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NC0020656_NPDES Permit Renewal App_20090210
Beverly Eaves Perdue Governor CRAIG F HONEYCUTT CITY MANAG_ ' CITY OF.. [WOW] t PO BOX 249 LAURINBURG NC 28353 Dear Mr. Honeycutt: kVA NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Coleen H. Sullins Director February 10, 2009 DENA-FRO =.3112 9 DWQ Dee Freeman Secretary Subject: Receipt of permit renewal application NPDES Permit NC0020656 Leith Creek WWTP Scotland County The NPDES Unit received your permit renewal application on February 9, 2009. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. If you have any additional questions concerning renewal of the subject permit, please contact James McKay at (919) 807-6404. Sincerely, Dina Sprinkle Point Source Branch cc: CENTRAL FTLFS Fayetteville:Regignal_Ofice/Surface Water Protection NPDES Unit Robert A. Ellis, Treatment Plants Director, Town of Laurinburg, P.O. Box 249, Laurinburg, NC 28353 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Raleigh, North,Carolina 27604 Phone: 919-807-63001 FAX: 919-807-64921 Customer Service: 1-877-623-6748 Internet: www.ncwaternuality.org An Equal Opportunity \ Affirmative Action Employer NorthCarohna aturaiij o► Caurirkurg OFFICE OF THE TREATMENT PLANTS DIRECTOR February 5, 2009 Mrs. Dina Sprinkle NCDENR / Water Quality / Point Source Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Renewal Application Packet Permit# NCO020656 Leith Creek Wastewater Treatment Plant Dear Mrs. Sprinkle: All -America City 1 I r $ 1967 FEB - 9 2009 DENR - WATER QUALITY POINT SOURCE BRANCH Enclosed is the NPDES Form 2A Application for Pemit NtimberNC0020656, the City of Laurinburg's Leith Creek WWTP, We are requesting a renewal for this permit. Question B 1: The governing board flngmally adopted the CIP March 19, 2002. Since then the CIP has been updatedannually to reflectthe needs of the collection system and pump stations to help eliminate inflow& Inf ltraton.concerns. Copies of the current CIP are attached for your review, • The Authorized Representative Sludge that is generated at this,facili connection with. Land Application of Residuals Permit Number WQ0002526. Leith Creek WWTP has two aerobic digestersaw th-a total volume of $00.0`00 gallons. We try to perform four land application events per-year:for a:total of 3.2 million gallons. However if we needto apply more we will lime stabilize to perform these events more frequently. Craig Honeycutt, City Manager. psis land applied at Laurinburg Marton Airport in We have one additional fathead minnow toxicity test to complete for the permit renewal requirements. This test is being analyzed by our contract lab at this time. We will forward the results as soon as we receive them. If you have any questions concerning this Renewal request please contact me at 910-277- 0214 Sincerely, t Robert E. Ellis Treatment Plants Director 603 LAUCHWOOD DRIVE • P.O. BOX 249 • LAURINBURG, N.C. 28353 • PHONE: 910/277-0214 • FAX 910/277-3633 FACILITY NAME AND PERMIT NUMBER: RIVER BASIN: 1 104 L'�E WwTP CoO_o109D APPLICATION OVERVIEW IV.43-161111 Form 2A has been developed in a modular format and consists of a `Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 MGD must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. FEB - 9 2009 B Additional Application Information for Applicants with a Design Flow z 0.1 MGD. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: DEAR - WATER QUALITY POINT SOURCE BRANCH D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to 1 MGD, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 MGD, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). Sills are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or - b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or c. Is designated as an SIU by the control authority. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: wkvr- IBC) 0 D,Q010 51.0 BASIC APPLICATION INFORMATI PERMIT ACTION REQUESTED: RIVER BASIN: X% Vt ' g9.5I K :iPARTA.:-•BASIQAPPLICATIONANFORMATIOtt FORA PLICANTS, All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet. A.1. Facility Information. Facility Name Mailing Address Contact Person Title Telephone Number Facility. Address (not P.O. Box) Oily of hmuo,NEw' - IE/T/m eREEK L wAr LRffAim 7RANT 0 MA 44q.. LA- jiv 3i p N1 2g3.53 Zp3ERT A. aLls f-rmE'fr ihNT3 1JI EC OR (9 ud i z77- 0ar4- 6,20 )/i- LJ- Aar' A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Mailing Address Contact Person Title Telephone Number 'tim ,q ,4&) Ye aRRI A- )-%NEVC'l Tr t'21w f7%fNYA%E/R (quo) �7�-g3z4 Is the applicant the owner or operator (or both) of the treatment works? Vowner ❑ operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. facility El applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued tothe treatment works (include state -issued permits). NPDES Fe 00 20L5&, PSD UIC Other RCRA Other A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type. of Collection System Ownership TV 0r/11(//V/10 e6 / z'Iz. &A.3T »� f ur too C e Total population served 17,z42_, NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: 467117,4/ Wwi/oozo(.56 ODES LamBEX.W1v 'RfiS/ V A.5. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes ieNo b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? ❑ Yes Q No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of "this year" occurring no more than three months prior to this application submittal. a. Design flow rate 4 b. Annual average daily flow rate c. Maximum daily flow rate A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment pl contribution (by miles) of each. [Separate sanitary sewer ❑ Combined storm and sanitary sewer A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? MGD Two Years Aqo Z. 95. b. • 5, 032. Last Year This Year 2. i06 2.483 ant. Check all that apply. Also estimate the percent /00 PrYes ❑ No If yes, list how many of each of the following types of discharge points the treatment works uses: i. Discharges of treated effluent ii. Discharges of untreated or partially treated effluent iii. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) v. Other Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? ❑ Yes If yes, provide the following for each surface impoundment: Location: N�A Annual average daily volume discharge to surface impoundment(s) Is discharge ❑ continuous or ❑ intermittent? c. Does the treatment works land -apply treated wastewater? If yes, provide the following for each land application site: d. Location: Number of acres: N /A 1 0 Q D N/A ❑ Yes MGD VNo N/a Annual average daily volume applied to site: Is land application ❑ continuous .or ❑ intermittent? N/A Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? MGD ❑ Yes ID' No NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: l ON eXl V/WrP o02of5cp PERMIT ACTION REQUESTED: /VP.S RIVER BASIN: If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). N/A If transport is by a party other than the applicant, provide: Transporter Name Mailing Address W/n Contact Person Title Telephone Number ( V For each treatment works that receives this discharge, provide the following: Name ! `A Mailing Address Contact Person Title Telephone Number ( ) V If known, provide the NPDES permit number of the treatment works that receives this discharge N/A Provide the average daily flow rate from the treatment works into the receiving facility. .0 MGD e. Does the treatment works discharge or dispose of its wastewater in a manner not included in A.8. through A.8.d above (e.g., underground percolation, well injection): 0 Yes I 'No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: N/i Is disposal through this method ❑ continuous or ❑ intermittent? NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: Ltr W 'W o2o40S PERMIT ACTION REQUESTED: liDE5 RIVER BASIN: J n e.evex sm/lif WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.B.ago to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 MGD." A.9. Description of Outfall. a. Outfall number b. Location 00 I (City or town, if applicable) 2835,E (Zip Code) eOTH/VLi (County) `` 14-5 ' 00 (Latitude) c. Distance from shore (if applicable) d. Depth below surface (if applicable) ' W itti jO[N e. Average daily flow rate f. Does this outfall have either an intermittent or a periodic discharge? If yes, provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: Months in which discharge occurs: g. Is outfall equipped with a diffuser? A.10. Description of Receiving Waters. a. b. c. d. Name of receiving water Name of watershed (if known) (State) 79 ° a 7 ' //5 N/A Z.710 (Longitude) . ft. LIACIE1 CREEK P IIANS . NDICITE ft. 171PE ENTER I 141-0 MGD 5TRthnt ❑ Yes IsYNo (go to A.9.g.) N/A ❑ Yes VNo Ltsme IrEP _l7iN United States Soil Conservation Service 14-digit watershed code (if known): Name of State Management/River Basin (if known): United States Geological Survey 8-digit hydrologic cataloging unit code (if known): Critical low flow of receiving stream (if applicable) EF�� /p acute cfs MGD chronic cfs e. Total hardness of receiving stream at critical low flow (if applicable): mg/I of CaCO3 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: LEtn4 2PEEK kiw P NC Oozo&56 A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. ❑ Primary [Secondary ❑ Advanced ❑ Other. Describe: b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal Design SS removal Design P removal Design N removal Other PERMIT ACTION REQUESTED: NHS RIVER BASIN: Lk/rem /JVAR 6451 90 9a go 75 c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe: JD7)ilu-r( %i ilLORWE If disinfection is by chlorination is dechlorination used for this outfall? Does the treatment plant have post aeration? L_1�es lit/Yes Yes ❑ No ❑ No %. A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number: on 1 pH (Minimum) pH (Maximum) Flow Rate Temperature (Winter) 'MAXIMUM DAILY ;AVERAGE DAILY VALUE Value' o .L /YIAXX 19 nix Units. S.U. S.U. /,jy/8 rnlrl. /t WVG is Value Avg 62299) i ure (Summer) P (AV * For pH please report a minimum and a maximum daily value Temperature }fit 2.1 Rohl MAXIMUM DAILY DISCHARGE Conc. Units` CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN DEMAND (Report one) BOD5 CBOD5 g.fmAx Units "Number;of Samples CAL =31,6 cis -AVERAGE DAILY DISCHARG :Conc..' .o llfl 1 Units uinber'of:- Samples ;Oda p ,ANALYTICAL. <, METHOD`' , l 62to FECAL COLIFORM MAX TOTAL SUSPENDED SOLIDS (TSS) >zotpo ;33�Iv�x 1 a7A6G 9AvU Bdnot ND OF PART A PLICATION OVERVIEW (PAGE 'l) TO DETERMINE WHICH OTHER PAR OF FORM 2A YO.U:MUST COMPLETE .25odAy.S 2,51k I Ao•i0Nh0 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: ZE1 ill egEE) W WIP lie O© aOCO LP PERMIT ACTION REQUESTED: f Tj As RIVER BASIN: , .Lit/n3:R BASIC APPLIGATION INFORMATION PART B ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DEN LOWSIGFGREATER THAN OR 'na EQUAL TO 0 MOD (7 n 00,000 gallos per day) All applicants with a design flow rate z 0.1 MGD must answer questions B.1 through B.6. All others go to Part C (Certification). B.1. Inflow and Infiltration.ti�Estimate the average number of gallons per ilk OOQ GPD CEj /n D) day that flow into the treatment works from inflow and/or infiltration. infiltration. Briefl explain any steps underway or plann o minimize inflow d ,/ d iiiil Q L( k./ A , B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within '/. mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (relatefrto wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ❑ Yes IIWNo If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). �1 Name: PO Mailing Address: Telephone Number: ( ) - Responsibilities of Contractor: B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or , uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. ❑ Yes ❑ No NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: LEiri-, ekeEi tVW71 NC 013206,56 PERMIT ACTION REQUESTED: NHS RIVER BASIN: Zia/reek ve in( c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable . d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as applicable. Indicate dates as accurately as possible. Implementation Stage - Begin Construction - End Construction -Begin Discharge - Attain Operational Level Schedule MM/DD/YYYY Actual Completion MM/DD/YYYY e. Have appropriate permits/clearances concerning other Federal/State requirements been obtained? 0 Yes ❑ No Describe briefly: B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combine sewer overflows in this section. All information reported must be based on data collected through analysis conducted • using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed. by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on -half years old. Outfall Number: 00 1 MAXIMUMDAILY DISCHARGE CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) CHLORINE (TOTAL RESIDUAL, TRC) DISSOLVED OXYGEN TOTAL KJELDAHL NITROGEN (TKN) NITRATE PLUS NITRITE NITROGEN OIL and GREASE PHOSPHORUS (Total) TOTAL DISSOLVED SOLIDS (TDS) 3.51 MAY 28mA !I.O my_ 1mr+t <.10 MIN h. l miry! 0.311111N /. inIN I,28num AVERAGE DAILY DISCHARGE Avr3.5o Avg, IS Av3.B. Avg 1.8 Avg fig AY3:2.n Number, of ;Samples. 250 251 12, az a Sm '1500iIN3F *4..500CLG 54 4500 - OG EPA, SI.2 EPA 353.2. EPA3b54 •/0m L OTHER END OF PART B . IE'APPLICATION OVERVIEW (PAGE 9) TO DETERMINE:_ WHICH M 2A YOU MUST COMPLET'' NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: SUPPLEMENTAL' APPLICATION INFORMATION PART E TOXICITY TESTING DATA' POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's oufalls: 1) POTWs with a design flow rate greater than or equal to 1.0 MGD; 2) POTWs with a pretreatment program (or those that ai'e required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • . If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. • E.1. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. ('chronic 0 acute E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conductedin the last four and one-half years. Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. A7— /4D Test number. Test number. Test number: a. Test information.!/ Test Species & test method number • Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) . c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: e L/ n(eoozozo_520 PERMIT ACTION REQUESTED: Test number: Test number: RIVER BASIN: Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected: f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both - Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water Salt water j. Give the percentage effluent used for all concentrations in the test series. k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100% effluent LCso 95% C.I. 0 0 Control percent survival 0/0 Other (describe) NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: 1-74 (),2EFMIWAw P /116Oozo66-6 PERMIT ACTION REQUESTED: /` E 6 RIVER BASIN: 1 &. vee3►Al Chronic: - NOEC % % 0 IC25 % % % Control percent survival - % % % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run (MM/DD/YYYY)? / / / / / / Other (describe) E.3. Toxicity Reduction Evaluation. ❑ Yes 0 No Is the treatment works involved in a Toxicity Reduction Evaluation? If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have cause of toxicity, within the past four and one-half years, provide the dates of the results. Date submitted: / / (MM/DD/YYYY) submitted biomonitoring test information, or information regarding the the information was submitted to the permitting authority and a summary Summary of results: (see instructions) - ��=b�r END OF PARTE r' ez REFER TO THE APPLICATION OVERVIEW (PAGE 'I) TOT DETERMINE- WHICH OTHER PARTS 2A YOU MUST COMPLETE r 4 % � i �� } � t `9''CYrk �� f ' Y*�Y° Y '" Gd P .� F ��� r { 3 d•y b NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: LEir-( 06)7W' NC ODzOCo3/ PERMIT ACTION REQUESTED: ODES RIVER BASIN:. l.iunt ,ei ve,• A/ ' SUPPLEMENTAL APPLICATION INFORMATION PART ':INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users complete part F. GENERAL INFORMATION: or which receive RCRA,CERCLA, ot, an approved pretreatment program? Users (CIUs). Provide the number or other remedial wastes must of each of the following types of F.1. Pretreatment program. Does the treatment works have, or is subject ❑ Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. b. Number of CIUs. SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. V F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. V Name: • Mailing Address: F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Raw material(s): F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into day (GPD) and whether the discharge is continuous or intermittent. GPD ( continuous or intermittent) the collection system in gallons per discharged into the collection system b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow in gallons per day (GPD) and whether the discharge is continuous or intermittent. GPD ( continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ❑ Yes ❑ No b. Categorical pretreatment standards ❑ Yes 0 No If subject to categorical pretreatment standards, which category and subcategory? NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: EI Tg (2/EEJ 14l v it 1)6,20656 PERMIT ACTION REQUESTED: Ili°/ ES RIVER BASIN: - Liijnt eC, % R /A) F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ❑ No If yes, describe each episode. RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? ❑ Yes ❑ No (go to F.12) F.10. Waste transport. Method by which RCRA waste is received (check all that apply): ❑ Truck ❑ Rail ❑ Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number Amount Units CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ❑ Yes (complete F.13 through F.15.), ❑ No F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the next five years). F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) F.15. Waste Treatment. a. Is this waste treated (or will be treated) prior to entering the treatment works? ❑ Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): b. Is the discharge (or will the discharge be) continuous or intermittent? ❑ Continuous ❑ Intermittent If intermittent, describe discharge schedule. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: ri 5E.EA a1- Ak' 00,2a 51n PERMIT ACTION REQUESTED: iNops RIVER BASIN: Lu 6� /Yee ,,t MBINED "SEWER5YSTE If the treatment works has a combined sewer system, complete Part G. G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and outstanding natural resource waters). c. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or on a separate drawing, of the combined sewer collection system that includes the following information. a. Location of major sewer trunk lines, both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed into the combined sewer system. c. Locations of in -line and off-line storage structures. d. Locations of flow -regulating devices. e. Locations of pump stations. CSO OUTFALLS: Complete questions G.3 through G.6 once for each CSO discharge point. G.3. Description of Outfall. a. Outfall number b. Location (City or town, if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) c. Distance from shore (if applicable) d. Depth below surface (if applicable) e. Which of the following were monitored during the last year for this CSO? O Rainfall ft. ft. 0 CSO pollutant concentrations ❑ CSO frequency O CSO flow volume ❑ Receiving water quality f. How many storm events were monitored during the last year? G.4. CSO Events. a. Give the number of CSO events in the last year. events (0 actual or ❑ approx.) b. Give the average duration per CSO event. hours (0 actual or ❑ approx.) NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: L�rn1( W o 11!LOdder S''b PERMIT ACTION REQUESTED: NPDES RIVER BASIN: Am 6L /02 6/iN) c. Give the average volume per CSO event. million gallons (❑ actual or El approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall G.5. Description of Receiving Waters. a. Name of receiving water: ' b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code c. Name of State Management/River Basin: (if known): United States Geological Survey 8-digit hydrologic cataloging unit G.6. CSO Operations. - Describe any known water quality impacts on the receiving water caused intermittent shell fish bed closings, fish kills, fish advisories, other recreational code (if known): by this CSO (e.g., permanent or intermittent beach closings, permanent or loss, or violation of any applicable State water quality standard). NDOFP RT 1) TO DETERMINE WHICH OTHER PARTS MUST COMPLETE,�� ' a .C„,a 9w _r tl°-,�.,?.' � _.- x 3,. �..g .>,.-, r .">E,a^...,_ .,. ..• ..,, ... +r,REFER TOTHE APPLICATION OVERVIEW (PAGE ��� . OF FORM52A YOU a L.i -,$ >, x, �Yi "i Ta Ka �, .5 Additional information, if provided, will appear on the following pages. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: MOP W oo /206.5 :SUPPL' EMEN'TAL APPLIGATION:INFORMATIO PERMIT ACTION REQUESTED: NOES RIVER BASIN: &iii PART. D PANDED EFFLUENT TESTING DAT Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 MGD and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 MGD or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM`DAILY DISCHARGE AVERAGE DAILY, DISCHARGE Conc:`z Units Massa Units METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. Units.: `Units .. `ANALYTICAL METHOD 'MGMDL ANTIMONY ARSENIC d3 L 2007 2oo.7 0. 02.0 0.020 BERYLLIUM CADMIUM CHROMIUM COPPER LEAD MERCURY DL L3bL BbL B17 3®L ]IL Zoo, 7 2O0•-7 2007 Zoo. Zoo. `7 2.45. 1' D. 00z0 06,50 0.010 0.020 0.0(o 0.000oa NICKEL SELENIUM 61)L ZOO, 7 Zoo. 0, 020 0. 02.0 SILVER THALLIUM 0.7" o. ©10 ZINC CYANIDE TOTAL PHENOLIC COMPOUNDS 0.003 BDL fDL HARDNESS (as CaCO3) Z2 Use this space (or a separate sheet) to provide information on other metals requested by the permit writer I I «'c611 E 4zo, � )and 0,030. 0650 0. 0I0 30. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: �7 cRE. ww-rP NC 00 2ara5(4 PLICATION INFORMATI PERMIT ACTION REQUESTED: f'J MS RIVER BASIN: zzine,g4itee z43,p1 T CERTIFicATI All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: Ef/Basic Application Information packet Supplemental Application Information packet: Ele/PPart D (Expanded Effluent Testing Data) Zart E (Toxicity Testing: Biomonitoring Data) 0 Part F (Industrial User Discharges and RCRA/CERCLA Wastes) ❑ Part G (Combined Sewer Systems) AF PLICANTS MUST QOMPLETE THE FOLLOWING CERTIFICATIO I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title Signature Telephone number Date signed (qIO'Dra)irp`i ) HA & Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina DENR 27699-(NT F E B - 9 2009 WATER QUALITY SOURCE BRANCH NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: LETN CieaA fit/ W7P NC 00 2.0105ln PERMIT ACTION REQUESTED: I�PbES Outfall number: 00I RIVER BASIN: litri6e9_ i vee.?i (Complete once for each outfall discharging effluent to waters of the United States.) , MAXIMUM',DAILY'DISCHARGE, • VOLATILE ORGANIC COMPOUNDS VERAGE:DAILY DISCHARGE;. ACROLEIN col 0.05o ACRYLONITRILE BENZENE 13DL 0.0010 BROMOFORM 1JL 6z4 0.00ID CARBON TETRACHLORIDE tDL �24 0.o6i() CHLOROBENZENE CHLORODIBROMO- METHANE • BDL 4z4 1p24 0•0010 O. 0616 CHLOROETHANE 2-CHLOROETHYLVINYL ETHER CHLOROFORM i1 R1�L 1 i GZ4 i 24 .D05b o . 050 0. Oo50 DICHLOROBROMO- METHANE 1,1-DICHLOROETHANE 2.4 O..00to 1,2-DICHLOROETHANE TRANS-I,2-DICHLORO- ETHYLENE 1,1-DICHLORO- ETHYLENE BDL 1 i z4 624 Da0010 D.Ooio 1,2-DICHLOROPROPANE 1024 0. 0610 1,3-DICHLORO- PROPYLENE ETHYLBENZENE METHYL BROMIDE 3DL 624 0.06)0 METHYL CHLORIDE METHYLENE CHLORIDE 1,1,2,2-TETRA- CHLOROETHANE TETRACHLORO- ETHYLENE Poi) D L f • 0.0650 0, 0OW TOLUENE 6 DL 2.4 0.6050 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: Lr•TM CIZEE ww7-P gea0ao15 PERMIT ACTION ODES REQUESTED: RIVER BASIN: LiurnZe,4 ve Pik Outfall number: 0 0 I (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT : ,MAXIMUM; DAILY DISCHARGE' -:-; AVERAGE DAILY DISCHARGE ANALYTICAL METHODS ML%MDL - ,Conc Units Mass"' Units Conc. Units Mass . ..Units Number' ` 3 '� of -Samples. TRICHLOROETHANE BD L I (c24- V J1, 0C/�y/1) 1,1,2- TRICHLOROETHANE j 1—J -I 6)1 O.0WO TRICHLOROETHYLENE VINYL CHLORIDE 1 DL. I &Pi 6.0010 Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS • P-CHLORO-M-CRESOL 2-CHLOROPHENOL (� Qo L 5 % Z5 (Q o. oro 2,4-DICHLOROPHENOL ��L. f I -/ 2 5 (j� aJ ,Q10 6,01o 2,4-DIMETHYLPHENOL 'l��j�i 1-11JL I 625 Q'. No 4,6-D I N ITRO-O-C RESO L 2,4-DINITROPHENOL Pt-DL • I �25 Q pr V ]L l /Z5V,D)D2-NITROPHENOL3,L 4-NITROPHENOL (rT5 0,.D>0 PENTACHLOROPHENOL 13D` PHENOL --B-DL I /025 6,610 2,4,6- TRICHLOROPHENOL 13bL I eZ5 ��� ��� y�� p( o V Use this space (or a separate sheet) to provide information on other acid extractable compounds requested by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE i}T L I 25 D. odi c) ACENAPHTHYLENE 1--_ I (O 6 Q, 00/0 ANTHRACENE BENZIDINE'ft L ) (O26 2.050 t�l BENZO(A)ANTHRACENE L I, 45 0. 06/0 BENZO(A)PYRENE ` -DL I Z 2 a.a6/e NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: Am" ezei< i / p NCB 020656 Outfall number: 3,4 BENZO- FLUORANTHENE BENZO(GHI)PERYLENE BENZO(K) FLUORANTHENE oot PERMIT ACTION REQUESTED: NPDfs RIVER BASIN: Lr,tBJ4&-7e- 234.s//�l (Complete once for each outran discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE Cone" ll1JL nits ,• Conc. AVERAGE DAILY<DISCHARGE" Units Units umber .of Samples' ANALYTICAL ,METHOD (z5 BIS (2-CHLOROETHOXY) METHANE BIS (2-CHLOROETHYL)- ETHER BIS (2-CHLOROISO- PROPYL) ETHER . 0, CVO 0.00/0 0, 6oi0 BIS (2-ETHYLHEXYL) PHTHALATE 4-BROMOPHENYL PHENYL ETHER . 0.610 0•000 BUTYL BENZYL PHTHALATE 2-CHLORO- NAPHTHALENE 0,010 4-CHLORPHENYL PHENYL ETHER 0-010 CHRYSENE DI-N-BUTYL PHTHALATE 0.6616 0.CoiD DI-N-OCTYL PHTHALATE DIBENZO(A,H) ANTHRACENE 1,2-DICHLOROBENZENE Lz4 O.Obib 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 3,3-DICHLORO- BENZIDINE DIETHYL PHTHALATE DIMETHYL PHTHALATE 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE 1,2-DIPHENYL- HYDRAZINE 1 (, 24 425 125 lz5 1Z5 Z5 62,5 0.0610 0.661 D 8. 011D Q 0 b(! 0,610 0. 01 0.bi0 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: ,LEinN�zgx WW1 NC00266569 PERMIT ACTION REQUESTED: ES RIVER BASIN: LLazazWver 3)N Outfall number: (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM_ DAILY`DISCHARGE Conc: Units' Mass :Units' Conc. AVERAGE DAILY DISCHARGE Mass Units Number - of „Samples ANALYTICAL METHOD ' MUMDL FLUORANTHENE FLUORENE FIEXACHLOROBENZENE IL 425 A(X),10 0, 0010 0.01D HEXACHLORO- BUTADIENE O.610 HEXACHLOROCYCLO- PENTADIENE HEXACHLOROETHANE INDENO(1,2,3-CD) PYRENE A01 6 6,616 6,6616 ISOPHORONE 0.0/0 NAPHTHALENE NITROBENZENE 0,0010 0. O IO N-NITROSODI-N- PROPYLAMINE 0.0/b N-NITROSODI- METHYLAMINE O•650 N-NITROSODI- PHENYLAMINE 0. 010 PHENANTHRENE O.OD/o PYRENE 1,2,4- TRICHLOROBENZENE V Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer v (5. obi b 6.0/0 Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides requested by the permit writer NPDES FORM 2A Additional Information 214 ewer Plan WO- CIP 5 Yr Plan Capital Improvements (5) Year Plan Sewer Lift Stations Year Pump Stations Cost 2008-2009 Upgrade 74 Bypass Pump Station (Pumps, Motors & Valves) $ 90,000.00 2009-2010 Engineering Study to minimize the number of pump stations 30,000.00 2010-2011 Engineering & Plans for Bridge Creek Pump Station 40,000.00 2011-2012 Upgrade Electrical Controls at Pump Station 30,000.00 2012-2013 Upgrade Electrical Controls at Pump Station 30,000.00 220,000.00 Five Year Capital Projects Sewer Projects Year Street Problem Est. Cost City cost Total cost 2009-2010 McKay Street total cost $675,000.00 $275,000.00 $ 775,000.00 grant $500,000.00 city cost $175,000.00 New Construction and repairs $100,000.00 2010-2011 Creedle St. and area total cost $748,438.00 $174,843.00 $ 848,438.00 grant $673,595.00 city cost $74,843.00 New Construction and repairs $100,000.00 2011-2012 Cronly Street bad pipe $287,548.00 $387,548.00 $387,548.00 New Construction and repairs $100,000.00 $387,548.00 2012-2013 Fairly Street bad pipe $202,559.00 $503,059.00 $503,059.00 Gill to Dickson Street bad pipe $200,500.00 New Construction and repairs $100,000.00 $503,059.00 2013-2014 S. Main to Biggs Street bad pipe $47,100.00 $362,975.00 $362,975.00 Biggs to Wilson Street bad pipe $121,675.00 Foraker to Taft Street bad pipe $94,200.00 New Construction and repairs $100,000.00 $362,975.00 pity of Cot,trip6urg: OFFICE OF THE TREATMENT PLANTS DIRECTOR April21, 2009 Division of Water Quality Attention: Central Files 1617 Mail Service Center Raleigh, N.C. 27699-1617 Re: Notification of Name Change NPDES Permit No. NC0020656 NPDES Permit No. NC0021661 NPDES Permit No. NC0036773 Dear Sir or Madam:: All -America City 11 IF 3 1967 p,* 21 7009 N1•10 .1z QUO( ,�E B�p,NCH This letter is to notify you'tlat our City Manager Craig Honeycutt is no Monger with the City of Laurinburg and.: council has ap'pointed'-an-Interim City Manager,Dolores A. Hammond. Please addressany future correspondence to: Dolor`es nterirh it I> ;P.O Box Laurinburg, • She will also be signing our monthly monitoring reports until ,further notice. If you have any questions please contact meat the number; below" Robert A. Ellis Treatment Plants Director Cc: Dolores A. Hammond, Interim City Manager 603 LAUCHWOOD DRIVE • P.O. BOX 249 LAURINBURG, N.C. 28353 • PHONE: 910/277-0214 • FAX: 9101277.3633 Oi of Cattriofturg, OFFICE OF THE TREATMENT PLANTS DIRECTOR March.18, 2009 Mrs. Dina Sprinkle NCDENR / Water Quality / Point Source Branch 1617 Mail Service Center Raleigh, NC 27699-1617 22 2 s MAR 2 3 2009 A ll -America re 1956 2bb3 1967 Subject: Renewal Application Packet DENR - WATER QUALITY Permit# NC0020656 POINT SOURCE BRANCH Leith Creek Wastewater Treatment Plant Dear Mrs. Sprinkle: We have enclosed the additional fathead Winn, toxicity test iil for the permit renewal requirements and a schematic of the wastewater flow and process rocess for your review. " " . Along with the above mentione process. The City of Laurinburg's collet throughout the system." There- mains. Our Leith Creek Plant consist o plant, consisting of 2 aeration basins, return sludge pump station with 3 pumps, total capacity 2.0 million gallons per day nat on we are sending a narrative of our treatment (MGD) Moff34 pump stations located avity sewers and24 miles of force es of treatment, one `extended aeration erg clarifiers, 2-chlorine contacfchambers and one The second plant is an. oxidation.;ditch�style with 1 clarifier, 1 chlorination point and 1 return sludge pump station with 3 dual"speed pumps, total capacity.2.0 MGD, for a total treatment capacity of 40 MGD. The facility has 2 aerobic digesters, (1) 150,000-gallon tank and (1) 650,000-gallon tank with course air diffusers. Sincerely, Robert A. Ellis City of Laurinburg Treatment Plants Director Cc: Dale Lopez, Division of Water Quality 603 LAUCHWOOD DRIVE • P.O. BOX 249 • LAURINBURG, N.C. 28353 • PHONE: 9101277-0214 • FAX: 910/277-3633 SC1 c 1`:'A71C of VvpSri: WATee RDN/ 4.116D Nr )=S-NCO3P0656- D1=-1A 5.e191- t>,.OD NA1' '� S iSok Co 111=L1.X.c: ).1 GAL EQ-1/4.&z.ZZATsclwj $4,Sr►J -rm.0=1.7 ctFrh -1.0 p;G DAY C.£1 COIL — ��v 7 S.O MuL? I\[oT To ANq Sri D-13Y GemtraZ A:)A:)d2 pump STAr1aa A MED 101r11d6 Isx E0X . E EA71kJ S1N O -!4o . Z A1=EATJGN SAS!Q 0 O No-1 ciA zI m=P No. 3 Siu�� DPY1Nb ZEDS V zr Lke...14 krrEt STAN -i3Y GEAtf2AT7A F 86TP PM/47S Effluent Toxiv.ity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:2/18/2009 Facility: Laurinburg NPDES # NCO() 20656 Pipe #: 001 County: Scotland Laporatory: Me itech, Inc. X _. Signature of Operator in Responsible Charge x Signature of Laboratory Supervisor Comments Inversion at 15.5% MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time %Elf: Control Repl. Surviving # Original # Wt/original (mg) 7.75 Surviving # Original # Wt/original (mg) 15.5 Surviving # Original # Wt/original (mg) Surviving # Original ,# Wt/original (mg) 31 62 Surviving # Original # Wt/original (mg) 100 Surviving # Original #, Wt/original (mg) Water Quality Data Control pH (SU) Init/Fin DO (mg/L) !nit/Fin Temp (C) Init/Fin High Concentration pH (SU) !nit/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date . Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (°C) Dilution H2O Batch # Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) 2/3/2009 1 2 1:15 PM 3 4 Avg Wt/Surv. Control 10 10 10 10 10 10 10 10 0.621 0.615 0.665 0.616 10 10 10 10 10 10 10 10 0.578 0.591 0.563 0.582 10 10 10 10' 10 10 10 10 0.551 0.620 .0.460 0.550 10 10 9 9 10 10 10 10 0.663 0.597 0.558 0.541 10 9 _ 10 9 10 10 10 10 0.628 0.583 0.638 0.556 10 10 10 10 10 10 10 10 0:633 0.522 0.515 0.554 Day % Survival Avg Wt (mg) % Survival Avg Wt (mg) % Survival • Avg Wt (mg) % Survival Avg Wt (mg) % Survival Avg Wt (mg) 0.629 100.0 0.629 100.0 0.579 100.0 0.545 95.0 0.590 95.0 0.601 I % Survival Avg Wt (mg) 100.0 0.556 Test Organisms r Cultured In -House I-4 Outside Supplier Hatch Date: 2/2/09 Hatch Time: 3:00 pm CT 1 2 3 4 6 8.09 / 7.96 8.06 / 7.75 7.96 / 7.71 7.92 / 7.93 8.17 / 7.98 7.98 / 7.68 7.98 / 7.54 7.60 ' / 6.94 7.70 17.01 7.91 / 6.88 7.70 / 7.83 8.02 / 7.79 7.90 . / 7.10 7.64 / 7.13 24.8 / 25.0 24.8 / 24.9 24.6 / 25.0 ' 24.9 / 24.9 24.8 / 25.0 24.9 / 24.9 ' 24.9 / 25.2 0 1 2 3 4 5 6.33 / 6.74 6.48 / 6.80 6.46 / 6.80 6:45 / 6.74 6.66 / 6.92 6.51 / 6.52 6.39 / 6.54 7.96. / 7.09 8.03 / 6.94 8.26 / 6.79 7.91 17.80 8.06 17.75 7.85 / 6.94 8.48 / 6.75 24.8 / 25.0 24.8 / 24.9 24.6 / 25.0 24.9 / 24.9 24.8 / 25.0 24.9 / 24.9 24.9 / 25.2 .1 2 3 2/1/2009. 2/2/2009 2/5/2009 26.0 24.1 24.6 22 22 22 12 10 10 324 326 334 <0.1 <0.1 <0.1 0.2 0.4 . 0.6 328 46 60 241 329 330 48 44 58 58 226 211 Normal Horn. Var. NOEC LOEC ChV Method Surv'val I(= ft� 100 >100 >100 Growth FIB Fl: 100 >100 >100 Steel's ' Dunnet's Overall Result ChV >100 Stats Conc. 7.75 15.5 31 62 Survival Critical 10 10 10 10 Calculated 18 18 14 14 Growth Critical Calculated 2.41 1.5817 2.41 2.41 2.41 2.6179 1.2310. 0.8726 DWQ Form AT-5 (1/04) 100 10 18 2.41 2.2829 Initials/Signature: • End Date: End Time: Client: Laurinburg NPDES #: NC 0020656 Initiated by: 1 / / Date/Time Fed: 2/3/09 /6364,n Date/Time Born: 2/2/09 3:00 PM CT Day 1 Day2 2/5 /03c2,,,_ yr�L Day 3 2/6 Day 4 2/7 1C; O M' Day 5 Day 6 2/9 —1 (Do"-&- 1/ ;Transferred by: Date 2/4 Time Initials 2/8 ) in0 M a Test Termination Data: f�7 AL -.2. A,UM-12-1\-"- 2/10/09 Meritech, Inc. Chronic Fathead Minnow Benchsheet Transfer and Feeding Dates and Times # of Organisms per Chamber: 10 Test Vessel Size: 400 ml Test Solution Volume: 250 ml Temp. of Stock: Z'-\ °C # of Reps: 4 Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Date Time 1 2/3 2/4 Start Date: 2/3/09 Time: End Date: 2/10/09 Time: l otiL C if No Randomization: Incubator #: Fed by: Initials Time 2 Initials Time 3 Initial 1030,41y) 13oP() mp. i l 'ram ti ` \\720 - YYl \ - 2/5 79,E -- 2/6 (:00Ain UU- 11,t,L�, 2/7 C• ,f�\ �/41 is-ti.%%i.o'--•-• 6, 2/8 1Z:Crep., M.L 2/9 7(�w m O /43 = Weekend, only 2 feedings needed i7C ® I ENVIRONMENTAL LABORATORIES A Division of Water 'Technology ant? C-or.trots. loc. FISH LARVAL SURVIVAUGROWTH DATA SHEET CHRONIC FATHEAD MINNOW Facility: Lk°r1 NPDES #: me_ Oc; 2.6 G S Date of Test: 2-/31oq Initial weights taken on: 2-2, - 09 by: Organism: Pimephales promelas Final weights taken on: .,'� !�• - .cY by: Page: / of 2 Outfall: 00 CONC REP PAN WT. (mg) PAN + ORG. WT. (mg) WT. OF ORG. (mg) # ORG. MEAN WTJORG. (mg) SURV % L O N 1 k L A 81o. 82 17./%3 (0. ?1 . I 0 O. t5,-2 t 100 B eo0.13 Ssl2, Ca. l to Li&lc- WV c PO(, 55r--,),. 11 (,, (, (0 0, (d.cS I( ID r(q (a. I2 - c> z ,9,8 r 1(.. (0 `'t I. L IW 7 75 / A 8co.'13 c6:. cl . --) 10 6, 5---n ECD B eol. 58 950 ,fir, 4; q C I° o . cc) ( . 00 c 1798, i.3 -6`t , (_3 10 o - C 00 D 802,42J Tcpwi.2. .l a a 10 JOb 6 g' KS A 803.36 gc .�-7 S---, S 1 10 D9 sr7 l W B Mc.81 13.O1 (0. 61 10 n 0 IOC c POO, rig c; 37 LI• c (0 C•46 2 lop o nqg. D4 �()1, .ii -GE.) 1 � e. s7s---6) (00 E ITEC , 11 C., ENVIRONMENTAL LABORATORIES A DiViSiOn of Water hnology and Colltrols, FISH LARVAL SURVIVAL/GROWTH DATA SHEET CHRONIC FATHEAD MINNOW Facility: L r14100,1 NPDES #: cy)2.0(0.5-6 Date of Test: Initial weights taken on: 2- 3-0 by: Mt, Final weights taken on: -- 9 by: Page: 2- of 2 Outfall: Organism: Pimephales promelas CONC REP PAN WT. (mg) PAN + ORG. WT. (mg) WT. OF ORG. (mg) # ORG. MEAN WT./ORG. (mg) SURV % • 31 rt A ficii,91 717. 6,, L.:?:, , ID r).&63 to-o B /NCI ,84 • W bc--,1 _ CeoC7 10 6.,5-q7 W . iff 0 c rig 1.5 —76417, C.) 5.--S-- C3( a, .s--5--• • D quigi '7 clqictS. :c-, 4 1 q Os-4 i . _ q0. 62 / - • A r192,98 pv- A • la-ol .- 1 C 2 7 - -lic i -•,?.. .2,k- 10 0, (::,2.• to B riga b(r) t i 5 Dciset __-.7,U• A c -805,05 V\ , ,1_; co ,7, g 10 c).. (03+g .fo) D - POS-.511 •c6 1) 4.6 s.,c-G 9 . IOD 7, • , A RA.(12, , ) i 5- (0.33 ID ei,633 . 100 B Boo/6 D S-, 0- 5---/ :?Ic3 10 c • 801.09 /-)i::., N -C. /-C- CO too' e),675 D 802AB q1) , Cp, s---:, 514 (0 Client: L,1urn.borg ENVIROtVMENTAL LABORATORIES A Division of 41atr_r Technology and Contr'o/s, /nc. Chemical and Physical Determinations NPDES#: roc CX O &SG, Start Date: Z/3)0 7 Test Organism: Pimephales promelas Analyst(s): 11(rill r,na- End Date: 2-1iO4 Time:. /S Time: /04.,- Da Concentration: control 0-1 1-2 2-3 3-4 4-5 5-6 6-7 , Remarks Batch # ,3 Z0 — 3 2ij ,30 1' pH Initial 8.09 57,0to -NI, ?,'Z. R--% i,()B 7 Final 7,q(o ,-75 7,7/ 7.9 3 rT, %g "7 (J ?•-S D.O. Initial 7 too -2 ,7 0 ?Ai 7.20 g- D? 1.1 G 7, 6, `7 Final (er-{ -2,01 ., c( 7 83 rt.' 1! 1C� 7.13 Temp. Initial Zi.�.e 2 q.,' . zy.4 2 y,cJ 7 �j.;�'/ 2.Ifi ve. `f Final 25,0 ZV . y 2-S. C `2 iI ,q 25.O 2..'L f 2 S2— Conductivity Initial 9,91 29-1 ..5.r- 221, CIS 2,J8 1% Final /FO 2 97 2t e xot G.rl(o 2I/6 2y Residual Chlorine G•O. 1 4.Q • i 40.1 2- C , / 4 0 •• / 40, / i0• l Hardness C/(; ig > qy — Alkalinity ([) .--- j �j — .6 ---> Da Concentration: 7,75 y 0-1 1-2 2-3 3-4 4-5 5-6 6-7 Remarks pH Initial 7.q1 -7•c17 ?,`41 ?f/o 7 9 q.cl4 7,675' Final 7,?/ -7,7t.f 7 (, g 7. 7 '7, Ito .76,0 ?,S3 D.O. Initial 7, (,1 7 ,71 . -i. ?? -7 6 0 55-O 7 r(. (E,i 7 /n K Final (0,13 7,Z3 (L. ( 7,g--R (1,111 7,/+ 7. OD Temp. Initial 2q,s 2.4,p, .. 2,1,6 7q,7 2ii,g/ 2,4,1 .7_tf• 1 Final 7_5;0 Zi 'I Z.51.0 22q•'t 25.0 Zy/( 2-S.2.— Conductivity Initial 2.91 258 Mb, 2 q q ) 9 232, 2. 3 Final ,201s Zq 1 2 t 5 31 d 321 L f7 •x i 7 Residual Chlorine GO . I LO • / 40, ( 40 • f Lv , ( i 0.1 L O. / Da Concentration: (6$ Y. 0-1 1-2 2-3 3-4 4-5 5-6 6-7 Remarks pH Initial 7,7 0 ' 7.$.7- 7,7' 7.Si / 7. L2. rt. 6l 7, 77 Final '7, (D / -7, %V 7, •7 g-3 '7. 62. ?,, 7 III( D.O. Initial7(o6. %77 _7. 7.R0 7,6'7 "3 r(,84 7,•7f_ Final 7,0? )•2-- (,G / 7, Va gin 7,0T ‘.qy Temp. Initial 2 7• 0 Z i. f zi.f b 29;,.r 7 c, - 21. CI l' y, Y Final 7.5•O z .q _-,c -,.q8 2S'.O 2.4U( 2,S,2- Conductivity Initial Q'j 1 2 (D. -21-,0 251 2S-9 2LIB Z 3 ✓ Final 26 8 7ifq. 273 31 1 319 2-(o(o 5--- Residual Chlorine 4O• / L.O. j L0.1 G0. ( 4.0 .1 GO. / GO • ( IV1ER0TE'C14; 1/V4"_ trer- ENVIRONMENTAL LABORATORIES A Division of ',Voter technology nna:/ Controls. ,nc. Chemical and Physical Determinations Page 2 of 2 Client: Loa) c' i vt 10 a rq NPDES#: Nc. CO2(', (,;, -G Start Date: 213 /Dy' Time: f // Test Organism: Pimephales promelas Analyst(s): p91 LIMP.- - End Date: Z/0/7 Time: Da Concentration: 317 0-1 1-2 2-3 3-4 4-5 5-6 6-7 Remarks pH Initial 7, .51e 7 WI 7,(0.1 7 (e ' 7, (03 .1. W.. 7, �2 Final 7.%f 7, 50 `7, (0_ ). 7 (0 17, q I 1,(i7 -7, z6 D.O. Initial 7,(o5 7.7(0 ?-gS -?,(e, y . b 1.iy) 7 79 . Final 707 (0A- (r t% `7• m '7, 9 ?: /3 1 y Temp. Initial Zt}.b 2y.D Zy6 211,7 .2.US Zta ci Z�l I Final 2.5.0 ZLI,9 2,1..CI ?1i,`7 25.o Zii,`( 25 - Conductivity Initial ag't, 2_72 2.60 2.6 (4 26$ 214, I 2-3 Final 3oS 3o4' 290 :7,0 314 27L% :..S �' Residual Chlorine L0, / L 0, / 40. i 10-/ L 0. 1 ' 0, / 1.0. / Da Concentration: (o z '7, 0-1 1-2 2-3 3-4 4-5 5-6 6-7 Remarks pH Initial 7,13 7, ?i(� 7, Z 7, - , .S I,.�i�a 7 I Final 7.tf . ?,30 7.Ll ?• �v tj:So -7,2 /9 D.O. Initial 7. 3 Z. 7, C1 3 '25,0 "7, ? ,s--- q.-, b 6 r(.'7'1 ?.q 7_ Final -7 IC 7.I9 L'•cQ 7tg1 1.'72, 4,,qZ. (Q.S,. Temp. Initial 24. j &/, 8 74.6 zit , l :vs/ 2e1,,cj z V, 7 Final 2,5: 0 Z t(.9 ZST& = , 25.O -Z'/ M ,s; a -- Conductivity Initial 309 2q8 LSO 290 �� 14 2q0 = V) Final 22.. ��! 315 3 359 303 3 Residual Chlorine 410, ( C 0, L - 40. ( io. / 1. O. ( I O. / 4O. Da Concentration: 100% 0-1 1-2 2-3 — 3-4 4-5 5-6 5-6 6-7 Remarks pH Initial 6, 33 // (D • L 71 t (0, ct1 L1 � .7r (a a S ( 6.) 3 75--- Final (p 1 41 W .gel ( , g'e r-((. to, 7 N1 . � sq D.O. Initial 7, qh WWF, o �,1(19,� l p91/eJa 7c0- V . V� Vl I�6,./}�{7 2 ti l5 f R Final 7. 0? '3t. (0 ,� Y' G .7q 7.g0 '7,'7S . Cagy 7S Temp. • Initial 214.8 z4.6 ' 24,5 2)4.3 2 r f , r 2 LI . ct Z7 . 7 Final Zs . 0 4J 2 , S • G %(-/' 25.0 7-1 , c( 7,-,CZ Conductivity Initial 3 2, 1 •32. (o 32 - 3 2 -1 3 3 q- 33 3 3 J Final 3 z 7 / 3(73 37 Rr1 .-5�2- 3'-t 7 Residual Chlorine G 0, I 10, / I 0, / 40./ L o • / L. 0.1 40.1 Hardness 2 22 9_2, . Alkalinity t L. 11 10 MERITECH, INC. Mortality Data: Chronic Fathead Test Client: L o c` (vL bo c`ej Start Date: Zj3�t�9 Start Time: I I End Date: 2/0/007 End Time: 164S0^,✓ Concentration Cori+rol Day 0 Day 1 Day 2 Dal/3 Day 4 Day 5 Day 6 Day17 Rep #1 0 0 0 q- 0 0 0 I.J Rep #2 C1 0 (0 c. 0 0 0 O Rep #3 0 0 0 C. C) 0 0 Rep #4 0 0 0 Ci 0 0 0 0 Concentration -7, 757, Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 0 0 0 c_ 0 0 0 0 Rep #2 0 0 0 C' 0 0 0 0 : Rep #3 0 0 0 ram l-' 0 00 0 Rep #4 0 0 0. C 0 O 0 0 Concentration I6 s Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 0 0 0 C 0 0 0 0 Rep #2 0 0 0 c' 0 0 0 0 Rep #3 0 0 0 0 0 0 0 Rep #4 0 0 0 (0 0 0 0 Client: Lau r i n to of j MERITECH, INC. Mortality Data: Chronic Fathead Test Start Date: 43�07 Start Time: ). J� End Date: 1�__ End Time: {`NSCI Concentration 31 v, Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 0 0 0. C' 0 0 ____Q__— 0 Rep #2 0 0 0 C 0 0 0 0 Rep #3 0 0 0 () 0 0 1 0 Rep #4 0 0 ___I-- L� 0 . 0 0 0 Concentration Z ' Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 0 0 C 'CI 0 0 0 0 Rep #2 0 .0 0 0 6 0 ___i— 0 Rep #3 0 0 0 L' 0 0 0 0 Rep #4 0 0 0. 0 ° 0 0 Concentration , /(j 1, Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Rep #1 V 0 0 C C) 0 0 0 Rep #2 0 0 0 0 0 0 0 0 Rep #3 0 0 0 G' 0 7 0 0 Rep #4 0 0 iJ V o Q Client: C, Contact Person: Address: City: County: vC Lete.; P o; e?) P S MERITECH, INC. Meritech Sample ID #: 3GI Bioassay Sample Chain of Custody 642 Tamco Rd, Reidsville NC 27320 Phone: 1-336-342-4748 Fax: 1-336-342-1522 Email: txmrtech(bellsouth.net Web Site: www.meritech-Iabs.com CLIENT INFORMATION LvW.-FP PO#: NPDES#: NC 9O�05 s G, Phone: 9/0 - /7/7 Pipe #: LJ — H1 7-7 State: ,4. L Zip: e 3 3-.2 SAMPLE INFORMATION Sample Site: �r/%e Sample Type: ❑ Grab Sampling Time: Start Date: End Date: Composite c9ja/a i # of containers: Start Time: ( 7?4� f 7 PM End Time: J O CPO AM PM —♦ CHRONIC TESTS SHOULD BE TAKEN AFTER 10:00 AM IF AT ALL POSSIBLE *** SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVE WITH ICE *** 1 Collectors Name: Print: j Gl_. C26 7 - Signature: Test Required: ❑ Chronic (7 days) ❑ Acute (24-48 hours) Comments: TOXICITY TEST INFORMATION Test Organism: ❑ Ceriodaphnia dubia (water flea) ❑ Pimephales prordelas (fathead minnow) ❑ Mysidopsis bahia (shrimp) Test Concentrations (if multiple dilutions): Relinquished by: Received b Relinquished by: o1_8 Received by: " ,_ 4i'-f- = ZL I, SHIPPING INFORMATION Date: a g�% 02/.09 Date: ©0407 Date: Date: 07' a-64' �.a_65 Sample Temperature (°C): Time: /4 ps AM PM Time: /p •`d AM PM Time/t0 /OA re4 PM Time: /% /d 033 PM Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up **Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ** SAMPLE RECEIVING (Laboratory Use Onlyi Relinquished by: .4- Received by: Sample Temperatures (°C): / G, a / Date: Time: 09c-t AM Sample Condition: 1711CCGtt PM WHITE = Laboratory copy YELLOW = Client copy MERITECH, INC. Meritech Sample ID #: 0 0 M`4 Bioassay.Sample Chain of Custody 642 Tamco Rd, Reidsville NC 27320 Phone: 1-336-342-4748 Fax: 1-336-342-1522 Email: txmrtechnbellsouth.net Web Site: www.meritech-Iabs.com j r f CLIENT INFORMATION Client C,51J �T i2 Contact Person: Address: City: County: 44-7f 1 "i349,( SC4.974 / State: //.<•, PO#: NPDES#: NC GBo`?O�S� Phone: 1// ' 07%r/ 2/6'" Pipe #: .544// Zip: 9A'35� a Sample Site: Sample Type: Sampling Time: SAMPLE INFORMATION ❑ Grab Start Date: End Date: [ Composite # of containers: . /3/,7 Start Time: /Qao 4) PM End Time: /OLDS- PM �► CHRONIC TESTS SHOULD BE TAKEN AFTER 10:00 AM IF AT ALL POSSIBLE *** SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVER WITH CE *** Collector's Name: Print:G �1%i'�� Signature: o' Test Required: 0 Chronic (7 days) ❑ Acute (24-48 hours) IWC: . • % Comments: TOXICITY TEST INFORMATION Test Organism: ❑ Ceriodaphnia dubia (water flea) 12- Pimephales pronielas (fathead minnow) ❑ . Mysidopsis bahia (shrimp) Test Concentrations (if multiple dilutions): Relinquished by: Received by: Relinquished by: Received by: tz ** Samples s SHIPPING INFORMATION Relinquished by: Received by: Date: Date: Date: Date: 0, Time: Time: Time: Time: AM 1 a: ` 3" re . /bZ Sample Temperature (°C): 2,d7, d 8 ys'' AM ,449.totrof Shipment: ❑ UPS ❑ Fed X V �j Meritech Pick-up 9 F t7 ped on Friday must be FedEx and must be cleatly labeled for Saturday delivery" SAMPLE RECEIVING (Laboratory Use Only) Ii Sample Temperatures (°C): U , Ll / i�, L\ / Date: PM PM PM Time: 0 '? '_ I go PM / Sample Condition: WHITE = Laboratory copy YELLOW = Client copy MERITECH, INC. Bioassay Sample Chain of Custody 642 Tamco Rd, Reidsville NC 27320 Phone: 1-336-342-4748 Fax: 1-336-342-1522 Email: txmrtecht bellsouth.net Web Site: www.meritech-Iabs.com CLIENT INFORMATION Client: C it 2 q,�J -';Ah 7 L re (i Contact Person: T J!! -� l L s Address: i1/U • &,r 3, YS City: C-j�/1f4 County: �Cv ;'Y State: Zip: Meritech Sample ID #: V � (o V 7? L PO#: NPDES#: NC Phone: 9/0`•01 Vl Pipe #:. 6 / 5? 1 Sample Site: Sample Type: Sampling Time: SAMPLE INFORMATION • ❑ Grab Composite # of containers: Start Date: - =5G' Start Time: 9 99!) <M PM End Date: ,, /1.1l End Time: . 4.2;L).-5-- AM .s- Z vNufY .—► CHRONIC TESTS SHOULD BE TAKEN AFTER 10:00 AM IF AT ALL POSSIBLE *** SAMPLE CONTAINERS ARE TO B//E.. COMPLETELY FULL (no air space), CHILLED AND CORED WITH ICE *** Collector's Name: Print: l' k}/ �/ �,/}^ Signature: Test Required: ❑ Chronic (7 days) ❑ Acute (24-48 hours) Comments: TOXICITY TEST INFORMATION Test Organism: ❑ Ceriodaphnia dubia (water flea) ❑ Pimephales pronielas (fathead minnow) ❑ Mysidopsis bahia (shrimp) Test Concentrations (if multiple dilutions): Relinquished by: Received by: Relinquished by. Received by: Relinquished by: Received by: SHIPPING INFORMATION Date: Date: Date: Date: Sample Temperature (°C): c .., 6 , ,3 9 0c) e Ofcrprn�eo-E1 UPS ❑ FRI / U ] Meritech Pick-up G 3 r //Pi ** Samples shipped on Fri ay must be FedEx and must be clearly labeled for Saturday delivery** SAMPLE RECEIVING (Laboratory Use Only) C Jo>7 �S Time: Time: Time: Time: /Pis 1 l ',$-0 (13� AM PM PM Ot PM P fikl,C��1� col 5 Date: Sample Temperatures (°C): 0 -7-09 I2Ice Time: 7)0 PM Sample Condition: / e e . WHITE = Laboratory copy YELLOW = Client copy Title: laurinburg File: laurinburg Transform: NO TRANSFORMATION Shapiro - Wilk's Test for Normality D= W= 0.0371 0.9591 Critical W = 0.8840 (alpha = 0.01 , N = 24) W = 0.9160 (alpha = 0.05 , N = 24) Data PASS normality test (alpha = 0.01). Continue analysis. Title: laurinburg File: - laurinburg Transform: NO TRANSFORMATION Bartlett's Test for Homogeneity of Variance Calculated B1 statistic = 7.6423 (p-value = 0.1771) Data PASS B1 homogeneity test at 0.01 level. Continue analysis. Critical B = 15.0863 (alpha = 0.01, df = 5). = 11.0705 (alpha = 0.05, df = 5) • Title: laurinburg File: laurinburg Transform: NO TRANSFORMATION ANOVA Table SOURCE DF SS MS F Between 5 0.0188 0.0038 1._8227 Within (Error) 18 0.0371 0.0021 Total 23 0.0558 (p-value = 0.1591) Critical F = 4.2479 (alpha = 0.01, df = 5,18) = 2.7729 (alpha = 0.05, df = 5,18) Since F < Critical F FAIL TO REJECT Ho: All equal (alpha = 0.05) Title: laurinburg File: laurinburg Transform: NO TRANSFORMATION Dunnett's Test - TABLE 1'OF 2 Ho:Control<Treatment GROUP IDENTIFICATION TRANSFORMED MEAN CALCULATED IN SIG MEAN ORIGINAL UNITS T STAT 0.05 1 control 0.6293 0.6293 2 7.75 0.5785 0.5785 1.5817 3 15.5 0.5453 0.5453 2.6179 * 4 31 0.5898 0.5898 1.2310 5 62 0.6012 0.6012 0.8726 6 100 0.5560 0.5560 2.2829 Dunnett critical value = 2.4100 (1 Tailed, alpha = 0.05, df = 5,18) Title: laurinburg File: laurinburg Transform: NO TRANSFORMATION Dunnett's Test - TABLE 2 OF 2 Ho:Control<Treatment NUM OF MIN SIG DIFF % OF DIFFERENCE GROUP IDENTIFICATION REPS (IN ORIG. UNITS) CONTROL FROM CONTROL 1 control 4 2 7.75 4 0.0773 12.3 0.0508 3 15.5 4 0.0773 12.3 0.0840 4 31 4 0.0773 12.3 0.0395' 5 62 4 0.0773 12.3 0.0280 6 100 4 0.0773 12.3 0.0733 Title: laurinburg - survival File: laurinsurviv Transform: NO TRANSFORMATION Shapiro - Wilk's Test for Normality D= W= 0.0200 0.7552 Critical W = 0.8840 (alpha = 0.01 , N = 24) W = 0.9160 (alpha = 0.05 , N = 24) Data FAIL normality test (alpha = 0.01). Try another transformation. Warning - The first three homogeneity tests are sensitive to non -normality and should not be performed with this data as is. Title: laurinburg - survival File: laurinsurviv Transform: NO TRANSFORMATION Hartley's Test for Homogeneity of Variance Bartlett's Test for Homogeneity of Variance These two tests can not be performed because at least one group has zero variance. Data FAIL to meet homogeneity of variance assumption. Additional transformations are useless. Title: laurinburg - survival File: laurinsurviv Transform: NO TRANSFORMATION Steel's Many -One Rank Test Ho: Control<Treatment MEAN IN RANK CRIT. SIG GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05 1control 1.0000 2 7.75 1.0000 18.00 10.00 4.00 3 15.5 1.0000 18.00 10.00 4.00 4 31 0.9500 14.00 10.00 4.00 5 62 0.9500 14.00 10.00 4.00 6 100 1.0000 18.00 10.00 4.00 Critical values are 1 tailed ( k = 5 ) MERITECH, INC. Meritech Sample ID #: Bioassay Sample Chain of Custody 642 Tamco Rd,;Reidsville NC 27320 Phone: 1-336-342-4748 Fax: 1-336-342-1522 Email: txmrtech anbellsouth.net Web Site: www.meritech-labs.com -141-117' 7 CLIENT INFORMATION Client: i %7' _JrI �r' �r 1 /z94 -7 / Contact Person: J_64? r / • S Address: e?,i'. L (/ City: County: S <- J 7r fe.: PO#: NPDES#: NC s Phone: 5% t/ /2 " Pipe #:a State: // - <. Zip: ' 3S Sample Site: Sample Type: ❑ Grab a Composite # of containers: y _r SAMPLE INFORMATION Sampling Time: Start Date: 2,.2; J 9 Start Time: 4M PM End Date: G/ 3/1 7 End Time: /J)) S `AM__� PM —► CHRONIC TESTS SHOULD BE TAKEN AFTER 10:00 AM IF AT ALL POSSIBLE *** SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND CO E WIT E k** Collector's Name: Print: C Z:),0,/7' \ Signature: d- _'. ...,.._TOXICITY TEST INFORMATION Test Required: ❑ Chronic (7 days) Test Organism: ❑ Ceriodaphnia dubia {water flea) Comments: ❑ Acute (24-48 hours) ❑ Pimephales pronielas (fathead minnow) ❑ Mysidopsis bahia (shrimp) IWC: . % Test Concentrations (if multiple dilutions): SHIPPING INFORMATION Relinquished by: Date: Time: AM _ PM r. . Received by: :'' `�;;,�- �h • ��-aK.t-._ Date: a ; Time: ` 7/ - EAM' PM Relinquished by:t •; ,,,�a ., L-�� h�- Date: Time: AM PM , -'. Received by: . Date: Time: AM PM Sample Temperature (°C): Method of Shipment: El UPS ❑ Fed EX ❑ Meritech Pick-up - ** Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ** SAMPLE RECEIVING (Laboratory Use Only) Relinquished by: Received by: Date: Time: AM PM Sample Temperatures (°C): / / I Sample Condition: WHITE = Laboratory copy YELLOW = Client copy MERITECH, INC. Meritech Sample ID tt: Bioassay Sample Chain of Custody 642 Tamco Rd, Reidsville NC 27320 Phone: 1-336-342-4748 Fax: 1-336-342-1522 Email: txmrtech(@bellsouth.net Web Site: www.meritech-labs.com CLIENT INFORMATION ,. Client: f A-4,0/14 A.--f 12 r Contact Person: ‘, Address: (.-1) C-7/ City: PO#: NPDES#: NC Phone: 9'lb ‘1P /-1 Pipe #: Z") County: State: /kJ Zip: Sample Site: r . f SAMPLE INFORMATION Sampling Time: Start Date: Sample Type: 0 Grab Composite cy5 # of containers: Start Time.: 4tvV PM End Date: a/ ‘4/1-"' /0 AS 7Thp End Time: / • LAM, M CHRONIC TESTS SHOULD BE TAKEN AFTER 10:00 AM IF AT ALL POSSIBLE **" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no airspace), CHILLED AND7ERED,1.TH ICE *** Collector's Name: Print: /Sri ky Signature: TOXICITY TEST INFORMATION Test Required: CI Chronic (7 days) Test Organism: El Ceriodaphnia dubia (water flea) . . , Comments: LI Acute (24-48 hours) I WC El Pimephales pronielas (fathead minnow) CI Mysidopsis bahia (shrimp) Test Concentrations (if multiple dilutions): SHIPPING INFORMATION Relinquished by: Date: Time: AM PM Received by: Date: Time: IANk PM Relinquished by: :- ..,k \ _,...,..j„..;, .... Date: Tin AM PM := • - Received by: — Date: Time: AM PM / . • / , / ----- ' 1.". Sample Temperature (°C): • Method of Shipment: CI UPS 0 Fed EX 111 Meritech Pick-up A.7. " Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ** SAMPLE RECEIVING (Laboratory Use Only) Relinquislid by: Received by: Date: Time: • f\ AM PM Sample Temperatures (°C): I I I Sample Condition: WHITE = Laboratory copy YELLOW = Client copy