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State of North Carolina DW Department of Environmental Quality Division of Water Resources WATER QUALITY REGIONAL OPERATIONS SECTION Division of Water Resources NON -DISCHARGE APPLICATION REVIEW REQUEST FORM October 7, 2019 To: ARO-WQROS: Landon Davidson / Zan Price From: Ranveer Katyal, Water Quality Permitting Section - Non -Discharge Branch Permit Number: WQ0002431 Applicant: Huffman Finishing Company Owner Type: Organization Facility Name: Huffman Finishing RLAP Signature Authority: Lee T. Huffman Address: PO Box 170, Granite Falls, NC 28630 Fee Category: Non -Discharge Minor Comments/Other Information: Permit Type: Land Application of Residual Solids (503) Project Type: Renewal Owner in BIMS? Yes Facility in BIMS? Yes Title: Treasurer County: Caldwell Fee Amount: $0 -Renewal Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 45 calendar days, please take the following actions: ® Return this form completed. ® Return a completed staff report. ❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact person listed above. RO-WQROS Reviewer: D J j I N . e: %U OCT 10 2019 Water Quality Regional Operations Asheville Regional Office FORM: WQROSNDARR 09-15 Page 1 of 1 ROY COOPER Governor MICHAEL S. REGAN Secretary LINDA CULPEPPER Director LEE T. HUFFMAN — TREASURER HUFFMAN FINISHING COMPANY PO Box 170 GRANITE FALLS, NORTH CAR0LfNA 28630 Dear Mr. Huffman: NORTH CAROLINA Environmental Quality October 7, 2019 Subject: Acknowledgement of Application No. W00002431 Huffman Finishing RLAP Residuals Management System Caldwell County The Water Quality Permitting Section acknowledges receipt of your permit application and supporting documentation received on October 3, 2019. Your application package has been assigned the number listed above, and the primary reviewer is Ranveer Katyal. Central and Regional Office staff will perform a detailed review of the provided application, and may contact you with a request for additional information. To ensure maximum efficiency in processing permit applications, the Division of Water Resources requests your assistance in providing a timely and complete response to any additional information requests. Please note that processing standard review permit applications may take as long as 60 to 90 days after receipt of a complete application. If you have any questions, please contact Ranveer Katyal at (919) 707-3661 or ranveer.katyal@ncdenr.gov. Sincerely, Nathaniel D. Thornburg, Supervisor Division of Water Resources cc: Asheville Regional Office, Water Quality Regional Operations Section Permit File W00002431 J Water Quality Regional Operations Asheville Regional Office North Carolina Department of Environmental Quality I Division of Water Resources 512 North Salisbury Street 1 1617 Mail Service Center I Raleigh. North Carolina 27699-1617 919.707.9000 APPLICATION FOR PERMIT RENEWAL PERMIT NO WQ0002431 HUFFMAN FINISHING COMPANY GRANITE FALLS, NORTH CAROLINA Prepared For: Huffman Finishing Company PO Box 170 Granite Falls, NC 28431 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill, SC 29732 September 2019 RECEIVEDINCDEUDWR OCT - 3 2019 Non -Discharge Permitting Unit Water Quality Regional Operations Asheville Regional Office C a1ft..�i BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd, Suite 103-291, Rock HUI, SC 29732 PHONE (336) 510-0340 CELL (336) 312-9007 September 28, 2019 NCDEQ -Division of Water Resources NonDischarge Branch Mail Service Center 1617 Raleigh, North Carolina 27699-1617 Attention: Mr. Nathaniel Thornburg Reference: RENEWAL OF PERMIT NO. W00002431 Huffman Finishing Company Land Application Program Granite Falls, North Carolina BR&S Job No. 2014-115 Dear Mr. Thornburg: Branch Residuals & Soils, LLC is under contract with Huffman Finishing Company to provide assistance in the preparation of a permit renewal for the above referenced facility. For a complete listing of enclosures with this request, please see the attached Table of Contents. Your attention in the review of this application would be greatly appreciated. Please contact me immediately if you require additional information or have questions in the review of the permit application. Sincerely, i� Robert T. Branch, L. S. S. Project Manager cc: Mr. Lee Huffman — Huffman Finishing Company TABLE OF CONTENTS Section No. Title I RESIDUALS LAND APPLICATION PROGRAM - RLAP 06-19 Operation and Maintenance Plan II RESIDUALS SOURCE CERTIFICATION WWTP - RSC 06-16 Facility Vicinity Map Process Flow Diagram and Narrative Justification for Residuals Production Rate Residuals Sampling Plan Lab Analytical Reports and Operational Data III LAND APPLICATION SITE CERTIFICATION - LASC - 06-16 Landowner Agreement Attachments Updated Maps Site Vicinity Map Buffer Map Buffer Map with Compliance and Review Boundaries Cumulative Pollutant Loading Rates RESIDUALS LAND APPLICATION PROGRAM - RLAP 06-16 RECEIVEDINCDEQIDWR I)WR Dlvlslon of Water Resources OCT - 3 2019 Non -Discharge Permitting Unit State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supportine documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .I 100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): ❑ Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0I06(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification' Major (land are permitted for >— 300 acres) $1,310 $395 Minor (land are permitted for < 300 acres) 1 $810 $245 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage unitstprocesses not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (Maybe Required —See 15A NCAC I C .0300) Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Page 1 of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. Submit the O&M Plan in accordance with 15A NCAC 02T. 1110 and include at a minimum: 0 Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. Maintenance schedules; may include equipment calibration, maintenance of signs, etc. 0 Safety measures; may include safety training program, manuals, signs, etc. El Spill response plan; including control, containment, remediation, emergency contact information, etc. E] Inspection plan including the following information; Fj Names and titles of personnel responsible for conducting the inspections. Q Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. 0 Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. 0 Sampling and monitoring plan including the following information; 0 Names and titles of personnel responsible for conducting the sampling and monitoring. 0 Detailed description of monitoring procedures including parameters to be monitored. 0 Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY, F. Program Determination F1 Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15X NCAC 02T .1102(12). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: Q Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. { , 0 Any land application site certified for the residuals land application program that is used primarily for rest l uals disposal, and agricultural crop production is of secondary importance. 0 Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. Ej Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information j Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. 0 Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) 0 Submit three (3) sets of standard size plans and two (2) sets of l 1" by 17" plans (electronic format is acceptable-iAdobe PDF only). For Modifications, submit plans specific to the modification(s) only. 0 Plans must include the following minimum items: EgA general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 250o the total site relief and showing all facility related structures and fences within the land application area. 0 The location of all wells (including usage and construction details if available), streams (ephemeral, int rmittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). 0 Delineation of the review and compliance boundaries 0 Setbacks as required by 15A NCAC 02T .1108 Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be, labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 I. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) ❑ Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) ❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: htto://www.ncwater.ora[Rules Policies and Regulations/. The document shall be signed, sealed and dated by a qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .I 104(d)(21. For Modifications, submit an updated site map specific to the modification(s) only. ❑ The design documents must include the following minimum items: ❑ Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; ❑ Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. El Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) Submit a completed and accurate water balance in accordance with 15A NCAC 02T .1104(d)(5) and current Division Policy available at: htip://www.ncwater.or2/Rules Policies and Regulations/. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) ❑ Property ownership documentation shall consist of one of the following: ❑ Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or ❑ An easement running with the land specifically indicating the intended use of the property and meeting the requirements of 15A NCAC 02L .0107(f), or ❑ A written notarized lease agreement signed by both parties, indicating the intended use of the property, as wiell as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Deliverv: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 1 Page 3 of 3 DRaCa1VEDNCDE010%R\ 1 Jn State of North Carolina �yj`Department of Environmental Quality OCT — 3 200 Division of Water Resources Division of Water Resources Non-D'~ 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM permitting Unit FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Huffman Finishing Company Applicant type: ❑ Individual ® Corporation ❑ General Partnership Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal Q County Signature authority's name per 15A NCAC 02T .0106: Mr. Lee T. Huffman Title: Treasurer Applicant's mailing address: Post Office Box 170 City: Granite Falls State: NC Zip: 28630 Telephone number: (828) 396-1741 Email Address: hufthoslth@aol.com 2. Consultant's name: Robert T. Branch License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: Branch Residuals & Soils. LLC.I Consultant's mailing address: 1735 Heckle Blvd. Suite 103-291 City: Rock Hill State: SC Zip: 29732-_ Telephone number: (336) 510-0340 Email Address: bbranch@branchrs.com 3. Agronomist's name: Robert T. Branch License Number: Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: Branch Residuals & Soils. LLC) Agronomist's mailing address: Same As Above City: _ State: _ Zip: Telephone number: (_) _ _ Email Address: 4. Soil Scientist's name: Robert T. Branch License Number: 1180 Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: Branch Residuals & Soils. LLC.) Soil Scientist's mailing address: Same As Above City: _ State: _ Zip " + Telephone number: (_) Email Address: 5. Fee submitted: 0_00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00002431 Date of most -recently issued permit April 13, 2015 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 4919 Hickory Blvd. City: Granite Falls Coordinates: Latitude: 35' 46' 1 I.10" N Datum: NAD 1983 UTM 17N Method of measurement: Mao State: NC Zip: 28630-1 Longitude: 81 ° 23' 3785" W Level of accuracy: 1" 2. County where residuals land application program is headquartered: Caldwell 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Robert T. Branch Branch Residuals & Soils 15676 Back -Up ORC Ray Gambill Bio-Green Services 995951 Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: I_ .1 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals. source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 31 dry tons per year. PAN Pounds of PAN per Dry Ton Pounds of PAN per Year (Weighted Average) Surface Incorporation Surface Incorporation or Injection or Injection First -Year 47.79 52.10 1,481.44 1,615.05 Five -Year Maximum Adjusted 73.88 78.19 2,290.20 2,423.81 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation LJ Row Crops Hay 12.8 Pasture Total: 12.8 Methods Surface 12.8 G� Incorporation or Injection 0 C] Total: 12.8 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Acres Required Using Acres Required Using Application Rate First -Year PAN Concentrations Five -Year Maximum Adjusted PAN (Ibs PAN/ac-}r) Concentrations Surface Incorporation or Surface Incorporation or Injection Injection 50 2116 23.07 32.72 34.63 100 14.81 16.15 22.90 24.24 150 9.88 10.77 15.27 16.16 200 7.41 1 8.08 11.45 12.12 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): Land is tight for this program but applications have been greater than every five years so first Year PAN can be used. 7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): i ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; = Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; i I ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation faciliti s cr irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Nam. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application Complete and submit the following Land Applications Site Certification and all associated documentation. ®B Land Application Site Certification.doc FORM: RLAP 06-16 1 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: E] Spray M Drip 2. Disposal system is: E] existing 0 proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation:`1 feet below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? 0 Yes or Q No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: F77-1 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate Recommended Loading Rate t(iin-//hrr)) ri—n-/---r) Cr7 C� C� C7 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? El Yes or 0 No If No, explain why 15A NCAC 02T .0505(n) is not met: �� 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field / Zone Design Area (ft') Number of Nozzles Maximum Application Rate ( allons/hr) Design Annual Loading Rate (galling / r) Total Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameter of nozzles ft Wetted area of nozzles] ft-'] L] Nozzle capacity gpm Nozzle manufacturer / model Elevation of highest nozzle �„� ft [^_] FORM: RLAP 06-16 1 1 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02'r.0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. N Yes 0 No, Explain;/ `` I, Lee T. Huffman Treasurer (Signature Authority's Name— PLEASE PRINT) (Title) attest that this application for Huffman Finishing Company Land Application Program (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned tome as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include,a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. i Signature: U I Date: FORM: RLAP 06-16 aae5of5 �I Operation and Maintenance Plan Operation & Maintenance Plan Huffman Finishing Company The WWTP ORC (or Backup ORC if ORC is unavailable) shall be in charge of the following items as it relates to the current land application program: • Collection of WWTP and WTP Samples (See Attached Sampling Plan) • TCLP Samples (See Attached Sampling Plan) • Pathogen reduction samples (See Attached Sampling Plan) • Vector attraction reduction samples (See Attached Sampling Plan) As Preparer for this facility under 40 CFR Part 503 - Being the individual that is familiar with the routine operation of this facility which includes: Insuring solids are ready for land application • Insuring solids have undergone proper treatment Proper operation of treatment units • Proper operation of sludge holding units • Proper maintenance of treatment and storage units • Notification of state and land appliers of abnormal conditions The Land Applier shall be in charge of: • Collection of Nutrient and Metal analyses • Buffering Land Application Fields Spreading Materials at Rates Given for Field, Crop & Soil. Calibrating Spreader • Inspections and Inspection log • Record keeping regarding disbursement & location of material spread. • Lime Stabilization (if applicable) —collecting pH measurements: ➢ Initial pH ➢ Raising the pH to 12 ➢ Monitoring the pH to see that it stays at 12 for 2 hours, and ➢ Making sure it doesn't drop below 11.5 for the next 22 hours. • Spill Response • Signage Both the WWTP ORC and Land Appliers will complete the aforementioned responsibilities before the commencement of each land applying event. In the event that an area Iof noncompliance is observed, the NCDEQ Asheville office will be contacted as well as Bob Branch. Inspections should be performed in the field at the beginning of every land application event, with every change in loading rate, and post application event for run off. An additional inspection will be performed, if rain occurs after the application event and before the residuals have had time to desiccate (typically 3 - 5 days). Each field will be inspected pre and post with each application event. The frequency of inspections will depend on the frequency of application events. A copy of the RSC Sampling Plan for the WWTP is attached and included as part of the Operations and Maintenance Plan. 1 Operation and Maintenance Plan Huffman Finishing Company Title Name Office Phone Cell Phone WWTP ORC M. Shuford Wise 828.244-9598 Land Applier Bob Branch 336.510-0340 336.312-9007 Backup Applier Ray Gambill 336.813-8063 2 Spill Control Plan Project: Huffman Finishing Company IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE IMMEDIATELY TAKEN: 1. MANAGEMENT OF CLEAN UP ACTIVITIES :The Project Manager shall take immediate charge and initiate cleanup activities. BioGreen Services labor and equipment are to be utilized. In the event additional labor and equipment are required, assistance shall be requested from the plant operator.The Project Manager shall also communicate with the public on scene, answering questions and advising of the clean up activities. 2. HALT SOURCE OF SPILL: Such as ruptured container or damaged transport unit 3. FORM A BARRIER : Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area. The Project Manager or the person in charge on the spill site will advise the cleanup personnel where to get the straw, lime and other items necessary to complete the cleanup operations, ie local farmers, farm supply center, nursery, ect. 4. CLEANUP : Employ front end loaders, vacuum equipment, sludge application equipment, and/or septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw and soaked material will be collected and remove to a disposal area approved by representatives of the state regulatory agency. 5. FINAL CLEANUP : Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the cleanup efforts by the state regulatory representative. If the event occurs on private property, the cleanup will be completed to the satisfaction of the property owner and state representatives. The ultimate goal will be to restore the spill area to it original condition if possible. 6. Notification :As soon as possible after the spill occurs the BioGreen Services' Environmental Project Manager or Assistant Manager will notify the WWTP ORC and Bob Branch, and they will then be responsible for notifying someone on the Project calling list. 7. Reporting : The WWTP ORC or Bob Branch will notify the Regional Office of the NCDEQ by telephone as soon as possible, but not more than 24 hours, or the next working day following the occurrence. The Project Manager shall provide a written report within 48 hours of the spill to Residuals Management Coordinator and the Director of Utilities (or appropriate project personnel). The report shall list all relative information and actions taken. A written report w i I I b e f i l e d to the appropriate regional office of the NCDEQ within 5 days of the occurrence. * SEE NEXT PAGE FOR NOTIFICATION LIST. Spill Control Plan WWTP ORC Telephone: Land Application ORC Telephone: Land Applier: Telephone: FACILITY CONTACT : Telephone: LOCAL POLICE, FIRE,EMERGENCIES: NCDEQ REGIONAL OFFICE: STATE OF NC WARNING POINT: OUT OF STATE INFORMATION: Shuford Wise 828-244-9598 Bob Branch 336-312-9007 Ray Gambill 336-813-8063 Lee T. Huffman 828-396-1741 911 or 828-296-4500 800-662-7956 For projects not in NC please list please personnel with phone numbers who should be contacted if a spill occurs. RESIDUALS SAMPLING PLAN Annually, or when land application occurs, multiple grab residual solid samples are collected from the aerated sludge digestion basins. These samples are composited for nutrient and metal analyses. The composited sample is mixed to keep the solids suspended and containers filled for this analysis. This facility may elect to meet Pathogen and vector attraction requirements by either lime stabilization or fecal values and SOUR test, aerobic digestion or volatile solids reduction. Testing or lime stabilization will occur when the sludge holding tank reaches capacity. After lime is added, field measurements of pH and temperature are collected for each stabilization event to insure pH requirements are met. pH values are later temperature corrected. Huffman Finishing Company may elect to meet pathogen reduction by the collection of 7 fecal samples. In addition, vector attraction reduction may be met by incorporation into the soil or collection of samples for the 30-day bench test for aerobic digestion or SOUR test depending on the percent solids. Annually, or when the residual solids are to be land applied if application occurs less than annually, a composite residual solid sample will be analyzed for: Arsenic, Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia — Nitrogen, Calcium, Nitrate -Nitrite, Nitrogen, Magnesium, % Total Solids, pH, Phosphorus, Potassium, TKN, and Sodium. From this information, the Plant Available Nitrogen (PAN) will be calculated. Once every permit cycle (if application occurs) a composite TCLP sample will be collected to include: Arsenic Hexachlorobenzene ph for Corrosivity Barium Hexachloro-1,3-Butadiene Benzene Hexachloroethane Flash point for ignitability Cadmium Lead Carbon Tetrachloride Lindane Sulfides and Cyanides for reactivity Chlordane Mercury 1,2-Dichloroethane Chlorobenzene Methoxychlor I,1-Dichloroethylene Chloroform Methyl Ethyl Ketone 2,4-Dinitrotoluene Chromium Nitrobenzene Endrin m-Cresol Pentachlorophenol Heptachlor and its Hydroxide o-Cresol Pyridine Trichlomethylene p-Cresol Selenium 2,4,5-Trichlorophenol Cresol Silver 2,4,6-Trichlorophenol 2,4-D Tetrachloroethylene 2,4,5-TP (Silvex) 1,4-Dichlorobenzene Toxaphene Vinyl Chloride RESIDUALS SOURCE CERTIFICATION ATTACHMENT - RSC 06-16 State of North Carolina Department of Environmental Quality Division of Water Resources Divlslon of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .I 100. Do not submit this certification for review without a corresponding application form (FORM: RLAP I1-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Man Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during - processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Huffman Finishing Company — Granite Falls, NC Status Code' Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current" Proposed R Huffman Finishing Company Huffman Finishing WWTP Caldwell W00002431 31 31 -Status Code for source facility are: ♦ N (New) o R (Renewed) ♦ M (Modifiedy ♦ D (Deleted) 'The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page I DDivlslon of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM,: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Huffman Finishing Company 2. Facility permit holder is: Federal, E] State, Q Local Government, or ® Private. Facility permit issued by: Div. of Water Resources, Div. of Environmental Health, or Other (explain:). 3. Facility contact person and title: M. Shuford Wise Complete mailing address: Post Office Box 170 City: Granite Falls State: NC Zip:28630-n Telephone number: (828) 244-9598 E-mail address: mshufordwise@outlook.com 4. Facility physical address: 4919 Hickory Blvd. City: Granite Falls State: NC Zip: 28630-4 Coordinates: Latitude: 35° 46' 11_10" N Longitude: 81' 23' 37_85" W Datum: NAD 1983 UTM 17N Level of accuracy: I" Method of measurement: Mao 5. Purpose of the facility: [] treatment of municipal wastewater, 0 treatment of I00%a domestic wastewater, 0 treatment of potable water, ED treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: 95 % industrial and 5 % domestic) I0. other (explain: ). 6. Does the facility have an approved pretreatment program: 0 Yes ® No 7. Facility permitted/design flow: 0.25 MGD and facility average daily flow: 1=I MGD 8. Average amount of residuals being generated at this facility 8 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals'treatment: 100.000 ,gallon Aerobic Sludge Basins Type and volume of residuals storage (i.e., outside of residuals treatment units): None IL RESIDUALS QUALITY INFORMATION (See Instruction C.): Specify if residuals are regulated under: 0 40 CFR Part 503 or Q 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological 0 Nan -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes I biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Pagel of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: [D yes no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes F11 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Research & Analytical Labs. Inc. and Date of analysis: 8/28/19 and 9/6/19 Passed corrosivity test: yes [] no. pH: s.u. (2 <pH < 12.5) Passed ignitability test: yes 0 no. Flashpoint: > 141 OF (> 140°F) Passed reactivity test: Eyes []no. HCN: <I mg/kg (<250) & H,S: <5 mg/kg (<500) TCLP Parameter Limit 0110) Result (ntgA) TCLP Parameter Limit (ntg/[) Result (ntgA) Arsenic 5.0 <0.10 Hexachlorobenzene 0.13 <0.05 Barium 100.0 0.131 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.05 Hexachloroethane 3.0 , <0.30 Cadmium 1.0 <0.005' Lead 5.0 <0.005 Carbon Tetrachloride 0.5 <0.05 Lindane 0.4 <0.04 Chlordane 0.03 <0.003 Mercury 0.2 <0.002 Chlorobenzene 100.0 <0.05 Methoxychlor lo.0 I <1.00 Chloroform 6.0 <0.5 Methyl Ethyl Ketone 200.0 I <0.05 Chromium 5.0 0.049 Nitrobenzene 2.0 I <0.2 m-Cresol 200.0 <20.0 Pentachlorophenol 100.0 <10.0 o-Cresol 200.0 <20.0 Pyridine 5.0 1 <0.50 p-Cresol 200.0 <20.0 Selenium 1.0 <0.100 Cresol 200.0 <20.0 Silver 5.0 <0.01 2,4-D 10.0 <1.00 Tetrachloroethylene 0.7 <0.05 1,4-Dichlorobenzene 7.5 <0.75 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.05 Trichloroethylene 0.5 <Q.05 1,1-Dichloroethylene 0.7 <0.05 2,4,5-Trichlorophenol 400.0 <40.0 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.20 Endri❑ 0.02 <0.002 2,4,5-TP (Silvex) 1.0 <0.100 Heptachlor and its Hydroxide 0.008 <0.0008 Vinyl Chloride 0.2 <0.05 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For DistributionfL.and Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 8/26/19 Parameter Ceiling Concentration Limits (ClassA & C1assB) (niglkg) Monthly Average Concentration Limits (ClassA Only) (ingAg) Result (inglkg) Arsenic 75 41 <11.10 Cadmium 85 39 <2 22 Copper 4,300 1,500 962.00 Lead 840 300 17.80 Mercury 57 17 116 Molybdenum 75 n/a <5.56 Nickel 420 420 52.90 Selenium 100 100 1 <11.10 Zinc 7,500 2,800 1,160.00 For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight i basis) for the following metal parameters: Laboratory: �� and Date of analysis: F-7 Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) [] > 0 but < 25 30 200 210 El > 25 but < 50 34 220 240 0 > 50 but < 75 39 260 270 ?:75 but < 100 46 300 320 Q > 100 but < 125 53 360 390 0 > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 4.51 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and C. W micronutrient parameters: Laboratory: Wavpoint Analytical and Date of analysis: 8/26/19 Parameter Result (mg/kg) Aluminum 5,130.00 Ammonia -Nitrogen 4,310.00 Calcium 4,980.00 Magnesium 1,940.00 Nitrate -Nitrite Nitrogen <22 20 pH (Standard Unit) 6.30 Phosphorus 5,380.00 Potassium 1,200.00 Sodium 1,070.00 Total Kjeldahl Nitrogen 76,700.00 Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.69 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the locaS Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): default value, or [] actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1") Year PAN Five -Year Maximum Adjusted PAN (^tglkg) (mg/kg) Surface 23,894 36,939 Injection/Incorporation 26,049 39,094 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Eattivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative I [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] -Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. EJ Alternative 5 [ 15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, thermophilic aerobic digestion, ❑ beta ray irradiation, gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class E: E Alternative 1 [ 15A NCAC 02T.1 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item U.S. below [15A NCAC 02T.1106(a)(2)]. El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1 107, specify how residuals will meet the VAR requirements: ® Alternative I [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Z Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 115A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. EJ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 i Facility Vicinity Map t Rhodhisr ,,�, ] in = 1.5 r cmc,ee, RTB oBnwn BY; RTB DAM 9/13/2019 MfS+ Huffman Finishing 1 Granite,Fatls i ra mishing Company ♦ \ „- 1'I1 t nonal S u'. eK WTr ;o any WWTP Sources: Esri, HERE, Del-orme, USCT,S, Intermap, II NRCan, Esri Japan, METI, Earl China (HongKong), (Thailand), Mapmylndia, NGCC, 0OpenStreetMap GIS User Community Huffman Finishing Comapny Facility Location BRANCH Granite Falls, NC RESIDUALS & SOILS, LLC �J� No. 2014-115 T P, Esri and the Facility Map Process Flow Diagram and Narrative PROCESS FLOW DIAGRAM AND NARRATIVE WWTP Huffman Finishing Company operates a 0.25 million gallon capacity aerobic wastewater treatment plant. After bar screening and grit collection, the influent goes into a equalization basin before entering an oxidation ditch. From the oxidation ditch, effluent enters a secondary clarifier where a portion on the sludge is recirculated back to the oxidation ditch and a portion of the sludge is sent to one of two aerated sludge holding tanks. Periodically air is removed from the holding tanks to allow settling and decant of the liquids. The decanted liquids are returned to the equalization tank. Water from the secondary clarifiers are sent to a chlorine contact chamber, on to cascading aeration step before discharge to a fountain aerator and discharge to Lake Hickory under permit NPDES NC0025135. This facility also has an additional clarifier that will allow sludge from the aerated holding tanks to be thickened and spread on drying beds if desired. INFLUENT SCREEN HUFFMAN FINISHING CO VIPA.NN' NV\t'TP PROCESS SCHEMATIC DECHLORINATION FACILITIES EQUALIZATION AERATION TANK TANK (OXIDATION DITCHI _ i CLARIFIER -1 EFFLUENT ..r.....n�.c '- CASCADE POST � CONTACT AERATION I SLUDGE REC(RCULAT(ON - TANK SLUDGE RECIRCULATION/ WASTE SLUDGE I WASTE PUMP STATION LAND APPLICATION I I �- FOUNTAIN AERATOR ALTERNATE SLUDGE HANDLING AER061C SLUDGE DIGESTION FACILITIES C7 LAKEHICKORY Justification for Residuals Production Rate JUSTIFICATION FOR RESIDUALS PRODUCTION RATE The dry tons limit for Huffman Finishing Company YPvV P should remain at 31 dry tons. Because application occurs rather infrequently ( last application was 2014), use of single year PAN rates is justified. Current production is well short of that and should provide enough margin for the next permit cycle. Residuals Sampling Plan RESIDUALS SAMPLING PLAN Annually, or when land application occurs, multiple grab residual solid samples are collected from the aerated sludge digestion basins. These samples are composited for nutrient and metal analyses. The composited sample is mixed to keep the solids suspended and containers filled for this analysis. This facility may elect to meet Pathogen and vector attraction requirements by either lime stabilization or fecal values and SOUR test, aerobic digestion or volatile solids reduction. Testing or lime stabilization will occur when the sludge holding tank reaches capacity. After lime is added, field measurements of pH and temperature are collected for each stabilization event to insure pH requirements are met. pH values are later temperature corrected. Huffman Finishing Company may elect to meet pathogen reduction by the collection of 7 fecal samples. In addition, vector attraction reduction may be met by incorporation into the soil or collection of samples for the 30- day bench test for aerobic digestion or SOUR test depending on the percent solids. Annually, or when the residual solids are to be land applied if application occurs less than annually, a composite residual solid sample will be analyzed for: Arsenic, Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia — Nitrogen, Calcium, Nitrate -Nitrite, Nitrogen, Magnesium, % Total Solids, pH, Phosphorus, Potassium, TKN, and Sodium. From this information, the Plant Available Nitrogen (PAN) will be calculated. Once every permit cycle (if application occurs) a composite TCLP sample will be collected to include: Arsenic Hexachlorobenzene ph for Corrosivity Barium Hexachloro-1,3-Butadiene Benzene Hexachloroethane Flash point for ignitability Cadmium Lead Carbon Tetrachloride Lindane Sulfides and Cyanides for reactivity Chlordane Mercury 1,2-Dichloroethane Chlorobenzene Methoxychlor 1,1-Dichloroethylene Chloroform Methyl Ethyl Ketone 2,4-Dinitrotoluene Chromium Nitrobenzene Endrin m-Cresol Pentachlorophenol Heptachlor and its Hydroxide o-Cresol Pyridine Trichloroethylene p-Cresol Selenium 2,4,5-Trichlorophenol Cresol Silver 2,4,6-Trichlorophenol 2,4-D Tetrachloroethylene 2.4,5-TP (Silvex) 1,4-Dichlorobenzene Toxaphene Vinyl Chloride Lab Analytical Reports and Operational Data 0 279Whitten Road, Memphis, TN3 aypo.ni. Main 901.213.2400 ° fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Mr. Bob Branch Project Huffman Finishing Report Date : 08/26/2019 1735 Heckle Blvd Information : Project# 2014-115 Received : 08/15/2019 Suite 103-291 Rock Hill , SC 29732 Report Number:19-227-0064 REPOR T OF A NA L YSrS Lab No : 93373 Sample ID : Huffman Finishing Matrix: Solids Sampled: Test Results Units MOL DF Date I Time Analyzed By Analytical Method Moisture 95.5 % 0.010 1 08/16/19 16:20 ADM 2540G-2011 Ammonia Nitrogen 4310 mg/Kg - dry 556 1 08/26/19 12:00 JPJ 4500NH3C-2011 Nitrate (NO3-N) <22.2 mg/Kg - dry 22.2 1 08/22/19 01:04 CCR 9056A Nitrite (NO2-N) <22.2 mg/Kg - dry 22.2 1 08/22/19 01:04 CCR 9056A Nitrate+Nitrite-N <22.2 mg/Kg - dry 22.2 1 08/22/19 01:04 9056A - pH 6.3 S.U. 1 08/22/19 07:40 JSL 9045 Total Solids 4.51 % 0.010 1 08/16/19 16:20 ADM 2540G-2011 Total Volatile Solids 83.2 % 0.010 1 08/16/19 16:20 ADM 2540G-2011 Total Kjeldahl Nitrogen 76700 mg/Kg - dry 5600 5 08/26/19 16:31 CLP 4500NORGD-2011 Phosphorus 5380 mg/Kg - dry ill 1 08/22/19 18:57 BKN 6010D Aluminum 5130 mg/Kg - dry ill 1 08/22/19 18:57 BKN 6010D Arsenic <11.1 mg/Kg - dry 11.1 1 08122/19 18:57 BKN 6010D Cadmium <2.22 mg/Kg - dry 2.22 1 08/22/19 18:57 BKN 6010D Calcium 4980 mg/Kg - dry 556 1 08/22/19 18:57 BKN 6010D Copper 962 mg/Kg - dry 5.56 1 08/22/19 18:57 BKN 6010D Iron 12500 mg/Kg - dry ill 1 08/22/19 18:57 BKN 6010D Lead 17.8 mg/Kg - dry 6.67 1 08/22/19 18:57 BKN 6010D Magnesium 1940 mg/Kg - dry ill 1 08/22/19 18:57 BKN 6010D Mercury 1.16 mg/Kg - dry 0.338 1 08/22/19 08:48 TJS 7471A Molybdenum <5.56 mg/Kg - dry 5.56 1 08/22/19 18:57 BKN 6010D Nickel 52.9 mg/Kg - dry 5.56 1 08/22/19 18:57 BKN 6010D Potassium 1200 mg/Kg - dry ill 1 08/22/19 18:57 BKN 6010D Selenium <11.1 mg/Kg - dry 11.1 1 08/22/19 18:57 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit ANALYTICAL 22972 Branch Residuals and Sails LLC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Mr. Bob Branch Project Huffman Finishing 1735 Heckle Blvd Information : Project# 2014-115 Suite 103-291 Rock Hill , SC 29732 Report Date : 08/26/2019 Received : 08/15/2019 Report Number :19-227-0064 REPORT OFANAL Y575 Lab No : 93373 Matrix: Solids Sample ID : Huffman Finishing Sampled: Test Results Units MQL DF Date l Time By Analytical Analyzed Method Sodium 1070 mg/Kg - dry 556 Zinc 1160 mg/Kg - dry 27.8 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit 1 08/22/19 18:57 BKN 6010D 1 08/22/19 18:57 BKN 6010D L Limit Exceeded a rs O Q y,, a point 279 a Whitten Road, Memphis, 21 .2440 �I as`i/ Main 901.213.2400 °Fax 901.213.2440 ANALYTICAL %, vw.waypointanalytical.com Cooler Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 19-227-0064 Shipping Method Fed Ex US Postal Lab UPS Client Courier Other: Thermometer ID: r45 Shipping container/cooler uncompromised? Yes _ No Number of coolers received Custody seals intact on shipping container/cooler? Yes No 0 Not Required Custody seals intact on sample bottles? - Yes No Not Required Chain of Custody (COC) present? Yes f No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? Yes No Sample containers intact? 0 Yes No Sufficient sample volume for indicated test(s)? S Yes No All samples received within holding time? Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Water - Sample containers properly preserved Yes No N/A Water - VOA vials free of headspace Yes No ® N/A Trip Blanks received with VOAs - Yes No N/A Soil VOA method 6035 - compliance criteria met Yes No N/A High concentration container (48 hr) Low concentration Encore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes No Comments Signature: Sovanchampa Yos Date & Time: 08/15/2019 11:49:46 The following parameters need to be analyzed on sample Huffman Finishing Regular Nutrient and Metal Residuals Analysis ,Crsenic /read Xckel ,Aluminum Total S011d5 �tassium ,ealcium Iron Bob Branch Branch Residuals & Soils 336 510-0340 Pidmium Mercury ,Sc4enium ,Attunonia-Nitrogen ,,,WN1 Yaanesium Project: Huffman Finishing Project Nc2014-115 mapper ,]biybdenum Zinc "Wrate-Nitrite Nitrogen Phosphorus41 Solids ,>Mlium I��I �I Q�I� ��II II�II� ulll ��II I��I VI�II Branch R�id.als and Sods LLC Huffman Fimshmu 19.227.0064 22972 08-15-2019 11 4836 (:;� JFJM -�q-15 6 5 � \ i 0 Ups RESEARCh & ANAlyTiCAl LAbORATORIES, BNCa Analytical/Process Consultations Toxicity Characteristic Leachale Procedure (TCLP) Analysis of Sample Identified as Huffman Finishing (A Branch Residuals & Soils Project #2014-115, collected 13 August 2019) [IF EPA IIW Quantitation Results Characteristic Number Contaminant Limit(m07L) (mP/L) Lcrel(me7L) EPA 0lclhud ), TCLP METALS D-004 Arsenic 0.010 - IIQL 5.00 6010C D-005 Barium 0.010 0.131, 100 6010C D 006 Cadmium 0.005 BQL- 1.00 6010C D-077 Chromium 0.010 0.049. 5.00 6010C D-008 Lad 0.005 BQL 5.00 6010C 6-009 Mercury 0.0020 BQL 0.200 7470A D-010 Selenium 0.100 BQL 1.00 6010C D-011 Silver 0.010 BQL 5.00 6010C ❑, TCLPVOLATILFS D-019 Benrene 0.050 BQL 0.500 8260B D-019 Carbon Tw3chloride 0.050 BQL 0.500 8260B D-021 Chlarabenzene 0.050 BQL 100 826011 D-022 Chlororarm 0.500 IIQL 6.00 8260B D 028 1,2-Dichloroethme 0.050 BQL 0.500 8260B D-029 1,1-Dichlornethylene 0,050 BQL 0.700 8260B D-035 Methyl Ethyl Krone 0.500 BQL 200 S2600 D-039 Tcnachlercethy1mc 0,050 BQL 0.700 82600 D-BI0 Triehloroethylene 0.050 BQL 0.500 6260D D-043 Vinyl Chloride 0.050 BQL 0200 8260B tll. TCLI'SE,%U-VOLATILES D-023 O-Creosol 20.0 IIQL 200 9270D D-024 \1-Crc0501 20.0 BQL 200 E270D 0-025 p-Creosol 20.0 BQL 200 8270D D-026 Creosol 20.0 BQL 200 8270D D-027 1,4-Diehloroberucoe 0.750 ' BQL 7.50 8270D D-030 2,4-Diniuotalucne 0,050 BQL 0.130 8270D D-032 Ilexachlorobcnnne 0.050 IIQL 0.130 8270D D-033 Hesachlmob nadicne 0.050 BQL 0.300 9270D D-034 Ilexachloraethae. 0.300 BQL 3.00 8270D D-036 Nitobrn oc 0.200 BQL 2.00 8270D D-037 Pentachlorophenal 10.0 BQL 100 8270D D-038 Pyridine 0.500 BQL 5.00 8270D D-041 2d,5.Trichlompheno1 40.0 IIQL 400 8270D D-042 2,4,6-Trichlorephenal 0.200 BQL 2.00 8270D IV. REACTIVITY 0-003 Cyanide 1.0 BQL 9010 D-003 Sul Ode 5.0 BQL 9030 V. CORROSIVITY D-002 pH Sul. Units 6.06 9045 VI. TCLP\IISCF.LLA\SOUS Paint Filter Test FLP VII. IGNITABILITY D-001 ILmiubility >141 1010 Sample Number 70658-01 Sample Date 08/13/19 Sample Time (It") 1027 Sample Niatrix Sludge WtiT - Will Not Ignite NFL = No Free Liquids mg/L = milligmms per Liter= parts pu million(ppm) FLP = Fee Liquids Present .,'kg -millignunsperkilogre=puupermillion(ppm) BQL Bela.Quantitation Limits v RESEARCH & ANALyTICAI ilO LALbORATORIES, INC. Analytical / Process Consultations ` Phone (336) 996-2641 CHAIN OF CUSTODY RECORD WATER I WASTEWATER MISC. CO PANYi i JOB NO. O o an•` ^ �2 \L �: °„ �°`„�"°' `'°ivy" °•r � ° 4oF QlC OF Q� f9 Q' Q' Q• �C ry h 'n v ,y v v v ly ry ry ry Ci, REQUESTED ANALYSIS STREETAOgRESS �Ye,�'�_ � a. 5.,..�� I a 3 Z! � PRONE T / -1�-��•tm� j�,Vr.,t,, CITY, ST��//l /.K�FI�� E,//��IP Sn� F LER NAME (PL5\SE PRINT) 1�YJ. CONTACT PHONE &13f�1�4 � R SAMPj SIGNAT � SAMPLE NUMBER (LABUSEONLS) DATE TIME COMP GRAD TEMP C TIES L hkl MMIII aE�.wvEo r s Xu Ew�ux Isow1 SAMPLELOCATI01111 -ORE1D:2 y y R Itf tll H 69I �jME J� 1 z1 RECEIVED BY 2 7 REMARKS: CnA SAMPLE TEMPERATURE AT RECEIPT 3 °C R LIND IS ED BY DATEINME RECEIVED BY Y Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Huffman Finishing (A Branch Residuals & Soils Project #2014-115, collected 06 September 2019) HF EPA HW Quantitation Results Characteristic Number Contaminant Limit(mfl/L) mg/L Level(m!/L) EPA Method I. TCLP PESTICIDES/lIERBICIDES D-020 Chlordane 0.003 BQL 0.030 SOS 1 B D-016 2,4-D 1.000 BQL 10.0 3151 A D-012 Endrin 0.002 BQL 0.020 8081 B D-031 Ileplachlor 0.0008 BQL 0.008 SON B D-013 Lindane 0.040 BQL 0.400 SOS 1 B D-014 Methoxychlor 1.000 BQL 10.0 SOSI B D-015 Toxaphene 0.050 BQL 0.500 8051 B D-017 2,4,5-TP(Silvex) 0.100 BQL 1.00 5151 A Sample Number 71651-01 Sample Date 09/06/19 Sample Time (hrs) 0942 Sample Matrix Sludee BQL = Below Quantitation Limits mgfL = milligrams per Liter = parts per million (ppm) mAg = milligrams per kilogram = pans per million (ppm) RESEARCH & ANALYTICAL LABORATORIES, INC. T Analytical / Process Consultations Phone (336) 996-2841 CHAIN OF CUSTODY RECORD WATER/WASTEWATER I MISC. C MPANY 7 ..c{ tE`,.�(.;ais sSs::is JOB NO. C,1Ll n; o i N �"�Uv a`2`day ��•�`' p'r y O �oF OF of 4� 0 Q' Q' Q• zc v ^! ry �,�" ryh �" �" ^ 0' '�� REQUESTED ANALYSIS STREETA�D/q RESS I. J Imo) J /(YC-���IC`J Zcl PROJE T Ir � j �. N-i��, )^ LTY, STATE, I3 SAMPLER NAM (PLEASE PRINT) CONTACT PHONE p—r�i72n 73l I [of SAjER SIGNA UE ifFi`Op•�oo'GOO' SAMPLE NUMBER (LAD USE ONLY) DATE TIME CDAP GARB TEMP .0 "Es pI ciaomuc n i sums R�%V) SAMPLE LOCATION I LO. 0 RELI Ql1 H 'F;Y A E�IME CEIVED BY REMARKS: SAMPLE TEMPERATURE AT RECEIPT J• I_°C RELINQUISHED BY DATE/TIME RECEIV BY LAND APPLICATION SITE CERTIFICATION ATTACHMENT - LASC 06-16 PY! Resources State of North Carolina Department of Environmental Quality Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T . 1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit the requested information for all land application sites. ❑ For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: ® The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes are as follows: ♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ❑ Attach the following in accordance with each status code: Status Code Required Item N R T M County Board Notification. doc Wt � ✓ ✓ ✓ Land Owner Agreement (If applicable) Setback Waiver Agreement An updated vicinity/setback map in accordance with the "Map Guidance ✓ ✓ ✓ for Residuals Land Avolication Permits' A soils and agronomic evaluation in accordance with the ".Soil Scientist ✓ ,k Evaluation Pot icy' INSTRUCTIONS FOR FORM: LASC 06-161'age 1 of An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs Status Code Required Item N R I T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation�" Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same timeperiod) This item may be required for land application site with a status code "M", please contact the Division if you need assistant in determining attachment requirements. ® Crop Type should include the most likely crop types for the life of the permit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ❑ For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. ® Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Digital or Raw Photo Extraction (EXT) • Aerial Photography with Ground Control (AER) • Geodetic Quality GPS Survey (GEO) • Cadastral Survey (SUR) • LORAN-C Navigation Device (LOR) • Conversion from Coordinate Plane (CP) • Navigation Quality GPS (GPS) • Conversion from Township -Section -Range (TSR) • Remote Sensing (RS) • Conversion from Universal Trans Merc (UTM) • Zip Code Centroid (ZIP) • Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) ❑ Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ❑ Surface water body classifications information may be found at: hitp•//deq.nc.2ov/about/divisionshvater- resources/plan n ins/classi ficali on-standards/classification s ❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: h ttp://deq. nc. a ov/c on tac t/re ei onal-o ft i ce s ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. I. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x I1-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link hltp'//den nc Qov/about/divisions/water-resources/plannine/classifteation-standards/classifications. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project information. ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15A NCAC 02B .0301(i). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah Basin And Savannah River drainage area entering South Carolina shall be classified "B Tr." River Drainage Area French Broad River Streams entering Tennessee will be classified "B." Basin Watauga River Basin Streams entering the State of Tennessee are classified 'C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Streams entering Virginia are classified "C," and such streams entering South Carolina are Basin classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described Roanoke River Basin shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River All drainage canals not noted in the schedule are classified "C Sw." except the main drainage Basin canals to Pamlico Sound and its bays which shall be classified "SC." Pas uotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16Page 3 of LAND APPLICATION SITE CERTIFICATION Applicant's name: Huffman Finishing Company Land application sites currently certified: 16.4 net acres and Total to be certified: 12.8 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Cade Site/Field ID Landowner(s) Lessee(s) or Operator(s) Net Acres County Crop(s) Predominant Soil Series Name n Mapping Unit or Rep. Slopee R 2 Lee Huffman 6.6 Caldwell Fescue Clifford CmB2 R 4 Lee Huffman 6.2 Caldwell Fescue Clifford CmB2 ' Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) ^ Soil Series Name (i.e. Appling, Cecil, etc.) ° Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed P Class lam" ❑° a a NAD 83 ADD Nearest Second [l° I? a u° [,' rj"" NAD 83 ADD Nearest Second El° D Do J° 11 Q" NAD 83 ADD Nearest Second ® ° L,l" G LJ [ ]0 ❑� 0" NAD 83 ADD Nearest Second a j' D [tT 0- NAD 83 ADD Nearest Second j° [2 ["j" El- E' []" NAD 83 ADD Nearest Second ['lo D j j" D° El,[]" NAD 83 ADD Nearest Second Uj° 11, El" Do D C" NAD 83 1 ADD Nearest Second Note: Please keep the site information (I.) and waterbody information (I1.) of the same field on the same page. FORM: LASC 06-16 Page I Landowner Agreement Attachments State of North Carolina D- WR 'Division of Water Resources Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Huffman Finishing Company hereinafter referred to as the Permittee, to land apply residuals from the following faeility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with tite stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) Z 4/o a M,`A.W/ )'eruct The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FnRM• T.11A 06-I F PROP. I of'; I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWI?, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Pennittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. S. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the .specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. _ 10. The landowner or his representative will provide the Permince with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Pernittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terns and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. II. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residualsisoil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the sail. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one). 15ANCAC 02L.0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T.0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance bounder provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundaryis needed for field(s) ID: _ (Please include the rationale for the requested re -location of the t boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) and attach a map showing the newly proposed compliance ❑ The land application field(s) ID: — is currently permitted udder another residuals land application program; Permit Number WQ: . The land owner hereby acknowledge that by �signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM- T )A O6-16 1 paoe..9 of 7 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of le land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: Address: City: rorAro%10- Era-bl5 State: C n Zip:2-R(,3 V Phone: Sag ' 301 L, - I I q I E-mail address: � �Y i� o S (� � ® A N, . bo m Signature: t 44t _n --- 1 re A�S 1am- rDate: clIII I to 1 9 VV NORTH CAROLINA, O �Gt� COUNTY I, the undersigned Notary Public do hereby certify that L_e� —T L7t'c M� d personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the t y� day of, 120 Signature and seal: 2 My commission expire . J Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified heiein. Signing official na e: Signature: OKI Ff1RM• LOA n6-16 Date: q[1712,06 -W Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Mon -Discharge Permitting Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM`. LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Huffman Finishing Company hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) do mA 4,j:IKA4 read The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM- T.nA n6-1F Pacer. 1 nf4 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terns and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non-Disebarge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must he kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. II. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. HLALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L.0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T.0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include therationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: . The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM- T.OA 06-16 Poor 9 nf4 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application sites) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: Address: N 0 5 0% t lI ICJ City: Co rAN tT -I_FineL l Q Y5 State: C zip: Z 8& 3 0 Phone: $ a 9 ��)�7„4 t E-mail address: is u F F 4 106 LTn ©A P H. Co /r%- - Signature, _�I i� ' "YWY^'^:— Date: q l t 1 120101 VV NORTH CAROLINA, (_� � LQn, COUNTY I, the undersigned Notary Public do hereby certify that Le - T �A V � personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the I j . day of Signature and seal: My commission expires: Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing off Signature: FC)RM• IfIA 06-16 Updated Maps Site Vicinity Maps rJJar, Air;,o Hai , °ry SCALE: I - 1.500 CHECKED BY: RTB DMWN BY: RTB DATE: 12/5/2014 erg a, Rive rbenr a� �a GudP° 0ld Farn Goat Lot T. � �Pa4✓eys Grove _Church - -_ } �m� I r gym/ Pe � yF c, Lee Huffman Farm L At 3 d Farm Gunpowder CrAek Boa � m; I Wolfe a<a Pr O Q L � Catawba River rt Huffman Finishing Company Land Application Program Site BRANCH Lee Huffman Farm Vicinity *&RSSOILLS, ESIDUALS Map LLC 2014-115 Buffer Maps 1aii3el e, �\ Y� r � r. v III It11 214� I J.- i 7 t 4 r rr tiF+r'IB2 N� a Legend Cemetery Church ■ Houses Off Property Structures Wells —Off —Site 100—YR Floodplain .— Drainage Feature K— Fences Parcel Lines - Streets Stream ® Buffer _ Huffman Application Fields Ponds ., i All locations are approximate and have not been suneycd. .'5...'y Data pmvidud by: Q USDA National Agricultmal Imagery Program and Caldwell County GI& Compliance Boundary is either 250 fret from the residuals land application area or 50 feet from the propoerty line, whichever is closest. Review Boundary is midway between the Compliance Boundary and the residuals land application area. scu.e: 1 " = 660 ft Huffman Finishing Company CHECKED BY: RTB Land Application Program Huffer 4i&k BRANCH Lee Huffman Farm Map DRAWNBY: RTB RESIDUALS n,rr:: 9/13/2019 & SOILS, LLC Emf nNo. 2014-115 Cumulative Pollutant Loading Rates ANNUAL LAND APPLICATIONFIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORMITO:BE COMPLETEIDAND. SUBM&ITEDTOR EACH APPLICATION FIELD. PLACE A "NIA"'IN A BLANK ORBOX WHEN NOT APPLICABLE. Facility Name: Hu fmzn.Finishing-Company WQ'Permit #1 W00002431 Field#: HufHnm AcresUdUtcd: 6.60 Owner: LeeHufriisn Annual:Dry Tons Applied: 16.54 Site:#: 2 Acres; Permitted: 6.60 Operator.' Lm Huffrcan Predominat Soil Series Fang Cation Exchange Capacity (non 503): NA CropJ Name; Fescoe Crop•1 Mu PAN: 194.00 Crop.2 Nome: #N/A Crop 2 MM PAN BNIA I ' - • .w--��aii '.'Y' ®�i��.-S®©���®��®t�l�tt.Yt:�7 ,_.��swiwlnrwsr+wrA�7��-111+it77aT1 a_.�@lr rr.,•.• _.rf?'--C#7d:.�� ••,• "I certify, WmW penalty of law„thrat this:docament•waaprepar'ea uuaer MY mrecouo oraupervmuu m.au u..+..+.........r. - deedgmed to assure' bat qualified,personnel properly gathered and evaluated the -information iobmitt d. I am,awam that:there an sipmeant penalties for submitting false information, including the posilbffity-of fines and imprisonmentfor"Inowing.Vlolatlom " •Applkadoa Method: S - Sudsce, IN - bjecdoi, INC - Incorporatim "VoUtd[utionRate:<Suiface-0.51-InjeetionantoWAtion:--1.0 Date ••'Minerallun Ra tes: - 0.1,•Anaerobledly Digested - 01, Signature of.Land Applier Aerobically Digested - OA Raw Sludge w OA r*a•C.P.LJL:-Cumu]Adve Pollutant Loading Rate, DENR FORM FSF (1212005) RECEIVED AQUIFER PROTECTION SECTION APPLICATION REVIEW REQUEST FOR]MAR 0 �U6 Date: March 3.2006 Asheville Regional Office AquMer Protection To: ® Landon Davidson, ARO-APS ❑ David May, WaRO-APS ❑ Art Barnhardt, FRO-APS ❑ Charlie Stehman, WiRO-APS ❑ Andrew Pitner, MRO-APS ❑ Sherri Knight, WSRO-APS ❑ Jay Zimmerman, RRO-APS From: David Goodrich , Land Application Unit Telephone: (919) 715-6162 Fax: (919) 715-0588 E-Mail: david.eoodrichna ncmail.net A. Permit Number: W00002431 B. Owner: Huffman Finishing Company C. Facility/Operation: Land Application Program ❑ Proposed ® Existing ® Facility ® Operation D. Application: 1. Permit Type: ❑ Animal ❑ Surface Irrigation ❑ Reuse ❑ H-R Infiltration ❑ Recycle ❑ I/E Lagoon ❑ GW Remediation (ND) ❑ UIC - (5QW) closed loop water only geothermal For Residuals: ® Land App. ❑ D&M ❑ Surface Disposal ® 503 ❑ 503 Exempt ❑ Animal 2. Project Type: ❑ New ❑ Major Mod. ❑ Minor Mod. ❑ Renewal ® Renewal w/ Mod. E. Comments/Other Information: ❑ I would like to accompany you on a site visit. Statutory Date: Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 30 calendar days, please take the following actions: ® Return a Completed Form APSARR. ❑ Attach Well Construction Data Sheet. ❑ Attach Attachment B for Certification by the LAPCU. ❑ Issue an Attachment B Certification from the RO*. * Remember that you will be responsible for coordinating site visits, reviews, as well as additional information requests with other RO-APS representatives in order to prepare a complete Attachment B for certification. Refer to the RPP SOP for additional detail. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office -Aquifer Protection Section contact person listed above. RO-APS Reviewer: Date: FORM: APSARR 02/06 Page 1 of 1 Request for Renewal and Minor Modification of Permit No. WQ0002431 Non -Dedicated Residuals Land Application Program Huffman Finishing Company July 2004 Prepared by: The Wooten Company 120 North Boylan Avenue Raleigh, North Carolina 276( (919) 828-0531 n FCVON JUr! 2 4 Z0,04 J AjI3E pEAMIT7ING THE WOOTEN COMPANY ENGINEERING 12MMILIEWRO A H CH IT EC TU RE 120 North Boylan Avenue °sleigh NC 27603-1423 919.828.0531 fax 919.834.3589 June 24, 2004 Mr. Kim Colson, Supervisor NCDWQ Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Residuals Land Application Program Permit Renewal & Modification Huffman Finishing Company Permit No. WQ0002431 Dear Mr. Colson: On behalf of Huffman Finishing Company, enclosed please find one (1) original and three (3) copies of an application to request renewal and modification of the above -referenced permit. Also enclosed is a check in the amount of $205.00 made payable to NCDENR to cover the permit modification fee. Each application package is divided into the following sections: Form NDRLAP with required attachments Form RSCA with required attachments Form LASCA with required attachments Forms LOAA with required attachments Please take note of the following items regarding the permit application contents: 1. The Permittee has used Bionomic Services Inc. as the residual management firm for providing the required Operator in Responsible Charge (ORC) and Backup ORCs for the residual land application program. The Permittee is currently in the process of selecting a new residual management firm to provide the same services. Once the selection for residual management is made, the required information for Section I11.1 of Form NDRLAP will be forwarded to your office. 2. The Permittee desires to increase its permitted disposal from 19 dry tons per year to its design condition for 31 dry tons per year. Calculations are provided to justify the requested increase. 3. The Permittee desires to decrease its permitted disposal area from 80 acres to 67.7 acres. The reduced acreage is based on net (buffered) acreage as shown in the site maps. No existing sites are proposed to be removed from the Permit. 4. Sludge has not been previously applied to the J.P. Baumgarner and J.F. Miller application sites by the Permittee. Therefore, no cumulative pollutant field loading summaries are available for these two (2) sites. The field loading summary from the 2003 Annual Report for the Huffman Finishing site is included in this package. Should you have any questions about the application contents, please contact our office at (919) 828-0531 or Mr. Lee Huffman at (828) 396-1741. Sincerely, THE W,OOTENf-034PANY cc: Lee Huffmfin, Huffman Finishing Company FC: gdh enclosures JUN 2 4 2n04 I NpN-p�gCHA State of North Carolina Department of Environment and Natural Resources Division of Water Quality NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAMS (THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL) Application Number: I. GENERAL INFORMATION (See Instruction B.): 1. Applicant's name: Huffman Finishing Company 2. Signing official's name and title: A.W. Huffman, Jr.. President 3. Complete mailing address of applicant: Post Office Box 170 (to be completed by DWQ) City: Granite Falls State: NC Zip: 28630 Telephone number: (_828_) 396-1741 Facsimile number: (_828_) 3964235 E-mail address: HUFFHOSLTH( AOL COM 4. Name and complete mailing address of contact person and/or consulting firm who prepared application: _ Gary Hartong The Wooten Company. 120 North Boylan Avenue City: Raleigh State: NC Zip: 27603 Telephone number: (_919_) 828-0531 Facsimile number: (_919_) 834-3589 E-mail address: GHartong@TheWootenComoanvcom 5. County where residuals land application program is headquartered: Caldwell 6. County(ies) where residuals source -generating facilities are located: Caldwell 7. County(ies) where land application sites are located: Caldwell 8. Fee submitted: S 205.00 II. PERMIT INFORMATION: 1. Application is for: ❑ new, ® modified, ® renewed permit (check all that apply). 2. If this application is being submitted to renew or modify an existing permit, provide the following: the permit number W00002431 the most recent issuance date Sept. 30, 1999 , and the expiration date Aug; 31. 2004 Date of most -recently certified Attachment A: Date of most -recently certified Attachment B: FORM: NDRLAP 02/02 Page 2 of 5 firCFIV�FD ..., SFCTION J U N 2 4 2004 Attachment Orden D16CHhn..L PERMITTING 3. Check all that apply to the requested permit modification: ® INCREASE ❑ DECREASE ❑ ADD ❑ DELETE ❑ INCREASE ® DECREASE ❑ ADD ❑ OTHER. ❑ DELETE Explain: the maximum permitted annual dry tonnage for existing residuals source -generating facility(ies) certified for this residuals land application program. residuals source -generating facility(ies) to/from those certified for this residuals land application program. the net acreage associated with land applications site(s) currently certified for this residuals land application program. land application site(s) to/from those certified for this residuals land application program. III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Who will be responsible for the day-to-day management of the residuals land application program: ❑ Permittee or ® residuals management firm. If a residuals management firm, complete the following: Firm contact person and title: To Be Determined (TBD) Firm name and complete mailing address: City: TBD State: TBD Zip: TBD Telephone number: ( ) TBD Facsimile number: (_) TBD E-mail address: TBD 2. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC TBD TBD TBD Back -Up ORC TBD TBD TBD Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: TBD FORM: NDRLAP 02/02 Page 3 of 5 Attachment Order 1 3. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitro¢en Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 31 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 50.6 55.5 1569 1721 Five -Year Maximum Adjusted 92.9 97.8 2881 3033 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation 0 Row Crops 0 Hay 0 Pasture 67.7 Total: 67.7 Methods Surface 56.7 Incorporation or Injection 11.0 Total: 67.7 r Restrictions Year -Round 67.7 Seasonal 0 Total: 67.7 — — =" PC c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: i "ON ?MITI'IlVG Assumed Acres Required Using Acres Required Using Application Rate First -Year PAN Concentrations Five -Year Maximum Adjusted PAN Qbs PAN/ac yr) Concentrations Surface Incorporation or Surface Incorporation or Injection Injection 70 22.41 24.58 41.16 43.33 150 10.46 11.47 19.21 20.22 250 6.28 6.88 11.52 12.13 FORM: NDRLAP 02/02 Page 4 of 5 Attachment Order I 4. Identify and provide a plan as well as a schedule to resolve any issues that would prevent all of the residuals currently certified and proposed for certification to be land applied without exceeding agronomic razes or violating any of North Carolina's standard permit conditions governing residuals land application programs (e.g., not enough storage, not enough land, etc.): Applicant's Certification: 1, Gary D. Hartong , attest that this application for Huffman Finishing Company Land Application Permit Renewal has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Quality may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Quality should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.613, any person who knowingly makes any false statement, representation, or certification in anVpplication shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 s well as c.. I p alties up to $25,000 per violation. Signature: Date: `�.��/.1'DM01 E COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHOULD BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 By Courier/Special Delivery: 512 NORTH SALISBURY STREET, SUITE 1219 RALEIGH, NORTH CAROLINA 27604 TELEPHONE NUMBER: (919) 733-5083 *** END OF FORM NDRLAP 02/02 *** I L ----. -- J nl 2 �n04 FORM: NDRLAP 02102 Page 5 of 5 Attachment Order 1 t�OUVU14�q go, INFANTS, CHILDREN'S, MISSES' AND MENDS HOSIERY June 16, 2004 Mr. Kim Colson, Supervisor NC DENR Division of Water Quality Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Non -Discharge Permit Renewal Application Permit No. WQ0002431 Dear Mr. Colson: JUN, 2 4 2004 This letter is to confirm that The Wooten Company is the Authorized Representative for Huffman Finishing Company, Inc. in the preparation of the enclosed Non -Discharge Permit Renewal Application. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submittingfalse information, including the possibility of fine and imprisonment for knowing violations. If you need additional information, please contact Gary Hartong with The Wooten Company at (919) 828-0531 or myself at (828) 396-1741. Sincerely, 4 w A.W. Huffman, Jr. President I -__j P.O. Box 170 • Granite Falls, North Carolina 28630 Telephone: (828) 396-1741 • tAX: (828) 396-4235 Applicant's name: Huffman Finishing Company Check all that apply: ❑ NEW RESIDUALS PROGRAM ® RENEWED RESIDUALS PROGRAM ® INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for this residuals source -generating facility certified for this residuals program. Current: _19_ and proposed: _31_ dry tons per year. ❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for this residuals program. ❑ OTHER Explain: N/A I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Name of facility: Huffman Finishing Company 2. Facility permit holder: Huffman Finishing Company Facility permit holder is (check one): ❑ federal, ❑ state, ❑ local government, or ® private. Facility permit number: W00002431 Facility permit issued by (check one): ® Div. of Water Quality, ❑ Div. of Environmental Health, or ❑ other (explain: 3. If the facility permit is not issued by the Div. of Water Quality, complete the following: a. Facility contact person and title: N/ Facility complete mailing address: City: N/A State: N/A Zip: N/A Telephone number: (_) N/A Facsimile number: (_) N/A E-mail address: b. Facility complete location address: 4919 Hickory Boulevard City: Granite Falls State: NC Zip: 28630 County: Caldwell Latitude: 35° 46' 17" N and longitude: 81' 23' 27" W 4. Purpose of the facility (check one): ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ® treatment of industrial wastewater mixed with domestic wastewater, or (approximate percentages: _>97_ % industrial and _<3_ % domestic) ❑ other (explain: 5. is the facility required to have an approved pretreatment program: ❑ yes ® no. If yes, please specify whether or not such a pretreatment has been approved: ❑ yes ❑ no. 6. Facility permitted/design flow: _0.250_ MGD and facility average daily flow: _0.111_ MGD. 7. Maximum amount of residuals to be certified for this facility: _31_ dry tons per year. _ r,-i P,II,-; N6 8. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Aerobic Sludge Digester (45,815 al Type and volume of residuals storage (i.e., outside of residuals treatment units): II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under (check one): ❑ 40 CFR Part 503 or ® 40 CFR Part 257. 2. Specify if residuals are intended for (check one): ❑ Land Application/Distribution (Class A or Equivalent). Complete all items EXCEPT Items II.4b, 4c., 7b., and 7c. ® Land Application (Class B or Equivalent). Complete all items EXCEPT Items II.4a., 4c., 7a., and 7c. ❑ Surface Disposal. Complete all items EXCEPT Items II.4a., 4b., 5., 7a., 7b., and 8. 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): N/A b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-§261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: laboratory: Test America and date of analysis: 11/26/02 & 2/6/04 (TCLP) Passed corrosivity test: ® yes ❑ no. pH: _7.8_ s.u. (2 < pH < 12.5). Passed ignitability test: ® yes ❑ no. Flashpoint: _>200_ °F (> 140°F). Passed reactivity test: ® yes ❑ no. HCN: _<50_ mg/kg (<250) & HZS: _< 100_ mg/kg (<500). TCLP Parameter Limit (mg/L) Result (mg/L) TCLP Parameter Limit (mg/L) Result (mg/L) Arsenic 5.0 <0.1 Hexachlorobenzene 0.13 <0.01 Barium 100.0 <1.0 Hexachloro-1,3-Butadiene 0.5 <0.01 Benzene 0.5 <0.02 Hexachloroethane 3.0 <0.01 Cadmium 1.0 <0.I Lead 5.0 <0.5 Carbon Tetrachloride 0.5 <0.02 Lindane 0.4 <0.0008 Chlordane 0.03 <0.0005 Mercury 0.2 <0.01 Chlorobenzene 100.0 <0.02 Methoxychlor 10.0 <0.0005 *** TABLE CONTINUES ON NEXT PAGE *** *** TABLE CONTINUED FROM PREVIOUS PAGE *** TCLP Parameter Limit (mg/L) Result (mg/L) TCLP Parameter Limit (mg/L) Result (mg/L) Chloroform 6.0 <0.02 Methyl Ethyl Ketone 200.0 <0.1 Chromium 5.0 <0.9 Nitrobenzene 2.0 <0.01 m-Cresol 200.0 <0.02 Pentachlorophenol 100.0 <0.01 o-Cresol 200.0 <0.02 Pyridine 5.0 <0.02 p-Cresol 200.0 <0.02 Selenium 1.0 <0.1 Cresol 200.0 <0.02 Silver 5.0 <0.1 2,4-D 10.0 <0.2 Tetrachloroethylene 0.7 <0.02 1,4-Dichlorobenzene 7.5 <0.01 Toxaphene 0.5 <0.01 1,2-Dichloroethane 0.5 <0.02 Trichloroethylene 0.5 <0.02 1,1-Dichloroethylene 0.7 <0.02 2,4,5-Trichlorophenol 400.0 <0.01 2,4-Dinitrotoluene 0.13 <0.01 2,4,6-Trichlorophenol 2.0 <0.01 Endrin 0.02 0.003 2,4,5-TP (Silvex) 1.0 <0.01 Heptachlor and its Hydroxide 0.008 <0.0006 Vinyl Chloride 0.2 <0.02 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 40 CFR Part 503 or 40 CFR Part 257: a. For Class A or Equivalent: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: laboratory: N/A - and date of analysis: N/A Parameter Analysis Required for Permitting by NC if Residuals are Regulated Under... Parameter Ceiling Concentration (mg/kg) Monthly Average Concentration (mg/kg) Result (mgAg) 40 CFR Parts 257 and 503 Arsenic 75 41 N/A 40 CFR Parts 257 and 503 Cadmium 85 39 N/A 40 CFR Parts 257 and 503 Copper 4,300 1,500 N/A 40 CFR Parts 257 and 503 Lead 840 300 N/A 40 CFR Parts 257 and 503 Mercury 57 17 N/A 40 CFR Parts 257 and 503 Molybdenum 75 n/a N/A 40 CFR Parts 257 and 503 Nickel 420 420 N/A 40 CFR Parts 257 and 503 Selenium 100 100 N/A 40 CFR Parts 257 and 503 Zinc 7,500 2,800 N/A b. For Class B or Equivalent: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: laboratory: A&L Eastern Aericultural Lab and date of analysis: 2/5/2004 Parameter Analysis Required for Permitting by NC if Residuals are Regulated Under... Parameter Ceiling Concentration (mg/kg) Result (mg/kg) 40 CFR Parts 257 and 503 Arsenic 75 1.00 40 CFR Parts 257 and 503 Cadmium 85 < 1.00 40 CFR Parts 257 and 503 Copper 4,300 222 40 CFR Parts 257 and 503 Lead 840 10 40 CFR Parts 257 and 503 Mercury 57 1.58 40 CFR Parts 257 and 503 Molybdenum 75 < 5.00 40 CFR Parts 257 and 503 Nickel 420 14 40 CFR Parts 257 and 503 Selenium 100 7.40 40 CFR Parts 257 and 503 Zinc 7,500 383 c. For Surface Disposal.* Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: laboratory: and date of analysis: Parameter Analysis Required for Permitting by NC if Residuals are Regulated Under... Closest Distance to Property Lines (meters) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) 40 CFR Parts 257 and 503 > 0 but < 25 30 200 210 40 CFR Parts 257 and 503 >_ 25 but < 50 34 220 240 40 CFR Parts 257 and 503 >_ 50 but < 75 39 260 270 40 CFR Parts 257 and 503 >_ 75 but < 100 46 300 320 40 CFR Parts 257 and 503 >_ 100 but < 125 53 360 390 40 CFR Parts 257 and 503 >_ 125 but < 150 62 450 420 40 CFR Parts 257 and 503 >_ 150 73 600 420 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: _0.37_%. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: laboratory: A&L Eastern Agricultural and date of analysis: Parameter Result (mg/kg) Aluminum 2,450 Ammonia -Nitrogen 8,100 Calcium 6,200 Magnesium 3,700 Nitrate -Nitrite Nitrogen 486 pH 7.80 Phosphorus 5,500 Potassium 13,300 Sodium 78,100 Total Kjeldahl Nitrogen 97,300 c. Using the results listed in Item II.5b. above, calculate the sodium adsorption ration (SAR): _I 1.10_. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: _30_ %. This rate is a ® default value or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: _ The biosolids primarily include the waste biomass from the activated sludge system at the plant so a 30% default value is used for the aerobically stabilized sludge Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following table: Application Method First Year Five -Year PAN Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 25,304 46,468 Injection/Incorporation 27,754 48,918 e. Are the residuals are a registered fertilizer with the NC Department of Agriculture and Consumer Services: ❑ yes ® no. If yes, provide date of registration approval: N/A the current registration number: N/A and the fertilizer equivalent: _N/A_ %, N/A_ %, and N/A_ %. 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and list the results of the latest analyses : 7. Pathoeen Reduction Determination: Specify which altemative(s) will be used to meet the pathogen reduction requirements: a. For Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids. OR ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed): ❑ Alternative 1 [40 CFR §503.32 (a)(3)] - Time/Temperature Compliance. ❑ Alternative 2 [40 CFR §503.32 (a)(4)] - Alkaline Treatment. ❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric VimsNiable Helminth Ova. ❑ Alternative 4 [40 CFR §503.32 (a)(6)] - No Prior Testing for Enteric V irusNiable Helminth Ova. ❑ Alternative 5 [40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation. ❑ Alternative 6 [40 CFR §503.32 (a)(8)] - PFRP-Equivalent Process. Explain: b. For Class B or Equivalent: ❑ Alternative 1 [40 CFR §503.32 (b)(2)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [40 CFR §503.32 (b)(3)] - Process to Significantly Reduce Pathogens (PFRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. ❑ Alternative 3 [40 CFR §503.32 (b)(4)] - PSRP-Equivalent Process. Explain: ® Not Applicable -Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. c. For Surface Disposal: ❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover. ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11.7b. above. ❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction Determination: Specify which altemative(s) will be used to meet the vector attraction reduction requirements: ❑ Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 (40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [40 CFR §503.33 (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 (40 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [40 CFR §503.33 (b)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization. ❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 (40 CFR §503.33 (b)(8)] - Drying ofUnstabilized Residuals. ❑ Alternative 9 140 CFR §503.33 (b)(9)] - Injection. ❑ Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover. ❑ Alternatives for Animal Processing Residuals Only: Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10. ® Not Applicable - Non -Animal Processing Residuals Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. *** END OF FORM RSCA 02/02 *** PAN Calculations 1. Design Considerations: Assume subsurface application: Total dry tons per year = TKN (mg/kg dry wt.) _ NH3-N (mg/kg dry wt.) _ NO2-NO3-N (mg/kg dry wt.) _ Dates of Analysis: t12m= 2/32004 31 80,150 (2 sample ave) 4,900 (2 sample ave) 279 (2 sample ave) Rate, % of Organic-N Mineralization Rate = Year Organic-N (MR) (Aerobic Digestion) 0-1 30% 1-2 15% 2-3 7.5% 3-4 3.8% — rp 2. Plant Available Nitrogen (PAN): 1st Year PAN (mg/kg) _ ((MR) x (TKN - NH3)) + (NH3) + (NO2-NO3-N) JUN 2 4 2-5 Year PAN (mg/kg) = Previous Year Pan + [(MR) x (TKN - NH3)] L I PAN (Ibs PAN/dry ton) = PAN (mg/kg) x 0.002 Wi'-DISCHARGE P_ERRMMM-lb PAN (Ibs PAN/year) = PAN (Ibs PAN/dry ton) x Total dry tons per year Required Acres = PAN (Ibs/year) / Application Rate (Ibs PAN/ac yr) 1) For first year: PAN = 27,754 mg/kg Loading 70 Rate (Ibs PAN/ac 150 yr) 250 PAN = 55.5 Ibs/dry ton PAN = 1721 Ibs/year Required Acres 24.58 11.47 6.88 2) For second year: PAN = 39,042 mg/kg PAN = 78.1 Ibs/dry ton PAN = 2421 Ibs/year Required Acres 34.58 16.14 9.68 3) For third year: PAN = 44,685 mg/kg PAN = 89.4 Ibs/dry ton PAN = 2770 Ibs/year Required Acres 39.58 18.47 11.08 4) For fourth year: PAN = 47,507 mg/kg PAN = 95.0 Ibs/dry ton PAN = 2945 Ibs/year Required Acres 42.08 19.64 11.78 5) For fifth year: PAN = 48,918 mg/kg PAN = 97.8 Ibs/dry ton PAN = 3033 Ibs/year Required Acres 43.33 20.22 12.13 PAN Calculations 1. Design Considerations: Dates of Analysis: 11rz4rzoo2 Assume surface application: =004 Total dry tons per year = 31 TKN (mg/kg dry wt.) = 80,150 (2 sample ave) NH3-N (mg/kg dry wt.) = 4,900 (2 sample ave) NO2-NO3-N (mg/kg dry wt.) = 279 (2 sample ave) Rate, % of Organic-N Mineralization Rate = Year Organic-N (MR) (Aerobic Digestion) 0-1 30% 1-2 15% 2-3 7.5% 3-4 3.8% 4-5 1.9% 2. Plant Available Nitrogen (PAN): 1 st Year PAN (mg/kg) = ((MR) x (TKN - NH3)) + (0.5 x NH3) + (NO2-NO3-N) 2-5 Year PAN (mg/kg) = Previous Year Pan + [(MR) x (TKN - NH3)] PAN (Ibs PAN/dry ton) = PAN (mg/kg) x 0.002 PAN (Ibs PAN/year) = PAN (Ibs PAN/dry ton) x Total dry tons per year Recuired Acres = PAN (Ibs/vear) / Application Rate (Ibs PAN/ac yr) 1) For first year: 2) For second year: 3) For third year: 4) For fourth year: 5) For fifth year: Loading Rate (Ibs PAN/ac yr) 70 150 250 PAN = 25,304 mg/kg PAN = 50.6 Ibs/dry ton PAN = 1569 Ibs/year Required Acres 22.41 PAN = 36,592 mg/kg PAN = 73.2 Ibs/dry ton PAN = 2269 Ibs/year Required Acres 32.41 PAN = 42,235 mg/kg PAN = 84.5 Ibs/dry ton PAN = 2619 Ibs/year Required Acres 37.41 PAN = 45,057 mg/kg PAN = 90.1 Ibs/dry ton PAN = 2794 Ibs/year Required PAN = 46,468 mg/kg PAN = 92.9 Ibs/dry ton PAN = 2881 Ibs/year 39.91 Acres 41.16 fi[ILid 6.28 15.12 9.07 17.46 10.47 18.62 11.17 19.21 11.52 FACILITIES EQUALIZATION TANK AERATION TANK (OXIDATION POST DECHLORINATION CHLORINE CONTACT TANK CLARIFIER POSTAERATION SCREEN �� I EFFLUENT 1 ♦ SLUDGE RECIRCULATIOW WASTE PUMP STATION • SLUDGE RECIRCULATION I SLUDGE STABILIZATION/ I 1 SLUDGE DRYING BEDS y STORAGE BASIN WASTE SLUDGE 1 1 DIGESTED SLUDGE -� _ _ DEWATERED STABILIZED - 1 SLUDGE TO LANDFILL I T I 1 I I 1 I 1 --_ _-_---- L BED UNDER DRAINAGE AEROBIC SLUDGE TO LAND APPLICATION SITES DIGESTION FACILITIES EXHIBIT RSCA-2 SCHEMATIC FLOW DIAGRAM HUFFMAN FINISHING WASTE TREATMENT PLANT NOTE: EITHER LIQUID OR DEWATERED STABILIZED SLUDGE WILL BE DISPOSED OF BY CONTRACT OPERATIONS WASTEWATER - - - - - - - SLUDGE PROCESS FLOW DIAGRAM AND/OR NARRATIVE ( Attachment Order 2-b ) Huffman Finishing Company operates a 0.25 mgd extended aeration type activated sludge plant which discharges its effluent into Unnamed Tributary of Catawba River in accordance with the requirements set forth in the NPDES Permit No. NC0025235. The unit operations/processes at the plant include screening, pre-dechlorination, flow equalization, extended aeration(Oxidation Ditch) type activated sludge system, chlorine disinfection, post dechlorination, cascade type post aeration, aerobic sludge digestion,sludge storage basin,and sludge drying beds. The excess sludge produced in the biological treatment(activated sludge system) is removed by wasting it to the aerobic digestion process. The sludge is stabilized in the aerobic digestion process and after stabilization it is decanted and discharged to either sand beds for dewatering or to sludge storage basin for further stabilization and storage. The dewatered sludge from the sand beds is disposed off at the County landfill while the liquid stabilized sludge is disposed off at the permitted land application sites, in accordance with the requirements set forth in the Permit No. WQ0002431. Exhibit RSCA-2 shows the process flow diagram of the treatment plant. ... QLL,saxi�cAti_.+.t, cTWtIM-tUtAYv�7:..._(FLrlt.. RL.si.��u-c...p.iRoia�axt.be� !tA'at G DODS V,&" . lbB.01, cl,.o3),c o.ol �ali-1'� Y�I Y&AUL"'" F+" 43�'O �h'� CljI na,%Lcw� r 'L 4.i-, 4 i g r�� dAL vi • .L 5 •aiiY.l ►t Flo, *-kO" ` 3.1 �v� a.•a.�lY.�.w+ .4e"LkIn 'A Jen n i w xLdga umi — . C2114. l — t�d r� 1 loco .itt G 6o-ao u� .2o-uo bbt`a.ny - r . o_ 5 5-tVL SAMPLING PLAN (Attachment Order 2-d) Sampling of biosolids will be performed in accordance with the guidance given in Chapter 6 of the EPA, -A Plain English Guide to the EPA Part 503 Biosolids Rule„ September 1994 and the pertinent requirements contained in the Permit. % A & L EASTERN AGRICUL IAL LABORATORIES, INC. 7621 Whilepine Road • Richmond, Virginia 23237 • (804) 743-9401 Fax No. 4604) 271-6446 R,342-02b ACCOUNT R 45671 P IGE 1 VC1, lrPtf: REPORT NUMBER `a...i' ..`. . 3I0--NOM'1.0 SERVICES, IHC. 516 RGUNDTREE RD CRORLOTTE NC 28217 LAB NUMBER = 44000 SAMPLE ID = HUFFMAN FINTSH'ING RESULT PARAMETER ( ) nn 1 }{UFFFIAN FIN1. 116�EC :'I;,' DAVTD MOT[L NC CERT 11257- -------------- ANALYSIS REPORT DATE SAMPLED 11/24/02 DATE RECEIVED 12/02/02 DATE REPORTED 12/06/02 DETECTION RESULT LIMIT ANALYSIS (MG/KG) (MG/KG1 ANALYST DATE TIME METHOD REFERENCE OL1DS(AS IS) 1,00 10000 100 JCM 12/02/02 16:00 SN 25-406 ITROGEN(TI(N) 6.33 63300 100 KCS 12/03/02 15:00 EPA- 351.3 HOSPHOR.US 0.61 6100 100 JCM 12/03/02 16:15 SW 846-60108 OTASSIUM 0.70 7800 100 JCM- 12/03/02 16:15 SW 046-60108 ULFUP, 1.74 L7400 100 JCM 12/03/02 16:15 SW 046-6010B ALCIUM 0.73 7300 100 JCM 12/03/02 16:15 SM 846-60108 AGNESIUM 0.41 4100 100 JCM 12/03/02 16415 SW 846-60100 ODIUM 3,17 31700 100 JCM 12/03/02 i6:L5 SW 846-6010D 5160 1 JCM 12/03/02 16:15 SW 846-GOIDB RON 3270 10 JCM 12/03/02 16:15 SW 846-6010H LIIMINUM 351 1 JCH 12/03/02 16:15 SW 046-GOIOO BNGANESE 266 1 JCM 12iO3/02 16:15 SW 846-60100 OPPER 410 1 JCM 12/03/02 16:15 SW 846-60108 INC MMONIA-HITROGE14 n.17 1700 100 KCS 12/03/02 12:00 EPA 350.2 10 LDR 12/03/02 15:00 SM 4500-NO3 F 03-F10:: NITROGEN72 NU 1 JCM L2/O3/02 16:15 SW 846-60106 ADMIUM 17 5 JCM 12/03/02 16:15 SW 846-GOLOB ICKEL TCM 11/03102 16:15 SH 046-601DD EAD 11 5 LL VALUES ARE qll A OR1' WEIGHT BASIS EXCEPT AS NOTED. J21�! 1 PA L C. H. CHU C NORNA JONES C1ur 4ap>rla and tel:ers are for 1pe esdusive and con'idemlal use of our dianls, and may not be reproduced in woofs or h part. nor may any role rence 6e made to the -.4wA. rerasuas or the oovary ;-try ad•:e,:ising, news release, or other public announcemarls wilheul obtaining our nrler wrBlen aurhor:zal•on. Copyright 1977 i A & L EASTERN AGRICUL IAL,LABORATORIES, INC. 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401 Fax No. �804) 271-6446 R342-026 ACCOUNT If45671 P GE 2 REPORT NUMBER BID—NDM1C SERVICES, INC. HUFFMAN FINISHING 516 RDUNOTREE RD EHAR.LOTTE NC 28217 NC CERT U257 ANALYSIS REPORT .AB ,NUMBER = 44900 ;AMPLE 10 = HUFFMAN FINISHING DETECTION RESULT RESULT LIMIT ANALYSIS 'ARAMETER ( ) (MG/KG) (MG/KG) ANALYST DATE TIME ISENIC 1.82 0'.2 "' KM 12/04/02 16:00 =RCURY 1.19 0.2 KM 12/04/02 15:00 _LENIUM 6.97 0.1 KM 12/04/02 16:00 ( (STO.UNITS,AS IS) 7.30 RD 12/03/02 12:00 ILCIUM CARBONATE E0 2.70 27000 100 LOR 12/03/02 15:OD 1LATILE SOLIDS 78.70 707900 100 DC" 12/03/02 16a0D lGANIC NITROGEN 6.17 61700 100 DCH 12/03/02 ILYBDENUM ND. 5 OEM: 12/03/02 16:15. DAVID MUTIL DATE SAMPLED 11/24/02 DATE RECEIVED, 12/02/02 DATE REPORTED 12/06/02 METHOD REFERENCE ------------------------ SW 846-7061A SM 846-7471A , SM 846-7741A EPA 150.1 AOAC 955.01 vv. SM, 2540G CALCULOTION_', SW 846-601.00 ,5yir 1. VALUES ARE DN FlTOR\' WEIGH7 BAaI5 ExCEPT A5 NOTED. � - ' P C. CHU ( HORMAN JOKES Our reports and •el:ers are for the exclusive and conlldeniial use of our clients, and may not be reproduced In whole or in pannot may any reference be made to the uadr. 11•e res+.11s. ar the rmnaar•� itany ache+Using• revs release, or other public announcements without obtaining our prior written awl-o: izeliai. Con sigh: 1977 RESIDUALS ANALYSIS+,COVER+SHEET ) luffmanFinishing Company Land Apphcation Program �'- Huffman Finishing Company WWTP Permit Number WQ0002431 Residuals Analysis Cover Sheet Date Sampled: November 24, 2002 Date Reported: December 06, 2002 Mineralization Rate (decimal) = Percent Solids = pH= Parameter 030 1.80 730 Concentration % Concentration mg/kg (Dry Wgt) Concentration lbs/dry ton (mo/ko *.002) TKN 6.330 iifi[i b3.3QF1R [ j><i'ii sI26 60(1 Phos horous 0.610 ::: ii 9'G 7O AQ i j`i i'» ,:.123ot# Potassium 0.780 PAN (Injected) PAN (Surface 1940 F9 402 00 38 804 Ammonia N Calcium .<.. 3ti0.� Calcium Carbonate Equiv. 2.700 isi <issil27`DOAO`.€'"[sst>""`' ::..., ... .........:::::�?IUtiD Magnesium 0,410 Sodium 3.170 i iii asi`>`31706 00,: G3'40(i' Sulfur — 17,400.00 ii 3.4 g Nitrate -Nitrite — 72.00 iii iiiOgS Manganese — 351.00 U7D2 Chloride — — iiii#V'YU�lji Ceiling Iron — 5,160.00 i 103211 Conc.(mg/kg) Aluminum 75 Arsenic — 1.82 00fld 85 Cadmium — 1.00 — Chromium4300 Capper — 266.00 840 Lead — 11 .00 i':iiiif [OjOZ2 57 Mercury— 1.19 iii 0i0U2: 75 Molybdenum — 5.00 <` O Utp 420 Nickel — 17.00 .. . 100 Se7enium — 6.97 p`0IQ 75 10 Zinc — 410.00 Calculation of Plant Available Nitrogen (PAN): Injected Application: % PAN = [decimal rein.rate'(TKN%-AmmoniaN%)]+AmmoniaN%+Nitrate-NitriteN% i Surface Application: % PAN = [decimal min.rate*(TKN%-AmmoniaN%)]+(0.5*AmmoniaN%)+Nitrate-NitriteN% Note: constituents not detected or < detection limits are entered at the detection limit fox. Report Number: 2004-RO38-070 Lab Number: 40333 Pagel Account Number: 45671 A&L EASTERN AGRICUL ii uRAL LABORATORIES, INC. 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401 Fax No. (804) 271-6446 Send To: BIO-NOMIC SERVICES- INC. 516 ROUNDTREE RD CHARLOTTE NC 28217 Sample ID: HUFFMAN FINISHING Samples Submitted By: t RANDY BIGHAM HUFFMAN FINISHING NC CERT #257 Date Sampled: 02/03/2004 Date Received: 02/04/2004 Date Reported: 02/11/2004 . 0 Detection Result Result Limit Analysis Analysis Parameter ( %) (mgfkg) (mg/kg) Analyst Date Time Method Reference SOLIDS(AS IS) 0.37 3700 100 JCM 02/04/2004 16:00 SM 2540 G NITROGEN(TKN) 9.73 97300 100 KCS 02/05/2004 16:00 EPA 351.3 PHOSPHORUS 0.55 5500 100 JCM 02/05/2004 10:42 SW 846-60106 POTASSIUM 1.33 13300 100 JCM 02/05/2004 10:42 SW 846-6010B SULFUR 2.49 24900 100 JCM 02/05/2004 10:42 SW 846-6010B CALCIUM 0.62 6200 100 JCM 02/05/2004 10:42 SW 846-6010B MAGNESIUM 0.37 3700 100 JCM 02/05/2004 10:42 SW 846-6010B SODIUM 7.81 78100 100 JCM 02/05/2004 10:42 SW 846-6010B IRON 4230 1 JCM 02/05/2004 10:42 SW 846-6010B ALUMINUM 2450 10 JCM 02/05/2004 10:42 SW 846-6010B MANGANESE 240 1 JCM 02/05/2004 10:42 SW 846-6010B 222 1 JCM 02/05/2004 10:42 SW 846-6010B COPPER 383 1 JCM 02/05/2004 10:42 SW 846-6010B ZINC AMMONIA -NITROGEN 0.81 8100 100 KCS 02/05/2004 15:00 EPA 350.2 NO3-NO2 NITROGEN 486 10 KCS 02/05/2004 15:45 SM 4500-NO3 F CADMIUM ND 1 JCM 02/05/2004 10:42 SW 846-6010B 14 5 JCM 02/05/2004 10:42 SW 846-6010B NICKEL 10 5 JCM 02/05/2004 10:42 SW 846-6010B LEAD PAUL C. H. C. NORMA JONES ALL VALUES ARE ON A DRY WEIGHT BASIS EXCEPT AS NOTED. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced In whole or in part, not may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Repo Tiber: 2004-RO38-070 Lab Number: 40333 Page 2 Account Number: 45671 ASL EASTERN AGRICUL • .ORAL LABORATORIES, INC. 7621 Whitepine Road Richmond, Virginia 23237 • (804) 743-9401 Fax No. (804) 271-6446 Send To: BIO-NOMIC SERVICES- INC. 516 ROUNDTREE RD CHARLOTTE NC 28217 HUFFMAN FINISHING Samples Submitted By: RANDY BIGHAM Date Sampled: 02/03/2004 Date Received: 02/04/2004 Sample ID: HUFFMAN FINISHING Date Reported: mr��nnna NC CERT #251 ••• • Detection Result Result Limit Analysis Analysis Parameter (%) (mg/kg) (mg/kg) Analyst Date Time Method Reference ARSENIC 1.00 0.2 KMM 02/06/2004 15:00 SW 846-7061A MERCURY 1.58 0.2 KMM 02/06/2004 15:00 SW 846-7471A SELENIUM 7.40 0.1 KMM 02/06/2004 15:00 SW 846-7741A PH (STD.UNITS;AS IS) 7.80 RD 02/05/2004 12:00 EPA 150.1 CALCIUM CARBONATE EQV 6.04 60400 100 KCS 02/05/2004 15:00 AOAC 955.01 VOLATILE SOLIDS 57.60 576000 100 KCS 02/05/2004 16:00 SM 254OG ORGANIC NITROGEN 8.92 89200 100 DCH 02/05/2064 CALCULATION MOLYBDENUM ND 5 JCM 02/05/2004 10:42 SW 846-6010B -- —---- ------ — ---- -- --- ------' � ALL VALUES ARE ON A DRY WEIGHT BASIS EXCEPT AS NOTED. PA�. H. CHU C. NORMA JONES our reports and letters are for the exclusive and confidential use or our clients, and may not be reproduced In whole or in pad, nor May any reference be made ; to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prim written authorization. ,- a ��:3 . RESIDUALS ANALYSIS COVER SHEET Huffman Finishing Company Land Application Program Huffman Finishing Company WWTP Permit Number WQ0002431 Residuals Analysis Cover Sheet Date Sampled: February 3, 2004 Date Reported: February 11, 2004 Mineralization Rate (decimal) Percent Solids Parameter I % Ceiling Conc-(mglkg) TWX Phosphorous Potassium PAN (Injected) PAN (Surface) Ammonia N Calcium Calcium Carbonate Equiv. Magnesium Sodium Sulfur Nitrate -Nitrite Manganese --- Chloride Iron Aluminum 75 Arsenic 85 Cadmium -- Chromium 4300 Copper 840 Lead 57 Mercury 75 Molybdenum 420 Nickel --- 100 Selenium 7500 Zinc I 7 0.550 1.330 6.040 0.370 7.810 mglkg (Dry Wgt) 240.00 1.00 1.00 222.00 383.00 lbs/dry ton Calculation of Plant Available Nitrogen (PAhD: Injected Application: % PAN = [decimal min.rate*(TKN%AmmoniaN%)]+AmmoniaN%+Nitrate-NitriteN% Surface Application: % PAN = [decimal min.r-ate*(TKN%-AmmoniaN'%)]+(0.5*ArnmoniaN%)+Nitrate-NitriteN% Note: constituents not detected or < detection limits are entered at the detection limit for calculations. TestAmerica. I H C 0 4 T 0 3 a T 6 0 ANALYTICAL REPORT ' BIO-NOMICS SERV., INC. 2102 DAVID MOTIL S16 ROUNDREE RD. CHARLOTTE, NC 28217 Project: Project. -Name- HUFFMAN FINISHING Sampler: JOHN s. THOMPSON.' Report paac Azsalyce Result ucica Limit Limit ----------------------- ____- ------ ------ I *GMURAL C1�.4' I8TzY PARAM.ETgR7e Reactive Cyanide Mn mg/Icg so.D Aeactive Sulfide ND mg/kg _ 100. Igmitahility NOT IGNITABLE 02. To 10ar Lab Number: 02-A197220 Sample ID: HUFFMAN FINISHING Sample Type: Solid waste Site ID: Date Collected: 11/26/02 Time Collected: 14:30 Date Received: 11/29/02 Time Received: 9:00 Page: 1 ➢1.1 Pector Rite Time Analyst MecLcd Batch 50.0 20 '12/ 2102 19;45 A.Bamarn! SW-846 3028 100. 20 121 2/02 19e45 A.Remarai BW-646 3032 1 22/ 1/02 11:25 S. Self 9045 AM22 12/ 3102 8.32 T. M wv ly lol OM 5350 TCLP Results - .L Mavis spike Analyte Result Ha_Cs Re Lim'C g Recovery IY) ➢ace Time ... .... Method• QC Hatch arsenic < 0.100 m5/1 5.0 302 12/ 3/02 21,17 C.,I b,-. 6oloB 5394 C°cmi11 term,0 < 1.00 mg/1 lo0 99 12/ 3/02 27:17 C.JohaeOn Gal OH 5394 chromiumD.10D < mg/1 1.0 96 12/ 1/62 21.17 C.JoLncaa 6D1DH 5394 :.cad . 0.500 mg/1 5.0 96 12/ 3/02 21:17 C.Joha:ma 60108 5394 mercury< < D.500 mg/1 S.0 97 12/ 3102 21:17 C.Jalasma sO:DH 5394 Salemlum O.D100 mg/1 D.2 111 12/ 4/02 1/:06 X.Hacchatt 7470A 5493 Sl lver < 0.300 mN/1 1.0 11D ;2/ 3/07 21:17 C.JDhaaoa 60108 0.130 mg/1 5.0 Ica 12/ 3102 21:17 5399 Dearme C. JoLcson 1 DD08 5391 CazLoa to tzacLloride < 0.0100 mg/1 0.5 311 12/ 5102 19:40 S. Udeae 8260 9021 Gil0r0bmeene < 0.0200 mg/] 0.5 106 12/ 5/02 19:a0 S. Uda2e e260 C2rlarof4-m < 0.9200 m g/1 100 114 11/ 5/02 19:a0 S. 0dete 6260 9071 mg/1 fi.D lla 12/ 5102 902; 191a0 B. Udete 0260 9011 Sample report eoatlaued . . 2960 Fos7vu Curbto l'u� Ulat h: / ylsun LLt:,Ti\ 37204 / G15-726-0177 / I+w 9 1 Testi. meirica ' imco3rD 6.,r:D ANALYTICAL, REPoRT Laboratory Number: 02-A197220 Sample ID: HUFFMAN FINISHING Project: Page 2 TCLr 8esults spike Analxatrix Iie_ult :uaicc „ Reg :.: _,c . Be00ves-y (e) Dace Time Analytic ____�e•__________________ _____•_____ � method QC Batch ..... .......... 1,]-➢iehl oxoetLana < 0.0200 mq/1 0.3 1,1-Dichl0r0ez hens < 0.0]00 mg/1 116 12/ 5/02 19:40 S. Ddexe 1260 90'-1 nethyleenylkecme 0.7 122 12/ 5/02 19:40 S. Ddexe 8290 $021 Tecrachl0ixthene < 0.100 mq/l 200 SOB 12/ 5/02 19:40 a, 9daze 0290 9021 Trl chlmroethene < 0. 0200 mg/1 0.7 108 12/ 5/02 13:40 S. Ddexe 9260 2021 C--myl Ch1orlCe < 0, 0200 mq/1 0,5 104 12/ 5/02 19:40 S. Ddexe 8260 9021 c--ma01e < 0.0200 mg/1 0.2 250 12/ 55/02 19:40 S. 9deze 8260 9023 1,4-Dic]slp-yheyxeye c 0.0100 mg/1 700 67 32( 5/02 11:51 'T.Salya:ak 8270 6685 2 ➢laitrm 4• < 0.0300 mg/1 7.5 6d 12/ 5/02 11,51 J.Seiyarak 6770 B685 a0xa<aloroEnaeme I aca ..e < 0.0100 mq/l 0.13 77 12/ 5/02 11:51 J.9aiyak a6 8770 8685 8exrhlOT•1, 3-bm Cmdi ed < 0.0100 mq/1 0,13 72 17/ 5/02 11:51 J.6aiyaeak ,370 6685 riazaenlozolrwy_! < 0.0100 mg/1 0.5 fi0 12/ 5/02 11:51 a.Baiyaaak 4270 0625 ASL:oheaxC70 < 0. 0100 m9/1 1.0 64 12/ 5102 11:51 7.Saiyasak 9210 Se as rentaenlazopneml c 0.0300 mq/1 7.0 76 12/ 5/02 11151 J.Saiyacak 6270 8685 PyrlCiae < 0.0100 mq/l 100 72 12/ 5/02 11:51 J.Saiyasak 8270 8685 2, a,5 ^ri c4loZopnenel e 0.0109 mg/1 5.0 34 12/ 5/02 11:51 J.SaiyaBak 8270 B6B5 ],4,6-lx:i ehl0ropnen0l c 0.0100 mq/1 400 74 12/ 5/02 11:51 J.Saiyaxak 0270 ages Chlcrd a < 010100 mg/l 2.0 72 12/ 5/02 ll;Sl J.Saiyaeak 3270 $ass < 0.0005 r0q/1 O.D70 100 12/ 4/02 19:35 Carmichael 5061A 7917 FSCrim mg/1 10.0 74 12J 9/02 11:51 carmicnael eIS, 1251 kepCechlOr < O. Ooa5 m - g/1 0.02 235 12/ 4/02 19:35 CL-mi=,! 6001A 1917 1�Sndane < 0.0005 m9/1 0.008 196 12/ 4/07 19:35 Carmi<nael e083A 7917 ychldx c D,0005 me/1 0.4 2-1 12/ 4/02 13:35 Cazmictael 6091A 7917 mra Tcxephene < 0.0005 mg/l 10.0 215 12/ 4/02 19:3s bsmienael e061A 7917 ailvex < p.o100 �/ 3 0.50 111 12/ 4/03 19:35 CL-xichael B081A 7917 xepGaenlor eP=i,c < 0.0100 m9/1 1.0 68 12/ 9/02 1L:51 zxrmichael B1 52A 1251 TLyp Lhceractiau < 0.0005 m5/1 D.OaB 195 12/ 4102 19:35 Carmichael 808LA 7917 Zero Meadapaee Extraction Initiated Initiated - 12/ 2/02 14:30 B. Powell 1311 3532 12/ 2/07 34;30 B. Pwc11 1312 3532 sample zepor_ coetiaucd , 1 29611 Yn57 f:k (,RY.IIJIT4\ Dkicr: / N).(nu.i.e.TN 37204 / 615-726.01 77 / f'��: 8I5-726.0954 i n r TestL merica I X C e a T P l= T t a .Y ANALYTICAL REPORT Laboratory Number: 02-A197220 Sample ID: HUFFMAN F2NISHING Project: : Page 3 =ample at(tricticn Data At/vol Para,ecer 3Yszarted LYtzact Vol Date Time TOLD Herhioides 5.0 ml 5.00 ml 3.21 4/02 rC7.7 pctieides i00, ml 10.0 ml la/ 5/07 T'=P 31A,a 500. m1 1.0 ml 12/ 4/02 Surrogate ------------- VOA Styr 1,2-DOA-d4 vok RoT TO"=, -dB 704 Burr, 4-BFB Raq "u�-x'bbebemreae-da 2th Sarr-2-Fluorcbiphem71 8Ra 11urr-Terpheayl-d14 HUA Burr-pheaPl-d5 Rsm SLr-2-i'lUoropheDol RAT 5T-=-1, A. 6-TribrOmophea0l Peet aarr-TCa surr-Di butylchloreadate m,-r-DCAA Analyst Kcthod K• Rieke ' 3510 K. Richa 3S10 K. Rieke 3310 4Recovery - Target Ramge 114. 73. - 1.33. 307. 90. - 121- 10s. 80. - 12B, 73. 40. - 127. 70. 42. - 117. 79. Al. - 129. 31. 1. - 75. 45. 3. = 97. 64. 35. - 174. 52. 33. - 127. so. 1. - 151. 7D% 61. - 159. LABORATORY COMMENTS: Rb m SOC detected at the report limit. B ' Amelyte eat detected is the method blank. J Fatimated 7a1ua be10V Report Limit. H 6eelnneed Value above the calibration limit of the 1Z.erumeac. 1 = ReeeVery outside Laboratory historical or method Prescribed limits. Fie.h Point/15ni eab111ey reported to the aeare:t 10 deg F. All rcPl ca reported on a set weight basis. Tad of Sanp14 Report, 29611 FOSTh.X CRkfl(MTII\ DwivF. / IVd9lll u.Lr.,TN 37204 / 515-726.0177 -- _-- --.. I rm iCe:aMv la+AJ rtO.n'1. Is:�O lYLKll.ri'��: ' ' TestLz ica .wa1rn�A1 itrnMa t;o0.DoxAneM f U:704 592 9M P.006�0i7 _ :.1 eYOu fffT1Y C=11INrok On.A hAa IIVu1.e,. T1NN9.a0.1a arjoi (InP•inM1•alda - OlG•7Pd•,{aP1 Iu " - ' ANALYT,rCAL RSPORT:',;. ,.. H-T,o-NOM_Cs sERv „ INC. 2102- 516 RO=REE RT]. _''- CHARLOTTE, NC 28217 I: Pr j ect :" Project Name: Sampler! TCL7 usulea Lab Number: 04- 16124 Sample ID: Mt1F FINISHING -sample Type; Li Id waste Site ID! Date Collected: 2/ 5/04 Time Collected: 10:00 -Date Received: 2/ 6/04. Time Received; '9:20 'Page: T XaMIA Wks Analytt x.nvlt''V'`" nniii AST a";;, xtc dry fkl harc -Lift AaAly.% herhad CC 9aoeh Ac.enia . 0.100 R0/1 S.a _, .IDS 7/ 1144 14e20 C.Meeerd a010i Liriu., IMP a 1.90 , gf/i_ Loa 91 7/ l/ea 74.;I C,noCO=6 col of cD CbiOi . 0, la `%*/1 i.a ip7 7y /0a 16+29 0.M0CC,rd 6plox O rary:.tq,i Tc1.T . 0.002. ,. .. n9/1 5.1 17 Al 7/04 19-29 0.McCord 601an Lad., TCLP < 0.600 "np/L 5.0 lot '- V 7/D4 16;:10 C. kcrra solo+ NarNr Y O.e100 Ty/y 0.2 DO -' 3/1D/41 14120 K. Al1iGL 71701 9a lahlvi < p. le0 /l alfi 1,0 lla 7/ ]/01 1<:29 O.Ma (2ar0 f01 Da 9ll vnr • 0-C 100' bg/1 6.0 Lai 2/ 7/0{ ].f r]9 0.1fcCara 60101 Mcn.CM < D,CTO g.�•.: 114/3 0.5 Soa ...�.' ., 1/id/0f, .. 1arr01 . C. lttnl OaeD CerhOn eeprneal Dzi QO t 0.0700�.124 1/lo/64i Gh:esehna2 an0 < 0.02.0 of/I too Lop 2/10/Ot 13:01 19i 01 C. .a of C. .agi 9160 A36, CSl.rt:orM . 0-DID a if/1 6.0 i0D 2/10/04 19 QL C. 2Aa5 g]5o 1,2-h Lei/a roe Ch,,, . 0.0200 IIIf/1 a,F 10V 2/10/0• 45.01 C. Nana alas Oichla ran chOM < 0.0200 &oil 0.7 91 1/10/04 251Ot C, •in1 g76a MetgylCrh YlN6 tang a 9,104 bq/1 200 SDa ]/ie/Ol Kral C. *.at 02aa T4crncNorOochene . o.ofae t'9/3 0.7 110 2/1.0/0{ 15.01 C. Nani 9260 7^lchlorgectl0pg c 0. 0109 %oil D.9 " ' 131, Lla/o< 15i01 C. Y4g1 eato wL yl o%Loe.dc . 0.0200 a4/1 0.2 ti 2lla/o1 18r0L C. Nat a26o C cpalp 0.9404 11[/1 100 a0 2/1p/Oft 12;12 010111M9v 1270 1.t•OLch la rehnpAaaO At < O.D SDO as%1' 9.s :+- :J14/o4 12+22 OI0111ngev 0270 2.4-A1M sraca1v07te < D.OlaO %10/04 12r13 QIo1l1a0n+ e21e ke+4hlor. ahrn20ha < pall- 0.1a 17" -. 2/10/Dt 12.22 =.l 1 Lq+. 107a Nhs4hloi. l,1•hu u0l.n O.c1-ndoAo 0 'd 100' 09/1 p,0 ap ]/1G/oa y1;A.3 at.11 Lngso gale Noaehl.r.e On.,, .,a.Oloo 69/1 3.0 46 11r20 gc011:0fer lllo a+mplc ro"rt conciuuea {rant a rk D Inc, cam T..IAmerlca Aeclygcel Tn,h ni Ccrp.,.)I.. I Te1lAm4Aco Orllll.p Corporallon I TurAmerlcO,Alr rnU11on C.rparallon 8470 1412 O+T2 ea-2 6472 0471 a412 4471 Sill 0711 9712 27u p7u 9710 9 11] 9112 0743 271a 9911 0511 99 L. $211 9911, 9911 tx id:14 I-Num; ItSI 1'81t7'lLCfi r TesukMerica AI,.4TnCAL7emr= CDRf0jATl0n T0:704 392I9073 2.,' 1p M1O POa70P GPxIBa7p8 QIIYA • ry720YLLC0, THHNDUtt 3T209 - ROV•7Bp•V08d - dli-1Z8.2 /Oa P.x I I ' ANAL2?ICAL• RRPOItT''- �", ! c' Lahorato±y Nulslbe} ; 04-P_ZB124 HMFF 7 FINIS.YING . 'J 11�L' ._ I-'�1'r.,',^F it` - . HB➢YACA ... .. I?^'ILYea .................... IAPaVi�_1 ........ aet7.ce Arg LtmiF_ ➢ecvueey lal DryCO ..TINS.. AlaalYed II?t1ia41 CC Batch j, ... ...... ......... ------------ _--_--_• �� •_ _ ....... ,...-_ ........ G,1 -N1 eecDcazano O. Clan•-- mo/1 , �, a.a---•—a d- — •m/iro/o4- lalal tilPSlln dr 9 Ba7o peaeechlarophm0l < O, a106 a9/1 102F�' 1:9: 9fii .li , 1 ; •�;,_ 7/10)Di- 1a;22 cilc_, lirlg:v 1-LI ayrtdla0 c O.OloO eg/S 5,ai�•'• » BD70 POLL 2/10/0\ 12122 CHol71,lroM 8271 SPAS 7, 4, d•T7Se1{SaLapkeaol c 0, a1a0 aq/1 /00 B] '2/10/DS L2i74 01P111np. 4270 9911 ], {, 6•Stich7 a-Dpli�.1 0.0100 'ag/1 ,2/y0/et 12171 C7ia11:-�7av 0770 9911 '[7iloradll.t < 0_Ooox ,r maJ]_, 0.010�;, �-106 .:. 1J 9I04 16:02 J. NgrlCaap 8O61A o90➢ 1,.•L c B.SOo MOIL • ld.B 71 2/10Je4 10.59 , .OMrA e15Yr. 3504 e,•J Lin 9.9919 M11 0.02 L18 a/ ]J04 16102 J. H .-Ico a 0o97p Ms Hl:pzochLoL c 010006 1.. ,',;mOJl•' :' .a.aCd ;_• l2➢' -� 7t o/a4 2r.02 T. 14. kham Po■ t% poor P/7r 0.1 1CR 2/ PICA 18.0A a. harkeAm MCQLA ➢DC$ N0ifi0rychla: a,0,0005 ., •BIg/1.. Sa.O 2/ 9/Oa 16: CZ J. }LLix',mm Bo➢L1 99a5 T0.<Ppn.:n0 c 0, 0:0 e._. , Ug/1 •' 0.50 Ito 2/ ]/04 15102 J. K%vMnn B➢n ZA PF05 �13,.ex a o. a;oa -ng/1 ••,1.0 95 Matta 10:5C Z. hcrkh= B:S3A ??CA Haptichlor epox10e - c O, OOOfi-''�.m0/L D-009 .•il7 - L 9/04' 16109 J, Xftrk'aw0 WRIA 9905 AxtrOac;an S.nl Clacaa 2/ 9/04 16120 6.r4nor 1311 100 iom HOadepaee �:WraCL•1Da Sp1 =d0had •'• r. 1'L 2I 6/05 19,00 9.Arwr "IL 1920 ___________..._..._•_•___•___________...................................._. ._.. .............................. 9-mPolu Extract, on uau CeraAotOe Cateaetea Cxtrnnt a.I DaLO 71mr Aralynt MCLRod ' TCLp NCrDl cLarp E.0 al 5.00 ml ,'. ¢/' 7/0A , r- TGLp ➢h➢dlcidam 104, ml 1d,e 101 ' N B/ai 1=0 $xn•P Sao, m1 1.0 01 r"27 a/Oa '^.a Sur. L:2-arJi-d< V4 Bur. To1Vcn•:-dB =0➢@LS report ecetinard , i m: Alcke ' 151a h• Alcks axle I;- zLckm ]Slh fit TPFIi00 M1a��c ------------ Tl alAmArl co 4nalelle nl Ta Apra CarOarollan I Tellnmartca Drlll,na Carmarnllon 1 T..Il.m.rlrn At, mh.lea C..nam 11.e Applicant's name: Huffman Finishing Company Check all that apply: ❑ NEW RESIDUALS LAND APPLICATION PROGRAM ® RENEWED RESIDUALS LAND APPLICATION PROGRAM ❑ ADD ❑ DELETE this/these land application site(s) to/from those certified for this residuals land application program. ❑ INCREASE ® DECREASE the net acreage associated with this/these land application site(s) currently certified for this residuals land application program. ❑ OTHER Explain: Land application sites currently certified: _80_ net acres and proposed for certification: _67.7_ net acres. Total to be certified: _67.7_ net acres. Approximate percentages: _0_ % forested, _I00_ % agricultural, and _0_ % reclamation sites. I. LAND APPLICATION SITE INFORMATION (See Instruction B.): 1. Complete the following table with the requested information: Status Code Site/Field ID Landowner(s) Lessee(s) or Operator(s) County Net Acres Predominant Soil Series Soil CEC It, M Huffman A.W. Huffman, Jr. TBD Caldwell 17.1 Cecil-Pacolet- Rion 5.60 R, M Miller J.F. Miller TBD Caldwell 24.8 Cecil-Pacolet- Rion 5.25 R Baumgatner J.P. Baumgamer TBD Caldwell 25.8 Cecil-Pacolet- Appling 6.50 - h6N-DISCHARGE PERMITTING FORM: LASCA 02/02 *** END OF FORM LASCA 02/02 *** Page 2 of 2 Attachment Order 3 JUN-23-2004 16:09 FROM:WAT e2B2964663 TO:919198343589 P:2/5 1 T State of North Carolina m Department of Environment and Natural Resources 5 ;1 Division of Water Quality M n WATERSHED CLASSIFICATION ATTACHMENT o FOR RESIDUALS PROGRAMS (THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not consider this attachment f complete unless all the instructions are followed. Failure to follow the instru submit all of the required items will lead to additional application processing time. C_ or ct^� For more information or far an electronic version of this form, visit our web site at: htip:llh2o.enr.siate.ne.ushulpu/ INSTRUCTIONS TO THE APPLICANT: A. Attachment Form: ✓ Do not submit this attachment form for review without a corresponding residuals profram application form (Form NDRLAP). ✓ Any changes to this attachment form will result in the application package being returned. B. Prepare the attachment form with the requested information for each location where the residuals program activities are planned to occur within a particular regional office county coverage. ✓ Additional copies of Page 2 of 2 of this attachment form may be used if necessary. ✓ Use a portion of an 8.5-inch by I I -inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities arc planned to occur as well as the closest downslope surface waters as clenrly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ✓ Latitudes and longitudes must reported as being based on either the NAD 27 or the NAD 83 data systems. ✓ Acceptable methods of determining location latitudes and longitudes and their corresponding codes arc as follows: _ Address Matching (ADD) _ Digital or Raw Photo Extraction (EXT) _ Aerial Photography with Ground Control (AER) _ Geodetic Quality GPS Survey (GEO) Cadasual Survey (SUR) _ LORAN-C Navigation Device (LOR) _ Conversion from Coordinate Plane (CP) _ Navigation Quality GPS (GPS) _ Conversion from Township-Scction- Range (TSR) _ Remote Sensing (RS) _ Conversion from Universal Trans Merc (UTM) _ Zip Code Gntroid (ZIP) Map Interpretation by Digital or Manual Extraction (MAP) ✓ Location accuracy must be provided to the nearest unit (e.g., nearest second, tenth of a second, etc.). C. Mail or fax the attachment form and the map portions to the appropriate regional office for review and to obtain the waterbody and classification information. ✓ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded from the web site at: http://h2o.em.state.nc.us/ndpu/. ✓ The Division will not consider this attachment form to be complete until it is completed by the appropriate regional office. To: Regional office: Ash_ey�lle Rro al Office __ Address of regional office: 59 Woodfin Place — City: Asheville State: tip_ Zip: 28801 Facsimile number: ( _828^ )— Please provide me with the waterbody name(s), stream index number(s), and current/proposed classificatlon(s) of the surface waters that are closest to and downslope from the location(s) where the proposed residuals program ac i sere planned to actor, es identified an the attached map segment. Signature of regional office staff: �tl �4 Dace:Z FORM: RWSCA 02102 Page I of 2 Attachment Order 3- Location ID County Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. (To Be Completed by DWQ) Current and Proposed Class (To Be Completed by DWQ) Huffman 1 Caldwell 35`45'33"N 81'23'45"W NAD 27 MAP Second Huffman Caldwell 35`45'33"N 81`23'45"W NAD 27 MAP Second Baumgamer Caldwell 35`48'57"N 81`21'42"W NAD 27 MAP Second Miller Caldwell 35°46'15"N 81'25'20"W NAD 27 MAP Second *** END OF FORM RWSCA 02102 *** FORM: RWSCA 02/02 Page 2 of 2 Attachment Order 3- M a Cn CTI r) ID W IT 2 00 (U a0 ¢H 3 LLLL �0 rru Location ID County Latitude Longitude Location Datum Location Method Code Location Accuracy Watetbody Subbasin and Stream Index No. (To Be Coopteted by DWQ) Current and Proposed Class (To Be Completed by D WQ) r;/it le yr dr //- s ws vs FORM: RWSCA 02102 •** END OF FORM RWSCA 02/02 •&* Page 2 of 2 Attachment Order 3-a /p- • f l � �C�_ ii Creek ff^ _ ( c Lat. 35' 48' 57" N� Long. 81' 21' 42" W Av f C J.P. Baum amer Site 7 •i ,e 1' • y t -7-D rf ;''Huffman Finishing Permit No. W0002431- Land Application Sites N i USGS: Bethlehem, NC �, 0' S00' 1000' 2000' ant.. ) J—))W \ 'I k < • :f�C��.) t 6 P, f THE WOOTEN COMPANY ENGINEERING PLANNING ARCHITECTURE 0 120 North Boylan Avenue Raleigh NC 27603-1423 0919.828.0531 fax 919.834.3589 June 2, 2004 Mr. W.R. White, County Manager Caldwell County P.O. Box 2200 Lenoir, NC 28645 CERTIFIED MAIL - RETURN RECEIPT REQUESTED Re: Land Application Permit Renewal Huffman Finishing Company TWC No. 2537-I Dear Mr. White: Enclosed please find one (1) copy of formal notification that Huffman Finishing Company will be renewing its permit for land application of biosolids on August 31, 2004. Huffman Finishing is currently permitted for 80 acres and does not intend to increase its permitted acreage during this renewal. If you wish to comment on the permit renewal, please do so as explained on page I of the attachment. Should you have any questions about the enclosures, please contact our office at (919)828-0531. Sincerely, THE WOOTE PANY G�Y• arton cc: Lee Huff an, Huffman Finishing Company FC: gdh enclosures State of North Carolina Department of Environment and Natural Resources Division of Water Quality COUNTY MANAGER NOTIFICATION ATTACHMENT (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not consider this attachment form to be complete unless all the instructions are followed. Failure to submit all of the required items will lead to additional application processing and review time. For more information or for an electronic version of this form, visit our web site at: hitp://h2o.enr.state.nc.us/ndpu/ INSTRUCTIONS TO THE APPLICANT: A. Attachment Form: ✓ Do not submit this attachment form for review without a corresponding residuals program application form (Form NDRLAP). ✓ Any changes to this attachment form will result in the application package being returned. B. Prepare a separate attachment form for each county in which the land application sites for which the applicant is seeking certification are located. C. Mail the attachment form to the appropriate county manager by certified mail with a return receipt requested. ✓ The most current publication of the Directory of State and County Officials may be downloaded from the web site at: http://www.secretary.state.nc.us/pubsweb/direct.asp. ✓ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded from the web site at: http://h2o.enr.state.nc.us/ndpu/. D. Attach an 8.5-inch by 11-inch copy of the return receipt to the back of this attachment form prior to submission of the application to the Division for review. To: County where land application sites are located: Caldwell Name and complete address of county manager: W R White City: Lenoir State: NC Zip: 28645 This is to notify you that the applicant listed in Item 1. 1. of this attachment form will be submitting an application for the land application of residual solids to land in your county to the Division of Water Quality (Division) for review. During this review, the Division will ensure that all federal and state regulations are enforced. Maps of the land application sites included in this application will be available at the following location no later than the listed expected application date: Name and complete address of appropriate regional office: Asheville Regional Office 59 Woodfin Place City: Asheville State: NC Zip: 28801 Telephone number: (_828_) 251-6208 Facsimile number: ( _828_) 251-6452 Expected date of application submission: July l 2004 Actual date of application submission (to be completed by DWQ): Deadline for county manager response (to be completed by DWQ): Should you desire to comment on this application as it related to your interests, please do so no later than 30 calendar days following the expected application submission date. If you have any questions or comments about this notification or if you would like more information, please contact the Water Quality Supervisor of the appropriate regional office at the telephone number provided above. Thank you in advance for your attention to this matter. I. GENERAL INFORMATION: 1. Applicant's name: Huffman Finishing Company 2. Signing official's name and title: A.W. Huffman, Jr.. President 3. Complete mailing address of applicant: City: Granite Falls State: NC Zip: 28630 Telephone number: ( _828_) 396-1741 Facsimile number:( _828_) 396-4235 E-mail address: HUFFHOSLTH@.AOL.COM 4. Name and complete mailing address of contact person and consulting fine who prepared application: Gary Hartong. The Wooten Company. 120 North Boylan Avenue City: Raleigh State: NC Zip: 27603 Telephone number: ( 919 ) 828-0531 Facsimile number: ( 919 ) 834-3589 E-mail address: GHartong@TheWootenComoany.com IL PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, and/or ® renewed permit. 2. If this application is being submitted to renew or modify an existing permit, provide: the permit number W Q0002431 the most recent issuance date September 30,1221 and the expiration date August 31.2004 . Date of most -recently certified Attachment A: Date of most -recently certified Attachment B: III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION 1. County(ies) where residuals source -generating facilities are located: Caldwell 2. Purpose of the residual source -generating facilities (check all that apply): ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ® treatment of 100% industrial wastewater, ❑ treatment of industrial mixed with domestic wastewater, and/or (approximate percentages: % industrial and % domestic) ❑ other (explain: n/a 3. Are land application sites currently certified for this residuals land application program in this county: ® yes ❑ no. If yes, provide the total number of acres (i.e., excluding buffers) that are certified: _80_ acres (approximate percentages: 0_ % forested, _100_ % agricultural, and _0_ % reclamation sites). 4. This application, if approved by the Division, will certify _n/a_ additional acres (i.e., excluding buffets) in this county for this residuals land application program (approximate percentages: _n/a_ % forested, _n/a_ % agricultural, and _n/a_ % reclamation sites). *** END OF FORM CMNA 02/02 *** .,,�m,.na:.,,..,,n,. IN Complete items 1, 2, and 3. Also complete item 4 if Restricted Delivery is desired. IN Print your name and address on the reverse so that we can return the card to you. ® Attach this card to the back of the mailpiece, or on the front if space permits. 1.. Article Addressed to: 2: Article Number d (Transfer from serelee label) PS Form 3811, August 2001 UUMPLETETHIS.. SECT, A. Signature ❑ Agent ❑ Addre B. Received by (Printed ame) C. Date of Delivery D. Is delivery address different from item 1? ❑ Yes If YES, enter delivery address below: ❑ No 3. Service Type it ❑ Express Mail ❑ Registered eBl iturn Receipt for Merchandise ❑ Insured Mail • ❑ C.O.D. 4. Restricted Delivery? (Extra Fee) ❑ Yes Domestic Return Receipt 1 q 102595-02-M-1540 810-NOMIC SERVICES, INC. Field Loading Rate Report NPDES Permit #W00002431 Owner: Huffman Finishing Company Operator: Huffman Finishing Company Residual Source: Huffman Finishing Company WWTP Total Dry Tons Applied (Annual): F1117 rl ®■ • r CuneraiNe Pollutant Loading Rate (IWai Cummulative information from 2001 Annual Report (Signature of Land Applier) 36 1 34 1 na 1 1.336 1 267 1 15 1 na 1 374 1 6g 2 498 2 _/p,0/{ (Date) 1 cerIlly, under, penalty of law, that thie docemenl was prepared under my direction or sWetieion In accordance with a syslem designed In assure that qualified personnel properly gathered and evaluated the information suhrralted. I en aware that Inere are signdrAnl panallieff to,wbnilling false information, ,rMudi g the pheara ily pl fines am arerhormant for anus afflalpM. Crop: Fescue Permit Until(Ihslactyr 250 State of North Carolina Department of Environment and Natural Resources Division of Water Quality LANDOWNER AGREEMENT ATTACHMENT (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not consider this attachment form to be complete unless all the instructions are followed. Failure to follow the instructions or to submit all of the required items will lead to additional processing and review time for the application. For more information or for an electronic version of this form, visit our web site at: http://h2o.enr.state.nc.uslndpul INSTRUCTIONS TO THE APPLICANT: A. Attachment Form: ✓ Do not submit this attachment form for review without its corresponding residuals program application form (Form NDRLAP). ✓ Any changes to this attachment form will result in the application package being returned. B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner and operated by a lessee/operator (i.e., if applicable) other than the applicant. ✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY -OWNED LAND APPLICATION SITES The undersigned landowner or his representative hereby permits: Applicant's name: Huffman Finishing Company Complete mailing address of applicant: P.O. Box 170 City: Granite Falls State: NC Zip: 28630 Telephone number: ( 828 ) 396-1741 Facsimile number: ( 828 396-4235 E-mail address: HUFFHOSLTH@AOL.COM hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -generating facility(ies) onto the following land application site(s) (i.e., see attached buffer maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Land Use or Cropping Patterns Intended Use or Disposition of Crops Residuals Source -Generating Facilities Miller Site Pasture Hay Huffman Finishing Co. The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modes or cancels. this Agreement. i I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with another municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement. The lend application of any additional residuals or waste, other than that generated by the residuals source -generating facilities specified by7 the Division's residuals land application program permit, is prohibited. _ i 2. The existing lessee or operator, if any, of the land application site(s) agrees, by execution of this Agreement, to comply with all provisions of this Agreement. 3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third party, the landowner shall be responsible to ensure that the third parry agrees and complies with the terms and -conditions of this Agreement 4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference to the subject matter of this Agreement 5. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of 18 months from the date of the most recent residuals land application event 6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWQ, Non -Discharge Permitting Unit 1617 Mail Service Center, Raleigh, NC 27699-1617. 7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a notice shall be given' by the current landowner to the new landowner that gives full details of the residuals applied or incorporated at the land application site(s). 8. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for Typical cropping patterns, and a description of the equipment used by the Permittee. 9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program permit that has been most -recently issued by the Division prior to commencement of any residuals land application event. This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws and regulations. 10. The land application site(s) shall be adequately limed to a soil pH of at least 6.0 prior to residuals land application. The only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided that a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least 6.0. 11. The Permittee will famish the landowner or his representative with a copy of the results of each soil analysis. 12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and the Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil samples. 13. The landowner or his representative will furnish the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 14. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee and/or the landowner or his representative prior to and during a residuals land application event 16. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting ofsigns that indicate the activities being conducted at the land application site(s). 17. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals land application program permit. 19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and to established monitoring facilities on or near the land application site(s) as required by the residuals land application program permit. 20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the Division's residuals land application program permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater, surface water, or leachate. 21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives to take necessary soil, surface water, and groundwater samples during the term of; and for 12 months after termination of, this Agreement. nnnnn. r n e e n' II. RESTRICTIONS: I l�� ILI " ic Landowner's Certification: ® I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners 2 that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations and restrictions, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: JOE Frank Mill Signature: ((�� Date: 6 14 10,4 NORTH CAROLINA, C Aj CLJ aj L COUNTY I, the undersigned Notary Public do hereby certify that J o h/t% F�A� f ► \ 1 personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS day of hand and official seal this the Signature and seal 1 My commission expires: 2004 Lessee's/Operator's Certification: ® I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Joel CoertBio-Nomic Services Signature: Permittee's Certification: Date: ® I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Signature: Abr_J� Date: *** END OF FORM LOAA 02/02 *** cnn�*. 1 n e * no. n___ o -,I day, ��-,__�rl�� -�:r.� 9 ^ �- _ 'dam; �t�r � , • if-\_ ' IF �- c F J 1 ' >. y .. •I +� h k itj ayt Iy so i y � i f� � � y t �r.f '�• �� • rl �� t4� fi'f•% �: yy iG xk \ xrY` i rye; ' `k a , :� y 4•yai a �, hr��.i,. q . ( �{ fi �` tit v �. 71 I% r•iI-- .'I'/, f l J . y - • State of North Carolina Department of Environment and Natural Resources Division of Water Quality LANDOWNER AGREEMENT ATTACHMENT (THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN OR%GINAL) The Division of Water Quality (Division) will not consider this attachment form to be complete unless all the instructions are followed. Failure to follow the instructions or to submit all of the required items will lead to additional processing and review time for the application. For more information or for an electronic version of this form, visit our web site at: http://h2o.enrstate.nc.uslndpul INSTRUCTIONS TO THE APPLICANT: A. Attachment Form: ✓ Do not submit this attachment form for review without its corresponding residuals program application form (Form NDRLAP). ✓ Any changes to this attachment form will result in the application package being returned. B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner and operated by a lesseeloperator (i.e., if applicable) other than the applicant. ✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS _ TO PRIVATELY -OWNED LAND APPLICATION SITES The undersigned landowner or his representative hereby permits: Applicant's name: Huffman Finishing Company Complete mailing address of applicant: P.O. Box 170 City: Granite Falls State: NC Zip: 28630 Telephone number: ( 828 ) 396-1741 Facsimile mmmber: ( 828 ) - 3964235 E-mail address: HUFFHOSLTH@AOL.COM hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -generating facility(ies) onto the following land application site(s) (i.e., see attached buffer maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Land Use or Cropping Patterns Intended Use or Disposition of Crops Residuals Source -Generating Facilities Baumgarner Pasture Hay Huffman Finishing Co. The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. Cnn\r.l nA A n1/n1 n.._ I _1r A»__L___. n_1__I n STIPULATIONS: 1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with mother municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement. The land application of any,additional residuals or waste, other than that generated by the residuals source -generating facilities specified 6y the Division's residuals land application program permit, is prohibited. •.. 2. The existing lessee or operator, if my, of the land application site(s) agrees, by execution of this Agreement, to comply with all provisions of this Agreement. 3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third parry, le landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement: 4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference to the subject matter of this Agreement. 5. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of18 months from the date of the most recent residuals land application event 1 6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWQ, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. i 7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a notice shall be given'by the current landowner to the new landowner that gives full details of the residuals applied or incorporated at the land application sitc(s). 8. The Permittee has provided the landowner or his representative with information and data conceming the residuals Is application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, and a description of the equipment used by the Permittee. 9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program permit that has been most -recently issued by the Division prior to commencement of my residuals land application event. This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws and regulations. 10. The land application site(s) shall be adequately limed to asoil pH of at least 6.0 prior to residuals land application. The only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided that a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least 6.0. 11. The Permittee will famish the landowner or his representative with a copy of the results of each soil analysis. 12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and the Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil samples. , 13. The landowner or his representative will furnish the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 14. The landowner or his representative will inform the Permittee of my revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 1 15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee and/or the landowner or his representative prior to and during a residuals land application event. 16. Appropriate measures must be taken by the Pennittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 17. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals lid application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals land application program permit. 1 19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and to established monitoring facilities on or near the land application site(s) as required by the residuals land application program permit. 20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and inspect any property, premises, or place on or related to the land application site(s) at my reasonable time for the purpose of determining compliance with the Division's residuals land application program permit; may inspect or copy my records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater, surface water, or leachate. 21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives,Ito, take necessary soil, surface water, and groundwater samples during the term of, and for 12 months after termination of, this Agreement cnnls. r nn A n'Lnl n......9 ..C'l A n_d..-] i D. RESTRICTIONS: Landowner's Certification: ® I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners QR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations and restrictions, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner n e: J.P. Baum amer Signature: Date: G 19 O L/ NORTH CAROLINA, 1, the undersigned Notary Public do hereby certify that personally appeared before me this day and acknowledg���edpp the due execution of the forgoing instrument. WITNESS my hand and official seal this the 4- h day of , C;L,-� 20y µ Signature and seal: / -' My commission expires: 4 /% M a Lessee's/Operator's Certification: ® I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Joel Coen Bio-Nomic Services Signature: Permittee's Certification: Date: ® I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing off Signature: *** END OF FORM LOAA 02/02 *** rnnl/. 1 n A A --- 1 -14 n «....t._.._. n_A.._ 9 .. Form 1 - Data Summary Report Prepared By: HydroLogic Laboratories, Inc. Client ID: HUFFMEN FINISHING Project Number: HUFFMEN FINISHING Sample ID: L5168-1 Site / Project ID: BIONOME SERVICES Run ID: R7582 Collection Date: 26-JUN-97 Received Date: 27-JUN-97 Report Date: 08-JUL-97 CAS No. Dil _ Sample Cone. SW846 Methods 1311/6010 Preparation Date: 02-JUL-97 Analysis Date: :03-JUL-97 00:34 Wohkgroup Number: WG11703 Arsenic 7440-38-2 Barium 7440-39-3 Cadmium 7440-43-9 Chromium 7440-47-3 Lead 7439-92-1 Selenium 7782-49-2 Silver 7440-22-4 h SN846 Metlibd 1311/7470 -- Analysis Date: 04:JUL-97'14.10 Workgroup :Number: WG11715' Mercury 7439-97-6 Review By: Rose Murphy Report Approved By: Karen "DiO - Sample Dilution Factor "ND" - Sample Concentration Not Detected above RL "RL" - Method Report Limit Units 1 NO mg/L 1 1.08 mg/L 1 ND mg/L 1 .0135 mg/L 1 ;iND umg/L, 1 •HID -mg/L 1 °.ND ffo/L 1 i;NO -mig/L n 2 D2 005 .01 .1 1 01 tm 002 1 r DATA PACKAGE Form 1 - Data Summary Report Prepared By: HydroLogic Laboratories, Inc. Client ID: Method Blank Project Number: Not Reported Sample ID: WG11669-1 Site / Project ID: Not Reported Run ID: R7546 Collection Date: Not Reported Received Date: 02-JUL-97 Report Date: 02-JUL-97 SW846 .Method. 1311/8240 Preparation Oaten '01-JUL-97 Analysis Date: '.01-JUL-97 11:22 Workgroup:Number. WG1.1669:: Benzene Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Methyl ethyl ketone Tetrachloroethene TrichLoroethene Vinyl chloride Dibrono fluoromethere Toluene-d8 4-Bromofluorobenzene 71-43-2 1 .ND ug/L 50 56-23-5 1 NO ug/L 50 108-90-7 1 NO ug/L i 50 67-66-3 1 NO ug/L 50 106-46-7 1 NO ug/L 100 107-06-2 1 NO ug/L. 50 75-35-4 1 NO ug/L '50 78-93-3 1 NO ug/L 250 127-18-4 1 :NO uglL 15o" 79-01-6 1 NO. - ug/L. ! :50 75-01-4 1 NO ug/L. SURROGATE 1 -108. - % - a; SURROGATE 1 - 102 % - (-'- SURROGATE 1 92 - % - I Review By: Rose Murphy Report Approved By: Karen Kuoppala "Dil" - Sample Dilution Factor "ND" - Sample Concentration Not Detected above RL "RL" - Method Report Limit Laboratory Control Spike / Laboratory Control Spike Duplicate DC Report Prepared By: HydroLogic Laboratories, IVc. Sample Id: /usr/users/seed2/target/A7503 Work Group Id: WG11669-2 Run Id: R7546 GALP Record Id: Not Reported Preparation Date: 01-JUL-97 Analysis Date: 01-JUL-97 Report Date: 09-JUL-97 Analyte CAS No. Low Limit High Limit RPD Limit LCS Add LCSD Add Units LCS VREC LCSD /REC LCS/LCSD RPD DUAL (1) SW846 Method 1311/8240 Preparation Date: 01-JUL-97 Analysis Date: 01-JUL-97 12:03 Workgroup Number: WG11669 Benzene 71-43-2 76 127 13 50 50 ug/L 78 86 10 --- Chlorobenzene 108-90-7 75 130 13 50 50 ug/L 84 90 7 --- 1,1-DichLoroethene 75-35-4 61 145 14 50 50 ug/L 68 82 19 --iJ Trichloroethene 79-01-6 62 137 24 50 50 ug/L 82 96 16 --- Note: Technical Review By: Rose Murphy Note: Report Approved By: Karen Kuoppala (1) OUAL - * = LCS Outside Control Limits; # = LCSD Outside Control Limits; a = RPD Outside Control Limits; '-' = Value Within Control Limits "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent "LCS,SD Add" - The conc. of analyte added to the LCS or LCSD sample. "LCS %REC" - Laboratory Control Sample Percent Recovery "CCSD-MEC- taboratory-Contmt- Sample-Duplir te-Percent-Rero ery "LCS/LCSD RPD" - Laboratory Control Sample / Laboratory Control Sample Duplicate Relative Percent Difference NR - Not Reported Form 1 - Data Summary Report Prepared By: HydroLogic Laboratories, Inc. Client 1D: Method Blank Project Number: Not Reported Sample ID: WG11661-1 Site / Project ID: Not Reported Run ID: R7572 Collection Date: Not Reported Received Date: 01--.JUL-97 Report Date: 07-JUL-97 Analyte CAS No. Did .Sample Conc. SW846 Method 1311/8270 Preparation Date: 01-JUL-97 Analysis Date: 05-JUL-97 15:00 Workgroup 'Number: WG11661 Cresol 106-44-5 1 NO ug/L. 2,4-Dinitroto Luene 121-14-2 1 NO ug/L Hexachlorobenzene 118-74-1 1 NO ug/L Hexachlorobutadiene 87-68-3 1 NO u§/L Hexachloroethane 67-72-1 1 NO ug/L Nitrobenzene 98-95-3 1 NO -ug/L Pentachloraphenol 87-86-5 1 NO -.ug/L: Py,p.idine 110-86-1 1 :NO.. ug/L. 2,4,5-Trichlorophenol 95-95-4 1 - ,. ND _, ug/L';.. 2,4,6-TrichlorophenoL 88-06-2 1 ND ug/l. Nitrobenzene-d5 SURROGATE 1 :62-z % 2-Fluorobiphenyl SURROGATE 1 72. ;%' Phenol-d6 SURROGATE 1 _51 % s. 2-FLuorophenoL SURROGATE 1 '`56 % 2,4,6-TribromophenoL SURROGATE 1 13r '-% Review By: Rose Murphy Report Approved By: Karen Kuoppala "Dil" - Sample Dilution Factor "ND" - Sample Concentration Not Detected above RL "RL" - Method Report Limit 00 00 Single Laboratory ControL Spike QC Report Prepared By: HydroLogic Laboratories, Inc. .t Sample Id: /usr/users/seed2/target/C2398 Work Group Id: WG11661-2 Run Id: R7572 GALP Record Id: Not Reported Preparation Date: 01-JUL-97 Analysis Date: 05-JUL-97 Report Date: 07-JUL-97 Analyte CAS No Semple Value Units Spike Cone. Low Limit High Limit SLCS XREC oUAL (1) SW846 Method 1311/8270 Preparation Date: 01-JUL-97 Analysis Date: 05-JUL-97 18:47 Workgroup Number: WG11661 2,4-Dinitrotoluene 121-14-2 Pentachlorophenot 87-86-5 Note: Technical Review By: Rose Murphy 76 ug/L 500 39 96 100 ug/L 1000 14 103 Note: Report Approved By: Karen Kuoppala (1) OUAL - - = LCS Outside Control Limits; '-- = Value Within Control Limits "Limits" - The '-Limits" reported above (Low and High) are in units of percent I%). "LCS-Add" - The-cone-of-anatyte-added-tcrthe-SLCS-sample. — -- -- "SLCS SREC" - Laboratory Control Sample Percent Recovery - NR - Not Reported Form 1 - Data Summary Report Prepared By: HydroLogic Laboratories, Inc. Client ID: Method Blank Project Nunber: Not Reported Sample ID: WG11689-1 Site / Project ID: Not Reported Run ID: R7573 Collection Date: Not Reported Received Date: 02-JUL-97 Report Date: 07-JUL-97 Analyte CAS No. Dim Sample Cone. Units i RL SW846 Methods 131:1/8080 Preparation Date: 02-JUL-97 Analysis Date: .03-JUL-97 16.48 Workgroup'Number:. WG11689 Lindane 58-89-9 1:NO ug/L .5 Chlordane 57-74-9 1 NO ug/L 5 Endrin 72-20-8 1 NO ug/L 1 Heptachlor 76-44-8 1 NO ug/L .5 Methoxychlor 72-43-5 1 NO ug/L 5 Toxaphene 8001-35-2 1 NO ug/L 24 Tetrachloro-m-xylene SURROGATE 1 ,:52 '% DepchlorobiphenyL SURROGATE 1 49 - X. Review By: Rose Murphy Report Approved By: Karen Kuoppala "Dill' - SampLe Dilution Factor "ND" - Sample Concentration Not Detected above RL 40 - Method Report Limit Laboratory Control Spike / Laboratory Control Spike Duplicate QC Report Prepared By: HydroLogic Laboratories, Inc. .$ Sample Id: LCS/LCSD Pair Work Group Id: WG11689-2 Run Id: R7573 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 Report Date: 07-JUL-97 Analyte CAS No. Low Limit High Limit RPD Limit LCS Add LCSD Add Units LCS %REC LCSD %REC LCS/LCSD RPD DUAL (1) SW846 Methods 1311/8080 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 17:31 Workgroup Number: WG11689 . Lindane 58-89-9 56 123 15 2 2 ug/L 65 67 3 --- Endrin 72-20-8 56 121 21 5 5 ug/L 97 100 3 --- Heptachlor 76-44-8 40 131 20 2 2 ug/L 68 69 1 --- Note: Technical Review By: Rose Murphy Note: Report Approved By: Karen Kuoppala (1) DUAL - * = LCS Outside Control Limits; # = LCSD Outside Control Limits; a = RPD Outside Control Limits; '-' = Value Within Control Limits "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent (%). "LCS,SD Add" - The conc. of analyte added to the LCS or LCSD sample. "LCS %REV - Laboratory Control Sample Percent Recovery _ _ "LCSD-Y.REC"- ---Laboratory Control —Sample Duplicate -Percent -Recovery -"LCS/LCSD RPD" - Laboratory Control Sample / Laboratory Control Samp Ce Duplicate ReCative"Percent Difference NR - Not Reported Matrix Spike / Matrix Spike Duplicate QC Report Prepared By: HydroLogic Laboratories, Inc. - Client Id: L5139-2 Work Group Id: WG11689-4 Run Id: R7573 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 Report Date: 07-JUL-97 Analyte CAS No. Lou Limit High Limit RPD Limit MS Add MSD Add Units Sample Conc MS %REC MSD %REC MS/MSD RPD DUAL (1) SW846 Methods 1311/8080 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 18:57 Workgroup Number: WG11689 Lindane 58-89-9 56 123 15 2 2 ug/L NO 55 55 0 •#-- Endrin 72.20-8 56 121 21 5 5 ug/L NO 88 88 0 ---- Heptach(or 76-44-8 40 131 20 2 2 ug/L NO 60 58 3 ---- Note: Technical Review By: Rose Murphy Note: Report Approved By: Karen Kuoppala ii) cuHL - - = ma uucsiae control Llmita; a = MSD Outside Control Limits; a = RPD Outside Control Limits; --I = Value Within Control Limits (1) OUAL - ! = The sample concentration is greater than two times the MS or MSD spike conc. High analyte Conc. wiLL effect the MS/MSD recoveries. "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent (%). "MS, MSD Add" - The conc. of analyte added to the MS or MSD sample (soil results are corrected for % moisture). "Sample Conc" - The units are the same as those reported on the Form 1 Data Summary Report (soil results are corrected for % moisture). "MS %REC" - Matrix Spike Percent Recovery "MSD %REC" - Matrix Spike Duplicate Percent Recovery __"MS/MSD RPD--= Matrix Spike /_Matrix -Spike Dup Licate-Relative-Percent-Di.f-ference— NR— - Not ReportedNO - Analyte "Not Detected" above the method detection limit. Form 1 - Data Summary Report Prepared By: HydroLogic Laboratories, Inc. Client ID: Method Blank Project Number: Not Reported Sample ID: WG11702-1 Site / Project ID: Not Reported Run ID: R7574 Collection Date: Not Reported Received Date: 02-JUL-97 Report Date: 07-JUL-97 I Analyte CAS No. _Dii Sample Cone. Units RL SW846 Methods 1311/8150 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 18:18 Workgroup ',Number. WG11702 .. 2,4-D 94-75-7 1 - '.NO ug/L 10 2,4,5-TP (Silvex) 93-72-1 1 ND ug/L 1 DCAA SURROGATE 1 79 % Y I Ir I.c 1 Review By: Rose Murphy Report Approved By: Karen Kuoppala "Di l" - Sample Dilution Factor � "ND" - Sample Concentration Not Detected above RL "RL" - Method Report Limit Review By: Rose Murphy Report Approved By: Karen Kuoppala "Di l" - Sample Dilution Factor � "ND" - Sample Concentration Not Detected above RL "RL" - Method Report Limit Laboratory Control Spike / Laboratory Control Spike Duplicate GC Report Prepared By: Hydrologic Laboratories, Inc. Sample Id: LCS/LCSD Pair Work Group Id: WG11702-2 Run Id: R7574 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 Report Date: 07-JUL-97 Analyte CAS No. Lou Limit High Limit RPD Limit LCS Add LCSD Add Units LCS %REC LCSD %REC LCS/LCSD RPD DUAL (1) SW846 Methods 1311/8150 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 18:55 Workgroup Number: WG11702 2,4-D 94-75-7 40 2,4,5-TP (Silvex) 93-72-1 40 Note: Technical Review By: Rose Murphy 160 25 20 20 ug/L 53 65 20 --- 160 25 2 2 ug/L 71 75 5 --- Note: Report Approved By: Karen Kuoppala 0 ) DUAL - ' = LCS Outside Control Limits; # = LCSD Outside Control Limits; iJ = RPD Outside Control Limits; '-' = Value Within Control Limits "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent "LCS,SD Add" - The conc. of analyte added to the LCS or LCSD sample. "LCS %REC" - Laboratory Control Sample Percent Recovery - "LCSD %REC"=.Laboratory_Control-Sample-Duplicate Percent Recovery - - "LCS/LCSD RPD" - Laboratory Control Sample / Laboratory Control Sample -Duplicate -Relative Percent Difference NR - Not Reported i Matrix Spike / Matrix Spike Duplicate DC Report Prepared By: Hydrologic Laboratories, Inc. Client Id: L5139-1 Work Group Id: WG11702-4 Run Id: R7574 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 Report Date: 07-JUL-97 Analyte CAS No. Lou Limit High Limit RPD Limit MS Add MSD Add Units Sample Cone MS %REC MSD %REC MS/MSD RPD DUAL (1) SWO46 Methods 1311/8150 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 20:10 Workgroup Number: WG11702 2,4-D 94-75-7 40 160 25 20 20 ug/L NO 83 72 14 ---- 2,4,5-TP (Silvex) 93-72-1 40 160 25 2 2 ug/L NO 79 77 3 ---- (1) DUAL "Limits" "MS, MSD Add" "Sample Cone" "MS %REC" "MSD 7REC" - "MS/MSD_RPD11- _—_.NR_ -- ND Note: Technical Review By: Rose Murphy Note: Report Approved By: Karen Kuoppala - = MS Outside Control Limits; # = MSD Outside Control Limits; a = RPD Outside Control Limits; '-' = Value Within Control Limits I = The sample concentration is greater than two times the MS or MSD spike cone. High analyte conc. will effect the MS/MSD recoveries. - The --Limits" reported above (Low, High and RPD) are in units of percent (%). - The conc. of analyte added to the MS or MSD sample (soil results are corrected for % moisture). - The units are the same as those reported on the Form 1 Data Summary Report (soil results are corrected for % moisture). - Matrix Spike Percent Recovery - Matrix Spike Duplicate Percent Recovery _Maid x-Spike_/ Matr-ix-Spike-Duplicate-Relative-Percent-Difiference ------ - -- - --- --- - - - - Not Reported _ - - ---- ----- - Analyte "Not Detected-' above the method detection limit. i. 0 I I Form 1 - Data Summary Report Prepared By: HydroLogic Laboratories, Inc. Client ID: Method Blank Project Number: Not Reported Sample ID: W01703-.1 Site / Project ID: Not. Reported Run ID: R7564 Collection Date: Not Reported Received Date: 02-JUL-97 Report Date: 03=JUL-97 Analyte CAS No, Di't Sample Conc. - Units ;.RL SW846 iMethods 1311/6010 PreparationDate: 02-JUL-97 Analysis Date.: '.02-JUL-97 23:50. - Workgroup:Number WG11703 Arsenic 7440-38-2 1 ND -mg/L, :,.2 Barium 7440-39-3 1 :ND. mg/L j:02 Cadmium 7440-43-9 1 ND ,;mg%L '005 Chromium 7440-47-3 1 AND mLq%L. ;.01 Lead 7439-92-1 1 :AND mg/L;.- .1 - Selenium 7782-49-2 1 - 'ND mg/L ,1 Silver 7440-22-4 1 ND mg/L ':. 1.01 Y Ad ll i 3 I F , I`[l 1 t f� L } 1 I i jI 1� l l I Review By: Rose Murphy Report Approved By: Karen Kuoppala "Dill' - Sample Dilution Factor "ND" - SampLe Concentration Not Detected above RL "RL" - Method Report Limit M P %IN Laboratory Control Spike / Laboratory Control Spike Duplicate OC Report Prepared By: Hydrologic Laboratories, .�Ic. Sample Id: /usr/users/seed2/pe3000/970702r5 Work Group Id: WG11703-2 Run Id: R7564 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 02-JUL-97 Report Date: 03-JUL-97 Analyte CAS No. Lou Limit High Limit RPD Limit LCS Add LCSD Add Units LCS %REC LCSD %REC LCS/LCSD RPD DUAL (1) ;W846 Methods 1311/6010 'reparation Date: 02-JUL-97 1naLysis Date: 02-JUL-97 23:54 )orkgroup Number: WG11703 Arsenic 7440-38-2 80 120 20 2 2 mg/L 102 101 1 --- Barium 7440-39-3 80 120 20 2 2 mg/L 98 98 0 --- Cadmium 7440-43-9 80 120 20 .05 .05 mg/L 92 94 2 --- Chromium 7440-47-3 80 120 20 .2 .2 mg/L 98 100 2 --- Lead 7439-92.1 80 120 20 .5 .5 mg/L 97 99 2 --- Selenium 7782-49-2 80 120 20 2 2 mg/L 96 94 2 --- Silver 7440-22-4 80 120 20 .05 .05 mg/L 73 73 0 *#- Note: Technical Review By: Rose Murphy Note: Report Approved By: Karen Kuoppala (1) OUAL - * = LCS Outside Control Limits; # = LCSD Outside Control Limits; a = RPD Outside Control Limits; '• = Value Within Control Limits "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent (X). "LCS,SD Add" - The conc, of analyte added to the LCS or LCSD sample. "LCS %REC" - Laboratory Control Sample Percent Recovery "LCSD-%RE 'C! —Laboratory-Control-Sample Dup L-icate-Percent-Recovery _ — - --- ----- -- --- - - - - — — — - "LCS/LCSD RPD" - Laboratory Control Sample /Laboratory Control Sample-Dup L-icate-Relative Percent -Difference NR - Not Reported L Replicate Sample QC Report Prepared By: Hydrologic Laboratories, Inc. .T Work Group Id: WG11703-4 Run Id: R7564 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 Report Date: 03-JUL-97 Analyte CAS No. Sample Cone REP Cone Units RPD SW846 Methods 1311/6010 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 00:12 Norkgroup Number: WG11703 Barium 7440-39-3 .491 .498 mg/L 1 Note: Note: Technical Review By: Rose Murphy Report Approved BY: Karen Kuc PPala Note - Only analytes with concentrations above the method detection limit are reported. Some samples may be reported above without any analyte concentrations. For these samples, analytes were not detected in the sample or in the sample replicate. "Sample Conc" - The sample concentration. "REP_Conc" - The replicate sample concentration. "R.PD" - Relative percent -difference "ND" - Not Matrix Spike / Matrix Spike Duplicate QC Report Prepared By: Hydrologic Laboratories,. Pc. Client Id: L5149-4 Work Group Id: WG11703-5 Run Id: R7564 GALP Record Id: Not Reported Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 Report Date: 03-JUL-97 Analyte CAS No. Low Limit Nigh Limit RPD Limit MS Add MSD Add Units Sample Conc MS %REC MSD %REC MS/MSD RPD DUAL (1) SW846 Methods 1311/6010 Preparation Date: 02-JUL-97 Analysis Date: 03-JUL-97 00:15 Workgroup Number: WG11703 Arsenic 7440-38-2 75 125 20 2 2 mg/L NO 95 92 3 ---- Barium 7440-39-3 75 125 20 2 2 mg/L .491 82 81 1 - --- Cadmium 7440-43-9 75 125 20 .05 .05 mg/L NO 85 84 1 ---- Chromium 7440-47-3 75 125 20 .2 .2 mg/L NO 86 83 4 ---- Lead 7439-92-1 75 125 20 .5 .5 mg/L NO 89 87 2 ---- Selenium 7782-49-2 75 125 20 2 2 mg/L NO 86 86 0 ---- Silver 7440-22-4 75 125 20 .05 .05 mg/L NO 61 58 5 *#-- Note: Technical Review By: Rose Murphy Note: Report Approved By: Karen KuoppaLa (1) OUAL - * = MS Outside Control Limits; # = MSD Outside Control Limits; a = RPD Outside Control Limits; '-' = Value Within Control Limits (1) OUAL - ! = The sample concentration is greater than two times the MS or MSD spike conc. High analyte conc. will effect the MS/MSD recoveries. "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent (%). "MS, MSD Add" - The conc. of analyte added to the MS or MSD sample (soil results are corrected for % moisture). "Sample Conc" - The units are the same as those reported on the Form 1 Data Summary Report (soil results are corrected for % moisture). "MS %REC" - Matrix Spike Percent Recovery "MSD Y.REC" - Matrix Spike Duplicate Percent Recovery --"MS/2•LSDJRPDII - M.atrixSpike_/_Matr-ix-Spike-DupL.icate-Relative-Percent-Differenc - -"-NR"-- - Not Reported — - - ---- "" — - -------- NO - Analyte "Not Detected" above the method detection limit. v Form 1 - Data Summary Report I - Prepared By: HydroLogic Laboratories, Inc. I Client ID: Methodelank. Project Number: Not Reported -- Sample ID: WG11715-1 - - Site / Project ID: Not Reported Run ID: R7582- CoLLection Date: Not Reported Received Date: 03-JUL-.97 - Report. Date: 08-JUL-97 Analyte CAS.No. Dil - Sample Conc..' Units. :RL SW846:;Method 1311/7470. - Analysis'.Oate: 04-:JUL-97 13-.35 Workgroup-Number: 1101715_ - Mercury 7439-97-6 1 :-ND: mg/L- - .0002.. y i i 11; l;. I�! i E , l Review By: Rose Murphy Report Approved By: Karen Kuoppala "Dil" - SampLe Dilution Factor "ND" - Sample Concentration Not Detected above RL "RL" - Method Report Limit rk um Laboratory Control Spike / Laboratory Control Spike Duplicate QC Report Prepared By: Hydrologic Laboratories, Inc. t Sample Id: LCS/LCSD Pair Work Group Id: WG11715-2 Run Id: R7582 GALP Record Id: Not Reported Preparation Date: 03-JUL-97 Analysis Date: 04-JUL-97 Report Date: 08-JUL-97 Analyte CAS No. Lou Limit High Limit RPD Limit LCS Add LCSD Add Units LCS %REC LCSD %REC LCS/LCSD RPD DUAL (1) SW846 Method 1311/7470 Analysis Date: 04-JUL-97 13:38 Workgroup Number: WG11715 Mercury 7439-97-6 80 120 20 .002 .002 mg/L 100 95 5 Note: Note: Technical Review By: Rose Murphy Report Approved By: Karen Kuoppala (1) DUAL - * = LCS Outside Control Limits; # = LCSD Outside Control Limits; iJ = RPD Outside Control Limits; '-' = VaLue Within Control Limits "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent (%). "LCS,SD Add" - The conc. of analyte added to the LCS or LCSD sample. _ "LLbU MLL" Laboratory Control Sample Duplicate Percent. Recovery--- --- - _—___ "LCS/LCSD .RPD" - Laboratory Control Sample / Laboratory Control Sample Duplicate Relative Percent Difference NR - Not Reported Ow i am Matrix Spike / Matrix Spike Duplicate QC Report Prepared By: HydroLogic Laboratories,.4 nc. Client Id: L5150-8 Work Group Id: WG11715-5 Run Id: R7582 GALP Record Id: Not Reported Preparation Date: 03-JUL-97 Analysis Date: 04-JUL-97 Report Date: 08-JUL-97 Analyte CAS No. Low Limit High Limit RPD Limit MS Add MSD Add Units Sample Cone MS YREC MSD VREC MS/MSD RPD DUAL (1) SW846 Method 1311/7470 Analysis Date: 04-JUL-97 14:04 Workgroup Number: WG11715 Mercury 7439-97-6 75 Note: Technical Review By: Rose Murphy 125 20 .002 .002 mg/L ND 105 100 Note: Report Approved By: Karen Kuoppala (1) OUAL - • = MS Outside Control Limits; # = MSD Outside Control Limits; a = RPD Outside Control Limits; '-' = Value Within Control Limits (1) OUAL - ! = The sample concentration is greater than two times the MS or MSD spike conc. High analyte conc. will effect the MS/MSD recoveries. "Limits" - The "Limits" reported above (Low, High and RPD) are in units of percent (X). "MS, MSD Add" - The conc. of analyte added to the MS or MSD sample (soil results are corrected for % moisture). "Sample Conc" - The units are the same as those reported on the Form 1 Data Summary Report (soil results are corrected for X moisture). "MS XREC" - Matrix Spike Percent Recovery "MSD %REC" - Matrix Spike Duplicate Percent Recovery -- - - "MS/MSD RPD" - Matrix Spike / Matrix Spike Duplicate Relative Percent Difference - - NR - Not Reported — — - - - - ND - Analyte "Not Detected" above the method detection limit. RI....LT---AL--3--_'A1'-_ JE�NI_. -' R1,':.-G18 7-021 Whitepine Road a Richmond, Virginia 23237 a (804) 743-9401 Fax No. (804) 271-6446 .lr At :>TG I SAMPI- NUMP' i EIO'-NOMIC SF_RVICES INC 516 ROUNDTR - RD CHARLOTTE NC 28217 06/20/97 PAGE 1 GROWER: HUFFMAN FINISHING SOIL ANALYSIS REPORT SAMPLES A C CT ✓a 46058 SUBMITTED BY: BIO—NOMIC SERVICES INC DATE.REC£IVED 06/18/97 DATE OF ANALYSIS 06/19/97 LAB ORGANIC PHOSPHORUS MATTER P1 P2 POTASSIUM MAGNESIUM CALCIUM SODIUM pH ',:. HYDRO= Cation Exchange PERCENT.:, ti .1 BASE SATURATION (COMPLTTED)"7 K Mg. Ca Na SOIL BUFFER NUMBER •• (Weak B: ly) (Strong Bray) ... ... GEN 7 H -.: Capacity C.E:O. % i. °ro EP.9 .:.. .... 15seA ppm.P R� f ppi 'P RATE ..:.. ppm K RATE .:. ppm-Mg RATE ppm-Ca RATE ppm-Na RATE pH pH ' ` meq/100g megN00g K Mg _ _RATE 10345, 4.1 126HI S L 14 L i 25 V4 144 VH 500 M 35 VL 6.4 6.9 0.4 4.3 1.5 27.9.58.1 8.9 3.5 i I i (SEE EXPLANATION ON BACK) Nm7ATC I SULFUR ZINC (MANGANESE IRON SAhITt 1;0� S I Zn hhT Fe. NUI'.IC .rc .N ,.A! E � (.pmdn RATE prve.,.I; RATE ppm-Fe RATE COPPER Cu ppm Cu RATE BORON B ppm-B RATE EXCESS LIME RATE '. SOLUBLE ' SALTS mmhos/cm RATE CHLORIDE - Cl ppm-CI RATE DENUM Mo' PPm-Mo '. RATE ,%; PARTICLE SIZE ANALYSIS :% SAND % SILT ' % CLAY SOIL - " TEXTURE 1 13 H 5.7 H j 11 h 30 H i i 1.2 P, 0.5 L <.3 VL L I j This report wd5 to the sample(s) tested. Samples are retained a M..imum I_..y aya after lasting. SoiIA I .pared by: ' a L ST AGRICULTURA B R ORIES. INC. - i by li M N J INS — — ix l"Pd '. RSr MULTIPLY THE RESULTS IN ppm BY J.e TO CONVERT TO LBS. PER ACRE P205 MULTIPL Y THE RESULTS IN To., BY 2 a TO CONVERT TO LBS. PER ACRE NCO .•^^-.:.......... ... .r..C.Xauy.......nnJ.pnf6m mov urcmuT ClH]nu-I--lr Vl" Wb INCHFe RFFP A & L EASTERN AGRICULTURAL LABORATORIES, INC. 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401 Fax No. (804) 271-6446 .t R1.25--165 ACCOUNT 45671 PAGE 1 MAY 15 1996 REPORT NUMBER BIO-NOMIC SERVICES, INC. 516 ROUNDTREE ROAD CHARLOTTE NC 28217 HUFFMAN FINISHING SLUDGE ANALYSIS REPORT BIO-NOMIC SERVICES, INC. DATE SAMPLED LAB NUMBER = 42276 DATE RECEIVED 05/07/96 SAMPLE II.I = HUFFMAN FINISHING DATE REPORTED 05/10/96 DETECTION RESULT RESULT LIMIT ANALYSIS PARAMETER ( % ) (MG/KG) (MG/KG) ANALYST DATE METHOII REFERENCE SOLIDS 1.56 15600 100 JCM 03/07/96 SM 25400 NITROGEN (TKN) 4.94 49400 100 L.DR 05/08/96 EPA 351..3 PHOSPHORUS 1.79 17900 100 JCM 05/08/96 EPA 363.4 POTASSIUM 0.27 2700 1.00 DCN 05/08/96 SW 846-60:1.0 SULFUR 0.98 9800 100 IICN 05/08/96 SW 846-6010 CALCIUM 1.32 13200 100 DCN 05/08/96 SW 846-6010 MAGNESIUM 0.83 8300 100 IICN 05/08/96 SW 846-6010 SODIUM 1.02 10200 100 DCN 05/08/96 SW 846-6010 IRON 37700 1 DCN 03/08/96 SW 846-6010 ALUMINUM 1.0800 10 DCN 0 5/00/96 SW 846--- 603.0 MANGANESE 774 1 DCN 03/0£3/96 SW 846-6010 COPPER 611 1 DCN 05/00/96 SW 846--601.0 ZINC 3880 1 DCN 05/08/96 SW 846-6010 AMMONIA NITROGEN 0.38 3800 100 LDR 05/08/96 EPA 350.2 NO3-NO2 NITROGEN 262 10 KCS 05/08/96 EPA 353.1 CADMIUM 2.0 1 DCN 05/08/96 SW 846-6010 CHROMIUM 331 5 DCN 05/08/96 SW 846-6010 _NLCKEf — __ _— _3S' S_ -- _ILCN 054QO./96___ - SW 846--6010 ILL VALUES EXCEPT SOLIDS AND TSS ARE ON A DRY WEIGHT BASIS. 'AUL C. H. CHU C. NORMAN JONES Our reports and letters are for the exclusive and confidential use of our clients, and may not be repr duc in whole or in part, nor may any reference be ma a to the work, the results, or the company in any advertising, news release, or other public announcements wi out obtaining our prior written authorization. Copyright 1977 A & L EASTERN AGRICULTURAL LABORATORIES, INC. 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401 ED Fax No. 804)271-6446 1T R125-165 ACCOUNT 45671 PAGE 2 REPORT NUMBER BIO—NOMIC SERVICES, INC. HUFFMAN FINISHING BIO—NOMIC SERVICES, INC. 516 ROUNDTREE ROAD CHARLOTTE NC 28217 SLUDGE ANALYSIS REPORT DATE SAMPLED LAB NUMBER = 4227L HATE RECEIVEII 05/07/96 SAMPLE ID = HUFFMAN FINISHING DATE REPORTED 05/10/96 IIETECTION RESULT RESULT LIMIT ANALYSIS PARAMETER ( % ) (MG/KG) (MG/KG) ANALYST DATE METHOD REFERENCE LEAD 27 5 IICN 05/08/96 SW 846-6010 ARSENIC 4.00 0.4 IICN 05/08/96 SW 846-7061 MERCURY loll 0.1 DCN 05/08/96 SW 846--7471 SELENIUM 0.08 0.1 IICN 05/08/96 SW 846-7741 PH (STANIIARD UNITS) 6,90 KM 03/08/96 EPA 150.1 CALCIUM CARBONATE EO ND 1.00 DCH 05/08/96 ASTM C602 VOLATILE_ SOLIIIS 64.41 644100 100 LDR 03/08/96 SM 254OG ORGANIC NITROGEN 4.55 45500 100 KCS 05/08/96 CALCULATED CHLORIDE 2780 1 DCH 05/08/96 SM 4500—CL )LL VALUES EXCEPT SOLIDS ANI.1 TSS ARE ON A DRY WEIGHT BASIS. ?a.C. H. CHU C.N ;MA4JO.-S Our reports and letters are for the exclusive and confidential use of our clients, and may not be rep duce in whole or in part, nor may any reference be made to the work. the results, or the company in any advertising, news release, or other public announcements w, out obtaining our prior written authorization. Copyright 1977 b �/Otl/a`J `J `J 1L: 15 tl[kid`lbtlSLb UKA1411t rNl.LS WWII" r'ti1Uc �I North Carolina Division of Environmental Management AGRE.E.MEl\7 FOR THE LAND APPLICATION OF WASTEWATER RESIDUALS TO PRIVATE LANDS perr.ittee Huffman Finishin .Compan Contact person' _ Lee T. Huffman Address ofPermittee: Post Office Box 170 Granite Falls. N_C_ 263o Lis; of wastewater residuals to be applied to these lands: Aerobically Digested industrial (textile) Wastewater Sludge. Site ID Number: 1 Field Number. L o:a7on of Land to be used for residual application (include map for each site): Grace rhapol �! Road. Travel 4 miles from U C 1 1 Fip1d on Right ! Owner of P:ope^. used for residual application: _ .t.z, Baumgarner :..'ssee 0.` Property (if appropriate): NA _�.., 1:5. �C cropping pallPCitS: Pasture III) :.-,t:.^.C'zz 'd5: o: disposition Of Crops: Hay III i ....,...>.;..e_landowner orhis representative hereby permits Huffman Finishing Com a 'l re`erred_ to as the Perrnittee, to apply the above listed residuals onto the land at the locla4'ion as des:r:bed herein in accordance with the restrictions and stipulations as given below.' ;:::soune: or his representative receives, in consideration, full use of the nutrient value of the applied res:d.:als' U4hi:e the Permittee receives_ in eensideratinn the use of the land deerriherl nhnve fnlr The thr ':sposal of wastewater residuals. This agreement shall remain in effect for the length of the Divisi Hn, ironmenta; Management land application permit and shall be renewed each time the land appli( -):?ni::S renewed. The undersigned land owner or his representative and the Permittee agree to abide .ae `o!loaring restrictions and stipulations until such time as written notification, given thirty (30) d - 4vance, modi!ies or cancels this Land owner's Agreement . Noti cation of cancellation of this agreement shall be immediately forwarded to: Division of Environmental Management Permits and Engineering Unit Post Office Box 29535 Raleigh, North Carolina 27626.0535 FORM: LARS 02195 Page 15 of 18 n of ir, 04 bt;;36/1999 12:15 8283968526 GRANITE FALLS WWTP PAGE Ob 1. J.P. Baumgarner have read this land owner's agreement and do hereby grant, w the Pertruxce to apply sludge/residual to my lands as specified herein, nn J NORTH CAROLINA, CALDWELL COUN^T�Y, 1 Lhe undersigned Notary Public, do hereby certify that J iJ u�g min. N e2 personally appeared before me this day and acknowledged the due execution of the forgoing iruwn w'ITNPSS my hand and official seal this day of 6 —.28" .19 - Q i NOTARY Pli LIC `— My commission Expires g O o SEAS.; • • • . . . . . . . . . . . . . . . . . • . • . • . • • ► ♦ • • . . . . . . . . • . . . r • . . . . i. have read this land owner's agreement and do hereby agree to the supulauons trd restrictions as specified herein. ent. 1, Lee T , Huffman have read this land owner's agreement and do hereby agree to:Iabide by the supulauons and restrictions as specified herein. ,1 , i FORM: LARS 02195 Page 18 of 18 06/29/1999 15.11 8283968526 '1��:'tCxl 4 IiLLU� 263 TE FALLS WWTP PAGE 01 na IIT• )� B \ Y I� I \ \ 1 rw n a t•a LaG1 ooa pt L d^ ` \�B V • pp• t�Y G.. PM AK° j1wLLNl W°L M � rRr /I «..ILL M.LMI.,11 -�yYui 1 / •n su � I a � M ck 1 C HgiY°L.L�L� n 3 «KL Gyn4 As ff„ I '6i➢ � �4 ``eqL1•�� • i�:A°' m_ ,., .:;: BURKE COUNTY nadE�t �x -- --__ - M U.a. - 321 1 Ak LOCATION MAP FARM: S.p- �u1�mcyACM.f FIELDS: um 09iC �1. q \\ •�� \Q ,. y;I As�I l,Iltv r :. i1. 1333 1000 CSC (\�,� - � °a, • a _.. i 1'.�, ,Ike. t Rdw�( wa ,W AMN •e� .:.�/i—.. r"�� � :', ..III �\ v�• n \`\ \ �` /�� :.�`. fit. ( y O `1 l/ D/) IVita (.�r .:f /°. � �i:.': �T (`% y't`�r '� �\j .� •`a� .�. 11 6so- \ r �„i Cs. ' /` Sl/ \ ✓I \l� '� 09 I 06/29/1999 15.11 8283968526 GRANITE FALLS WWTP PAGE' 01 v.,' 'l lay � r•' .: ! Norm ✓;k "11 >' J, L b + V eg A N Ll W°M«u. 01r ��/ ♦1i b':n . N. was am J � !k. C:. a V% •i +4F fl°. ° 1�1,, t � rw n IMAM fJ 'a. e I1 `� e ' arc to AW ic ou.l. �s1o+,• W0l M Ir9.Gll. l♦ E'. ' .. wrl.ra • nr —►-- I f AaMTu1 11 ■ •, ` oI ° j Ian Mr •nn I«� • _1. "ti. ° � 6i 1 f• I ' •� I pa• wlLa ' 0.1 321 ttn yp�p.y1N.�°p.M �ani ♦•.K♦ � Ir♦.gWY•f0 M w , I {`, n 4YLLI.l�OI _err «1 M" �� •• �' � �� • J S i. - I MWIf ,.� I (�.IC'r^II;" .:, •r BURKE COUNTY Y.I. '•b 311 4 --- 1 - LOCATION MAP FARM: n ips�i,r� Ca. FIELDS': I i !W�!•'..�•.i., •:)�! +tpf,••• •':.••• •.��\ l �1j,11�11W� 1 ._931 _ '1\.Gu p d C�r1eekgm n , Iss 1 .' .- -' i%T1, l:, ., 1, ' .,� , • � 1 _•. •..' , `\ 11I /_V\ 1^-�1 'Yr( �• {'-1 � ��J / �i ,II�. ��/ _ / - ,�,5< .tea .+� -1 \� `- ±I t)�• J.,1�. I F'1t��`.tt\��/ /v �/l l•�,. ,II I._/�. 7 _r ' �'.�• I l \ I \21 �1 ���-I �T r �(/ter,/ 'T ;It, /fl "`Y ���I- \ ~��� \:. 1� I/�l�l'. 1-��7'l_`r`II ' /I•• \,`� ll `.I� .z ,sk •- � � / rill '' . - � _ 1 '/ I a _ -„/� 1/ 1••` ��^ 1' \ On, itOn /.�/ tH�• �' I T ! �•`' �I� J �I' I (l,�r� ,"-�`/ i i i 1; liV l \ r a,o � .:�, .� J%N� •,� j � ilj1/Il` 1 .1 ••1.'� n�\) i'1�\ ` /.. "''•�,. +� �` HE`S / C: �.1 /1 (r r ' R,1,\ \�` C`D_5Y E L L Li C �� (' ` I Gb; a0/I"'J 12:1D 828d'db852b 6HAN11E FALLS WW1P 'h'46L d? 'north Carolina Division of Environmental Management ACREEMENT FOR THE LAND APPLICATION OF WASTEWATER RESIDUALS TO PRIVATE LANDS Pe,�:,:nee. Huff Contact Person. Le( Address of Permittee: L:si of wastewater residuals to be applied to these lands: Aerobically Digested Industrial (textile) wastewater Sludge. Site ID Number: Field,Number: L c,cz uon of Land to be used for residual application (include map for each site): US 321 A Travel C',tc;r of Propert)' used for residual application: Less:: of Property (if appropriate): 'se C. ; Cpping paUerns: Pa us: or disposition of crops: ...........................,..........................I:I. T^e undersi ned land owner or his representative hereby permits `ere:naner referred to as the Petmittee, to apply the above listed residuals onto the land at the Iota t�oµn as described herein in accordance with the restrictions and stipulations as given below,. :cndowner or his representative receives, in consideration, full use of the nutrient value of the epp residuals while the Permitme receives, in consideration, the use of the landdescribed above for sposal of wastewater residuals. This agreement shall remain in effect for the length of the Divisio c^\ ironmental'vlanagement land application permit and shall be renewed each time the land applica ,ermii is renewed. The undersigned land owner or his representative and the Permittee agree to abide :.he following restrictions and stipulations until such time as written notification, given thiny (30) da) advance, modifies or cancels this Land owner's Agreement . Notification of cancellation of this agreement shall be immediately forwarded to: Division of Environmental Management Permits and Engineering Unit Post Office Box 29535 Raleigh, North Carolina 27626-0535 FORM: LARS 02195 Page 15 of 18 tad/bU/1777 12: 10 b2bJ7bboLb UKAN11t rHLLb WW.r Yi-Il'�t ♦b John Frank Miller have read this land owner's agreement and do bereb1 grant �•r ='�=^ '^ apply sludge/restdual to mp lands M specified berein. FORTH CAROLINA, CALDWELL COUNTY, 11�n -.• ars:enedNotaryPublic, dohereby certifythat_ oko C"R-qnk lkIIiQn -ers: a_"y appeared before me this day and acknowledged the due execution of the forgoing ins 1 SS my hand and ofLcial seal this day of fO 2 19 _ Expires 41A_0 O SEA!• have read this land owner's agreemcn; and do bercbp agree r� inc rest-icuons as specified hereto Lee T. Huffman bave read this land owner's agreement and do hereby agree to _a V., _.elc s z. resuwuons as specified bert:in. T FORA: LARS 02195 Page 18 of 18 M. ioc 1999 15:11 8283968526 r:.auv iof axt..gt. LIP iwn tw , I� E FALLS WWTP \ `. PAGEi 01 wrt. � • i ,yt � \ 18 � !:ox hr � eitx R ■.r n tN aaa r " oee A `*9 •• ,11 lip INetMtre�•x v..coe• '�' { yuwe. M Ct". MU" Is °II e BURKE COUNTY R—__—__--___. �x LOCATION MAP FARM oi.n �. {ht��ef FIELDS 00 3 yvnri ) U Mit LJ)� vy�7 U"•��'�" ��/ 4 �y\ ��/� �,r'I'. .i '•"I ii .-` y ...��/IV--•iJ '�' .l ..f./', +��l.w-�2�_\i: G_ - ���V., Y, - �„` 71,.,,, �-�l' �. - ..fib.:- .-;,�:_<::.._- _- �, •• �:. ANN • �. �\ "I�it(•1•... � ./-� ` _ � J, ,-.i �+.�):+� ��i! 01 .'��:* I.y,, � • ,��, }I�1.l�-J�^� r1hri% %...t • � tJ' �•'�0 1 I IJr,..— , tit v pnoditnt) �aa.t� C6 i r�/iy r/' "1�4 ,(�� • l/ I�l�I: i 7\�r_-Ffi 1�, 10M �\, 1, �q � % i�. ��\ `� � �iJ L� � i �S �,,r<� i�' iTr.• zn NP . 1 , �-`• j);!� �il?�i .,�` .ate, STIPULATIONS- l • The landowner or his representative hereby authorizes the Permittee, County and State Officials or their representatives to inspect each parcel of property prior to, during, and after residual applicAtion and toestablished monitoring facilities on og near the application site as required by.the residual Il'and application permit. 2. The landowner or his representative authorizes the Permittee, County and State Officials or [heir representatives to take necessary soil, surface and ground water samples during the term of, and twelve (12) months after termination of, this Agreement. 3. The Permittee will provide each landowner or his representative with a copy of the land application permit as issued by the N.C. Department of Envirgnment, Health and Natural Resources (NCDEHNR) Division of Environmental Management (DEM) for the land described above prior;to commencement of residual application. The NCDEHNR-DEM permit will specify maxi application rates, limitations and other restrictions prescribed by the laws and regulations. 4. The Permittee has provided the landowner or his representative with information and data concerning the program for land application of residuals to privately owned lands which includes an analysis of constituents of the residual, residual application methods and schedules for typical cropping patterns and a description of the equipment used by the Permittee for residual application. 5. The Perminee will furnish each landowner or his representative with a copy of the results of each soil v analysis. 6`:` The site shall be adequately limed to a soil pH of at least 6.0 prior to residual application. Residua 3 may be applied to sites with a pH of less than 6.0 provided a sufficient amount of lime is also applied to achieve a final pH of the lime, residual and soil mixture of at least 6.0. 111 7. The landowner or his representative will inform the permittee of any revisions or modifications intended use and cropping patterns shown above prior to each planting season to enable the Per to amend this Agreement and schedule applications at appropriate periods. Within the limits NCDEHNR-DEM permit, the owner or his representative and the Permittee will determine re. application rates and schedules based on crop patterns and the results of soil samples. 8. Crops for direct human consumption shall be harvested in accordance with the conditions permit 9. The landowner or his representatives or successors shall adhere to the provisions of this Agteer for a period of eighteen U8) months from the date of the most recent residual application. 10. Appropriate measures must be taken by the Permittee or Land Owner (Lessee) to control pu access to the land application sites during active site use and for the twelve (12) month pe following residual application. Such controls may include the posting of signs indicating activities being conducted at each site. 11. Specific residual application area boundaries shall be clearlymarked on each site by the Permitta Land Owner (Lessee) prior to and during application. 12. Should the landowner or his representative lease or otherwise permit the use of the land by a a party, the landowner shall be responsible to insure the third party agrees and complies with the ter and conditions of this Agreement 13. The existing lessee, if any, of the site agrees, by execution of this Agreement, to comply with provisions of this Agreement. FORM: LAORS 02/95 Page 16 of 18 14. This Agreement shall be binding on the grantees, the successors and assigns of the parties) hereto with reference to the subject matter of this Agreement. 15. Animals should not be grazed on residual applied lands within a thirty (30) day period following the residual application. Application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after each application. 16. Prior to a transfer of this land to a new owner, a permit modification must be requested and obtained from the Division of Environmental Management. The request shall contain appropriate fees and agreements. In addition, a notice shall be given by the current landowner to the new landowner that gives full details of the materials applied or incorporated at each site. i 17. Any duly authorized officer, employee, or representative of the Division of Environmental Management may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the application site and facility at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that most be kept r unde the terins and conditions of this permit; or may obtain samples of groundwater, surface water, leachate, r 18. The landowner shall not enter into any additional waste disposal contracts or agreements with another municipality, contractor, of other permitted entity for the land specified by this Agreement. The land application of any additional wastewater residual sources, other than the residuals spec ified by this permit, is prohibited. Mvt 1 4 R t t f I t Y t I R R t f f Y 1 t f Y f t 1 R t t t R R f f Y R f 1 1 f t f Y f t Y f f R I t t •�f t R RESTRICTIONS: FORM: LAORS 02195 Page 17 of 18 nor E1,y,1.0a1AVC^ . Cj i9g� DIVISION OF ENVIRONMENTAL MANAGEMENT �(QR GROUNDWATER SECTION �aFsn� sccwNw February 28, 1990 TO: Don Safrit THROUGH: Bob Cheek FROM: Bill Reidy\� SUBJECT: Huffman Finishing Company Land Application of Sludge Caldwell County WQ0002431/GW89391 (Jack Floyd: DEM SERG Review Engineer) The Groundwater Section has reviewed the subject) application and recommends issuance of the permit with the f conditions: permit lowing 1. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. 2. Sludge shall not be applied within 100 ft. of a wate well. JWR/MC/ja cc: Barbara Christian Central Files Permit Issuance Files supply W o rJ7 RECORD OF WASTE DISPOSAL PERMIT APPLICATION REVIEW REVIEW BY e 55 e- ti/ kfe 115 DATE � /� �c� FIELD INVESTIGATION? J21 rl COUNTY C (Y/N )�— FACILITY NAME NurCm -;2 Fi �i s LOCATION I/Qr; ccis l i z ld5 TYPE OF DISPOSAL SYSTEM (LAGOON, ETC.) I�-nd cc G c:� DESIGN CAP. (GPD )— DESCRIPTION OF FACILITY5/ud e c ¢ a�ecF Fom then' /i' �c d �le5ieru G e <. SIZE OF IMPOUNDMENT (FT. SQ) & / OR SIZE OF APPLICATION AREA //.5 cures WASTE SOURCE : ❑MUN. SLUDGE MUN. W. WATER: PRIMARY SECONDARY 0, TERTIARY QIND. SLUDGE FIND. W. WATER OTHERS DISTANCE FROM WASTE SOURCE TO NEAREST: STREAM mac= FT., WELL : FOR WELL: TYPE OF USE Jorres'ric_ , DEPTH , PUMP RATE ( EST.) 'I / WHAT DESIGN CONDITIONS WILL RED / INCREASE CHANCE OF GW CONTAMINATION: ayy(;'ca�ie» wi T� WHAT NATURAL SITE CONDITIONS WILL REDUCE / INCREASE CHANCE OF GW CONTAMINATIONI: n / c DEPTH TO: BEDROCK %,50 Ff., SEASONAL HIGH W. T. FT. , ANNUAL W. T. FLU ; $- I o FT. -URFICIA•.. A,OUIFER BEDRO• K / ARTESIAN. AQUIFER) GEN. LTTHOLOGY Geci'/ Sandy C/4cr J6a)w -- i o L4e 6,.eiss r- :5c- s r HYD. COND. L- Q� FT./DAY MEAS ERU D 7, p FT./DAY MEASURED ESTIMATED [2ESTIMATED THICKNESS lLJ - 4 D FT. NO. OF MONITOR WELLS: PROPOSED: UP 0 DOWN 0 ; EXISTING : UP 0 DOWNI FROM WORKSHEET: SITE NUMERICAL DESCRIPTION=L _(r_-Q -4-b- 2—D `>F A — _,L' .9- T 1 2 3 4 5 6 6A 6B SITE GRADE (HYDROGEOL.) = C� PROPOSED SAMPLING SCHEDULE & PARAMETER(S): NeNe. SITUATION GRADE _ -9cc•o periled REMARKS/RECOMMENDATIONS:— hiell eooslruc6edz (eeords near sec/c"Pon soil horina -,e 0-6p --edny/ie�yiim��pc�-6eld5y oUcl- amd %L reVic t&) o{ Ae 5iz<e.J ,QQat4r Sul L�/e• �r a- �L orot�mrlr )a�Y %tnu('CP m zi eup�e, 1G aD,Q-e./ aLn lcdu-PeQ /i2. i7n�Kii' AOQ/1 `U1Yi�Pcc� a K_ S udr� lrrsis Glid I n no� la,ya4 e bial, )rganir• roam mi nad levels 'toluene de_Qed of /.3901 me Lhh . GW-48 Revised-8/87 HYD. REGIONAL SUPERVISOR I Lo ♦Truly �VCKMII n ru,,.AI m-m KtVltr( XiJJ1C7..bt�[.0 F,r•;..:.. Ferry: hruYl.�(2n !-;ir�ish�n9 1 V : Icl_t �. •I Card:_ c-lt/ it cwr: 3 / Pav,o.v9(: / Colo: iG 51,01 0.1.r..h. Irw d+dctio. Pohl vol" 0 1 2 3 A 6 7 6 9 1�C, on p-ouvd befw con- lorrk,ocbn. and Dklono. h 3(p -9Sp 76- 1-W 35 --f9 lo- 10 Dklwrw wofH rz9ply(wera ms1•n 1�- 150-299 60-]. - 20-34 0-9 .Cram), Dkl� h 62N. 1001 -3100 251 -SN 101 - I60 31-60 Ids Erhrns tho dopm lotr Aw Iobw bebw bo.e or wn- Iorkr,Abnra rrvxs m 5%0( o M) . Fx hk .wwor Cobb procrord ' M1om t'ranloTh- • olbn ai. SI.O / Fithn(s of panr/ bWy- ✓a'p(bnto:tt» . wet. dkppd SAO. L..1 310) - 62M 501 - 1 W0 161. 2--0 61 - 107 N01.•. N wofo! lobes h p. blo b.dork a. voue -6: h pP pemwoble b.o.vck Pohl woe 0 1 2 3 5 6 7 6 I.telen 40. 33-W 20-29 12-29 b11 b7 34 I6-26 5.1 Feel 2M 91.200 61-90 36-60 26-M 16-25 9.15 3-6 02 Wdw lable Grodort Groc;od podlonl or�d c`•'ay ham C4m nq dfedbn dwle< rot n9pL thOl o cbw( thv IOx1 male. 0-30 9 2(3.5 0 Doplh 0 W.T. Groderi b thm Grodoa 'Lau lhm Groc%.N Drealor G+ot Q.o.r 2pxcent 2pxoeri lrw 2 I 2 Iwad torroed Ps( a P-Monl wler vvlor lowotd (word rPPO W -"* W. 10( wdf rot the mdk the suppty u9* CrXrpdod mOCV>o(od Wrn( ordk the d.ectton of drodi on of tt» "o mlbpoled tbw 6w clpotod dxibn Ckedbn or rw of 11o+r C1ac-+- ro Sad wth Scr'd with 0rovs( a rl fo%• 16-20% Jwmthcsom&coon• CIO: Bond -oay 15%dov said " •mod ILA"✓-��- . MOro tfn 30 OA 2A AA dA AA 9A itm 95 I) I I 11 I II I 11 I 'll 1 II 25-29 OB 1C ID 7F 3E AG a 6E 7F ✓E 9G 9M 75-44 . 20-24 OC 2C IE 30 4D 6E 5G 6F -7H 7G BF 9H 9N 60-74 15-19 00 38 IF 4C 4E 6C M 70 6G _ 91 90 46-69 . 10-14 OE -4B '2D 68 AF 6D 51 7E 71 9D 9J 9P 26-AS J-9 18 65 2E 711 6C 7c 5.1 00 7J 9E 9K 90 10-27 L.w tlwn3 1B M x 6C • *W 9B 6K 9C 7K W 9( 9p lmritanl - Ifeckock of la wdaco; i - 62, I I -9Z I . fbls : H B.drock a fond Mooe, U.e 10 (p" opWoprbt• D-v+ o(oonrde kl o urocy o(vo4. s A - wry cod %Jfti c -wVh low OWV6 nos � Slog 6A Pohl of oono..n bth r+pad 10 axiaNwi .ouo. Y : W - r byvH . . 5 - rp6ro / ee B - P.A. Iw of oarptu 54to 69 kck t r l ewN6.f (CJ(ci. (D,iy C,,) D - Cores of doW"ilon or n.o(by PoTx*k 0 w.l hw . a M Mc.1/, hrk»rlos coriornhori lbw E- D61 n h a.p I bo"4 o lopc'oBon from oo.iorrinori pky roehw thou pow sows F - Wod. soups h P'ouid..0 dsct a or.O, *- rr:4na plwrd..cL.(oonlmJichon a d.pth / drm+o. K-Arwud*6-jn by oa.+ kn.don. M - FUd moo r.3no u We(As t lo* I4.IV P - 644 ho. Poa Psrcokdbn Poj. w (wkm of 3 a L 0 - Wo" .o.+os h Owed-of.r r+CwM.a.a 1 . WHst lobl. h wry 1i{jiy kodLu drock : - s*- urd.AOln by I a rt+o•. oi.dorl oq.i.. .2.O PI. VOL'O (Step 3) e ti �5E COloOor (Slop 4) Cor(dsnc (Sl.p 6) S P.:ri a(co Vt p a Crays 011sp 65) WASTE DISPOSAL PERAAIT APPLICATION REVIEW WORKSHEET'(CC+tT.) `lt 8 si. lJ,rrt»rfOof d«cx�f.,jn _�p ioki 31.p 1 Shp 2 3hp 3 3hp 4 Shp G Shp Fl. 3hp (,r7 (Add Shp 7 - t corm {.I1+n) ) sh Grod, C-J .d on fi�drap.:+Jp�' Paromotan Hmord Polonrbiikw tdonurro ( Fir" ) (0Ona) D G I 0 E H A c F S� FNN1 (1) M1kxnerbol Srte Do,,eplbn (tranS},p 7 ) C2) PAR VALUE (Slopo 3) -VTL I)ON RATING : (1) - CZ) -NTUATK>N GRADE no m (iw fob:a tx+� G►e fob;# below) Totd Pare/Sorp. WIA l7 5 + G _19 C T _. SUMWN RATM TABLE To b4 u..d for ahp 4( NArol) and Shp TO( M cow Rhp 7rD )NG NMT1ON RATPRO&INJTy OF &TUATTON (c«nbbod Vok>.) CONYA}AMNTION DEGREE OF A0C9lLkM fY GRADE a «{.K._ krpfobobio Prab3bY A -- -7fo'4 ? Pnbcbiy000*pk)b6a B a fo+o ? rrn«foh c -14lo+7 PloWby praboby Ur. pk 1. D ' +8amon VogP"bobfr Ahiodorrk)hto F «woo.pbb4 ' TM Probabrty o(Owdb mhotlon kom WuaKortr hawhp YcA� W~n 17 «)d - 7 k drrtsA to oofsporR. �. Th.r.(orr. thk tc n" o(wk» mpt* an -- f by pod" 6 and 4 dokr,4d afy by o q,» j mock A000p4ono. or r.).ctbn of oa .tf. f« ri. h *. d.d purpo.. k a rnpon&bwy of " Portta{or rpi:abry opwxy and my dop*nd on prcbf r•gvl-*n nh of tt» op*r) y on sty oral **ocuFbri o(opp"r d •no.h*o ip o(o %'$* (Stopo 4). _ lb. r .nvla luu._u vrll m ..... x •• n. .... ..nna..... x. 1l—\Lulrl.lrb Ilipp— UrWin lra.I.r ylrinlilnuut IA dill 11 . vgln ua p_\I.wKrna 111 LpL—nxnla'Ir Marra ur qur r nJ ill n.wI,.tn, Ill III' I' — MI h1.11rh IIi1al-mall in ana ur y.mnhr and.d Rn-n 11.11gndinr 1.—Iligl.—Lp:r ill it,.I ... qm. nJ 1.1 nl, Jrcly nrgm'm'c . 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I I fl.1nil t a uJa r. 111 ni'yo Ilµ'lir•Ia\nl•iJrmli...11.. l..':Il.piir.l In 111a'p,M1wutn, t-A,n,a'IMr•i l I l a J l l l"lilla'J it 1111a' right I.ncnJIhnhiFh rMlm lanuminno n'.arn, IIbr highIx'f..ianvm'n, Inpha nll.rn¢niun: nr higl. dn...... nnc,a- .nlilinn•nnuld .44 th, wli.t. it, Ihr ku _ Step 8 The position in IM mtdx hr oafi .`i1411P is (mill hr exEcMling pnkition of conumimnt xaenryanic Ily aMl aquJerrernirnity honzooulll'unlil111cv TCCI. The kuer In this sym s ld ix addN (prtttJN by to the lav nrn. cllmlcoti, larcr idcmihar M the sin' dcxnprims from Rep T. Evmplcc of S.wtiorts in T,, dIkt;ncs of Wott,. S.r A. M ,it still m.nhna1 M6an Merrua, Tam• This' miurga' am Rrlcmuahk- lincu Inc. Jw k4i, ,: 4.. .Mi.,Glun i in arJIkiNn.A."tmaJ innxn in nutria uui a'l IWl DI rav 4&-ri . ik<-Gxu<ntnfun aw(C) I inmrni b MNN. hill ayalloalurxvnvi<r ury�v IlvtaN oilmi:ri i, likh'mi il. Fv ll: A..niv Un U in Ilk tinth Onlim MNnxm M.hnui9. rurttiJcrNa mull kiW avnImia'o'wrs arc ilram J..mry,J nd rxtrtJ. Vipbnyfnaun lFnr.in'aNvh n1r rnanxJarnrhpnrayuilanlu. is to ,iMyuauJn n u.l\watirxr Jpunnl LIn nulnn ir.Jiave• ta m 1.Jcn:aly aIlil). Di kne Nntn.n.rn'.•: m1 Ionu.nnxnl .. akvinlc, l,ut v xm'-1n ni.n and llrluri..n-I—h I,,Irralnl. Fr 1: IM.nalrl lvvkkk reuJu' frunaam,Mx nv Ilk, an mnn r{o.i,W InarkiJk- kii ua• li u. a J.. m Mr_Vlanriv Gusul Min nlwra' link' la nWiim n.J,, rrlrran' a nukkkn ctr pl'rnw lsIv mlorvf: 3yr111 rit Thin a.J n.t v\trn m. Ix*wkil lra- in lliv ali imlkan> a -I liplr l\Ynt rl \'nrxnrn'•a 01uwFhmnm Ali lim.inuxvT in ni Ink' ay.ufn dnua:nuiav rrryr4ot au.-11yarJrn aN 11111tis'. is Ind, In .it anv la .\ muniallvt v ilan WIWill 1:1 Iannl 1\nnaba.na i 'Ihic\ dua• na+lk' IvwalpGx. unJ JIaIr. a1J v.nlamw Ml� n'wLinp in qv nrpivFl hlµayui:a': xlu\II i• w: v'm n a v.Jayxa-nl r.nra.n rulilna Ik+vunJ h�an..n.n n '.uliol.\a ]1.•4n:vlon'IkY;nerl4'rinwv'r'A:11^tiv Jucd.enstil� it Ilk.,t nok, I-- nl .•IJrp: rill rxv, ,..ma.'...'r F`-a1x1 k:xlu.a'Ymrq;• p�py (I'hil II,, ia�:uW Appmirhoj .............. .n,.........n....r...n n..r._a...._.vr.xx...a. .un...u.�r T•iw_.F'c:...............e..... ...........rn u...-....... o. n.:..........nru...a... .............................. ...,.._.-....... ... ................... :............. ..a.;.,........i.,,..,.o-.}-...:.�.:.. ,... p..,t ..-....... I I:V.AR1) 1101 EN ILV. NA''RI\ (I )tgrcc u( �-6,In>nc..p DLrpoebo DEGREE OF Sk3UGlJSNESS Modrnlciy Nigh '®mt 7`. r C iii a a': x ras W }y Y 'S 5,• a yi I c Guc (cnam. W. N.uw. anJ. <aav Mining ' (rirJLxnl IIUN 'f.l — Mlnnl USm'. U4J, ISIwo'routlr l `.AJ•I (h. s fus hrlwn' h\v. Imgj (rury;) Jleulh tiul Mini, ltstil� tiniJlhµ Mlp Nibs Laiax \11'g. WAOa eN'aa's .. Iknv 11a.1• F.n. ..Ira 11�Ja.d. •(Y •OOIs) H7 o)o aV•^4oj• e tolddo )o ugV)D" • P• AIMCP+ ) uo) Aou•Oo .LA)o y,. ,,k>.J pp.d. uo pu.d*p Acw puo �nOsj )oYn .y4 )o AjXGft%Jdf•I o' •todlnd P`P"4 044 M •iP oo )Ougloei'I Io aouoldrrlY. b o Aq AW P•uQ,°P)iIO Pw B "PO)O Aq P•luo+gld.l wnp^ )o f= NiU'awl )qu L 'A1,opo)`>✓ o' I� a 4?'vUJIP M L - PuoL. tuo4 uogoululoulo' o3lO N7Mo4o)d ° a Us S) at4wgOpm p air dl-aA p st4IXda�lAR°4°d a14�4 p �{. B ... • � • V1d3y)y DmiDK Nd1VN1WY1N00 (arlpA Paul4w�0) I - . . j0 Wygdgpyd MlLLV21 NOLLdf117S ( PaUIPPY'{) o! dalS P— (P"ON) b.0 aNS,o) P� eq o1.' . ..:3)G':S=s,`\1`fa•NCiA:fLlio i _ — oz< Z — 0 01> ,uapansg Y Z — (wnwxnu) :wipup >IrIY, (wnw!:Inu) iiul 'Pup vond,v; ,>,q;� »untgl In4L �.�illgvxw4l _ _ ; hill Iron LO ,.�P•.uugl ii: — 1 -! U' .t]i2t-'uql >i<OIuYtO,ll III J t)o P>;' l >Pup i, _ - BAKER PiEDMOiNT WELL & PUMP C�.: gN�QX 27687 — RALEI6H, II,C, 21611 ROUTE 6 BOX 523 HICKORY, N. C. 28601 /= ILLING LIONTRACTOR REG. NO WELL CC 1. WELL LOCATION: (Show sketch of ..the location below) Nearest Town: (")�l'NA /r- /.a S County: fi Ai /y � •�.z / /a f..bZ� /-C Y I//! C:.� \ j f=_nuadra n<j le No. y �'h i,c :iq f Rcad, Comm�unit or Subdivision and No. 2. OWNER: i J. ADDRESS: /.t/ / i '-i/\ DRILI 4. TOPOGRAPHY: draw,valley,sl_ opeoe,h4_lltop,flat(cirele one) DEPTH 5. USE OF WELL: •,• -.�- DATF: 6. DOES THIS WELL REPLACE AN EXISTING WELL? i 7. TOTAL DEPTH: 4Q{ " RIG TYPE OR METHOD: X,l ram,? S. FORMATION SAMPLES COLLECTED: YES NO N V 9. CASING: Depth Inside Wall thick. type Dia, or weight/ft. From _to //,l ft C"l,_ ,/Li:I' �1,,. /�• 10. GROAT Depth Material Method From to •,%C-, ft j//�7•e,-. �r �_7 11. SCREEN: Depth Dia. From— to —ft — 12. GRAVEL: Depth Size From _ to _ ft 13. WATER ZONES(depth): Type 6 Opening Material 14. STATIC WATER LEVEL:_ ft.above below top of casing Casing is ft. above land surface ELEV: :;6. YIELD (gpm): METHOD OF TESTING:,>-,� = 16. PUMPING WATER LEVEL: ft after hours at gpm. 17. CHLORINATION: Type 1,41 Amount t' 18. WATER QUALITY: r•[.;/_TEMPERATURF.(oF) 19. PEUMANENT PUMP: Date Installed Type Capacity (gpm)-Hp_ Make Intake Depth. Airline Depth Tim Pf.RNIT R'.1. /47 NC. LOC. FORMATION DSSCRIPTIO14 I I,N, •i C If additional space is needed „usG back of LOCATION SKETCH (Show distance to numbered roads, or other map reference pc J- F-f,I15 ram,. 20. HAS THE OWNER BEEN"PROVIDED A -COPY OF THIS RECORD'AND INFORMED OF THE DEPARTMENTS RECOMMENDATIONS? /: 21. REMARKS n V S AND I do hereby certify that this well was constructed in accordance with R.C. Well Constructiu�� Regulations and Standards and �PHa this well ,l g6ord is tiue and exact. ATURE OF CPNR'RA TOR OR AGENT DATE f..• Form CW-1 Revised 10/l/76 Submit one copy to Groundwater Section and -no I to owner I LiK,: CL?ARTHENT GF ::ATE"n Al2 A 1 R RESOURCcS 1`72 J G141Si0N OF GROUND WATER - 8 BOX 27048 - RALEIGH, IN. C. Req. No. .:-J ..� Well Pcrr•;t No. ._ ✓,.. �«x�_-�--- County ,,,n bxcA of form �j �` ✓ Pot. ....... 1y'yF/":�"._pp-�??•• / / 'frog; ie I:,., ..,1 ,,.:. 4. Topography: draw slope, hilltop, valley, flat 1~ 5. We of Well-���''-^'-�° Date, Completed 6. Rig type or method !� eel ,4L() Total Depth T,7 7. Casing: Depth Diam. Type From O to - 'a—ft. in. 8. Grout: Depth Material Method From to �fZft. �'v�iti_ ' 9. Screen: Depth Clam. Type and opening From to ft. in. — 10. Water Zones (depth) Static Water Level: ft, above top of casing a 11. below which is ft. above land surface. Elev. Date 12. Yield (gpm) 4 Method of testing 13. Pumping Water Level: ft. after hrs. at gpm. 14. Water Quality Temperature (OF) 15. Well sterilization method 16. Permanent Pump: _ Type Make Installed- _ Date By Capacity (gpm) Hp. Intake depth Airline depth 17. Remarks: I do hereby certify that this wall record is true and exact./ SIGNA URE OF CONTRACTOR OR AGENT -- White coDY - Department of Water-3-Air-Resources;--Blue-Drii-lerecopy;- Green-OwnerLs_copy. I Form GW-1 WELL 'N.1 fik-3 P.C.. BOXI 27C37 1INTLIANG CON'-11,.-- :G J1U.f:l9?-n VIVU 11 RUM CO o P F (S."01., SKoL:h Of ,Nearest To•,n: (T.".., In e Fa .1 C. DEN' twL c ngs 0/11b` RALJ & ECONO z0l:i Toc No.) o. , irr. 2. O'.-,'M:R! Co..) 3. Af)D11i:5S; Lw:L� 521, P.0. `�om 170, 4 . TOPOGRAPHY: dra.i,vi !it. Y '% 5. USE OF WFLL: W=: VVY7 6. DW:S THIS Wi 'LL RF2 7. 7CTAL D2.1"TH: Pot 9. CASING: Depth tea 1. DID e Y 5 8 P. q apLh �:a-uri 20. GROUT: D a 1 Front 0 to 20 fti—' Conci-ete, 2 -7 11. SCREEN: Dapth Dia. From —to—,-. 12. GRAVEL: Depth Size From —to—ft ,y.pa . Opening Vaterial 13. WATER ZONES (depth) 82 & 210 ft. 14. STATIC EATER LEVET.: ft.al�o-,*o —L5— � below*tO.3 Of casing CaSing is _—ft. above lan'-1. surface WLXV: 15. =*Lu (qpm)_: 100 Gz 1s5TI NG: _n�ch. 16. PUMPITIC WATER LEVEL: 210 It after hours at 9P.M_ 7- additional spat t is .ed.dus, LOCATION S.KUCH (Show c4c-.Lne, co n=b=red roads, or other cap rcierc li punLTTii.f v t'l TyIX: M.ake Intake je, th Airline Dcj),tY.._ 20. HAS "IM: PP.1VIDM) 1. COPY OF THIS rECORP AN_ 07 THE NKPARTXENTS RECOMMENDATI(XIS? 21. PUIAMMS I do her-,hy co r. i F, :`:at th1F wc.1 1 1:.v; Cc.n.i ti-Go:.'! in -.Z7 with N. C. We I I C'nu; t lo-clulations ar"I t1l:'. :.`:in tIC-11 a - ---------- Form rW--1 HI'vised 10/1/76 cnc ccpy to Groun1water Section ,it:! 7—. Date: January 8, 19901 STAFF REPORT AND RECOMMENDATIONS County: Caldwell WQ No. 0002431 MRO No. 89-272 PART I - GENERAL INFORMATION 1. Facility and Address: Huffman Finishing Company Land Application of Sludge Post Office Box 170 Granite Falls, NO 28630 2. Date of Investigation: December 21, 1989 1 3. Report Prepared By: Michael L. Parker, Environmental' Engineer II 4. Person Contacted: Mr. Lee Huffman; telephone numberi(704) 396-1741 5. Directions to Site: Directions to all four (4) sludge land application sites can be found in the report as submitted by the applicant. i 6. Discharge Point: N/A Attach a USGS Map Extract and indicate sludge disposal sites. USGS Quad No.: D 13 SW and D 13 SE 7.' Size (land available for expansion and upgrading): Approximately 115 acres are available for sludge disposal. 8. Topography (relationship to flood plain included): Ranges from gently rolling to slopes >18%. None of the four sites appear to be in a flood plain area. 9. Location of Nearest Dwelling: occupied dwellings are located at or near sites No. 1, 2 and 3 and will require appropriate buffers as prescribed in 15 NCAC 2H 0.020.0. 10. Receiving Stream or Affected Surface Waters: N/A PART II - DESCRIPTION OF SLUDGE i 1. Type of Sludge: 0% Domestic 100% Industrial a. Volume of Sludge: 18.7 tons/year (dry weight),I79,190 gals/year (wet volume) Page Two b. C. d. Types and quantities of industrial sludge: _he�sludge i is generated from the finishing process of hos,ry products. Prevalent toxic constituents analysis has determined the and non -hazardous. Pretreatment Program (POTWs in c-.astewater: A kludge sludge to be both n®n-toxic only): N/A 2. Production Rates (industrial discharges only) in Pounds: N/A 3. Description of Industrial Process (for industries only) and Applicable CFR Part and Subpart: N/A 4. Type of Treatment (specify whether proposed or existfi'ng): N/A 5. Sludge Handling and Disposal Scheme: Dewatered sludge will be transported to the sites in dump trucks. Liquid sludge will be transported in sealed tanker trucks. Application will be by either surface application and/or subsurface injection. PART III - OTHER PERTINENT INFORMATION 1. Is this facility being constructed with Construction Grants Funds (municipals only)? N/A 2. Special monitoring requests: N/A 3. Additional effluent limits requests: N/A 4. Other: N/A PART IV - EVALUATION AND RECOMMENDATIONS Huffman Finishing Company has submitted an applicat permit to land apply sludge from on -site wastewater trea facilities to approximately 115 acres of pasture land. Application method will be either surface or subsurface on the moisture content prior to disposal. Application restricted to agronomic rates and applied to each'site e three years. The primary use of all four (4) sites are with Sites No. 1 and No. 2 supporting livestock. for a 1 be every ture Soils at all four sites are of -a Cecil sandy loam t e have physical properties ideally suited for sludge land application. Site borings did not encounter any evidence of saprolite above 48 inches. Soil sampling did reflect a low pH which should be adjusted by liming at least three (3) ion prior to sludge application. Phosphorous has been found to be the limiting consti for this project. A phosphorous loading of 120 lbs/acre/ and soil the is Page Three recommended by Dr. A. R. Rubin with North Carolina State University Agriculture Extension. This office recommends that a quarterly sludge analysis be made and the results submitted on an annual basis to this iffice. The report should include, but is not limited to: TKN NH as N PoLssium Copper Nickel Arsenic Calcium Sodium Solids Total P Nitrate Zinc Lead Cadmium Mercury Magnesium pH In addition, the annual report should include an annual analysis of the soils and site vegetation at the receiver 'sites (those which have received sludge). This will insure thatl the soils and vegetation are not accumulating waste constituents and the nutrients necessary for plant growth are being provided. Some topographic constraints (slope) exist on Sites No. 1 and No. 3 and should be buffered by flagging. The northern most part of Site No. 1 (approximately 3-4 acres) should be eliminated due to the proximity of two (2) homes. All applicable buffers as noted in 15 NCAC 2H 0.0200 should be included in the.Permiit, Pending further review, recommendations and/or comments from the ERG and Groundwater Sections, it is recommended that a! non -discharge permit be issued to the Huffman Finisbi-g Company. a RECEIVED DIVISION Of ENVIRONMENTAL YMRREYEIfi ,IAN 25 1990 YOORE$VIILE GROUNDWATER SECTION RMONIE OFIlCB MEMORANDUM [ // TO 134%�Q/Q CR�IST/EG/i1 FROM: Mike Cleary DATE: //;"a` go , SUBJECT: T�4mam 1-i T— c� S?-y 3c/ / (/ 1. Attached is a copy of the additional information we have received'on the subject project. I 2. It is our understanding that a copy of the additional information that we have received concerning this project has been sent directly I Please review this information and provide your comments and recommendations by FeA �- 1979- If for any reason you find that the supplied additional information is still insufficient to make an evaivation of the project, please let us know _immediately, so that either the needed data can be requested from thel applicant, or some other appropriate action taken: If you have any questions concerning this matter, or require additional information, please advise! mdc/adinnot i �1a JAN 19 1990 , 2RWJND!"IATEP, SECT!()"' The Wooten January 22, 1990 Company Engineering Mr. Bill Reed Planning Groundwater Section Architecture NC Division of Environmental Management P.O. Box 27687 Raleigh, NC 27611-7687 Re: WQ0002431/GW89391 Land Application of Sludge Huffman Finishing Company Caldwell County 120 N. Boylan Avenue Dear Mr. Reed: Raleigh. NC 27603 Reference is made to the October 25, 1989 letter from Mr. Michael D. Cleary concerning the additional information' requested on the analysis of sludge for (1) volatile organic compounds, and (2) acid/base neutral extractables. The requested 919-828-0531 information is attached to complete the review of the referenced project. I Should you have any questions concerning this matter, please call me at (919) 828-0531. Sincerely, �THE \�WOOTEN COMPANY :P \ 11 4 Shankar R. Mistry, PhD, P.E. SRM/hsc c: Mr. Jack Floyd, Environmental Engineer Mr. Lee Huffman, Huffman Finishing Company Since 1936 i JAN 19 190 17:45 CHEN ENVN TECH 683 P02 Chemical & Environmental Technology, Inc: �•' C, ENVIRONMENTAL ENGINEERING AND LABORATORY SERVICES JOHN M. OGLE P. 0. BOX 12298 PRESIDENT RESEARCH TRIANGLE PARK N. C. 27709 PHONE (9191 467-3090 FAX'(919) 467-3515 MR. SHANKAR MISTRY THE WOOTEN COMPANY 120 N. BOYLAN AVE RALEIGH, NC 27601 RE: HUFFMAN FINISHING COMPANY 'TG�3 o_.1tis�� P nilu'I",4 v-• S?41t-1 (J`;r,L Js w�) SAMPLE HISTORY CLIENT ID CET SAMPLE DATE RECEIVED EFFLUENT 33495 12-28-89 SLUDGE 33496 12-28-89 PARAMETER ALUMINUM, mg/1 ANTIMONY, mg/1 ARSENIC, mg/1 BARIUM, mg/1 BERYLLIUM, mg/1 CADMIUM, mg/1 CHROMIUM, IOTA, mg/1 COPPER, mg/1 LEAD, mg/1 MERCURY, mg/1 NICKEL, mg/1 SELENIUM, mg/1 SILVER, mg/1 ZINC, mg/1 ANALYTICAL RESULTS FEDERAL REGISTER, VOL 49, NO. TL/bws METHOD JANUARi 18, 1990 DATE ANALYZED 12-30-89 TO 1-12-90 1-08-90 i EFFLUENT 202.1 01.14 204.1 0�17 206.2 0:041 208.1 0148 210.1 <01001 213.1 0:018 218.1 0f013 220.1 01045 239.2 01002 245.1 <010002 249.1 0.094 270.1 <0:001 272.1 0�004 289.1 0:406 209, OCTOBER 26, 1984 CHEMICAL & ENVIRONMENTAL TECHNOLOGY, i TE RIE LITZ ERGS ASSISTANT LABORATORY MANAGER IN .NUFv[go'R� fif�rjlj.,„ JRN 19 '90 17:45 CHEN ENUN TECH 688 P03 PURGEABLE HALOCARBONS METHOD 8240 DATE ANALYZED: 1-08-90 CLIENT ID: SLUDGE CET SAMPLES 33496 DETECTION PARAMETER LIMIT (ug/kg) BENZENE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM DIBROMOCHLOROMETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE 1,1-DICHLOROETHENE TRANS-I,2-DICHLOROETHENE 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRANS-I,3-DICHLOROPROPENE ETHYL BENZENE METHYLENE CHLORIDE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROMETHANE VINYL CHLORIDE XYLENES BDL - BELOW DETECTION LIMIT 5.0 5.0 5.0 5.0 5.0 5.0 10.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 RESULTS (ug/kg) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1390 BDL BDL BDL BDL BDL BDL "TEST METHODS FOR EVALUATING SOLID WASTES", SW-846, VOLUMi 3, SEPTEMBER, 1986 J - Indicates an estimated value. This flag is used when1the mass spectral data indicated the presence of a compound that meets the indentification criteria but the result is less than the specified detection limit. JAN 19 '90 17:46 CHEM ENUN TECH 683 PO4 BASE NEUTRAL/ACIDS METHOD 8270 DATE ANALYZED: 1-08-90 CLIENT ID+ SLUDGE CET SAMPLE, 33496 BASE NEUTRAL DETECTION PARAMETER LIMIT RESULTS (ug/kg) I(ug/kg) ACENAPHTHENE 200 BDL ACENAPHTHYLENE 200 BDL ANTRACENE 200 BDL BENZO(A)ANTHRACENE 200 BDL BENZO(B)FLUORANTHENE 200 BDL BENZO(K)FLUORANTHENE 200 BDL BENZO(GHI)PERYLENE 200 BDL ,BIS(2-CHLOROETHYL)ETHER 200 BDL 5IS(2-CHLOROETHOXY)METHAME 200 BDL BIS(2-STHYLHEXYL)PHTHALATE 200 BDL BIS(2-CHLOROISOPROPYL)ETHER 200 BDL 4-SROMOPHENYL PHENYL ETHER 200 BDL BUTYL BENZYL PHTHALATE 200 BDL 2-CHLORONAPHTHALENE 200 BDL 4-CHLOROPHENYL PHENYL ETHER 200 BDL CHRYSENE 200 BDL DIBENZO(A,H)ANTHRACENE 200 BDL DI-N-BUTYLPHTHALATE 200 BDL 1,2-DICHLOROBENZENE 200 BDL 1,3-DICHLOROBENZENE 200 BDL ICHLOROBENZENE 200 BDL ( 3,3'DDICHLOROBENZIDINE 200 I BDL DIETHYL PHTHALATE 200 BDL DIMETHYL PHTHALATE 200 BDL 2,4-DINITROTOLUENE 200 BDL 2,6-DINITROTOLUENE 200 BDL DI-H-OCTYLPHTHALATE 200 BDL FLUORANTHENE 200 BDL FLUORENE 200 BDL HEXACHLOROBENZENE 200 BDL HEXACHLOROBUTADIENE 200 BDL HEXACHLOROETHANE 200 BDL IDENO(1,2,3-CD)PYRENE 200 BDL ISOPHORONE 200 BDL 2-HETHYLNAPHTHALENE 200 BDL NAPHTHALENE 200 BDL NITROBENZENE 200 BDL N-NITROSODI-N-PROPYLAMINE 200 BDL PHENANTHRENE 200 BDL PYRENE 200 BDL 1,2,4-TRICHLOROSENZENE 200 BDL A JRN 19 190 17:46 CHEN ENUN TECH 689 POS I PAGE #2 BASE NEUTRAL/ACIDS METHOD 8270 CLIENT IDe SLUDGE CET SAMPLEa 33496 • I ACIDS DETECTION PARAMETER LIMIT RESULTS (ug/kg) (ug/kg) 4—CHLORO-3—METHYLPHENOL 200 BDL 2—CHLOROPHENOL 200 BDL 2,4—DICHLOROPHENOL 200 BDL 2,4—DIMETHYLPHENOL 200 BDL 2,4—DINITROPHENOL 1000 BDL 2—METHYL-4,6—DINITROPHENOL 1000 BDL 2—NITROPHENOL 200 BDL 4—NITROPHENOL 1000 BDL PENTACHLOROPHENOL 1000 BDL PHENOL 200 BDL 2,4,6—TRICHLOROPHENOL 200 BDL BDL — BELOW DETECTION LIMIT II "TEST METHODS FOR EVALUATING SOLID WASTES", SW-846, VOLUME 3, SEPTEMBER, 1986 J - Indicates an estimated value. This flag is used when the mass spectral data indicated the presence of a compound that meets the indentification criteria but the result is less than the specified detection limit. 11 The Wooten Company Engineering Planning Architecture 120 N. Boylan Avenue Raleigh, NC 27603 919-828-0531 Since 1936 December 15, 1989 Mr. Jack Floyd Environmental Engineer Permits and Engineering Section N.C. Division of Environmental Management P.O. Box 27687 Raleigh, NC 27611-7687 Re: W00002431 Land Application of Sludge Huffman Finishing Company Caldwell County, North Carolina Dear Mr. Floyd: Reference is made to your October 7, 1989 letter to Mr. A.W. I Huffman, Jr., concerning your review comments on the referenced project. The comments are addressed as follows: 1. Four (4) copies of the completed Waste Determination Form lare attached herewith. 2. The new site maps showing the property line and sludge application area are attached herewith. The topographic features along with the nearest well and dwelling for each' site are given on Exhibits 1 and 2 in the Preliminary Engineering Report. Buffer zones are included in the Operation Plan given in the Preliminary Engineering Report. Buffer zones will be flagged prior to land application of sludge. ii We appreciate your assistance in this matter. Should you have any questions concerning this matter, please call me at (919) 828-0531. Sincerely, -::51�rt„PuvCpa. C-11 N. C. DEp . Shankar R. Mistry, Ph.D., P.E. CoalalREso�mccsNAT°it+ I UNITY DLYEECP IEN7' SRM/sjf EDEC 1 9 1989 Enclosure DIVISION OF MDDRESV1�YZIONIIOT � enlrAs w I CC: /Mooresville Regional Office LtE p7 1/ Mr. A.W. Huffman, Jr. OfflC6 •0 'v =• :'�'�1➢q• o`Lr �i'/J.'%l Rv y y� �f :I [ter r•: , e�td{p^•er •'�;?a��'�Ya.�f'i y �2�1 �Lj���r KN-!�'"'�+"�_.n�:a� �+•LFf�.�..�' .,:. IN 41 so _��T�dllr< f"�i �c4;a,�'.,':1�`i,JS.u.�.. `v.. :•t'��.+tL.�'•��.-rirY ..'.,';"�!� • :"~..y'..4 I ~f � � • - In " y ••�? � `:'.y i ��i•.1 •' � � i•ht'u. ./ \Ja�.'7 • : {��+C :�,�r '�.•Rr�.'w:;�.p r. T {. .lam; ,_�� �' i. A. _ S •+c 1{eT� c, r.'��• � s y �ny ' •' r j. 4 j j ft7%'�Y�f • � � � �.:�, i � �--Cy`�f'i`. t ram•,• � . •' r f e- J•••• +�t•� y ... fit. ,�.: f _ i:•_-'.. c-r ^+.�• Sri yr. � r f.•�. �i'4 i,:.�� Ir•V�� �• / �' � L• �. • -s' ,�!%h� � ai !_EGEND SCAtE_ L" 0 600' PR-oPERTY LLNE LAND /+�pruu+�fua rattan SITE h10. I 1 S '�ilc'z <r SI'✓i �., w- ,; a r .sue (. �i.^. 1 'Yoi IP 7111. 4-11 fi Y a ��lae�y b l � L 1 � � � r♦..'' � r• • t r a,,. � u r � y# �f• y t. Y, t r a r � �9�: , 1 I • l •� •- r f ! r O r r zi r • it � ..a .l "i 1 "£ ' >< !s ..♦ iJ' �J r � y"`�"'�'.�.i18r}�/ ,t*w >,� ?r aJ.l r , t lr ♦ t�}.4..a 6. -ei '. a r ♦ f "a Y as _rt�� ♦ r ire Vital S> ♦,�' I „a r r y.r + �t•jar Q S .{ � e,t r � r�I,i �s�l� Iv..� z I ♦ Y t'. s r v.t' a .V`"� , ri. 1. 3 •! Y> :f i ' r , ��� r4�e>�. >+}MY��S aar rl ' t. :fit �al� �! ♦4 '' ^.(a ,aa Y . .ry<<< f♦ . "' 3 1 f'+( :.r' FLPf T. ♦ _�. f,{ors/,. Pf .r�Y / wiJ4it Y ♦ �.-. ll i aryrwl •s 4. ' L�.X �r r �� a � a ' � � {r h' , , : a� ♦ _ t r a ^ F r'+ 1 1} . �efn ei�:• t { d as:.r ,n ��: �r.7,,,. ,`. i. r'ia'. . � Y. er • a. C: :. 4 to � � N i > >• 1 t c: r Y Y,. 9 Pi rr I .",'. 1 L10 0 3 AV Ml c �. SfAIEo RECEIV: D s .. 81YISION GG ENVIRONMENTAL MPN0.6EMEN4 �u3 OCT 30 taP4 MOORESVILLE REGIONAL GFROE State of North Carolina 1 Department of Environment, Health, and Natural Resources Division of Environmental Management 512 North Salisbury Street a Raleigh, North Carolina 27611 James G. Martin, Governor WiWam W. Cobey, Jr., Secretary Mr. A.W. Huffman, Huffman Finishing P.O. Box 170 Granite Falls, N. Dear Mr. Huffman: October 25, 1989 Jr., President Company C. 28630 SUBJECT: Huffman Finishing Company R� Paul Wilms Director Land Application of Sludge Caldwell County WQ0002431/GW89391 I As part of the Division of Environmental Management's comprehensive approach in addressing the impact of waste treatment, storage, or disposal projects on the environment, your permit application has been forwarded to us for assessment of the potential impact of the project on groundwater quality; I Our initial review indicates that the data submitted is not sufficient to make this assessment. Before your application can be processed therefore, you are requested to submit the following information 'to the Groundwater Section. This information should be submitted in full within 60 days of the date of this letter. Failure to comply may result in the returning of this application as incomplete. I. From a sludge analyses previously submitted, it is noted that the concentration of total organic halides wasireported to be 1.339 mg/l. You are therefore requested to submit an analysis of the sludge for (i) volatile organic compounds, and (ii) acid/base neutral extractables. These analyses should be performed using the appropriate EPA methid having the lowest detection limits. Pollution Preventlan Pays P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-7015 An Equal Opportunity Affirmative Action Employer Please feel free to contact the Groundwater Section, at (919) 733-3221, if clarification or information is required.) Sincerely, Michael D. Cleary/ Hydrogeologist Permits Group MDC/ja cc:,e, e, Jack Floyd Mike Cleary Mr. Shankar R. Mistry 120 N. Boylan Avenue Raleigh, NC 27603 Central Files Permit Issuance Files DIVISION MEMORANDUM TO: Lrie DATE: /0-4--g9 FROM: Bill Reid SUBJECT: Application Facility Name County Type of Project Applicable Permit GROUNDWATER ENVIRONMENTAL MANAGEMENT I x C nrrT cosr_i:R;,j�U2� SN, r a�T 0 3 1g8 !1'•O�fS!7ilf �f�Uil�( Ofh��lC�rNr ,Renewal/Amendment Y New Permit WQ 006 24.3t We have received a copy of the above referenced app which was sent to Your regional office for comment on or 9�Z4 1989. You should review the application package for compl adequacy of relevant information and submit your request additio al information to me (via telephone or memo) by �� /4 1989 so that all required information requested from the applicant at one time. A copy of our request to the applicant for additional information will provided.to you.. 1. If you do not require additional information from th applicant to complete your evaluation of .the project, you review the application package and submit' -your comments t _/0 Z7 1989. If a`copy of the application package has not been ma available'to your office, PLEASE LET ME KNOW IMMEDIATELY copy can be forwarded to you as soon as possible. that a MDC/APPMEMO r Engineering Planning Architecture September 21, 1989 Ms. Carolyn McCaskill, Supervisor Engineering Section N.C. Division of Environmental Management P.O. Box 27687 Raleigh, N.0 27611-7687 N. C. DEPT. or I�1,1TUIRU R FSOURCES AND COS[.l'U\TTY DEVEL01'D[ ENT I SEP 2 7 1989 OIVISrtl OF EIIV1001MENiALI IM1.4GEOLU MiORESYILLE REGIONAL OFFICE J I Re: Non -Discharge Permit Application i Land Application of Sludge 12O N. Boylan Avenue Huffman Finishing Company Raleigh, NC 27603 Dear Ms. McCaskill: Attached please find four (4) copies of the Non -Discharge Permit Application for land application of stabilized sludge s1s-eze-BSB1 generated at the Huffman Finishing Company's Wastewater Treatment Plant. A check of $250.00 for the permit fee is also attached. Should you have any questions concerning this matter, please call me at (919)828-0531. Sincerely, 21, � Shankar R. Mistry SRM/smj Enclosure cc: Mooresville Regional Office V Huffman Finishing Company Since 1936 �L D E M USE ONLY North Carolina Department of Natural Resources and Community Developments p, permit Number: Environmental Management Commission NON -DISCHARGE PERMIT APPLICATION* COV aty: • in accordance with N.C. General Statutes Chapter 143, Article 21 Cal dwell Applicant (name of board, individual, or others): Application Date:1 A.W. Huffman Jr. August 4 1989 project (name of city, village, town, sanitary district, establishment): CompanyHiiffmAn Finishing I Sludge Disposal Brief Project Description: 1�FIOR' µ4 Non -Discharge Treatment/Digposel Facilities ❑ Pretreatment Facilities Land application of aerobically digested sludge ❑ Sewer Collection System (private) generated at Huffman Finishing ComD nn 'C � 6F NATVRA4- ❑ Extend Sewer and Sewer Systems (public) wastewater treatment plant. N. C. RESOSOIJTiCES AND NATURE OF WASTEWATER: CO30._N1T' DEVELOPDIEN' Sewage SEP P 7 1989 Sludge/Industrial Waste Other Waste From (sewers, pretreatment facilities, treatment plants): Serving (city, institution, industry): lY1$ION OF DiY1l�llk)Er1 it "M G"t { I Huffman Finishing Company WWTP Huffman Finishing Com REGIONAL OFFICE Into (name of treatment plant): Tributary To (name of water course): _ N/A 1 I At (location of treatment plant): Name and Complete Address of Engineering Firm: Zip Code: Telephone No. The Wooten Company, 120 N. Boylan Ave. Raleigh, N.C. 27603 919-828-0531 Treatment Works Capacity to Serve (name of project): or (no. ynJ Average Daily Gallons Sewage or Waste Flow: i Affect Overall Reduction in Pollution (not applicable for sewer projects): N A Estimated Costs: B.O. D. (5-day 2dr C) Toxic Materials (specify % each, add pages if needed) % % Sewers S I Pumping Suspended Solids % % Station S Treatment TOTAL SOLIDS % % Plant i Other (specify) Estimated Completion, Date: Coliform Bacteria % TOTAL TOXIC MATERIALS % October 15 1989 Applicant assures that proposed works will be constructed, supervised, operated and maintained in accordance with approved plans and specifications or approved changes thereto. Print Nam.: Title: Mailing Address: Zip Code. A.W. Huffman, Jr. President 1'-0.3OX 170 GPLAN1'r1C RAL.LS N'.C.X8630 Telephone No. 704 396-1741 Si gnaturo: A r_ _ i INSTRUCTIONS: V' V I. Fill-in ALL spaces. If not applicable, enter N/A. 1 2. Secure appropriate signature (mayor/city manager for municipality; chairman for sanitary district board; owner/proper official of corporation; or legally constituted board or commission in charge of proposed works). A letter of authorization is required from prof per official if design engineer or other agent signs application. 3. Submit 1. N.C. Department of Natural Resources and Community Development, Environmental Management, Rolaigh, NC, the original and first copy of application, 2 sets of finalised plans, specifications and other supporting data as required by Commission Rules. NOTE: tppll*etiopnaleviews are scheduled on receipt of COMPLETE information. Generally, 30 days are required for pollution abatement projects; 90 days For Assistance, call the State Central Office 919/733-5083, P.O. Box 27687, Raleigh, N.C. or: Asheville (704) 253-3341 159 Woodfin Street Asheville, NC 28801 -Mooresville (704) 663-1699 919 North Main Street Mooresville, NC 28115 ,Washington (919) 946-6481 *Winston-Salem (979)1761-2351 1502 North Market Street 8003 Silas Creek Parkwoy Extension Washington, NC 27889 Winston-Salem, NC 27106 *Fayetteville (919) 486-1541 *Raleigh (919) 733.2314 'Wilmington (919) 256�4161 Suite 714 Wachovia Building Be. 27687 7225 Wrightsville Avan.. Fayetteville, NC 28301 Raleigh, NC 27611 Wilmington, NC 28403 I PRELIMINARY ENGINEERING REPORT FOR LAND APPLICATION OF SLUDGE HUFFMAN FINISHING COMPANY WASTEWATER TREATMENT PLANT GRANITE FALLS, NORTH CAROLINA SEPTEMBER 1989 0 C'GR - :7�'..�'MJEEe:' Shankar R. Mistry, Ph.D., P.E. THE WOOTEN COMPANY Engineering — Planning — Architecture RALEIGH — GREENVILLE, NORTH CAROLINA TABLE OF CONTENTS SECTION TITLE PAGE NO. 1.0 Introduction I i i 2.0 Sludge Quantity and Characteristics 2 I 3.0 Land Application Sites 3 4.0 Application Rate and Area Requirements 3 5.0 Expected Site Life 7 6.0 Operation Plan B 7.0 Summary and Recommendations I 11 I TABLES I 1 Land Application Site Data 4 EXHIBITS 1 Location and Topographic Map - Site No. 1 I 12 2 Location and Topographic Map - Site No. 2, 3, & 4 13 3 Soil Map - Site No. 1 14 4 Soil Map - Site No. 2 15 5 Soil Map - Site No. 3 16 6 Soil Map - Site No. 4 I 17 APPENDIX I 1 Dr. Rubin's Site Investigation Report 2 Agreement Letters 3 Sludge Analysis and EP Toxicity Test Results I I I PRELIMINARY ENGINEERING REPORT FOR LAND APPLICATION OF SLUDGE HUFFMAN FINISHING COMPANY WASTEWATER TREATMENT PLANT GRANITE FALLS, NORTH CAROLINA 1.0 INTRODUCTION Huffman Finishing Company operates a 0.25 MGD extended aeration -type activated sludge plant which discharges its effluent into an unnamed triI bu- tary of Catawaba River. The unit operations/processes at the plant include screening, dechlorination, flow equalization, extended aeration (oxidation ditch) type activated sludge system, chlorination, post aeration, aerobic sludge digestion, sludge storage basin, and sludge -drying beds. The screenings removed in the preliminary treatment are trucked to the sanitary landfill site for ultimate disposal. The excess sludge produced in the biological treatment (activated sludge) system is removed by wasting I it to the aerobic digestor. The sludge is stabilized in the aerobic diges- tion process, and after stabilization it is decanted and either discharged to sand beds for dewatering or to the sludge storage basin for ulimate dis- posal. The dewatered sludge from the beds is manually removed and trucked to the sanitary landfill for ultimate disposal. In order to comply with the recent changes in the sludge disposal regulations, the Company is planning to dispose of the aerobically digested i liquid as well as dewatered sludge by land application on the privately owned pasture land. The sludge will be applied on an agronomic basis. Accordingly, the purpose of this report is to provide necessary supporting) data such as sludge quantity and characteristics, land application site data, sludge application rates, expected site life, and operation plan for the Permit Application for disposal of sludge by land application. -1- 2.0 SLUDGE QUANTITY AND CHARACTERISTICS A. Sludge Quantity: 1. Dry weight basis = 37,405 lb/year I = 18.7 tons/year 2. Wet volume basis = 79,170 gals/year at 5.5% solids B. Sludge Characteristics mg/l mg/kg* Total Kjeldahl Nitrogen, TKN 1,772.00 32,218.00 Ammonia Nitrogen, NH 176.00 3,182.00 Nitrate, NO 4.50 81.80 Total Phosphorus, P 4,046.00** 73,573.00** Potassium, K 500.00 9,091.00 Zinc, Zn 20.00 364.00 Copper, Cu 3.00 54.50 Lead, Pb 0.30 5.45 Nickel, Ni 0.41 7.45 Cadmium, Cd 0.15 2.73 Arsenic, Ar 0.60 10.90 Mercury, Hg 0.017 0.31 Calcium, Ca 1,650.00 30,000.00 Magnesium, Mg 300.00 5,455.00 Sodium, Na 1,200.00 21,818.00 pH 6.50 Standard Unit Percent Solids 5.50 Percent *Results reported in mg/kg are on dry weight basis. **Average results of the three analyses for phosphorus _ (131,818 + 54,400 + 34,500)/3 = 73.537 mg/kg -2- 3.0 LAND APPLICATION SITES I Four (4) sites consisting of approximately 235 acres will be used for land application of aerobically digested liquid as well as dewatered sludges. Approximately 115 acres of land area are available at the site Is for land application of sludge. Details of the sites are given in Tablell. Location and topography of the sites are shown on the Exhibits labelled as location and topographic map. The landowner agreements participating inthe land application of sludge generated at the Huffman Finishing Company's wastewater treatment plant are given in the Appendix. All the land applica- tion areas at the sites are located outside of the 100-year flood prone I area. The nearest dwelling and water supply well at each of the sites are I shown on the Exhibits labelled as location and topographic map. The sites were evaluated by Dr. Rubin with the Agricultural Extension Service, N.C. State University. Dr. Rubin's report on the evaluation of the sites for land application of sludge is given in the Appendix. F,:•.ed upon Dr. Rubin's report, the sites are suitable for land applic.d:i.: • ie•robill- ally digested liquid as well as dewatered sludges generated at the Huffman Finishing Company's wastewater treatment plant. 4.0 APPLICATION RATE AND AREA REQUIREMENTS A. Nitrogen Loading I 1. Sludge Quantity - 18.7 dry tons/year 2. Nitrogen in Sludge: Total Kjeldahl Nitrogen, TKN, mg/kg = 32,218 Ammonia Nitrogen, NH3 -N, mg/kg = 3,182 Nitrate Nitrogen, NO3 -N, mg/kg = 81.8 - 3 - TABLE 1 LAND APPLICATION SITE DATA (SITE NO. PROPERTY OWNER ACREAGE Total Available 1 J.P. Baumgarner 60 25 2 Huffman Finishing Co. 35 20 3 John Frank Miller 80 35 4 Ricky L. Winkler 60 35 TOTAL 235 115 0 PREDOMINANT SOIL TYPE COVER CROP Cecil Sandy Loam (31) Fescue Pasture Cecil Sandy Loam (31) Fescue Pasture Cecil Sandy Loam (31) Fescue Pasture Pacolet Fine Sandy Loam (30) Cecil Sandy Loam (31) Fescue Pasture 3. Nitrogen Loading Rate: Property/Farm Cover Crop lb PAN/Ac/Year Bumgarner Fescue Hay Pasture 180 Huffman Finishing Fescue Hay Pasture Company 180 John Frank Miller Fescue Hay Pasture 180 Ricky L. Winkler Fescue Hay Pasture 180 I 4. Organic Nitrogen Mineralization = 20 percent 5. Nitrogen Loss Due to Volatilization, Denitrification, arld Percolation Loss: a. Subsurface Injection Application = 0.0 percent b. Surface Application = 50 percent 6. Plant Available Nitrogen (PAN) in Sludge: a. Subsurface Injection: I PAN = (TKN -NH3) x 0.2 + (NH 3 + NO2 + NO3) = (32,218 - 3,182) x 0.2 + (3182 + 0.0 + 81.8) = 5807.2 + 3263.8 = 9071 mg/kg = 9071 mg/kg x 0.002 = 18.14 lb/dry ton b. Surface Application: PAN = (TKN-NH3) x 0.2 + (NH 3 + NO 2 + N% ) x 0.5 = (32,218 - 3,182) x 0.2 + (3,182 + 0.0 + 81.8) x 0.5 = 5807.2 + 1631.9 = 7439.1 mg/kg = 7439.1 mg/kg x 0.002 = 14.88 lb/dry ton 7. Land Area Required: I a. For Subsurface Injection: - 5 - I Area, Acres = 18.14 LB PAN/ton x 18.7 ton/year 180 lb PAN/ac/yr = 1.88 acres b. For Surface Application: Area, Acres = 14.88 lb PAN/ton x 18.7 Lori/year 186 lb PAN/ac/yr 1.55 acres B. Phosphorus Loading: 1. Phosphorus in Sludge = 73,572 mg/kg = 73,573 mg/kg x 0.002 147.15 lb/dry ton 2. Phosphorus Loading Rate = 120 lb P/acre/year 3. Land Area Required: Area, Acres = 147.15 lb P/ton x 18.7 ton/year 120 lb P/acre/yr = 22.93 acre C. Cadmium Loading 1. Cadmium in Sludge = 2.73 mg/kg = 2.73 mg/kg x 0.002 I = 0.005 lb Cd/dry ton 2. EPA Cadmium Loading Criteria = 0.45 lb Cd/ac/year 3. Land Area Required: i Area, Acres = 0.005 lb Cd/ton x 18.7 ton/year 0.45 lb Cd/ac/yr = 0.21 acres I D. Solids Loading 1. Sludge Quantity = 18.7 ton/yr 2. Solids Loading Rate = 5 dry ton/ac/yr 3. Land Area Required: - 6 - Area, Acres = 18.7 dry ton/_vr 5 dry ton/ac/yr = 3.74 acres E. Summary of Area Requirements: Loading Parameter Area,Acres Nitrogen Loading (180 lb PAN/ac/yr) 1.88* 1.55** Phosphorus Loading (120 lb P/ac/yr) 22.93 Cadmium Loading (0.45 lb Cd/ac/yr) 0.21 Solids Loading (5 dry ton/ac/yr) 3.74 *For Subsurface injection application **For Surface application Considering the area requirements for various loading parameters, it can be seen that the sludge application rate will be limiting to PHOSPHORUS LOADING. Based upon the phosphorus limiting sludge application i rate, i approximately 23 acres of land area are needed for the land application of sludge. Referring to Table 1, the total land area available for land appli- cation of sludge is approximately 115 acres. 5.0 EXPECTED SITE LIFE Considering the metal constituents in sludge and maximum metal loading allowable at sites having soil CEC of < 5.0 mgq/100 gm of soil, the expected site life is calculated as follows: Heavy Maximum Metal Metal Content Total Quantity' Metals Loading Allowable in Sludge of Sludge Allowed, lb/acre mg/kg lb/ton ton/acre Pb 500 5.45 0.011 I 45871 Zn 250 364 0.728 343 Cu 125 54.5 0.109 1146 Ni 50 7.45 0.015 3355 Cd 5 2.73 0.0055 915 7 i From the above site life calculations, it can be seen that ZINC will be the limiting metal for total sludge application at the site. Considering the PHOSPHORUS LIMITED sludge loading, the expected side life is estimated as follows: Site Life, Years = 3.43 ton/ac x 22.93 ac 18./ ton/ac = 420 years Considering the total acreage available (115), the expected site life is estimated as follows: Site Life, Years = 343 ton/ac x 115 ac 18./ ton/yr = 2109 years 6.0 OPERATION PLAN: Land application of sludge will be performed in accordance with the following guidelines: 1. The dewatered sludge will be transported in a dump truck and applied at the site with a manure spreader. The liquid sludge willl be transported in a sealed tank truck and applied to the site byl surface spreading and/or subsurface injection. Surface -applied sludge will be plowed or disced-in immediately after application on i fields with no cover crop. 2. Prior to the initial sludge application, each field will be limed to a pH of 6.5. Thereafter, soil tests shall be performed annually i and lime additions will be made in accordance with the rc..ommen& tions given in the soil tests reports. 3. The land applicaton of sludge+will be carried out by setting -up thti sites to receive sludge on a 3-year rotation basis. Agronomic rates will be used for the land application of sludge. 4. The sludge application shall not exceed the following loading rates: a. Annual Loadings: Plant Available Nitrogen, PAN = 180 lb/ac/yr Phosphorus, P = 120 lb/ac/yr Cadmium, Cd = 0.45 lb/ac/yr Solids = 5 dry ton/ac/yr b. Cumulative Loadings: Lead, Pb = 500 lb/ac Zinc, Zn = 250 lb/ac Copper, Cu = 125 lb/ac Nickel, Ni = 50 lb/ac Cadmium, Cd = 5 lb/ac 1 5. Sludge shall not be applied in inclement weather or until 24 hours following a rainfall event of 1/2 inch or greater in 24 hours. The existing aerobic sludge digestion tanks, sludge storage basin, ai4 the sludge -drying beds will be used for sludge storage t...ilitie-J when the sludge application cannot take place due to ir..ienient I weather conditions or during hay -cutting operations on the field!.!. 6. No crops for direct human consumption shall be raised on the field's for a period of 18 months following sludge application. 7. Lactating dairy animals shall not be grazed on sludge -applied areas for a period of one year following sludge application. All other' animals should not be grazed on sludge -applied land within a 30-day period following the sludge application. If grazing is allowed on I the fields, then fencing will be used to prevent access after each application. - 9 - I 8. No land application of sludge shall be conducted where the depth to the seasonal high water table is less than 3 feet. 9. The following buffer zones shall be maintained during land I application of sludge operation. a. 400 feet from residences under separate ownership for surfaIce application method. b. 200 feet from residences under separate ownership for I subsurface injection application method. C. 100 feet from "SA and SB" classified waters and public surface water supplies for both sludge application methods. d. 50 feet from "WS" classified waters and other streams, creeks, lakes, rivers, and surface water drainage h.:.. for subsurface injection application method. e. 100 feet from "WS" classified waters and other streams, creeks, lakes, rivers, and surface water drainage ways for surface application method. f. 100 feet from any property line for both methods. g. 50 feet from public rights -of -way for surface application method. I h. 10 feet from upslope interceptor drain and surface water ! diversions for both methods. i. 25 feet from downslope interceptor drains, surface water diversions, and groundwater drainage systems for both methods!. j. 100 feet from any well with the exception of an approved !, groundwater monitoring well. 10. Collect annual soil samples and analyze for pH; lime requirement;! plant available N, P, and K; total Pb, Zn, Cu, Ni, Cd, CEC, and organic C; and base saturation. organic C; and base saturation. I 11. Collect hay tissue and analyze for Pb, Zn, Cu, Ni, Cd, N, P, K,. and nitrate. I 12. Maintain a recorded log of sludge applications, including amouni ts applied, dates, method of application, field(s) used for applica- tion, and loading rates for nutrients, and metals. Maintain a j record of soil and hay tissue analyses, lime application, and hay production. 7.0 SUMMARY AND RECOMMENDATIONS: Four (4) sites consisting of approximately 115 acres in pasture arel available for land application of sludge generated at the Huffman Finishing i Company Wastewater Treatment plant. The soils at the sites are suitable for land application of aerobically digested (stabilized) liquid and dewatered sludge on an agronomic basis. Considering the properties of the soils at the sites, the land application of sludge could be beneficial to the site's and hay management in terms of improved tilth, water holding capacity, CEC i of soil, nutrients, and trace elements availability for cover crops from the sludge. This report should be submitted to the North Carolina Division of Environmental Management in the aerobically digested liquid and dewatered sludge by land application on an agronomic basis. Al 77 . Oak Gmve INN \ rox�—�c �`\" � `fir �� •.1. V`�; `� ill ^'1 �1 �� I'\� �� n �.._/• ^ : \7)\ ii`)P' j!/:.: /I U 1 J4, : 1 9 1 S(Sl\ )1 ,i� \ �(T \ \ °Ob% � i1;=+"�' ;!5.=�=::✓i�;�%,'./`• !i 1�:?fi;l \!'` '\ �S%'•;1C�J 1\ \ c �! V X WAND A4GEX poKtj&. EXHIBIT 1 LOCATION AND TOPOGRAPHIC MAP SITE NO. 1 SCALE: 1" = 2000' I; ON .fin r//! °zV< 11 rll`/ 7j(__•�z. -� r��l�i - �) t•7 '' ��� /ll ,- 1 � �^�\\ ��.. �\� !\� ""8 �, J)�f�IJ :�' `•�l.\!%��o'�%%'��16i .-`:.i. •.. \�� ( ..�� `( I\.1J�_�.. �\,\`/,�`}�}�J.11 '•�/.`)>'�� .fl61 JCreek I 47'30" 1 Q)) 11 �' •V' 11 oa /lll - Gun'powd r _I) _ -1h / I'I ����' ��,�\/ �✓/ ,j dr 'n' 1'`,I O � %�11 i / 'll r^) I�\ \\I}�� 1�1},I I �1`` I' , �� ��� 3 (%., ��'1�"•�'% \ ui (Ir. 1,i `1}h 1 I',� leii r, �L,I i I' \.. �1 `/ r/� 1♦\\ �� _ ( n /1•\t\./ •i '' .-Rad1- 1( \ `c�� I).'(� ;; /��^�yJ7 �. �(I+• �1• ,♦Ilia \�• d'i N Ci.9 �`��`.-!�\_. \\ n, /�I ►� frf '/r) Ir � / `� 5 Pt``•.`�r'% l 1/,`I��. (�� 11} J�,$/, �/ II 1 I ./.�• r. w r ry •rn Crave I,� �/.:`��i\ r'� AEI .9\,`�JC Imo\ j`( '� ((a _ �• f/. 1�1, �i / Rea !(�� ll� �11` 1 � �� ' r /(''/ 1/�lll 1h �.\� .; ��ti /' ll��li�rr �i ♦\�' "I'� 11 �`f\� / (', �� \air � / ' I , 1_L � h �. l'F' i ( .r7� �2. 12 T / '�� � \ •l \. 0 r}'.. .. �:,c-�� � li, s I, �1'.. rr� !�\I. �I.c •I \•�/� ��./J1": 4i11 ilai/ �' •�i'I i 1:.• - 11 � AMO II �• ��ri , 1 '. ilk � f � / . Lrl/, e(I � �� i� iVI ills ♦ '� ( \) �}i 1 a�� p,_ R,., Ir .v - � .,o `/(',�-I/�� / `fi•-I µono \V�,)` `I 9`�/�. iiJl �I(( r(� (,1 t ��n. `\�I �l L o'1 9% `.. \\`l l" YJ/ 1 � k"orhCvnitH[ ��,. __ 1�. �. " ld+ ( � �((_ )) �" 1 i11', 1 �`�� `- -w1� j1 �(-, it � 1 •`� 1� � . ��` 1n ✓ — '1 m 9 1 � . , � M ( � .. \1 \ y( ll)rl `�1I\ i.�'� \, �I1r1'� / Q HOIRY hw ,'i�\ • � �/IimJ r- � )m �/ '!/ �.I -_-1(1.`� ��-C ELL�,� ��2 � (+) � � „a / � � l \./ •-� � /�,• , �. } / � 1 (�� 'S� BURKE CO 1 �'. '4E / Ira: ! ♦ / \�.: r.���i6 1 (i � '\ J�%� 9 4 `�_ � " n¢ ,. /11_\.:��� n•i,r (• �' _- . r%,�IIG�e(e } '�lir-�'. � �� \'1�'•,/;rr^. �1;1 __ � ,�I� I��;, � K 14AND A4G61Z 50moL- SCALE: 111 = 2000, EXHIBIT 2 LOCATION AND TOPOGRAPHIC MAP SITE NO. 2, 3, & 4 - 13 - m I 1! • Sfi Vi) - L3 ii- / 1.0 lty X ti 'T Of I 1� I � APPENDIX I. Dr. Rubin's Site Investigation Report 2. Agreement Letters 3. Sludge Analysis and EP Toxicity Test Results Site Investigation For Huffman Knitting Mills Caldwell County, North Carolina The Huffman Knitting facility is located near Granite Falls, North Carolina. The Huffman facility is a textile knit and finishing plant whe�e athletic socks are manufactured. The wastewater treatment operation at this plant is being upgraded and one important step in the upgrade is to develop a sludge management plan. One option available to the management of this textile operation is to land treat the material and utilize the nutrient and hydraulic component of, the waste stream for agricultural or silvicultural production. Prior to application of any waste to land, tests must be accomplished to determine the i nutrient content of the material and to determine whether the material is toxic or hazardous. No material which is toxic or hazardous can be applied I to agricultural lands in North Carolina. The test data generated at Huffman Mills indicates that the waste textile plant sludge is both non -toxic and non- hazardous and does contain low levels of essential plant nutrients and meths. Prior to application of waste sludge to land, a thorough site and soil analysis, a vegetation establishment and management plan, and an overall sijte management plan must be developed and submitted to the state regulatory agencies for their approval. Once the plans have been approved, then a permit I for the land application operation will be issued. There are two purposes to the brief report which follows. The first is to describe conditions encountered on the proposed waste receiver sites. The second is to make recommendations regarding appropriate hydraulic and constituent loadings onto these sites. i -2- Site Evaluation - Topography and Location Several potential waste treatment sites were evaluated as potential Ireas to receive the waste sludge from the Huffman Mills Wastewater Treatment Plant operation. These are listed as: Site 1 - Bumgardner Property Site 2 - Huffman Property Site 3 - Site 4 - Site 1 - Bumeardner Property: Several well defined fields were evident on the Bumgardner site. These fields were designed by fence rows separating the pastures on this property. Portions of the northern most field do appear to be too close to existing offsite dwellings to be utilized as potential receiver sites for waste sludge. This entire northern most field was excluded for consideration because of the proximity of this home. The remaining fields are typical of the foothill region of the state. Slope ranged from gently sloping along the ridge lines to moderately steep along the side slope positions. Site 2 - Huffman ProuertV The large acreage tract located immediately adjacent to The Huffman Knitting Mill Facility is also somewhat atypical for the Piedmont and Foot i Hill region of the state. Slope over this site ranged from nearly level tola maximum of approximately 4 or 5 percent. There is one residence located I immediately east of the existing field and a 400-foot buffer must be provided I between this facility and this residential dwelling. Other than this minor site limitation, topograhy on the Huffman site is ideal for operation of a I land treatment program. There were no well defined drainage ways or channels 3- coursing through the property. Site erosion appears to be maintained at a very low level. Site 3 - Topography on this large acreage tract is typical of the Piedmont and Foot Hill Region of the state. Slope ranges from as little as 4 or 5 percent I along the ridge line and uppermost elevations of the site to as much as 15 percent along the steeper sloping side slope positions. The site is I characteristically a hog -back and application of waste on the uppermost portions of the site will not be topographically limited. Applications of waste on the steeper sloping side slope positions will be more critical anld extreme caution must be taken to insure no runoff occurs. There appear tobe no well defined drainage ways on this property and soil erosion appears to, have been maintained at a minimum. The land has recently been cut for timber and some vegetative stabilization will be essential prior to application of any waste sludge onto this parcel. Site 4 - This large acreage tract consists of several small fields located immediately adjacent to Gun Powder Creek. Portions of these fields drain directly into Gun Powder Creek. Other portions of this large acreage tractl appear to drain in a westerly direction and application of liquid sludge oni to the more gentle portions of those pastures which drain in a westerly direction or which face in a westerly direction could easily be allowed and will provide valuable nutrients and liquid to this pasture land. There are some terraces which have been cut across the largest of the pastures and this will i facilitate retention of liquid sludge onsite and minimize soil loss and s-M erosion. The topography on the last of the sites evaluated does appear tl be very well suited for this land application program. i In general the topography on all sites ranges from moderately acceptable to very well suited for operation of this land application program. Portions of Site 3 do contain the most serious of the topographic limitations. Those portions of Site 3 where the slope exceeds 12 percent will require injection of sludge. Those portions of Site 1 where the slope exceeds 12 percent will i also require injection of sludge. The remaining portions of each field can very well accept liquid sludge with surface application. Topography will not significantly reduce the suitability of the sites evaluated. Topography it I essential to provide a gradient along which constituents applied to each site I will move. With careful operation of these facilities, topography can be used to facilitate treatment and management of sludge and portions of all siteslcan easily serve as receivers for the waste. Soils The soils information necessary to develop design criteria for a lands i based waste treatment system must address both agronomic and engineering properties of the soil material encountered on a site. These properties can be evaluated on a preliminary basis by examining published literature such �s that contained in the modern soil survey of Caldwell County. In addition, hand auger borings must be advanced on each of the potential waste receiver) sites to confirm the soil mapping units. Further, 1-inch diameter soil core samples must be collected from each site to determine optimum fertility levels on each site. In support of this evaluation, hand 'auger borings were advanced at representative locations on each site and the soil material extracted with the -5- I hand auger was evaluated with increasing depth for selected properties. Those properties are all important in both design and operation of a land based, waste treatment system. The properties evaluated in the field include: depth, color, texture, structure, and consistence. Each of these factorslis used to characterize or describe a representative soil profile description. The soil maps prepared by the Soil Conservation Service indicate that thelsoil i material encountered on the sites proposed for the Huffman Mills wastewater treatment operation consists primarily of Cecil soils. These soil mapping units are present on each of the potential waste receiver sites. A characteristic or representative soil profile description would indicate that the soil material consists of a sandy loam topsoil to a depth of between 61and 12 inches. Underlying this was a characteristic red clay subsoil which extended to a depth of over 48 inches. The auger borings were advanced tola depth of at least 72 inches. Saprolitic material was encountered in some borings from 48 inches to 72 inches and in other borings saprolitic material was encountered of between the 60-inch and 72-inch depth. Soil physical properties are ideally suited for operation of a land treatment program. The sandy loam topsoil will allow rapid incorporation of waste constituents whine the heavier textured clay subsoil will provide numerous sites on which nutrients will adsorb and later be available for plant uptake. I The 1-inch diameter soil core samples were collected and composited from each site. These samples were analyzed to determine the soil pH and exchange capacity of the material onsite. In general both pH and exchange capacity are low. This will require maintenance of the lowest allowable metal loadings I currently permitted by the U.S. Environmental Protection Agency. The low soil pH must be adjusted upwards by the addition of lime. Either calcitic or M I dolomitic lime could be applied to the site. The liming recommendations will be discussed subsequently in the section on recommendations. i In general the soil material encountered on each of the sites is very well suited as a receiver soil for waste. There was no evidence of a seasonal high water table encountered on any of the sites. The primary soil limitation I is the low pH and this can easily be overcome by application of agricultural I lime. These soils can accept moderate hydraulic loadings. The maximum recommended hydraulic load should be maintained at approximately 10,000 gallons per acre per application event and application events should be limited to 4 or 5 times per year per acre. This will limit the maximum allowable hydraulic loading to 50,000 gallons per acre per year. This hydraulic loading is consistent with the characteristics of the soil material encountered on the site. It does not appear, however, that the hydraulic !load will be a serious limitation based on the nutrient content of this sludge.I With careful operation and attention to soil sampling, the sites proposed for inclusion in this program will last for many years as receiver sites for sludge. The soil sampling and vegetation analysis required to best manage I the soil/plant system must be accomplished annually to optimize the land treatment program proposed for The Huffman Knitting Mills. Recommendations Several samples of sludge were collected from The Huffman Knitting Mill facility and evaluated by various laboratories. The results of these analyses are reasonably consistent. The analyses indicate that the most limiting of! the constituents contained in the sludge is the phosphorus level. Reasonably high phosphorus levels were noted in the'waste sludge. Maximum recommended agricultural load for phosphorus based on the soil test program is 120 pounds ! -7- per acre per year. This does not allow for any potential storage for phosphorus in the soil and phosphorus adsorption potential was ignored in determining this loading. The phosphorus requirement will be reduced slightly with time so soil sampling is essential to best manage this land treatment facility. The land area required to assimilate the phosphorus contained in the sludge is approximately 25 acres. The soil sampling program indicates that there is also a deficiency of potassium on several of the sites and a moderate potassium level on only the Bumgardner site (Site 1). The phosphorus recommendation of 120 pounds per acre per year was required on each site evaluated. Further, nitrogen requirements on each site ranged from 150 to 180 pounds per acre per year. The most limiting of the constituents in the sludge, however, is phosphorus. Subsequent sludge sampling is essential to determine the accurate level of phosphorus in the sludge and to tailor the waste loadings based on these analyses. The North Carolina Department of Agriculture will analyze sludge samples for a reasonable fee and provide valuable information which can be used to tailor this land application program to the specific needs of each site. Soil sampling indicates that pH in the soil on each site is moderate to low. Soil pH on the Bumgardner site was the highest encountered while soil pH on Site 3 and Site 4 was the lowest. Soil pH on the Huffman site was at a moderate level will require elevation if that site is enrolled in this program. A minimum application of between .5 tons per acre on Site 1 to 1.5 tons per acre on Sites 3 and 4 will be required to optimize pH in each field. Application of approximately 1.5 tons of lime per acre per year will be necessary to insure optimum pH on each of the fields evaluated. The liming material should be applied either late in the fall or early in the spring. S:9 Waste can be applied to the site when the soil conditions are trafficable. Should the waste application vehicle create a rut greater than 2 or 3 inches in depth, then soil conditions do not permit access to the field and the waste application event must cease. Frequent (monthly) waste analysis performed by the North Carolina Department of Agriculture would be very valuable to insure the success of this program. Annual soil sampling is essential to insure waste constituents are applied at a rate appropriate to each waste receiver site. Vegetation should be sampled several times during the growing season to insure that waste constituents are not accumulating in the soil or vegetation and that waste application events are providing the nutrients necessary for the growing plants. Supplemental fertilizers may be necessary to optimize fertility levels in the soil and produce crops which are valuable to the land owners. With careful operation and attention to the sampling and monitoring program and with careful record keeping, the sites evaluated should serve for many years as receiver sites for sludge generated by Huffman Mills. Neither the characteristics of the waste, the soil, or the site will significantly limit the potential of either site to treat and receive waste from this facility: Conclusion The four sites evaluated as potential sites for Huffman Mills each appear reasonably well suited as receiver sites for the waste sludge from this textile finishing operation. Some topographic limitations do exist on portions of the fields evaluated and these limitations can be easily corrected with a flagging program to preclude application of waste in these areas. With careful operation, attention to sampling'and monitoring, and meticulous record keeping, the sites proposed as receiver sites should last for many years for the sludge generated at the Huffman facility. R78/D7a/ARR:sb Site 1 Grace Chapel Road, Bumgardner Site Caldwell County, North Carolina 0 - 8" light brown loamy sand; granular structure; friable to loose; many fine roots. 8 - 16 light gray brown loamy sand; lots of roots; granular structure; friable. 16 - 24" reddish brown clay loam; weak, medium, subangular blocky structure; few roots;, few mica flakes; few fine roots. 24 - 36" red clay, clay loam; weak, fine, subangular blocky structure; clay films on ped faces, few roots; few fine mica flakes. 36 - 40" red sandy clay loam and saprolite; weak, fine, subangular blocky structure; firm, slightly sticky slightly plastic; few roots, few clay films on ped faces; few mica flakes. 40" boring terminated with no evidence of seasonal high water table. The field is approximately 3 acres in size, long and narrow; slope is about 5 percent. Site 2 Huffman Site, Highway 321 0 - 6" dark brown loamy sandy; granular structure; many fine and medium roots. 6 10" light tan to light brown sandy loam; weak granular structure. 10 - 12" red clay loam; weak, fine, subangular blocky structure; few roots; few mica flakes; few quartz flakes and clay' films on ped faces. 12 - 36" red clay loam; weak, fine, subangular blocky structure; few roots; little more mica flakes; few quartz flakes and clay films on ped faces. 36 - 38" red clay loam and saprolite; few fine mica flakes. 38" boring terminated with no evidence of seasonal high water table. Site 3 Miller Site, Highway 321A 0 - 4" brown sandy loam; granular structure; friable; many fine roots. 4 - 10" light brown sandy loam; granular structure; friable; many fine roots. 10 - 24" red clay; weak, fine, subangular blocky structure; firm; slightly sticky and slightly plastic; few mica flakes. 24 - 30" red clay; weak, fine, subangular blocky structure; firm; slightly sticky and slightly plastic; many mica flakes; few roots and numerous quartz fragments. 30 - 36" coarse saprolite. 36" boring terminated. The topography on Field 3 is about 15% on the toe, and about 8 to 10% at the uppermost elevations on the site. Site 4 Wrinkler Site, West of Highway 321 0 - 6" dark brown loam sandy; y; granular structure; many fine and medium roots. 6 10" light tan to light brown sandy loam; weak granular structure. 10 - 12" red clay loam; weak, fine, subangular blocky structure; few roots; few mica flakes; few quartz..flakes and clay films on ped faces. 12 - 36" red clay loam; weak, fine, subangular blocky structure; few roots; little more mica flakes; few quartz flakes and clay films on ped faces. 36 - 38" red clay loam and saprolite; few fine mica flakes. 38" boring terminated with no evidence of seasonal high water table. Soil Test Results. Huffman (PPM or Std Units) Site PH C.E.C. K P 0_M 1 5.8 4.4 48 84 .4 2 5.7 4.8 60 80 .4 3 4.9 4.2 42 58 .2 4 5.2 5.1 72 87 .3 Recommendations (No/ac) N P K lime Site (lb/ac) (lb/ac) (lb/ac) (T/A) 1 180-200 20-40 50-70 .5 2 180-200 40-60 40-60 .6 3 180-200 120-140 50-70 1.3 4 180-200 20-40 50-70 1.0 I N.C. DIVISION OF ENVIRONMENTAL MANAGEMENT STANDARD AGREEMENT FOR THE LAND APPLICATION OF WASTE SLUDGE ON PRIVATE LAND NAME OF WWTP: Huf LOCATION OF WWTP: H OWNER OF WWTP: Hu TYPE OF SLUDGE: AE FARM NAME OR NUMBER: FIELD NUMBERS: LOCATION OF LAND: S Finishi OWNER OF PROPERTY: John Frank•Miller LESSEE OF PROPERTY: LAND USE OR CROPPING PATTERNS: Pasture INTENDED USE OR DISPOSITION OF CROPS: Ha The undersigned landowner or his representative hereby permits the Huffman Finishing Company hereinafter referred to as the Permittee, to apply . sludge from the Huffman Finishing Company's WASTEWATER TREATMENT PLANT upon the land at the location shown as described in the attached documents in accordance with the restrictions and stipulations shown below. The Landowner or his Representative receives, in consideration, full use of the nutrient value of the applied sludge while the Permittee receives, in consideration, the full use of the land described above for the disposal of digested sludge. The undersigned Land Owner or his Representative and Permittee agree to abide with the following stipulations and restrictions until such time as written notification given ninety (90) days in advance, modifies or cancels this agreement. STIPULATIONS: 1. The landowner or his representative hereby authorizes the Permittee, County and State Officials or their representatives to inspect each parcel of property prior to, during, and after sludge application and to establish monitoring facilities on or near the application -site as required by the sludge disposal permit. - 1 - SLUDGE APPLICATION AGREEMENT 2. The Landowner or his Representative authorizes the Permittee, County and State officials or their representatives to take necessary soil, surface and ground water samples during the term of the twelve (12) months after termination of this Agreement. 3. The Permittee will provide each Landowner or his Representative with a Copy of the land application permit as issued by the N.C. Department Of Natural Resources and Community Development (NCNRCO), Division of Environmenal Management (OEM) for the land described above prior to com- maximumnapplication rates,alimitationst of sluge applictio. The l,Cand-ottherNRC-DEMprestrictionseprescribed by the laws and regulations. 4. The Permittee has provided the Landowner or his Representative with information and data concerning the program for land application of sludge to privately owned lands which includes an analysis of constituents of the sludge, sludge application methods and schedules for typical cropping pattern and, a description of the equipment used by the Permittee for sludge application. 5. The Permittee will furnish each Landowner or his Representative with a copy of the laboratory analysis stating constituents of the sludge applied to the property. 6. The Permittee will furnish each Landowner or his Representative with a copy o the results of each soil analysis. 7. The Landowner or his Representative will inform the Permittee of any changes in the intended use and/or cropping patterns of the permitted land at least ninety (90) days perior to each application of sludge. With- in the limits of the NCNRCD-DEM permit, the Landowner or his Representative and the Permittee will determine sludge application rates based on crop patterns and results of soil samples. 8. No crops for human consumption shall be raised on the land receiving sludge application. Root crops and leafy vegetaoles can be grown only after a period of twelve (12) months from the last date of sludge application. 9. The Landowner or his Representative or successors shall adhere to the provisions of this Agreement for a period of twelve (12) months from the date of the most recent sludge application. 10. The Permittee will exercise all reasonable care and precautins o in the execution of this Agreement. The Permittee will not be held liable for any damages to the property or persons in the execution of this Agreement unless due directly to negligence on behalf of the Permittee. z - 2 - SLUDGE APPLICATION AGREEMENT 11. Should the Landowner or his Representative lease or otherwise Permit the use of the land by a third party the Landowner shall be responsible to insure the third party agrees and complies with the terms and conditions of this Agreement. 12. The existing Lessee, if any, of the site agreec., by execution of this Agreement, to comply with all provisions of this Agreement. 13. In consideration of the signing of this Agrccii,,nt, Inc ,sties thereof for themselves, their agents, officials, employees ano servants agree not to discriminate in any manner on the basis of race, color, creed or national origin with reference to the subject matter of this Agreement. no matter how remote. 14. The land application disposal sites shall not be yratea upon by any animals whose products (including their meat) is consumed by humans for a period of thirty (30) days or until rainfall equaling one inch (111) occurs after the last application of sludge. 15. The Landowner or Lessee will provide access onto all fields which will be used for the land application of sludge. 16. In any future transfer of the land where sludge has been applied, a notice shall be given to the new landowner that gives full details as to the constituents and amounts of the sludge that was applied or incorporated at this site. Date Date 9-S-s9 Date - 3 - XWAN ANN,ER's Signature LESSEE's Signature CO PANY's ;OEC SENTATIVE SLUDGE APPLICATION AGREEMENT STATE OF NORTH CAROLINA COUNTY OF I' - U k a '` � "- the undersigned Notary Public, do hereby certify that Chn` PraH(( A,(� r personally appeared before me this day and acknowledged the due execution of the foregoing instrument on Sludge Disposal. WITNESS MY HAND and notarial seal this S _ day of f4AP. 198q MY COMMISSION EXPIRES: - 4 - N.C. DIVISION OF ENVIRONMENTAL MANAGEMENT STANDARD AGREEMENT FOR THE LAND APPLICATION OF WASTE SLUDGE ON PRIVATE LAND NAME OF WWTP: LOCATION OF WWTP: OWNER OF WWTP: TYPE OF SLUDGE: Huffman Finishing Company Aerobically digested sludge FARM NAME OR NUMBER: FIELD NUMBERS: LOCATION OF LAND: OWNER OF PROPERTY: Ricky L. Vinkler LESSEE OF PROPERTY: LAND USE OR CROPPING PATTERNS: Pasture INTENDED USE OR DISPOSITION OF CROPS: Hay / The undersigned landowner or his representative hereby permits the Huffman Finishing Company hereinafter referred to as the Permittee, to apply sludge from the Huffman Finishing Company's WASTEWATER TREATMENT PLANT upon the land at the location Shownown ass described in the attached documents in accordance with the restrictions and stipulations shown below. The - Landowner or his Representative receives, in consideration, full use of the nutrient value of the applied sludge while the Permittee receives, in consideration, the full use of the land described above for the disposal of digested sludge. The undersigned Land Owner or his Representative and Permittee agree to abide with the following stipulations and restrictions until such time as written notification given ninety (90) days in advance, modifies or cancels this agreement. STIPULATIONS: 1. The landowner or his representative hereby authorizes the Permittee, County and State Officials or their representatives to inspect each parcel of property prior to, during, and after sludge application and to establish monitoring facilities an or near the application -site as required by the sludge disposal permit. - 1 - SLUDGE APPLICATION AGREEMENT 2- er orhe dow County andTStatenofficials orstheirerepresentatives rtoetakeenecessaryesail , surface and ground water samples during the term of the twelve (12) months after termination of this Agreement. 3. The Permittee will provide each Landowner or his Representative with a Copy of the land application permit as issued by the N.C. Department of Natural Resources and Community Development (NCNRCD), Division of Environmenal Management (OEM) for the land described above prior to com- mencement of sludge application. The NCNRCD-DEM permit will delineate maximum application rates, limitations, and other restrictions prescribed by the laws and regulations. 4. The Permittee has provided the Landowner or his Representative with information and data concerning the program for land application of sludge to privately owned lands which includes an analysis of constituents of the sludge, sludge application methods and schedules for typical cropping pattern and, a description of the equipment used by the Permittee for sludge application. 5. The Permittee will furnish each Landowner or his Representative with a copy of the laboratory analysis stating constituents of the sludge applied to the property. 6. The Permittee will furnish each Landowner or his Representative with a copy o the results of each soil analysis. 7. The Landowner or his Representative will inform the Permittee of any changes in the intended use and/or cropping patterns of the permitted land at least ninety (90) days perior to each application of sludge. With- in the limits of the NCNRCD-DEM permit, the Landowner or his Representative and the Permittee will determine sludge application rates based on crop Patterns and results of soil samples. 8. No crops for human consumption shall be raised on the land receiving sludge application. Root crops and leafy vegetables can be grown application. only after a period of twelve (12) months from the last date or sludge 9. The Landowner or his Representative or successors shall adhere to the provisions of this Agreement for a period of twelve (12) months from the date of the most recent sludge application. 10. The Permittee will exercise all reasonable care and precautions in the execution of this Agreement. The Permittee will not be held liable for any damages to the property or persons in the execution of this Agreement unless due directly to negligence on behalf of the Permittee. - 2 - SLUDGE APPLICATION AGREEMENT 11. Should the Landowner or his Representative lease or otherwise permit the use of the land by a third party the Landowner shall be responsible to insure the third party agrees and complies with the terms and conditions of this Agreement. 12. The existing Lessee, if any, of the site agree, by execution of this Agreement, to comply with all provisions of this Agreement. 13. In consideration of the signing of this Agreement, ; arties thereof for themselves, their agents, officials, employees and servants agree not to discriminate in any manner on the basis of race, color, creed or national origin with reference to the subject matter of this Agreement, no matter how remote. 14. The land application disposal sites shall not as yrcLeo upon by any animals whose products (including their meat) is consumed by humans for a period of thirty (30) days or until rainfall equaling one inch (111) occurs after the last application of sludge. 15. The Landowner or Lessee will provide access onto all fields which will be used for the land application of sludge. 16. In any future transfer of the land where sludge has been applied, a notice shall be given to the new landowner that gives full details as to the constituents and amounts of the sludge that was applied or incorporated at this site. 9-6- T9 Date Date q-(9-29 Date LANDOWNE 's SianatLre LESSEE's Signature a CO PANY'S REPRESENTATIVE - 3 - SLUDGE APPLICATION AGREEMENT STATE OF NORTH CAROLINA COUNTY OF the undersigned Notary Public, do hereby certify that ick personally appeared before me U this day and acknowledged the due execution of the foregoing instrument on Sludge Disposal. WITNESS MY HAND and notarial seal this — - day of 198 MY COMMISSION EXPIRES: 4-19 -qO ROTA Y FpdBLIC - 4 - N.C. DIVISION OF ENVIRONMENTAL MANAGEMENT STANDARD AGREEMENT FOR THE LAND APPLICATION OF WASTE SLUDGE ON PRIVATE LAND NAME OF WWTP: LOCATION OF WWTP: OWNER OF WWTP: Huffman Finishing Company TYPE OF SLUDGE: Aerobically Digested Sludge FARM NAME OR NUMBER: FIELD NUMBERS: LOCATION OF LAND: See Location OWNER OF PROPERTY: J.P. LESSEE OF PROPERTY: LAND USE OR CROPPING PATTERNS: Pasture INTENDED USE OR DISPOSITION OF CROPS: Hay The undersigned landowner or his representative hereby permits the Huffman Finishing Company hereinafter referred to as the Permittee, to --apply sludge from the Huffman Finishing fmm�'nv WASTEWATER TREATMENT PLANT upon the land at the location shown as described in the attached documents in accordance with the restrictions and stipulations shown below. The Landowner or his Representative receives, in consideration, full use of'the nutrient value of the applied sludge while the Permittee receives, in consideration, the full use of the land described above for the disposal of digested sludge. The undersigned Land Owner or his Representative and Permittee agree to abide with the following stipulations and restrictions until such time aS written notification given ninety (90) days in advance;, modifies or cancels this agreement. STIPULATIONS: III Permittee, County and State Officials or their representativI. The landowner or his representative hereby authorizes the li es to inspect) each parcel of property prior to, during, and after sludge application and to establish monitoring facilities on or near the application site as 1' required by the Sludge disposal permit. - 1 - SLUDGE APPLICATION AGREEMENT 2. The Landowner or his Representative authorizes the Permittee, County and State officials or their representatives to take necessary sail, surface and ground water samples during the term of the twelve (12) months after termination of this Agreement. 3. The Permittee will provide each Landowner or his Representative with a copy of the land application permit as issued by the N.C. Department of Natural Resources and Community Development (NCNRCO), Division of Environmenal Management (OEM) for the land described above prior to com- mencement of sludge application. The NCNRCO-DEM permit will delineate maximum application rates, limitations, and other restrictions prescribed by the laws and regulations. 4. The Permittee has provided the Landowner or his Representative with information and data concerning the program for land application of sludge to privately owned lands which includes an analysis of constituents of the sludge, sludge application methods and schedules for typical cropping pattern and, a description of the equipment used by the Permittee for sludge application. 5. The Permittee will furnish each Landowner or his Representative with a copy of the laboratory analysis stating constituents of the sludge applied to the property. 6. The Permittee will furnish each Landowner or his Representative with a copy o the results of each soil analysis. 7. The Landowner or his Representative will inform the Permittee of any changes in the intended use and/or cropping patterns of the permitted land at least ninety (90) days perior to each application of sludge. With- in the limits of the NCNRCD-DEM permit, the Landowner or his Representative and the Permittee will determine sludge application rates based on crop patterns and results of soil samples. 8. No crops for human consumption shall be raised on the land receiving sludge application. Root crops and leafy vegetaoles can be grown only after a period of twelve (12) months from the last date of sludge application. 9. The Landowner or his Representative or successors shall adhere to the provisions of this Agreement for a period of twelve (12) months from�the date of the most recent sludge application. 10. The Permittee will exercise all reasonable care and precautions in the execution of this Agreement. The Permittee will not be held liable; for any damages to the property or persons in the execution of this I. Agreement unless due directly to negligence on behalf of the Permittee. I� - 2 - SLUDGE APPLICATION AGREEMENT 11. Should the Landowner or his Representative lease or otherwise Permit the use of the land by a third party the Landowner shall be responsible to insure the third party agrees and complies with the terms and conditions of this Agreement. 12. The existing Lessee, if any, of the site agrees, by execution of this Agreement, to comply with all provisions of this Agreement. 13. In consideration of the signing of this Agreei„cnt, tnu arties thereof for themselves, their agents, officials, employees and servants agree not to discriminate in any manner on the basis of race, color, creed or national origin with reference to the subject matter of this Agreement, no matter how remote. 14. The land application disposal sites shall not be yrateo upon by any animals whose products (including their meat) is consumed by numans for a period of thirty (30) days or until rainfall equaling one inch (111) occurs after the last application of sludge. 15. The Landowner or Lessee will provide access onto all fields which will be used for the land application of sludge. 16. In any future transfer of the land where sludge has been applied, a notice shall be given to the new landowner that gives full details as to the constituents and amounts of the sludge that was applied or incorporated at this site. i Date ANDOWNER's Signatu� I, Date Date LESSEE', Sinnar:.,. 11 - 3 - SLUDGE APPLICATION AGREEMENT STATE OF NORTH CAROLINA COUNTY OF I, _ k) rthe undersigned Notary Public, do hereby certify that �� �ctryigQrher personally appeared before me this day and acknowledged the due execution of the foregoing instrument on Sludge Disposal. WITNESS MY HAND and notarial seal this � ' day or 1d�;�vGf�at. 198 MY COMMISSION EXPIRES: i NOT BLIC 0 - 4 - WL11(tC!' C1l�Cr -ler " c ` r I� P.O Box tbC29 Ashevliie. North Carou�•28�11��— a it11 Inn cc 04;254.5 1 69 -liens: Huffman Finishing -Sludge -,ate Received: 1-5-89 Date Analyzed: 1-5 to 1-29-89 -ertified By: Dr. Fred Holtkamo RESULTS MG/L MG/KG Arsenic 0.60 Cadmium 10.9 0.15 2.73 Calcium 1650.0 Lead 30.000.0 0.30 5.45 Mercury 0.017 Mangnesium 0.31 300.0 5455.0 Copper 3.0 54.5 Nickel 0.41 7.45 Zinc 20.0 364.0 Sodium 1200.0 21,818.0 Nitrate 4.50 pH 81.8 6.5 Potassium 500.0 Percent Solids 9091.0 5.50, T. Phosonorus 7250.0 TKN 131,818.0 1772.0 32,218.0 Ammonia Nitrogen 176.0 '3182.0 -omolete wastewater treatment Services • Consulting • Start-uos • Ooeration • Maintenance • Momtonna • Aeoorttng State Car tried Laboratory . Charter Member Commercial Laboratories Assnciwr v,n ,.. m n roW@tAtcU�U@lrcer 0mf, II :___..L P.O. Box 18029 . Asheville, North Carolina 28814-0029 • 704/ 169, JUN 1 9 ?989 c June 13, _.,:.,._-, G t., A' Huffman Finishing Company Results of analysis of your wastewater treatment plant are listed below. j 1 I 2 3 4 sludge I Down 1 Parameters Units Upstream! Influent) ISt N&XX stream i Dissolved Solids mQ/I ! ! I flaTo Cam nice Total Nitrogen ! mgll 1 Collected: 6-7-89 j Date Received: 6-9-89 Volitile Suspended Residue j mg/1 ! j Volitile Total Residue mq/1 I pH Units Date Sample Analyzed Setteable Solids m1/I 1 m /I 8 6-9-89 Guv I moll Date Reported 6-13-89 Fecal Coliform I o L1100 ml Total Residue m /I Total Suspended Residue moll j Certified by Total Kieldahl Nitrogen mg/I j Ammonia Nitrogen m /I Oil & Grease m ll ! I i Comments J ! Turbidity! NTU M.B.A.S. (Detergents) Mgt( Nitrate mg/ I 1 Nitrate -Nitrite mg/ I Total Phos horns I m /I 1725.0 Phenol ug/I Cyanide mg/I f you have any questions, or if we can be of further,service, please let us know. I Complete Wastewater Treatment services • Consulti,o . Start-ups • operation . Maintannnrn . U....n...i.,,.. oe......,.... state uerimep Laboratory • Charter Member Commercial Laboratories Association of N.C. - - I I Chemical & Environmental Technology, Inc. 1 L ENVIRONMENTAL LABORATORY SERVICES JOHN M. OGLE PRESIDENT P. O. BOX 12298 RESEARCH TRIANGLE PARK. N. C. 27709 f_. PHONE (919) 467-3090 FAX (919) 467-3515 M.R. SHAN}:AR MISTRY THE WOOTEN COMPANY 120 N. BOYLAN AVE. RALEIGH, NC 27603 RE: HUFFMAN ;'INISHING SAMPLE HISTORY CLIENT ID CET SAMPLE DATE RECEIVED SLUDGE 26580 6-16-89 ANALYTICAL RESULTS-1 PARAMETER METHOD-2 PHOSPHORUS, TOTAL 365.3 PERCENT SOLIDS ----- JULY 7, 1989 DATE ANALYZED? 6-24-89 TO 7-04-69 SLUDGE " 54400 8.4 1 - ALL RESULT UNITS ARE EXPRESSED IN MG/KG, DRY WEIGHT, EXCEPT PERCE14T SOLIDS...............PERCENTAGE 2 - FEDERAL REGISTER, VOL 49, NO. 209, OCTOBER 26, 1984 CHEMICAL & ENVIRONMENTAL TE TERRIE LITZENBERGER ASSISTANT LABORATORY MANAGER THL/bws SDWA PESTICIDES / HERBICIDES IEA Sample Number: 344-126-1 Sample Identification: Huffman Date Extracted: 1/19/89 Date Analyzed: 1/26/89 Number Compound Pesticides: 1 Endrin By: K. Hinshaw Water Quantitation Results Limit Concentration ux/L u8/L 2 Lindane 0.0002 BQL 3 Methoxychlor 0.0002 BQL 4 Toxaphene 0.001 BQL 0.005 BQL Herbicides: 1 2,4-D 2 2,4,5-TP 0.01 BQL 0.002 BQL Comments: BQL = Below Ouantitation Limit EP-TOX Analysis Comments BELOW QUANTITATION LI N/R - NOT REACTIVE Reactivity IEA SaM*Ia IN_ 344026 1 S2006 Ideatificatiaa Huffman Date heal" Janueru t 9 1989 Bq Lloyd Number Compound Results I pH 2 Reactivity toward water 6.1 N/R 3 Sulfide Reactivity <20 m9 /L 4 Cyanide Reactivity 5 - <1.0 m/L 9 Explosive Nature 6 Overall ReactivityN/R N/R IEA LABORATORY RESULTS IEA Project ll: 344-126 Client Name: Wastewater Services Sample # Client ID Parameter 1 1 Huffman Corrosivity 1 Huffman Huffman Silver - EP TOX 1 Huffman Arsenic - EP TOX 1 Huffman Barium - EP TOX 1 Huffman Cadmium - EP TOX 1 Huffman Chromium -EP TOX 1 Huffman Mercury - EP TOX 1 Huffman Lead - EP TOX 1 Huffman Selenium - EP TOX -. t*axba Ignitability 1 * 2- Huffman �a Total Aroclors Date Results <6.35 mmpy 1/25/89 <0.05 mg/L 1/24/89 0.035 mg/L 1/24/89 <0.10 mg/L 1/24/89 <0.01 mg/L 1/24/89 <0.03 mg/L 1/25/89 <0.002 mg/L 1/24/89 0.02 mg/L 1/31/89 <0.005 mg/L 1/25/89 >200 F 1/16/89 0.0 mg/kg 1/19/89 NIA A451S Fv+� C odµcm T�� i acma,J ,-r�