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HomeMy WebLinkAboutWQ0000543_Modification_20210924Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0000543 Applicant/Permittee City of Sanford Applicant/Permittee Address 5327 Iron Furnace Rd, Sanford, NC 27330 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Municipal Facility Name City of Sanford RLAP County Lee Fee Category Major Fee Amount $395 Is this a complete application?* r Yes r No Complete App Date 09/24/2021 Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd .......................................................... ronc su_ - Name * Chris Wynne Email Address* cwynne@synagro.com Project Information ........ ......... .......................................................................................................................................... Application/Document Type* r New (Fee Req ui red) c Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 13369098627 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WO0000543 Fbs Current Existing permt number Applicant/Permittee * City of Sanford Applicant/Permittee Address* 5327 Iron Furnace Rd, Sanford, NC 27330 Facility Name * City of Sanford RLAP Please provide comments/notes on your current submittal below. Find attached all required documentation to increase the permitted dry tonnage for Big Buffalo WWTP. Let me know if you have any questions or concerns. Thanks for your time. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) WQ0000543 mod ification_09242021.pdf 36.69MB Woad only 1 RCFdocurrent (less than 250 W). IvLfliple documents nest be corrbined into one RJFfile unless file is larger than upload limit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 9/24/2021 SYNAGRO YOUK Ph.ATNLR FOR A CLEANER, CiR1,F,-_?YERN0K0 09/24/2021 NCDENR-DWQ Division of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 ATTENTION: Mr. Nathaniel Thornburg REFERENCE: MODIFICATION OF PERMIT NO. W00000543 City of Sanford Dear Mr. Thornburg, Synagro is submitting, on behalf of the City of Sanford, an application to modify the residuals land application permit. Listed below are the changes to the existing permit: )> Increasing permitted dry tonnage from 1000 dry tons/yearto 1500 dry tons/year No other modification to the permit is requested at this time. If you have any questions or concerns about this modification, contact me at 336-909-8627. 1 look forward to working with you to ensure that this is an efficient review process. Sincerely, Chris Wy e Technical Services Specialist Cc: Scott Siletzky; City of Sanford Enc: Application Package (4) State of ► Carolina Department of ► cnmental Quality PW Division of ► Division of Water Resources .:.. NCAC. . APPLICATION . INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Aron-Discha e Permitti Unit General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .11.00. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A, NCAC 027' .W 06 U . An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .010�(b�. If this project is for a modification of an existing permit, submit one copy of the existing permit. Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages ,involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification i Major (land are permitted for > 300 acres) $1,310 $395 Minor (land are permitted for < 300 acres) $810 $245 I - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) ED List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (May be Required — See 15A NCAC I C ..03Ci0) E Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Paget of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. 0 Submit the O&M Plan in accordance with 15A NCAC 02'i�.1110 and include at a minimum: Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. Maintenance schedules; may include equipment calibration, maintenance of signs, etc. 0 Safety measures; may include safety training program, manuals, signs, etc. 0 Spill response plan; including control, containment, remediation, emergency contact information, etc. { Inspection plan including the following information; Names and titles of personnel responsible for conducting the inspections. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. 0 Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. Fj Sampling and monitoring plan including the following information; M Names and titles of personnel responsible for conducting the sampling and monitoring. 0 Detailed description of monitoring procedures including parameters to be monitored. 0 Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination 0 Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T �1102(. Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. El Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. 0 Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. [] Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information El Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) Submit three (3) sets of standard size plans and two (2) sets of I V by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. 0 Plans must include the following minimum items: 0 A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). Delineation of the review and compliance boundaries Setbacks as required by 15A NCAC 02T .1108 Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. 0 Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 1. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) F-1 Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) F-1 Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T . I 104Ldl U4 and current Division Policy available at: hjtRL//wwwaicwa_(enor & es t gau ions4. The document shall be signed, sealed and dated by a -1h_ J�olicies 4EL(Relqt qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) FJ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T 1.1 lk4Ld)f2). For Modifications, submit an updated site map specific to the modification(s) only. 0 The design documents must include the following minimum items: Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; fl Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) F] Submit a completed and accurate water balance in accordance with 15A NCAC 02T 3 104fdU5 and current Division Policy available at: h1M-�.//wAw.ncweq r org/Rules Policies and Re ulatio h1M-//www.ncweq g_n�z. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) Property ownership documentation shall consist of one of the following: n Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or An easement running with the land specifically indicating the intended use of the property and meeting the requirements of 15A NCAC 02L0107(D, or A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ILI U W a] 'AN I k' I -a 10 1 X I I h"40i F-1 N (1161F 'T Iffim, , . OIL 11041110 F. A 101 % is . KUM I I I I I 14raskm r JOL I N 0 "M y so I a all) IN IN]"IM 0 TT-4-A-f WU- =tFumm- DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM; RLAP 06-16 Page 3 of 3 State of North Department of EnvironmentalQuall Division of Water Resoure Division of Water Resources 15A NCAC 02T.1100 — RESIDUALS LAND APPLICATION PROGRA O. .LAP 16'r 1. Applicant's name: City of Sanford Applicant type: Q Individual ❑ Corporation ( General Partnership Q Privately -Owned Public Utility El Federal Q State Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Hal Heg_wer Title: City Manager Applicant's mailing address: PO Box 3729 City: Sanford State: NC Zip: 27331 Telephone number: (919) 775-8202 Email Address: hal.hegwergsanfordnc.net 2. Consultant's name: Christopher Wynne License Number (for P.E.): Affiliation: M On Staff Q Retained (Firm: ) Consultant's mailing address: 284 Boger Rd City: Mocksville State: NC Zip: 27028- Telephone number: (336) 909-8627 o.com Email Address: gw e@synagro.co 3. Agronomist's name: License Number: Affiliation: Q N/A 0 On Staff F ; Retained (Firm: ) Agronomist's mailing address: City: State: Zip: Telephone number: Email Address: 4. Soil Scientist's name: License Number: Affiliation: ❑ N/A Q On Staff [] Retained (Firm: ) Soil Scientist's mailing address: City: State: Zip: - Telephone number: (_) Email Address: 5. Fee submitted: $395.00 (See Instruction B) 1. Application is for (check all that apply): Q new, S modified, Q renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00000543 Date of most -recently issued permit: 1/14/2019 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 1. Residuals Processing Facility's physical address: 5327 Iron Furnace Rd City: Sanford State: NC Zip: 27331 Coordinates: Latitude: 35' 32' 47.25" Longitude: 790 13' 10.22" Datum: NAD 84 Level of accuracy: Second Method of measurement: Man 2. County where residuals land application program is headquartered: Chatham 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Robert N. Roth Synagro 1001672 Back -Up ORC John A. Culp Synagro 1000733 Additional Back -Up ORCs if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Sumarwr Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 1500 dry tons per year. PAN Pounds of PAN per Dry Ton Pounds of PAN per Year (Weighted Average) Surface Incorporation Surface Incorporation or Injection or Injection First -Year 23.01 30.61 34509 45909 Five -Year Maximum Adjusted 32.92 40.52 49375 60775 b. Land Ayplieation Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation 0 Row Crops 0 Hay 96.17 Pasture 732.08 Total: 828.25 Methods Surface 828.25 Incorporation or Injection 0 Total: 828.25 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land An lication Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Acres Required Using Acres Required Using Application Rate First -Year PAN Concentrations Five -Year Maximum Adjusted PAN (lbs PAN/ac yr) Concentrations Surface Incorporation or Surface Incorporation or Injection Injection 50 690.2 918.2 987.5 1215.5 100 345.1 459.1 493.7 607.7 150 230.1 306.1 329.2 405.2 200 172.5 229.5 246.9 303.9 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): ENon-dedicated [] Dedicated If Dedicated, specify the following (check all that apply): [] Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; El Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. a Land Application Siite Certification. doc FORM: RLAP 06-16 Page 3 of 5 Note: Item V1. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM I . The irrigation system is: [:] Spray [3 Drip 2. Disposal system is: [] existing ❑ proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T,05Q5requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? 1:1 Yes or [I No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate (in/hr) Recommended Loading Rate in/ r 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? r_1 Yes or R No If No, explain why 15A NCAC 021.OL05Ln) is not met: 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameter of nozzles ft Wetted area of nozzles ft2 Nozzle capacity gpM Nozzle manufacturer / model Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. M; Yes ❑ No, Explain; I, Hal Hegwer City Manager (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Sanford WWTP (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, andfor criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.68, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Z Signature: Date: FORM: RLAP 06-16 Page 5 of 5 State of North Carolina num RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two Copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non-DischaiXe PermitliLg Jni4 General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02 ' T.1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCA R 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11 - 15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "MQ_Guidance for Residuals -Lan i A. Liggitiga rnits". L--M — _Eq�L_ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: For each source facility, attach the following: Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 A O m vi � b o � O Uo 0 m b P� e C O �C o o pw° � O � w a CD Ci � O O � to �. o C � b O b e t p "s o � D, W��,�_ North FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: City of Sanford 2. Facility permit holder is: Federal, 0 State, 0 Local Government, or Q Private. Facility permit issued by: Div. of Water Resources, 0 Div. of Environmental Health, or Other (explain: `% ). 3. Facility contact person and title: Scott Siletzky, Water Reclamation Administrator Complete mailing address: PO Box 3729 City: Sanford State: NC Zip: 27331- Telephone number: (919) 777-1781 E-mail address: scott.silei&y@sanfordnc.net 4. Facility physical address: 5327 Iron Furnace Rd City: Sanford State: NC Zip: 27331_""' Coordinates: Latitude: 35' 32' 47.25" Longitude: 79' 13' 10.22" Datum: MaR Level of accuracy: Second Method of measurement: Man 5. Purpose of the facility: treatment of municipal wastewater, [ treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, { treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages L% industrial and % domestic) Ej other (explain:-. ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 6_8 MGD and facility average daily flow: 63 MGD 8. Average amount of residuals being generated at this facility 611 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Aerobically digested liquid, 2 — 1 million gallon tanks Type and volume of residuals storage (i.e., outside of residuals treatment units): Aerobically digested liquid, 4 — 1 million gallon tanks H. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 040 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.LI02(§ _I as: ......... _ Biological Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste (Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes } no. If yes, list the number(s). b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0, yes S no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental. Technologies, Inc. and Date of analysis: 1/13/2021 Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: �140 °F (> 140°F) Passed reactivity test: Eyes `; no. HCN: ND mg/kg (<250) & HaS: 30 mg/kg (<500) TCLP Parameter Limit (Mg/1) result (Mg/1) TCLP Parameter Limit (mg/1) Result (m9/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium LO ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachloropbenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1, 1 -Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAQ 02T .1105. a. For Distribution/Land Application Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Pace Analytical Services, LLC and Date of analysis: 01/26/2021 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 3.9 Cadmium 85 39 0.74 Copper 4,300 1,500 190 Lead 840 300 15 Mercury 57 17 ND Molybdenum 75 n/a 8.7 Nickel 420 420 23 Selenium 100 100 3.5 Zinc 7,500 2,800 490 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: 2M and Date of analysis: �� Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) > 0 but< 25 30 200 210 > 25 but < 50 34 220 240 0 > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 5.13 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Pace Analytical Services, LLC and Date of analysis: 01/29/2021 Parameter Result (mg/kg) Aluminum 8400 Ammonia -Nitrogen 7600 Calcium 8300 Magnesium 2800 Nitrate -Nitrite Nitrogen 83 pH (Standard Unit) 7.5 Phosphorus 14000 Potassium 3800 Sodium 1400 Total Kjeldahl Nitrogen 33000 c. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 0,77 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 3tl %. This rate is a (check one): 0 default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (I It) Year PAN Five -Year Maximum Adjusted PAN (m91k9) (mg/kg) Surface 11503 16458 Injection/Incorporation 15303 20258 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or 0 A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC 02T.I106(b)(3)(13)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. EJ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, 0 heat drying, 0 heat treatment, thermophilic aerobic digestion, beta ray irradiation, C1 gamma ray irradiation, or pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: E3 aerobic digestion, air drying, anaerobic digestion, 0 composting, or lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: M Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). El Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. j Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. r Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. E; Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. El Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 VICINITY MAP SYNAGRA COUNTY: Lee OV�NER(S): Sanford-WW'I'P 0Lu UJ � « z a�CL Z)0- / n w c� a af yp r B.9 � P,t to 03 ., 4Yi z Z d t!) U ✓Y �=. w �l 0 W 4y 0 r > ux m FLULL _ wCa7� 2 w jJ t!! i r' pr J !f' vi �uj # Off.• " !' x" F a `"cs ii/✓, i� cn ��il/ ' r .�.t CC W LL T✓ f Qr' vs }— L w ww: cr u ee CL Z ;= w w r�. Big Buffalo WWTP is currently permitted for 1000 dry tons/year. Based on the significant increase in dry tonnage land applied for 2020, current dry tonnage for 2021, and residuals storage capacity, we are requesting an increase in permitted dry tons. The proposed dry tonnage is 1500 dry tons/year. 2018: 450.86 dry tons 2019: 427.30 dry tons 2020: 953.75 dry tons 2021: 553.08 dry tons See Residuals Source Facility Summary (RSC 06-16) for proposed dry tonnage and residuals storage information. Chris Wynne Technical Services Specialist OPERATIONS SUMMARY - LAND APPLICATION - ALL STATES ALL COUNTIES - ALL SITES MmwTor/EAm AMOUNT UNIT ormrromm umn DRY METRIC TONS Jamuuryuou1 *71,20000 G 100.80 o e1/3 xpri/zo21 1,550,000.00 o 202.90 D 238.45 may2021 415,40000 G 48.85 D 44.31 Juneuoz1 4*e,400.00 o 52.49 o 47.61 Ju|y2O21 688,200.00 G 88.04 D 79.88 TOTAL 3.571.200.00 o 553.08 o 501.64 Report Date: 9110/2021 10:07:10 AM Residuals Sampling Plan City of Sanford, Residuals Land Application Program Big Buffalo Wastewater Treatment Plant Nutrients and Metals Analysis Sampling Point: Basin Sampling Frequency: Based on Dry Tons Land Applied Sample Type: Composite Lab: Pace Analytical Services, LLC Pathogen (Fecal Coliform Density Demonstration) Sampling Point: Basin Sampling Frequency: Based on Dry Tons Land Applied Sample Type: Grab (Set of 7) Lab: Cameron Testing Vector (38% VSR) [rem, Sampling Point: Basin Sampling Frequency: Based on Dry Tons Land Applied Sample Type: Composite Lab: Cameron Testing Sampling Point: Basin Sampling Frequency: Annually Sample Type: Composite Lab: Summit Environmental Technologies, Inc ✓ �rrrrr tdrl,r� �tordv,vry dU ,r � f»r 01,'r p January 13, 2021 Alex Fox Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: FAX: M.171 Dear Alex Fox: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX., (330) 253-4489 Website: htW.-Ilwww.settek.com Order No.: 2101.0192 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/6/2021 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada 011009232020-1, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP C1,0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania Oil, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C p�pauimnr jr y mmitEnvironmental Technologies, Inc. 0 Case Narrative 3310 Win St. Cuyahoga Falls, Ohio 44223 UIVIM", IT su WO#: 21010192 TEL: (330) 253-8211 FAX (330) 253-4489 Website: http://Www.settek-com Date: 1/13/2021 CLIENT; Synagro Project: WWTP WorkOrder Narrative: 21010192: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditation/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Report" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Original ig�� y�du��U�,�"P'j m% TAG Summit Environmental Technologies, In 'p#10433og es, 11a11i1ers aAcronyms "/ l% c Cuyahoga Falls, Ohio44Z WO#: 21010192 TEL: (330) 253-8211 FAX- (330) 253-445 Website: httn://www.settek.co Date: 1/13/2021 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. P The result exceeded the linear range of the calibration or is estimated due to interference. C The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GUMS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM /+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+), S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLv1 Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this fist or for additional information regarding the use of these Qualifiers on reported data. Original �14� 2ti Summit Environmental Technologies, Inc. 3310 Win St. l . Cuyahoga Falls, Ohio 44223 TEL. (330) 253-8211 FAX- (330) 253-4489 CLIENT: Synagro Project: WWTP Lab SampleID Client Sample ID 21010192-001 Sanford WWTP Website: htto://www.settek.com Tag No Date Collected 1/5/2021 1:00:00 PM Workorder 1- WO#: 21010192 13-Jan-21 Date Received Matrix 1/6/2021 11:10:00 AM Sludge 9�• I. lvo)?" O�SUORA4,111 Summit Environmental Technologies, Inc.'Analytical Report �rr%rrl 3310 Win St. r�,i.r,7 .w,,,r . •; Cuyahoga Falls, Ohio 44223 (base report) TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 21010192 Website: ht 2-11www.settek.com Date Reported: 1/13/2021 CLIENT: Synagro --- -- -- Tag Number: -- -- Matrix; SLUDGE Collection Date: 1/5/2021 1:00:00 PM Lab ID: 21010192-OOIA Project: WWTP Client Sample 11 D Sanford WWTP Analyses Result RIL Qual Units DF Date Analyzed TCLP METALS, VOC, SNA, PEST, HERS -SOLID S 7470A SW7470A Analyst: ERA TCLP MERCURY ANALYSIS (SW1311/7470) TCLP Mercury ND 0.00200 mg1L 1 1/11/2021 2:02:00 PM TCLP METALS, VOC, SNA, PEST, HERS -SOLID SW6010D S3010A Analyst: EAM TCLP METALS ANALYSIS (SW1311/6010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/11/2021 12:00:29 PM TCLP Barium(Ba) ND 5.00 mg/L 1 1/11/2021 12:00:29 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/11/2021 12:00:29 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 1/11/2021 12:00:29 PM TCLP Lead(Pb) ND 0.500 mg/L 1 1/11/2021 12:00:29 PM TCLP Selenium(Se) ND 0.0500 mg/L 1 1/11/2021 12:00:29 PM TCLP Silver(Ag) ND 0.500 mg/L 1 1/11/2021 12:00:29 PM TCLP METALS, VOC, SNA, PEST, HERS -SOLID SW8270 SW3510C Analyst: SIFG TCLP SEMI-VOLATILES ANALYSIS (SW131118270) 1,4-Dichlorobenzene ND 0.200 mg/L 2 1/9/2021 1:06:00 AM 2,4,5-Trichlorophenol ND 0.500 mg/L 2 1/9/2021 1:06:00 AM 2,4,6-Trichlorophenol ND 0.500 mg/L 2 1/9/2021 1:06:00 AM 2,4-Dinitrotoluene ND 0.100 mg/L 2 1/9/2021 1:06:00 AM Cresols, Total ND 10.0 mg1L 2 1/9/2021 1:06:00 AM Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 1/9/2021 1:06:00 AM Hexachlorobenzene ND 0.100 mg/L 2 1/9/2021 1:06:00 AM Hexachloroethane ND 0200 mg/L 2 1/9/2021 1:06:00 AM Nitrobenzene ND 0.200 mg/L 2 1/9/2021 1:06:00 AM Pentachlorophenol ND 0.500 mg/L 2 1/9/2021 1:06:00 AM Pyridine ND 0.500 mg/L 2 1/9/2021 1:06:00 AM Surr: 2-Fluorophenol 81.1 10 - 157 m %Rec 2 1/9/2021 1:06:00 AM Surr: Phenol-d6 77.5 10 - 169 %Rec 2 1/9/2021 1:06:00 AM Surr; Nitrobenzene-d5 65.6 32.1 - 130 %Rec 2 1/9/2021 1:06:00 AM Surr: 2,4,6-Tribromophenol 102 45.4 - 166 %Rec 2 1/9/2021 1:06:00 AM Surr: 2-Fluorobiphenyl 86.4 35.7 - 130 %Rec 2 1/9/2021 1:06:00 AM Surr: p-Terphenyl-d14 114 74.7 - 145 %Rec 2 1/9/2021 1:06:00 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Original RL Reporting Detection Limit U Samples with CaleVa1 < MDL ! Yh summu"t 5ummitEnvironmental Technologies, Inc.ytic 1 R eort 3310 Win Sr. F 4 F, C Cuyahoga Falls, Ohio 44223 (base report) TEL: (330) 253-8211 FAX. • (330) 253-4489 WO#: 21010192 Website: hL2.11www.settek.com Date Reported: 1/13/2021 CLIENT; Synagro 'Tag Nurnberg Matrix: SLUDGE Collection mate; 1/5/2021 1:00:00 PM Lab ID: 21010192-OOIA Project: WWTP Client Sample ED Sanford WWTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW3510C Analyst: CSS TCLP PESTICIDES ANALYSIS (SW131118081) Chlordane, total ND 0.0250 mg/L 1 1/11/2021 11:20:00 PM Toxaphene ND 0.0500 mg/L 1 1/11/2021 11:20:00 PM Endrin ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM gamma-BHC ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM Heptachlor ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM Heptachlor epoxide ND 0.00250 mg/L 1 1/11/2021 11;20;00 PM Methoxychlor ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM Surr: TCMX 66.0 10 - 119 %Rec 1 1/11/2021 11:20:00 PM Surr: DCB 82.3 10 - 119 %Rec 1 1/11/2021 11;20:00 PM TCLP HERBICIDES BY EPA 8321B SW8321A Analyst: JPG 2,4-D ND 0.500 mg/L 50 1/9/2021 9:33:00 PM 2,4,5-TP ND 0.500 mg/L 50 1/9/2021 9.33:00 PM Surr: 2,4-Dichlorophenylacetic aci 101 70 - 130 %Rec 50 1/9/2021 9:33:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260 SW1311 M Analyst: SLV TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM 1,2-Dichloroethane ND 0.250 mg/L 50 1/8/2021 10:05:00 PM MEK ND 5.00 mg/L 50 1/8/2021 10:05:00 PM Benzene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM Carbon tetrachloride ND 0.250 mg/L 50 1/8/2021 10:05:00 PM Chlorobenzene ND 2.50 mg/L 50 1/8/2021 10:05:00 PM Chloroform ND 0.250 mg/L 50 1/8/2021 10:05:00 PM Tetrachloroethene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM Trichloroethene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM Vinyl chloride ND 0.100 mg/L 50 1/8/2021 10:05:00 PM Surr: 4-Bromofluorobenzene 92.4 70 - 130 %Rec 50 1/8/2021 10:05:00 PM Surr: Dibromofluoromethane 105 70 - 130 %Rec 50 1/8/2021 10:05:00 PM Surr: Toluene-d8 97.6 70 - 130 %Rec 50 1/8/2021 10:05:00 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Original RL Reporting Detection Limit U Samples with CaloVal < MDL r O"", "v)%�'Ngo ve F'r'3X SSummit Environmental Technologies, Inc. Analytical Report 3310 Win St. UMM17 Cuyahoga Falls, Ohio 44223 (base report) TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 21010192 Website: hUp.-11Wivwsettekcom Date Reported: 1113/2021 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/5/2021 1:00:00 PM Lab ID: 21010192-OOIA Project: WWTP Client Sample ID Sanford WWTP Analyses Result RL Qual Units DID Date Analyzed RCI SW9014 Analyst: MS REACTIVE CYANIDE (901417.3.3.2)-SOLID Cyanide, Reactive ND 0.495 mg/Kg 1 1/7/2021 4:50:00 PM IGNITABILITY OF SOLIDS (SW-846:1030) SWI030 Analyst: SEE Ignitability nonflammable mm/sec 1 1/13/2021 11:15:56 AM PERCENT SOLIDS BY SM2540MOD A2540B Analyst: MMA Percent Solids 3.15 % 1 1/12/2021 10;05:00 AM RCI SW9045D Analyst: DHC PH (SW9045D) pH 7.2 S.U.@19.00 1 1/7/2021 11:00:00 AM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide, Reactive 30.0 25.0 mg/Kg 1 1/7/2021 4:50:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected PL Permit Limit RL Reporting Detection Limit E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds P Second column confirmation exceeds R RPD outside accepted recovery limits Original U Samples with CalcVal < MDL ZKOMEEM r anau ni7r or r r., e e t� ,(,��)SUMMIAT Summit Environmental Technolo ies, Inc. ccre itation rorai 4���r�a��rr��y, icy' 3310 Win St. 1I1`di te3 Ort Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 21010192 Website: h=.•11www.settek.com 13-Jan-21 Client: Synagro State: NW Project: WWTP Program Name: NC WW_SCM Sample ID Matrix Test Name Analyte Status 21010192-OOIA Sludge Ignitability of Solids (SW-846: 1030) Ignitability A Sludge Percent Solids by SM2540Mod Percent Solids N Sludge pH (SW9045D) Hydrogen Ion (pH) A Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive N Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive N Sludge TCLP Herbicides by EPA 8321 B 2,4,5-TP A Sludge TCLP Herbicides by EPA 8321B 2,4-D A Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A Sludge TCLP Metals Analysis (SW1311/6010) Barium A Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A Sludge TCLP Metals Analysis (SW1311/6010) Chromium A Sludge TCLP Metals Analysis (SW1311/6010) Lead A Sludge TCLP Metals Analysis (SW1311/6010) Selenium A Sludge TCLP Metals Analysis (SW1311/6010) Silver A Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A Sludge TCLP Pesticides Analysis (SWI311/8081) Endrin A Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene N Sludge TCLP Serni-Volatiles Analysis (SW1311/8270) Hexachloroethane N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene N Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol N NC WW SCM A Accredited NC WW SCM N Not Accredited Original #1 /rf y oos z �, , f U; Summit Environmental Technologies, Inc. Accreditation Program 3310 Win St. Cuyahoga Falls, Ohio 44223 Anal tes Report TEL: (330) 253-8211 FAX., (330) 253-4489 WO#: 21010192 Website: ha.-Ilwww.settek.com 13-Jan-21 Client: Synagro State; NW Project: WWTP Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 21010192-OOIA Sludge TCLP Semi-Volatiles Analysis (SW131118270) Pyridine N Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A Sludge TCLP Volatiles Analysis 2-Butanone A Sludge TCLP Volatiles Analysis Benzene A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Chlorobenzene A Sludge TCLP Volatiles Analysis Chloroform A Sludge TCLP Volatiles Analysis Tetrachloroethene A Sludge TCLP Volatiles Analysis Trichloroethene A Sludge TCLP Volatiles Analysis Vinyl chloride A NC_WW SCM A Accredited NC WW SCM N Not Accredited Original #1 -? ■ F' N O N" CD N Lo et O w O cD m M -ITN 4P M dM M M M to P C2 to - M Mt � OJ 62 µ�r r r r r r r r r r r r r r r r r N 0 0 O M 0 O M NI r* O h N M M�t 0 Lo ® h am t® R Cn N, r n' O M R r g r Cl) N N N r r N' M N r N N M Lo o r O O w r N do M et rY CD g ONO _O �T coM M o co M M M M co M O- CO M O o co °� O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O w O O O O O O O O O O O O O OD O O O r O OD m O aD O r r r r r r 0 ® ® ® ® O O O O O O O O O O O O O 0 0 0 0 0 6 0 0 0 0 0 0 N to Lo r to V �- o In N N t 0 00 O O ® O O O O C.O I-coa`°Mz P-toMZM t'- [O N OD h h CD le q N N M M M r CO r O O O O O O O O O O O O O O Lo N Qc=c CD (D'0 ccc BCD CDe NL e a) a W Q C M�O O O � O 4' O t O O p 2 C LL 0— d' LL h^ O U V ~ O o O N® N d Z Cti N Q LE n t!> w® v N N sV0 O@ _� O a> o> d' d• d� V U N y y y :: T U) in f!i (/3 U),- N N No 0=== 2 d d h h R a E CL CM h N d O O � C cr -OR co 0 CL T � 0 0 e4 ns E r< J T T m Q 0. v, E 2 _N CL >• � J Q U W C� 0 em E O �g T > U U ®^ O > Y a Z D U aN) J N r ® T N � C Q E (6 (� m O Go cy o N CD � � N C m cn C7 Q E Of O O O O O O O O O O O C. 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U E CO ( n li W) 4 0 Q M Cl ffi- A (0 E m v5 U Q _ CY E J co co co R N T M a 0 o K Z Z o N iL r N N M E � J r OM N 93 = m co ❑ ❑ Q N E e1 2 9 C J Q U W d' � o N E Y N d I U) O � r > Y � N � Z 0 m r d 1- 0 N 0 O N N V U a � o D (rV fy a _ N ch E it r s 2) D D o. N E d � J Q V W 0 U H E � N > C Y d U) O � m O > a y Y CL 0 0 Zcn U J ~ d co O N CL cm r N N d jL, s E yr @ co V/ Co qL J Q 0 M C O s O +U' N m v ® v CL 5 Eca w U Q � O ❑ Of N tt c+a E J r M N m D D Q. (n E C J Q LU W cr 0 U E � C � D Y N a U) O C O C'6 .0 'n z w U) J W O N C N N N F... s r E @ c6 m U) J a O r®'s Ci O � O � N O CL C T w E U) U Q Cn m D nt � N n E J a= .G D D CL V) E 2 'N Q C J Q LU W 0 U h E @ C Y d co 4 � O > � N � -v0 w w m J ~ a N O O N N v r ce) 4- 0 eY) M O nn � O � O N @ E E C 0 c M oq vi � V• � N o o U M � N W O M L K,r 9h ✓�J y�9r��mi m ai r✓�i;� oo q ,por mpq ¢lr ra,r�d+u�r ��rviHy� 90 O vt N wN W IM O a N O N d F- s G Co6 s�(q VJ IL T T m 8 � U P, to U O N N N a Q � E B m a. 9 v � � m ct0o U N O N E co G O C .n m P d' a N 0 D N N ~ U Q E co '(^6 m Vt a. g v a >, E cD m co U 0 N O c� J co 0 N N LO V. T M � Z Z 0 C � ry cn ❑ N � N M w .J r � ai ai _ m is a O c Q U w 0 v d N E E @ C � Y n. i U) o � J2 O � N U) Z o — 03 W ~ d N C� C� M tm r- O le M O O ca yyMI// / ur � ✓;J ✓�• if',N < rn rn N E E ca a _ Q v c E t6 M CO n. M 0 Ws V M Ci o v m v CO I] w iJ (D E c rn U Q °1 W N y B ct3 m 0 o V o t o m c�c m a � N E caa CO U d d co E E m c 0 c >, .E r9 I S Summit Environmental Technologies, Inc. WM 3310 Win St. l -I heck List ,kr Cuyahoga Falls, Ohio ...... TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htW.-Ilwww.settak.com Client Name: SYN-NC-27028 Work Order Number: 21010192 RcptNo: 1 Logged by: Jacqueline Rasile Gompleted By: Jacqueline Rasile Reviewed By: Jennifer Woolf 1 /6/2021 11 A 0:00 AM 117120219:20:55 AM 1/7/2021 11:14:58 AM ,0 , Chain of Custody 1. Is Chain of Custody complete? Yes 91 No ❑ Not Present ❑ 2. How was the sample delivered? FedEx Log In 3. Coolers are present? Yes S6 No ❑ NA ❑ 4, Shipping container/cooler in good condition? Yes MI No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present W No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes ® No ❑ NA ❑ 6. Were all samples received at a temperature of >0° C to 6.0°C Yes ® No ❑ NA ❑ 7, Sample(s) in proper container(s)? Yes 0 No ❑ $, Sufficient sample volume for indicated test(s)? Yes W No ❑ 9, Are samples (except VOA and ONG) properly preserved? Yes ® No ❑ 10. Was preservative added to bottles? Yes ❑ No W NA ❑ 11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials 0 12. Were any sample containers received broken? Yes ❑ No 91 13. Does paperwork match bottle labels? Yes 0 No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes 0 No ❑ 15. Is it clear what analyses were requested? Yes ® No ❑ 16. Were all holding times able to be met? Yes 0 No ❑ (If no, notify customer for authorization.) Special Handling (if apgiicablei 17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA Person Notified: Date: By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ in Person Regarding: s Client Instructions: 18, Additional remarks: Cooler Information Cooler No I Terms°O Condition Seal intact Seal No Seal DateSi ned By 1�- �— 1.5 _ Good TNot Present I — ace Analytical @) Synagro 12701 Lancaster Hwy Pineville, NC 28134 • Ad I Project Name: Sanford WWTP Lot Number:WA06023 Date Completed: 0 1 /26/2021 01/26/2021 11:21 AM Approved and released by: Project Manager 11: Lucas Odom A C C R E D I T F D TESTING LAEORATOBY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel: 803-791-9700 Fax- 803-791-9111 www.pacelabs.com Page 1 of 7 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case R Synagro %Number—WA06023 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. loz Reduced volume was used for samples due to sludge matrix. Phosphorus The method blank for analytical batch 80524 contained the analyte total phosphorus greater than the method acceptance criteria. The associated sample contained detections for this analyte at concentrations greater than 1 OX the value found in the method blank; therefore sample results are not impacted. The data has been reported. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 7 Client: Synagro Description: Sanford WWTP Date Sampled:0110512021 1300 Date Received:0110612021 Laboratory ID: WA06023.001 Matrix: Solid % Solids: 5.13 01/07/2021 0115 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 254OG 1 01/07/2021 0115 MOM 78694 1 350.1 (Ammonia - N ) 350.1 10 01/08/2021 1034 DRD 78739 1 (Nitrate - N ) 9056A 1 01/08/2021 1542 AMR 79020 1 (Nitrite - N ) 9056A 1 01/08/2021 1542 AMR 79022 3 (Phosphorus) 365.1 20 01/22/2021 1530 DMA 01/13/2021 2032 79352 1 (Soil pH meal) 9049D 1 01/08/2021 2194 AAB 78048 3 351.4 (TKN) 351.2 2 01/21/2021 1222 DMA 01/19/2021 1952 79979 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 5.13 % 1 Ammonia - N (gas diffusion) 350.1 7600 190 100 mg/kg 1 Nitrate - N (soluble) 9056A 57 9.7 1.9 mg/kg 1 Nitrite - N (soluble) 9056A 25 3.9 1.9 mg/kg 1 Phosphorus 7723-14-0 365.1 14000 1900 390 mg/kg 3 Soil pH measured in water @ 18 ° C 9045D 7.5 su 1 TKN 351.2 33000 970 970 mg/kg 3 r ' " Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 74718 7471B 1 01/07/2021 0903 JAB2 01/07/2021 0614 78704 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 1.4 0.35 mgfkg 1 a Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 01/13/2021 1356 KSH2 01111/2021 0946 78716 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 601OD 8400 130 48 mg/kg 1 Arsenic 7440-38-2 601OD 3.9 J 4.8 1.6 mgfkg 1 Cadmium 7440-43-9 6010D 0.74 J 1.6 0.40 mg/kg 1 Calcium 7440-70-2 6010D 8300 1600 200 mg/kg 1 Chromium 7440-47-3 6010D 41 3.2 0.80 mg/kg 1 Copper 7440-50-8 6010D 190 3.2 1.4 mg/kg 1 Iron 7439-89-6 601OD 11000 32 15 mg/kg 1 Lead 7439-92-1 6010D 15 3.2 1.4 mg/kg 1 Magnesium 7439-95-4 6010D 2800 1600 200 mgfkg 1 Manganese 7439-96-5 6010D 740 4.8 1.9 mgfkg 1 Molybdenum 7439-98-7 601013 8.7 J 13 3.2 mg/kg 1 Nickel 7440-02-0 6010D 23 13 3.4 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLG (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Client:Synagro Description: Sanford WWTP Date Sampled:01105/2021 1300 Date Received:01/06/2021 Laboratory ID: WA06023-001 Matrix: Solid % Solids: 5.13 01/07/2021 0115 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 01/13/2021 1356 KSH2 01/11/2021 0946 78716 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Potassium 7440-09-7 6010D 3800 1600 200 mg/kg 1 Selenium 7782.49.2 6010D 3.5 J 6.4 2.6 mglkg 1 Sodium 7440-23-5 601OD 1400 J 1600 200 mg/kg 1 Zinc 7440-66-6 601OD 490 16 4.0 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result - LOQ and > OL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 7 Mir 1 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 Y 777- 4 E�-� ct;tkt fit, '39F930 pa dl , w- a, `. (oate CD u0 Iasi dew j , )N e k ti 2dt; c ti le 4 (d ra ;tea f d� cs � I 7 a: ISO a - a to ngXq ift. r CL Lq MY'•• R41f Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 4h w BE PA PACE ANALYTICAL SERVICES, LLC SaWfeg R9CPfPt ChecMi,-kt (SRC) rME0018C.1,41 MAI,' Authority, Pict:ENV - WC,,)t, 9129/2020 satilple Reccipt Ch -exist C) WA06023 CkvIler:115pecied by;, at Lot ,M47RM k, Pace int Up� F C Y" c No 1, Were utstody s -,als preiie'rt Strip I 7eskod by:- I 'x i ctrr Mol'id S-nap.cop ED: fti of t w Jcc' Vadz IDly kzc Nowe a Cum-w inn Pantor 49LIC 'ir, r- Y,:�s NaLI'l If rej11P;:r4tvV of wJ Cooley Mftrl5.�T, teas Proicet -Manager Notifici? I PM was Notifit:4 .Iy. pbone-e entail i Race -to face (Cirej-1 one), y No ON A I the cease memisl 4mlriw's wvkingifip aftl1rh 'o 1--isfoml" it No S. Wen 1yoiler 4cuswdy pfx)rAriktrf.,,s (relinqui3hcdhvcehed) rollowcc:l No 6. Wmre sail oil the coc"? as 'No 7, W�rc sari ira tip, IEst i cis all sawplt LQ1:t4jDCM'Z E]Xus NrA -14. Wws CoLemon date& timo Lsted on I all szrnpl e. I con I tah I 10, Did all Cony aver l0ef jnfoliumiioa (TT-1, dalc time) amewill te COC? es t No �te%s 10 �P,- FOrfOrMed ILIV66 on tho CGO Noi 12- DW 141 jmplc3 arrive in We proyiz;L�vjilujrmrs for each M51 2rVilpr in good condi(ion On, crc.)7 Yes N1 14wele all surjpM ruckyed wi'lut 'A the -holdnig (iinq or 48 hoUM, Whicb-nver c4lues first? BEY sarralrlc containers (circle 2pc) sanjyjeN�ot ti:j,rd (m, COC? UJ yes NO,! E]'NA (14`40F Omm 41 diamew-1-1 IM 0.1y ofthe VOA vial-0 y No A ".7. VV=rt 411 TA-0imctals.hiat-T iet% �4U:npleS raceiW-4 at a TTH Of < 2? No �NA I S,',here All cyraik e saniples recciNred at a PTJ and llrw 84: 1r., C3 rcceived DH At a , Yes o !�V Wert 0 applicd7le sai-aple. NA ors Tdr; 24i. V7,4�ro client reotarksArculuc3ts requw5teS 11jutorks, mswhjq) clesit nation a, etc...; corm(Aly transcribed fronn ll?t toC into Cwcvmmunt secdor. in, f,,(kfS,7 'Eyr,51, LPN t2}, W45 the quwe number iasteci OD tle wItI41111crize-T If �es, 0110te 9 1117-IJOW kwoutwulty Preseyved or with jlaaapaU,) libunTectly waserd -cure adjust-.0 j sample receiving, with JnL of eircle One: A2SO4,14NOI, 110, N,,09, u'-ng sj� era mc of prestrVatior, M Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 7 Cameron Testing Services, Inc. Laboratory Report Synagro Sanford WWTP Sample Information prv�m m 40 , as 07/12121 )1141 C. Wynne Analyses and Results NC DENR #654 NO PHH$ 03770, US EPA #NCO1918 2107-0094 DW Cert # 37799 U-M "ik i E 07112121 . Puckett 2107-0094 -03 3Wdge Gr Fec. Cofiform�S 23700 CFU/9 23700 07/13/21 RL 9222D - MF -04 23400 0RY9 23400 -06 23200 CFU1Q 23200 -06 826000 0FU/0 23600 -07 1520000 CFU1q 23400 -08 295()0 GFUIQ 29500 -09 23600 CFUIV 23000 Geomean 2107-0094 -03 3WgE Gar TS M 423% 001 07/13/21 RL 2540 G -TS -04 4,27% 0,01 -05 4.30% 0.01 -06 4.23% 0.01 -07 4,27% 0,01 -08 3.39% 0,01 -09 424% 0,01 Report Review Lab Director 19 5, Steele Sir, 919-208-4240 Sanfind NC 27330 //r ip/' l'1�1��✓'�%��i9%�/i/% ' j � `-4' fir, G��nl/i ��i: i�(��✓!jam/�i�i �%//''�i'%, ' � "'.,, { , r i I 0 s. v s.w i/ " E ' on Cy /'IM ii%//% wo , IGS VOA d 1 L t rwe qr, u, F' d OE No ut { woo YJ � t k �. oleo to All olio%/ ; /%� r tJ �� r� �r/il / za Y �Er� �rl�r ����1r r,, �� /ri % /� �' J �r , I