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HomeMy WebLinkAboutNC0001899_permit issuance_19961112State of North Carolina Department of Environment, Health and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E., Director Mr. Bill Boyer AlliedSignal Inc P.O. Box 166 Moncure, North Carolina 27559 AVA I�EI-1NFt November 12, 1996 Subject Permit Issuance NPDES Permit NC0001899 AlliedSignal FIBERS Chatham County Dear Mr. Boyer: In accordance with your application for discharge permit received on September 29, 1995, we are forwarding herewith the subject State - NPDES permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated December 6, 1983. In response to Allied's draft permit comment letter dated October 25, 1996, the following modifications/comments are offered: • Instream Monitoring - The Division is aware of the accessibility issue for the downstream sampling point and encourages Allied Signal to work with the Raleigh Regional Office in finding a feasible point that is 100 yards or more below the discharge point and above the confluence of the Deep and'Haw Rivers. Instream monitoring requirements will take effect on May 1, 1997. • Reporting Upstream and Downstream Results - Forms for this purpose are attached. • Representative Sampling - Taking the sample for acute toxicity testing purposes from the effluent pipeline is acceptable. No additional language is needed in the permit. The following minor changes were also made to the draft permit: • Footnote for pH Monitoring - For outfall 001, part of the language from 40 CFR 401.17 regarding continuous pH monitoring has been added. • Footnote for OCPSF Parameters - In the last sentence, the word "After" has been changed to ..If If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to an adjudicative hearing upon written request within thirty (30) days following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina 27611-7447. Unless such demand is made, this decision shall be fmal and binding. P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper Please take notice this permit is not transferable. Part II, E.4. addresses the requirements to be followed in case of change in ownership or control of this discharge. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning this permit, please contact Mr. Dave Goodrich at telephone number 919/733-5083, ext. 517. Sincerely, Original Signed By David A. Goodrich A. Preston Howard, Jr., P.E. Enclosure cc: Central Files Mr. Roosevelt Childress, EPA Raleigh Regional Office, Water Quality Section Facility Assessment Unit Aquatic Survey & Toxicology Unit Technical Assistance & Certification Group Permits and Engineering Unit Permit No. NC0001899 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF WATER QUALITY PERMIT TO DISCHARGE WASTEWATER UNDER TH E NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, AlliedSignal, Inc is hereby authorized to discharge wastewater from a facility located at AlliedSignal FIBERS off of NCSR 1972 east of Haywood Chatham County to receiving waters designated as the Haw River (outfall 001), and an unnamed tributary to Shaddox Creek (outfall 002) in the Cape Fear River Basin in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV hereof. This permit shall become effective December 1, 1996 This permit and authorization to discharge shall expire at midnight on March 31, 2001 Signed this day November 12, 1996 Original Signed By David A. Goodrich A. Preston Howard, Jr., Director Division of Water Quality By Authority of the Environmental Management Commission Permit No. NC0001899 SUPPLEMENT TO PERMIT COVER SHEET AlliedSignal, Inc. is hereby authorized to: 1. Continue to operate the existing 0.244 MGD wastewater treatment facility consisting of an aeration basin, clarifier, sludge drying bed, chlorine gas chlorination, and chlorine contact chamber with discharge through outfall 001, and continue to discharge stormwater, condensate, and firepond overflow through outfall 002,1ocated at AlliedSignal FIBERS, off of NCSR 1972, east of Haywood, Chatham County (See Part III of this Permit), and 2. Discharge from said treatment works at the location specified on the attached map into the Haw River (outfall 001) and into an unnamed tributary to Shaddox Creek (outfall 002), both classified as Class WS-IV waters in the Cape Fear River Basin. 676 177 2'30" 7 9110 00D' , • • 5155 II NE 4674 675 j (MERRY OAKS, .475 �- Little Sha �- am---• � e chapel! 1 A. (). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL Permit No. NC0001899 During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from outfall(s) serial number 001. Such discharges shall be limited and monitored by the permittee as specified below: Effluent Characteristics Discharge Limitations Monitoring Requirements Lbs/day Units (specltvl Measurement Sample *Sample Mon. Avg, Daily Max Mon. Avg. Daily Max, frequency Type Location Flow 0.244 MGD Continuous Recorder I or E BOD, 5 Day, 20 °C 10.4 16.7 Weekly Composite E TSS 5.0 10.6 Weekly Composite E Oil and Grease 20.0 30.0 Weekly Grab E Total Nitrogen (NO2+NO3+TKN) Monthly Composite E Total Phosphorus Monthly Composite E Fecal Coliform (Geometric mean) 200 /100 mi 400 /100 ml Weekly Grab E Total Residual Chlorine Monthly Grab E Dissolved Oxygen Monthly Grab E,U,D Temperature Monthly Grab E,U,D Acute Toxicity** Quarterly Composite E * Sample locations: E - Effluent, I - Influent, U - Valve at Permittee's river water pump house, D - At the nearest accessible point at least 100 yards below the outfall and above the confluence of the Deep and Haw Rivers. Instream sampling will commence on May 1,1997. ** Acute Toxicity (Daphnid 48 hr) LC50 90%; January, April, July and October, See Part III, Condition E. The pH shall be monitored continuously at the effluent. In accordance with 40 CFR 401.17, the total time during which the pH values are allowed to be less than 6.0 standard units or greater than 9.0 standard units shall not exceed 7 hours and 26 minutes in any calendar month, and no individual excursion outside the 6.0 to 9.0 range shall exceed 60 minutes. There shall be no discharge of floating solids or visible foam in other than trace amounts. A. (). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL Permit No. NC0001899 During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from outfall(s) serial number 001. (Continued) Effluent Characteristics Conductivity Discharge Limitations Other Units {specifv) Mon. Avg, Daily Max Mon. Avg. Daily Max. Lbs/dav Monitoring Measurement Frequency Monthly Requirements Sam DI0 Ty DO Grab *Sample Location E,U,D A. (). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL Permit No. NC0001899 During the period beginning on the effective date of the permit and lasting until expiration, the Penmittee is authorized to discharge from outfall(s) serial number 002 (Stormwater, Condensate, and Firepond Overflow). Such discharges shall be limited and monitored by the permittee as specified below: Effluent Characteristics Discharge Limitations Monitoring Requirements Lbs/day Units (speclfvl Measurement Sample *Sample Mon. Avg, Daily Max Mon. Avg. Daily Max, Frequencv Zvpe Location. Flow Weekly Instantaneous E Temperature * * * ' Weekly Grab E Total Residual Chlorine*** Weekly Grab E Fluoride 1.8 mg/I Quarterly Composite E Zinc Quarterly Composite E Acute Toxicity**** • • * • Grab E THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER. * Sample Locations: E - Effluent ** The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than 2.8° C and in no case cause the ambient water temperature to exceed 32° C. *** Monitoring requirements only apply if chlorine is added to the cooling water. **** Acute Toxicity (Fathead Minnow 24 hr) Monitoring, Episodic, See Part III, Condition F. The permittee shall obtain authorization from the Division of Water Quality prior to utilizing any biocide in the cooling water (See Part III of this Permit). The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored weekly at the effluent by grab sample. There shall be no discharge of floating solids or visible foam in other than trace amounts. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL NC0001899 During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from outfall serial number 001. Such discharges shall be limited and monitored by the permittee as specified below: Effluent Characteristics Acenapthene Acrylonitrile Benzene Carbon Tetrachloride Chlorobenzene 1,2,4-Trichlorobenzene Hexachlorobenzene 1,2-Dichloroethane 1,1,1-Trichloroethane Hexachloroethane 1,1-Dichloroethane 1,1,2-Trichloroethane Chloroethane Chloroform 2-Chlorophenol 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethylene 1,2-trans-Dichloroethylene 2,4-Dichlorophenol 1,2-Dichloropropane 1,3-Dichloropropylene 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Ethylbenzene Fluoranthene Methylene Chloride Methyl Chloride Hexachlorobutadiene Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol 2,4-Dintrophenol 4,6-Dintro-o-cresol Phenol Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Mon. Avg lbs/day 0.001 0.005 0.002 0.001 0.001 0.003 0.300 0.003 0.001 0.001 0.001 0.001 0.005 0.001 0.002 0.004 0.002 0.001 0.001 0.001 0.002 0.008 0.001 0.001 0.006 0.013 0.002 0.001 0.002 0.004 0.001 0.001 0.001 0.002 0.004 0.004 0.004 0.001 0.005 0.001 0.004 0.001 Daily Max lbs/day 0.003 0.012 0.007 0.002 0.001 0.007 0.001 0.011 0.003 0.003 0.003 0.003 0.013 0.002 0.005 0.008 0.002 0.001 0.001 0.003 0.006 0.012 0.002 0.002 0.014 0.032 0.005 0.003 0.004 0.010 0.002 0.003 0.003 0.003 0.006 0.006 0.014 0.001 0.014 0.003 0.010 0.002 Measurement Sample *Sample Frequency+ Type Location Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Quarterly Grab E Effluent Characteristics Mon. Avg lbs/day Benzo(a)anthracene Benzo(a)pyrene 3,4-Benzofluoranthene Benzo(k)fluoranthene Chrysene Acenaphthylene Anthracene Fluorene Phenanthrene Pyrene Tetrachloroethylene Toluene Trichloroethylene Vinyl Chloride Dibenz (a,h) anthracene** Indeno (1,2,3-ed) pyrene** 0.001 0.001 0.001 0.440 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.005 Daily Max lbs/day 0.003 0.003 0.003 0.003 0.003 0.003 0.003 0.003 0.003 0.003 0.003 0.004 0.003 0.013 Measurement Sample *Sample Frequency+ Type Location Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E Grab E *Sample Location: E-Effluent ** Monitoring is necessary to determine the amount of total PAHs discharged. Total PAH's are comprised of Benzo(a)pyrene; 3,4-Benzofluoranthene; Benzo(a)anthracene; Benzo(k)fluoranthene, Chrysene, Dibenz (a,h) anthracene and Indeno (1,2,3-ed) pyrene. + Should any annual monitoring result in detection of any OCPSF parameters contained in 40 CFR 414 Subpart I (excluding metals), then quarterly monitoring will begin immediately for the detected parameter(s). If four consecutive quarterly samples resulting in non -detection are achieved, the monitoring frequency will revert to annually. Part DI Permit No. NC0001899 E. ACUTE TOXICITY PERMIT LIMIT (QRTRLY) The permittee shall conduct acute toxicity tests on a quarterly basis using protocols defined as definitive in E.P.A. Document 600/4-85/013 entitled "The Acute Toxicity of Effluents to Freshwater and Marine Organisms." The monitoring shall be performed as a Daphnia pulex or Ceriodaphnia 48 hour static test, using effluent collected as a 24 hour composite. The LC50 of this effluent using the previously stated methodology may at no time in any toxicity test be less than 90%. Effluent samples for self -monitoring purposes must be obtained during representative effluent discharge below all waste treatment. The first test will be performed after thirty days from the effective date of this permit during the months of January, April, July and October. The parameter code for this test if using Daphnia pulex is TAA3D. The parameter code for this test if using Ceriodaphnia is TAA3B. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1) for the month in which it was performed, using the appropriate parameter code. Additionally, DWQ Form AT-1 (original) is to be sent to the following address: Attention: Environmental Sciences Branch North Carolina Division of Water Quality 4401 Reedy Creek Road Raleigh, N.C. 27607 Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to quarterly in the months specified above. Should any test data from either these monitoring requirements or tests performed by the North Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute noncompliance with monitoring requirements. F. ACUTE TOXICITY MONITORING (EPISODIC) The permittee shall conduct FIVE acute toxicity tests using protocols defined as definitive in E.P.A. Document 600/4-85/013 entitled "The Acute Toxicity of Effluents to Freshwater and Marine Organisms." The monitoring shall be performed as a Fathead Minnow (Pimephales promelas) 24 hour static test, using effluent collected as a single grab sample. Effluent samples for self -monitoring purposes must be obtained below all waste treatment. Sampling and subsequent testing will occur during the first five discrete discharge events after the effective date of this permit. After monitoring of the first five toxicity tests, the permittee will conduct one test annually, with the annual period beginning in January of the next calendar year. The annual test requirement must be performed and reported by June 30. If no discharge occurs by June 30, notification must be made to the Division by this date. Toxicity testing will be performed on the next discharge event for the annual test requirement. The parameter code for this test is TAE6C. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Form (MR-1) for the month in which it was performed, using the appropriate parameter code. Additionally, DWQ Form AT-1 (original) is to be sent to the following address: Attention: Environmental Sciences Branch North Carolina Division of Water Quality 4401 Reedy Creek Road Raleigh, N.C. 27607 Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should any test data from either these monitoring requirements or tests performed by the North Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test. Failure to submit suitable test results will constitute noncompliance with monitoring requirements. G. Biocide Condition The permittee shall not use any biocides except those approved in conjunction with the permit application. The permittee shall notify the Director in writing not later than ninety (90) days prior to instituting use of any additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported to the Division of Water Quality. Such notification shall include completion of Biocide Worksheet Form 101 and a map locating the discharge point and receiving stream. H. After monitoring for a minimum of a three year period, upon written request, OCPSF monitoring data will be reviewed by the Division of Water Quality to determine if a reduction in monitoring frequency is warranted. Data submitted for review should be in a tabular format for the sampling period under consideration. I. When an approved analytical protocol with the appropriate minimum detection level is followed and a result of "non -detectable" or "below quantitation limit" is obtained, the permittee will be considered to be in compliance with the numerical permit limit for that pollutant. J. ALTERNATIVE TEST METHODS FOR OCPSF PARAMETERS The use of EPA test method 524.2 is allowed as a substitute for test methods in 40 CFR Part 136 to monitor OCPSF parameters. DIVISION OF ENVIRONMENTAL MANAGEMENT July 12, 1996 MEMORANDUM To: Jason Doll Rapid Assessment Group From: Greg NizichG5 �l ' NPDES Permits Group Subject: Updated Permit Limits Permit # NC0001899 Allied Signal Chatham County Allied Signal has completed sampling of their individual process and non -process wastestreams. Based on the information submitted, a process flow of 0.006 MGD was used in applying effluent guidelines. The following summarizes the proposed limits for this facility: Parameter Monthly Avg. Daily Max. (#/day) (#/day) BO D5 10.7 17.0 TSS 5.0 10.6 The most recent sampling information submitted by Allied Signal is attached. Attachment cc: Raleigh Regional Office, Water Quality SENT BY:ALLIED SIGNAL ; 7-10-96 ; 16:04 ; WAREHOUSE-, 919 733 0719;# 3/ 4 ATTACHMENT 1 AlliedSignal Inc. Moncure, North Carolina NPDES Permit No. NC0001809 PROCESS AND NON -PROCESS WASTEWATER MONITORING DATA Sample Date: 5/20/95 PROCESS RELATED SOURCES 1 ' : ; . . . . . . - - .:::::•••'..: r, '1':'.S.C::;,'-4,:- ''' ....'',....:,..:'1. __::::._•:,,,-::,,,f;F,':__'•;'?..:':'::::::!:•;...ii:?:•::::::',::;:'x.:::740. 1 t. t. SULTAKEJ,",::. 7:•::,::::' : ' ,..„‘,;:;z:, gseg . .6:1717AY -:.,..... ITOADINO-' : - '':.:F...:'• :fLBS/DATI • •„, ;:;•,.., ,,;;;; 7.5 0.07 BEAM CLEANIN(3 BOD TSS 4,086 37 0.15 220 UL'I'RAFILTRATION (H.00H UN1T) BOD TSS 10,000 13 0.87 1,248 104.1 0.14 KOLENE QUENCH BK111 BOD TSS 16,200 650 0.07 100 13.5 0.54 , DESCALING BATI3 BOD TSS 24.8 262 0.01 14 0,003 ° KOLEN F. RINSE (10/9/90 testing) BOD TSS 220 13 0.07 100 C0t.'0°13: TEO RINSE BOD TSS 164 29 0.12 170 0.23 0.04 PREPOLYMYR QUENCH Not sampled* 0011 110 --- COOLING TOWER BLOWDOWN (4 TOWERS) HOD TSS 188 46 31 44,640 70 -4.23 AIR CoMPRUSSORS (12 UNITS) i — BOD TSS 162 183 2.31 3,328.8 0.45 5.08 Comments: *Propolymer quench is a mate hatel up:union that occurs approximately 14 - 20 times per year. Prepolluner quench activity d10 not occur at the tittle uf sampling. SENT BY:ALLIED SIGNAL. ; 7-10-96 ; 16:05 ; WAREHOUSE-1 919 733 0719;# 4/ 4 ATTACHMENT II CALCULATION CIF EFFLUENT LIMITATIONS `,..31:iiiiiR??1:4:. ;:i..g.,..,:.MQq• '..::..-n,;:••••;:,:; ....:"..:L.:i;:,,:i.:;;i'l:'i.,,,,:,:9;•1•.:•:',:"' ii:.kiikiiii::.•:,:.-.iiiiii.w..4.4..,::iiij: :'...,.... „......:;'":::'.:.:. ::',; : ; :Std. '' f; ''' •i:: ''''' ,....,,,,,.....:IgThriggiqumtp4.. ..iiiitf;:IYAiV ' • ' ...144.,:::•6: '.•:ia'6;''AtC::. •i;:0'•X.,tt)?:, ,. ••:.n:::::F: TROCBSS DODS 0,002--(n) o . oo (1, 18 '. . . )30D5 0.0015 (b) 48 '''.--.• ... - - 2.40 TSS 0;4302-(a) o , oo( 36 43760- i . 6 T TSS 0.006 (b) 115 5.75 , ..,..,...„ SANITARY BODS 0.010 30 , 2.50 RODS 0.010 45 ,, 3.75 TSS 0.010 30 2.50 TSS 0.010 45 3.75 NON -PROCESS BODS 0.047 , 201 (c) 2/.9 DODS 0.047 /' 16, (9 304-(d) is 7, TSS 0.047 0.047 1-81-(c) 2 . 7 - • ri I , TSS , 0.047 1, f3 2-746 (d) -10. 6 Comments: (a) Process flow determined from actual now measurement or by calculated volumes over lime. Process related sources include: beam cleaning, ultrafiltration unit Kolene quench bath, &scaling bath, rinse bath. TEG rinsc and prepolymer quench. - o 0 fpcf vdect -fpo (b) Daily max flow includes the addition of 4.000 gpd of stormwatcr from process chemical handling or storage area& (0) Calculated using a worse case removal efileieticy of 90% for DODS and TSS though thc wastewater ticatmcat (d) Daily max concentration was calculated using a 1.5 multiplier (1.5 x monthly average). PROPOSED LIMITS FOR OTJTFALL 001 PARAMETER morrri 1 1 X AVG, (lbs/day) DAILY MAX. (lb/day) DODS 4078- I 0 , 7 ifri- 17 0 TSS 404- 6, P -201- 10, Lo ciolo iz‘" omiTTC-1, Page 1 Note for Jason Doll From: Greg Nizich Date: Mon, Nov 4, 1996 7:29 AM Subject: RE: Glitch with Allied Signal To: Jason Doll Good idea, however, Dave told me we were dissuaded from doing this gentle coaxing with Greensboro and therefore he said we couldn't do it here either. Since Bill's letter suggests we determine IF d/s sampling is needed, but that we give them some time to make an accessible path (i.e. greenway, pier, dock, etc.) I says lets pick something and put it in the final permit and get it out the door, before I'm gone. From: Jason Doll on Fri, Nov 1, 1996 4:39 PM Subject: RE: Glitch with Allied Signal To: Greg Nizich No we can't drop it, if for no other reason at this point than Bill's whining and squirming has become annoying, and the issue has become a matter of principle for me on that basis. Allied is a huge a corporation with more money than God (or Trump). If they wanted, they could by a chunk of river front, lanscape it with a greenway and build a pier with a floating dock for convient sampling. If he wants sampling guidance it's simple. Tell him to START A MONITORING COALITION AND GET A WAIVER. Somebody has to take a leadership role in that part of the basin, and I say Bill's the man. From: Greg Nizich on Fri, Nov 1, 1996 1:44 PM Subject: Glitch with Allied Signal To: Dave Goodrich Cc: Jason Doll instream sampling point d/s is not available. They want to know if it is REALLY necessary. They claim they do not have an accessible point d/s of their effluent pipe. They offer no alternative for d/s, only u/s. If and when we select a d/s location, they want guidelines on sampling, and techniques to deal with wide variations in water levels. In the interest of my duration of employment can we drop it? SENT RY:AILIED SIGNAL ;10-28-96 ; 8:39 ; WAREHOUSE-) 919 733 0719;# 2/ 3 41IiedSignaI P I R 1 R S Mr. David A. Goodrich, Supervisor NPDES Permits Group Division of Environmental Management N. C. Department of Environment. Health and Natural Renvucoe P. O. 13os 20535 Raleigh, North Carolina 27626-0535 Dar Mr, Goodrich: Alliedsignat Inc. P.O. flux 166 Moncurr, NC 27559 October 25, 1998 919 5-12 2200 919 542 12514 Fax AlliedSignal has reviewed the Draft NPDFS Permit issued on September 25, 1996 and received on October 1, 1996 for its facility in Moncnre, North Carolina. Our conunonts end questions portaln primarily to the instream monitoring requirements. Clarifinatiun irs also requested to bettor understand some reporting and monitoring requirements in tho permit. f. ketro tm Monitoring The draft permit requires that the upstream sample be collected at the U,S. Highway 1 bridge and the "nearest accessible point" ttnwnstream of the effluent pipo. AIliedi nal hue no objection to instroani monitoring as long as the sampling does not jeopardize tho safety of our employees. The Upstream monitoring point specified in the draft permit "upstream at U.S. Highway 1" bridge is unacceptable to AlliedSignal for several remains. There is inadequate parking spaeo fora vehicle near the bridge. the bridge is erttremely narrow for vohiele and pedestrian traffic:, and it doesn't have a safe pedestrian walkway. At the current time this in also a very oongveted area with numetvus driver distraoti ne due to the construction of the new Highway 1 bridge. Monitoring from the river bank under or near the bridge hag the same parking vvnnern. In addition, the bridge embankment, is steep and it creates a safety hazard to employees having to walk up and down the embankment carrying sample bottlos or monitoring equipment. During the summer months vegetation from the embankment to the river would have to be routinely cleared (non-AlliedSignal property) to allow Rafe entry to the area. AlliedSignal is unaware of any public ameba to the river between the Highway 1 bridge and AlliodSignal's property downstream of bridge. AlliodSignal currently has two acrees paints to the Haw River that aro on nornpany owned property. Theses are at the river water pump house and Lho effluent pipe, As an alternative upstream sampling point, AlliodSignal euggeets the use of a discharge valve from its: river water pumps. This would provide a representative sample without having to maneuver a steep, sometime slippery hank. A 36' pipo maintaine a constant river water level in a 12' x 12' concrete sump adjacent to the river. Two ,;No gpm centrifugal pumps piuvicla a constant flow of river water to the plant's fire ponds, An upstream river water sample could bo collected from a valve located on the pump discharge line for dissolved oxygen, temperature and Conductivity monitoring. The pumping station is located approximately 150 yards upstream of the effluent pipe. AlliedSignal does not have an accessible point to the Haw River that ie downstr um of its offluont pipe and the same bridge safety concerns that worn raised for the Ilighway 1 bridge also apply to the Old Highway 1 bridge as a clownetroam eamplu point, AlliodSignal tvquonte that the NPDEEI Permits Group reassess the distance to the next clvaost inatrearn monitoring location below AlliodSignal's effluent pipe to determine if another monitoring Irx:stivn is really necessary. If the reassesearent concludes that another monitoring point is necessary, sufficient time would be needed for AlliedSignal to clear a safe pathway to a point along the river bank. Monitoring from AlliodSignal's property along tho river hank could be conducted, approximately 60 - 75 yards downstream of the effluent pipe. if AlliodSignal is required to conduct monitoring, clarification ie requested on river bank sampling guidelines and eampling techniques when dealing with wide variations in water levels. DIVISION OF ENVIRONMENTAL MANAGEMENT July 12, 1996 MEMORANDUM To: Jason Doll Rapid Assessment Group From: Greg Nizich6,5 A NPDES Permits Group Subject: Updated Permit Limits Permit # NC0001899 Allied Signal Chatham County Allied Signal has completed sampling of their individual process and non -process wastestreams. Based on the information submitted, a process flow of 0.006 MGD was used in applying effluent guidelines. The following summarizes the proposed limits for this facility: Parameter Monthly Avg. Daily Max. (#/day) (#/day) BOD5 10.7 17.0 TSS 5.0 10.6 The most recent sampling information submitted by Allied Signal is attached. Attachment cc: Raleigh Regional Office, Water Quality SENT BY:ALLIED SIGNAL. ; 7-10-96 ; 16:04 ; ATTACHMENT 1 WAREHOUSE-, 919 733 0719;# 3/ 4 AlliedSignal [nc. Moncure, North Carolina " NPDES Permit No. NC0001SW PROCESS AND NON -PROCESS WASTEWATER MONITORING DATA Sample Date: 5/20/96 PROCESS RELATED,. URCES 1 �RB3UL7 t MC /19. Jl'1V1 Cr r1I117AcY .•«.. 1131►"Yi BEAM CLEANING BOD TSS 4,0116 37 0.15 220 ... .. _ ,..., 7.5 0.07 UL:TRAFILTRATION 2K0CH MITI 730D 8S 10,000 13 0.87 1,248 104.1 0.14 KOLENE QUENCH BATH 1301) TSS 16,200 650 0.07 100 13.5 0.54 DESCALING BATH 13OD) T89 24.8 262 0.01 14 0,003 (0,03 KOLENt; RINSE (1019/90 testing) BOD TSS 220 13 0.07 100 0.18 0.01 TEO. RINSE BOD TSS 164 29 0.12 170 0.23 0.04 PREPOLYMER QUENCH Not sampled' 0.08 110 COOLING TOWER RLOWDOWN (4 TOWERS) BOD TSS 188 1..A 31 44,640 70 <2.23 AIR C0M1'11.1138ORS (12 UNITS) BOD TSS 16.2 183 2.31 3,328.8 0.45 5.08 Cc uments: `Prcpolymcr quench is a rauiiuc tkail upciutiva dad ixcucs approximately 14 - 20 times per your. Prepolymer quc nch activity did not occur at the [hoc of sampling. SENT BY:ALLIED SIGNAL ; 7-10-96 ; 16:05 ; WAREHOUSE-) 919 733 0719;# 4/ 4 ATTACHMENT 11 CALCULATIQN QF EPP LUENT LIMITATIONS ap;P.i:latigii:;;:nq:::!'i .,:i.::.•;;?sovim,E,;:z.:,,:::5•,:ii.: ;::':::.:*: .....:',.::;:a.. PARittt.....s.::.:.1.51.0.v i,:,;,:;:ii,:::::;,,,,::::', .:s.::::••;:.:::::,..••• ailGI:i.y. ' ::::MAtt : ' • • - ' :::, ',:.lif.D.:ZAkrfttekt :;1; EBTE,uplapo :Mil$,;;AVd:;:.:;pilLy.i..i.A)c;:-,:v: 43:3fri. 0 . "to rRocEss DOD5 0,4102-(a) 0. 00 (s 18 DODS 0.006 (b) 48 . , 2.40 ' TSS 070021a) o vole, 36 43760- I . 6 TSS 0.006 (b) 115 5.75 . , , SANITARY GODS 0.010 30 1 ' 2.50 RODS 0.010 45 3.75 TSS 0.010 30 2.50 TM MOH, 45 3.75 NON -PROCESS BODS 0.047 207f(c) 21.9 •840-: DODS 0.047 18. Co 30:16-0) \ 7. 3 TSS 0.047 1411-(e) 2:7 t.11-- I .1 TSS 0.047 1. 82-7.45 (d) -10d6 Comments: (a) Process flow detennined from actual flow mcasurfancnt or by calculated volumes over time. Process related sources induclet beam cleaning, ultrafiltration unit, Kolene quench bath, dcscaling bath, rinse bath. TEO rinse and prerxilymer quench. - coo pe in1:1 -fa°. (b) Daily max flow includes the addition of 4.000 gpd of stommate from proems chemical handling or storage areas. (G) Calculated using a worse case removal efficiency of 90% for DODS and TSS though thc wastewater beementplant (d) Daily max_ concentration was calculated using a 1.5 multiplier (1.5 x monthly average). PROPOSED LIMITS FOR OUTFALL 0D1 PARAMETER MONTI ILY AVO. (lbs/day) DAILY MAX. (lb/thy) TIOD5 4078-- I 0 , 7 lei— 1'7 • 0 TSS 404- 6, 0 i0r3- 1 o , (.., g‘" %ITU, Page 1 Note for Jason Doll From: Greg Nizich Date: Thu, Jul 11, 1996 8:02 AM Subject: Numbers for Allied are In To: Coleen Sullins; Dave Goodrich; Jason Doll The long wait is over! BOD and TSS results were rec'd yesterday afternoon. BODs are: Koch Unit 10,000 mg/1 Kolene quench 16,200 mg/1 The big surprise: CTBD - 188 mg/I. At 44,000 gpd this is their second largest load to the WWTP. Bill thought the additives for corrosion inhibition, anti -scaling, etc. were most likely the source of this load. Also, he has included stormwater from process chemical handling or storage areas in the daily max. process flow calcs., but not the monthly. In dealing with Clariant, we used a "long term avg." type value for SW and used that number in determining both monthly and daily limits. Shouldn't that be done here? State of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E., Director April 30, 1996 Ms. Michelle Mathious AlliedSignal Inc. P.O. Box 166 Moncure, North Carolina 27559 ArA �EHNR Subject: Determination of Permit Limits NPDES Permit NC0001899 AlliedSignal FIBERS Chatham County Dear Ms. Mathious: Review of the process and non -process flow analysis performed in 1989 and updated in 1995 has been completed. Based on this evaluation, limits are proposed for outfall 001 as follows: Mo. Avg.* D. Max.* (lbs/day) (lbs/day) BOD5 2.8 6.2 TSS 3.1 9.6 * Values include allocations for sanitary wastewater at 30 mg/1 monthy & 45 mg/1 daily. The limits for BOD5 and TSS were determined by applying the effluent guidelines (40 CFR 414 Subpart C) to a process flow of 6,142 gpd. This figure includes a stormwater flow of 4,000 gpd and a beam cleaning flow of 900 gpd, in addition to 1,242 gpd for the Kolene and Koch operations. Due to the intermittent nature of stormwater, this component was only accounted for in determining daily maximum allocations. EPA guidance specifies using a long-term average flow (defined as a 3-5 year average where available) when calculating effluent limitations. If additional wastestreams should be included in this process flow figure, such as the system flush water indicated in your letter of February 8, 1996, an appropriate long-term average flow should be provided to the Division. No other OCPSF facility permitted by the Division has been given BOD5 or TSS allocations for non - process wastestreams. The Division does not believe the information presented to date warrants deviation from that policy at AlliedSignal. The lab analysis of the process flows performed in 1990 cannot be considered a valid wastewater characterization since three of the four samples were not measured accurately due to the sample matrix. Subsequently, the non -process flow calculations cannot be considered valid either. If Allied Signal believes that the non -process concentrations provided are truly representative, then sampling and testing of the individual wastestreams (cooling tower blowdown, boiler blowdown, stormwater, condensate, and filter backwash) should be conducted during the next permit cycle and submitted for reevaluation. P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper Any information regarding additional long-term average process flows should be submitted by May 30, 1996. If additional time is required, or if you have any questions regarding these matters, please contact me at 919-733-5083, ext. 541. Sincerely, Greg Nizich, Environmental Engineer NPDES Permits Group Attachment cc: Raleigh Regional Office Rapid Assessment Group Permit File Page 1 Note for Jason Doll From: Coleen Sullins Date: Sun, Apr 7, 1996 9:08 AM Subject: RE: "Clarification" Letter from Allied To: Greg Nizich cc: Dave Goodrich; Jason Doll Greg - I think you were going to also look at what their highest influent load and lowest removal efficiency they proposed. How does that change the analysis? It certainly is interesting that the Development Document states that BOD removal rates should be 95%. Coleen From: Greg Nizich on Wed, Apr 3, 1996 2:58 PM Subject: "Clarification" Letter from Allied To: Coleen Sullins; Dave Goodrich Cc: Jason Doll The information we requested during our site visit is essentially the same as the data provided in 1991. A slight adjustment was made so process flows weren't double counted. Even so, their non -process BOD value is 38 mg/1 (PROCESS per 40 CFR is 18 mg/1), and non -process TSS is 12 mg/1 (PROCESS per 40 CFR is 36 mg/1). They claim the influent BOD load from all sources is 230 mg/l. Their effluent data from the last year has 7 of 12 monthly BOD values of 0.0. The other 5 months average a CONC. of 1.07 mg/l. This means their % removal is around 99.5. Their sample values seem very high for non -process - the average is 109 mg/l, but they were supposedly taken over 1 year which makes them hard to argue with. The 85% removal value that they assume is questionable since they are either doing much better than that, or their influent load is not as high as their sampling study indicates. Using 95% would reduce their non -process BOD load to 12.6 mg/1, which is at least less than the Process flow. The development document says that 95% is an appropriate removal rate for BOD5. The DD also recognizes several contaminated "non -process" waters as being covered under process waters, so they may have some justification for receiving an allocation for a portion of this flow. AlliedSignal FIBERS February 8,1996 Mr. Greg Nizich N.C. Department of Environment, Health and Natural Resources P. O. Box 2935 Raleigh, NC 27626-0535 AlliedSignal Inc. P.O. Box 166 Moncure, NC 27559 919 542 2200 919 542 1258 Fax RE: NPDES Permit Renewal Application Clarification of Items Dear Mr. Nizich: Each of the items listed in your letter of December 13, 1995 have been addressed and the clarifications are described below. Item 1 & 2: The upper table lists wastewater from three Kolene operations and the Koch Unit. The flows from those four components on the date sampled (10/9/90) total 1215 gallons. Since these are the only non -process flows listed, how was the figure of 0.062 MGD in the lower table determined? What other components make up the 0.062 MGD flow? The Koch Unit and the Kolene operations are process flows and therefore are included in the process flow figure of 0.008 MGD instead of the non - process flow figure of 0.062 MGD. The process flow figure of 0.008 MGD is an estimated flow of which 0.004 MGD is stormwater. The Koch Unit, Kolene operations, stormwater and other infrequent activities ( i.e. flush water) are all components of process flow. Item 3 & 4: Please provide calculations showing how the BOD conc. of 55 mg/1 (daily avg.) was calculated. What was the basis for the avg. influent BOD value referenced in footnote #3. The non -process daily average BOD concentration of 55 mg/L was determined using the following calculation: Non -process BOD = (avg. influent BOD (Attachment A) + two standard deviations) x 85% removal efficiency. Due to the large number of sample points and difficulty in obtaining representative samples from non -process wastewaters (boiler blowdown, cooling towers, etc.), a sampling plan was developed to sample Page 2 of 2 Item 3 & 4: the limited number of process wastewater sources and determine the Cont. BOD and TSS pollutant concentrations of these sources. Non -process wastewater contributions would be determined by subtracting the process results from the wastewater treatment plant influent data (Attachment A). Item 5: What component of non -process flow was assumed to be stormwater from diked chemical storage areas? Has sampling and/or testing been conducted on these areas? No information was provided in 1991. Stormwater from certain diked chemical storage areas is accounted for in the stormwater flow figure of 0.004 MGD which is a component of the process flow (0.008 MGD). Stormwater in diked areas is inspected prior to discharge. No sampling and/or testing has been conducted on these areas. If further information is required, please call me at (919) 542-2200 ext. 543. Sincerely, Michelle Mathious Environmental Engineer Attachment cc: W. L. Boyer ATTACHMENT A Wastewater Treatment Plant Influent Data for 1989 Month Flow (mgd) BOD (mg/L) TSS (mg/L) January 0.098 210 9 0.094 58 18 February 0.099 0.148 March 0.095 0.066 April 0.095 0.134 May June July 0.097 0.126 240 280 7100* 170 220 320 260 43 21 10 38 25 62 14 7 18 0.106 110 30 0.100 55 24 0.148 140 38 0.141 170 25 0.104 38 12 0.121 400 14 0.119 110 24 August 0.110 0.111 0.101 0.108 27 85 380 140 9 70 34 51 September 0.101 44 30 0.092 110 31 0.095 220 29 0.152 21 4 October 0.078 110 41 0.127 290 28 November 0.097 220 380 0.084 260 70 December 0.050 180 6 0.098 190 20 n x an 31 30 31 0.106 170 38.4 0.023 103 64.7 Non -process BOD (daily avg.) = (x + 2an) x 85% removal efficiency = 55 mg/L * Omitted from calculations ATTACHMENT A Wastewater Treatment Plant Influent Data for 1989 Month Flow (mgd) BOD (mg/L) TSS (mg/L) January 0.098 210 9 0.094 58 18 February 0.099 0.148 March 0.095 0.066 April 0.095 0.134 May June 0.097 0.126 0.106 0.100 0.148 0.141 0.104 0.121 0.119 August 0.110 0.111 0.101 0.108 September 0.101 0.092 0.095 October 0.078 November 0.097 0.084 December 0.050 0.098 n x 6n 0.127 31 0.106 0.023 240 280 7100* 170 220 320 260 43 110 55 140 170 38 -11 110 27 85 380 140 44 110 220 21 110 290 220 260 180 190 30 170 103 21 10 38 25 62 14 7 18 30 24 38 25 12 14 24 9 70 34 51 30 31 29 4 41 28 380 70 6 20 31 38.4 64.7 Non -process BOD (daily avg.) = (x + 26n) x 85% removal efficiency = 55 mg/L * Omitted from calculations big,1°our5-'> N 'proc 35 //ikar1 -pow e.(5 pco be State of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E., Director December 13,'1995 Mr. Bill Boyer AlliedSignal Inc. P.O. Box 166 f h� Moncure, North Carolina 27559 c a � cortt Subject: Process Wastewater Sources ' NPDES Permit NC0001899 AlliedSignal l~'l13 ERS Chatham County A7A QEI-1N FZ- =rin°5 it,g Aoia Dear Mr. Boyer: In 1991, sampling data was submitted on four different non -process wastewater sources to aid in limits determination during permit renewal. A copy of that information is attached. Some additional clarification of this information is required in order to evaluate limits during this permitting cycle. Please provide the following information contained in Attachment A, page 1 of 2, of that document: • The upper table lists wastewater from three Kolene operations and the Koch Unit. The flows from those four components on the date sampled (10/9/90) total 1215 gallons. Since these are the only non -process flows listed, how was the figure of 0.062 MGD in the lower table determined? • What other components make up the 0.062 MGD flow? • Please provide calculations showing how the BOD conc. of 55 mg/1 (daily avg.) was calculated. • What was the basis for the avg. influent BOD value referenced in footnote #3? • • What component of non -process flow was assumed to be stormwater from diked chemical storage areas? Has sampling and/or testing been conducted on these areas? No information was provided in 1991. If you have any questions regarding these matters, please contact Mr. Greg Nizich at 919 733 5083. ex:.. 541. Sincerely, A. Preston Howard, Jr., P.E. Attachment cc: Raleigh Regional Office Rapid Assessment Group Permit File P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper 4' Allied-Signal Inc. Moncure, North Carolina NPDES Permit No. NC0001899 ADDENDUM TO NPDES PERMIT APPLICATION RENEWAL Project Summary Introduction The Allied-Signal Inc. facility in Moncure, North Carolina manufactures high strength polyester fiber to serve producers of passenger car tires, seat belts, in -rubber applications (conveyor belts), cordage (ropes and lines) and broad woven fabrics such as tarpaulins. On November 5, 1987 EPA issued regulations establishing effluent limitations and standards for the Organic Chemicals, Plastics and Synthetic Fibers (OCPSF) industrial category. Provisions of Subpart C - Other Fibers and Subpart D - Thermoplastic Resins are applicable to "process wastewater" discharges from the manufacture of polyester fiber and resin. The Moncure Plant operates an activated sludge wastewater plant that treats primarily non -process wastewater and sanitary wastewater along with some "process wastewater". The term "process wastewater" means any water which, during manufacturing or processing, comes into direct contact with or results from the production or use of any raw material, intermediate product, finished product, by-product, or waste product (40 CFR Section 401.11(q)). Purpose The purpose of the study was to determine the "non -process" wastewater contributions, i.e. biological oxygen demand (BOD) and total suspended solids (TSS), to the wastewater treatment plant. The degree of treatment for non -process wastewater BOD and TSS is not addressed in OCPSF effluent limitations. Instead, the appropriate degree of treatment is determined by the permit writer's best professional judgement (BPJ). This separation of process and non -process wastewaters is important to assist the N.C. Water Quality Section in determining realistic and attainable effluent limitations for the zcncure Procedures Due to the large number of sample points and difficulty in obtaining representative samples from non -process wastewaters (boiler blow -down, cooling towers, etc), a sampling plan was developed to sample the limited number of "process wastewater" sources and determine the BOA and TSS pollutant concentrations of these sources. Non -process Wastewater contributions would be determined by subtracting the process results from the wastewater treatment plant influent data. Concurrence was received from Ms. Bosanne Barona.of the N.C. Division of Environmental Management during development of this study. f'E2 I4R5 APPL•. i'Rocess 5ke ro, OOO C. 6 D 15, S O D D6D /0, 000 CDND. /5, OD v 5w I2,Don t ;4 L ski �r&' b` J FiII.6j. Co,DDp 6e�� Chi q o U r Procedures (continued) Four process wastewater sources are identified as contributing BOD and TSS to the wastewater treatment plant_: These sources are listed in Table 1 along with their discharge flow and frequency. Influent refers to the sample obtained from the composite sampler located at the wastewater treatment plant. Sanitary wastewater enters the aeration basin through a different pipeline than process wastewater so there was no interference from this source during the study. Dry weather conditions during the sampling period also assisted the study and no corrections or assumptions had to be made on organic and solids loading from contaminated rain water. All Kolene process wastewater samples were collected by grab. sample on October 9, 1990 and placed in plastic containers provided by the contract analytical laboratory. Kolene units are part of a molten salt bath and parts quench system that is operated on a batch mode. The water quench discharges about 50 gallons per day of overflow and the quench bath is drained once per week. All process wastewater sources were sampled during a typical cleaning cycle. Kolene quench, descaling and rinse baths were drained to the wastewater treatment plant following sampling on the morning of 10/9/90. The Koch (ultrafiltration) unit operates on a 5 day continuous cycle to separate waste fiber finish oil from water. Grab samples from the Koch unit were collected every four hours from 0800 hours on 10/9/90 to 0800 hours on 10/10/90 and composited in a cooler. Samples were delivered to the contract laboratory, Industrial & Environmental Analysts, Inc., on the morning of October 10, 1990 for analysis. Enclosed is a copy of the analytical results. Results Results are summarized on Attachment A - Process Wastewater Sources_...As expected, a significant portion of the influent BOD and TSS comes from non -process related operations. The process BOD and TSS accounted for < 2% of the influent BOD and 45% of the influent solids. To develop fair and attainable effluent limitations the organic and soliai loadings from the following three general sources of wastewater should be considered: sanitary; non -process; and process wastewater. Process wastewater must also include contaminated rain water from diked chemical storage and handling areas. The degree of treatment for each source of wastewater should be determined separately based on guidelines for sanitary wastewater, BPJ and OCPSF guidelines. rLD 1994 BOD Results Sample Identification ATTACHMENT A Page 1 of 2 PRIMARY PROCESS WASTEWATER SOURCES 10/9/90 Sample Result Discharge 10/9/90 BOD (mg/1) Frequency Flow (MGD) Wastewater Treatment Plant Influent 230 NA 0.125 Kolene water Quench 2,000 (1) 50 gpd + 360 gpw 0.101 E-3 Kolene Descaling Bath 2,000 (1) 100 gpw 0.14 E-4 Kolene Rinse Bath 220 100 gpd izi59Pd U..LU L-_t Koch Unit 200 (1) 1,000 0. 1 )-2 J1 , d 1 .. (:I) Limit of detection due to sample matrix Pounds/Dav 240 1.7 0.2 0.2 1.7 Calculation - Effluent BOD • ,limitations (mg/L) (2) Effluent Limitations (lbs/day) Source Flow (MGD) Daily Avq. Daily Max. Daily Avq. Daily Max. Process 0.008 18 1.2 0.008 48 3.2 Sanitary 0.01 30 2.5 0.01 45 3.8 Non -process 0.062 55 (3) 28.4 0.062 110 (4) 56.8 Daily Avg. Daily Max. 32.1 53.8 Process and Sanitary limitations proposed by DEM Non -process daily avg. = (average influent BOD + two standard deviations) x 85% reduction efficiency Non -process daily max. = two x non -process daily average TSS Results Sample Identification Wastewater Treatment Plant Influent Kolene Water Quench Kolene Descaling Bath Kr)l.nn( Ri nnn flat h Koch Unit Calculation - Effluent TSS ATTACHMENT A Page 2 of 2 10/9/90 Sample Result Discharge 10/9/90 TSS (mq/1) Frequency Flow (MGD) Pounds/Day 25 NA 0.125 26 14,000 50 gpd + 360 gpw 0.101 E-3 11.7 64 10C gpw 0.14 E-4 0.01 1.1 100 qp.1 0.10 E-1 0.01 9 1,000 gpd 0.1 E-2 0.08 Source Limitations (mg/L) (5) Effluent Limitations (lbs/day) Flow (MGDL Daily Avq. Daily Max. Daily Avq. Daily Max. Process 0.008 36 2.4 0.008 115 Sanitary 0.01 30 2.5 0.01 45 Non -process 0.062 25 (6) 12.9 0.062 50 (7) Daily Avg. Daily Max. 17.8 7.7 3.8 25.8 37.3 Process and Sanitary limitations proposed by DEM Non -process daily avg. = (average influent TSS + two standard deviations) x 85% removal efficiency Non -process daily max. = two x non -process daily average —n in G EX88/MP COMPLIANCE EVALUATION ANALYSIS REPORT 11/28/95 PAGE 1 PERMIT--NC0001899 PIPE-001 REPORT PERIOD: 9410-9509 LOC---E FACILITY --ALLIED SIGNAL, FIBER DIV. DESIGN FLOW-- .2440 CLASS--2 LOCATION--MONCURE REGION/COUNTY--05 CHATHAM 50050;'':`00310 00530 31616 50060 00340 TAA3B TAA3D MONTH Q/MGD BOD RES/TSS FEC COLI CHLORINE COD CERI48AC DAPH48AC LIMIT F .2440 F 32.10 F 17.8 F 200.0 NOL 94/10 .0597 .00 .0 1.0 341.379 100 100 94/11 .0405 .00 .0 .0 353.571 94/12 .0388 .35 .0 .0 372.413 95/01 .0499 .00 .0 .0 296.774 100 100 95/02 .0606 .32 .0 .0 178.571 95/03 .0615 .00 .0 .0 137.931 95/04 .0587 .00 .0 .0 234.482 100 100 95/05 .0786 .00 .0 .0 261.290 95/06 .1124 .65 650.OF 5.4 240.000 95/07 .1083 .52 2.1 .0 206.451 100 100 95/08 .0841 .00 1.2 1.0 277.419 95/09 .0825 .00 .0 1.7 350.000 AVERAGE .0696 .15 54.4 .7 270.856 100 100 MAXIMUM .1530 2.60 680.0 830.0 900.000 100 100 MINIMUM .0100 LESSTHAN LESSTHAN 100.000 100 100 UNIT MGD LBS/DAY LBS/DAY #/100ML UG/L LBS/DAY PERCENT PERCENT G(EX88/MP COMPLIANCE EVALUATION ANALYSIS REPORT 11/28/95 PAGE 2 PERMIT--NC0001899 PIPE--001 REPORT PERIOD: 9410-9509 LOC---E FACILITY --ALLIED SIGNAL, FIBER DIV. DESIGN FLOW-- .2440 CLASS--2 LOCATION--MONCURE REGION/COUNTY--05 CHATHAM 00010 00400 00556 00600 00625 00665 32102 34200 MONTH TEMP PH OIL-GRSE TOTAL N TOT KJEL PHOS-TOT CARBNTET ACENAPHT LIMIT NOL 9.0 6.0 F 20.000 F10.0000 NOL F .00 F .0010 94/10 18.19 7.4-6.8 .000 .7300 .00 .0000 94/11 15.95 7.4-7.0 .000 .5960 94/12 7.7-7.1 .000 .5800 95/01 7.4-6.7 .000 .6050 95/02 7.4-6.7 .000 2.3750 95/03 7.1-6.5 .000 1.0560 95/04 7.3-6.6 .000 .7075 95/05 7.5-6.9 .000 .9960 95/06 7.2-6.9 1.400 1.5000 95/07 7.4-6.8 .000 1.2250 95/08 7.4-7.0 .000 1.1020 95/09 7.3-6.7 .000 1.4700 AVERAGE 17.07 .116 1 0785 .00 .0000 MAXIMUM 21.00 7.700 5.600 4.7000 MINIMUM 13.00 6.500 .3900 UNIT DEG.0 SU LBS/DAY LBS/DAY LBS/DAY LBS/DAY LBS/DAY LBS/DAY 0 Pa irt t,r- 4dn) .601 r ,a • I.a-1.5 7714 in-r4p 4l ac,(d) 066 (e-Ay'tme-gcycA0 SQ L(61114311-ar) Overflow HAW 261 6 e-S 0 VER Discharge : NO. 002 (139k GPD) 1 7, Steam Bo lers 10 HVAC, Air Compressor and Steam Condensate 0.5 Storm Water Air Dryer 12 74 117 5� Fire Ponds 179, Potable Water Treatment 172 4 I Storm Process Water Oil Mist Fliminainr Oil Treatment 7 4/el'?' s-� ,) GayciC 4, 5 ems �7 1 Alum Settling Pond Cooling Towers 62 Oil To Burning (Energy Recovery) WATER_—' 4E VAPORATION ip STEAM OILS D art 1'- ' d c3/ Ecru 14 r C rhLr Low -55u Cc'not4iLl tYvt proaL 6 i Sanitary SCHEMATIC OF WATER FLOW ALLIEDSIGNAL INC. MONCURE, CHATHAM COUNTY NORTH CAROLINA All values are in Thousands of Gallons Per Day 6 0.91714ik Q Beam Cik Cleaning (71.9k GPD) tcp to Wastewater Treatment Plant 61.9 rfr'yt e$ 3/J%I4r, fro 4nneno a.r+S e:l e..�. af1of Se-o( . y'4,rriI5 n1c e.- be,o,(ri Dyer 61 1s Discharge ,1A1- s-1A yac/15 NO. 001 68k GPD) ��d i'n � �' on �.5. Ec-Yrl � ik `6(S- jc 4 41-6 Please print or type in the unshaded areas only (fill—in areas are spaced for elite type, i.e., 12 characters/inch 1. Form Approved. OMB No. 2040-0086 Approval expires 7-31-88 FORM 1 GENERAL EPA LABEL ITEMS 1. EPA I.D. NUMBER \\\\\ ♦III. FACILITY NAME FACILITY MAILING ADDRESS FACILITY LOCATION 11. POLLUTANT CHARACTERISTICS U.S. ENVIRONMENTAL. PROTECTION AGENCY GENERAL INFORMATION Consolidated Permits Program (Read the "General Instructions" before starting.) PLEASE PLACE LABEL IN THIS SPACE 1. EPA I.D. NUMBER FNC,D05 3488409 3 /A 16 GENERAL INSTRUCTIONS If a preprinted label has been provided, affix it in the designated space. Review the inform- ation carefully; if any of it is incorrect, cross through it and enter the correct data in the appropriate fill—in area below. Also, if any of the preprinted data is absent (the area I to the left of the label space lists the information that should appear), please provide it in the proper fill—in areas) below. If lane label is complete and correct, you need not complete Items I, III, V, and VI (except VI-B which must be completed regardless). Complete all items if no label has been provided. Refer to the instructions for detailed item descrip- tions and for the legal authorizations under which this data is collected. INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must submit this form and the supplemental form listed in the parenthesis following the question. Mark "X" in the box in the third column if the supplemental form is attached. If you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity is excluded from permit requirements; see Section C of the instructions. See also, Section D of the instructions for definitions of bold—faced terms. SPECIFIC QUESTIONS A. Is this facility a publicly owned treatment worn which results in a discharge to waters of the U.S. (FORM 2A) C. Is this a facility which currently results in discharges to waters of the U.S. other than those described in A or 8 above? (FORM 2C) E. Does or will this facility treat, store, or dispose of hazaraous wastes? (FORM 3) C Do you or will you Inject at this facility any produced water or other fluids which are brought to the surface in connection with conventional oil or natural gas pro- duction, inject fluids used for enhanced recovery of oil or natural gas, or inject fluids for storage of liquid hydrocarbons? (FORM 4) I. Is this facility a proposed stationary source which is one of the 28 industrial categories listed in the in- structions and which will potentially emit 100 tons per year of any air pollutant regulated under the Clean Air Act and may affect or be located in an attainment area? (FORM 5) 11 . NAME OF FACILITY 1 YES NO FORM ATTACH En X 16 17 16 X X 22 23 24 X L 25 30 X 36 35 36 X A,L,L,IEDSIGNAL INC IV. FACILITY CONTACT 2 SPECIFIC QUESTIONS YES MARK NO 'X FORM ATTACHE' B. Does or will this facility (either existing or proposed) include a concentrated animal feeding operation or aquatic animal production facility which results in a discharge to waters of the U.S.? (FORM 2B) D. Is this a proposed facility (other than those described in A or B above) which will result in a discharge to waters of the U.S.? (FORM 2D) F. Do you or will you inject at this facility industrial or municipal effluent below the lowermost stratum con- taining, within one quarter mile of the well bore, underground sources of drinking water? (FORM 4) H. Do you or will you inject at this facility fluids for spe- cial processes such as mining of sulfur by the Frasch process, solution mining of minerals, in situ combus- tion of fossil fuel, or recovery of geothermal energy? (FORM 4) 3 J. Is this facility a proposed stationary source which is NOT one of the 28 industrial categories listed in the instructions and which will potentially emit 250 tons per year of any air pollutant regulated under the Clean Air Act and may affect or be located in an attainment area? (FORM 5) BOY ER ,W . L . ENV . SUPERVISOR 16 V. FACILITY MAILING ADDRESS A. STREET OR P.O. BOX c r I I I I 3 3,3.8, .P,E,A, RI,D,G,E, ,R,O,A.D P 0 ,BOX 4 B. CITY OR TOWN 1 1 I I I I T I 1 I I I I IN;ONCURE 16 V . FACILITY LOCATION A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER C r I r I i I I I T I f I 1 T I I 1 3, 3. 8, P, E A, , R, I, D, G, E, ,ROAD 16 B. COUNTY NAME 1 I T 1 1 1 1 1 T 1 1 1 1 HA THAN C. CITY OR TOWN 1 1 r 6 M,O,N,C U.R.E 1Q EPA Form 3510-1 (Rev. 10-80) B. PHONE (area code & no.) 1 6 6 C.STATE D. STATE N C 41 42 66 D. ZIP CODE E. ZIP CODE I T 1 I 33 CONTINUE ON REVERSE ONTINOED tHUm Inc rrsv+.. • VII. SIC CODES (4-digit, inorder of priority) A. FIRST B. SECOND c 7 1 i 2 8 2 4 (specify) Polyester Fiber 7 I 1 I 71R,711 (specify) ' Polyester Resin + 15 16 I9 C. THIRD D. FOURTH " e 7 I I i (specify) e 1 1 I (specify) 15 VHI. 16 19 OPERATOR 15 IK INFORMATION A. NAME 8. IS the name fisted to Item VIII-A also the 8 1 1 i 1 1 1 1 1 1 1 1 1 1 1 I 1 1 I I 1 i 1 1 i i I I i I I I 1 1 I i I I I I ALLIED S IGNAL INC s • , 1 I I 1 owner? {AYES ENO 1s + +s 55 66.. C. STATUS OF OPERATOR (Enter the appropriate letter into the answer box; if "Other'. specify.) D. PHONE (area code & no.) F FEDERAL M= PUBLIC (other than federal or state) S =STATE O =OTHER (specify) P=PRIVATE P J (specify) A II 91 9 116 Illi 5 4 2 ITT 2 2 0 0 16"- 21 12' - 25 15 - u 56 111 E. STREET OR P.O. BOX r 1 I 1 I 1 1 1 1 1 1 I I 1 1 1 1 1 I 1 1 1 1 I I 1 i I P O B 0 X 1 6 6 , 24 - 55 F. CITY OR. TOWN G.STATE H. ZIP CODE IX. INDIAN LAND c, 6M,01N,CIUIR,E 1 1 1 1 1 I if i 1 1 1 1 1 1 1 I I I I 1 1 1 i 1 IN,C 1 1 1 1 2,7,5,5,9 Is the facility located on Indian lands? 0YES I.�NO 52 15 X. 16 - EXISTING ENVIRONMENTAL PERMITS 40 41 42 47 - 51 A. NPOES (Discharges to Surface Water) D. Pso (Air Emissions from Proposed Sources) c r 1 11 1 1 1 1 1 1 i i I I .. I 1 1 1 I 1 I 1 1 1 1 i I 9� N N 1 0, 0, 0, 1, 8, 9, 9, 1, 9 1 1 1 15 16 17 14 30 15 16 17 IS 30 B. uiC (Underground Injection of Fluids) E. OTHER (specify) C T i I 1 1 1 I 1 T- 1 1 1 I i j T i 1 I T 1 1 1 1 1 1 1 I 1 2 6 5 7 R 1 4 (specify) Emis16 sion Permit N. C. Air 9C 17 14 30 15 Ij 16 17 /4 - 0 C. RCRA (Hazardous Wastes) E. OTHER (specify) C T 1 I 1 I 1 1 1 1 1 1 i 1 1 C T 1 1 1 1 1 1 1 1 1 1 1 I 1 (specify) 9 R N C D , 0, 5, 3 4 8 8 4, 0 9 `30 9 N C,_5, 01 0, 0, 1, 0, 0, , , , N. C. Stormwater Permit 15 XI. 16 MAP 17 14 - - 1s 16 1 10 - 30 Attach the treatment, water XII. to this application a topographic map of the area extending to at (east one mile beyond property bounderies. The map must show outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste storage, or disposal facilities, and each well where it injects fluids underground. Include all springs, rivers and other surface bodies in the map area. See instructions for precise requirements. NATURE OF BUSINESS (provide a brief description • XIII. A chemical plant engaged in the manufacture of an organic polyester resin and a synthetic polyester fiber. I i • CERTIFICATION (see instructions) • - I attachments application, false certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all and that, based on my inquiry of those persons immediately responsib/e for obtaining the information contained in the / believe that the information is true, accurate and complete. l am aware that there are significant penalties for submitting information, including the possibility of fine and imprisonment. A COMMENTS NAME & OFFICIAL TITLE (type or print) Bentley E. Park Plant Manager FOR OFFICIAL USE ONLY B. SIGNATURE 6 & A44 C. DATE SIGNED $ - 2 7- 9 1.- c C' I , , I 15 55 Ifi- EPA Form 3510-1 (Rev. 10-80) Reverse SENT BY:AILIED SIGNAL ;10- 4-95 ; 15:00 ; WAREHOUSE-9 919 733 0718;# 2/ 4 plat,& print or type in the unshaded areas only EPA 1.0. NUMBER/Copy train Itera ! el Fonri I) NCD053488409 form approve.. OM9 No. 2000-Oo69 Approvalexpres 12-31 85 MmmmiM U.S. ENVIRONMENTAL PROTECTION AGENCY .y.A APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER EPA EXISTING MANUFACTURING, COMMERCIAL. MINING AND SILVICULTURAL OPERATIONS Consolidated Perm(ts Program • I.OUTFAL,L LOCATION fof aatil ou elf; lilt the latitude erid I Orfpttude pr Its locatioh to the merest 15 seconds end the name of the receiving water. AuOL)TL - NU� - B. LATITUDE C. LONGITUDE O. ReceiviNG WATER (name) 1. ere. ere. L vita, I. sac. 1. one, a, MIa, ,. sac. 001 35 37 01 79 03 25 Haw River 002 35 37 00 79 02 36 Shaddox Creek I. FLOWS. SOURCES OF POLLUTION. AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the' water flow through the facility- Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment drifts labeled to correspond to the more detailed descr'ptians in Item 6. Construct a water balance on the line drawing by showing average p;iptakos,, eperatio t ,ynitsa,enc{.outfalla, •1f a water Wens!canpot be..determcertain ined (erg., for mining activltie&J, provide a Pjipn o xhdllnjurp• tligni.PSyrim of •WaIBr and any; coliectidatet;tteatmetttliwasules. S..For each esatfall, provide a description of: {11 All operations contributing wastewater to the affluent, Including process wastewater, sanitary wastewater, toglingWater, and storm water runoff:121 The average flew contributed by each operation: and (3) The treatment received by the wastewater, Continue .�pn add tkmal •ilieets if naceaae'ry. • 1,C1/T- �eter1 "girl Z. OPCRATIONl151 G6NTRIp1TING FLOW _ _ TREATMENT O. OPERATION Kist) t/. AVERAGE FLOW (include unfit/ a, DESCRIPTION b. LIST COOLS IRON TAMA = 1 001 process Wastewater 9,000 GPD 0i1 Pretreatment XX Sanitary Wastewater 10,000 GPD Grinding 1-L Cooling Water Slowdown 15,000 GPD tteutralizarinn 2-K Boiler. Rlowdown 10 000 GPD Activated Sludge 3--A • HVAC, Air Compreepors & _ _ Steam Condensate 15,000 GPD Clarifier 1-U Stormwater Runoff 12.000 GPD Polishing Pond AX Potable Water Plant Alum Settling Pond 5-T Filter Backwash and Disinfection Z-F 4-A clarifier Bl.owdown 6,000 QPD Discharge of Surface Seam Cleaning 900 GPI) Water Ja y tng 5 -R 002 Fireoond Overflow 74,000 GPD -Slud&P Off -Site Landfill 5-H Stormwater Runoff 63,500 coP 0i1 Baffles and Weirs 1-H Steam and HVAC Condensate 1,Q0Q QPD Emergency Containment XX Air Dryer 500 cm Sludge to Brick XX Manufacturing Feedstock r...••.,.-. . vox F .,t., r narr.,a.., n..,..,..-...................s... Please print or type in the unshaded areas only. EPA LD. NUMBER(cOpy from Item 1 of Form I) NCD053488409 Form Approved OMB No. 2000-0059 Approval expires 12-31-85 V.S. ENVIRONMENTAL PROTECTION AGENCY APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OP ' ATIONS Consolidated Permits Program For each outfall; list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A.,OUTFALL NUMBER (list) B. LATITUDE. - C. LONGITUDE D. RECEIVING WAT R (name) I. ora. 2. MIN. 9. SEC. 1. DEG. 2. MIN. 9. SEC. 001 35 37 01 79 03 25 Haw River 002 35 37 00 79 02 36 Shaddox Creek 11. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. indicate sources of inta - water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Co - ruct a water balance on the line drawing by showing average flows between intakes, operations,rxreatment • units, •and_outfa(Is. kif a water balance•-ca . t be determined (e.g, for certain. mining activities), provide a - n .:pictorial `description of the nature and amount of. any sources of water and any -collection • r treatment measures. . B. For each outfall, provide a description of:,(1) All -operations contributing wastewat to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; (2) The average. flow contributed by each o• -ration; and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. • LOUT- FALLNO (Ust) 2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT a. OPERATION (list) b. AVERAGE FLO (include units) a. DESCRIPTION b. LIST CODES FRON TABLE 2C-1. 001 Process Wastewater 0i1 Pretreatment XX Sanitary Wastewater 10,00t GPD Grinding 1-L Cooling Water Blowdown NPtitrA1izatinn 2-K Boiler Blowdown Sludge 3-A HVAC, Air Compressors & );)Actlniated Steam Condensate L? Clarifier 1-U Stormwater Runoff ) Polishing Pond XX Potable Water Plant cS Alum Settling Pond 5-T Filter Backwash and Disinfection Z-F Clarifier Blowdown Discharge of Surface 4-A Beam Cleaning Water SltlrigP Drying 5-H 002 Firepond 0verfl. Off -Site Landfill 5-H Stormwater Ru •ff Oil Baffles and Weirs 1-H Steam and HV'C Condensate Emergency Containment XX Air Dryer Sludge to Brick XX Manufacturing Feedstock OFFICIAL USE ONLY (effluent guidelines sub -categories CONTINUED FROM THE FRONT I. OUTFALL NUMBER,cr (♦ {ISL� -. _ _ -,2. OPERATION(s) , ' '_ ' 6.,'.CONTRIBUTING FLOW / (Ltftl 3. FREQUENCY 4. FLOW a. DAYS PER WEEK auerage) uer gel b. MONTHS PER YEAR ver gel average) a. FLOW RATE (in mgd) b. TOTAL VOLUME (specify with units) C DUR- I. LONG TERM AVERAGE 2. MAXIMUM DAILY I. LONG TERM AVERAGE 2. MAXIMUM DAILY ATION In days) ( Y ) I. PRODUCTION C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? EYES (complete the following table) NO (go to Section III) 1I A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? !]YES (complete Item III-B) Refer to Supplementary Informati p 0 (to to Section IV) B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? OYES (complete Item III-C) NO (go to Section IV) C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. 1. AVERAGE DAILY PRODUCTION a. QUANTITY PER DAY b. UNITS OF MEASURE C. OPERATION, PRODUCT. MATERIAL, ETC. (specify) 2. AFFECTED OUTFALLS (list outfatl numbers) N/A V. IMPROVEMENTS A. Are you now required by any Federal, State or ocal authority to meet any implementation schedule for the construction, upgrading or operation of waste- water treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant Or loan conditions. AYES (complete the following table) [3iJ No (go to Item IV-B) 1. IDENTIFICATION OF CONDITION, AGREEMENT, ETC. 2. AFFECTED OUTFALLS a. NO. b. SOURCE OF DISCHARGE 3. BRIEF DESCRIPTION OF PROJECT 4. FINAL COM PLIANCE DATE 8. R£- b. PRO- QUIREC IECTEO B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for construction. EMARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (Rev 2-RBI PA(F r1P ,1 r`nnITIn11 or noon n A cc CONTINUED FROM PAGE 2 EPA 1.0. NUMBER (copy from Item 1 of Form 1) NCD05348840 Form Approved. OMB No. 2000-0059 Approval expires 12-31-85 V. INTAKE AND EFFLUENT CHARACTERISTICS A, B, & C: See instructions before proceeding — Complete one set of tables for each outfall — Annotate the outfall number in the space provided. NOTE: Tables VA, V-8, and V-C are included on separate sheets numbered V-1 through V-9. D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession. 1. POLLUTANT 2. SOURCE 1. POLLUTANT 2. SOURCE Acetaldehyde Cresol Crotonaldhyde Cyclohexane Xylene Possible process by- product used in Q.C. lab Possible process by- product Used in Q C Lab Used in Q C Lab VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed inItem V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct? YES (list all such pollutants below) NO (go to Item VI-B) Antimony Phthalate Esters (Possible process byproduct) (Refer to Supplementary Information) FPA Fnrm ZF1l1.9r` PAGE 3 OF 4 CONTINUE ON REVERS CONTINUED FROM THE FRONT VI1. BIOLOGICAL TOXICITY TESTING DATA V Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? [EYES (identify the test(s) and describe their purposes below) ONO (go to Section VIII) Acute Toxicity at Discharge 001 and 002 Permit Requirement III,CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? ®YES (list the name, address, and telephone number of, and pollutants analyzed by, each such laboratory or firm below) NO (go to Section IX) A. NAME Industrial & Environmental Analysts, Inc. Aqua Tech. Environmental Laboratories, Inc. Hydrologic IX. CERTIFICATION B. ADDRESS 3000 Western Pkwy Cary, NC 27513 936 N. Horner Blvd. Sanford, NC 27330 2500 Gateway Center Suite 900 Morrisville, NC 27560 C.-TELEPHONE (area code & no.) (919)677-0090 (919)776-5999 (919)380-9699 D. PO-CLUTANTS ANALYZED (list) BOD, TSS, TOC, F-Coliform, TKN, T-Solids, Oil & Grease Pollutants Acute Toxicity / certify under penalty of law that this document and aft attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete- ' am aware that there are significant penafties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. NAME & OFFICIAL TITLE (type or print) Bentley E. Park Plant Manager B. PHONE NO. (Area code & no.) (919) 542-2200 C. SIGNATURE L D. DATE SIGNED 2-2'' - 23 EPA Form 3510-2C (Rev. 2-85) PAGE 4 OF 4 HAW 261 VER Overflow Discharge NO. 002 (139k GPD) 71 Steam Boilers 10 74 117 HVAC, Air Compressor and Steam Condensate 48 15 63.5 0.5 Storm Water Air Dryer 12 Process Fire Ponds 179- Potable Water Treatment 172 69 Storm Water Alum Settling 7 Pond 77 Cooling Towers Oil Mist Fliminatnr 011 Treatment -♦ WATER�� DEVAPORATION b STEAM Sanitary 10 51 62. 1 Oil To Burning (Energy Recovery) SCHEMATIC OF WATER FLOW ALLIEDSIGNAL INC. MONCURE, CHATHAM COUNTY NORTH CAROLINA All values are in Thousands of Gallons Per Day 6 Beam Cleaning 0.9 Jr (71.9k GPD) 10 Wastewater Treatment Plant 61.9 Discharge NO. 001 (68k GPD) FORM 2C NPDES HAZARDOUS SUBSTANCES (SECTION 311) EXEMPTION REQUEST Section V-D The Moncure Plant stores and uses various materials listed under Section 311 - Hazardous Substances. The accompanying list shows which materials are on site in more than laboratory quantities, the approximate total amount stored, and the size of the individual unit being stored for use. The receiving, unloading, and storage methods used are consistent with accepted spill prevention and control practices which are designed to prevent any discharge. All surface drainage from the developed areas is collected and discharged through either the wastewater treatment plant outfall 001 or the stromwater, firepond overflow outfall 002. The outfall 002 drainage system includes a series of baffles and weirs designed to contain accidental spills. Spills that get beyond the baffle/weir system can be contained in a holding pond and pumped to a storage tank or the wastewater treatment plant. All personnel that handle raw materials receive both classroom and on the job training in their job functions and on spill and pollution control. In addition, personnel are kept current through daily contact with their supervisors and through monthly safety meetings. SENT BY :ALLIED SIGNAL ;10- 4-95 ; 15:01 ; WAREHOUSE-) 919 733 0719;# 4/ 4 HAZARDOUS SUBSTANCES (SECTION 311) EXTREMELY HAZARDOUS SUBSTANCES (SARA 'IT fLE AND CERCLA SUBSTANCES SPILL INFORMATION SUBSTANCES Acetone Aluminum Antimony Compound Chlorine Cresol/ Chloroform APPROX. AMT. a.,B) 725 6,500 12,000 1,800 CONTAINER SIZE 5 gal. drum 50 lb. bags 35 lb, bucket 1501b. Cylinders STORAGE METIIOD Curbed areas inside buildings Inside building Inside building Cylinder storage area & inside water and wastewater treatment plant buildings 1,300 15 gal. drums Curbed area & inside building Cyclohexane 1,000 Diehlorodifluoro- 11,700 methane Methyl Chloroform < 300 Phenol/1,1,2,2- 1,160 Tetrachloro- ethane Polychlorinated 68,000 Biphenyls Sodium Hydroxide Sodium Nitrite Sulfuric Acid Trichlorotri- fluoromethane 45,000 1,700 3,000 1,500 55 gal. drum Various 55 gal, drum 15 gal. drum Various size Transformers 12,000 gal. tank & drums 55 gal, drum 15 gal, drum Various Curbed area & inside building Used in refrigeration units inside buildings Inside MSI building Curbed area & inside building Outdoor transformer areas Curbed areas & inside buildings Curbed areas & inside building Curbed areas & inside building Used in refrigeration units inside buildings LEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of its information on separate sheets (use the same format) instead of completing these pages. EE INSTRUCTIONS. EPA I.D. NUMBER (copy from Item 1 of Form 1) NCD053488409 Form Approved. OMB No. 2000-0059 Approval expires 12-31-85 V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) PART A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. .POLLUTANT Biochemical )xygen Demand 80D) Chemical )xygen Demand COD) . Total Organic :arbon (TOC) . Total Suspended olids (TSS) 2. EFFLUENT a. MAXIMUM DAILY VALUE b. MAXIMSta 3QaPA)Y VALUE c.LONG T FM AVRG. VALUE : auadable) (I) CONCENTRATION 2.5 * 42 11.0 (2) MASS 2.6 21.3 8.7 (II CONCENTRATION .69 19 2.7 (2) MASS .65 9 2.2 (1) CONCENTRATION .15 10.5 .23 Ammonia (as N) * (2) MASS .16 5.9 .18 d, NO. OF ANALYSES 51 51 51 3. UN TS (specify if blank) a. CONCEN- TRATION mg/L mg/L mg/L b. MASS lb day lb/day lb/day OUTF - LL NO. 001 4. INTAKE (optional) a. LONG TERM AVERAG VALUE (I) CONCENTRATION (2) MASS b. NO. OF ANALYSES Flow . Temperature 'Water) . Temperature :umrner) VALUE 0.153 VALUE 26 VALUE 28 MINIMUM VALUE 0.112 VALUE 23 VALUE VALUE 0.068 VALUE 18 VALUE 365 144 105 MGD oC oC VALUE VALUE VALUE Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirect y but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis forthat po lutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. . POLLUT- ANT AND CAS NO. (if availabie) 2. MARK 'X'i 3. EFFLUENT a. 0E- LIPR PRE- SENT b. BE- ES, LI EAB- SENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAj VALUE (i oua a e c.LONG Tf2M PVR VALUE t avatla e? d. NO. OF ANAL- YSES (1) (2) MASS (II(t) CONCENTRATION (2) MASS CONCENTRATION I2J MASS (2) Bromide >_4959-67-9) * Chlorine, otal Residual X 0.9 0.5 0.4 0.2 0.3 0.2 365 m Color * Fecal oliform X 1 30.2 3.43 51 .^.:o Fluoride 16984-48-8) * N itrate— itrite (as N) * PA Form 3510-2C (Rev. 2-85) 4. UNITS ONCEN- RATION b. MASS 5. INTAKE (optional) a. LONG TERM AVERAGE VALUE (I) CONCENTRATION (2) MASS b. NO. OF ANAL- YSES g/L lb/day 1/100m 1 * NO SAMPLING REQUIRED PAGE V-1 CONTINUE ON REVERSE TEM V-B CONTINUED FROM FRONT .POLLUT- ANT AND CAS NO. (if available) Nitrogen, otal organic Is N) 2, MARK 'X' a. BE- b.BE- iI6VEDLIEVED PRE- AB- SENT SENT 3. EFFLUENT a. MAXIMUM DAILY VALUE b. MAXINWNalva30a e) DAY VALUE CONCENTRATION (2) MASS ll) CONCENTRATION (2) MASS C.LONG TlI 12 QAy Re�, VALUE d. NO.OF available) ANAL- (2) MASS YSES CONCENTRATION a. c TR * Oil and ,rease Phosphorus s P), Total '723-14-0) Radioactivity I) Alpha, otal ') Beta, otal 12.0 11.0 .169 0.08 3.0 2.2 .3 0.18 51 1 m m i) Radium, otal I) Radium 26, Total Sulfate s SO4) 4808-79-8) Sulfide 's S) I. Sulfite s S03) 4265-45-3) X. 29.77 4 .g * * * Surfactants Aluminum, 3tal 42 9.9 0-5 ) * * Barium, �tal 440-39-3) Boron, �tal 440-42-8) Cobalt, nal 440-48-4) * * Iron, Total 439.8 9.6 ) Magnesium, rtaI 439-95-4) Molybdenum, rtal 439-98-7) Manganese, ltal 439-96-5) Tin, Total 440.31-5 ) Titanium, 3tal 440-32-6) * * * * * * PA Form 3510-2C (Rev. 2-85) * NO SAMPLING REQUIRED PAGE'V-2 4. UNITS 5. (optional) DNCEN- ATION b. MASS VINTAKE TE AERAGE VUE b• NO.OF (t) CONCENTRATION - (2) MASS ANAL - YSES ;IL lb/day r/.L lb/day I/L 1 1 CONTINUE ON PAGE V -3 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER NCD053488409 CONTINUED FROM PAGE 3 OF FORM 2-C 001 Form Approved. OMB No. 2000-0059 Approval expires 12-31-85 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater ourfaf/s, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at (east one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (a// 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK 'X' 3. EFFLUENT 4. UNITS a.TESY- IN G OUIR- L--D b. BE- C RE- LIEVED LIEVEG SENT RE- SENT a. MAXIMUM DAILY VALUE ) CONCENTRATION METALS, CYANIDE, AND TOTAL PHENOLS (2) MASS b. MAXIMUM 30 DY VALUE 0/available) ) (2) MA55 CONCENTRATION C.LONG TM Q a e noble I .VALUE CONCENTRATION (/) MASS d, NO.OF ANAL- YSES 8. CONCEN- h. MASS TRATION 5. INTAKE (optional) a. LONG TERM AVERAGE VALUE (t) t-oNCI'N- (2) MASS HAT, b. NO.OF ANAL- YSES 1M. Antimony, Total (7440-36-0) 48 .02 2M. Arsenic, Total (7 440-38 -2 ) LT3 3M. Beryllium, Total, 7440-41-7) LT5 4M. Cadmium, Total (7440-43-9) 5M. Chromium, Total (7440-47-3) 0.9 LT20 .0004 6M. Copper, Total (7440-50-8) 7M. Lead, Total (7439-92-1) 8M. Mercury, Total (7439-97-6) 109 .05 3.7 LT.2 .002 9M. Nickel, Total (7440-02-0) 10M. Selenium, Total (7782-49-2) 11M. Silver, Total (7 440.2 2-4 ) 20 LT3 LT1 .01 12M. Thallium, Total (7440-28-0) LT1 13M. Zinc, Total (7 440-66-6 ) 219 0.1 14M. Cyanide, Total (57-12-5) LT.005 15M. Phenols, Total DIOXIN 2,3,7,8-Tetra- chlorodibenzo-P- Dioxin (1764-01-6) LT.01 ug/L lb/day ug/L ug/L ug/L lb/day ug/L ug/L lb/day ug/L lb/day ug/L ug/L lb/day ug/L lb/day ug/L lb/day ug/L lb/day ug/L mg/L lb/day mg/L lb/day DESCRIBE RESULTS EPA Form 3510-2C (Rev. 2-85) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT '1. AND CAS POLLUTANT NUMBER (if available) 2- atEST• ING pU1R- - EO MARK b, eE- LIEVEOLIEVEn 9ENT 'X' C, ee- 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. LONG TERM AVERAGE YALUE ANAL- YSES a. MAXIMUM DAILY VALUE b. MF.XI•iv M 34 rr� Y VALUE fiaVQEa[J{e�%QUQ{fQbte�•b.NO.OF o.LONG 7 }iM Se{�(� VALUE d. NO.OF ANAL- YSES 4 a. CONCEN- TRATION b. MASS SENT (') CONCENTRATION (2) MASS (I) CONCENTRATION (x) MASS 1') CONCENTRATION (z) MASS (I) CO ION TR ATION (2) MASS - GC/MS FRACTION - VOLATILE COMPOUNDS . ug/L ug/T, ug/L 1 V. Acrolein (107-02-8) X X X LT100 LT100 2V. Acrylonitrile (107.13-1) LT100 - - ih/clay, 1b/day 3V. Benzene (71-43-2) LT.5 LT.5 4V. Bis (Chloro- methyl) Ether (542-88-1) * 5V. Bromoform (75-25-2) X 6.2 0.003 uglL lhLday 6V. Carbon Tetrachloride (56-23-5) X X X X X X X * X X LT.5 LT.5 4 r 8V. Chlorodi- bromomethane (124-48-1) 17.3 0.009 - t- 1 4 1 ug/L ug/L ug/L lb/dad lb/day lb/day 9V. Chloroethane (75-00-3) LT.5 LT.5 _ _ 10V.2-Chloro- ethylvinyl Ether (110-75-8) LT10 - 11 V. Chloroform (67-66-3) LT.5 LT.S 4 1 4 ug/L 1_7/L ugjl lb/day 1h/day lb/clay, 12V. Dichloro- bromomethane (75-27-4) 15.6 LT.5 008 13V. Dichloro- difluoromethane (75-71-8) 14V. 1,1-Dichloro- ethane (75-34-3) LT.5 lb/day 15V. 1,2-Dichloro- ethane (107-06-2) LT.5 T,T_. - �._.4 ug/L ]tg/T, fib_/day ., 16V. 1,1-Dichloro- ethylene (75-35-4) X X X X X - X IRwv - 9-RKI LT.5 LT.5 4 17V. 1,2-Dich loro- propane (78-87-5) LT.5 LT.5 4 4 4 1 4 ug/T. "�/L ugh., _ ug/L ug/L ug/L 1 h/riay 1 b/day lb/day._ 15V. 1,3-Dichloro- propylene (542-75-6) LT.5 LT.5 19V. Ethylbenzene (100-41-4) LT.5 LT.5 20V. Methyl Bromide (74-83-9) LT10 lb/day 21V. Methyl Chloride (74-87-3) LT.5 LT.5 1 lb/day EPA Form 3510-2C * Refer to Supplementary Information ` Y CONTINUE ON PAGE V. CONTINUED FROM PAGE V-4 EPA I.D. NUMBER (copy from Item 1 of Form 1) NCD053488409 OU ("FALL NUMBER 001 . <</.,,,,,.I.I.. OMB No. 2000-0059 L Approval expires 12-31-85 •• I. POLLUTANT AND CAS NUMBER (If available) 2. MARK 'X' 1. 3. EFFLUENT 4. UNITS 5. INTAKE (optional)' aIN ST, INc OVER- ED b, ee- LIEV Ep LENT G aE- LIBV ED e. MAXIMUM DAILY VALUE b. MAXIMI.lM 3Q DAY VALUE 11 I bl (1 QUQta ¢}1 C.LONG T M VALUE j� y R QUQI/Q f¢� d. NO.OF ANAL- YSES YSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAG VALUE b. NO.OF ANAL - Y$ES SENT III CONCENTRATION (2) MASS III CONCENTRATION (a) MASS III CONCENTRATION (2) MASS (1) CONCE N- TR ATION (2) MASS GC/MS FRACTION - VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2) X LT.5 LT.5 4 ug/L lb/day 23V. 1,1,2,2-Tetra- chloroethane (79-34-5) X LT 5 1 ug/L lb/day 24V. Tetrachloro- ethylene (127-18-4) X LT.5 LT.5 4 ug/L lb/day 25V. Toluene. (108-88.3) X LT.5 LT.5 4 ug/L lb/day 26V. 1,2-Trans- Dichloroethylene (156.60.5) X LT.5 LT.5 4 ug/L lb/day 27V. 1,1,1-Tri- chloroethane (71.55-6) X LT.5 LT.5 4 ug/L lb/day 28V. 1,1,2-Tri- chloroethane (79-00-5) X LT.5 LT.5 4 ug/L lb/day 29V. Trichloro- ethylene (79-01-6) X LT.5 LT.5 4 ug/L lb/day 30V. Trichloro- f(uoromethane (75-69-4) * 31V. Vinyl Chloride (75-01-4) X LT.5 LT.5 4 ug/L lb/day GC/MS FRACTION - ACID COMPOUNDS 1 A. 2-Chlorophenol (sg 57 8) X LT5 LT5 4 ug/L lb/day 2A. 2,4-Dichloro- phenol (120-83-2) X LT3 LT3 4 ug/L lb/day 3A. 2,4-Dimethyl- phenol (105-67-9) X LT3 LT3 4 ug/L lb/day 4A. 4,6-Dinitro-O- Cresol (534-52-1) X LT10 LT10 4 ug/L lb/day 5A. 2,4-Dinitro- phenol (51-28-5) X LT10 LT10 4 ug/L lb/day 6A. 2-Nitrophenol (88-75-5) i X LT3 LT3 4 ug/L lb/day 7A. 4-Nitrophenol (100-02-7) X LT10 LT10 4 ug/L lb/day 8A. P-Chloro-M- Cresol (59-50-7) X LT5 1 ug/L 9A. Pentachtoro- phenol (87-86-5) X LT10 1 ug/L 104. Phenol (108-95.2) X LT3 LT3 4 ug/L lb/day 11 A. 2,4,6-Tri- chlorophenol (88-06-2) X LT3 1 ug/L r nnlTln111C r ) OF\/C OC CONTINUED FROM THE FRONT 1, POLLUTANT, AND CAS NUMBER (ifauailgble 2. MARK •X' r 3. EFFLUENT 4. UNITS 5. INTAKE (optional) aTEST• INc at b. sE- LIEVEULIEV SENT C !E- Er1 a, MAXIMUM DAILY VALUE p. MAXI 1-EM 3Q DAY VALUE auatla ¢) C.LONG T M p�tjN�[[�R VALUE �j`(�gUgl'jqlrl¢�� d, NO.OF ANAL- YSES YSES a. CONCEN- TRATION TRATION b. MASS a. LONG TERM AVERAGE= VALUE b. NO.OI ANAL- YSES •!NT 1 (I1 CONCENTRATION (_► MASS CONCENTRATION (�) MA55 (I) CONClNTNATION I:) MASS (I) CONCEN- TRATION (=1 MA/8 GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 18. Acenaphthene (83-32-9) X LT2 LT2 ug/L lb/day 2B. Acenaphtylene (2oa-ss-a) X _ - LT2 _ LT2 _4 4 ug/L - 3B. Anthracene (120-12-7) X LT2 LT2 4 ug/L ,lb/day lb/day- 4B. Benzidine (92-87-5) X LT15 - 1 ug/L 58. Benzo (a) Anthracene (56-55-3) X LT3 LT3 —` 4 ug/L lb/day 613. Benzo (a) Pyrene (50-32-8) X LT4 LT4 4 ug/L lb/day 7B.3,4-Benzo- fluoranthene (205-99-2) X LT4 LT4 _ 4 ug/L - lb/day - 8B. Benzo (ghi) Perylene (191-24-2) X LT5 1 ug/L 9B. Benzo (k)Fluoranthene (207-08-9) X LT4 LT4 4 ug/L lb/day 108. Bis (2-Chloro- ethoxy) Methane (111-91-1) X - LT2 1 ug/L 11 B. Bis (2-Chloro- ethyl) Ether �(111-44-4) X LT2 1 ug/L 128. Bis (2-Chloroiso- propyl) Ether (102-60.1) X LT2 1 ug/L 13B. Bls (2-Ethyl- hexyl) Phthalate (117-B1-7) X LT2 LT2 4 ug/L lb/day 14B. 4-Bromo- phenyl Phenyl Ether (101-55-3) X LT3 - 1 ug/L 158. Butyl Benzyl Phthalate (85-68-7) x J LT2 _ 1 ug/L i 1613. 2-Ch lbro- naphthal s1-5s (91-58-7) X LT1 — 1 ug/L - 17 B. 4-Chloro- phenylPhenyl Ether (7005-72-3) X LT2 1 ug/L 18B. Chrysene (218-01-9) X LT3 LT3 4 ug/L lb/day 19B. Dibenzo (a,h) Anthracene (53.70-3) X * - LT25 4 ug/L _ 20B. 1,2-Dichloro- benzene (96-50-1) X- LT.5 LT.5 4 ug/L lb/day 21B. 1,3-Dichloro- benzene (541-73-1) GDA C...... 9G9 r1 7r` X /O.-.. .f orI LT.5 .1 LT.5 4 ug/L lb/day J ncluded in Total PAHs PAGE V-6 CONTINUO ON PAGE V EPA I.D. NUMBER (copy from Item 1 Of Form 1) CONTINUED FROM PAGE V-6 1 NCD053488409 OUTFALL NUMBER 001 Form Approved. OMB No. 2000-0059 • Approve/ expires 12-31-85 `1.POLLUTANT AND CAS NUMBER (if available) 2.MARK 'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) _ a�NOT RE- QUIR- EO a2fvco �wE- SENT �lev�o we- PENT a. MAXIMUM DAILY VALUE b. MAXIMUM 3,0 DAY VALUE ( available) c.LONG TjtM y�[RC�, VALUE (11 QUQtlQbleJ Id. NO.L- a. CONCEN• TRATION b• MASS a. LONG TERM AVERAGE VALUE b. NO.OI 1 coNCEN- ( I ,RATION 12) MASS ANAL - YSES (1)' CONCENTRATION (2) MASS CONCENTRATION I2) MASS (') CONCENTRATION l:) MASS ANAL- YSES GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued' 22B. 1,4-Dichloro- benzene (106-46-7) X LT.5 LT.5 4 ug/L 23B. 3,3'-Dichloro- benzidine (91-94-1) X LT15 1 ug/L 24B. Diethyl Phthalate (84-66-2) X LT1 LT1 4 ug/L 256. Dimethyl Phthalate (131-11-3) 1 X LT1 LT1 4 ug/L 26B. DI-N-Butyl Phthalate (84-74-2) X LT1 LT1 4 ug/L 276. 2,4-Dinitro- toluene (121-14-2) X LT4 LT4 4 ug/L 28B. 2,6-DInItro- toluene (606-20-2) X LT4 LT4 , 4 ug/L , 29B. Di-N-Octyl Phthalate (117-84-0) X LT1 1 ug/L 30B. 1,2-Diphenyl- hydrazine (as Azo- benzene) (122-66-7 v LT1 1 ug/L 31B. Fluoranthene (206-44-0) X LT2 LT2 4 ug/L 32B. Fluorene (86-73-7) X LT3 LT3 4 ug/L 33B. Hexacnlorobenzene (11R-7d-11 X LT2 LT2 4 ug/L 34B. Hexa- chlorobutadiene (87-68-3) X LT3 LT3 4 ug/L 35B. Hexachloro- cyclopentadiene (77-47-4) X LT5 l 1 ug/L 36B. Hexachloro- ethane (67-72-1) X LT3 LT3 - 4 ug/L 376. Indeno (1,2,3-cd) Pyrene (193-39-5) X * LT25 4 ug/L 38B, Isophorone (78-59-1) X LT1 1 ug/L 398. Naphthalene (91-20-3) X LT2 LT2 4. ug/L 408. Nitrobenzene (98-95-3) X LT 2 LT2 4 ug/L 41B. N -N itro- thylamine (62-75-9) X LT 10 1 ug/L 42B. N-Nitrosodi- N-Propylamine 621-64-7) x LT2 . 1 u /L nnlllrinri in Tnfial PARR OA/MC' NI.7 CONTINUE ON REVEF CONTINUED FROM THE FRONT ,1. POLLUTANT AND CAS NUMBER I (if (mailable) 2. MARK 'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) &t STD IA E- DUIR- b. aE- tIPR!'--�"ABED Sl NT C. eE- a. MAXIMUM DAILY VALUE b. MAXIMI.IM 30 pAY VALUE 11 l bl {I auai a e) C.LONG T }aM �[R VALUE 1 auat a e 7 -1 bl d. NOOF YSES a. CONCEN-a. TRATION b• MASS LONG AVERAGE TERM VALUE ICI MA85 b. NO. ANA YSE 6E NT (,) CONCENTRATION (3) MASS (I) CONCENTRATION (2) MASS II) CONCENTRATION (l) MASS (1) CONCFN• TRATION GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) "--- ` 438. N-Nitro- sodiphenylamine (86.30.6) X LT2 1 448. Phenanthrene (85.01-8) L12 LT2 ��g-/L ---_ 458. Pyrene (129-00-0) LT LT3- - T �I GC/MS FRACTION - PESTICIDES 1 ug/L 1P. Aldrin (309.00-2) X LT-07 1 ug/L - 2P. a-BHC (319-84.6) X LT._n^ - 1 ug/L 3P. g-BHC (319-85-7) X LT.117 1 ug/L 4P. 7-BHC (58-89-9) X X T.T.02 1 ug/L 5P.8-BHC (319-86-8) X LT.02 1 ug/L 6P. Chlordane (57-74-9) X LT.1 1 ug/L 7P, 4,4'-DDT (50-29-3) X LT.03 1 ug/1 8P. 4,4'•DDE (72-55-9) X LT.03 1 ug/L 9P. 4,4'-ODD (72.54-8) X LT.02 1 ug/L 10P. Dieldrin (60-57-1) X LT.02 1 ug/L 11P. a-Endosulfan (115.29-7) X LT.03 1 ug/L 12P. a-Endosulfan (115-29-7) X LT.03 1 ug/L 13P. Endosulfan Sulfate (1031-07-8) X LT.03 1 ug/L 14P. Endrin (72-20-8) X , LT.05 - 1 ug/L 15P. Endrin Aldehyde (7421-93-4) X LT.05 1 ug/L 16P. Heptachlor (76-44-8) FP4 Fnrm 3F1fL9f` X 10n. .7.00% 1 LT.03 _ - __ - 1 ug/L L_.- CONTINUF ON PAIOE V CONTINUED FROM PAGE V-8 EPA I.D. NUMBER (copy from Item 1 of Form 1) NCD053488409 OUTFALL NUMBER 001 Form Approved. . 6 OMB No. 2000-0059 Approval expires 12.31-85 1. POLLUTANT 2. MARK 'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) AND CAS NUMBER arEsr- ING b. DE- LIEVEOILIEVETI c.E• a, MAXIMUM DAILY VALUE b. MAXIMI..IM 3D DAY VALUE (1 aUa a e 1 l bl) C,LONG T M p VALUE ft vb 5 . ! aUQiO a d. NO.OF a. CONCEN• a. LONG Ay LRA�iE TERM VALUE b.NO.LF' (If available RE- pU1R- LQ vRE- LENT we• •ENT I ( ) CONCENTRATION (il MASS 111 CONCENTRATION (2) MA!! (I) CONCENTRATION ).) Mw55 ANAL- YSES TRATION b. MASS III co.c TRATION (z) MASS gNAL- YSES GC/MS FRACTION — PESTICIDES (continued) 17P. Heptachlor Epoxide (1024-57-3) X LT.03 ---- - - - -- 1 ug/T. 18P. PCB-1242 ---�.- --- (53469-21-9) X LT.1 1 lig/T. 19P. PCB-1254 (11097-69-1) X LT.1 1 ug/L 20P. PCB-1221 (11104-28-2) X LT.1 _- 1 ug/L 21P. PCB-1232 -- (11141-16-5) X J LT.1 1 ug/L 22P. PCB-1248 -- _ (12672-29-6) X LT.1 1 ug / L 23P. PCB-1260 "� (1 1096-82-5) X LT.1 -+�- 1 ug/L 24P. PCB-1016 (12674-11-2) X LT.1 1 ug/L 25P. Toxaphene (8001-35-2) X LT.1 1 ug/L EPA Form 3510-2C (Rev. 4-84) PAGE V-9 FPA Form 351n-2r IR.w 2-851 LEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of its information on separate sheets (use the same format) instead of completing these pages. EE INSTRUCTIONS. Form Approved. OMB No. 2000-0059 Approval expires 12-31-85 V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) PART A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 2. EFFLUENT 3. UN TS b. MAXIM,4M 39 KY VALUE (specify if blank) (I avarllaBbie -POLLUTANT Biochemical ?xygen Demand BOD) ). Chemical )xygen Demand COD) a. MAXIMUM DAILY VALUE (I) CONCENTRATION, * Total Organic 1arbon (TOC) * 12) MASS 11) CONCENTRATION (2) MASS C.LONG T j m eArf7s?a, VALUE (if avaiiam (1) CONCENTRATION (2) MASS d NO. OF ANALYSES a. CONCEN- TRATION b. MASS 4. INTAKE (optional) a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS LL NO 002 b NO. OF ANALYSES i, Total Suspended solids (TSS) Ammonia (es N) Flow 1, Temperature winter) * * VALUE 1. Temperature summer) .pH .443 VALUE 22 VALUE VALUE .202 VALUE 21 VALUE 139 VALUE 13.7 56 MGD 30 oC 26 MINIMUM 6.8 VALUE 25 VALUE 22.4 21 51 °C STANDARD UNITS VALUE VALUE VALUE PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirect y but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that po lutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. I. POLLUT- ANT AND CAS NO. (if available) 2. MARK 'X' a. eE- LpEVEC PRE- SENT b, eE- LIEVEO AB- SENT 3. EFFLUENT a. MAXIMUM DAILY VALUE b. MAXI T)a maig ) VALUE C.LONG T t2a QAaV RG. VALUE (I) CONCENTRATION (2) MASS CONCENITRATION (2) MASS (I) CONCENTRATION (2) MASS d.NO. of ANAL- YSES 4. UNITS a. LONCEN-i "RATION b. MASS 5. INTAKE (optional) a. LONG TERM AVERAGE VALUE (1) CONCENTRATION 12) MASS b.NO. OF ANAL. YSES Bromide 24959-67-9) * Chlorine, -otal Residual . Color Fecal iioliform * * * Fluoride 1698 4.48.8 ) . Nitrate— Jitrite (as N) * .3 .3 .2 4 _ mg/L EPA Form 3510-2C (Rev. 2-85) * No Sampling Required PAGE V-1 CONTINUE ON REVERSE ITEM V-B CONTINUED FROM FRONT I. POLLUT- ANT AND CAS NO. (if available) 2. MARK 'X' 3. EFFLUENT a. BE- RIEV EDLIEV PRE- SENT b.BE- ED AB SENT a, MAXIMUM DAILY VALUE b. MAXIM M 3a 4p{p�Y VALUE ()�QUQiQQbie) [ C.LONG TERM �Mp�•/j+' VALUE I aUQi Q e dam ) ' Id CONCENTRATION MASS II) II)I2I CONCENTRATION (2) MASS _ (I) CONCENTRATION (2) MASS . Nitrogen, 'otal Organic as N) * L - I. 011 and 3rease * Phosphorus as P), Total 7723-14-0) * Radioactivity 1) Alpha, ota1 * 2) Beta, otal * 3) Radium, otal * 4) Radium 26, Total Sulfate * . s SO4) 14808-79-8) Sulfide la S) i. Sulfite * Is S03) 14265-45-3) . * . Surfactants Aluminum, * . otal 1429-90-5) Barium, * otal 7440-39.3) Boron, * otal 7440-42-8) Cobalt, * otal '440.48-4) * Iron, Total '439-89-6) * Magnesium, otal 7439-95-4) Molybdenum, otal 7439-98.7 ) Manganese, * otal 7439-96-5) * . Tin, Total 7440-31-5) Titanium, * . otal i 440-32-6 ) -2C (Rev. 2- PAGE'V-2 d, NO.OF ANAL- YSES 4. U a. CONCEN- TRATION IT b. 5 5.INTAKE(optional) MASS R A0EL)Ara A UE b. NO.OF ANAL - YSES II) CONCENTRATION (2) MASS * No Sampling Required CONTINUE ON PAGE V -3 ' CONTINUED FROM PAGE 3 OF FORM 2-C EPA I.D. NUMBER (copy from Item 1 of Form 1) NCD053488409 OUTFALL NUMBER 002 , • Form Approved. OMB No. 2000.0059 Approval expires (2-31.85 , PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfaffs, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER (ifavailable) 2. MARK .x. 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a.TEST- ING ING RE- iQ b. BE- LIEV EO PRE- SENT C. sE- LIEVE� AB- SENT 8. MAXIMUM DAILY VALUE b. MAXIMt.JM 30 (tf aU6 gra� VALUE a e C.LONG T 17M AVRG. VALUE tii oUa a e ) d NO.OF a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO.OF ()) CONCENTRATION (2)MASS (I) CONCENTRATION (�) MASS / 0) CONCENTRATION I2) MASS ANAL- ANAL- YSES (I TRATIO�NN (J,l MA55 gNAL- YSES METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony, Total (7440-36.0) * 2M. Arsenic, Total (7440.38-2) * 3M. Beryllium, Total, 7440-41-7) * 4M. Cadmium, Total (7440-43-9) * 5M. Chromium, Total (7440-47-3) * 6M. Copper, Total (7440-50-8) * 7M. Lead, Total (7439-92-1) * 8M. Mercury, Total (7439-97-6) * 9M. Nickel, Total (7440.02.0) * 10M, Selenium Total (7782-49-2) * 11M. Silver, Total (7440-22-4) * 12M. Thallium, Total (7440-28-0) * 13M. Zinc, Total (7440-66-6) X .5 .5 .5 .5 .2 .14 4 mg/L lb/day 14M. Cyanide, Total (57-12-5) * 15M. Phenols, Total * DIOXIN 2,3,7,8-Tetra- chlorodlbenzo-P- Dioxin (1764-01-6) * DESCRIBE RESULTS EPA Form 3510-2C (Rev. 2-85) * No Sampling Required PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT `1. POLLUTANT AND CAS NUMBER (if available) 2. MARK 'X' - 3. EFFLUENT 4. UNITS 5, INTAKE (optional)_ aTEST• ING Rt- oulR- b. BE- LIEVEOLIEVEn PRE- sENt C. BE- a. MAXIMUM DAILY VALUE b. Mf.XI M 3 I QUa pp Y VALUE Q ¢ bl lavailable)' C.LONG ?rem A R VALUE 1 d. NO.OF ANAL- ANAL- YSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALVE b.NO.OF ANAL- YSESEO Ae- SENT 11) CONCENTRATION (x) MASS 111 CONCENTRATION _ (xl MAsS I11 CONCENTRATION Ill MA55 (1) CONCEN- TRATION IZ) MASS GC/MS FRACTION — VOLATILE COMPOUNDS L 1 V. Acrolein (107-02-8) 2V. Acrylonitrile (107-13-1) * 3V. Benzene (71-43-2) * 4V. Bis (Chloro- methyl) Ether (542-88-1) 5V. Bromoform (75-25-2) * 6V. Carbon Tetrachloride I (56-23-5) 7V. Chlorobenzene (108-90-7) * — 8V. Chlorodi- bromomethane (124.48.1) - 9V. Chloroethane (75-00-3) * 10V. 2-Chloro- ethylvinyl Ether (110-75-8) 1 11V. Chloroform (67-66-3) * 12V. Dichloro- bromomethane (75-27-4) 13V. Dichloro- difluoromethane (75-71-8) * 14V. 1,1-Dichloro- ethane (75-34-3) * 15V. 1,2-Dichloro-� ethane(107-06-2) * 16V. 1,1-Dichloro- ethylene (75-35-4) * 17V. 1,2-Dichloro- propane (78-87-5) * 18V. 1,3-Dichloro- propylene (542.75-6) * 19V. Ethylbanzene (100-41-4) * 20V. Methyl Bromide (74-83-9) * 21V. Methyl Chloride (74-87-3) * - - __ - EPA FnrmAMn_91^ in.., .3_ocl * No Samn1 in¢ Recrlli_red CONTINUE ON PAGE V- CONTINUED FROM PAGE V-4 EPA I.D. NUMBER CO rom Item 1 of Form 1) OU rFALL NUMBER NC�DO53488409 002 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK 'X' &TEST- ING R E- QUIP- EO b. BE- LIEV EO PRE- SENT C. BE- LIevEn SENT a. MAXIMUM DAILY VALUE (I) (2) MASS CONCENTRATIONI GC/MS FRACTION — VOLATILE COMPOUNDS (continued) 3. EFFLUENT b. MAXIMj.IM 30 DAY VALUE Of available) (I) CONCENTRATION (2) MASS C.LONG T 1•t M1Aab1e)• VALUE (1) CONCENTRATION (2) MASS d NO.OF ANAL- YSES 4. U a. CONCEN- TRATION OMB No. 2000-0059 Approval expires 12-31-85• NITS 5. INTAKE (optional)' b. MASS a. LONG TERM AVLRAGF,VALVE (I) CONCEN- I (a) MASS TRATION' b. NO.OF ANAL- YSES 1 22V. Methylene Chloride (75-09-2) * 23V. 1,1,2,2-Tetra- chtoroethane (79-34-5) * 24V. Tetrachloro- ethytene (127-18-4) * I 25V. Toluene (108-88-3) * * 26V. 1,2-Trans- Dichloroethylene (156-60-5) * _ l 27V. 1,1,1-Tri- chloroethane (71-55-6) * 28V. 1,1,2-Tri- chtoroethane (79-00-5) * 29V. Trichioro- ethylene (79-01-6) * 30V. Trichloro- fluoromethane (75-69-4) * r • 31V. Vinyl Chloride (75-01-4) * GC/MS FRACTION — ACID COMPOUNDS 1A. 2-Chlorophenol (95-57-8) * 2A. 2,4-Dichioro- phenol (120-83-2) * 3A. 2,4-Dimethyl- phenol (105-67-9) * 4A. 4,6-Dinitro-O- Cresol (534-52-1) * 5A. 2,4-Dinitro- phenol (51-28-5) * 6A. 2-Nitrophenol (88-75-5) * 7A. 4-Nitrophenol (100-02-7) * 8A. P-Chloro-M- Cresol (59-50-7) * 9A. Pentachloro- phenol (87-86-5) * 10A. Phenol (108-95-2) * 11A. 2,4,6-Tri• chlorophenol (88-06-2) * CONTINUED FROM THE FRON 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK 'x' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) &TEST- INO QUER• b. et- LIEVEOLIEVEN se°ir G me- a. MAXIMUM DAILY VALUE P. MAXIMI.1M 3l) DAY VALUE t avaI Ote) C.LONG Tg�p�2tm AAVRRGG VALUE (ttavailable)' d.NO.OF ANAL- USES a. CONCEN- TRATION b. MASS AVa. LONG ERAGE=VALVE b. NO.O' ANAL- YSES YSES se°IT (I) CONCENTRATION (t) MASS CONCE NITA ATION (2) MA55 (Ii ({) MASS (I) CONCEN- TR AYION (_) MAtB GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS r 18. Acenaphthene (83-32-9) * . 28. Acenaphtylene (208-96-8) * 3B. Anthracene (120-12-7) * 4B. Benzidine (92-87-5) * 58. Benzo (a) Anthracene (56-55-3) —' J" 6B. Benzo (a)• Pyrene (50-32-8) * 7B. 3,4-Benzo- fluoranthene (205-99-2) * 8B. Benzo (ghl) Perylene (191-24-2) * 9B. Benzo (k) F luoranthene (207-08-9) 10B. Bis (2-Chloro- ethoxy) Methane (111-91-1) * 11 B. Bis (2-Chloro- ethyl) Ether (111-44-4) * * 128. Bis (2-Chloroiso- propyl) Ether (102.60-1) 13B. Bis (2-Ethyl- hexyl) Phthalate (117-81-7) * - 148. 4-Bromo- phenylPhenyi Ether (101-55-3) * 15B. Butyl Benzyl Phthalate (85-68-7) * 166. 2-Clito ro- naphthalene (91-58-7) * 17B. 4-Chloro- phenyl Phenyl Ether (7005-72-3) * J 18B. Chrysene (218-01-9) 19B. * Dibenzo (a,h)t Anthracene (53-70-3) * 20B. 1,2-Dichloro- benzene (95-50-1) * 21B. 1,3-Dtchioro- i benzene (541-73-1) * EPA Form 3510-9C !Rau 9-I:R1 * No Sampling Required AGE V-6 CONTINUE ON PAGE V s CONTINUED FROM PAGE V-6 EPA I.D. NUMBER (copy from Item 1 of Form 1) NCD053488409 OUTFALL NUMBER 002 Form Approved. OMB No. 2000-0059 Approval expires 12-31-85 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) - a .TEST• ING pI11R- :IN.- EO b. eE• LIEVEouEVEq ►R E- SCNT C. SE- we• /ENT 8. MAXIMUM DAILY VALUE - b. MAXIM M 30 DAY VALUE (+�aaaiQag�) C.LONG T M AA��[[RR(G' VALUE �avatlafjie' d. NO.OF ANAL.b. YSES a. CONCEN- TRATION MASS a. LONG TERM AVERAGE VALUE b. NO.OI ANAL* YSES ill CONCENTRATION (2) MASS II) CONCENTRATION (2) MASS III CONCENTRATION I.) MASS (1) CONCEN• TNATION I2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued' 22B. 1,4-Dichloro- benzene (106-46-7) * 23B. 3,3'-Dichloro- benzidine (91-94-1) * 24B. Diethyl Phthalate (84-66-2) * 25B. Dimethyl Phthalate (131-11-3) * 26B. DI-N-Butyl Phthalate (84-74-2) * 278. 2,4-Dinitro- toluene (121-14-2) * 28B. 2,6-Dinitro- toluene (606-20-2) * 29B. Di-N-Octyl Phthalate (117-84-0) 30B. 1,2-Diphenyl- hydrazine (as Azo- benzene) (122-66-7) * 318. F(uoranthene (206-44-0) * 328. Fiuorene (86-73-7) * 33B. Hexachlorobenzene (11R-74-11 �34B. * Hexa-. chlorobutadiene (87-68-3) * 35B. Hexachloro- cyclopentadiene (77-47-4) * 368. Hexachloro- ethane (67-72.1) * 37B.Indeno (1,2,3-cd) Pyrene (193-39-5) * 38B. 1 sophorone (78-59-1) * 39B. Naphthalene (91-20-3) * 40B. Nitrobenzene (98-95-3) * + 41B. N-Nitro- sodimethylamine (62-75-9) 42B. N-Nltrosodi- N-Propylaniine 621-64-7) * CONTINUE ON REVEF CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (if available) GC/MS FRACTION 2. MARK 'X' 3. EFFLUENT a .TEST- b. BE- c BE- ING LIEVEOLIEVE4 RE- PRE- Ae- OVIR• SENT SENT co — BA SE/NE UTRAL a. MAXIMUM DAILY VALUE (I) (E) MASS CONCENTRATION COMPOUNDS (continued) b. MAXIMUM 39 DAI VALUE (I) (2) MASS CONCENTRATION 4. UNITS C.LONG T}7 atlabl) - VALUE CONCENTRATION (1) MASS (1. NO.OF ANAL- YSES 43B. N-Nitro- sodiphenylamine (86-30-6) 44B. Phenanthrene (85-01-8) 458. Pyrene (129-00-0) * * * 46B. 1,2,4- Tri- chlorobenzene (120-82-1) GC/MS FRACTION * a. CONCEN- v MASS TRATION 5. INTAKE (optional) a. LONG TERM AVERAGE VALUE (I) CONCEN• TRATION (a) MASS h. NO. ANA. YSE' — PESTICID ES 1P. Aldrin (309-00-2) * 2P. a-OHC (319-84-6) 3P. 13-BHC (319-85-7) * * 4P. 7-BHC (58-89-9) * 5P. S-BHC (319-86-8) * 6P. Chlordane (57-74-9) * 7P, 4,4'-DDT (50-29-3) 8P. 4,4'-DDE (72-55-9) * * 9P. 4,4'-DDD (72-54-8) 10P. Dieldrin (60-57-1) * * 11P. a-Endosulfan (115-29-7) * 12P. Q-Endosu'fan (115-29-7) * 13P. Endosulfan Sulfate (1031-07 -8 ) 14P. Endrin. (7 2-2 0.8 ) 15P. Endrin Aldehyde (7421-93-4) * * * 16P. Heptachlor (76-44-8) * EPA Form 3510-2C (Rev. 2-85) * No Sampling Required PAGE V-8 CONTINUE ON PAGE V. CONTINUED FROM PAGE V-8 EPA I.D. NUMBER (copy from Item 1 Of Form 1) NCD053488409 OUTFALL NUMBER 002 1. POLLUTANT AND CAS NUMBER a .TEST. b. BC- C. OE- a. MAXIMUM DAILY VALUE ING LIEVEOLIEVE'Z (if available RE- PRE- An- QUIP- SENT SENT II) (z) MASS Eo CONCENTRATION GC/MS FRACTION — PESTICIDES (continued) 2. MARK 'X' 17P. Heptachlor Epoxide (1024-57-3) * 3. EFFLUENT b. MAXIMUM 3e, PAY VALUE or ava tabtee) (1) CONCENTRATION (z) MASS C.LONG T 7 a allai! J . VALUE (I) G14) MASS CONCENTRATION i1 NO.OF ANAL- YSES Form Approved. OMB No. 2000-0059 Approval expires 12.31.85 4. UNITS e. CONCEN- TRATION b. MASS 5. INTAKE (optional) a. LONG TERM AVERAGE VALUE (1) CONCE N- tz) MAss TWATION b. NO.OF ANAL- YSES 18P. PCB-1242 (5 3469-21-9 ) 19P, PCB-1254 (11097-69.1) * 20P. PCB-1221 (1 1104-28 -2 ) * 21P. PCB-1232 (11141-16-5) * 22P. PCB-1248 (12672-29-6) * 23P. PCB-1260 (1 1096-82-5 ) * 24P. PCB-1016 (12674-1 1-2 ) * 25P. Toxaphene (8001-35.2 ) * EPA Form 3510-2C (Rev. 4-84) * No Sampling Required PAGE V-9 EPA Form 3510-2C /Rev. 2-85) FORM 2C SUPPLEMENTARY INFORMATION ITEM II. B: Outfall 001: Sanitary wastewater flows to a pumping station equipped with a comminutor, a bar screen bypass and a Parshall flume for flow recording. Waste is pumped to the aeration basin, entering about 40 feet from the process waste influent point. Fiber finish oil, which is primarily composed of fatty acid esters, organo-silane esters, and alkylamine, oleate and trioleate emulsifiers, is segregated from other process waste for pretreatment. An ultrafiltration unit is used to separate the oil from the water. The water is pumped to the wastewater treatment plant and the oil is burned on -site for energy recovery. Process wastewater flows to a pumping station equipped with a manually cleaned bar screen and a Parshall flume for flow recording. It is pumped to a 1200 gallon mixing chamber which allows for pH adjustment. During emergencies, the flow can be diverted to a 600,000 gallon holding pond. The aeration basin has a volume of approximately 650,000 gallons and is equipped with four (4) 20 HP floating aerators. The waste then flows to a 20 feet diameter clarifier with a design overflow rate of 440 gallons per square foot per day. A surface skimmer and holding sump are provided. Pumps are provided to return settled sludge to the aeration basin or to a sludge drying bed. Clarifier overflow is piped to a one acre polishing pond operating at a 3 foot depth or directly to the chlorine contact chamber . A .4 acre alum settling pond is provided for the potable water plant backwash and blowdown. The clarified discharge from the alum pond is pumped to the polishing pond. Effluent from the polishing pond flows through a 3600 gallon retention chamber for chlorine disinfection. A V-notch weir at the effluent end of the chamber provides for flow recording. Approximately 130,000 pounds of sludge is wasted during the year to a sand drying bed. Wastewater that drains through the sand is pumped back to the aeration basin. Wasted sludge is either landfilled at the Sampson County Landfill or recycled by Cherokee in brick manufacturing. Outfall 002: This drainage system includes a series of baffles and weirs designed to contain accidental spills of oil and Dowtherm. In an emergency, flow can be contained in a holding pond and pumped to storage or pumped to the process sewer. Storm water runoff from most of the manufacturing areas and chemical storage areas of the plant is discharged through permitted outfalls 001 and 002. Storm water runoff from other areas of the plant that are associated with industrial activity discharge through four storm water outfalls that are covered by NPDES Permit No. NCS 000100. ITEM III. A&B: On November 5, 1987 EPA issued regulations establishing effluent limitations for the Organic Chemicals, Plastics, and Synthetic Fibers (OCPSF) industrial category. Provisions of Subpart C (414.31) and Subpart I (414.90) Direct Discharge Point Sources That Use End -of -Pipe Biological Treatment are applicable to process wastewater discharges from the manufacture of polyester fiber and resin. OCPSF effluent guidelines are not expressed in terms of production. No metal -bearing waste streams or cyanide -bearing waste streams listed in Appendix A to Part 414 exist in the manufacture of polyester fiber and resin. ITEM V. A-C Wastewater characteristics tabulated in item V reflect data from the period August 1, 1994 to July 31 1995. For some parameters, testing was conducted throughout the year and for other parameters annual testing was conducted. Special tests were conducted for most of the parameters. Bis-chloro-methyl ether(FR 2-4-81), dichlorodifluoromethane(FR1-1-81) and trichlorofluoromethane(FR 1-8-81) have been dropped from the 2C GC/MS Fraction -Volatile Compound list by the EPA. ITEM V. D: This list is as complete as possible; however, since some manufacturers consider their products proprietary they will not release information on the specific composition. Therefore, there may be other materials on the plant site that contain one or more of the chemicals in Table 2C-3. In addition, new materials may be obtained that may have one or more of the chemicals listed and whose compositions may or may not be known. ITEM VI: The following is a list of Part V. C pollutants that are present on the plant site. None of these materials are used as a raw material or intermediate and none of these materials are manufactured as a product or a by-product of the manufacturing process. The list may not be exhaustive because some commercial products are considered proprietary by the manufacturer and their specific composition is not known to us. In addition, some new materials may be obtained in the future that contain one or more of the listed chemicals and whose composition may not be known to us. Pollutant Antimony Chromium Copper Lead Mercury Nickel Silver Zinc Phenols Carbon Tetrachloride Chloroform Dichlorodifluoromethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,1,1-Trichloroethane Trichloroethylene Phenol Dichlorobenzene 1,2,4-Trichlorobenzene PCB Use on Site Lab Reagents Lab Reagents Lab Reagents Lab Reagents Lab Reagents, Instrumentation Lab Reagents Lab Reagents, Electrical Equipment Lab Reagents Lab Reagents Lab Reagents Lab Reagents Lab Reagents, Refrigerant, Leak Checks Lab Reagents Solvent Lab Reagents Solvent Solvent Lab Reagents Lab Reagents Electrical Equipment Electrical Equipment ITEM V. Part C: IIV. Chlorinated Organics (trihalomethanes) Chlorinated organics (bromoform, dibromochloromethane, and bromodichloromethane) were detected in the Outfall 001 effluent. Positive results were expected based on studies conducted in 1988 and 1989 on OCPSF process related wastewater sources, wastewater treatment plant influent, clarifier overflow and effluent. The studies focused on the formation of trihalomethanes in wastewater using chloroform as the tracking compound. Sampling showed that choroform was not detected in either the OCPSF process related wastewater sources or the clarifier overflow. However, chloroform was detected in the influent due to the chlorination of river water at the plant's drinking water treatment plant and it was detected in the effluent due to chlorination prior to discharge. The results of the studies conducted in 1988 and 1989 have been further confirmed by the past year of quarterly choroform results at the clarifier overflow. All chloroform results have been less than 0.5 µg/L (ppb). Chloroform is used in the Quality Control Laboratory for product testing, but handling procedures require that all waste solvent be placed into a hazardous waste drum for off -site incineration at an EPA approved facility. AlliedSignal requests that chloroform monitoring continue to be required on clarifier overflow and not effluent from the chlorine contact chamber. APPENDIX A CHEMICAL INVENTORY The attached is a listing of process and non -process chemicals used at the plant. Many of these chemicals are not routinely monitored for and are not normally present in our discharge, but they could at times appear as a result of events beyond our control. APPENDIX A PROCESS CHEMICAL INVENTORY RAW MATERIALS Ethylene Glycol Terephthalic Acid CATALYSTS Antimony Trisethylene Glycoxide Titanium Chelate PROCESSING AID Diisopropylamine Dow Corning Antifoam Polyphosphoric Acid PRODUCTS Polyethylene Terephthalate (Polyester) BYPRODUCTS Aldehydes (i.e., acetaldehyde & crotonaldehyde) Diethylene Glycol Spent Ethylene Glycol 1,4-Dioxane FINISH OIL COMPONENTS Intracid Scarlet Tint Mineral Oil Silane 187 Coconut Oil Sulfonated Glycerol Trioleate Polyoxyethylene Alkylamine Silicone Emulsion Laurylether Octylphenoxy Polyethoxy Ethanol Glycerol Monooleate Sulfonated Aliphatic Polyester Aqua Hue Yellow Tint Phosphate Anistat N-Tetradecanol N-dodecanol Isobutyl Stearate Aqua Hue Blue Tint Cocamine Ethoxylate Isocetyl Stearate FINISH OIL COMPONENTS (cont.) Decaglycerol Giv-Gard DXN Petrusol L-60 Polyethylene Glycol Monotallate R & D CHEMICALS A pilot plant is operated at the site for research and development work. This work periodically involves the use of small quantities of a variety of chemicals as polymer ad ditives and finish components. MSDS Index - Sorted by Product II-Aug-95 (dent Product Company Date 0931 0809 1180 0903 1150 1084 0971 0565 0566 0567 0988 0551 1026 0395 0028 0203 0744 0204 0986 0205 0494 uyu1 0359 1156 1123 0717 0074 0331 0804 0991 1163 0465 0948 0042 0737 0738 0736 1-Propanol 1065/5046/5047/5065 Dry Ink 245 Conductivity Standard 460 294S - EZE 915D Cleaning Fluid A-100 Flat Latex House & Trim A-100 Gloss Latex House Paint A-100 Stain & Finish B22 R 1 R A-187 A-9 A-970 Spinneret Lubricant Absolute Strip Accudri SF6 Acetic Acid, Glacial Acetone Acetone Acetone Acetonitrile Acetylene Acidproof Concrete - No. 54L Activator, 1 Gal 707, Item 7077 Adhesive 520 Adhesive Sealant No. 242 Adhesive/Sealant 290 Afilan AICS Afilan HDS Afilan ICS Afilan ICS Afilan PP Al-30 Air Jet II (Anti -Static) Airco Marvel 162 Alcad and Cladding Products - Alcad and Cladding Products - Alclad and Cladding products - Fisher Scientific Xerox Corporation Betz EZE Products Meriam Instrument Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company OSi Specialties Incorporated Relton Corporation Stoner lncorporated Maintenance Supply Company, Allied Signal Fisher Scientific Allied-Signal Fisher Scientific McKession Chemical Corporati Fisher Scientific National Welders Sauereisen Cements Company Loctite Corporation Armstrong World Industries Loctite Corporation Loctite Coproration Hoechst Celanese Corporation Hoechst Celanese Corporation Hoechst Celanese Hoechst Celanese Corporation Hoechst Celanese Asinco Incorporated GC Thorsen American Solder & Flux Co., In Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company 3/3/94 9/22/86 7/24/91 6/18/92 4/29/92 3/20/86 3/24/86 3/21/86 6/7/95 12/10/93 2/1/93 3/4/93 1/1/89 11/2/93 1/1/89 11/2/93 2/14/86 11/2/93 11/25/85 11/1/85 8/19/93 8/7/90 11/1/85 8/19/93 4/19/94 7/6/93 7/6/93 3/5/93 9/6/94 9/28/92 5/10/93 2/7/92 9/24/93 9/24/93 9/24/93 1 (dent Product Company Date 0055 1136 Alizarine Green BB Liquid 25% 0343 Alkaline Cleaner 8755 0206 Alkaline Iodide Sodium Azide S 0387 Almasol High Temp Lubricant 1 0298 Alum (Dry) 0876 Alumina Grade A 0926 Aluminum Alloy Series 1000,20 0539 Aluminum Asphalt Roof Coatin 1124 Aluminum Filled Plastic Filler 0142 Aluminum Liquid (F-2) - Resin 0143 Aluminum Putty (F) - Resin 0149 Aluminum Putty Hardener (Putt 0923 Alusa 0316 Aluver 3 Aluminua Reagent 1019 Amino Acid Reagent 0207 Ammonium Hydroxide 0208 Ammonium Phosphate 0779 Amoco Syntholube Polybutean 0892 Amoco TA-33 LP 0043 Amoco TA-33 MP (Purified Ter 0510 Anderol ** 500 OIL 0255 Antimony Potassium Tartrate 0211 Antimony Reference Standard 0389 Antimony Trisethylene Glycoxi 0368 Antiseize Thread Compound P 0040 AO Superclear Lens Cleaning F 0041 AO Superclear Lens Cleaning F 1155 AP Armaflex and Armaflex II 0139 Apexior #1 0140 Apexior No. 3 1170 Aqua Hue Blue BGG 9521 1169 Aqua Hue Red BR3B 0477 Aqua Hue Red BR3B 0894 Aqua Hue Yellow B2G 0463 Aqueous Prylog Adhesive Activ 0495 Argon 0648 Ascarite II 0317 Ascorbic Acid 0056 Atanyl Green GN Liquid Alizarine Green BB 12 1/2% Liq Crompton and Knowles Incorpo Crompton and Knowles EZE Products Incorporated Fisher Scientific Lubrication Engineers, Inc. General Chemical Corporation C. M. Kemp Manufacturing Co Marmon/Keystone Corporation Courtaulds Coatings Dynatron/Bondo Corporation Devcon Corporation Devcon Corporation Devcon Corporation Harbison -Walker Refractories Hach Company Betz Laboratories Fisher Scientific Fisher Scientific Amoco Amoco Chemical Company Amoco Nuodex Inc. Fisher Scientific Fisher Scientific M & T Chemicals Loctite Corporation Cabot Safety Corporation Cabot Safety Corporation Armstrong World Industries Dampney Co., Inc. Dampney Co., Inc. Blackman Uhler Blackman Uhler Blackman Uhler Chemical Divis Blackman -Uhler AlliedSignal National Welders Thomas Scientific Hach Company Crompton & Knowles Corporati 7/23/93 7/23/93 2/16/94 6/14/89 7/13/93 12/1/93 11/1/91 1/1/93 3/11/90 8/25/88 6/10/92 5/11/92 5/11/92 10/1/84 4/22/93 5/13/93 11/2/93 11/2/93 9/20/93 5/17/93 8/26/93 3/30/92 11/2/93 11/2/93 9/6/88 8/19/93 7/1/92 11/10/92 4/4/91 10/1/93 10/1/93 8/6/93 8/6/93 4/5/91 9/8/92 3/1/95 11/25/85 1/4/93 4/15/93 7/23/93 2 Ident Product Company Date 0802 ATL Brill Crocein Scarlet M 0854 Atlantic Brilliant Croceine Scar! 0745 Aura Dishwashing Compound 0998 Aviation Form -A -Gasket #3 800 0061 B Line Anti -Spat Bering B1620 1038 B'Laster Penetrating Catalyst 0491 Balanced Polymer 64Y74 0541 Ballotini Impact Beads 0109 Bar Belt Dressing #10073/#100 0885 Bare Knuckles Ultra Stripper 0277 Barium Chloride 0960 Barium Chloride, dihydrate 0448 Barrage Industrial Strength Bo 1113 Barrierta L 55/2 1051 Basic Violet 10 - Bingo Marker I 0060 Bausch & Lomb Anti -Fog Liquid 0360 Bearing/MT/ADH Sealant 10 M 0615 Belt Dressing 00607 0213 Benzoic Acid 0180 Bis(2-(2-Methoxyethoxy)ethy!) 0185 BL-15 Cell Fluid 0626 Black & Decker Band Saw Gea 0686 Black Developer Part No 5R15 1097 Blazer Torch Model GB-2001 0318 Bleaching 3 Reagent 0412 Blue Fluid #175 0855 Blue Fluid #200 0657 Blue P/N 03/00-00-067427 1037 BOLD Dust Control Treatment 0154 Boraxo Powdered Hand Soap 0396 Bottom Layer 0322 Brazing Fluxes Stay Silv White 0257 Bromocresol Green 0215 Bromocresol Purple, Sodium S 0980 Bromophenol Blue, A.C.S. Rea 0278 Bromothymol Blue 0188 Bronzochrom 10185 0663 Brown Aluminum Oxide 0621 BSTFA,25ML 1072 BuCAIM Low Na+ Liquid Causti Crompton & Knowles Corporati Atlantic Industries, INc. Calgon Corporation Loctite Corporation Bearing Sales Inc. William K. Westley Company Betz Potters Industries Cling Surface Company Butcher Company Fisher Scientific Fisher Scientific National Laboratories Kluber Lubrication Corporation Keystone Aniline Corporation Bausch & Lomb Loctite Corporation Sprayon Products Fisher Scientific Fisher Scientific Emery, A. H., Company Tech-Lube Corporation Xerox Corporation Premier Industrial Corporation Hach Company Meriam Instrument Meriam Instrument VDO instruments Butcher Company Dial Corporation Maintenance Supply Company, Harris, J. W., Co., Inc. Fisher Scientific Fisher Scientific Aldrich Chemical Company Fisher Scientific Eutectic Corporation Washington Mills Electro Miner Supelco Inc. Baker, J.T. Incorporated 4/3/94 9/28/90 6/24/94 7/1/94 7/17/92 2/19/91 11 /1 /87 5/1/93 11/2/93 2/11/93 5/27/87 7/3/90 2/26/92 8/19/93 8/19/88 11/2/93 8/24/86 10/14/92 1 /1 /93 1/27/89 1/11/93 4/22/93 2/28/94 10/18/93 4/1/92 4/24/92 3/3/93 6/1/92 5/17/94 11/2/93 8/1/90 11/2/93 3/15/93 9/1/93 7/6/94 5/29/91 3 (dent Product Company Date 0695 Buffer Powder Pillows, Citrate 0848 Buffer Solution (pH 10) 0961 Buffer Solution - pH 4.0 0958 Buffer Solution - pH 7.0 0849 Buffer Solution pH 7.0-8.0 0217 Buffer Solutions 0397 Buffing Polish 0873 Butyl Stearate 0285 C. I. Mastic (Spray) 0286 C. I. Mastic (Trowel) 0259 Calcium Carbonate 0219 Calcium Chloride 0959 Calcium Chloride, Dihydrate 1018 Calcium Indicator 1178 Calibration Gas Mixture 0086 Caplube 8337 0085 Caplube 8369 0929 Carbon and Alloy Steel AISI/SA 0279 Carbon Black 0047 Carbon Dioxide 0496 Carbon Dioxide 0221 Carbon Tetrachloride 0010 Carboxybenzaldehyde (4- 1062 Carpet and Upholstery Cleaner 1060 Carpet Extraction Cleaner - Ne 0769 Castoglas Hardner 0770 Castolite AP Resin 0828 Catalyst S-21 Antimony Triacet 0934 Catalyst S-24 0669 Catalyst/Thinner - Sales Code: 0009 Caustic Potash 1078 Caustic Potash Standard Flake 1081 Caustic Soda 50% and 73% 0801 Caustic Soda Liquid 0114 Caustic Soda Liquid 50% 0619 Caustic Soda Liquid 50% 1039 Cement - Heavy Duty Clear Sol 1016 Certainium 601 1/8 0907 Certanium 34C 1/16 Tube Sold 0093 Certanium 707-SP Hach Company Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Maintenance Supply Company, Henkel Corporation Fuller, H. B., Company Fuller, H. B., Company Fisher Scientific Fisher Scientific Fisher Scientific Betz Laboratories Supelco Capital City Products Company Karlshamns - Lipid Specialists Marmon/Keystone Corporation Fisher Scientific Ansul Fire Protection National Welders - Cardox Fisher Scientific Aldrich Chemical Company Defender Services Defender Services Polymer Additives Group Reichhold Chemicals Atochem North America Elf Atochem North America DuPont Alcad Inc. Occidental Chemical Vulcan Chemicals Van Waters & Rogers Inc. Continental Industries Suffolk Chemical Company Oatey Company Certanium Alloys and Research Certanium Alloys and Research Certanium Alloys & Research C 6/9/93 11/2/93 3/23/93 5/17/94 11/20/91 11/2/93 1/1/92 4/1/90 8/19/93 8/19/93 11/2/93 11/2/93 9/18/92 10/12/92 10/4/94 3/3/86 1/1/91 1 /1 /93 5/17/94 1/25/93 9/1/93 11/2/93 8/18/93 1/1/92 6/1/93 8/2/93 8/23/93 5/5/93 7/8/91 11/19/90 8/17/90 5/30/89 3/1/93 7/21/87 8/30/86 6/1/94 12/8/93 1/5/92 1/5/92 4 Ident Product Company Date 0906 Certanium 934 Soldering Flux 0909 Certanium PMC Prep -Clean 0094 Certaspray 2040 1077 Cesco CS-700 AM 1080 CG8, CG8-C, CG8-F, CG8-UP 0067 CGR #30 Packing 0095 Channel Master Contact Sheild 0908 Chem Weld 20707 0697 Chembuild Series 135 0889 Chemgrate Chemgrit Chemtred 0678 Cheveron AW Hydraulic Oil 68 0682 Chevron AW Hydraulic Oil 32 0677 Chevron AW Hydraulic Oil 46 0684 Chevron Delo 400 Plus Motor 0681 Chevron Dura-Lith Grease EP 0680 Chevron MW Fluid 31C 0665 Chevron Soluble Oil B 0679 Chevron Ultra -Duty Grease 1 0137 CHICO A Sealing Compound 0138 CHICO X Fiber 0872 Chisel Gasket Remover 0497 Chlorine 0660 Chlorine Liquified Gas 0945 Chlorine Solution 0261 Chloroform 0989 Chloroform - Technical 0054 Chloroform Technical 0927 Chrome Plated Carbon Steel 1 0979 CITGO High Sulfur No. 2 Fuel 0078 CITGO No. 2 Diesel Fuel 0935 CITGO No.2 Diesel Fuel 0403 Citric Acid 0762 Citrikleen XPC 0369 Clean Up Solvent For Instant A 0358 Cleaner Detergent, Sun Light 0113 Cleaner, Ajax 0870 Cleaner-Window/Glass Sesco 0826 Cleaner/Degreaser MNB 0505 Clear Cement #999125 0111 Clover Silicon Carbide Grease Certanium Alloys and Research Certanium Alloys and Research Certanium Alloys & Research C Browning -Ferris Industries ResinTech Incorporated CGR Products, Inc Channel Master, Division of Av Certanium Alloys and Research Tnemec Company, Inc. Chemgrate Corp Chevron Chevron Chevron Chevron Chevron Chevron Chevron Chevron Crouse -Hinds ECM Div. Coope Crouse -Hinds EMC Div. Coope Loctite Corporation National Welders Van Waters & Rogers Inc. Hach Company Fisher Scientific AquAir Corporation Ashland Chemical Company Marmon/Keystone Corporation CITGO Petroluem Company CITGO Petroleum Corporation CITGO Petroleum Corporation Mallinckrodt Penetone Corporation Loctite Corporation Lever Brothers Colgate-Palmolive Cello Corporation Mop-N-Bucket Janitorial Supply New Hermes, Inc. FeI-Pro Incorporated 1/5/92 1/5/92 3/25/93 3/11/94 7/14/88 9/2/92 2/13/92 11 /1 /90 5/10/91 2/27/92 2/27/92 2/27/92 9/6/90 3/3/92 3/20/92 1/16/91 3/18/92 7/1/92 3/1/93 7/1/94 12/22/88 7/21/92 11/2/93 11/1/84 5/25/94 1/1/93 9/22/93 11/4/93 11/4/93 12/29/86 6/14/89 8/19/93 2/11/92 10/4/93 2/18/92 4/1/93 10/8/93 5 (dent Product Company Date 0066 Coconut Oil 76 0476 Colilert Comparator 0475 Colilert Reagent 0814 Command Center Neutral Floor 0347 Complete 0504 Compressed Air 1095 Conducto-Pen P.C. Board Pen 0069 Contact Cleaner (Aerosol) #307 1149 Continuum 29K-29137 0973 Contiuum - 29137 0871 Convoy Parasynthetic Motor Oi 0115 Cool -Amp 0492 Copaltite 0741 Copper - Sheet, Plate, Rod, Ba 0761 Copper Sulfate Pentahydrate 0291 Corona Dope 0292 Corona Dope (Aerosol) 1173 Corr -Shield 736 1130 CP-9 Ak-Cryl(TM),CP-10/11 Vi- 0068 CRC Contact Cleaner (Aerosol) 0011 Cresol Red, Indicator Grade 0121 Cronabraze 21 - Brazing Wire 0122 Cronabraze 30F - Alloy Wire 0123 Cronabraze 55 - Alloy Wire 0124 Cronabraze 99 (CW 1026) 0125 Cronacast 211 - Welding Electr 0126 Cronacast 222 - Welding Electr 0127 Cronamig 321M - Alloy Wire fo 0117 Cronamig 3880M (CW 1938) 0128 Cronasil 43F (CW 1024) 0129 Cronatig 333T - Iron Base Alloy 0130 Cronatig Eagle 665T (CW 1840 0136 Cronatig Eagle 665T (CW 1841 0118 Cronaweld 311 (CW 1852) 0132 Cronaweld 321 - Welding Electr 0133 Cronaweld 344 (CW 1068) 0119 Cronaweld 344 T (CW 1886) 0134 Cronaweld 344T (CW 1887) 0120 Cronaweld 510 (CW 1039) 0135 Cronaweld 510 (CW 1826) C & T Refinery, Inc. Idexx Laboratories Idexx Laboratories Butcher Company Johnson, S. C. & Son, Inc. National Welders Premier Industrial Corporation CRC Chemicals Betz Betz Maintenance Supply Company, Cool -Amp Coducto-Lube Co. National Engineering Products, Reynolds Metals Company Chem One Corporation GC Electronics GC Electronics Betz Childers Products Company CRC Chemicals Aldrich Chemical Company Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronation Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronation Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronation Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In Cronatron Welding Systems, In 6/4/92 11/10/93 11/12/93 5/1/93 1/13/93 1/1/91 2/14/94 3/9/93 2/20/92 2/20/92 3/12/87 4/28/93 4/26/93 9/24/93 5/25/94 5/7/91 5/7/91 2/1/95 1/1/93 8/12/92 8/18/93 9/1/93 9/1/93 6/26/91 9/1/93 9/1/93 9/1/93 9/1/93 4/4/86 9/1/93 9/1/93 6/18/91 6/18/91 9/1/93 9/1/93 9/1/93 4/4/86 4/4/86 9/1/93 9/1/93 6 !dent Product Company Date 0131 Cronaweld Eagle 3880 0223 Cupric Sulfate-Sulfamic Acid S 1167 Current Tubes (CH25301) 0324 CX-1019 30% 0325 CX-1026 30% 0280 Cyclohexane 1055 DAB 'B Glo Bingo Markers and 1054 DAB 'B Glo Bingo Markers and 1052 DAB 'B Glo Bingo Markers and 1053 DAB 'B Glo Bingo Markers and 1087 Dacospin 092 0141 Datakoat Protective Coating Kit 1042 Daylight Fluorescent Pigment F 0303 Deco -Rex Epoxy Resin Glaze 3 0861 Deco-Rez Ceramic Granules 0304 Deco-Rez Epoxy Resin Glaze 3 0305 Deco-Rez Epoxy -Cote 3544 Pa 0306 Deco-Rez Epoxy -Cote Hardene 0307 Deco-Rez High Performance E 0308 Deco-Rez High Performance E 1064 Defoamer - Anti -Foam 0674 DeGrease It "Orange" & Vandal 1023 Degreaser, MNB-100 1068 Degreaser, Non -Butyl - Rocket 1056 Dermapro Enriched Lotion Soa 0146 Devcon Flexane 80 Putty Curin 0150 Devcon Flexane 80 Putty Resin 1030 Developer - 7041 0726 Diamond or Cubic Boron Nitrid 0225 Dichloromethane 0079 Diesel No. 2 0263 Diethylene Glycol 0181 Diethylene Glycol Monomethyl 0008 Diisopropylamine 0337 Diisopropylamine 0651 Diisopropylamine 0821 Dimension Turf Herbicide 1101 Discosoft 567 1013 Dissolved Oxygen Reagent, Hi 0159 Dow Corning 111 Valve Lub an Cronatron Welding Systems, In Fisher Scientific National Draeger Henkel Corporation Henkel Corporation Fisher Scientific Clarence J. Venne Incorporated Clarence J. Venne Incorporated Clarence J. Venne Incorporated Clarence J. Venne Incorporated Henkel Corporation Datak Corporation United Mineral & Chemical Cor General Polymers Corporation General Polymers Corporation General Polymers Corporation General Polymers Corporation General Polymers Corporation General Polymers Corporation General Polymers Corporation Defender Services Applied Research, Inc. MISCO Products - Mop N' Buck Defender Services Go -Jo Industries Devcon Corporation Devcon Corporation Xerox Corporation Norton Company Fisher Scientific Exxon Company Fisher Scientific Fisher Scientific Air Products and Chemicals, In ICI Americas, Inc. Union Carbide Monsanto Callaway Chemical Company Hach Company Dow Corning Corporation 3/16/93 1/25/92 9/1/92 9/29/88 12/7/88 11/2/93 1/1/91 1/1/91 1/1/91 1/1/91 8/9/89 9/23/88 10/25/93 5/20/93 1/15/92 5/20/93 6/9/93 6/9/93 1/20/93 1/20/93 1/1/92 2/10/92 1/1/94 1/1/92 1/5/87 5/11/92 6/15/92 6/8/92 11/2/93 10/19/88 9/11/92 11/2/93 12/11/86 5/1/93 7/25/89 4/1/85 1/1/91 10/20/87 9/12/93 10/18/88 7 Ident Product Company Date 0160 0161 0162 0163 0890 0917 0164 0165 0166 0167 0891 0168 1049 1050 0158 0714 0467 0319 0045 0617 0320 0858 0293 0965 0175 0177 0920 1119 0534 0543 0406 1166 0690 0184 0792 1014 0170 0932 0688 0033 Dow Corning 111 Valve Lub. an Dow Corning 200 Fluid 50 CS Dow Corning 41 EXT High Tem Dow Corning 44 High Temp Be Dow Corning 561 Silicone Tran Dow Corning 561 Silicone Tran Dow Corning 732 Multi -Purpose Dow Corning 736 Heat Resista Dow Corning G-N Metal Assem Dow Corning Medical Antifoam Dow Corning Z 6040(R) Silane Dow Corning Z-6040 Silane Dowicil Antimicrobial Agent - Bi Dowicil Preservative 75 - Bingo Dowtherm (R) A Heat Transfer Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Dow Corning Corporation Van Waters and Rogers Incorp Van Waters and Rogers Incorp Dow Chemical Company DP51 Dye Penetrant Sherwin Incorporated DRD Compound for Free&Total Hach DPD Free Chlorine Reagent Drain Opener Drewpol 10-4-0 Drierite Dry Ink 1065/5046/5065 Dry-Kleen Duo Seal Oil No. 1407K Dural 337, 200% Fast & Slow S Dykem Hi -Spot Blue No. 107 E-Series Ultrajet ES670,ES120 Easy -Off Oven Cleaner Eclipse Neutral CleanerNery N Elastomeric 10 - Fine Electro-Solv Emerest 2324 (15965) Emerest 2324-U Stearic Acid, I Emerest 2421 Glycerol Monool Emerest 2421/15948 - Glycerol Endust Endust Dusting and Cleaning S EPAL 12 Alcohol Epal 1214 Alcohol EPDXO 1000B Non -Skid Floor Hach Company Anderson, James H. Co. Stepan Company Hammond, W. A., Company Xerox Corporation GC Electronics Sargent -Welch Scientific Comp Dural Internation Corporation Dykem Corporation Chemtronics American Home Products Pioneer/Eclipse Corp. Proko Industries, Inc. Marchem Company Henkel Henkel Corporation Henkel Corporation Henkel Corporation Kiwi Brands Drackett Products Company Albemarle Corporation Ethyl Corporation - Chemical G American Abrasive Metals Com 11/11/92 11/7/89 11/11/92 11/11/92 8/31/92 7/7/92 10/18/88 5/8/93 11/11/92 6/5/93 11/11/92 6/5/93 1/4/91 4/17/91 5/10/94 3/9/92 1/1/95 7/15/93 9/2/92 4/21/92 9/22/86 5/9/91 8/29/91 5/30/86 11/6/89 1/1/91 6/23/87 3/4/93 9/29/87 4/29/86 6/30/94 6/30/94 7/5/94 5/26/93 5/26/93 10/1/88 4/22/93 10/19/92 1/1/87 8 (dent Product Company Date 0147 Epoxy Kit # 1 (EK-1) - Hardene 0148 Epoxy Kit #1 (EK-1) - Resin 0692 Epoxy Resin (5-Minute) and Ep 0947 Epoxy -Cote Hardener 0946 Epoxy -Cote Resin 0969 Epoxylite #C301 0057 EPY 500 (Part A) and (Part B) 0796 Erythrosin B, Spirit Soluble, 95 0080 Esso Low Sulfur No. 2 Diesel 0186 Ethal LA-4 0881 Ethfac 103 0882 Ethox 1122 0462 Ethox CO-25 0187 Ethox TO-16 0227 Ethyl Alcohol, Denatured 0743 Ethylene Glycol - Fiber Grade 1135 Ethylene Glycol 75018 1161 Ethylene Glycol Monoacetate, t 0842 Ethylene Glycol, Antifreeze Gra 0652 Ethylene Glycol, Polyester Gra 0641 Ethylene Glycol -Polyester Grad 0857 Ethylene Oxide 0189 Eutecto-Mask Compound 0190 Eutector 190 Flux 0771 Experimental Lubricant CX-969 0975 Exxal 16 1021 Eyesaline Concentrate - Part 5 0519 EZ Weld Clear PVC Solvent C 0520 EZ Weld Gray PVC Solvent Ce 0007 Fastbond Brand 900 Duct Seal 0664 FB-2651 0003 Feathering Disc Adhesive. 3M, 0194 FeI-Pro C-300 (Aerosol) 0195 FeI-Pro C-300 (Lead Free) 0196 FeI-Pro C-670 0197 FeI-Pro C5-A High Temperatur 0198 Fel-Pro C5-A High Temperatur 0348 Ferric Chloride Solution - Wast 0720 Ferrous Iron Reagent 0977 Ferti-Tome Weed -Out Lawn We Devcon Corporation Devcon Corporation ITW Devcon Corporation General Polymers Corporation General Polymers Corporation The Epoxylite Corporation BLH Electronics Aldrich Chemical Company Exxon Company Ethox Chemicals, Inc. Ethox Chemicals, Inc. Ethox Chemicals, Inc. Ethox Chemicals Ethox Chemicals, Inc. Fisher Scientific Shell Oil Company Huntsman Aldrich Chemical Company Union Carbide Union Carbide Huntsman Balchem Corp. Eutectic Corporation Eutectic Corporation Henkel Corporation Exxon Chemical FendAll Company P. C. I. Industries Inc. P. C. I. Industries, Inc. Company 3M Zchrimmer & Swartz Company 3M FeI-Pro Incorporated FeI-Pro Incorporated FeI-Pro Incorporated FeI-Pro Incorporated FeI-Pro Incorporated K. A. Steel Chemicals Hach Company Voluntary Purchasing Groups I 1/1/85 5/11/92 5/2/92 6/16/92 6/16/92 1/1/91 6/16/93 8/18/93 7/27/93 1/21/94 10/1/90 10/1/90 10/1/90 10/1/90 11/2/93 11/13/85 7/15/94 1/3/95 5/20/93 3/16/92 7/1/94 12/15/92 3/13/93 3/15/93 7/21/93 12/15/92 10/1/93 1 /1 /93 10/15/87 10/17/88 10/6/92 12/8/92 11/8/90 8/19/93 6/12/92 4/5/93 4/23/88 1/5/93 7/1/90 9 (dent Product Company Date 1140 1160 0862 0517 0851 0015 0016 0017 0018 0019 0822 0750 0027 0021 0022 0753 0023 0752 0024 0025 0704 0029 0026 1134 1093 0535 0144 0145 0151 0404 1115 1063 1069 1061 1071 1058 0415 1044 1082 0537 Fiber Glass Divison Articles Fiber Glass Insulation Fiberglass Insulation Fiberglass Insulation Finish Oil N-121-2 Finish Finish Finish Finish Finish Finish Finish Finish Finish Finish Finish Oil N-23-89 and N-23-30 Oil N-25-5 and N-31-10 Oil N-32-32 and N-57-33 Oil N-43-30 & N-43-100 Oil N-44-100 Oil N-44A-100 Oil N-74-22 Oil N-77-15 Oil NXT-994-15 Oil PXY-1-1805-30 Oil PXY-1720-100 Finish Oil PXY-1721-100 Finish Oil PXY-1737-100 Finish Oil PXY-1773-35 Finish Oil PXY-1825-100 Finish Oil PXY-1942-25 Finish Oil PXY-207R-26 or N-1 Finish Oil PYX-1814-20 Fire Barrier 2001 Silicone RTV Fire Stop Foam Paris A,B First Step Sealer /T/W Bottom Flexane 94 Liquid - Hardener Flexane 94 Liquid - Resin Flexane Putty Hardener Flexboard II - Autoclaved Flint Gray Spray Paint Floor Finish - Durashine Floor Finish - Ultra Shine Floor Finish Restorer - Innovat Floor Sealer - Spectrum Floor Wax Stripper - Chisel Fluid #295 Foam Burst 320CT - Bingo Mar Foam-Trol CT FoamGlas Insulation Schuller Schuller International Owens/Corning Fiberglas Corp Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal Allied Signal 3M Company Dow Corning Corporation Pioneer/Eclipse Corp. Devcon Corporation Devcon Corporation Devcon Corporation Schuller International - Manville Sherwin-Williams Defender Services Defender Services Defender Services Defender Services Defender Services Meriam Instrument Ross Chem Incorporated Betz Laboratories Pittsburgh Corning 5/15/92 8/1/94 6/1/91 6/1/91 11/18/91 4/21/86 4/21/86 4/21/86 4/21/86 5/21/86 5/20/92 4/8/88 1/1/88 1/25/89 7/17/87 6/10/88 8/6/87 3/8/88 10/28/88 9/6/89 1/1/88 12/29/93 9/18/89 3/3/93 6/8/92 6/5/92 1/1/85 1/2/90 8/10/87 1/1/92 1/1/92 1/1/92 1/1/92 4/1/93 10/18/93 10/18/93 3/23/92 3/15/93 10 (dent Product Company Date 0833 Fomofill, Handi-Foam 0048 Foray Dry Chemical Extinguishi 0996 Form -A -Thread Release Agent 0370 Form -a -Thread Strip Thread Re 0938 Formazin Turbidity Standard 40 0344 Forward DC 1171 Foster 81-27/81-27Q Adhesive 0313 Foxboro 1500 Ink 0314 Foxboro 1600 Ink 0315 Foxboro 1800 Ink 1043 Fragrance #15535 - Bingo Mark 0469 Free Chlorine Buffer for CL-17 0468 Free Chlorine Indicator Solution 0868 Froth Pak #12 Kit Components 1154 FSK Pressure Sensitive Perm 0808 Fuel Oil #2 0032 Fuel Oil,#6 Residual H/S 1027 Fuel-Solv FS-850 0335 G-3780A 0740 Galvanized Steel - Sheet, Build 0830 Galvicon Compound 0297 Garlock 101-S Soft Set Gasketi 0837 Gasoline - Citgo Premium Unle 0838 Gasoline - Citgo Unleaded 0442 Gear Oil GX 80W-90 0030 Genesolv D Solvent 1075 Genetron (HFC) - 134a 0013 Genetron 12 dichlorodiflourome 0031 Genetron 22 chlorodifluorometh 0309 Giv-Gard DXN 0978 Glufpride Super Premium 10W- 0281 Glycerin 0705 Glycerin 0478 Glycolaldehyde Dimer, Crystalli 0310 Glyptal 1201A 0777 Go -Jo Liquid Protective Skin C 0311 Go -Jo Original Hand Cleaner 0618 Graphite Rust Preventative C-7 0402 Great Grape Concentrate 0409 Green Concentrate #1000 Fomo Products, Inc. Ansul Fire Protection Loctite Corporation Loctite Corporation Hach Company Johnson, S. C. & Son, Inc. Foster Products Graphic Controls Graphic Controls Graphic Controls Atlanta Fragrance Incorporated Hach Hach Insta-Foam Products, Inc. Compac Corporation Amerada Hess Corporation Amerada Hess Corporation Betz Laboratories ICI Americas Inc. Reynolds Metals Company Southern Coatings Garlock, Inc. Citgo Petroleum Company Citgo Petroleum Company Exxon Company Allied Signal Allied-Signal Allied Signal Allied Signal Givaudan Corporation Gulf Oil Corporation Fisher Scientific Fisher Scientific Aldrich Chemical Company Glyptal, Inc. Go -Jo Industries Go -Jo Industries Stoner Incorporated Maintenance Supply Company, Meriam Instrument 5/1/94 10/29/92 8/19/93 8/19/93 2/3/93 4/10/91 3/17/94 1/1/93 2/11/94 4/22/93 1/21/94 9/12/93 1/1/95 11/20/92 8/12/85 1/1/93 1 /1 /94 7/5/94 1 /31 /94 9/24/93 3/3/92 6/21/94 3/24/93 3/24/93 9/15/93 1/1/87 12/17/91 1/1/85 1/1/87 7/28/95 2/1/82 5/17/94 3/14/89 6/12/95 8/17/93 8/30/90 9/23/91 11 /1 /88 8/26/93 10/15/93 11 (dent Product Company Date 0658 0112 0099 0100 0703 0101 0102 0103 0104 0105 0106 0107 0075 0284 0670 0049 0050 0473 0754 0643 0644 0645 0646 0647 1172 1065 0070 0063 0498 0856 0229 0328 0329 0201 0562 1076 0398 1010 1110 0540 Green P/N 03/00-00-067429 VDO Instruments Grinding Compound, Clover Gr Clover Manufacturing Compan Gulf E. P. Lubricant HD150 Chevron Gulf E. P. Lubricant HD460 Chevron Gulf E.P. Lubricant HD 220 Chevron Gulf Harmony 115 Chevron Gulf Harmony 46 AW Chevron Gulf Harmony 68 AW Chevron Gulf Transgear Lubricant E.P. 2 Chevron Gulfcrown Grease E. P. No. 2 Chevron Gulflube Single 20W/20 Chevron Gulfway 68 Chevron H-300 Microbiocide H.I. Mastic, Trowel H.S.Poly.Anhyd. - Shale Gray L Halon 1211, BCF Halon 1301, Freon FE 1301 Hardness Titrating Solution Hazorb-Pillow Heat T5ransfer Cement Grade Heat Transfer Cement Grade T Heat Transfer Cement, Grade Heat Transfer Cement, Grade Heat Transfer Cement, Grade Heat -Shrinkable Polymeric Pro Heavy Duty Cleaner / Degreas Heavy Duty Degreaser (Aerosol Heavy Duty Silicone Helium Heptane Heptane Heresite VR-502 Finish Heresite VR-502 Primer Hexafluoro-2-Propanol (1,1,1,3, Hg Absorb Hi-Bild Aliphatic Polyurethane Hi -Speed Coating Hi -Spot Blue Base #107 High Gloss Polyurethane Varni High Heat Coating Calgon Corporation Fuller, H. B., Company DuPont Ansul Fire Protection Ansul Fire Protection Betz Laboratories Occidental Chemical Thermon Manufacturing Comp Thermon Manufacturing Comp Thermon Manufacturing Comp Thermon Manufacturing Comp Thermon Manufacturing Comp Raychem Defender Services CRC Chemicals Bowman Distribution National Welders Centimark Corp. Fisher Scientific Heresite Protective Coatings, I Heresite Protective Coatings, I Fisher Scientific Science Related Materials Sherwin-Williams Company Maintenance Supply Company, ITW Fluid Products Group DeSoto Courtaulds Coatings 4/25/88 4/25/88 4/25/88 4/22/88 4/22/88 4/22/88 11/24/87 4/25/88 11/24/87 4/25/88 7/17/92 8/19/93 11/19/90 10/7/92 5/7/93 8/19/91 9/22/89 5/30/86 5/29/86 5/29/86 7/16/90 5/29/86 10/1/94 1/1/94 3/4/93 7/30/90 11/25/85 4/5/91 11/2/93 11/2/93 11/2/93 9/30/86 11/20/85 7/31/86 3/3/93 3/31/93 1/29/87 1/7/94 12 (dent Product Company Date 1103 High Heat Coating 0813 High Noon Urethane Floor Finis 1067 High Performance Detergent - 0671 High Solids Activator - Sales C 0622 HMDS,100ML 0345 Horizon 400 General Purpose 0515 HTH Dry Chlorinator Tablets 0700 Humidity Salts 0489 Hydranal Composite 5-34805-1 0059 Hydraulic Handgun Fluid 0365 Hydraulic Sealant 50 ML Item 5 0371 Hydraulic Sealant Part 69 0386 Hydraulic Sealant, 250 ML Bottl 0276 Hydrobromic Acid 48% 0231 Hydrobromic Acid In Acetic Aci 0266 Hydrochloric Acid 36-37% 0499 Hydrogen 0832 Hydrogen Peroxide 3% 0233 Hydrogen Peroxide 30% 0747 Hydrosep 0334 Hysol-1-C Epoxy Patch Kit 0662 Ice -Foe 0883 Igepal CO-630 0939 Igepal CO-630 0399 In Focus 0568 Industrial Enamel B54 T 104 UI 0569 Industrial Enamel B54 W 101 P 0574 Industrial Enamel B54 W 103 D 0570 Industrial Enamel B54 Y 27 Saf 0571 Industrial Enamel Non -Lead Co 0572 Industrial Enamel Non -Lead Co 0573 Industrial Enamel Non_lead Col 0699 Industrial Heat Resistant Coatin 1184 Inergen 0668 Inhibisol 0341 Inland-19 1133 Inorganic Salts 1144 Insul-Sheet, Insul-Tube 0696 Inswool Moldable 0783 Intex 8655 Porter Paint Coating Butcher Company Defender Services DuPont Supelco Inc. Johnson, S. C. & Son, Inc. Olin Corporation Mallinckrodt Hoechst Celanese BTR Valve Sealants, Inc. Loctite Corporation Loctite Corporation Loctite Corporation Fisher Scientific Fisher Scientific Fisher Scientific National Welders Fisher Scientific Fisher Scientific Engon Safety Products Hysol - Petree & Stoudt Associ Johnson, S.C. & Son GAF Chemicals Corporation Rhone-Poulenc Maintenance Supply Company, Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Flame Control Coatings, Inc. Ansul Fire Protection Penetone Corporation Inland Vacuum Industries Mallinckrodt Halstead Industries Green, A.P. Industries, Inc. EZE Products Incorporated 3/22/85 5/1/93 5/1/92 11/19/90 7/6/94 6/14/94 1/5/89 3/7/80 7/1/92 12/1/92 7/1/94 7/1/94 11/2/93 11/2/93 11/2/93 11/25/85 3/10/92 11/2/93 8/22/88 11/10/93 1/10/94 1/1/83 2/1/92 6/28/90 10/9/86 10/9/86 10/9/86 10/9/86 10/9/86 10/9/86 10/9/86 4/30/90 10/23/92 2/7/90 8/12/93 12/1/86 8/21/91 1/28/93 11/8/85 13 (dent Product Company Date 0784 Intex 8676 0976 Intracid Scarlet Moo Conc 0273 Iodine Solutions 1N and Conce 1001 lrgafos 168 1004 Irganox 1010 1005 Irganox 1076 1003 Irganox MD 1024 0235 Iron Reference Standard Soluti 0757 Iron Stone Acrylic Seal 1132 Isobutane 0354 Isoflex NBU 15 1112 Isoflex Super LDS 18 0350 Isoflex Tel 3000 Altemp 0351 Isoflex Topas L 32 1048 Isopropyl Alcohol - Bingo Mark 0812 Isopropyl Alcohol and Water 0746 Isopropyl Alcohol and Water 0886 J-Shop 600 0956 J-Shop 600 0884 Jackhammer Baseboard and B 0509 K-156 0895 K260 Spinneret Lubricant 0268 Karl Fisher Reagent 0877 Kast-O-Lite 25 (and 25 Plus) 0518 Kaylo 10 AF Insulation 0575 KEM A&A Epoxy Enamel B61 0576 KEM A&A Epoxy Enamel B61 0577 KEM A&A Epoxy Enamel B61 0578 KEM A&A Epoxy Enamel B61 0579 KEM A&A Epoxy Enamel B61 0580 KEM A&A Epoxy Enamel B61 0584 Kem A&A Epoxy Enamel Non- 0585 Kem A&A Epoxy Enamel Non- 0581 KEM A&A Epoxy Primer B61 N 0582 KEM Lustral Enamel F65 B 50 0583 KEM Lustral Enamel F65 G 16 0586 Kem Lustral Enamel Non -Lead 0831 Kemp K-3 Silica Gel 0817 Kemp K-4 Type Molecular Siev 1183 KI-2 EZE Products Incorporated Crompton & Knowles Corporati Fisher Scientific Ciba-Geigy Corporation Ciba-Geigy Corporation Ciba-Geigy Corporation Ciba-Geigy Corporation Fisher Scientific Butcher Company National Specialty Gases Kluber Lubrication Corporation Kluber Lubrication Corporation Kluber Lubrication Corporation Kluber Lubrication Corporation Van Waters and Rogers Incorp Nice -Pak Products, Inc. Nice -Pak Products, Inc. Johnson, S. C. & Son, Inc. SC Johnson & Son, Inc. Butcher Company Nonfluid Oil Corp. Stoner Incorporated Fisher Scientific A. P. Green Industries, Inc. Owens/Corning Fiberglas Corp Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company C.M. Kemp Manufacturing Com C. M. Kemp Manufacturing Co Betz 4/8/92 5/4/94 11/2/93 5/24/91 8/3/92 8/3/92 6/14/91 11/2/93 5/1/93 10/1/92 4/10/86 5/27/87 4/10/86 4/10/86 2/22/90 8/23/89 8/23/89 4/13/93 11/10/87 5/1/93 7/11/94 10/6/92 11/2/93 6/21/93 10/1/93 10/6/86 10/6/86 10/3/86 10/3/86 10/3/86 10/2/86 10/3/86 10/3/86 10/20/86 12/5/86 12/5/86 12/5/86 7/1/93 2/1/94 9/30/91 14 (dent Product Company Date 0073 Kilz Caldwell Paint Mfg. Co., Inc. 3/26/85 0155 Kleen-Kool DoAll Company 1/31/94 0555 Klingerit (Red) Richard Klinger Inc. 11/20/85 0556 Klingerit Universal Blue Richard Klinger Inc. 11/20/85 0764 Kolene 6-2-3 Reducing Agent Kolene Corporation 1/18/94 0355 Kolene KGC Kolene Corporation 10/1/93 0356 Kolene No. 6 Kolene Corporation 10/1/93 0587 Kromik Metal Primer E41 N 1 Sherwin-Williams Company 10/1/86 0171 Krytox 240 Series & GPL Fluori Du Pont 10/3/94 0765 Krytox GPL 22X Fluorinated Gr DuPont 10/3/93 0676 KSL-111 Aerosol (Synthetic Aer Elf Lubricants North America 4/4/94 0441 Kutwell 40 Exxon Company 2/22/95 0237 L-Ascorbic Acid Fisher Scientific 5/17/94 0970 LA -CO Regular Flux Paste Lake Chemical Company 0287 Lagfas Adhesive Fuller, H. B., Company 8/19/93 0357 Leak Tracy LS-77 Leak Chemicals (Heman & Ass 9/8/86 0039 Leek-Tec 415 American Gas and Chemical C 8/1/93 0071 Lectra Clean (Aerosol) #2018, CRC Chemicals 2/22/93 0072 Lectra Clean (Bulk) #02020, 02 CRC Chemicals 3/5/93 0760 Legend Ultra High Speed Floor Butcher Company 5/1/93 1092 Leomin FA-NF Hoechst Celanese 8/30/93 0879 Lexolube 4N-415 Inolex Chemical Co. 4/18/91 0457 Lidok EP 0 Exxon Company 2/22/95 0859 Lift -Off Correction Tape Xerox Corporation 4/24/90 0922 Lins 50 Castabie Premier Refractories and Chem 8/1/92 0846 Liqui-Nox Alconox, Inc. 7/21/87 0546 Liquid Fire Quick Starting Fluid Radiator Specialty Company 7/1/92 0152 Liquid Hardener 0202 Devcon Corporation 6/15/92 0153 Liquid Hardener 0203 Devcon Corporation 6/29/92 0500 Liquid Nitrogen National Welders 11/25/85 0547 Liquid Wrench Super Lubricant Radiator Specialty Company 4/1/93 0548 Liquid Wrench Super Lubricant Radiator Specialty Company 6/1/92 1083 LITE-DRI Absorbent #PLP201 New Pig Corporation 8/6/92 0966 Lithium Chloride EM Science 2/25/88 0274 Lithium Chloride Fisher Scientific 11/2/93 0936 Lithium Chloride in Methanol Analyticon Instruments Incorpor 3/18/93 1034 Lock 'n' Pop A Key Tech Corporation 7/1/92 0666 Locks Nut Removable Threadlo Permatex Industrial Corporatio 8/9/88 0718 Locquic Primer N Loctite Corporation 5/1/91 0372 Locquic Primer N (Aerosol) Par Loctite Corporation 7/1/94 15 (dent Product Company Date 0373 Locquic Primer T (Aerosol) Part 0361 Loctite 10ML EV Item 7921 0362 Loctite 4 Oz 404 Item 46548 0955 LP Gas Propane with Odorant 0332 LPS 3 Heavy Duty Rust Inhibito 1073 LPS Precision Clean 1074 LPS PreSolve (Aerosol) 0819 LS 10 Liquid Shield 1012 LS 10 Liquid Shield 0091 Lubriclens 0282 Lubriplate "130" Series 0710 M & T Catalyst S-21 0182 M-Cresol 0967 Magnesium Nitrate 0400 Maintenance No -Scrub Emulsifi 0239 Manganese Sulfate Solution 0405 Marinite 1 0866 Marker Board Cleaner #202 0865 Marker Board Cleaner #404 0333 Marlotherm S 0997 Master Gasket Flange Sealant 0374 Master Gasket Sealant Part 00 1035 Masterflow 928 Grout 0816 Masterkote/Mobilekote Aluminu 0715 Mega Steel Stick 0270 Mercuric Oxide Solid 0241 Mercury 0417 Mercury 0588 Metalastic II Enamel B53 W 10 0589 Metalatex Semi -Gloss Enamel 0590 Metalatex Semi -Gloss Enamel 0591 Metalatex Semi -Gloss Enamel 0592 Metalatex Semi -Gloss Enamel 0593 Metalatex Semi -Gloss Enamel 0594 Metalatex Semi -Gloss Enamel 0595 Metalatex Semi -Gloss Enamel 0596 Metalatex Semi -Gloss Enamel 0597 Metalatex Semi -Gloss Enamel 0418 Metco 102 0419 Metco 130,130SF Loctite Corporation 8/19/93 Loctite Corporation 10/2/89 Loctite Corporation 11/7/89 Blossman Gas LPS Laboratories Incorporated 1/31/94 LPS Laboratories LPS Laboratories Dabco Products Inc. 1/1/88 Delta Industrial Products 5/17/93 Carter, A. B., Inc. 9/2/93 Fiske Brothers Refining Co. 1/1/94 M & T Chemicals 3/15/88 Fisher Scientific 11/9/86 EM Science 10/27/87 Maintenance Supply Company, 6/18/92 Fisher Scientific 11/2/93 Schuller International - Manville 1/2/90 Chemical Packaging Corp. 2/1/93 Chemical Packaging Corp. 2/1/93 Huls America Inc. 2/28/92 Loctite Corporation 8/19/93 Loctite Corporation 8/19/93 Master Builders Incorporated 10/16/91 Master Products Company X-Ergon, A Portsmaster Co., Di 1/16/92 Fisher Scientific 11/2/93 Fisher Scientific 5/17/94 Meriam Instrument 10/13/93 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Sherwin-Williams Company 10/10/86 Metco 11/25/85 Metco 7/16/92 16 (dent Product Company Date 0420 Metco 14E, 15E Metco 2/18/93 0421 Metco 185 Microcrystalline Wa Metco 8/13/93 0422 Metco 442 Metco 11/22/93 0423 Metco 444 Metco 5/3/93 0424 Metco 447, 447NS Metco 2/4/93 0425 Metco 448 Metco 8/25/93 0426 Metco 449, 449P Metco 4/26/93 0427 Metco 450, 450NS Metco 11/25/85 0428 Metco 451 Metco 8/10/93 0429 Metco 505, 501 Metco 11/17/93 0430 Metco 51, 51NS, 51F-NS Metco 1/12/94 0431 Metco 52C Metco 5/26/93 0432 Metco Anti -Bond Metco 2/16/94 0433 Metco Cleaning Solvent Metco 4/19/93 0924 Methane National Welders 12/10/86 0275 Methanol Fisher Scientific 5/17/94 1045 Methocel E and F Series - Bing Van Waters and Rogers Incorp 1/4/91 0179 Methoxyethoxy) Ethanol * 2-(2- Fisher Scientific 7/11/80 0243 Methyl Isobutyl Ketone Fisher Scientific 11/2/93 0272 Methyl Orange Fisher Scientific 11/2/93 0481 Methyl Purple Indicator Betz Laboratories 12/7/92 0245 Methyl Red Fisher Scientific 11/2/93 0795 Methyl Yellow, Indicator Grade Aldrich Chemical Company 8/18/93 0897 Methyldioxalane Fluka Chemical Corporation 3/9/93 0264 Methylene Blue Fisher Scientific 11/2/93 0995 Methylene Chloride Fisher Scientific 5/17/94 0199 Methylparabin ABA + FendAll Company 12/15/92 1107 Micro Hardness Titrant 834 Betz 7/30/91 1148 Mist Eliminator Sump Solution AlliedSignal 9/1/94 0044 Misty Glycol Air Sanitizers Amrep, Inc. 3/22/93 0905 Mobil Hydraulic Oil NZ 46 Mobil Oil Corporation 1/29/92 0781 Mobil SH6 632 Mobil Oil Corp 3/19/88 0434 Mobil Velocite Oil No. 10 Mobil Oil Corp 3/19/88 0702 Mobilgear 630 Mobil Oil Corp 8/25/89 0623 MOL-SIEVE (Act) 8/12 Mesh 1 Supelco Inc. 7/6/94 0863 Molybdate Reagent for Phosph Betz Laboratories 6/16/93 0941 Molybdenum Reagent Molyvar Hach Company 9/29/92 0942 Molybdenum Reagent Molyvar Hach Company 1/9/92 0943 Molybdenum Reagent Molyvar Hach Company 1/25/93 0944 Molybdenum Standard Solution Hach Company 7/30/92 17 (dent Product Company Date 0169 Molykote C-40 Hi Temp Chain 0782 Monawet MO-705 1153 Monocomponent Toner 30 0673 Monoglass Spary-On Insulation 0388 Monolec Rock Drill Lubricant 6 0435 MR-778 1179 MS-122 TFE Release Agent 0247 N,N-Dimethylformamide 0326 N-97-10 (Same as CX-810) 0867 N-Methylpyrrolidone 0952 Natural Gas 0982 Natural Gas 0874 Natural Red Rubber 0289 Nekal WS 25 I 0727 Nekal WS-25I 0508 Neutra Rust 661 1066 Neutral Cleaner - Opti-Clean 0756 Neutral Cleaner 118WP 1070 Neutral pH Disinfectant - Q21 0265 Neutral Red 0780 Never Seez Regular Grade 0787 Nickel Anti -Seize - 77124, 7716 0928 Nickel Based Alloy Steel 200,4 0742 Nickel Steel - Sheet, Plate, Rod 0191 Nitec 10224 0249 Nitric Acid 0501 Nitrogen 0502 Nitrous Oxide 0910 No-Tri-Aerosol 0911 No-Tri-Liquid 0338 Noalox Anti -Oxidant 0174 Nokorode Soldering Paste 0449 Nuto H 32 0443 Nuto H 46 0446 Nuto H 68 0267 0-Cresol 0301 0-cresol 0810 O-Cresol/Chloroform 0751 O-O'Butylene bis (Caprolactim) 0512 Oakite 202 Dow Corning Corporation Mona Industries Inc. Kodak Monoglass Inc. Lubrication Engineers, Inc. Modern Research Corporation Miller -Stephenson Chemical Fisher Scientific Henkel Corporation BASF Corporation Exxon Company Exxon Company Fisher Scientific GAF Chemicals Corporation Rhone-Poulenc New York Bronze Co. Defender Services National Milling & Chemical Co Defender Services Fisher Scientific Bostick Loctite Corporation Marmon/Keystone Corporation Reynolds Metals Company Eutectic Corporation Fisher Scientific National Welders National Welders Enviro-Solv Enviro-Solv Ideal Industries, Inc. Dunton, M. W. Supply Exxon Company Exxon Company Exxon Company Fisher Scientific General Electric Company Harrell Industries, Inc. Allied Signal Oakite Products, Incorporated 8/20/93 3/1/89 3/10/94 4/1/93 4/12/94 9/1/92 11/2/93 10/17/84 3/31/93 8/15/92 8/15/92 6/9/90 7/7/86 12/1/93 4/10/86 1 /1 /92 1 /1 /94 11/2/93 9/8/93 7/1/94 1 /1 /93 9/24/93 3/15/93 11/2/93 11/25/85 11/25/85 1/25/93 7/27/90 9/9/92 11/21/91 9/26/94 9/26/94 9/26/94 11/2/93 1/1/89 5/1/93 4/7/87 3/17/93 18 (dent Product Company Date 0513 0514 1032 0691 0598 0974 0655 0983 1117 1118 0516 0806 0251 0503 1036 0925 0183 0523 0557 0558 0524 0097 0823 0526 0527 1102 0525 0452 0899 0482 0483 0484 0900 0902 0904 0376 0377 0378 0672 0898 Oakite 220 NP Oakite Penetrant Oil Saturated Wick Oil -Flo Safety Solvent & Degre Opex Lacquer Thinner R7 K 12 Opti-Meen 85538 Oakite Products, Incorporated Oakite Products, Incorporated Xerox Corporation Titan Laboratories Sherwin-Williams Company Betz Organofunctional Silane A-187 Union Carbide Ortho Cresol Low PB AquAir Corporation OSHA Green Spray Paint B54T Sherwin-Williams OSHA Red OTC Hydraulic Oil Overkrete Oxalic Acid Oxygen Oylite Stik P-10 Electron Capture P-Toluic Acid Patton's QSI Oil Pen -Green Pen -Red Peneteck Penetrant and Lubricant (Aeros Penetrating Oil Lubricant Penetrating Oil No. 1 Penetrating Oil No. 2 Penflex Penn Drake Petrosul 742 Pennex N 47 Perfectothane Concrete Perma Fil (Part A) Perma Fil (Part B) Perma Fil (Part C) Perma Patch (Part A) Perma Patch (Part B) Perma Patch (Part C) Mixture and Te Sherwin-Williams Owatoona Oil Company Concrete Protection Systems, I Fisher Scientific National Welders La -Co Industries National Welders Fisher Scientific Patton's Inc. Robert Shaw Controls Robert Shaw Controls Penreco Chesterton, A. W. Company Stoner Incorporated Penwalt Corporation Penwalt Corporation Penford Products Company Penreco Exxon Company Maintenance Supply Company Tri-Chem Corporation Tri-Chem Corporation Tri-Chem Corporation Consolidated Chemical Corpor Consolidated Chemical Corpor Consolidated Chemical Corpor Permatex Aviation Form -A -Gas Loctite Corporation Permatex Form -A -Gasket No. Loctite Corporation Permatex Form -A -Gasket No. Petcat ATA Petrosul L-60 SOD Sulfate Loctite Corporation Amspec Chemical Corp. Penreco 9/30/93 12/2/92 6/8/92 10/1/92 12/30/86 1/13/94 7/29/92 7/1/85 8/10/87 8/10/87 12/15/87 11/5/89 11/2/93 11/25/85 12/26/90 1/1/92 5/20/83 9/16/88 5/18/92 10/1/86 7/8/88 2/7/86 1 /1 /82 8/17/92 11/13/85 2/22/95 2/20/86 4/7/93 4/7/93 4/7/93 4/7/93 4/7/93 4/7/93 3/27/86 8/19/93 8/19/93 10/1/90 10/2/92 19 (dent Product Company Date 0528 PG 2089 Part A - Epoxy Resin 0529 PG 2089 Part B - Epoxy Harde 1109 PG T-250 Parts A&B 0701 PH Indicators 0844 Phenol 0321 Phenol 0269 Phenol Red Solution 0.02% 0811 Phenol/1,1,2,2 Tetrachloroetha 0253 Phenolphthalein 1022 Phenolphthalein Indicator 0271 Phosphoric Acid 0693 Phosphoric Acid 105-117% 1033 Photoreceptor - 7041 0082 PhreeGuard 1000N 0083 PHreeGuard 2350 0506 PIG Mats#MAT201, #MAT202, 0785 PIG Model O.R. 1011 Piston Lube 0820 Piston Seal Liquid 1174 PITTSEAL 444/444-N Sealant 0954 Plastite 7100 Anti -Corrosive Pri 0953 Plastite C-757 Epoxy Black 0209 Platinum Cobalt Color Standard 0051 Plus -Fifty C Dry Chemical 0379 Pneumatic/Hydraulic Seal 545 0538 Polar Chip 347L 0407 Polvyn Crack Filler 0436 Polychlorinated Biphenyls (PC 0012 Polyester Fiber & Resin 0440 Polyester Prepolymer 1147 Polymer 1160XL 1176 Polymer 1170 1181 Polymer 1190 1165 Polymer 1195 1151 Polymer CDP-92009 0834 Polyphosphoric Acid 0616 Polyphosphoric Acid 0455 Polyrex 0604 Polyurethane Clear Spray Varni 0605 Polyurethane Floor Enamel A3 Permagile Industries Inc. Permagile Industries Inc. Permagile Industries Aldrich Chemical Company Fisher Scientific Harrell Industries, Inc. Fisher Scientific Harrell Industries, Inc. Fisher Scientific Betz Laboratories Fisher Scientific FMC Corporation Xerox Corporation Calgon Corporation Calgon Corporation New PIG Corporation New Pig Corporation Delta Industrial Products Dabco Products Inc. Pittsburgh Corning Wisconsin Protective Coatings Wisconsin Protective Coatings Fisher Scientific Ansul Fire Protection Loctite Corporation Polar Chip Inc. Master Builders, Inc. Monsanto Allied Signal AlliedSignal Betz Betz Betz Betz Betz Rhone-Poulenc Stauffer Chemical Company Exxon Company Sherwin-Williams Company Sherwin-Williams Company 7/1/93 5/7/86 1/22/87 8/1/90 11/2/93 9/1/93 11/2/93 1/1/94 11/2/93 12/7/92 11/2/93 7/8/93 6/8/92 2/10/93 5/13/93 4/26/94 1/22/86 5/17/93 1 /1 /88 3/9/90 11/8/90 6/21/91 11/2/93 8/26/92 8/19/93 3/19/86 7/25/88 10/1/88 1 /1 /86 1 /1 /95 1/26/94 7/22/93 10/4/93 10/2/92 7/1/94 11/18/91 2/22/95 5/5/86 3/20/86 20 (dent Product Companv Date 0210 0212 0214 0216 0218 0220 0694 0222 1025 0224 0845 0719 0226 0046 0919 0156 1126 0461 1099 0380 0606 0607 0599 0600 0601 0602 0603 0841 0470 0775 0987 0062 0202 0052 1158 0014 0773 0984 0778 0763 Potassium Potassium Potassium Potassium Potassium Potassium Potassium Potassium Potassium Potassium Potassium Bisulfate Bromide Chloride Chloride Solutions Hydrogen Phthalate Hydroxide (Dry Soli Hydroxide Solution Iodide Iodide -Iodate Permanganate Permanganate Solut Potassium Permangnate Potassium Thiocyanate Pow R Tox Insect Killer Power Pak #8009,8010,8011 Power -Cut No. 360 Poxy-Pak Fast Cure Epoxy Premium Solvent Prime Neatsfoot Oil Compound Prism 410 Instant Adhesive Par Pro Mar 400 Latex Flat Paint B Pro Mar 400 Latex Flat Paint B PRO -MAR 400 Latex Flat Paint PRO -MAR 400 Latex Semi-Glo PRO -MAR Block Filler B25 W PRO -MAR Traffic Marking Pain PRO -MAR Traffic Marking Pain Process Cooling Water Process pH Electrolyte Product FB 2651 Produkt FB 2606 Propane Propanol * 2-Propanol Purple-K Dry Chemical Extingu PVC Fitting Covers PXY 1676-100 Finish - Spin Fin PXY-1773-35 Pet A-101 Spin Fi PXY-1840-20 PXY-1942-25 Pet Overfinish PXY-2099-100 Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Fisher Scientific Betz Laboratories Fisher Scientific Fisher Scientific Prillaman Chemical Corp. Fisher Scientific Anderson, James H. Co. Crown Industrial Products DoAll Company Permatex Industrial Safety-Kleen Fiebing Company Loctite Corporation Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Allied Signal Hach Zschimmer & Swarz Zschimmer & Schwarz Bernzomatic Fisher Scientific Ansul Fire Protection Proto Corporation Allied Signal Allied Signal Allied-Signal Allied Signal Allied Signal 5/17/94 11/2/93 11/2/93 5/17/94 8/17/93 11/2/93 11/2/93 11/2/93 2/16/91 5/17/94 11/2/93 5/1/92 5/17/94 4/13/92 3/26/93 1/31/93 10/1/85 2/11/93 1/1/82 8/19/93 3/24/86 3/24/86 3/24/86 3/25/86 4/9/86 2/23/87 2/23/87 12/6/89 10/24/94 9/2/88 3/25/86 9/10/93 11/2/93 1/6/92 3/24/88 1/1/87 7/11/88 4/3/89 9/6/89 8/24/90 21 (dent Product Company Date 1100 PXY-2099M-100 or N-125M-10 1085 PXY-2466-25 or N-133-25 1091 PXY-2696-100 1086 PXY-2709-100 1089 PXY-2710-24 1090 PXY-2711-24 0852 Pyridine 0228 Pyridine 0294 Q-Dope 0847 Quartz - Q11 and Q28 Colored 0999 Quick Set Industrial Adhesive 4 1029 Rapi-Cide 0552 Rapid Tap 0414 Red Dye #200 0413 Red Fluid #190 0410 Red Fluid Hi -Vac #104 0416 Red Oil #827 0659 Red P/N 03/00-00-067428 0408 Red Unity Oil #100 ' 0561 Refined Petroleum Oil 0544 Refractive Index Liquid Series 0545 Refractive Index Liquid Series 1168 Refractory Ceramic Fiber Prod 0110 Regular Clorox Bleach 0460 Regular Unleaded Gasoline 0366 Removable TL 50 ML 242 Item 0799 Repellan 77/80 0798 Repellon 80 (15927) 0624 Replacement Charcoal 400cc 0869 Residual Fuel Oil #4 0723 Resinoid Beonded Grinding Wh 0722 Resinoid Bonded Grinding Whe 0887 Rhenodiv LE 0805 Rik-Lub Gasket Lubricant 0698 Rik-Tef Thread Compound w/T 0450 Ronex Extra Duty 1 0451 Ronex MP 0553 RP Super Filter Coat #418 0707 RTV 1200 Prime Coat - Clear 0302 RTV60 Allied-Signal Allied-Signal Allied-Signal Allied-Signal Allied-Signal Allied-Signal Baker, J. T., Inc. Fisher Scientific GC Electronics Dur-A-Flex, Inc. Loctite Corporation Polychem - B&S Industries Relton Corporation Meriam Instrument Meriam Instrument Meriam Instrument Meriam Instrument VDO Instruments Meriam Instrument Sargent -Welch Scientific Comp R. P. Cargille Laboratories, Inc. R. P. Cargille Laboratories, Inc. Thermal Ceramics Clorox Company Exxon Company Loctite Corporation Henkel Corporation Henkel Corporation Supelco Inc. Amerada Hess Corporation Norton Company Norton Company RheinChemie Riken Metal Products Riken Metal Products Exxon Company Exxon Company Research Products Corporation Dow Corning Corporation General Electric Silicones 4/25/92 11/30/92 3/24/94 3/29/94 3/29/94 3/29/94 3/9/92 11/2/93 5/7/91 6/1/93 7/1/94 11/12/93 10/3/85 10/18/93 4/26/91 10/13/94 10/13/93 8/1/87 8/13/92 4/28/89 12/15/94 11 /1 /92 9/11/92 8/19/93 8/16/91 7/5/94 7/6/94 4/1/94 4/17/90 12/16/93 8/7/91 1/5/89 1/5/89 9/26/94 2/22/95 3/4/93 5/8/93 9/2/93 22 (dent Product Company Date 0724 Rubber & Shelia Bonded Grindi 1040 Rust Stopper 0843 RVC (RayVolve Cap) 0559 Safetap 1116 Safety Yellow Spray Paint B54 0353 Safety-Kleen 105 Parts Washin 0749 Safety-Kleen 105 Parts Washin 0004 Safety -Walk Brand Edge Sealin 0797 Salicylic Acid, 99%, A.C.S. Rea 0628 Sandy Beige Urethane Color C 0560 Sani-Tuff Heavy Duty Cleanser 0880 Santowhite Powder Antioxidant 0835 SBS-44 Protective Cream Wat 0836 SBS-46 Protective Cream Solv 1157 SC-0438 Solvent -based Adhesi 0001 Scot -Seal 800 Industrial Sealan 0005 Scotch Brand 1607 Heavy Duty 0716 Scotchcast Brand Electrical Re 0002 Scotchkote Brand Electrical Co 1000 Screw Lock Grade EV 7921 0058 Sealant 921 (Stick Grade) 0853 Sealtight CS-309 Curing Comp 0949 Sesco Dust Mop Treatment 0860 Signle-Strike Correctable Black 0803 Sikaflex-1 a 0230 Silica Gel 0807 Silica Sand 0290 Silicone Heat Sink Compound 0937 Silicone Oil 0116 Silver Goop 0232 Silver Nitrate Solutions 0608 Silver-Brite Aluminum Paint B5 0609 Silver-Brite Aluminum Paint Hi- 0620 Simple Green Concentrated Ind 0390 SKC-NF/ZC-7B Cleaner/Remo 0391 SKD-NF Developer 0392 SKD-S Spotcheck Developer 0824 Skid A490 0507 Skimming PIG Mats #MAT212, 0393 SKL-HF/S Spotcheck Penetrant Norton Company Fel-Pro Incorporated Raychem Safetec, Ltd. Sherwin-Williams Safety-Kleen Corporation Safety-Kleen Corporation Company 3M Aldrich Chemical Company Tennant Company Sani-Fresh International, Inc. Monsanto SBS Products, Inc. SBS Products, Inc. H.B. Fuller Company 3M Company 3M Company 3M Company 3M Loctite Corporation BTR Valve Sealants, Inc. Meadows, W. R., Inc. Cello Corporation Xerox Corporation Sika Corporation Fisher Scientific Southern Products & Silica Co GC Electronics Hach Company Crawford Fitting Company Fisher Scientific Sherwin-Williams Company Sherwin-Williams Company Sunshine Makers Magnaflux Corporation Magnaflux Corporation Magnaflux Corporation Stoner Incorporated New PIG Corporation Magnaflux Corporation 12/16/93 7/21/89 3/1/93 8/10/87 3/12/90 3/12/90 8/9/93 8/18/93 11/21/88 6/27/89 8/7/92 10/1/92 4/8/92 1/9/93 3/19/86 7/17/92 7/20/93 3/15/93 7/1/94 12/1/92 11/18/93 3/30/93 3/3/90 3/22/85 11/2/93 1/1/85 12/27/93 3/1/92 5/17/94 8/12/86 8/12/86 3/25/91 9/22/93 1/1/94 1/1/91 5/1/94 4/26/94 1/30/92 23 (dent Product Company Date 0394 SKL-W Water Washable Spotc 0972 Slimicide C-72P 0363 Small Screw Thrdlcker 50 ML 2 0342 Smooth Kote Insulating Finishi 0438 SN60 WRAP3 Solder 0511 Snoop 0108 Sodium Bicarbonate 0234 Sodium Bicarbonate 0299 Sodium Bisulfite Solution 0236 Sodium Carbonate 0968 Sodium Chloride 0238 Sodium Hydroxide Dry Solid, FI 1020 Sodium Hydroxide, 1N 0300 Sodium Metabilsulfite 1145 Sodium Metabisulfite 0878 Sodium Periodate for Mangane 0193 Sodium Persulfate 0768 Sodium Petroleum Sulfonate L- 0240 Sodium Thiosulfate Solution 0. 0087 Solar Salt Pellets 0549 Solder Seal Liquid Wrench No. 0550 Solder Seal Liquid Wrench No. 1143 Solest Series 0675 Solidaire Red Label 0706 Solvent Resistant Sealant 730 0464 Solvit All 0888 SorbaSet 0081 Sparkleen 0957 Sparkleen 0456 Spartan Synthetic EP 220 0708 Special Corning Cast Iron Wire 0065 Speedball Power Cleaner 0381 Speedbonder 324 Structural Ad 0364 Speedbonder 50 ML 319 Adh. 0076 Speede Mop 119-WP 0759 Speedtrack Clean & Burnish Fr 0815 Speedtrack Clean & Burnish Fr 0020 Spent Ethylene Glycol 0098 Spinerette Lubricant (Aerosol) 0825 Spinneret Lubricant K240 Magnaflux Corporation Betz Loctite Corporation Insulation Industries, Inc. Multicore Solders, Inc. Nupro Church & Dwight Co., Inc. Fisher Scientific General Chemical Corporation Fisher Scientific EM Science Fisher Scientific Betz Laboratories General Chemical Corporation Fisher Scientific Hach Company FMC Corporation Penreco Fisher Scientific Cargill Salt - Leslie Salt - A Ca Radiator Specialty Company Radiator Specialty Company CPI Engineering Services Airkem Professional Products Dow Corning Corporation Asinco Incorporated Omni Division/Ajax Calgon Corporation Calgon Vestal Laboratories Exxon Company Cronatron Welding Systems, In Butcher Company Loctite Corporation Loctite Corporation Namico Corporation Butcher Company Butcher Company Allied Signal Chesterton, A. W. Company Stoner Incorporated 10/22/91 1/14/92 8/19/93 8/1/88 8/27/86 3/6/89 4/10/94 11/2/93 10/1/90 5/17/94 10/27/87 11/2/93 2/16/91 5/1/92 9/5/93 7/16/93 7/1/93 12/16/85 5/17/94 4/28/93 9/1/92 6/1/92 11 /1 /93 1/7/92 11/11/92 7/27/92 4/14/94 6/24/94 6/24/94 2/22/95 5/2/90 5/1/93 8/19/93 8/19/93 1 /1 /93 5/1/93 12/1/90 11/22/91 7/1/89 5/1/94 24 (dent Product Company Date 0766 Spinnerette Lubricant Number 0006 Spray Adhesive,3M Brand Sup 0295 Spray Kleen 10-8666, 10-8666- 0912 SRI Grease NLGI 2 0340 SSR Ultra Coolant 0554 STA-FIL 0739 Stainless Steel - Sheet, Rod, B 0930 Stainless Steel AISI/SAE 300,4 0192 Staintec 10670 0721 Standafin CP/Code 15966 1017 Standapol 1611/15919 0839 Stantex 1026 0327 Stantex 1026-P (Code 15960) 0242 Starch 0244 Starch Indicator 0864 Static Stopper 0323 Stay Clean Soldering Fluxes 0157 Steel Ink Remover Aerosol 0447 Step Off Stripper 0346 Step Off Stripper 0288 Stic-Safe Adhesive (Flammabl 1121 Stop Lea 0092 Stop Leak # ROOSL 0200 STP Oil Treatment 0176 Stude Pull Electrode 0610 Style Perfect Interior Latex Ena 0611 Style Perfect Interior Latex Ena 0612 Style Perfect Interior Latex Ena 0613 Style Perfect Interior Latex Ena 0614 Style Perfect Interior Latex Ena 0088 Sul -Fury Drain Opener 1028 Sulfite 3 1024 Sulfite Indicator 1164 Sulfite Indicator Plus 219P 0940 Sulfonated Glycerol Trioleate 0493 Sulfonated Glycerol Trioleate 2 1131 Sulfuric Acid 0471 Sulfuric Acid N/50 0875 Sulfuric Acid Solution (2.5%) 0472 Sulfuric Acid Solution - 10N Chesterton, A. W. Company Company 3M GC Electronics Chevron Ingersoll-Rand Revere Products Reynolds Metals Company Marmon/Keystone Corporation Eutectic Corporation Henkel Corporation Henkel Corporation Henkel Corporation Henkel Corporation Fisher Scientific LabChem Incorporated Texwipe Company Harris, J. W., Co., Inc. DoAll Company Butcher Company Johnson, S. C. & Son, Inc. Fuller, H. B., Company Centimark Corporation Centimark Corp. First Brands Corporation Duratrode Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Sherwin-Williams Company Carroll Company Betz Laboratories Betz Laboratories Betz National Starch and Chemical National Starch And Chemical Rhone-Poulenc Betz Laboratories Fisher Scientific Betz Laboratories 12/17/85 4/10/86 2/9/91 8/1/88 3/1/93 9/24/93 1/1/93 2/1/92 3/26/92 5/2/94 6/30/94 4/17/91 11 /2/93 5/17/94 2/1/93 8/1/92 1/31/93 5/11/87 6/14/94 8/19/93 11/15/85 4/1/87 5/23/88 9/1/89 3/24/86 3/24/86 3/24/86 3/24/86 3/24/86 9/23/93 1/25/94 4/16/93 10/25/94 6/4/92 5/20/86 10/29/92 4/23/92 5/17/94 8/17/93 25 (dent Product Company Date 0474 Sulfuric Acid Solution 19.2N 0248 Sulfuric Acid Solutions, 0.05-4. 0246 Sulfuric Acid Solutions, 10N to 0172 Sulfuric Acid, 77 to 100% 0758 Sundance Floor Cleaner 1088 Sunflower Oil 0921 Super 3000 Mortar 1129 Super Caltemp 0951 Super Phos 105 0542 Super -Set Solder .025 X 1 Lb 1094 Super -Set Solder .032 X 15.5 ft 1098 Super -Set Solder .062 1096 Super -Set Solder .093 0382 Superbonder 495 Instant Adhes 1108 Superflex Ultra Blue Silicon 77 0383 Superflex(R) H Temp Silicone 0827 SupraCem Fiber Cement Buildi 0444 Supreme Gasoline 0349 Sure-Poxy Hi-Bild clear & color 1125 Sure-Poxy HM 1122 Surewall Surface Bonding Cem 0375 Swak 0625 Swen Sonic Dirl Strip 0453 Synesstic 100 0454 Synesstic 68 0788 Tak Pak Accelerator 0367 Tak Pak Accelerator 80 ML (Ite 1128 Tan Mask 0077 Tanatex RL-3739 0685 Tartan B (Welding Electrode) 0564 TAT'L Leak Detector 0985 TEAM Low Na+ Liquid Acid Ne 1162 TEMP -MAT Insulation 0627 Tempilstik Temperature Indicat 0638 Tennant STS (440)- Standard T 0084 Terephthalic Acid PTA 0439 Teresstic 32 0458 Teresstic SHP 320 0990 Tetrachloroethane 0178 Tetrachloroethane (1,1,2,2- Hach Fisher Scientific Fisher Scientific Du Pont Butcher Company Karlshamns - Lipid Specialists Premier Refractories and Chem Pabco Insulation Rhone-Poulenc Premier Industial Corporation Premier Industrial Corporation Premier Industrial Corporation Premier Industrial Corporation Loctite Corporation Loctite Corporation Loctite Corporation Cemfort Incorporated Exxon Company Kaufman Products, Inc. Kaufman Products American Home Products Cajon Company Swen Sonic Corporation Exxon Company Exxon Company Loctite Corporation Loctite Corporation Mohawk Finishing Products Inc Sybron Chemicals Incorporated Nassau Research Corporation Shamrock Specialties Baker, J.T. Incorporated Pittsburgh Corning Corporation Tempil Division, Big Three Indu Tennant Company Cape Industries Exxon Exxon Company Fisher Scientific Fisher Scientific 9/12/93 5/17/94 5/17/94 1/1/88 5/1/93 8/27/93 8/1/92 4/1/92 6/27/91 7/26/88 11/7/85 1/29/93 1/29/93 8/19/94 8/17/88 7/1/94 4/10/90 9/11/92 4/19/90 11 /1 /85 6/14/88 9/1/91 1/1/88 4/16/94 2/22/95 7/1/94 7/1/94 4/6/88 10/27/93 1/25/91 6/29/94 4/15/87 6/14/88 1 /1 /92 2/10/87 2/22/95 8/1/94 10/31/81 7/15/91 26 (dent Product Company Date 0250 Tetrahydrofuran 0772 Tetrahydrofuran 1-QA600 0640 Texacar EC 75435 1106 Thermal Wave Absolute Strip 1105 Thermal Wave Bottom Layer 0642 Thermal Arc Torch Coolant (Co 0916 Thermal Green Cleaner 0913 Thermal Green Finish 0914 Thermal Green Remover 0915 Thermal Green Sealer 0786 Thermal Wave Buffing Polish 0401 Thermal Wave Extender 0437 Therminol VP-1 Heat Transfer 1120 Thermo-12 Calcium Silicate Ins 1007 Thermo -Ceram Braided and Ro 1008 Thermo-Sil Cloth, Tape, Tubing 0479 Thermyl-Glyde Extreme Servic 0633 Thick Coat Resurfacer Part A 7 0636 Thick Coat Resurfacer Part A 7 0634 Thick Coat Resurfacer Part B 7 0637 Thick Coat Resurfacer Part B 7 0635 Thick Coat Resurfacer Part C 7 0629 Thin Coat Resurfacer Part A 71 0631 Thin Coat Resurfacer Part A 71 0630 Thin Coat Resurfacer Part B 71 0632 Thin Coat Resurfacer Part B 71 1002 Tinuvin 622 LD 1006 Tinuvin P 0252 Titanium Dioxide 0254 Titanium Reference Standard S 0918 Toner - 3M Brand Type 148 1031 Toner-7041 1057 Toner - Black for DC-3648 0536 Total Eclipse/T/W Hi -Speed Flo 0667 TPC Solvent 0521 TPD Thinner 0639 Traction Grit 295 1059 Traffic Lane Cleaner / Prespray 0901 Transfer Recording Cartridge 0649 Tremfix Fisher Scientific BLH Electronics Huntsman Pioneer/Eclipse Corporation Pioneer/Eclipse Corporation Thermal Dynamics Corporation Maintenance Supply Company Maintenance Supple Company Maintenance Supple Company Maintenance Supply Company Pioneer/Eclipse Corp. Maintenance Supply Company, Monsanto Schuller Garlock Incorporated Garlock Incorporated Royal Purple Tennant Company Tennant Company Tennant Company Tennant Company Tennant Company Tennant Company Tennant Company Tennant Company Tennant Company Ciba-Geigy Corporation Ciba-Geigy Corporation Fisher Scientific Fisher Scientific Company 3M Xerox Corporation Mita Industrial Company Pioneer/Eclipse Corp. Penetone Corporation PDI, Inc. Tennant Company Defender Services Xerox Corporation Tremco 11/2/93 10/3/91 7/1/94 1/1/85 1/1/85 10/1/91 7/31/91 7/31/91 7/31/91 7/31/91 7/1/92 9/15/92 11/30/93 6/22/89 4/18/90 2/15/91 1/1/92 1/1/92 1/1/92 1/1/92 1/1/92 1/1/92 1/1/92 7/23/87 1/1/92 5/24/91 4/30/92 11/2/93 11/2/93 8/20/92 6/8/92 9/1/92 3/3/93 1/23/90 12/1/84 1/1/92 1 /1 /94 4/22/86 6/1/89 27 (dent Product Company Date 1146 Tri Water Plug 0650 TRI-DEX MSP-21 0522 Tri-Ethane 0713 Trichloroethan III Degrs CoIdN 0256 Triethylene Glycol 0330 Triethylene Glycol 0336 Triethylene Glycol 0653 Triethylene Glycol 0053 Trifluoroacetic Acid 1152 Trim Sol 0258 Tris (Hydroxymethyl) Aminome 0689 Triton X-100 Surfactant 0485 Troysan 174 1104 Trycol 5904 (15926) 0829 Tubeboard 0767 Turbo Oil 2380 1127 Turmotemp 11/400 Series Fluori 1047 Tween 80 - Bingo Marker Ink C 1015 Type 152 Developer Premix 0173 Tyzor TE Titanate 0654 UCON Heat Transfer Fluid 500 0712 Ultra Black RTV Silicone 0384 Ultra Blak(TM) RTV Silicone 1041 Ultra Gear Lubricant 85W-140 0683 Ultra Gear Lubricant SAE 80W- 0774 Unisilkon TK 017/200 Therm 0352 Unisilkon TK 017/200 Therm 1111 Unisilkon TK44N2RECA 1175 Univolt N 61 0530 Uniweld 100 Part A - 100% Soli 0531 Uniweld 100 Part B - 100% Soli 0532 Uniweld Part A 0533 Uniweld Part B 1177 Used Fiber Finish Oil Emulsion 0748 Uvitex OB 0755 Uvitex RSB 0096 Vaseline Petroleum Jelly 0034 Velodur Metal Standard Activat 0035 Velodur Metal Standard Base 1 0036 Velodur Rapid Activator 1003 Tri-Chem Corporation Trion, Inc. PPG Industires Ashland Chemical Company Fisher Scientific Hoechst Celanese Corporation ICI Americas Inc. Union Carbide AquAir Corporation Mater Chemical Corporation Fisher Scientific Van Waters & Rogers Inc. Troy Chemical Henkel Corporation Sunoco Products Company Exxon Company Lubricant Consult/Triple Crown Van Waters and Rogers Incorp Company 3M Du Pont Union Carbide Loctite Corporation Loctite Corporation Chevron Chevron Kluber Lubrication Kluber Lubrication Corporation Kluber Lubrication Corporation Exxon Permagile Industries Inc. Permagile Industries Inc. Permagile Industries Inc. Permagile Industries Inc. AlliedSignal Ciba-Geigy Corporation Ciba-Geigy Corporation Chesebrough-Pond's Inc. American Durweld Sales Inc. American Durweld Sales Inc. American Durweld Sales Inc. 1/28/91 9/1/91 1/1/82 6/27/94 11/2/93 1/1/88 9/12/89 12/10/93 1 /1 /89 6/1/91 11/2/93 2/12/91 12/1/92 9/14/94 7/1/85 3/15/88 12/28/90 12/1/92 10/3/93 4/8/92 3/23/90 7/1/94 9/15/89 3/18/92 2/15/89 2/15/89 4/9/87 9/15/93 7/2/94 7/2/94 4/29/94 7/2/94 3/1/95 6/14/91 9/22/93 10/20/88 5/1/92 5/1/92 5/1/92 28 (dent Product Company Date 0037 Velodur Rapid Base 1004 VEL 0038 Velodur Special Bio-Cleaner 10 0064 Viscosity Standard Fluid 10 (10 0725 Vitirfied Bonded -Abrasive Prod 0563 Wash -A -Bye -Baby Wet Wipe 0089 Wasp/Hornet Jet Stream 1009 Water Cut -Off Mastic 0090 Wax Emulsifier 1079 WBMP, WBMP-HP 0661 WD-40 Aerosol 0850 Welding Electrode Twenty Thirt 1046 White Mineral Oil, USP/NF - Bi 0776 Wolfracoat C 1114 Woodbin Spray Paint 0728 Wrought Aluminum Alloy - 1)0( 0729 Wrought Aluminum Alloy - 2XX 0731 Wrought Aluminum Alloy - 4XX 0732 Wrought Aluminum Alloy - 5XX 0733 Wrought Aluminum Alloy - 6XX 0734 Wrought Aluminum alloy - 7XX 0735 Wrought Aluminum Alloy - 8XX 1182 Wrought Aluminum Alloy 6XXX 0730 Wrought Aluminum Alloys - 3X 0385 X-MNS(TM) Clean up Solvent f 0711 X-NMS Clean up Solvent for In 0687 X-NMS Clean Up Solvent for In 0445 XD-3 Extra 15W-40 0818 XL-2G Preemergence Herbicid 0260 Xylenes 0339 Yellow 77 Wire Pulling Lubrica 0411 Yellow Oil #120 0283 Yellow/Green Liquid Concentrat 0480 York C Oil 0296 Zero Mist Circuit Cooler 1159 Zeston PVC Pipe Covers and J 0262 Zinc Acetate Dihydrate 0312 Zonolite: Masonry Insulation BI American Durweld Sales Inc. American Durweld Sales Inc. Brookfield Engineering Laborat Norton Company Scott Carroll Company Centimark Corporation Carroll Company ResinTech Incorporated WD-40 Company Duratrode Van Waters and Rogers Incorp Kluber Lubrication Sherwin-Williams Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Reynolds Metals Company Loctite Corporation Loctite Corporation Loctite Corporation Exxon Company DowElanco Fisher Scientific Ideal Industries, Inc. Meriam Instrument Formulabs, Inc. Delta Petroleum Company GC Electronics Schuller International Fisher Scientific Grace, W. R. & Company 5/1/92 1/1/88 3/11/94 12/14/93 9/23/93 5/1/93 9/23/93 3/22/94 1/1/89 4/11/91 2/12/91 3/7/89 5/27/87 7/29/93 7/29/93 7/29/93 7/29/93 12/3/93 7/7/93 9/24/93 12/3/93 7/29/93 7/1/94 8/19/93 2/12/91 2/22/95 11/2/93 7/29/93 10/18/93 3/31/93 9/19/88 5/9/91 2/28/94 11/7/93 3/11/93 29