dto92 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 N/A mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Dissolved Solids:Total 70300 N/A mg/L Al - Aluminum 01105 N/A mg/L pH (Lab) 00403 N/A units Ba - Barium 01007 N/A ug/L TOC 00680 N/A mg/L Ca - Calcium 00916 N/A mg/L Chloride 0094o N/A mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils o0552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 N/A ug!L Fe - Iron 01045 N/A u /L g Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? • Yes (1) n No (0) VOC 7873 , method # Specific Conductance 000ss N/A µMhos K - Potassium 00937 N/A mg/L Total Ammonia 00610 N/A mg/L Mg - Magnesium 00927 N/A mg/L , method # (Ammonia Nitrogen; NHsas N; Ammonia Nitrogen, Total) Mn - Mananese 01055 N/A 9 ug/L , method # TKN as N 00625 N/A mg/L Ni - Nickel D1067 N/A ug/L , method # or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A I certify that. to the best of my knowledge and belief, the information submitted in this report is true. accurate. and complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisonment for knowing violations. William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 05-02-2017 Signature of Perm'ttee (or Authorized Agent) -5724Si e z( (Date) Date: Time: Tech: PCS Phosphate�,Co., Inc. - Tank Farm Remediation System Quarterly Monitoring /5/z // c25-1/.44//e/o74,-/1/2 System Gauge Pressures SWW-1 N/A SWW-7 N/A CWW-1 N/A CWW-7 N/A File: 12-07-02 pc: TLB Reference L Point MSL ;vel Rel [o MSL Ditch 12.91 >Jr Barge Slip 10.59 Water Level Control Tank ek = MSL Sand Layer Pelzometers Level Indicators Well ID TOC Elevation MSL' TOC Stc Wtr Level' Level Relative To MSL Ft. Well ID TOC Elevation MSL' TOC Stc Wtr Level' Level Relative To MSL Ft. y Spz-1 10.47 c":1' e X�� Cpz-1 10.51 //0'1/� _ _ Spz-2 11.21 CP• S' ? 6 - Cpz-2 10.25 //'4/ "0 7 Spz-3 11.87 C���• g#' L t b ' Cpz-3 11.12 ,/Q,�J� ®- .6 '7 Spz-4 11.45 '// /0 /� S�5� CPW 9.65 /7;. 9 " / 3/ Spz-5 11.45 r � / �L5 MWTF-1A * 14.35 - .. �S. / /440 Spz-6 11.23 7- 7�r .5 ` -i MWTF-1 B * 14.36 •• �1 /49. 41 Spz-7 11.59 U/-li 1 " `//G MWTF-1C * 14.44 9'---• E/� •,,% ' / Spz-8 11.57 ,,k/e' ecfy - MWTF-2A 14.05 ', 4 4,9 9 Spz-9 11.01 ,5-:-.00 / 9. MWTF-2B 14.02 / .0c(� g 9 / 6 Spz-10 12.16 %' / 5-- �, 14.08 !-„'„ Cn - SPW 9.95 ®/ ��7 G 2- lib' WMWTF-2C MTF-3A 12.21 tom/ •2Z2 GO/ MWTF-3B 12.18 'X O ram -5 W MTF-3C 12.19 /?. 9/ �-7,✓ ' 7s_ Revised 7/29/02 * Riser length added to TOC elevation 1/24/97 D:1Data\Forms\Well Fonn\Tank Farm Remed Wells.xls PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR THE.INJECTION AND WITHDRAWAL WATER WELLS February 2021— April 2021 The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north side of the Tank Farm Area. Infection Water Well System The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system during the period. Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs Department. The total monthly and quarterly volumes of water injected as well as the month end water level in the Water Level Control Tank are: DPW WATER GALLONS TOTAL GALLONS AVERAGE GPM TANK LEVEL FEET, MSL February 245,220 0 245,220 7.1 15.0 March 343,356 0 343,356 7.7 15.0 April 276,031 0 276,031 6.2 15.0 TOTALS 864,581 0 864,581 3 Withdrawal Well System The withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for the period are: SAND FORMATION GALLONS CROATAN FORMATION GALLONS TOTAL GALLONS AVERAGE GPM February 172,628 1,243,475 1,416,103 54.6 March 162,759 872,376 1,035,135 66.3 April 164,121 1,169,300 1,333,421 56.2 TOTALS 499,508 3,285,150 3,874,658 Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning, and troubleshooting on individual pumps in the system were experienced. Details of these activities are: Confined Sand Formation Withdrawal Well (SWW) Pumps SWW- 1: SWW-2: SWW-3: On 3/5 replaced pump. SWW-4: SWW-5: On 3/5 replaced pump. SWW-6: On 2/3 replaced counter. SWW-7: On 2/5 pulled pump. 4 Croatan Formation Withdrawal Well (CWW) Pumps CWW-1: CWW-2: CWW-3: Pump down 15 days in March. Repaired April 1. CWW-4: CWW-5: CWW-6: CWW-7: 5