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NC0027103_NPDES Permit App_20131231
ATA NCDENR North Carolina Department of Environment and Natural Resources Division of Water Resources Pat McCrory Thomas A. Reeder John E. Skvarla, III Governor Director Secretary December 31, 2013 Attn: Marie Moore, Manager Town of Pembroke PO Box 866 Pembroke, NC 28372 Subject: Receipt of permit renewal Permit NC0027103 Robeson County Dear Ms. Moore: The NPDES Unit received your permit renewal application on December 30, 2013. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. If you have any additional questions concerning renewal of the subject permit, please contact Charles Weaver (919) 807-6398. Sincerely, e)1 Wren Thedford Point Source Branch cc: Central Files -Fayetteville-Regional-Office-j NPDES Unit 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 Phone: 919.807-63001 Fax: 919-807-6492JCustomer Service: 1-877-623-6748 Internet:: www.ncwater,orq DENR-FRO JAN 0 6 2013 o Q An Equal OpportunityVAffirmative Action Employer Town of Pembroke POST OFFICE BOX 866 PEMBROKE, NORTH CAROLINA 28372 MILTON R. HUNT MAYOR ORYAN D. LOWRY MANAGER AMIRA HUNT CLERK December 23, 2013 NC Department of Environment and Natural Resources Division of Water Quality/NPDES Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Permitting Unit: COUNCILMEN: LARRY BROOKS ALLEN G. DIAL RYAN SAMPSON E..m.©E•ow DEC 31 2013 DENR-WATER QUALITY POINT SOURCE BRANCH Subject: NPDES Permit Renewal Town of Pembroke NPDES Permit #NC0027103 Robeson County The Town of Pembroke is submitting the renewal application for NPDES permit #NC0027103. The permit application consists of: - Cover letter One original of Form 2A — NPDES Application for Permit Renewal Supplemental Application Information— Parts D & E Topographic Map - Process Flow Schematic Annual Pollutant Scan for the years 2011, 2012, and 2013 - Two copies of Form 2A — NPDES Application for Permit Renewal The Town was unaware that a second species toxicity test was required for the permit renewal. Once we were told of this requirement, we made arrangements to conduct the tests. One second species test has been concluded and the other three are scheduled to be concluded prior to permit expiration. The Town would like to request that the following modifications be made to the permit: - We request that monitoring for BOD, TSS, Ammonia Nitrogen and Fecal Coliform be reduced under the "exceptionally performing facilities" criteria. The attached data (summarized in the following table) indicates that the WWTP effluent has exceeded the minimum criteria for reduced monitoring. In addition to the monitoring results, the plant meets the other listed criteria. Analysis of testing results for the past three years: - Percent of Monthly Average Limit Parameter Monthly Limit 3-Year Average % of Limit BOD5 18.0 mg/L 4.6 mg/L 24% TSS 20.0 mg/L 2.4 mg/L 12% Ammonia N 12.0 mg/L 0.55 mg/L 12% Fecal Coliform 200/100 ml 3 colonies/100 ml 2% - Number of Samples Over 200% of Monthly Avera Parameter 200% of Monthly Limit Number of Samples Over BOD5 36 mg/L 0 TSS 40 mg/L 3 Ammonia N 24.0 mg/L 0 Four (4) Fecal Coliforms exceeded 200% of the weekly average limit It is requested that upstream/downstream monitoring be eliminated. We feel that monitoring the stream for temperature and dissolved oxygen provides no useful data regarding the WWTP impacts upon the receiving waters. Permit limitations are issued to protect water quality, including a minimum effluent dissolved oxygen. "Outside" influences such as stormwater runoff and reduced velocity in the swampy areas that are subject to decay and placid conditions makes taking dissolved oxygen levels and temperatures inconclusive in determining wastewater impacts If second species monitoring is to be continued to be required for permit renewal, we request that one per year be included in the permit. We thank you for your consideration in these matters. If you have any additional questions or comments, please call Rhonda Locklear at 910/521-2989. Sincerely, Marie Moore, Manager Town of Pembroke FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber FORM 2A NPDES APPLICATION OVERVIEW arm 2A''has,-been developed in a modular format and consists of a "Basic Application Information" packe and a "Supplemental Application Information" packet The:Basic Application Information packet is,divide • into two.parts All applicants must;complete Parts A and C :;Applicants with a design flow'greater than'or equal to 01 mgd must also complete Part B Some applicants must also,complete the Supplemental Application Information packet The following items explain'which parts of Form 2A you must complete BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow >_ 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions 6.1 through 6.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (Sills) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b_ Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or c. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber BASIC APR CAT! IINFORMATIQNg y -... ��fi�,rs'�i1?4...`..�1.. ._ Fc".zf= 3q � .. �. �'ti ...3d'':`-. .a. a.,�:�. PART A BAS 0,7,A , Li ATtON': 1FORMA, ,1 OR ALi 4CANTS '4y s All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet. A.1. Facility Information. Facility Name Pembroke WWTP Mailing Address PO Box 866 Contact Person Marie Moore Title Interim Manager Telephone Number (910) 521-9785 Facility Address 8257 Deep Branch Road (not P.O. Box) Pembroke, NC 28372 A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Town of Pembroke Mailing Address PO Box 866 Pembroke, NC 28372 Contact Person Rhonda Locklear Title Wastewater Plant Superintendent Telephone Number (910) 521-2989 Is the applicant the owner or operator (or both) of the treatment works? ® owner ❑ operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. ❑ facility ® applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES NC0027103 PSD UIC Other WQCS0013729 RCRA Other A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership Town of Pembroke 4111 Separate Municipal Total population served 4111 FACILITY NAME AND PERMIT NUMBER: Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber A.5. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes ® No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? ❑ Yes ® No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of this year" occurring no more than three months prior to this application submittal. a. Design flow rate 1.33 mgd Two Years Ago b. Annual average daily flow rate 0.77 c. Maximum daily flow rate 2.38 Last Year This Year 0.84 0.73 1.89 2.66 A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. ® Separate sanitary sewer 100 ❑ Combined storm and sanitary sewer NA % A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes ❑ No If yes, list how many of each of the following types of discharge points the treatment works uses: i. Discharges of treated effluent ii. Discharges of untreated or partially treated effluent iii. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) v. Other b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? ❑ Yes If yes, provide the following for each surface impoundment: Location: NA 1 NA NA NA NA ►1 No Annual average daily volume discharge to surface impoundment(s) NA mgd Is discharge ❑ continuous or ❑ intermittent? c. Does the treatment works land -apply treated wastewater? ❑ Yes ® No If yes, provide the following for each land application site: Location: NA Number of acres: NA Annual average daily volume applied to site: NA mgd Is land application ❑ continuous or ❑ intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? ❑ Yes El No FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber e. If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). If transport is by a party other than the applicant, provide: Transporter Name Mailing Address Contact Person Title Telephone Number ( ) For each treatment works that receives this discharge, provide the following: Name Mailing Address Contact Person Title Telephone Number ( ) If known, provide the NPDES permit number of the treatment works Provide the average daily flow rate from the treatment works into Does the treatment works discharge or dispose of its wastewater in A.8. through A.8.d above (e.g., underground percolation, well If yes, provide the following for each disposal method: that receives this discharge the receiving facility. mgd in a manner not included injection): ❑ Yes ® No Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: Is disposal through this method ❑ continuous or 0 intermittent? FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.B.ago to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number 001 b. Location Pembroke 28372 (City or town, if applicable) (Zip Code) Robeson (County) NC (State) 34'39'55" 79° 12'00" (Latitude) (Longitude) c. Distance from shore (if applicable) NA ft. d. Depth below surface (if applicable) NA ft. e. Average daily flow rate NA mgd f. Does this outfall have either an intermittent or a periodic discharge? ❑ Yes ® No (go to A.9.g.) If yes, provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: mgd Months in which discharge occurs: g. Is outfall equipped with a diffuser? ❑ Yes ® No A.10. Description of Receiving Waters. a. Name of receiving water Lumber River b. Name of watershed (if known) Lumber United States Soil Conservation Service 14-digit watershed code (if known): c. Name of State Management/River Basin (if known): Lumber United States Geological Survey 8-digit hydrologic cataloging unit code (if known): d. Critical low flow of receiving stream (if applicable) acute cfs chronic cfs e. Total hardness of receiving stream at critical low flow (if applicable): mg/I of CaCO3 FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber A.11. Description of Treatment a. What level of treatment ❑ Primary ❑ Advanced b. Indicate the following Design BOD5 Design SS Design P Design N Other c. What type of disinfection Chlorination are provided? Check all that apply. ® Secondary 0 Other. Describe: removal rates (as applicable): removal or Design CBOD5 removal removal removal removal outfall? If disinfection varies 91 % 90 % NA % 60 % % is used for the effluent from this by season, please describe: If disinfection is by chlorination is dechlorination used for this outfall? ® Yes 0 No Does the treatment plant have post aeration? ® Yes 0 No A.12. Effluent Testing Information. parameters. Provide discharged. Do not include All Applicants that the indicated effluent testing information on combined conducted using other appropriate QAIQC data must be based discharge to waters of the US must provide required by the permitting authority sewer overflows in this section. 40 CFR Part 136 methods. In addition, this requirements for standard methods for analytes on at least three samples and must be no effluent testing data for the following for each outfall through which effluent is All information reported must be based on data data must comply with QAJQC requirements of not addressed by 40 CFR Part 136. At a more than four and one-half years apart. collected through analysis 40 CFR Part 136 and minimum, effluent testing Outfall number. 001 ET PARAMER MAXIMUM DAILY7VALUE AVERAGE DAILY VALUE Value Units Value i Unrts =; Number of Samples pH (Minimum) 6.32 s.u. j // pH (Maximum) 7.98 s.u. ° jjj j/ Flow Rate 2.66 MGD 0.73 MGD 365 Temperature (Winter) 19.0 °C 25.9 °C 60 Temperature (Summer) 28.2 °C 17.6 °C 60 ' For pH please report a minimum and a maximum daily value POLLUTANT MAXIMUM DISCHARGE DAILY AVERAGE DAILY DISCHARGE ANALYTICAL METHOD `; MUMDL „. ... Conc. Unrts Conc Unrts Numbers Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN DEMAND (Report one) BOD5 8.3 Mg/L 3.9 Mg/I 72 52106 2.0 CBOD5 FECAL COLIFORM 720 Col/100 ml 4.7 come nil 72 9222D(MF) 1 TOTAL SUSPENDED SOLIDS (TSS) 11.4 Mg/L 3.1 Mg/L 27 2540(D) 1 $ 4 n _ ' -. _ a i } �'' , ?. ,_ `, 3f }j .1-T$ 4END OF PART A, FE..W ICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH.OTHER PARTS J OF FORM,- A; U, MUST COMPL FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber 3 a -ga.... Frxe IO-N BACACATION INFORMAT- .t-¢ . i Y € rc''E`4 ��- PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS$WITH A DESIGN FLOW GREATER THAN OR= . 7 ✓ { i.. F r ,� EQUAL TO 01 MGD (100�000 gallons perday) "• All applicants with a design flow rate >_ 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification). B.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. 10 000 gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. During this permit period, sewer lines have been rehabilitated and manholes have been repaired. There is an on -going Program to identify and repair I&I sources. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within ''/ mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? 0 Yes ® No If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). Name: Mailing Address: Telephone Number. ( ) Responsibilities of Contractor: B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. 0 Yes 0 No FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). d. Provide dates imposed applicable. For improvements applicable. Indicate Implementation Stage - Begin Construction - End Construction - Begin Discharge - Attain Operational e. Have appropriate Describe briefly: by any compliance schedule planned independently dates as accurately as possible. Level permits/clearances conceming other or any actual dates of completion for the implementation steps listed of local, State, or Federal agencies, indicate planned or actual completion Schedule Actual Completion MM/DD/VYYY MM/DD/YYYY below, as dates, as Yes 0 No / / / / / / / / / / / / / / / / Federal/State requirements been obtained? 0 B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD Applicants that discharge to waters of the US must effluent testing required by the permitting authority on combine sewer overflows in this section. All information using 40 CFR Part 136 methods. In addition, this data QA/QC requirements for standard methods for analytes based on at least three pollutant scans and must be Outfall Number. 001 ONLY). provide effluent testing data for the following parameters. Provide for each outfall through which effluent is discharged. Do not include the indicated information conducted other appropriate data must be reported must be based on data collected through analysis must comply with QA/QC requirements of 40 CFR Part 136 and not addressed by 40 CFR Part 136. At a minimum effluent testing no more than four and on -half years old. MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE` ANALYTICAL Y METHOD ML/MDL POLLUTANT ° Conc Units : y Conc Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) 5.2 Mg/I 0.74 Mg/I 72 SM 4500(NH3)F. 0.1 CHLORINE (TOTAL RESIDUAL, TRC) 43 Ug/L 4.0 Ug!L 72 SM 4500(CL2)G 10 DISSOLVED OXYGEN 8.7 Mg/L 8.1 Mg/L 72 SM 4500(0) C. 1 TOTAL KJELDAHL NITROGEN (TKN) 4.23 Mg/I 1.6 Mg/I 6 EPA 351.2 0.5 NITRATE PLUS NITRITE NITROGEN 11.2 Mg/I 5.0 Mg/l 6 EPA 353.2 0.1 OIL and GREASE <5 Mg/I <5 Mg/I 3 1664A 5 PHOSPHORUS (Total) 4.38 Mg/l 1.8 Mg/I 6 EPA 365.2 0.1 TOTAL DISSOLVED SOLIDS (TDS) 200 Mg/L 170 Mg/L 3 SM 2540 C. 10 OTHER _ MRqEFO TIO,OVEW END OF PART B TEETREIGOLNE�WHICH OTst ER PARTS FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber BASIC APp,P,�LICATIONINFOkigRMAT- lO� w Y�g ���A s' ,r.7 § . '—.c`A9g 7 xH�`�$ "i�`-'. . yr2`t'$ r--1,, -�.b y ,� y'? mot`.'"; 3af_ ,��r ,�.r, .1_ rka , r w :,45. �a :,.:w•t .... ,... K ;..yr t'' 4� '_ az ' zri `�m:" ! �.. ;x �•!' 3^�fi ` 1 ' .a�:i !� 9YVM.2 '( _ +-j i -may Y # 4 -- q.�... SLY 1. # ' €' F i - C- ,, ', . ..CERTIFICATI011t- �2 � w �{ sir to ssf.r (r n r _3 hrx° � zrr s ,-„ ta` o,,a d. '. :vY' (N. , ,,,, ,i_,_,.., ,,,. ,, Pft. L.e •R..5 = ..r. `/ M1"`c ti} ... �-w •"ti .n'4`.'nt3::,. I.l}-&Y:..i'., s[6: All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Information packet: ® Part D (Expanded Effluent Testing Data) ® Part E (Toxicity Testing: Biomonitoring Data) ❑ Part F (Industrial User Discharges and RCRA/CERCLA Wastes) ❑ Part G (Combined Sewer Systems) `� yy l-.} , '(,..:,* ice' -ss .g +X a.r 4 'r-v r� W, mkt, 3, A 0 L. x+ , A` i r '�' -4 f_ - P4+ r rs 7u ALL?:APPl:ICANTS II(Ilt)ST GOMPLETEA7HEFOLLOWINGCERTIFICATIOIIt` �,� �.> I certify under penalty of law that this document and all attachments were prepared designed to assure that qualified personnel property gather and evaluate the information manage the system or those persons directly responsible for gathering the information, accurate, and complete. I am aware that there are significant penalties for submitting for knowing violations. Name and official title Mane Moore, Interim Manager under my direction or supervision in accordance with a system submitted. Based on my inquiry of the person or persons who the information is, to the best of my knowledge and belief, true, false information, including the possibility of fine and imprisonment !1 I , Signature L _ YA Q'el_!,. Telephone number (910) 521-9758 - Date signed i 1 — 01%. 3 — / 3 Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. , SEND COMPLETED FORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber SUPPLEMENTAL APPLICATION INFORMATION � �. '. , fi r,as.+ 3 er 4s('"x 7��5„v r ,''. € 3? -. t ,, a ..ro h .R r rr,� fi �-„ r�'7 2t �. . .w,-:.xe �A.x., ..Wp S . ,._4 M.. -tit ;.y. 13. r t .r„. i J. 'r..aq hv._. .�.= ,.4a w„.� Ltl - f .mob xa v r....} ... a,. .-, It mx�ie AK .�'�.?. �1$'u��s�.. ar.`+1'n..'>» PART I EXPANDED EFFLUENT TESTING DATA `*+ _, ,-. T <-< ,�z Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number:001 (Results attached per discussion with NC DWR(Complete once for each outfall discharging effluent to waters of the United States.) `POLLUTANT .MAXIMUM DAILY DISCHARGE : ;AVERAGE DAILY DISCHARGE ANALYTICAL METHOD ML/MDL Conc Units, Mass Units Conc. Units Mass Units Number of Samples METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY ARSENIC BERYLLIUM CADMIUM CHROMIUM COPPER LEAD MERCURY NICKEL SELENIUM SILVER THALLIUM ZINC CYANIDE TOTAL PHENOLIC COMPOUNDS HARDNESS (as CaCO3) Use this space (or a separate sheet) to provide information on other metals requested by the permit writer FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001 (Results attached) (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM,DAILYDISCHARGE Mass VOLATILE ORGANIC COMPOUNDS Units AVERAGE Units Mass Units ACROLEIN ACRYLONITRILE BENZENE BROMOFORM CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMO- METHANE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM DICHLOROBROMO- METHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE TRANS-1,2-DICHLORO- ETHYLENE 1,1-DICHLORO- ETHYLENE 1,2-DICHLOROPROPANE 1,3-DICHLORO- PROPYLENE ETHYLBENZENE METHYL BROMIDE METHYL CHLORIDE METHYLENE CHLORIDE 1,1,2,2-TETRA- CHLOROETHANE TETRACHLORO- ETHYLENE TOLUENE FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number:001 (Results attached) (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE ERAGE DAILY DISCHARGE E{ ANALYTICAL METHOD � ....,�.. MLlMDL __ POLLUTANT Conc Units Mass Units Conc Units Mass Units Number of .Samples 1,1,1- TRICHLOROETHANE 1,1,2- TRICHLOROETHANE TRICHLOROETHYLENE VINYL CHLORIDE Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL 2-CHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 4,6-DINITRO-O-CRESOL 2,4-DINITROPHENOL 2-NITROPHENOL 4-NITROPHENOL PENTACHLOROPHENOL PHENOL 2,4,6- TRICHLOROPHENOL Use this space (or a separate sheet) to provide information on other acid-extractab e compounds reques ed by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE BENZIDINE BENZO(A)ANTHRACENE BENZO(A)PYRENE FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001 (Results attached) (Complete once for each outfall discharging effluent to waters of the United States.) IMUM DAILY DISCHARGE : 3,4 BENZO- FLUORANTHENE ERAGEeDAILY DISCHAR BENZO(GHI)PERYLENE BENZO(K) FLUORANTHENE BIS (2-CHLOROETHOXY) METHANE BIS (2-CHLOROETHYL)- ETHER BIS (2-CHLOROISO- PROPYL) ETHER BIS (2-ETHYLHEXYL) PHTHALATE 4-BROMOPHENYL PHENYL ETHER BUTYL BENZYL PHTHALATE 2-CHLORO- NAPHTHALENE 4-CHLORPHENYL PHENYL ETHER CHRYSENE DI-N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE DIBENZO(A,H) ANTHRACENE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 3,3-DICHLORO- BENZIDINE DIETHYL PHTHALATE DIMETHYL PHTHALATE 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE 1,2-DIPHENYL- HYDRAZINE FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Outfall number: 001 (Results attached) (Complete once for each outfall discharging effluent to waters of the United States.) '*410,i44#;,1-;:01i01400C-; AVERAGE DAILY NIVIVID1_,:'., PO,_ _ , kuITA ' , ' '4-k-' .,,, ..?"--''' E-..-.J. 01*,,,, lYt21':',.:`,;;"3::: ,.„.:„.,;.„:, '''-'''''''!'-':':;; •utift:0--,-,:,::**-: S';',41.4'1.- :;"' Y '- ',---'::;. 1:1;:' -- : Y-;;; ,.,.„ , - ,-- '''-PE14-l'i, 4.:.6,44-t.:'%:;14:„.., .,,.,, .,--(, 6‘,:%`$',- :-C°1*A'''"Vnil:4':-.. ::: .-:f:4;f':_';`,7.,' X' .--.1';:in,: d',,,,,',2K:i, ,,„,.,.:..,r.. N,-.;14--;,.:-,"‘4. Mass f:.':•:7';', :',:.t: f'-'__.'- ''' - '': ';Orifrg''' :"irj:: Number-,---,, '.'' ] -:''',':;;PC':','"2,.T • :44):ill: .,A144yTia*L„,...;:::.-Y,::-..---;_-,--:-:::,, . ' cr .. ,-. r.'-:., - ' rtIF.!-.7‘":1:.:" FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLORO- BUTADIENE HEXACHLOROCYCLO- PENTADIENE HEXACHLOROETHANE INDEN0(1,2,3-CD) PYRENE ISOPHORONE , NAPHTHALENE NITROBENZENE N-NITROSODI-N- PROPYLAMINE N-NITROSODI- METHYLAMINE N-NITROSODI- PHENYLAMINE PHENANTHRENE PYRENE 1,2,4- TRICHLOROBENZENE Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g , pesticides) requested by the permit writer •,‘401-c'';;;--'--,-," TO THE APPLICATJON OF OVERVIEW DETERMINEREFER ,:-.' FORM ' ' - COMPLETEMUST '5Wi'i-'1,f1:Y5f,:;1:,:lwgW=it-Z,,,,:-4k:Z4,'W:,;a1-,0:,.-"A:,,:-AS., FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber ' UPPLEMENTALAPPLICrATION INFORMATION ;l . y. t ..>_ ,... i(, 'Rr'' ,,,, „,.. �¢`5z'ex. "``5'S'U 9Zv7 P43r�i' y ^ !r y�'3 t J l ..k "w Kc 1 '/. e'z"s: - -FY �As✓ �x PART E TOXICiT1F TESTINGrD T�A a!:�1?.t. h„'�-....,t's?,..�^.,.ti .;tit..a t �..'''?, � ., w'X.'S 1�M. POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. . E.1. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. ® chronic 0 acute E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. ' Test number: Test number. Test number. a. Test information. Test Species & test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection ' After disinfection After dechlorination FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Test number: Test number: Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected:, f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water Salt water j. Give the percentage effluent used for all concentrations in the test senes. k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100°% effluent LC50 95°% C.I. % % % Control percent survival % % % Other (describe) FACILITY NAME AND PERMIT NUMBER: Town of Pembroke, NC0027103 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Lumber Chronic: NOEC ICn % % % Control percent survival % % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run (MM/DD/YYYY)? Other (describe) E.3. Toxicity Reduction Evaluation. o Yes ® No Is the treatment works involved in a Toxicity Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted:Per permit requirements. results have been submitted each year in the months of January. April. July, October Summary of results: (see instructions) All biomonitoring have been a "pass". One 2"d species (Fathead Minnow) has been completed and was a "pass" y.. x ,c `s..s h s.�.- 1 9' y 4p�, -.[ ` >cc �,: * -, .:_ i �, ;; s,.� •-i 'A,� € '' r Jet E DO .A .� __ REFER TO T E . PLICATIO OVE VI (PAG 1'j TO ® E ERMIN ICH ()THEPARTS , s OF FORM2'A OF U�MUST _COMPLETE ,`f � 't . W .l s„ ' . , fi,' F' .', "S 'tt "Ra ? i ' 5..{�� �..4_ ,r x.., fi '� `'$ -. v' ?vi ±' 2 Li Attachment Order 2-6: Town of Pembroke NC0027103 Process Flow Diagram Generator Mechanical- —� /Manual Screening__— . Grease.— - removal Pre. - Aeration Influent Flow .83 MGD. Return Activated Sludge Waste Sludge Influent Pump Station Digester Return Line Chlonne Contact Effluent Discharge .83 MGD 1 Y cka i K-brk4lw .: o rrnw 3 rzp h. +c, %SC 14 a • •\ \\--� �' 52 ea Pembroke WWTP - NC0027103 USGS Quad Number: 122 NW Receiving Stream: Lumber River Stream Class: WS-IV B Sw HOW Subbasin: Lumber - 030751 Lat.: 34°39'55" Long.: 79°12'00" r. North j i oke Outfall 001 166 • Lod1 oUt .. `.7bwe;ld. • (33� SCALE 1:24,000 t � -- — - _— _ i -- - r o w t7 Z O D c` c` D T 0 Z O I^ D c` K D K �' m` o Z 0 C^ D c` D„ m` p < C W G �. CU 7 C �* 0CC ,G 7 d a n< ID !C C 3 d a Iv p- c m c in n c rD 3 ro — 3 m In CD m 3 r c cCT s•Cr M En rc p w S N Cr N cr. C N '+ 3 fDID p -t -i ID O rD F. N W �A W 61 W O O N In V Ln co Ol V i� U1 W W W In in W ID 01 U1 ID 00 01 V I--� 00 N N N V W 00 F+ U1 44 in N O N O I -� O W W ID I-. N i(g O 00UlW V PUiLnlDNNN N W ID 00 'CO N W A U1 LD V N LD V V A O 01 A W N N p CO V N N N .p N N N ID ID CO I-. I-. I-. N . LD 0 O1 ID A V CO to F+ O O I-+ O O O O O O O O W� U.) O1 IIDD I- lD W OOj p In W 0 0 O O O O O O O O O V . W IN0 0 + U IN-% op ILD W \ 1� V W N it n V 00 N W 17 W 01 W 00 N 00 61 oO 01 ID .A 00 W 4 N I" 0o N F+ I-� F+ I." I." 1" O O W O 1--� N I-+ N CO N W In Ol Ol W ID I- % W. W W 00 W W N N N W W O1 ID N 01 01 I-. N ID ID ) -� I- ID . W N F, I.a W N I-. I--. {a F+ ID W W I-' 01 CO N O IW-� W 00 01 LA) In 0 U1 In I-+ I-. I-. In 0 ID I--+ U1 O O O O O O O O O O O O O O N 0 0 0 0 b 44N i-+ ID 00 I-. .P W 01 . F. CO W N U7 PPPPPPPPPPPP I-� i-4 N I--+ NJ W N ID V W U7 W I' W lD 00 N F+ W W N U7 A W 4 U7 V1 W A V N 01 V in I-. A I n 01 00 01 V I--. 01 N W 00 V P ID U1 U9 N N N 00 W W !- N N N I--. N ? U1 N 41. V I-. 00 V W W N U7 W In U1 0o 01 W A A LD CO 00 CO 41. W Ol W N 00 N U1 N CO CO .{] N NO co W O A A O O F+ W N O O O F-� O lD W O ID V W W 01 0 0 U7 0 0 0 N i-. W U1 LO N o W A 01 CO Three Year Data Summary - Pembroke NC0027103 Permit No: NC0027103 Outfall: 001 Facility Name: Town of Pembroke Date of Sampling: Analytical Laboratory: Parameter Ammonia (as N) Dissolved Oxygen Nitrate/Nitrite Total Kjeldahl Nitrogen Total Phosphorus Total Dissolved Solids Hardness Chlorine (total residual,TRC) Annual Monitoring and Pollutant Scan 01/06/2011 Town of Pembroke, TBL, ESC, Meritech • Sample Analytical; .Type 1 Method Composite ISM4500-NH3F Grab SM4500-OG Composite 1 9056 Composite EPA. 351.2 Composite 365.1 Composite 1 2540C Composite i 130.1 Oil and Grease Grab 1664A Metals (total recoverable), cyanide and total phenols Antinomy Arsenic Beryllium Cadium Chromium Copper Lead Mercury Mercury Nickel Selenium Silver Thallium Zinc Cyanide Total phenolic compounds Volatile -.organic •compounds Acrolein Acrylonitrile Bromoform Carbon tetrachloride Chlorobenzene Ch lorodibromomethane Chloroethane 2-chloroethylvinyl ether Chloroform Dichlorobromomethane 1,1-dichloroethane 1,2-dichloroethane Trans-1,2-dichloroethylene Form-DMR-PPA-1 Grab SM 4500 CIG Composite Composite Composite Composite Composite Composite Composite Grab Composite Composite Composite Composite Composite Composite Grab Composite Quantitatian. Level 0.1 1.0 0.10 0.1 0.1 10.0 30 10 5.3 200.7 200.7 200:7 200.8 200.7 200.7 200.7 1631 E 245.1 200.7 200.7 200.7 200.8 200.7 4500 CN-E 420.1 0.020 0.020 0.0020 1.0 0.010 0.020 0.0050 1.0 0.00020 0,020 0.020 0.010 0.0200 0.030 0.005 0.040 0.0010 0.0010 0.0050 0.0025 0.0010 0.0010 0.0010 0.0010 Month: January Year. 2011 ORC: Rhonda H.Locklear Phone: (910) 521-2989 Sample,• Result: < 0.10 9.83 0.43 9.30 1.10 150.0 39.0 • 10.0 • 5.3 - Units of Measurement < 0.020 < 0.020 ▪ 0.0020 < 1.0 < 0.010 • 0.020 < 0.0050 < 6.99 0.020 < 0.020 0.010 < 0.0200 0.038 < 0.0050 < 0.040 < 0.050 < 0.010 • 0.0010 < 0.0010 ▪ 0.0010 < 0.0010 < 0.0010 < 0.0050 < 0.050 < 0.0025 < 0.0010 < 0.0010 • 0.0010 0.0010 mg/I mg/I mg/I mg/I mg/I mg/I mg/I ug/I mg/I mg/I mg/I mg/I ug/I mg/1 mg/I mg/I ng/I ng/I mg/I mg/I mg/I mg/I mg/I mgll mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/1 mg/I mg/I mg/I mg/I mg/I mg/I Number of Samples 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Page 1 L_J Permit No: NC0027103 Outfall: 001 Annual Monitoring and Pollutant Scan Month: January S Sample Analytical Quantitation Sample rear. LUI1 Units of Number Parameter Type Method Level Result Measurement of Samples Volat,le:-:organc'compounds(Cont.) 1 1-dichloroeth ., . Y lene 1,2-dichloropropane Grab 624 0.0010 � < 0.0010 � mg/I s: 1 Grab 624 0.0010 < 0.0010 mg/I 1,3-dichloropropylene cis, trans Grab 624 1 0.0010 < 0.0010 Ethylbenzene Grab mg/I 1 624 0.0010 < 0.0010 mg/I Methyl bromide Grab 624 1 Methyl 0.0050 < 0.0050 mgn 1 Chloride Methylene Grab 624 0.0025 < 0.0025 mg/I 1 Chloride Grab 624 0.0050 < 0. mgn 1,1,2,2-tetrachloroethane Grab 624 1 Tetrachloroethylene 0.0010 < 0.00100010 10 mg/I 1 Grab 624 0.0010 < 0.0010 mg/I Toluene 1,1,1-trichtoroethane Grab 624 0.0050 < 0.0050 mg/I 1 1 1,1,2-trichloroethane Grab 624 0.0010 < 0.0010 mg/I 1 Trichloroethylene Grab 624 0.0010 < 0.0010 mg/I 1 Vinyl Chloride Grab 624 0.0010 < 0.0010 mg/I 1 Acid -extractable Grab 624 0.0010 < 0.0010 mg/I 1 compounds p-chloro-m-creso 2-chlorophenol Comp 625 0.010 < 0.010 mg/I 1 2,4-dichlorophenol Comp 625 0.010 < 0.010 mg/I 1 2,4-dimethylphenol Comp 625 0.010 < 0.010 mg/I 1 Comp 625 0.010 < 0.010 4,6-dinitro-o-cresol Comp 625 mg/I 1 2,4-dinitrophenol 0.010 < 0.010 mg/I 1 P henol 2-nitro henol Comp 625 0.010 < 0.010 mg/1 1 p 4-nitrophenol Comp 625 0.010 < 0010 . mg/I Pentachlorophenol Comp 625 0.010 < 0.010 mg/I 1 Phenol Comp 625 0.010 < 0.010 1 2,4,6-trichlorophenol Comp 625 0.010 < 0.010 mg/I 1 Base Comp 625 0.010 < 0.010 mg/I 1 -neutral compounds Acenaphthene Acenaphthylene Comp 625 0.010 < 0.010 mg/I Comp 625 0.010 < 0.010 1 Anthracene Comp 625 m•/I 1 Benzidine 0.010 < 0.010 mg/I Benzo(a)anthracene Comp 625 0.050 < 1 Benzo(a) Comp 625 0.010 < 0.010 mg/I 1 pyrene 3,4-benzofluoranthene Compmg/I 625 0.010 < 0.010 mg/I 1 Benzo(ghi)perylene Comp 625 0.010 < 0.010 mg/I 1 Benzo(k)fluoranthene Comp 625 0.010 < 0.010 mgn 1 Bis(2-cMoroethoxy) Comp 625 0.010 < 0.010 mgn 1 methane Bis(2-chloroethyl) Comp 625 0.010 < mg/I 1 ether Bis(2-chloroisopropyl) Comp0.010 625 0.010 < 0.010 mg/I 1 ether 3is(2-ethylhexyl) Comp 625 0.010 < 0.010 mg/I 1 phthalate 1-bromophenyl Comp625 .010 < 0.010 mg/I 1 phenyl ether 3utyl benzyl Comp 625 0.010 mg/I 1 phthalate ?-Chlorona hthalene Comp0.010 625 0.010 < 0.010 mg/I 1 p 625 0.010 1 I- chlorophenyl phenyl ether Form-DMR-PPA-1 Comp 625 0.010 < 0.010 < 0.010 mg/I mg/I1 1 Page 2 Permit No: NC0027103 Outfall: 001 Parameter Annual Monitoring and Pollutant Scan lummummumu Type Base -neutral compounds (Cont.) Chrysene Di-n-bu 1 •hthalate Di-n-oc I •hthalate Dibenzo a,h anthracene 1,2-dichlorobenzene 1,3-dichlorobenzene 1,4-dichlorobenzene 3, 3-dich lorobenzidine Dieth I •hthalate Dimeth ! • htha(ate 2,4-dinitrotoluene 2,6-dinitrotoluene 1,2-di • hen lh drazine Fluoranthene Fluorene Hexach(orobenzene Hexachlorobutadiene Hexachloroc clo- • entadiene Hexachloroethane Indeno 1,2,3-cd • rene !so. horone Naphthalene Nitrobenzene N-nitrosodi-n-•ro• (amine N-nitrosodimeth 'amine N-nitrosodi• hen famine Phenanthrene P rene 1,2,4,-tichlorobenzene Corn Com Comp Com Com Com Comp Com Com Com Com Com • Comp Com Com Com Com Com Com Com Com Com Com Com Com• Com Com Comp • • • Method 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 625 Quantftation Level 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 Month: January Year: 2011 Sam • le Result 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 Units of mg/I 1 certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibility for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. ! am aware that there are significant penalties for submitting false information, includin the possibility of fines and imprisonment for knowing violations. g Form-DMR-PPA-1 MCDuffle Cummings (Permittee) Authorized Represent Name Signature Number of Samples 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Page 3 Permit No: NC0027103 Outfall: 001 Facility Name: Town of Pembroke Date of Sampling: Annual Monitoring and Pollutant Scan 04/19/2012 TBL ESC Meritech Month: April Year: 2012 ORC: Rhonda H.Locklear Phone: (910) 521-2989 Analytical Laboratory:i own or r•ernbroke J Y4C ic= + s.®. » 4.4 f3 w1:,p p,0 b ofilif om i ES 6a imatitigi �''f p,Ifz a I I,.Px" ,,,61ampiw � =�,� hY j�G4 • .4- t . 't at 7L J.6t`„1 ,; 1J' 1pAY, ,S3W31 y;I ,..,, b ^ Yy �1Mf1fV SU C> t . ,Gff 5CC ::. 7t u[ili'} v, ri Sqmg 1^, r„t, IFA�ys9 W ch,_,e�,f � ; Ammonia (as N) Composite SM4500-NH3F 0.1 0.63 mg/I . 1 Dissolved Oxygen Grab SM4500-OG 1.0 8.10 mg/I 1 Nitrate/Nitrite Composite 9056 0.10 11.00 mg/I 1 Total Keldahi Nitrogen Composite EPA. 351.2 0.1 1.90 mg/I 1 Total Phosphorus Composite 365.1 0.1 1.10 mg/I 1 Total Dissolved Solids Composite 2540C 10.0 200.0 mg/I 1 Hardness Composite 130.1 30 37.0 mg/I 1 Chlorine (total residual,TRC) 'Grab • SM 4500 CIG 10 10.0 ug/I 1 Oil and Grease Grab,-r16 64A 5.3 53 mg/I 1 1 tart _vim.a rGvcbe sS,WW, t,*,AVi iy ar e„a.lrirr4; . lW's f /. fiS1,7 buf0, Y�� rie t . Antinomy Composite 200.7 0.020 < 0.020 mg/I 1 Arsenic Composite 200.7 0.020 < 0.020 mg/I 1 Beryllium Composite 200:7 0.0020 < 0.0020 mgll 1 Cadium Composite 200.8 1.0 < 1.0 ug/l 1 Chromium Composite 200.7 0.010 < 0.010 mg/I 1 Copper Composite 200.7 0.020 < 0.020 mg/I 1 Lead Composite 200.7 0.0050 < 0.0050 mg/I 1 Mercury Grab 1631 E 1.0 < 6.99 ng/I 1 Mercury Composite 245.1 0.00020 7.3 ngll 1 ,Nickel Composite 200.7 0.020 < 0.020 mg/I 1 'Selenium Composite 200.7 0.020 < 0.020 mgll 1 Silver Composite 200.7 0.010 < 0.010 mg/I 1 Thallium Composite 200.8 0.0200 < 0.0200 mg/I 1 Zinc Composite 200.7 0.030 0.081 mg/I 1 Cyanide Grab 4500 CN-E 0.005 < 0.0050 mg/I 1 Total phenolic compounds Composite 420.1 0.040 < 0.040 mg/I 1 rrr r yrJ'rrt art,O iti C© 0,..,.isu< �: �. �. .f. : ..._F!+.,.. f. sit 1' ,_, .. )) .:. ..:� "it t �. i u� a� �{^_..,x ,♦I r5 .:: ..( r, I 1 J. �. f t. ., r�Y St f.H :. r, .:^r � t _...r k S r r t F ti I ��,f ....a...., r, .,>tia:;. �nl 5� fy tmrhl, �,+-� u r,�n �s�II r h4 ,.x; � I{: �A.. is ,��4 r r r s,,� +; e�M Al�, Tq.v.:I. tt. ty Acrolein Grab 624 0.050 < 0.050 mg/I 1 Acrylonitrile Grab 624 0.010 < 0.010 mg/I 1 Benzene Grab 624 0.0010 : < 0.0010 mg/I 1 Bromoform Grab 624 0.0010 < 0.0010 mg/I 1 Carbon tetrachloride Grab 624 0.0010 < 0.0010 mg/I 1 •Chlorobenzene Grab 624 0.0010 < 0.0010 mg/I 1 Chlorodibromomethane Grab 624 0.0010 < 0.0010 mgll 1 :Chloroethane Grab 624 0.0050 < 0.0050 mg/I 1 2-chloroethylvinyl ether Grab 624 0.050 < 0.050 mg/I 1 Chloroform Grab 624 0.0025 < 0.0025 mg/I 1 Dichlorobromomethane Grab 624 0.0010 < 0.0010 mg/I 1 1,1-dichloroethane Grab 624 0.0010 < 0.0010 mg/I 1 1,2-dichloroethane Grab 624 0.0010 , < 0.0010 mg/I 1 Trans-1,2-dichloroethylene Grab 624 0.0010 < 0.0010 mg/I 1 Form-DMR-PPA-1 Page 1 r• Annual Monitoring and Pollutant Scan Permit No: NC0027103 Month: April Year: 2012 Outfall: 001 S Sample analytical Quantiiation Sample Units of Number of Type T e Method Level Result Measurement Samples n. NiAilatil�'giOni rl.#10 1•j '.....(940 `l��r .rn?' N S t � as �';."1:4 7'.a. , kp:: 1 p16v41.;'�efzai,; 0.0010 :.. yr,',+,,,r,,q �i,,,,,T. r' W7,,, ,g{,4. )v�N,M,k` `i:'t,G.JA14`,I,r;,j trr < 0.0010 mg/I 1 1,1-dichloraet%yiene Grab 624 1,2-dichloropropane Grab 624 0,0010 < 0.0010 mg/I 1 1,3-dichloropropylene cis, trans Grab 624 0.0010 < 0.0010 mgll 1 Ethylbenzene Grab 624 0.0010 < 0.0010 mg/I 1 Methyl bromide Grab 624 0,0050 < 0.0050 mg/I 1 Methyl Chloride Grab 624 0.0025 < 0.0025 mgll 1 Methylene Chloride Grab 624 0.0050 < 0.0050 mg/I 1 1,1,2,2-tetrachloroethane Grab 624 0.0010 < 0.0010 mg/I 1 Tetrachloroethylene Grab 624 0.0010 < 0.0010 mg/I 1 Toluene Grab 624 0.0050 < 0.0050 mg/I 1 .1,1,1-trichloroethane Grab 624 0.0010 < 0.0010 mg/I 1 1,1,2-trichloroethane Grab 624 0.0010 < 0.0010 mg/I 1 Trichloroethylene Grab 624 0.0010 < 0.0010 mg/I 1 Vinyl�ChlorideJJ Grab 624 0.0010 < 0,0010 mg/1 1{ , y� y' 1 liill54Kti4',34WL� ��Co# 01011f�3}� , t 1, 'v , ..,,;G•.r ra t+,.e:: �t f �. , ,� .i.. C w h o-)?,� t'1i r�,aV ,.�,. f•� l ri, '�,:;ai )r, o., t:-;2 i, ,, , ,dial o..4- .�t.�. i x ,,,,:.**,,),,,,,,,,,,.:4ag p-chfaro-rn-creso Comp 625 0,010 < 0.010 mg/I 1. 2-chlorophenol Comp 625 0.010 < 0.010 mgll 1 2,4-dichlorophenol Comp 625 0.010 < 0.010 mgll 1 2,4-dimethylphenol Comp 625 0.010 < 0.010 mg/I 1 4,6-dinitro-o-cresol Comp 625 0.010 < 0.010 mg/l 1 2,4-dinitrophenol Comp 625 0.010 < 0.010 mg/I 1 2-nitrophenol Comp 625 0.010 < 0.010 mg/I 1 4-nitrophenol Comp 625 0.010 < 0.010 mg/I ' 1 I( Pentachlorophenol Comp 625 0.010 < 0.010 mg/I 1 Phenol Comp 625 0.010 < 0.010 mg/I 1 2,4,6-trichloro�phenrol Comp 625 0.010 < 0.010 mg/I (: 1 C�'^7I ..-rigi'Itr 7ifi ui�sr P.v�?.3�bo.�,w, .'�-a<•.�r,���.��,..,....,-..t.��„�,th..,- 1f(.�As. )S I� Sl,rit .�, r, !'fo IiarriiAh rd <t"�n,,.,,, _�!,� �.� i 5',y, ,,,flaw,“ .,mlt..�.1 .....v a.vl�.t 4fY.�:� iiV ,.� „+ i.n. h40 w.� "� 6 Fug? I�Y1, hU�n(yN)Cd ((.^1,-; ,.��� �„ '� .. r�. 3 h }�,n'.�d i7 S3iNq 5., �I"d�i .r Acenaphthene Comp 625 0,010 < 0.010 mgA 1 Acenaphthylene Comp 625 0.010 < 0.010 mgA 1 Anthracene Comp 625 0.010 < 0.010 mg/I 1 Benzidine Comp 625 0.050 < 0.050 mg/I 1 Benzo(a)anthracene Comp 625 0.010 < 0.010 mg/I 1 Benzo(a) pyrene Comp 625 0.010 < 0.010 mg/I 1 3,4-benzofluoranthene Comp 625 0.010 < 0.010 mg/I 1 Benzo(ghi)perylene Comp 625 0,010 < 0.010 mg/I 1 Benzo(k)fluoranthene Comp 625 0.010 < 0.010 mg/I 1 t, Bis(2-chloroethoxy) methane Comp 625 0.010 < 0.010 mg/I 1 Bis(2-chloroethyl) ether Comp 625 0.010 < 0.010 mg/1 1 Bis(2-chloroisopropyl) ether Comp 625 0.010 < 0,010 mg/I 1 Bis(2-ethylhexyl) phthalate Comp 625 0.010 < 0.010 mg/I 1 4bromophenyl phenyl ether Comp 625 0.010 < 0.010 mg/I 1 Butyl benzyl phthalate Comp 625 0.010 < 0.010 mgA 1 2-Chloronaphthalene Comp 625 0.010 < 0.010 mg/I 1 4- chlorophenyl phenyl ether Comp 625 0.010 < 0.010 mg/I 1 orm-D M R-PPA-1 Page 2 Annual Monitoring and Pollutant Scan Permit No: NC0027103 • Month: April Year: 2012 JULIdU. UU 1 Sample Analytical Quantitation Sample Units. of Number of Parameter Type Method Level Result easuremei Samples y� yJj A etrt'aF iaYCCbci'p Ijl. A .n . -.. n ��� .7 ......,,.-�n.,��at , _ t � � .���lt�l�' , v � Cornp l -df,� ('.. } �1. i � 5Ib} /L btt .. tM1Ftt414. i{ �„� t � I .. �i , ., )I, �.Y �i t �.i M,�(y{.'d� t�l��l k .*i 4 N ` , F � 6k�� 1 � ? I?.i'�M .. �i v"�17:4 -0. {.^ E< !`'W � 1 . p Yi! ,'3 S(;i .s.Jr i ff �'Mi^�tXi t, .�tl%f�(�(: f- .,r..:.. Cltrysene W 625 0.010 < 0.010 rnglt 1 Di-n-butyl phthalate Comp 625 0.010 < 0.010 mg/I 1 Di-n-octyl phthalate Comp 625 0.010 < 0.010 mg/I 1 Dibenzo(a,h)anthracene Comp 625 0,010 < 0.010 mg/I 1 1,2-dichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 4 1,3-dichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 1,4-dichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 3,3-dichiorobenzidine Comp 625 0.010 < 0.010 mg/I 1 ,Diethyl phthalate Comp 625 0.010 < 0.010 mg/I 1 Dimethyl phthalate Comp 625 0.010 < 0.010 mg/1 1 2,4-dinitrototuene Comp 625 0.010 < 0.010 mg/I 1 2,6-dinitrotoluene Comp 625 0.010 < 0.010 mg/I 1 1,2-diphenylhydrazine Comp 625 0.010 < 0.010 mg/1 1 'Fluoranthene Comp 625 0.010 < 0.010 mg/I 1 Fluorene Comp 625 0.010 < 0.010 mg/I 1 !Hexachlorobenzene Comp 625 0.010 < 0.010 mg/I 1 Hexachlorobutadiene Comp 625 0.010 < 0,010 mg/1 1 Hexachlorocyclo-pentadiene Comp 625 0.010 < 0.010 mg/I 1 Hexachloroethane Comp 625 0.010 < 0.010 rng/I 1 Indeno(1,2,3-cd)pyrene Comp 625 0.010 < 0.010 mg/I 1 ,Isophorone Comp 625 0.010 < 0.010 mg/I ' 1 Naphthalene Comp 625 0.010 < 0.010 mg/I 1 Nitrobenzene Comp 625 0.010 < 0.010 mg/I 1 'N-nitrosodi-n-propylamine Comp 625 0.010 < 0.010 mg/I 1 ;N-nitrosodimethylamine Comp 625 0.010 < 0.010 mg/I 1 :N-nitrosodiphenylamine Comp 625 0.010 < 0.010 mg/I 1 Phenanthrene Comp 625 0.010 < 0.010 mg/I 1 Pyrene Comp 625 0.010 < 0.010 mg/I 1 1,2,4,-trichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibility for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Maire Moore (Permittee) Authorized Representative Name Nit*10 Signature Form-DMR-PPA-1 Page 3 | Permit No: mon027103 Facility Name: Town ofPembroke Date of Sampling: Analytical Laboratory: Annual Monitoring and Pollutant Scan o4ne/2u1u Town mPembroke, TaL, ESm Month: April Year: 2013 ORC: Rhonda H.Locklear Ammonia (aom) Composite anw*500-NM3r 0.1 9.80 mQ0 1 Dissolved Oxygen Grab Sm4*00-oo 1.0 8.70 mg0 1 Nitrate/Nitrite Composite 9056 �� � o80 mgU 1 Total KjomamNitrogen _ Composite sPA.as1.o 01 1.2.00 mox � Total Phosphorus Composite 365.1 uA 0.93 mox 1 Total Dissolved Solids Composite oo*oc 10.0 160.0 mux � Hardness omnpvuuo 1301 on 39.0 mu/l � Chlorine (total moiuua|.TgC) Grab oM *580o\G. 25 < 25.0 u0/| Oil and Grease Grab 1664A 5.0 < 5.0 'n08 � Andnamy Composite 2007 0.028 < 0.820 mg8 1 amonio oamn000a 200.7 0.020 < 0.020 nnn/| � Beryllium Composite uouJ 0.0020 < 0.0020 mox � Cauium Composite 200.8 1.0 < to ug8 � Chromium Composite 280J 0.010 « 0\01:0 mg8 � Copper Composite 200.7 0.020 < o-000 mo/| � b,ao Composite 2007 0.0050 < 0.0050 mg0 � Mercury Gn,u 1631s 0.5 3.03 ng8 1 Mercury Composite 245./ um} oo |« u.808e0 m0/l � w/cm,/ Composite 200.7 0.020 < 0.020 mox � Selenium Composite 200.7 0.020 < 0.020 mg0 1 Gi|,a, Composite 200.7 . 0.010 < 0D10 mo0 1 Txumum composite 200.8 0z200 x 0-0200 mux � Zinc Composite uouJ 0`030 0.048 mo0 1 Cyanide emu 4500cw`s 0.005 x 0.0050 mo/l � Total phenolic compounds Composite 420.1 0.040 ^ 0.040 m8/| 1 . acmlein Grab 824 8.050 < 0.858 mgN 1 acrymnxmo m,ou 624 0.010 < 0.010 mg8 1 . Benzene Grab 624 0-0010 « 0.0010 mox � ommmonn Grab 62* 0`0010 ^ 0.0010 mgx � Carbon tetrachloride Grab 824 0.0010 < 0.0010 m0/i 1 omomuanzaoo emu e24 0u010 " 0.0010, mox Omnmdibmmomethooe Grab 824 0.0010 < 8.0010 mg/| 1 � cxmmemano Grab 624 0.0050 ^ unoso mox '2'cNomsuhylvinylaLhor Grab 624 OO�0 � � 0O5� ' m0� 1 ' ohmmfonn Grob 824 0.8025 < ' 0.0025 mg0 1 ` oioh|nmummometxane Grab 624 0.0010 < 0.0010 mg8 1 '1.1'd/oh|omothane Grab 624 0.0010 < 0.0010 mg8 � 1.2-mcx|onoethane mrou 624 0o010 < 0.0010 mox � _ Trans'1.2-ummiomenv�ne ~"="'..""~`"""^ emu n�* uoo1u .mu0 � 0.0010 � Annual Monitoring and Pollutant Scan Permit No: NC0027103 Outfatl: 001 Month: April Year: 2013 Sample Analytical Quantitation Sample Units of Number of Parameter Type Method Level Result Measurement Samples Volatile;org0.1,:0001prounds,(CoMA . ;; �k ;r', ..r; r?; ,.._.,. ` ,` ' „,,A, .ti, {ym, ' `{ 4 ,r 1,1-dichloroethylene :Grab 624 0.0010 • < 0.0010 mg/I 1 1,2-dichloropropane Grab 624 0.0010 < 0.0010 mg/I 1 1,3-dichloropropylene cis, trans Grab 624 0.0010 < . 0.0010 mg/I 1 Ethylbenzene Grab 624 0.0010 < 0.0010 mg/I 1 Methyl bromide Grab 624 0.0050 < 0.0050 mg/I 1 Methyl Chloride Grab 624 0.0025 < 0.0025 mg/I 1 Methylene Chloride Grab 624 0.0050 < 0.0050 mg/I 1 1,1,2,2-tetrachloroethane :Grab 624 0.0010 < 0.0010 mg/I 1 Tetrachloroethylene Grab 624 0.0010 < 0.0010 mg/I 1 Toluene Grab 624 0.0050 < 0.0050 mg/I 1 1,1,1-trichloroethane Grab 624 0.0010 < 0.0010 mg/I 1 1,1,2-trichloroethane Grab 624 0.0010 < 0.0010 mg/I 1 Trichloroethylene Grab 624 0.0010 < 0.0010 mg/1 1 Vinyl Chloride Grab 624 0.0010 < 0.0010 mg/I 1 hcid-extractabl0 Gbmpotthdsk sr a k, . !Yrr, , 3 ;'' . , t, . i,+: a, " 4.. ,' *.t . , `. .; p-chloro-m-creso Comp 625 0.010 < 0.010 mg/I 1 2-chiorophenol Comp 625 0.010 < 0.010 mg/I 1 2,4-dichlorophenol Comp 625 0.010 < 0.010 mg/I 1 2,4-dimethylphenol Comp 625 0.010 < 0.010 mg/I 1 4,6-dinitro-o-cresol Comp 625 0.010 < 0.010 mg/I 1 2,4-dinitrophenol Comp 625 0.010 < 0.01•0 mg/I 1 2-nitrophenol Comp 625 0.010 < 0.010 mg/I 1 4-nitrophenol Comp 625 0.010 < 0.010 mg/I 1 Pentachlorophenol Comp 625 - 0.010 < 0.010 mg/I 1 Phenol Comp 625 ' 0.010 < 0.010 mg/I 1 2,4,6-trichlorophenol Comp 625 0.010 < 0.010 mg/I 1 .` "Base -neutral c k 7:0nds, t1 ; f :g' Grr 1,...-,,r si;r...,. 1{, , '' 1 n y{:: f n }S Acenaphthene Comp • 625 0.010 < 0.010 mg/I 1 Acenaphthylene Comp 625 0.010 < 0.010 mg/1 1 Anthracene Comp 625 0.010 < 0.010 mg/I 1 Benzidine Comp 625 0.050 < 0.050 mg/I 1 Benzo(a)anthracene Comp 625 0.010 < 0.010 mg/I 1 Benzo(a) pyrene Comp 625 0.010 < -0.010 mg/I 1 3,4-benzofluoranthene Comp 625 0.010 < 0.010 mg/I 1 Benzo(ghi)perylene Comp 625 0.010 < 0.010 mg/I 1 Benzo(k)fluoranthene Comp 625 0.010 < 0.010 mg/I 1 Bis(2-chloroethoxy) methane Comp 625 0.010 < 0.010 mg/I 1 Bis(2-chloroethyl). ether Comp 625 0.010 < 0.010 mg/I 1 Bis(2-chloroisopropyl), ether Comp 625 0.010 < 0.010 mg/I. 1 Bis(2-ethylhexyl) phthalate Comp 625 0.010 < 0.010 mg/I 1 4-bromophenyl phenyl ether Comp 625 0.010 < 0,010 mg/1 1 Butyl benzyl phthalate Comp 625 0.010 < 0.010 mg/1 1 2-Chloronaphthalene Comp 625 0.010 < 0.010 . mg/I 1. 4- chlorophenyl phenyl ether Gnrm_r111/10_DDA d Comp 625 0.010 < 0.010 mg/1 1 Page 2 Annual Monitoring and Pollutant Scan Permit No: NC0027103 Outfall: 001 Month: April V....... Sample Analytical Quantitation Sample Units of Number of Parameter Type Method Level Result leasuremei Samples Base -neutral coat; ounds :(,c ..,. . ..�._ �..,,... ... ,. ontsl. , j ,.i `r '..,v , .' , � a_ .{s. , , , �<, os= ., i,� , } s � ;. < ,e��{.0 4 {h,' F ..[ 7wi ._ ., r.,� sue. '���� ,v .. :_tea h.,Asy Chrysene Comp 625 0.010 < 0.010 mg/I 1 Di-n-butyl phthalate Comp 625 0.010 < 0.010' mg/1 1 Di-n-octyl phthalate Comp 625 0.010 < 0.010 mg/I 1 Dibenzo(a,h)anthracene Comp 625 0.010 < 0.010 mg/I 1 1,2-dichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 1,3-dichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 1,4-dichlorobenzene Comp 625 0.010 < 0.010 mg/I 1 3,3-dichlorobenzidine Comp 625 0.010 < 0.010 mg/I 1 Diethyl phthalate Comp 625 0.010 < 0.010 mg/I 1 Dimethyl phthalate Comp 625 0.010 < 0.010 mg/I 1 2,4-dinitrotoluene Comp 625 0.010 < 0.010 mg/I 1 2,6-dinitrotoluene Comp 625 0.010 < 0.010 mg/I 1 1,2-diphenylhydrazine Comp 625 0.010 < 0.010 mg/I 1 'Fluoranthene Comp 625 0.010 < 0.010 mg/I 1 Fluorene Comp 625 0.010 < 0.010 mg/I 1 Hexachlorobenzene Comp 625 0.010 < 0.010 mg/I 1 Hexachiorobutadiene Comp 625 0.010 < 0.010 mg/I 1 Hexachlorocyclo-pentadiene Comp 625 0.010 < 0.010 mg/I 1 Hexachloroethane Comp 625 0.010 < 0.010 mg/I 1 Indeno(1,2,3-cd)pyrene Comp 625 0.010 < 0.010 mg/I 1 Isophorone Comp 625 0.010 < 0.010 mg/I 1 Naphthalene Comp 625 0.010 < 0.010 mg/I 1 Nitrobenzene Comp 625 0.010 < 0.010 mg/I 1 N-nitrosodi-n-propylamine Comp 625 0.010 < 0.010 mg/I 1 N-nitrosodimethylamine Comp 625 0.010 < 0.010 mg/I 1 N-nitrosodiphenylamine Comp 625 0.010 < 0.010 mg/I 1 Phenanthrene Comp 625 0.010 < 0.010 mg/I 1 Pyrene Comp 625 0.010 < 0.010 mg/I 1 1,2,4,-trichlorobenzene Comp _ 625 0.010 < 0.010 mg/I 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibility for gathering the information, the information submitted is,. to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Oryan D. Lowry (Perrnittee) Authorized Representative Name Lure Form-DMR-PPA-1 Page 3