WQ0040265_More Information Received_20210916

Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?*
Permit Number (IR)*
Applicant/Permittee
Email Notifications
Does this need review by the hydrogeologist?*
Regional Office
CO Reviewer
Admin Reviewer
Annual Report
Residual Annual Report
r Additional Information
r Other
WQ0040265
City of Durham
r Yes r No

Submittal Form
Project Contact Information
Rease provide infornation on the person to be contacted by N B Staff
Name * Jorge Luis Montezuma
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
c Additional Information
r Other
Phone Number*
8643450190
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00040265
Fbs Current Existing permt number
Applicant/Permittee Address* 101 City Hall Plaza, Durha„ NC 27701, Att'n: Wayne Fenton
Facility Name * North Durham Composting DCAR
Please provide comments/notes on your current submittal below.
2020 laboratory analytical results for Brown WTP residuals.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
Brown WTP 2020 - Lab Analyticals.pdf 3.3MB
Upload only 1 PCFdocurrent (less than 250 fvB). Miltiple documents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
�rf� ��fC�tdiA'1E
Submission Date 9/17/2021

SummitEnvironmentalTechnologies,Inc.
3310 WinSt.
CuyahogaFalls,Ohio44223
TEL:[phone]FAX:[phone]
Website:http://www.settek.com
May 06, 2020
RyanCopeland
Synagro
284BogerRd.
Mocksville,NC 27028
TEL:[phone]
FAX:
[phone]
RE:
DurhamBrown
OrderNo.:20041280
DearRyanCopeland:
Summit EnvironmentalTechnologies,Inc.received 1 sample(s) on 4/24/2020forthe
analyses presentedinthefollowingreport.
Therewere no problemswiththeanalyticaleventsassociatedwiththisreport unless noted
intheCaseNarrative.
Qualitycontrol dataiswithinlaboratory definedormethod specifiedacceptancelimits
exceptwhere noted.
Ifyou haveany questionsregardingthesetestsresults, pleasefeelfreetocallthe
laboratory.
Sincerely,
Jennifer Woolf
ProjectManager
3310 Win St.
Cuyahoga Falls,Ohio44223
Arkansas88-0735,California2943,Colorado,ConnecticutPH-0108,FloridaNELACE87688,IdahoOH00923,Illinois200061,IndianaC-OH-13,Kansas
E-10347,Kentucky(UndergroundStorageTank)3,Kentucky90146, Maryland339,Michigan9988, Minnesota1780279,NevadaOH009232020-1,New
Hampshire2996,New JerseyOH006,NewYork11777,NorthCarolina39705and631,NorthDakotaR-201,OhioDW,OhioVAPCL0052,Oklahoma
2019-155,OregonOH200001,Pennsylvania011,RhodeIslandLA000317,SouthCarolina92016001,TexasT104704466-19-16,UtahOH009232020-12,
VirginiaVELAP10381,WestVirginia9957C
Page 1 of 31

SummitEnvironmentalTechnologies,Inc.
CaseNarrative
3310 WinSt.
CuyahogaFalls,Ohio44223
WO#:
20041280
TEL:[phone]FAX:[phone]
Date:
5/6/2020
Website:http://www.settek.com
CLIENT:Synagro
Project:DurhamBrown
Thisreportinitsentiretyconsists ofthefollowingdocuments:CoverLetter,CaseNarrative,Analytical
Results,QCSummaryReport,ApplicableAccreditationInformation,Chain-of-Custody,Cooler
ReceiptForm,and otherapplicableformsas necessary.All documentscontaintheSummit
Environmental Technologies,Inc.,WorkOrderNumberassignedtothisreport.
Summit Environmental Technologies,Inc., holdstheaccreditations/certificationslistedatthe bottomof
thecoverletterthatmay ormaynot pertaintothisreport.Pleaserefertothe"AccreditationProgram
AnalytesReport"foraccreditedanalyteslist.
Theinformationcontainedinthisanalyticalreportisthesole property ofSummitEnvironmental
Technologies,Inc.andthat ofthecustomer.Itcannot bereproducedinanyformwithouttheconsent of
Summit Environmental Technologies,Inc. orthecustomerforwhichthisreportwasissued. Theresults
containedinthisreportare onlyrepresentative ofthesamplesreceived.Conditionscan varyat different
timesandat different samplingconditions.SummitEnvironmental Technologies,Inc.is notresponsible
for useorinterpretation ofthe dataincluded herein.
AllresultsforSolidSamplesarereported on an"asreceived" or"wetweight" basis unlessindicatedas
"dryweight" usingthe"-dry" designation on thereportingunits.
Thisreportis believedtomeetall oftherequirements oftheaccreditingagency,whereapplicable.Any
comments or problemswiththeanalyticaleventsassociatedwiththisreportare noted below.
PrepCommentsforHGPrep_(7470),Samplemb2-43232: 22.5 ml ofKMnO4added.
Original
Page 2 of 31

SummitEnvironmentalTechnologies,Inc.
QualifiersandAcronyms
3310 WinSt.
CuyahogaFalls,Ohio44223
WO#:
20041280
TEL:[phone]FAX:[phone]
Date:
5/6/2020
Website:http://www.settek.com
ThesecommonlyusedQualifiersandAcronymsmayormaynotbepresentinthis report.
Qualifiers
Thecompoundwasanalyzedforbutwasnotdetected.
U
ThereportedvalueisgreaterthantheMethodDetectionLimitbutlessthantheReportingLimit.
J
HTheholdtimeforsamplepreparationand/oranalysiswasexceeded.
Theresultisreportedfromadilution.
D
Theresultexceededthelinearrangeofthecalibrationorisestimatedduetointerference.
E
Theresultisbelowthe MinimumCompound Limit.
MC
*TheresultexceedstheRegulatoryLimitorMaximumContaminationLimit.
Manualintegrationwasusedtodeterminethearearesponse.
m
Manualintegrationinwhichpeakwasdeleted
d
TheresultispresumptivebasedonaMassSpectrallibrarysearchassuminga1:1response.
N
PThesecondcolumnconfirmationexceeded25%difference.
TheresulthasbeenconfirmedbyGC/MS.
C
TheresultwasnotconfirmedwhenGC/MSAnalysiswasperformed.
X
Theanalytewasdetectedintheassociatedblank.
B/MB+
GTheICBorCCBcontainedreportableamountsofanalyte.
TheCCVrecoveryfailedlow(-)orhigh(+).
QC-/+
TheRPDwasoutsideofacceptedrecoverylimits.
R/QDR
TheLCSorLCSDrecoveryfailedlow(-)orhigh(+).
QL-/+
QLRTheLCS/LCSDRPDwasoutsideofacceptedrecoverylimits.
TheMSorMSDrecoveryfailedlow(-)orhigh(+).
QM-/+
TheMS/MSDRPDwasoutsideofacceptedrecoverylimits.
QMR
TheICVrecoveryfailedlow(-)orhigh(+).
QV-/+
SThespikeresultwasoutsideofacceptedrecoverylimits.
Deviation;Adeviationfromthemethodwasperformed; PleaserefertotheCaseNarrativefor
Z
additionalinformation
Acronyms
NDNotDetectedRLReportingLimit
QualityControlMethodDetectionLimit
QCMDL
MBMethodBlankLODLevelofDetection
LaboratoryControl SampleLevelofQuantitation
LCSLOQ
LaboratoryControl SampleDuplicatePracticalQuantitationLimit
LCSDPQL
QualityControl SampleContractRequiredQuantitationLimit
QCSCRQL
DUPDuplicatePLPermitLimit
Matrix SpikeRegulatoryLimit
MSRegLvl
Matrix SpikeDuplicateMaximumContaminationLimit
MSDMCL
RelativePercentDifferentMinimumCompoundLimit
RPDMinCL
InitialCalibrationVerificationReanalysis
ICVRA
ICBInitialCalibrationBlankREReextraction
ContinuingCalibrationVerificationTentativelyIdentifiedCompound
CCVTIC
CCBContinuingCalibrationBlankRTRetentionTime
ReportingLimitCheckCalibration Factor
RLCCF
DilutionFactorResponseFactor
DFRF
ThislistofQualifiersandAcronymsreflects themostcommonlyutilizedQualifiersandAcronyms forreporting.
Pleasereferto theAnalyticalNotesintheCaseNarrative foranyQualifiersorAcronymsthatdonotappearin this
list orforadditionalinformationregarding theuseof theseQualifiersonreporteddata.
Original
Page 3 of 31

SummitEnvironmentalTechnologies,Inc.
Workorder
3310 WinSt.
SampleSummary
CuyahogaFalls,Ohio44223
TEL:[phone]FAX:[phone]
WO#:
20041280
Website:http://www.settek.com
06-May-20
CLIENT:Synagro
Project:DurhamBrown
TagNo
Lab SampleIDClient SampleIDDateCollectedDateReceivedMatrix
20041280-001Durham BrownWTP4/23/202011:30:00AM4/24/202010:10:00AMSludge
Page 4 of 31

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SummitEnvironmentalTechnologies,Inc.
AnalyticalReport
3310 WinSt.
(basereport)
CuyahogaFalls,Ohio44223
WO#:
20041280
TEL:[phone]FAX:[phone]
Website:http://www.settek.com
DateReported:
5/6/2020
TagNumber:
CLIENT:Synagro
CollectionDate:4/23/202011:30:00AM
Matrix:SLUDGE
LabID:20041280-001A
Project:DurhamBrown
ClientSampleIDDurhamBrownWTP
AnalysesResultQualUnitsDFDateAnalyzed
RL
Analyst:
TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW7470ASW7470AMJM
TCLPMERCURYANALYSIS (SW1311/7470)
TCLPMercuryND0.00200mg/L15/1/20201:07:00 PM
Analyst:
TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW6010DEAM
TCLPMETALSANALYSIS (SW1311/6010)
TCLP Arsenic(As)ND0.500mg/L15/1/20201:31:46 PM
TCLP Barium(Ba)ND5.00mg/L15/1/20201:31:46 PM
TCLPCadmium(Cd)ND0.100mg/L15/1/20201:31:46 PM
TCLPChromium(Cr)ND0.200mg/L15/1/20201:31:46 PM
TCLPLead(Pb)ND0.500mg/L15/1/20201:31:46 PM
TCLP Selenium(Se)ND0.0500mg/L15/1/20201:31:46 PM
TCLP Silver(Ag)ND0.500mg/L15/1/20202:49:45 PM
Analyst:
TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW8270SW3510CSFG
TCLPSEMI-VOLATILESANALYSIS(SW1311/8270)
1,4-DichlorobenzeneND0.200mg/L25/4/20203:38:00 PM
2,4,5-TrichlorophenolND0.500mg/L25/4/20203:38:00 PM
2,4,6-TrichlorophenolND0.500mg/L25/4/20203:38:00 PM
2,4-DinitrotolueneND0.100mg/L25/4/20203:38:00 PM
Cresols,TotalND10.0mg/L25/4/20203:38:00 PM
Hexachloro-1,3-butadieneND0.0400mg/L25/4/20203:38:00 PM
HexachlorobenzeneND0.100mg/L25/4/20203:38:00 PM
HexachloroethaneND0.200mg/L25/4/20203:38:00 PM
NitrobenzeneND0.200mg/L25/4/20203:38:00 PM
PentachlorophenolND0.500mg/L25/4/20203:38:00 PM
PyridineND0.500mg/L25/4/20203:38:00 PM
Surr:2-Fluorophenol85.610-109%Rec25/4/20203:38:00 PM
Surr: Phenol-d685.210-109%Rec25/4/20203:38:00 PM
Surr:Nitrobenzene-d572.719-120%Rec25/4/20203:38:00 PM
Surr:2,4,6-Tribromophenol11610-120%Rec25/4/20203:38:00 PM
Surr:2-Fluorobiphenyl86.122-117%Rec25/4/20203:38:00 PM
Surr:p-Terphenyl-d1412334-116S%Rec25/4/20203:38:00 PM
BAnalytedetectedinthe associatedMethod BlankEValue abovequantitationrange
Qualifiers:
HHolding timesforpreparationor analysisexceededMManualIntegrationusedtodetermine arearesponse
MCValue isbelowMinimum CompoundLimit.NTentatively identified compounds
NDNotDetectedPSecond column confirmation exceeds
PLPermitLimitRRPDoutside acceptedrecoverylimits
Original
RLReportingDetectionLimitUSampleswith CalcVal<MDL
Page 6 of 31

SummitEnvironmentalTechnologies,Inc.
AnalyticalReport
3310 WinSt.
(basereport)
CuyahogaFalls,Ohio44223
WO#:
20041280
TEL:[phone]FAX:[phone]
Website:http://www.settek.com
DateReported:
5/6/2020
TagNumber:
CLIENT:Synagro
CollectionDate:4/23/202011:30:00AM
Matrix:SLUDGE
LabID:20041280-001A
Project:DurhamBrown
ClientSampleIDDurhamBrownWTP
AnalysesResultQualUnitsDFDateAnalyzed
RL
Analyst:
TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW8081SW3510CMES
TCLPPESTICIDESANALYSIS(SW1311/8081)
Chlordane, totalND0.125mg/L55/4/20207:27:00 PM
ToxapheneND0.250mg/L55/4/20207:27:00 PM
EndrinND0.0125mg/L55/4/20207:27:00 PM
gamma-BHCND0.0125mg/L55/4/20207:27:00 PM
HeptachlorND0.0125mg/L55/4/20207:27:00 PM
HeptachlorepoxideND0.0125mg/L55/4/20207:27:00 PM
MethoxychlorND0.0125dmg/L55/4/20207:27:00 PM
Surr:TCMX19.610-119%Rec55/4/20207:27:00 PM
Surr:DCB18.210-119%Rec55/4/20207:27:00 PM
Analyst:
TCLPHERBICIDES BY EPA8321BSW8321ASW1311MBJH
2,4-DND0.500mg/L505/2/20206:32:00 AM
2,4,5-TPND0.500mg/L505/2/20206:32:00 AM
Surr:2,4-Dichlorophenylaceticacid10570-130%Rec505/2/20206:32:00 AM
Analyst:
TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW8260SW1311MRMT
TCLPVOLATILESANALYSIS
1,1-DichloroetheneND0.250mg/L504/30/20201:09:00 PM
1,2-DichloroethaneND0.250mg/L504/30/20201:09:00 PM
MEKND5.00mg/L504/30/20201:09:00 PM
BenzeneND0.250mg/L504/30/20201:09:00 PM
Carbon tetrachlorideND0.250mg/L504/30/20201:09:00 PM
ChlorobenzeneND2.50mg/L504/30/20201:09:00 PM
ChloroformND0.250mg/L504/30/20201:09:00 PM
TetrachloroetheneND0.250mg/L504/30/20201:09:00 PM
TrichloroetheneND0.250mg/L504/30/20201:09:00 PM
VinylchlorideND0.100mg/L504/30/20201:09:00 PM
Surr:4-Bromofluorobenzene91.270-130%Rec504/30/20201:09:00 PM
Surr:Dibromofluoromethane10270-130%Rec504/30/20201:09:00 PM
Surr:Toluene-d899.970-130%Rec504/30/20201:09:00 PM
BAnalytedetectedinthe associatedMethod BlankEValue abovequantitationrange
Qualifiers:
HHolding timesforpreparationor analysisexceededMManualIntegrationusedtodetermine arearesponse
MCValue isbelowMinimum CompoundLimit.NTentatively identified compounds
NDNotDetectedPSecond column confirmation exceeds
PLPermitLimitRRPDoutside acceptedrecoverylimits
Original
RLReportingDetectionLimitUSampleswith CalcVal<MDL
Page 7 of 31

SummitEnvironmentalTechnologies,Inc.
AnalyticalReport
3310 WinSt.
(basereport)
CuyahogaFalls,Ohio44223
WO#:
20041280
TEL:[phone]FAX:[phone]
Website:http://www.settek.com
DateReported:
5/6/2020
TagNumber:
CLIENT:Synagro
CollectionDate:4/23/202011:30:00AM
Matrix:SLUDGE
LabID:20041280-001A
Project:DurhamBrown
ClientSampleIDDurhamBrownWTP
AnalysesResultQualUnitsDFDateAnalyzed
RL
Analyst:
RCI-SOLID-W/ IGNITABILITY1030SW9014MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide,ReactiveND0.490mg/Kg14/27/20209:09:00 AM
Analyst:
PAINTFILTERFREELIQUIDSTEST (SW-846:9095)SW9095DHC
FreeLiquidpass14/29/20208:30:00 AM
Analyst:
RCI-SOLID-W/ IGNITABILITY1030SW1030AJT
IGNITABILITYOF SOLIDS (SW-846:1030)
Ignitabilitynon-flammablemm/sec15/1/20203:00:00 PM
Analyst:
RCI-SOLID-W/ IGNITABILITY1030SW9045DDHC
PH (SW9045D)
pH6.1s.u.@21.9C14/30/202010:07:00 AM
Analyst:
RCI-SOLID-W/ IGNITABILITY1030SW9034MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide,ReactiveND25.0mg/Kg14/27/20209:09:00 AM
BAnalytedetectedinthe associatedMethod BlankEValue abovequantitationrange
Qualifiers:
HHolding timesforpreparationor analysisexceededMManualIntegrationusedtodetermine arearesponse
MCValue isbelowMinimum CompoundLimit.NTentatively identified compounds
NDNotDetectedPSecond column confirmation exceeds
PLPermitLimitRRPDoutside acceptedrecoverylimits
Original
RLReportingDetectionLimitUSampleswith CalcVal<MDL
Page 8 of 31

SummitEnvironmentalTechnologies,Inc.
AccreditationProgram
3310 WinSt.
AnalytesReport
CuyahogaFalls,Ohio44223
TEL:[phone]FAX:[phone]
WO#:
20041280
Website:http://www.settek.com
06-May-20
Client:SynagroState:NW
Project:DurhamBrownProgramName:NC_WW_SCM
SampleIDMatrixTestNameAnalyteStatus
SludgeIgnitabilityofSolids(SW-846:1030)IgnitabilityA
20041280-001A
SludgePaintFilterFreeLiquidsTest(SW-846:9095)FreeLiquidN
SludgepH(SW9045D)HydrogenIon(pH)A
SludgeReactive Cyanide(9014/7.3.3.2)-SolidCyanide, ReactiveN
SludgeReactiveSulfide(9034)/7.3.4.2Sulfide, ReactiveN
SludgeTCLPHerbicidesbyEPA8321B2,4,5-TPA
SludgeTCLPHerbicidesbyEPA8321B2,4-DA
SludgeTCLPMercuryAnalysis(SW1311/7470)MercuryA
SludgeTCLPMetalsAnalysis(SW1311/6010)ArsenicA
SludgeTCLPMetalsAnalysis(SW1311/6010)BariumA
SludgeTCLPMetalsAnalysis(SW1311/6010)CadmiumA
SludgeTCLPMetalsAnalysis(SW1311/6010)ChromiumA
SludgeTCLPMetalsAnalysis(SW1311/6010)LeadA
SludgeTCLPMetalsAnalysis(SW1311/6010)SeleniumA
SludgeTCLPMetalsAnalysis(SW1311/6010)SilverA
SludgeTCLPPesticidesAnalysis(SW1311/8081)Chlordane, totalA
SludgeTCLPPesticidesAnalysis(SW1311/8081)EndrinA
SludgeTCLPPesticidesAnalysis(SW1311/8081)gamma-BHCA
SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorA
SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorepoxideA
SludgeTCLPPesticidesAnalysis(SW1311/8081)MethoxychlorA
SludgeTCLPPesticidesAnalysis(SW1311/8081)ToxapheneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)1,4-DichlorobenzeneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,5-TrichlorophenolA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,6-TrichlorophenolA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4-DinitrotolueneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)Cresols,TotalA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobenzeneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobutadieneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachloroethaneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)NitrobenzeneA
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PentachlorophenolA
KeyKey
NC_WW_SCMAAccreditedNC_WW_SCMNNotAccredited
Original#1
Page 9 of 31

SummitEnvironmentalTechnologies,Inc.
AccreditationProgram
3310 WinSt.
AnalytesReport
CuyahogaFalls,Ohio44223
TEL:[phone]FAX:[phone]
WO#:
20041280
Website:http://www.settek.com
06-May-20
Client:SynagroState:NW
Project:DurhamBrownProgramName:NC_WW_SCM
SampleIDMatrixTestNameAnalyteStatus
SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PyridineA
20041280-001A
SludgeTCLPVolatilesAnalysis1,1-DichloroetheneA
SludgeTCLPVolatilesAnalysis1,2-DichloroethaneA
SludgeTCLPVolatilesAnalysis2-ButanoneA
SludgeTCLPVolatilesAnalysisBenzeneA
SludgeTCLPVolatilesAnalysisCarbon tetrachlorideA
SludgeTCLPVolatilesAnalysisChlorobenzeneA
SludgeTCLPVolatilesAnalysisChloroformA
SludgeTCLPVolatilesAnalysisTetrachloroetheneA
SludgeTCLPVolatilesAnalysisTrichloroetheneA
SludgeTCLPVolatilesAnalysisVinyl chlorideA
KeyKey
NC_WW_SCMAAccreditedNC_WW_SCMNNotAccredited
Original#1
Page 10 of 31

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Page 30 of 31

SummitEnvironmentalTechnologies,Inc.
3310 WinSt.
CuyahogaFalls,Ohio44223
SampleLog-InCheckList
TEL:[phone]FAX:[phone]
Website:http://www.settek.com
ClientName:WorkOrderNumber:RcptNo:
SYN-NC-27028200412801
Loggedby:4/24/202010:10:00AM
JacquelineRasile
Completed By:4/24/20202:34:37PM
JacquelineRasile
Reviewed By:4/24/20203:54:08PM
Sara E. Kidd
Chainof Custody
IsChainofCustody complete?YesNoNot Present
1.
Howwas the sampledelivered?
UPS
2.
LogIn
Coolersarepresent?YesNoNA
3.
Shipping container/cooleringood condition?YesNo
4.
Custody sealsintactonshipping container/cooler?YesNoNot Present
No.Seal Date:SignedBy:
Wasanattemptmadetocool the samples?YesNoNA
5.
Wereall samplesreceivedata temperatureof>0°Cto6.0°CYesNoNA
6.
Sample(s)inpropercontainer(s)?YesNo
7.
Sufficient samplevolumeforindicated test(s)?YesNo
8.
Are samples(exceptVOAandONG)properlypreserved?YesNo
9.
Waspreservativeaddedtobottles?YesNoNA
10.
Is theheadspaceintheVOAvialsless than1/4inchor6mm?YesNoNo VOA Vials
11.
Wereany sample containersreceivedbroken?YesNo
12.
Doespaperworkmatchbottlelabels?YesNo
13.
(Notediscrepancieson chainof custody)
Arematrices correctlyidentifiedonChainofCustody?YesNo
14.
Isit clearwhatanalyseswererequested?YesNo
15.
Wereallholding timesable tobemet?YesNo
16.
(Ifno,notifycustomer forauthorization.)
Special Handling(ifapplicable)
Was clientnotifiedofalldiscrepancieswith thisorder?YesNoNA
17.
PersonNotified:
Date:
ByWhom:Via:eMailPhoneFaxInPerson
Regarding:
Client Instructions:
Additionalremarks:
18.
Cooler Information
CoolerNoTempºCConditionSealIntactSeal NoSeal DateSigned By
11.4GoodNot Present
Page 31 of 31

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Page 1 of 7

Page 2 of 7

Client:SynagroLaboratory ID:VG31065-001
Description:DURHAM BROWNMatrix:Solid
Date Sampled:07/30/2020 0910% Solids:20.1 08/01/2020 2011
Date Received:07/31/2020
Inorganic non-metals
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
1(% Solids) SM 2540G108/01/2020 2011SRB62017
1350.1(Ammonia - N ) 350.1108/06/2020 1649DMA62563
1(Nitrate - N ) 9056A108/05/2020 1459AMR62554
1(Nitrite - N ) 9056A108/05/2020 1459AMR62552
1(Phosphorus) 365.1208/05/2020 0855DMA08/04/2020 125862258
1(Soil pH meas) 9045D108/07/2020 2327SRB62831
1351.4(TKN) 351.2108/05/2020 1718DMA08/05/2020 100562372
CASAnalytical
ParameterNumberMethodResultQLOQ DLUnitsRun
% SolidsSM 2540G20.1%1
Ammonia - N (gas diffusion)350.1395.0mg/kg1
2.6
Nitrate - N (soluble)9056A2.0J2.5mg/kg1
0.50
Nitrite - N (soluble)9056AND0.99mg/kg1
0.50
Phosphorus7723-14-0365.163050mg/kg1
9.9
Soil pH measured in water @ 21.3 ° C9045D5.2su1
TKN351.210000120120mg/kg1
CVAA
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
17471B7471B508/05/2020 0857JAB208/01/2020 164162042
CAS
Analytical
ParameterNumberMethodResultQLOQ DLUnitsRun
Mercury7439-97-67471BND1.9mg/kg1
0.46
ICP-AES
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
13050B6010D108/05/2020 1635KSH208/04/2020 142262041
23050B6010D1008/06/2020 1324KSH208/04/2020 142262041
CAS
Analytical
ParameterNumberMethodResultQLOQ DLUnitsRun
Aluminum7429-90-56010D1000032mg/kg1
12
Arsenic7440-38-26010D1412mg/kg2
3.9
Cadmium7440-43-96010DND3.9mg/kg2
0.99
Calcium7440-70-26010D1100390mg/kg1
49
Chromium7440-47-36010D200.79mg/kg1
0.20
Copper7440-50-86010D21000.79mg/kg1
0.35
Iron7439-89-66010D32000079mg/kg2
36
Lead7439-92-16010D9.17.9mg/kg2
3.5
Magnesium7439-95-46010D270J390mg/kg1
49
Manganese7439-96-56010D750012mg/kg2
4.7
Molybdenum7439-98-76010DND3.2mg/kg1
0.79
LOQ = Limit of QuantitationB = Detected in the method blankE = Quantitation of compound exceeded the calibration rangeDL = Detection Limit
ND = Not detected at or above the DLN = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%J = Estimated result < LOQ and > DL_
H = Out of holding timeW = Reported on wet weight basis
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:SynagroLaboratory ID:VG31065-001
Description:DURHAM BROWNMatrix:Solid
Date Sampled:07/30/2020 0910% Solids:20.1 08/01/2020 2011
Date Received:07/31/2020
ICP-AES
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
13050B6010D108/05/2020 1635KSH208/04/2020 142262041
23050B6010D1008/06/2020 1324KSH208/04/2020 142262041
CASAnalytical
ParameterNumberMethodResultQLOQ DLUnitsRun
Nickel7440-02-06010D5332mg/kg2
8.3
Potassium7440-09-76010D340J390mg/kg1
49
Selenium7782-49-26010D6.5J16mg/kg2
6.4
Sodium7440-23-56010D200J390mg/kg1
49
Zinc7440-66-66010D583.9mg/kg1
0.98
LOQ = Limit of QuantitationB = Detected in the method blankE = Quantitation of compound exceeded the calibration rangeDL = Detection Limit
ND = Not detected at or above the DLN = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%J = Estimated result < LOQ and > DL_
H = Out of holding timeW = Reported on wet weight basis
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC

Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC

Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Page 1 of 7

Page 2 of 7

Client:SynagroLaboratory ID:VJ16007-001
Description:DURHAM BROWNMatrix:Solid
Date Sampled:10/14/2020 0912% Solids:23.1 10/17/2020 0144
Date Received:10/15/2020
Inorganic non-metals
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
1(% Solids) SM 2540G110/17/2020 0144LSH70234
1350.1(Ammonia - N ) 350.1110/19/2020 1658DRD70365
1(Nitrate - N ) 9056A110/21/2020 2048AMR70656
1(Nitrite - N ) 9056A110/21/2020 2048AMR70657
1(Phosphorus) 365.1510/20/2020 1735DMA10/20/2020 130070385
1(Soil pH meas) 9045D110/20/2020 2240AAB70569
2351.4(TKN) 351.2110/21/2020 1736DMA10/21/2020 120170594
CASAnalytical
ParameterNumberMethodResultQLOQ DLUnitsRun
% SolidsSM 2540G23.1%1
Ammonia - N (gas diffusion)350.11804.3mg/kg1
2.3
Nitrate - N (soluble)9056A1.9J2.2mg/kg1
0.43
Nitrite - N (soluble)9056A0.47J0.87mg/kg1
0.43
Phosphorus7723-14-0365.1690110mg/kg1
22
Soil pH measured in water @ 19.4 ° C9045D5.5su1
TKN351.26000110110mg/kg2
CVAA
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
17471B7471B110/20/2020 1345JAB210/20/2020 091070438
CAS
Analytical
ParameterNumberMethodResultQLOQ DLUnitsRun
Mercury7439-97-67471BND0.34mg/kg1
0.083
ICP-AES
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
13050B6010D110/22/2020 0135KSH210/17/2020 151870258
23050B6010D510/22/2020 1410KSH210/17/2020 151870258
43050B6010D2510/23/2020 1514KSH210/17/2020 151870258
CAS
Analytical
ParameterNumberMethodResultQLOQ DLUnitsRun
Aluminum7429-90-56010D740027mg/kg1
10
Arsenic7440-38-26010D7.11.0mg/kg1
0.33
Cadmium7440-43-96010DND0.33mg/kg1
0.084
Calcium7440-70-26010D940330mg/kg1
42
Chromium7440-47-36010D170.67mg/kg1
0.17
Copper7440-50-86010D11003.3mg/kg2
1.5
Iron7439-89-66010D390000170mg/kg4
76
Lead7439-92-16010D2.10.67mg/kg1
0.30
Magnesium7439-95-46010D200J330mg/kg1
42
Manganese7439-96-56010DND1.0mg/kg1
0.40
LOQ = Limit of QuantitationB = Detected in the method blankE = Quantitation of compound exceeded the calibration rangeDL = Detection Limit
ND = Not detected at or above the DLN = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%J = Estimated result < LOQ and > DL_
H = Out of holding timeW = Reported on wet weight basis
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:SynagroLaboratory ID:VJ16007-001
Description:DURHAM BROWNMatrix:Solid
Date Sampled:10/14/2020 0912% Solids:23.1 10/17/2020 0144
Date Received:10/15/2020
ICP-AES
RunPrep MethodAnalytical MethodDilutionAnalysis DateAnalystPrep DateBatch
13050B6010D110/22/2020 0135KSH210/17/2020 151870258
23050B6010D510/22/2020 1410KSH210/17/2020 151870258
43050B6010D2510/23/2020 1514KSH210/17/2020 151870258
CASAnalytical
ParameterNumberMethodResultQLOQ DLUnitsRun
Molybdenum7439-98-76010DND2.7mg/kg1
0.67
Nickel7440-02-06010D6413mg/kg2
3.5
Potassium7440-09-76010D220J330mg/kg1
42
Selenium7782-49-26010DND33mg/kg4
14
Sodium7440-23-56010D300J33042mg/kg1
Zinc7440-66-66010D1003.30.84mg/kg1
LOQ = Limit of QuantitationB = Detected in the method blankE = Quantitation of compound exceeded the calibration rangeDL = Detection Limit
ND = Not detected at or above the DLN = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%J = Estimated result < LOQ and > DL_
H = Out of holding timeW = Reported on wet weight basis
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC

Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC

Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7