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HomeMy WebLinkAboutWQ0003504_Modification_20210915Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0003504 Applicant/Permittee City Of Durham Applicant/Permittee Address 101 City Hall Plaza Durham, NC 27701 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Municipal Facility Name City of Durham RLAP County Durham Fee Category Major Is this a complete application?* c Yes r No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Fee Amount $395 Complete App Date 09/15/2021 Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff Name * Ryan Copeland Email Address* rcopeland@synagro.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) c Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 336-607-4494 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00003504 Fbs Current Existing perrrit number Applicant/Permittee * City Of Durham Applicant/Permittee Address* 101 City Hall Plaza Durham, NC 27701 Facility Name * City of Durham RLAP Please provide comments/notes on your current submittal below. Payment will be mailed in along with Upload Confirmation At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Spec'rfications, Calculations, Rc.) 2021 Durham Modification.pdf 162.94MB upload only 1 RCF document (less than 250 NS). NL@iple documents nest be combined into one RDF file unless file is larger than upload lirrit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 8/29/2021 MODIFICATION OF PERMIT PERMIT # WQ0003504 Land Application of City of Durham, NC Residuals Prepared by: SYNAGRO CENTRAL, LLC 284 Boger Road Mocksville, NC 27028 P (336) 998-7150 F (336) 998-8450 August 12th, 2021 N.C. Department of Environment and Natural Resources Division of Water Resources Water Quality Permitting Section – Non-Discharge Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 ATTENTION: Mr. Nathaniel Thornburg REFERENCE: APPLICATION FOR MODIFICATION OF PERMIT # WQ0003504 CITY OF DURHAM Dear Mr. Thornburg: On behalf of the City of Durham, Synagro is submitting this application to modify the referenced residuals land application permit. All new and modified fields are listed, on for “LASC”, as “New” and “Modified” with all other fields listed as “Renewal” Forms RLAP, LASC, and RSC are included, along with other required forms and documentation. The following sites are listed as “renewed” with no changes: The following sites are listed as “New” NC-AM-10 Field 1 NC-PS-3 Fields 5 & 6 The following sites are listed as modified NC-OR-15 Field 1 NC-OR-87 Fields 1 & 2 This application package should contain all of the information necessary to complete the requested modification of the City of Durham’s permit. However, if you require additional information or have further questions, please contact me at (336) 607-4494 or rcopeland@synagro.com. Thank you in advance for the timely and efficient review of this renewal application. Sincerely, Ryan Copeland 284 Boger Road, Mocksville, NC 27028 Phone: (336) 998-7150 Fax: (336) 998-8450 State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 – RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section’s Non-Discharge Permitting Unit General – This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. The Applicant’s Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). If this project is for a modification of an existing permit, submit one copy of the existing permit. Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). 1 Facility Classification New Permit Major Modification Major (land are permitted for 300 acres)$1,310 $395 Minor (land are permitted for < 300 acres) $810 $245 1 - A major modification shall be defined as any permit modification that: increases the generating facility’s residuals dry tonnage; adds additional land application areas not previously approved for that particular program \[including transferring of field(s) from one program to another\]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (May be Required – See 15A NCAC 1C .0300) Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Page 1 of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: Operational functions;describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. Maintenance schedules; may include equipment calibration, maintenance of signs, etc. Safety measures;may include safety training program, manuals, signs, etc. Spill response plan; including control, containment, remediation, emergency contact information, etc. Inspection plan including the following information; Names and titles of personnel responsible for conducting the inspections. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. Sampling and monitoring plan including the following information; Names and titles of personnel responsible for conducting the sampling and monitoring. Detailed description of monitoring procedures including parameters to be monitored. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T .1102(12). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. Please contact the Non-Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G.Program Information Provide an explanation of why a dedicated system is required instead of a conventional non-dedicated system. Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) Submit three (3) sets of standard size plans and two (2) sets of 11" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. Plans must include the following minimum items: A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). Delineation of the review and compliance boundaries Setbacks as required by 15A NCAC 02T .1108 Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist’s evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 I. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: http://www.ncwater.org/Rules_Policies_and_Regulations/. The document shall be signed, sealed and dated by a qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .1104(d)(2). For Modifications, submit an updated site map specific to the modification(s) only. The design documents must include the following minimum items: Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) Submit a completed and accurate water balance in accordance with 15A NCAC 02T .1104(d)(5) and current Division Policy available at: http://www.ncwater.org/Rules_Policies_and_Regulations/. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) Property ownership documentation shall consist of one of the following: Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or An easement running with the land specifically indicating the intended use of the property and meeting the requirements of 15A NCAC 02L .0107(f), or A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON-DISCHARGE PERMITTING UNIT By U.S. Postal Service:By Courier/Special Delivery: 1617 MAIL SERVICE CENTER 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27699-1617 RALEIGH, NORTH CAROLINA 27604 TELEPHONE NUMBER: (919) 807-6464FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3 State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 – RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I.APPLICANTINFORMATION: 1.Applicant's name: City Of Durham Applicant type: Individual Corporation General Partnership Privately-Owned Public Utility Federal State Municipal County Signature authority’s name per 15A NCAC 02T .0106: Don F. Greeley Title: Director Of Water Management Applicant’s mailing address: 101 City Hall Plaza City: Durham State: NC Zip: 27701- Telephone number: (919) 560-4381 Email Address: don.greely@durhamnc.gov 2.Consultant’s name: Ryan CopelandLicense Number(for P.E.): Affiliation: On StaffRetained (Firm: ) Consultant’s mailing address: 284 Boger Road City: Mocksville State: NC Zip: 27028- Telephone number: (336) 607-4494 Email Address: rcopeland@synagro.com 3. Agronomist’s name: License Number: Affiliation: N/A On Staff Retained (Firm: ) Agronomist’s mailing address: City: State: Zip: - Telephone number: ( ) - Email Address: 4. Soil Scientist’s name: Eric Thompson License Number: 1238 Affiliation: N/A On Staff Retained (Firm: ) Soil Scientist’s mailing address: City: State: Zip: - Telephone number: ( ) - Email Address: 5. Fee submitted: (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): new, modified, renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0003504 Date of most-recently issued permit: 10/21/2015 Date of most-recently certified Attachment A(if different than the permit): 4/4/2017 Date of most-recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility’s physical address: 1900 East Club Blvd. City: DurhamState: NCZip: 27704- Coordinates: Latitude: 36 0142 Longitude: 78 5133 Datum: NAD 84 Level of accuracy: Second Method of measurement: Map 2. County where residuals land application program is headquartered: Durham 3. List the Operator In Responsible Charge (ORC) and all Back-Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC John Dodson City Of Durham LA25935 Back-Up ORC Charles Cocker City Of Durham LA13526 Additional Back-Up ORCs (if applicable) If an ORC and at least one Back-Up ORC are not currently designated for this residuals land application program, provide the candidates’ names, affiliations, and an estimated time schedule for each candidate’s completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source-generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 9292 dry tons per year. PAN Pounds of PAN per Dry Ton Pounds of PAN per Year (Weighted Average) Surface Incorporation Surface Incorporation or Injection or Injection First-Year 30.92 38.87 287,309 361,180 Five-Year Maximum Adjusted 48.14 56.09 447,319 521,190 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 605 Hay 2026.5 Pasture Total: 2631.5 Methods Surface 2631.5 Incorporation or Injection Total: 2631.5 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Acres Required Using Acres Required Using Application Rate First-Year PAN Concentrations Five-Year Maximum Adjusted PAN Concentrations (lbs PAN/ac-yr) Surface Incorporation or Surface Incorporation or Injection Injection 50 5746.2 7223.6 8946.4 10423.8 100 2873.1 3611.8 4473.2 5211.9 150 1915.4 2407.9 2982.1 3474.6 200 1436.5 1805.9 2236.6 2605.9 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): Non-dedicated Dedicated If Dedicated, specify the following (check all that apply): Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Siite Certification.doc FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: Spray Drip 2. Disposal system is: existing proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one-foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? Yes or NoIf Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Recommended Recommended Soil Series Fields within Soil Area Loading Rate Loading Rate (in/hr) (in/yr) 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? Yes or No If No, explain why 15A NCAC 02T .0505(n)is not met: 7. Non-dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Design Area Number of Maximum Application Design Annual Loading Field / Zone 2 (ft) NozzlesRate (gallons/hr) Rate (gallons/yr) Total Plan Sheet Specification Spray Irrigation Design Element Number Page Number Wetted diameter of nozzles ft 2 Wetted area of nozzles ft Nozzle capacity gpm Nozzle manufacturer / model / Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 SPILL RESPONSE PLAN PROJECT: City of Durham Permit WQ0003504 IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN IMMEDIATELY: 1.MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Synagro Operations Manager shall take immediate charge and initiate clean-up activities. Synagro labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the City of Durham NC or the NC Department of Transportation, and other private contractors as necessary. 2.HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3.CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Synagro Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean- up operation, i.e., local farmers, farm supply centers, nurseries, etc. 4.CLEAN-UP: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand-soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5.FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6.NOTIFICATION: As soon as possible after the spill occurs, the Synagro Operations Manager or assistant will notify the Synagro Central office, and they will then be responsible for notifying other key Synagro personnel. 7.REPORTING: Synagro Central personnel will notify the Winston Salem Regional office (336) 776-9800 or the Raleigh Regional office (919)791-4200 for the City of Durham as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The Operations Manager shall provide a written report within 48 hours of the spill to the Technical Services Director. The report shall list all relative information and actions taken. Synagro Central personnel will file a written report to the Winston Salem Regional office of the NCDENR within 5 days of the occurrence. For after hours reporting the Division’s emergency number shall be called to report all incidences (1-800-858-0368). State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section’sNon-Discharge Permitting Unit General – This certification provides detailed information of residuals source generating facility and its residuals quality for land . Do not submit this certification for review without application, distribution, or disposal in accordance with 15A NCAC 02T .1100 a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A.Residuals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit a separate certification for each source facility. For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B.Residuals Source-Generating Facility Information: For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the “Map Guidance for Residuals Land Application Permits”. Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan - A detailed sampling plan for the residuals source-generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division-certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C.Residuals Quality Information: For each source facility, attach the following: Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 1 Page 900 600 42123580 Proposed s Per Year Dry Ton b 900600 42123580 Maximum Current 10(B) -0 0023841 32010(A) 32 - - NCNC0047597 03 03 Permit Number D (Deleted) County DurhamDurhamDurhamDurham M (Modified) ent reatment ham WRF PlantPlant Durham WRF h Dur Facility Name R (Renewed) NortSouth Brown Water T Williams Water Treatm N (New) 16 - 06 hamhamhamham are: RSC : RM facility FO City Of Durham City Of DurCity Of DurCity Of DurCity Of Dur source Facility Permit Holder a RR R R atus StCode Status Code for RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: a SUMMARY FOR of 5 2 Page (i.e, not applicable to new facility). distribution, land application, or disposal for permitted 16 - residuals currently 06 he amount of T b FORM: RSC State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE-GENERATING FACILITY INFORMATION (See Instruction B.): 1.FacilityName: North DurhamWRF 2. Facility permit holder is: Federal, State, Local Government, or Private. Facility permit issued by:Div. of Water Resources,Div. of Environmental Health, or Other (explain: ). 3. Facility contact person and title: John Dodson WWTP Superintendent Complete mailing address: 1900 E Club Blvd. City: Durham State: NC Zip: 27701- Telephone number: (919) 560-4384E-mail address: john.dodson@durhamnc.gov 4.Facility physical address: 1900 E Club Blvd. City: Durham State: NC Zip: 27701- Coordinates: Latitude: 36 0142 Longitude: 78 5133 Datum: NAD 84 Level of accuracy: Second Method of measurement: Map 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water,treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes No 7.Facility permitted/design flow: 20MGD and facility average daily flow: 8.9MGD 8.Average amount of residuals being generated at this facility 2129.53dry tons per year. 9.Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 4 Million Gallon Anaerobic Digester Type and volume of residuals storage (i.e., outside of residuals treatment units): 4.5 Acre Covered Storage Pad II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6)as: Biological Non-Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-hazardous under RCRA:(Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non-municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: yes no. If yes, list the number(s): b.Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR§261.21- 261.24: yes no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental Technologies and Date of analysis: 10/01/2019 Passed corrosivity test: yes no. pH: 7.9 s.u. (2 < pH < 12.5) oo Passed ignitability test: yes no. Flashpoint: >140 F (> 140F) Passed reactivity test: yes no. HCN: ND mg/kg (<250) & HS: ND mg/kg (<500) 2 TCLP Parameter Limit Result TCLP Parameter Limit Result (mg/l) (mg/l) (mg/l) (mg/l) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 1/27/2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mg/kg) (mg/kg) (mg/kg) Arsenic 75 41 4.89 Cadmium 85 39 0.925 Copper 4,300 1,500 408 Lead 840 300 15.8 Mercury 57 17 0.419 Molybdenum 75 n/a 18.6 Nickel 420 420 13.7 Selenium 100 100 5.58 Zinc 7,500 2,800 2590 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Arsenic Chromium Nickel Unit to Boundary to Closest Property Line (meters, check one) (mg/kg) (mg/kg) (mg/kg) > 0 but < 25 30 200 210 34 220 240 39 260 270 46 300 320 53 360 390 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 15.9 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 1/27/2020 Parameter Result (mg/kg) Aluminum 14,500 Ammonia-Nitrogen11,800 Calcium 14,200 Magnesium 7,250 Nitrate-Nitrite Nitrogen31.3 pH (Standard Unit) 8.8 Phosphorus 33,100 Potassium 3,480 Sodium 598 Total Kjeldahl Nitrogen 60,500 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): .41 \[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth\]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This rate is a (check one): default value, or actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: st ) Year PAN Application Method First (1Five-Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 15,671 23,166 Injection/Incorporation 21,571 29,066 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp.density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non-biological residuals): Alternative 1 \[15A NCAC 02T.1106(b)(3)(A)\] - Time/Temperature Compliance. Alternative 2 \[15A NCAC 02T.1106(b)(3)(B)\] - Alkaline Treatment. Alternative 3 \[15A NCAC 02T.1106(b)(3)(C)\]-Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 \[15A NCAC 02T.1106(b)(3)(D)\] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 \[15A NCAC 02T.1106(b)(3)(E)-(K)\] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, gamma ray irradiation, or pasteurization. b. For Land Application of Class B: Alternative 1 \[15A NCAC 02T.1106(c)(1)\] - Fecal Coliform Density Demonstration. Alternative 2 \[15A NCAC 02T.1106(c)(2)\] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, air drying, anaerobic digestion, composting, or lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt - If Daily Cover Alternative is chosen in Item II.8. below \[15A NCAC 02T.1106(a)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 \[15A NCAC 02T.1107(a)(1)\] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 \[15A NCAC 02T.1107(a)(2)\] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 \[15A NCAC 02T.1107(a)(3)\] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 \[15A NCAC 02T.1107(a)(4)\] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 \[15A NCAC 02T.1107(a)(5)\] - 14-Day Aerobic Processes. Alternative 6 \[15A NCAC 02T.1107(a)(6)\] - Alkaline Stabilization. Alternative 7 \[15A NCAC 02T.1107(a)(7)\] - Drying of Stabilized Residuals. Alternative 8 \[15A NCAC 02T.1107(a)(8)\] - Drying of Unstabilized Residuals. Alternative 9 \[15A NCAC 02T.1107(a)(9)\] - Injection. 3504 Alternative 10 \[15A NCAC 02T.1107(a)(10)\] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover \[15A NCAC 02T.1107(b)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Residuals Sampling Plan City of Durham Land Application Program North Durham WRF Nutrients and Metals Analysis Sampling Point:Dewatered Residuals Storage Shed Sampling Frequency: 6/yr Sample Type: Composite Lab: Waypoint Analytical Pathogen Reduction (Fecal Coliform Density Demonstration) Sampling Point: Dewatered Residuals Storage Shed Sampling Frequency: 6/yr Sample Type: Grab – Fecal Coliform tests Lab: In house Vector Attraction Reduction (38% Volatile Solids Reduction) Sampling Point: Digester Influent & Effluent & Dewatered Residuals Storage Sampling Frequency: 6/yr Sample Type: Composite Lab: In house TCLP Sampling Point: Dewatered Residuals Storage Shed Sampling Frequency: Annually Sample Type: Composite Lab: Summit Environmental Technologies, Inc 203803131! 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ZftOp Tbnqmft!xfsf!dpotjefsfe!bddfqubcmf!bt!dppmjoh! qspdftt!ibe!cfhvo/ ZftOpO0B Xbufs!.!Tbnqmf!dpoubjofst!qspqfsmz!qsftfswfe OpO0B Xbufs!.!WPB!wjbmt!gsff!pg!ifbetqbdfZft ZftOpO0B Usjq!Cmbolt!sfdfjwfe!xjui!WPBt ZftOpO0B Tpjm!WPB!nfuipe!6146!€!dpnqmjbodf!dsjufsjb!nfu Ijhi!dpodfousbujpo!dpoubjofs!)59!is*Mpx!dpodfousbujpo!FoDpsf!tbnqmfst!)59!is* Ijhi!dpodfousbujpo!qsf.xfjhife!)nfuibopm!.25!e*Mpx!dpod!qsf.xfjhife!wjbmt!)Tpe!Cjt!.25!e* Tqfdjbm!qsfdbvujpot!ps!jotusvdujpot!jodmvefe@ZftOp Dpnnfout; Tjhobuvsf;Csboej!XbutpoEbuf!'!Ujnf;1202803131!22;4:;23 Qbhf!6!pg!7 Qbhf!7!pg!7 SummitEnvironmentalTechnologies,Inc. 3310 WinSt. CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com October 01, 2019 RyanCopeland Synagro 284BogerRd. Mocksville,NC27028 TEL:(336) 998-7150 FAX: (336) 998-8450 RE: Durham OrderNo.:19090846 DearRyanCopeland: Summit Environmental Technologies,Inc.received 1 sample(s) on 9/12/2019forthe analyses presentedinthefollowingreport. Therewere no problemswiththeanalyticaleventsassociatedwiththisreport unless noted intheCaseNarrative. Qualitycontrol dataiswithinlaboratory defined ormethod specifiedacceptancelimits exceptwhere noted. Ifyou haveany questionsregardingthesetestsresults, pleasefeelfreetocallthe laboratory. Sincerely, Jennifer Woolf ProjectManager 3310 WinSt. CuyahogaFalls,Ohio 44223 Arkansas88-0735,California07256CA,Colorado,ConnecticutPH-0108,Delaware,FloridaNELACE87688,GeorgiaE87688,IdahoOH00923,Illinois 200061,IndianaC-OH-13,KansasE-10347,Kentucky(UndergroundStorageTank)3,Kentucky90146,Louisiana04061, Maryland339, Minnesota 409711,NewHampshire2996,New JerseyOH006,NewYork11777,NorthCarolina39705and631,NorthDakotaR-201,OhioDW,OhioVAP CL0052,Oklahoma9940,OregonOH200001,Pennsylvania010,RhodeIslandLA000317,SouthCarolina92016001,Texas T104704466-11-5,Utah OH009232011-1,VirginiaVELAP9456,WashingtonC891 Page1of39 SummitEnvironmentalTechnologies,Inc. CaseNarrative 3310 WinSt. CuyahogaFalls,Ohio44223 WO#: 19090846 TEL:(330)253-8211FAX:(330)253-4489 Date: 10/1/2019 Website:http://www.settek.com CLIENT:Synagro Project:Durham WorkOrderNarrative: 19090846: Thisreportinitsentiretyconsists ofthefollowing documents:CoverLetter,CaseNarrative, AnalyticalResults,QCSummaryReport,ApplicableAccreditationInformation,Chain-of-Custody, CoolerReceiptForm,and otherapplicableformsas necessary.All documentscontaintheSummit Environmental Technologies,Inc.,WorkOrderNumberassignedtothisreport. Summit EnvironmentalTechnologies,Inc., holdstheaccreditations/certificationslistedatthe bottom of thecoverletterthatmay ormay not pertaintothisreport.Pleaserefertothe"AccreditationProgram AnalytesReport"foraccreditedanalyteslist. Theinformationcontainedinthisanalyticalreportisthe sole property ofSummit Environmental Technologies,Inc.andthat ofthecustomer.Itcannot bereproducedinanyformwithouttheconsent of Summit EnvironmentalTechnologies,Inc. orthecustomerforwhichthisreportwasissued. Theresults containedinthisreportare onlyrepresentative ofthe samplesreceived.Conditionscan varyat different timesandat different samplingconditions.Summit Environmental Technologies,Inc.is notresponsible for use orinterpretation ofthe dataincluded herein. AllresultsforSolidSamplesarereported on an"asreceived" or"wetweight" basis unlessindicatedas "dryweight" usingthe"-dry" designation on thereporting units. Thisreportis believedtomeetall oftherequirements oftheaccreditingagency,whereapplicable.Any comments or problemswiththeanalyticaleventsassociatedwiththisreportare noted below. AnalyticalSequenceSampleNotes: 19090846-001ATCLP-SVOC_8270E:Surrogateoutsiderecoverylimits.Minimummethodcriterion of one surrogatewithinestablishedrecoverylimitswasmet. 19090846-001a TCLP-SVOC-CPest(8081B):CCVexhibited high biasedrecoveriesfor several analytes;associatedsampleresultsareN.D. 19090846-001ATCLP-SVOC-Herb_TCLP(8321):Sampleexhibited outlyingrecovery ofSurrogate: DCAA. Original Page2of39 SummitEnvironmentalTechnologies,Inc. QualifiersandAcronyms 3310 WinSt. CuyahogaFalls,Ohio44223 WO#: 19090846 TEL:(330)253-8211FAX:(330)253-4489 Date: 10/1/2019 Website:http://www.settek.com ThesecommonlyusedQualifiersandAcronymsmayormaynotbepresentinthis report. Qualifiers Thecompoundwasanalyzedforbutwasnotdetected. U ThereportedvalueisgreaterthantheMethodDetectionLimitbutlessthantheReportingLimit. J HTheholdtimeforsamplepreparationand/oranalysiswasexceeded. Theresultisreportedfromadilution. D Theresultexceededthelinearrangeofthecalibrationorisestimatedduetointerference. E Theresultisbelowthe MinimumCompound Limit. MC *TheresultexceedstheRegulatoryLimitorMaximumContaminationLimit. Manualintegrationwasusedtodeterminethearearesponse. m Manualintegrationinwhichpeakwasdeleted d TheresultispresumptivebasedonaMassSpectrallibrarysearchassuminga1:1response. N PThesecondcolumnconfirmationexceeded25%difference. TheresulthasbeenconfirmedbyGC/MS. C TheresultwasnotconfirmedwhenGC/MSAnalysiswasperformed. X Theanalytewasdetectedintheassociatedblank. B/MB+ GTheICBorCCBcontainedreportableamountsofanalyte. TheCCVrecoveryfailedlow(-)orhigh(+). QC-/+ TheRPDwasoutsideofacceptedrecoverylimits. R/QDR TheLCSorLCSDrecoveryfailedlow(-)orhigh(+). QL-/+ QLRTheLCS/LCSDRPDwasoutsideofacceptedrecoverylimits. TheMSorMSDrecoveryfailedlow(-)orhigh(+). QM-/+ TheMS/MSDRPDwasoutsideofacceptedrecoverylimits. QMR TheICVrecoveryfailedlow(-)orhigh(+). QV-/+ SThespikeresultwasoutsideofacceptedrecoverylimits. Deviation;Adeviationfromthemethodwasperformed; PleaserefertotheCaseNarrativefor Z additionalinformation Acronyms NDNotDetectedRLReportingLimit QualityControlMethodDetectionLimit QCMDL MBMethodBlankLODLevelofDetection LaboratoryControl SampleLevelofQuantitation LCSLOQ LaboratoryControl SampleDuplicatePracticalQuantitationLimit LCSDPQL QualityControl SampleContractRequiredQuantitationLimit QCSCRQL DUPDuplicatePLPermitLimit Matrix SpikeRegulatoryLimit MSRegLvl Matrix SpikeDuplicateMaximumContaminationLimit MSDMCL RelativePercentDifferentMinimumCompoundLimit RPDMinCL InitialCalibrationVerificationReanalysis ICVRA ICBInitialCalibrationBlankREReextraction ContinuingCalibrationVerificationTentativelyIdentifiedCompound CCVTIC CCBContinuingCalibrationBlankRTRetentionTime ReportingLimitCheckCalibration Factor RLCCF DilutionFactorResponseFactor DFRF Thislist of QualifiersandAcronymsreflects themostcommonlyutilizedQualifiersandAcronyms forreporting. Pleaserefer to theAnalyticalNotesin theCaseNarrativeforanyQualifiersorAcronyms thatdonotappearin this list or foradditionalinformationregarding theuseof theseQualifiersonreporteddata. Original Page3of39 SummitEnvironmentalTechnologies,Inc. Workorder 3310 WinSt. SampleSummary CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 19090846 Website:http://www.settek.com 01-Oct-19 CLIENT:Synagro Project:Durham TagNo Lab SampleIDClient SampleIDDateCollectedDateReceivedMatrix 19090846-001NorthDurham9/11/20199:10:00AM9/12/201910:10:00AMSludge Page4of39 te l a PMPMPMPMPMPMPMPM AMAMAM AM a D n 19 i s -0000000011000000 45000000 i :::::::: t :::: g s RT i c r 2517173256031339 90846 35491200 :::::::: :::: 0 aly -O 55543164 O O 5 101011 19 01 An P 999 111 20192019201920192019201920192019 0002019 //////// E / 222 78877596 8 21111211 1 //////// / R 99999999 #:9 9/27/9/26/9/25/ O S W A A PMAMPMPM 0041 TE :: 00000000 :::: 0330 :: 45020000 :::: 11111955 DA te a 201920192019201920192019 D ////// 768655 p 111111 ////// re 9M99M999 P PMPMPMPM 0000 0000 :::: 00000000 te :::: a 5555 D 9999 e 1111 t 0000 a 2222 h c a 9/15/9/15/9/15/9/15/ : Le LP id C 846 ol - T - s W )-S e 1311/8081) 2 11/6010) d . (S s .21311/7470) i 3i 3W t 4 010) c s . 1 . si S W 1 y 3 ( e3 bl ( . S . r a ( Ts 7 7 e n i / /n s s(SW s isis o ) 4 i H dAss y 4s s il iyy 1 y 39 s a s l alal 901 n y ale inati f ( iqul 903nn n A ( a 832 L m e o ati AA rn A s : e e ss e ol tA eey id nid D)5 rr e lele f s a l u F846l -V D i y- c u ratiati ticid e rta ll S e sm ee CW t me 9045 g ee intl ee S i a o MMPSVoVo vv FW N C PPPPPP 1311/8270) hp c.t (S Pa sntLLLLLL St. sactiacti nom W a Iee CCCCCC lai H n 4223 , 4489 FP9095)pRRSVOTTTT(STT Te - s 4 ek.c e t Wi o t i e 253 s . ) Oh w 3310 , ix s w ge hnologil 330 r ( t al ec :aud //w l F: T S M FAX http ntal : e ahoga m 211 ite y ns 8 u - ob C r 3 i v We 25 AM n te ) E 00 Da it: 330 n ( 10 : mm io 9 t L: Su 9 E ec 1 T 0 oll 2 C 9/11/ ID e l p am ro h m r am g a u ah S r D n u y nt th r SD lie No C 1A 0 0 - t: ID c t: le e n p oj m r a 19090846 ClieP S SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 19090846 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 10/1/2019 TagNumber: CLIENT:Synagro CollectionDate:9/11/20199:10:00AM Matrix:SLUDGE LabID:19090846-001A Project:Durham ClientSampleIDNorthDurham AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW7470ASW7470AMJM TCLPMERCURYANALYSIS(SW1311/7470) TCLPMercuryND0.00500mg/L19/17/20194:32:00PM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW6010DSW3010AEAM TCLPMETALSANALYSIS(SW1311/6010) TCLP Arsenic(As)ND1.25mg/L19/17/20193:56:11PM TCLP Barium(Ba)ND12.5mg/L19/17/20193:56:11PM TCLPCadmium(Cd)ND0.250mg/L19/17/20193:56:11PM TCLPChromium(Cr)ND0.500mg/L19/17/20193:56:11PM TCLPLead(Pb)ND1.25mg/L19/17/20193:56:11PM TCLP Selenium(Se)ND0.125mg/L19/17/20193:56:11PM TCLP Silver(Ag)ND1.25mg/L19/17/20193:56:11PM Analyst: FLASHPOINT DETERMINATION (1010)SW1010TAH Flashpoint(140°F)>140°F19/27/201910:35:45 AM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8270SW3510CSFG TCLP SEMI-VOLATILESANALYSIS (SW1311/8270) 1,4-DichlorobenzeneND0.200mg/L29/18/20195:00:00AM 2,4,5-TrichlorophenolND0.500mg/L29/18/20195:00:00AM 2,4,6-TrichlorophenolND0.500mg/L29/18/20195:00:00AM 2,4-DinitrotolueneND0.100mg/L29/18/20195:00:00AM Cresols,TotalND10.0mg/L29/18/20195:00:00AM Hexachloro-1,3-butadieneND0.0400mg/L29/18/20195:00:00AM HexachlorobenzeneND0.100mg/L29/18/20195:00:00AM HexachloroethaneND0.200mg/L29/18/20195:00:00AM NitrobenzeneND0.200mg/L29/18/20195:00:00AM PentachlorophenolND0.500mg/L29/18/20195:00:00AM PyridineND0.500mg/L29/18/20195:00:00AM Surr:2-Fluorophenol14.210-109%Rec29/18/20195:00:00AM Surr: Phenol-d617.310-109%Rec29/18/20195:00:00AM Surr:Nitrobenzene-d57.1019-120S%Rec29/18/20195:00:00AM BAnalytedetected in the associatedMethod BlankEValueabovequantitationrange Qualifiers: HHoldingtimesforpreparationor analysisexceededMManualIntegrationused todetermine arearesponse MCValueisbelowMinimum CompoundLimit.NTentativelyidentified compounds NDNotDetectedPSecond column confirmationexceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal < MDL Page6of39 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 19090846 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 10/1/2019 TagNumber: CLIENT:Synagro CollectionDate:9/11/20199:10:00AM Matrix:SLUDGE LabID:19090846-001A Project:Durham ClientSampleIDNorthDurham AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8270SW3510CSFG TCLP SEMI-VOLATILESANALYSIS (SW1311/8270) Surr:2,4,6-Tribromophenol24.010-120%Rec29/18/20195:00:00AM Surr:2-Fluorobiphenyl9.9022-117S%Rec29/18/20195:00:00AM Surr:p-Terphenyl-d1419.234-116S%Rec29/18/20195:00:00AM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8081SW3510CRIS TCLP PESTICIDESANALYSIS (SW1311/8081) Chlordane, totalND0.0250mg/L109/25/20191:03:00PM ToxapheneND0.500mg/L109/25/20191:03:00PM EndrinND0.00200QC+mg/L109/25/20191:03:00PM gamma-BHCND0.00200mg/L109/25/20191:03:00PM HeptachlorND0.00200QC+mg/L109/25/20191:03:00PM HeptachlorepoxideND0.00200mg/L109/25/20191:03:00PM MethoxychlorND0.00200dQC+mg/L109/25/20191:03:00PM Surr:TCMX46.410-119%Rec109/25/20191:03:00PM Surr:DCB70.410-119%Rec109/25/20191:03:00PM Analyst: TCLP HERBICIDES (SW846:1311/8321)SW8321ABJH SVOC SW-846:8321HERBICIDES-TCLP 2,4-DND0.0100mg/L19/25/201911:12:00 AM 2,4,5-TPND0.0100mg/L19/25/201911:12:00 AM Surr:2,4-Dichlorophenylaceticacid0.23070-130S%Rec19/25/201911:12:00 AM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8260SW1311MRMT TCLP VOLATILESANALYSIS 1,1-DichloroetheneND0.500mg/L1009/19/20196:13:00PM 1,2-DichloroethaneND0.500mg/L1009/19/20196:13:00PM MEKND10.0mg/L1009/19/20196:13:00PM BenzeneND0.500mg/L1009/19/20196:13:00PM Carbon tetrachlorideND0.500mg/L1009/19/20196:13:00PM ChlorobenzeneND5.00mg/L1009/19/20196:13:00PM ChloroformND0.500mg/L1009/19/20196:13:00PM TetrachloroetheneND0.500mg/L1009/19/20196:13:00PM BAnalytedetected in the associatedMethod BlankEValueabovequantitationrange Qualifiers: HHoldingtimesforpreparationor analysisexceededMManualIntegrationused todetermine arearesponse MCValueisbelowMinimum CompoundLimit.NTentativelyidentified compounds NDNotDetectedPSecond column confirmationexceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal < MDL Page7of39 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 19090846 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 10/1/2019 TagNumber: CLIENT:Synagro CollectionDate:9/11/20199:10:00AM Matrix:SLUDGE LabID:19090846-001A Project:Durham ClientSampleIDNorthDurham AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8260SW1311MRMT TCLP VOLATILESANALYSIS TrichloroetheneND0.500mg/L1009/19/20196:13:00PM Vinyl chlorideND0.200mg/L1009/19/20196:13:00PM Surr:4-Bromofluorobenzene95.070-130%Rec1009/19/20196:13:00PM Surr:Dibromofluoromethane10070-130%Rec1009/19/20196:13:00PM Surr:Toluene-d897.970-130%Rec1009/19/20196:13:00PM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9014MS REACTIVE CYANIDE(9014/7.3.3.2)-SOLID Cyanide,ReactiveND0.495mg/Kg19/18/20195:17:00PM Analyst: PAINTFILTERFREELIQUIDSTEST (SW-846:9095)SW9095DHC FreeLiquidpass19/27/20195:25:00PM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9045DDHC PH (SW9045D) pH7.9s.u.@20.0C19/26/201910:49:00 AM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9034MS REACTIVE SULFIDE(9034)/7.3.4.2 Sulfide,ReactiveND25.0mg/Kg19/18/20195:17:00PM BAnalytedetected in the associatedMethod BlankEValueabovequantitationrange Qualifiers: HHoldingtimesforpreparationor analysisexceededMManualIntegrationused todetermine arearesponse MCValueisbelowMinimum CompoundLimit.NTentativelyidentified compounds NDNotDetectedPSecond column confirmationexceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal < MDL Page8of39 SummitEnvironmentalTechnologies,Inc. AccreditationProgram 3310 WinSt. AnalytesReport CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 19090846 Website:http://www.settek.com 01-Oct-19 Client:SynagroState:NW Project:DurhamProgramName:NC_WW_SCM SampleIDMatrixTestNameAnalyteStatus SludgeFlashpointDetermination(1010)Flashpoint(140°F)A 19090846-001A SludgePaintFilterFreeLiquidsTest(SW-846:9095)FreeLiquidA SludgepH(SW9045D)HydrogenIon(pH)A SludgeReactive Cyanide(9014/7.3.3.2)-SolidCyanide, ReactiveU SludgeReactiveSulfide(9034)/7.3.4.2Sulfide, ReactiveU SludgeSVOCSW-846:8321Herbicides-TCLP2,4,5-TPN SludgeSVOCSW-846:8321Herbicides-TCLP2,4-DN SludgeTCLPMercuryAnalysis(SW1311/7470)MercuryA SludgeTCLPMetalsAnalysis(SW1311/6010)ArsenicA SludgeTCLPMetalsAnalysis(SW1311/6010)BariumA SludgeTCLPMetalsAnalysis(SW1311/6010)CadmiumA SludgeTCLPMetalsAnalysis(SW1311/6010)ChromiumA SludgeTCLPMetalsAnalysis(SW1311/6010)LeadA SludgeTCLPMetalsAnalysis(SW1311/6010)SeleniumA SludgeTCLPMetalsAnalysis(SW1311/6010)SilverA SludgeTCLPPesticidesAnalysis(SW1311/8081)Chlordane, totalA SludgeTCLPPesticidesAnalysis(SW1311/8081)EndrinA SludgeTCLPPesticidesAnalysis(SW1311/8081)gamma-BHCA SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorA SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorepoxideA SludgeTCLPPesticidesAnalysis(SW1311/8081)MethoxychlorA SludgeTCLPPesticidesAnalysis(SW1311/8081)ToxapheneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)1,4-DichlorobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,5-TrichlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,6-TrichlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4-DinitrotolueneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)Cresols,TotalA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobutadieneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachloroethaneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)NitrobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PentachlorophenolA KeyKeyKey NC_WW_SCMAAccreditedNC_WW_SCMNNotAccreditedNC_WW_SCMUUnavailable Original#1 Page9of39 SummitEnvironmentalTechnologies,Inc. AccreditationProgram 3310 WinSt. AnalytesReport CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 19090846 Website:http://www.settek.com 01-Oct-19 Client:SynagroState:NW Project:DurhamProgramName:NC_WW_SCM SampleIDMatrixTestNameAnalyteStatus SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PyridineA 19090846-001A SludgeTCLPVolatilesAnalysis1,1-DichloroetheneA SludgeTCLPVolatilesAnalysis1,2-DichloroethaneA SludgeTCLPVolatilesAnalysis2-ButanoneA SludgeTCLPVolatilesAnalysisBenzeneA SludgeTCLPVolatilesAnalysisCarbon tetrachlorideA SludgeTCLPVolatilesAnalysisChlorobenzeneA SludgeTCLPVolatilesAnalysisChloroformA SludgeTCLPVolatilesAnalysisTetrachloroetheneA SludgeTCLPVolatilesAnalysisTrichloroetheneA SludgeTCLPVolatilesAnalysisVinyl chlorideA KeyKeyKey NC_WW_SCMAAccreditedNC_WW_SCMNNotAccreditedNC_WW_SCMUUnavailable Original#1 Page10of39 al n i g i ual r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1032572340758 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 25 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 56 m i 130130130 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se 707070 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .8.5.6 ds EC in R ee 949695 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m at u al f n 11 n n o o s: ntit f V o t 1311M e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s 4 tin a C-M ek.c e r te nd Wi o t o O iuo e l 253.0.0.0 p c ue s V a e l . e ) - Oh a VManuaSR w 3310 P , v 8260 500500500 s w L hnologil 330 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 500 e 1. P C r 3 05000500050005000500050005000200 i T ....0.... v We 00000000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDNDNDNDNDNDNDND LK s o 474483478 m d i B l e Re y M39425 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro ene eeut e tt am z hane o g yy t D ll ah e aat r n nn PD u m y AANoR SD oroben u de uoro il l d8 f r f J nene BR - ne o o o ND ea le e B-39425 hh n BSh m m tt h ne ne t c e o o MPee r er a u de l he r i z b oeB t t: i r o r - s orooro e rm llo ID o 4DT l l t o hh D:er t: ::: h f eh i I cc l c te f t:iioroe c ene t l c p y e l urrurrurr lz n h orobenoro ray ali ll ma tc en oj i n 1-D2-D u EK li eni an er ,, r Q SCA11MBCarbonChChTTV S S S ClieP al n i g i ual r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1032782344117 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 25 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 6 m i 131137163132139139129187138147126125117 S 1 H PL / MC 9 hL g i H e: e: t t it Da Da .4.6.1.1.7.3.3.2.1.1.4.3 se 82 m935332964200 n s p i i o 775767756287 e L s r p y s w l P e a r Lo n a A e r a e .4.7.3 ds EC in 103112102107111111107110117102 R ee 809999 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 0000000000 at u al f n 12 n n o o s: ntit f V o t 1311M e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s 4 tin a C-M ek.c e r te nd Wi o t o O iuo e l 253p c ue000000 s V a e l .... e ) - 100 Oh a .VManuaSR w 3310 P 020002000200020002000200020002000200 , v 8260 ..0.......505050 s w L hnologil 330 000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b 100 e . P C r 3 0500 i T 0. v 0050000500005000050000500005000050000200 We ........ 0 25nk n a 00000000 ) l E it B 330 d ( its o mm m th L: i e l Su lt E .1.8.6 its u n T M ND s o 102 m .514949 d i 02070224021402230213021902340161 l e CS ..0...... Re y 00000000 L39425 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro ene eeut e tt am z hane o g yy t D ll ah e aat r n nn PD u m y AANoR SD oroben 03278 u de uoro 1il l d8 f r -f J nene BR - ne o o o ND ea SSS le e hh n h m CCm tt h ne ne t c e o o LLee r er a u de l he r i z b oeB t t: i r o r - s orooro e rm llo ID o 4DT l l t o hh D:er t: ::: h f eh i I cc l c te f t:iioroe c ene t l c p y e l urrurrurr lz n h orobenoro ray ali ll ma tc en oj i n 1-D2-D u EK li eni an er ,, r Q SCA11MBCarbonChChTTV S S S ClieP al n i g i S ual r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349918 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 109109120120117116 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se 101019102234 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .2.1.5.0.7.2 ds EC in R ee 384421552135 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m at u al f n 13 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 000000000000000 000 Oh a C-BN ......VManuaSR w 3310 , v 8270 111111 s O w hnologil 330 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5.... P C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDNDNDNDNDNDNDNDNDND LK s o 382441215550217352 m ......d i B l e 000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n u enolenolol e z J b pb BR ene i e bd6 z hhn ne n ND r neoo - z- h nl ppaerr B-39428e e 3 T n BS p e o oo,hoo h - b u r rrt lal MPbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i S SSSSS ualm r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349919 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 130 132133130130130130130130130130130130130130130130130 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da .4.7.1.3.9.7.4.1.5.5.1.6.8.4 se 34101043 m611321136972.16 n s p i i o 333433343313443 e L s r p y s w l P e a r Lo n a A e r a e .6.2.1.0.8.3.1.6.4.4.0.6.0.0.2.9.0.3 ds EC in R ee 326060634749315230415437434824622135 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 14 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 600000000000000000 000 Oh a C-BN .......VManuaSR w 3310 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s O w hnologil 330 00000000000 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5... P. C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M ND s o 261481481504383249420243331432301430480242629210353 m .................d i l e CS 00000000000000000 Re y L39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad 9428 o ty nephen henolene-d5ri 3 n u enolenolol e -z J b pb BR ene i e bd6 z hhn ne n ND r neoo SSS- z- h nl ppaerr e e 3 T n CCp e o oo,hoo h - b u r rrt lal LLbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i S ualm r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349926 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 126 144153155148148126134132158176130130130154130130156 S 11 H PL // MC 99 hL g i H e: e: t t it 5 Da Da .8.7.8.4.7.8.5.5.4 se 1010292010103986 m382032.494. n s p i i o 32123331138 e L s r p y s w l P e a r Lo n a A e r a e .5.2.6.6.4.1.1.4.4.2.4.6.0.8.2.4.6.8 ds EC in R ee 397373785760376835516043515728722643 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 15 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 600000000000000000 000 Oh a C-BN .......VManuaSR w 3310 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s O w hnologil 330 00000000000 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1..... P C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDND s o 316586589628297547283409510578282724266438 m ..............d i l e 00000000000000 Re y MS39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e MS t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i SS ualm r Q O 19 t- RT c it O 303030303030303030303030 O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r 00000000 p 1034232349938 e .5.6.5.0 o O 839915166141 PD ...... m Y pt 29105111061188 o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y 00 al r s w e MM e o it f V 3156586058926284459629685472283240924832 mov el .......... m c b i 0000000000 ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 126 144153155148148126134132158176130130130154130130156 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da .8.7.8.4.7.8.5.5.4 se 101029201010391086 m382032.494. n s p i i o 32123331138 e L s r p y s w l P e a r Lo n a A e r a e .4.0.8.7.6.5.4.8.7.8.7.6.9.4.1.2.4.1 ds EC in R ee 388181826467337231556542546230742844 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 16 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 600000000000000000 000 Oh a C-BN .......VManuaSR w 3310 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s O w hnologil 330 00000000000 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1.... P. C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDND s o 307648654662516267582254446526549624301742284441 m ..........d ......i SD l e 0000000000000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t SD eeid ct s dd e M t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i S ual r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349964 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 109109120120117116 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se 101019102234 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .2.1.5.0.7.2 ds EC in R ee 384421552135 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m at u al f n 17 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 000000000000000 000 Oh a ......VManuaSR w 3310 P , v 8270 111111 s w L hnologil 330 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5.... P C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDNDNDNDNDNDNDNDNDND LK s o 382441215550217352 m ......d i B l e 000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n u enolenolol e z J b pb BR ene i e bd6 z hhn ne n ND r neoo - z- h nl ppaerr B-39428e e 3 T n BS p e o oo,hoo h - b u r rrt lal MPbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i S SSSSS ualm r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349965 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 130 132133130130130130130130130130130130130130130130130 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da .4.7.1.3.9.7.4.1.5.5.1.6.8.4 se 34101043 m611321136972.16 n s p i i o 333433343313443 e L s r p y s w l P e a r Lo n a A e r a e .6.2.1.0.8.3.1.6.4.4.0.6.0.0.2.9.0.3 ds EC in R ee 326060634749315230415437434824622135 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 18 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 600000000000000000 000 Oh a .......VManuaSR w 3310 P 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s w L hnologil 330 00000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5... P. C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M ND s o 261481481504383249420243331432301430480242629210353 m .................d i l e CS 00000000000000000 Re y L39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad 9428 o ty nephen henolene-d5ri 3 n u enolenolol e -z J b pb BR ene i e bd6 z hhn ne n ND r neoo SSS- z- h nl ppaerr e e 3 T n CCp e o oo,hoo h - b u r rrt lal LLbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i S ualm r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349966 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q .2 67 m i 124 152150141132132156142131135134146130156183153154 S 11 H 64 PL // MC 99 hL g i H e: e: t t it Da Da .2.6.6.9.6.3.3.4.7.9.3.4.8 .3 se 58922177 m507674.7.03714 50 n s p i i- o 13222514921225 1 e L s - r p y s w l P e a r Lo n a A e r a e .5.2.6.6.4.1.1.4.4.2.4.6.0.8.2.4.6.8 ds EC in R ee 397373785760376835516043515728722643 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 19 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 600000000000000000 000 Oh a .......VManuaSR w 3310 P 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s w L hnologil 330 00000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1..... P C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDND s o 316586589628297547283409510578282724266438 m ..............d i l e 00000000000000 Re y MS39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e MS t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i S ualm r Q O 19 t- RT c it O 303030303030303030303030 O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r 00000000 p 1034232349967 e .5.6.5.0 o O 839915166141 PD ...... m Y pt 29105111061188 o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y 00 al r s w e MM e o it f V 3156586058926284459629685472283240924832 mov el .......... m c b i 0000000000 ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q .2 67 m i 124 152150141132132156142131135134146130156183153154 S 11 H 64 PL // MC 99 hL g i H e: e: t t it Da Da .2.6.6.9.6.3.3.4.7.9.3.4.8 .3 se 58922177 m507674.7.03714 50 n s p i i- o 13222514921225 1 e L s - r p y s w l P e a r Lo n a A e r a e .4.0.8.7.6.5.4.8.7.8.7.6.9.4.1.2.4.1 ds EC in R ee 388181826467337231556542546230742844 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 20 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 600000000000000000 000 Oh a .......VManuaSR w 3310 P 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s w L hnologil 330 00000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1..... P C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDND s o 307648654662516267582254446526549624301742284441 m ..........d ......i SD l e 0000000000000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t SD eeid ct s dd e M t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al n i g i ualual r QQ O 19 t- RT c itit O O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10326023412421032602341243 e o O PDPD m Y pt o RR W on i t C %% a acce r m a eqNo:eqNo: u AR p 40 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alal r s w e MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 2019201920192019 itit //// Q 6666 mm ii 120 120120120120120120 S 1111 H PL //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 80808080808080 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .9 ds ECEC in 104107106109105108 RR ee 95 m c r %% x e t e ge e 39 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 0000000 at u alal f n 21 n n o o s:s: ntit f Vf V o tt 3010A3010A e ii a c cti atine g WW ReRe t r qu UnUn e m SS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a -7(6-7(6 ek.c e r te nd Wi o t PP o iuo e l 253p LL c ueue s a e ll . e ) 000000000000000 CC000000 Oh aa .......VManuaSR w 3310 , TT vv 6010D6010D 2222222 s-- w ll hnologil 330 tt ( WW al ec : //w MSMS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y 0000 ns stst T 8 T QLQL u .. - o b 500100200500500500100200500500 ee .5...5.... P..P C r 3 0500 0500 i TT 0000.00000.0 v We 0 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu 089212181116 n T M ...... NDNDNDNDNDNDNDND LK ss o m 212222 d i B l e CS ReRe y M39440L39440 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 9440 e)e) 3 Cd)(Cr)Cd)(Cr) - SS J BR s)s) (( a)(a)( ND SSS mm AA BB g)g) mm B-39440 (( mm BSuu b)b) (( CC ii uu cAcA uu ii ii MPPiLLPi (( mm mrmr nn mm uu ee oo ii: enen ee rlrl s vv ss IDID raeilraeil D:D:er t: eCadChrLead(eCadChrLead(i II ll c tete f t: tt pp yy e P AP BPPPP SP SP AP BPPPP SP S ll n ali mama enen oj u lili anan CLCLCLCLCLCLCLCLCLCLCLCLCLCL r Q SCATTTTTTTSCATTTTTTT ClieP al n i g i ualual r QQ O 19 t- RT c itit O 20202020202020 O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r 0 p 10332023468751033202346876 e o O 199695935256 PDPD ...... m Y pt 111122 o RR W on i t C %% a acce r m a eqNo:eqNo: u AR p 40 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y 0 alal r s w e MM e o 280962058048344258 it ...... f Vf V mov el 212222 m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 2019201920192019 itit //// Q 6767 mm ii 130130 130130130130130130130130130130130130 S 1111 H PL //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 7070707070707070707070707070 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .9.8.8 ds ECEC in 114103102117113115102105104120116 RR ee 989799 m c r %% x e t e ge e 39 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 0000000000 at u alal f n 22 7474 n n o 88 o s:s: .. ntit f Vf V o tt 3010A3010A e ii a 22 c cti atine g WW ReRe t 005326005326 r qu .. UnUn e m SS g e 00 e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a -7(6-7(6 ek.c e r te nd Wi o t PP o iuo e l 253p LL c ueue s a e ll . e ) 000000000000000000000000000000 C000000C000000 Oh aa ..............VManuaSR w 3310 , TT vv 6010D6010D 22222222222222 s-- w ll hnologil 330 tt ( WW al ec : //w MSMS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y 0000 ns stst T 8 T QLQL u .. - o b 500100200500500500100200500500 ee .5.....5.... PP C r 3 0500 0500 i TT 0000.00000.0 v We 0 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu 289606053426310010094032 n T M ............ NDND ss o m 212222222222 d i SD l e ReRe y MS39440M39440 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah aat r n nn PD u y AANoR SD e)e) 0818-0120818-012 hQChQC Cd)(Cr)Cd)(Cr) SS J BR s)s) (( 99 a)(a)( ND tctc mm 0A0A BB g)g) mm (( mm aa uu b)b) (( 99 ii uu cAcA uu ii ii 1BPi1BPi (( mm mrmr nn mm uu ee oo ii: enen ee rlrl s vv ss IDID raeilraeil D:D:er t: eCadChrLead(eCadChrLead(i II ll c tete f t: tt pp yy e P AP BPPPP SP SP AP BPPPP SP S ll n ali mama enen oj u lili anan CLCLCLCLCLCLCLCLCLCLCLCLCLCL r Q SCATTTTTTTSCATTTTTTT ClieP al n i g i ualualualual r QQQQ O 19 t- RT c itititit O 20 O - mmmm iiii LLLL 19090846 01 P DDDD PPPP y E ov l RRRR c a e n r R und a o #: d r p 1033592346192103359234619310335923462001033592346201 e o O 75 PDPDPDPD . m Y pt 2 o RRRR W on i t C %%%% a acce r m a eqNo:eqNo:eqNo:eqNo: u AR p 61 SSSS RunNo:RunNo:RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alalalal r s w e MM e o it f Vf Vf Vf V 0111 mov el . m c b i 0 ti e D: ReReReRe L s g I SU i R DDDD it e e din ch u PPPP m l l t r a RRRR epik C HoVPS Ba 20192019201920192019201920192019 itititit //////// Q 77777777 mmmm iiii 120125125 S 11111111 H PL //////// MC 99999999 hLhLhLhL gggg iiii HHHH e:e:e:e: e:e:e:e: tttt tttt itititit DaDaDaDa DaDaDaDa se 807575 mmmm n ssss pppp iiii iiii o eeee LLLL ssss rrrr p yyyy s wwww llll PPPP e aaaa r LoLoLoLo nnnn a AAAA e r a e ds ECECECEC in 112111108 RRRR ee m c r %%%% x e t e ge e 39 nn d a o f ri o t tit o a d m on i m ie r s L i PPMPPMPPMPPM 000 at u alalalal f n 23 n n o o s:s:s:s: ntit f Vf Vf Vf V o tttt 7470A7470A7470A7470A e iiii a c cti atine g WWWW ReReReRe t r qu UnUnUnUn e m SSSS g e e u c. 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CCCC e ) Oh aaaa VManuaSR TTTT w 3310 040001000100 , vvvv 7470A7470A7470A7470A .. ____ s w 0 hnologil 330 .00 ( GGGG WWWW 0 al ec : //w HSHSHSHS P E M F: T RL SPKSPKSPKSPK FAX http No:No:No:No: ntal : e stststst ahoga Code:Code:Code:Code: m eeee 211 ite y ns stststst T 8 TTT QLQLQLQL u - o b eeee PPPP C r 3 i TTTT v 00200002000050000500 We .... 25nk n a 0000 ) l E it B 330 d ( its o mm m th L: i e l Su ltltltlt E its uuuu n T M ND LK ssss o m d i 044601110108 BSD l e CS .. 0 ReReReRe y .00 M39461L39461MS39461M39461 itati r t 0 e ciat n v o a e:e:e:e: o D:D:D:D:s u pppp s c I I I I q yyyy e a hhhh r TTTT e pppp tctctctc d h ow e aaaa t mmmm el n BBBB pt aaaa b ie SSSS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah aat r n nn PD u y AANoR SD 9461 3 0845-0010845-001 hQChQC - J BR 99 ND SSS tctc 00 B-39461 aa BS CC 99 ryryryry MPLL1B1B uuuu cccc : rrrr s IDIDIDID eeee D:D:D:D:er t: eMeMeMeM i IIII llll c tetetete f t: tttt pppp yyyy e PPPP llll n ali mamamama enenenen oj u lililili anananan CLCLCLCL r Q SCATSCATSCATSCAT ClieP al n i g i ual r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1033592346201 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 61 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 77 m i S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e ds EC in R ee m c r % x e t e ge e 39 nn d a o f ri o t tit o a d m on i m ie r s L i PPM at u al f n 24 n n o o s: ntit f V o t 7470A e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s (74 4 tin a ek.c e r te nd Wi P o t o iuo L e l 253p c ue s a e l . C e ) Oh a VManuaSR T w 3310 , v 7470A _ s w hnologil 330 ( G W al ec : //w HS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M s o m d i SD l e Re y M39461 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t SD eeid ct s dd e M t ro eeut e A tt am o g yy D ll ah aat r n nn PD u y AANoR SD 0845-001 hQC J BR 9 ND tc 0 a 9 1B : s ID D:er t: e i I l c te f t: t p y e l n ali ma en oj u li an r Q SCA ClieP al n i g i C+C+C+C+ ualual r QQQQ QQ O 19 t- RT c itit O 3030303030 O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r 00 p 10368223767551036822376756 e .4.8.7 o O 2523 PD ..PD m Y pt 10101299 o R W R on i t C %% a acce r m a eqNo:eqNo: u AR p 80 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alal r s w e MM e o it f Vf V 011001170188 mov el ... m c 0075200965 b i 0.0.0 ti e D: ReRe L s 00 g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 20192019 itit //// Q 8585 mm ii 224224 192197208251157194192197208251157194 S 1212 H PL // // MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 1010101010101010101010101010 mm n ss p p ii ii o e e LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .0.5.0.2.2.2.5.6.9 ds ECEC in 103172110117188 RR ee 996788596975966569 m c r %% x e t e ge e 39 nn d a o f ri o t tit /L/L o a d m g on g i m ie r s L i mm 0000000000 at u alal f n 25 n n o o s:s: ntit f Vf V o tt 3510C3510C e ii a c cti atine g WW ReRe t r qu UnUn e m SS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 C-C- c l - s 4 tin a ek.c e OO r te nd Wi o t o iuo e l 253p c ue0000ue0000 s SVSV a e ll ... ..e ) -- Oh aa VManuaSR w 3310 PP 0100010001000100010001000100010001000100 , vv 80818081 ....2020....2020 .. s w LL hnologil 330 0000000000 ( WW CC al ec : //w TST S P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst 8 TT QLQL u - o b ee PP C r 3 i TT v 00500005000050000500005000050000500005000050000500 We ...... .... 25nk n a 0000000000 ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E .1.0 .8.8 its uu n T M ss o m 1314 d 1113 i 0990067501030880017201100752011709650188 SD l e ..... 00000 ReRe y ..0.00.0.0 M39480MS 39480 itati r t 00000 e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a h h r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t sd eeid ct s dd e mms t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 0844-001a 0844-001a hQChQC dede J ii BR 9 9 ND xx tctc 0 0 oo aa 99 pp 1B1B ee oror MXMX ll : HCHC hh CC s orororor llcllc BB IDID TDCBTDCB yy hhhh D:D:er t: :::: ee i Ia-Ia- xx cccc ll c tete f t: tt inaainaa pp yy e tturrurrtturrurr ll n hoho ali tt mama enen mmmm oj u ee lili ndrndr anan r Q SCAEgaHepHepM S SSCEgaHepHepM S S A ClieP al n i g C+C+ i C+C+ d ualual r QQ QQ QQ dd O 19 t- RT c itit O O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10368223767571036822376758 e o O PDPD m Y pt o RR W on i t C %% a acce r m a eqNo:eqNo: u AR p 80 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alal r s w e MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 2019201920192019 itit //// Q 8585 mm ii 130 130130130178130130119119 S 1212 H PL //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 101010101010101010 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .6.0.8.9.8.9.6.7 ds ECEC in 130 RR ee 5938574732513253 m c r %% x e t e ge e 39 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 00000 at u alal f n 26 n n o o s:s: ntit f Vf V o tt 3510C3510C e ii a c cti atine g WW ReRe t r qu UnUn e m SS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 C-C- c l - s 4 tin a ek.c e OO r te nd Wi o t o iuo e l 253p c ue0000ue0000 s SVSV a e ll ... ..e ) -- Oh aa VManuaSR w 3310 PP 01000100010001000100 , vv 80818081 ....20202020 . s w LL hnologil 330 00000 ( WW CC al ec : //w TSTS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst T 8 T QLQL u - o b ee PP C r 3 i TT v 0025000500 We .. 25nk n 000500000500 000500000500000500000500000500000500000500000500 a .....00..... ) l E 00 00000000 it B 330 d ( its o mm m th L: i e l Su ltlt E .4.7 its uu 5551 n T M .. NDNDNDNDNDNDND LK ss o m 610610 d i 05960380057804790130 B l e CS . 0000 ReRe y ....0 L39480M39480 itati r t 0000 e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD dede J ii 39480 BR 39480 - ND -xx SS bal soo BS t C cpp o lLmP t ee oror MXMX ll , : HCHC hh CC s orororor llcllc BB IDID TDCBTDCB yy hhhh D:D:er t: :::: ee i Ia-Ia- xx cccc ll c tete f t: tt inaainaa pp yy e tturrurrtturrurr ll n hoapheneho ordane ali tt l mama x enen mmmm oj u ee lili ndrndr anan o r Q SCAEgaHepHepM S SSCAChTEgaHepHepM S S ClieP al n i g i ualual r QQ O 19 t- RT c 5 itit O O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10346323517351034632351736 e o O PDPD m Y pt 275 .o RR W on i 0 t C 63 %% a acce r 4 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal r s w e MM e o 156 it . f Vf V mov el 9 m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q 88 mm ii 122122 S 11 H PL // MC 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa .6.6 se m1m1 n ss pp ii ii o 88 ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .5.7 ds ECEC in RR ee 9090 m c r %% x e t e ge e 39 nn d a o f ri o t tit KgKg //o a d m gg on i m ie r s L i mm at u alal f n 27 9292 n n o o s:s: ntit f Vf V o tt 1010 e ii a .. c cti atine 00 g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r ReaRea te nd Wi o,, t o iuo e ee l 253p c ue00ue00 s a e ll .d.d. e ) ii Oh aa VManuaSR w 3310 , nn vv 90149014 1010 s w aa hnologil 330 ( yy WW al ec : //w CSCS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst 8 TT QLQL u - o b 495481 ee . PP. C r 3 i TT 00 v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu 1618 n T M .. ss o m 99 d i SD l e ReRe y MSR103463MR103463 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah aat r n nn PD u y AANoR SD 0844-0010844-001 hQChQC J BR 9ve9ve ii ND tctc tt 00 aa cc 99 aa 1B1B ee : RR s IDID ,, D:D:er t: ee i II ll dede c tete f t: ii tt pp yy e ll n ali mama enen oj u lili anan r Q SCACyanSCACyan ClieP al n i g i ualualual r QQQ O 19 t- RT c ititit O O - mmm iii LLL 19090846 01 P DDD PPP y E ov l RRR c a e n r R und a o #: d r p 103463235172010346323517211034632351723 e o O PDPDPD m Y pt o RRR W on i t C 63 %%% a acce r 4 m a eqNo:eqNo:eqNo: u 3 AR p SSS RunNo:RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alalal r s w e MM e o it f Vf Vf V mov el m c b i ti e D: ReReRe L s g I SU i R DDD it e e din ch u PPP m l l t r a RRR epik C HoVPS Ba 201920192019 ititit /// Q 888 mmm iii 115150 S 111 H PL /// MC 999 hLhLhL ggg iii HHH e:e:e: e:e:e: ttt ttt ititit DaDaDa DaDaDa se 8550 mmm n sss ppp iii iii o eee LLL sss rrr p yyy s www lll PPP e aaa r LoLoLo nnn a AAA e r a e .9 ds ECECEC in 109 RRR ee 93 m c r %%% x e t e ge e 39 nn d a o f ri o t tit /L/L/L o a d m ggg on i m ie r s L i mmm 00 at u alalal f n 28 n n o o s:s:s: ntit f Vf Vf V o ttt e iii a c cti atine g ReReRe t r qu UnUnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r ReaReaRea te nd Wi o,,, t o iuo e eee l 253p c ueue00ue s a e lll .dd.d e ) iii Oh aaa VManuaSR w 3310 5000 , nnn vvv 901490149014 10. s w aaa hnologil 330 0 ( yyy WWW al ec : //w CSCSCS P E M F: T RL SPKSPKSPK FAX http No:No:No: ntal : e ststst ahoga Code:Code:Code: m eee 211 ite y ns ststst TT 8 T QLQLQL u - o b 485495495 eee ... PPP C r 3 i TTT 000 v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltltlt E its uuu 39 n T M . ND LK sss o 543 m 9.d i B l LC e CS 0 ReReRe y MR103463LR103463RR103463 itati r t e ciat n v o a e:e:e: o D:D:D:s u ppp s c I I I q yyy e a hhh r TTT e ppp tctctc d h ow e aaa t mmm el n BBB pt aaa b ie SSS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD hQC J BR veveve LK iii ND SW tc ttt B LCa BW ccc CSC aaa MPLLRB eee : RRR s IDIDID ,,, D:D:D:er t: eee i III lll dedede c tetete f t: iii ttt ppp yyy e lll n ali mamama enenen oj u lilili ananan r Q SCACyanSCACyanSCACyan ClieP al n i g i ualual r QQ O 19 t- RT c itit O O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10347023521491034702352150 e o O PDPD m Y pt o RR W on i t C 70 %% a acce r 4 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal r s w e MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q 88 mm ii 115 S 11 H PL // MC 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 85 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e ds ECEC in 101 RR ee m c r %% x e t e ge e 39 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 0 at u alal f n 29 n n o o s:s: ntit f Vf V o tt e ii a c cti atine g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o ReactReact iuo e,, l 253p c ueue s a ee e ll . e ) Oh dada VManuaSR w 3310 ii 4800 , vv 90349034 ff s w ll hnologil 330 ( uWuW al ec : //w SSSS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y.0.0 ns stst T 8 T QLQL u 55 - o b ee 22 PP C r 3 i TT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu n T M ND LK ss o m d i 4830 B l e CS ReRe y MR103470LR103470 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 103470 R - J BR ND SSW veve B-R103470ii BW tCCt cc MPLL : s IDID ReaRea D:D:er t: ,, ee i II ll c tete f t: tt pp yy e dede ll n ii ff ali malmal enen oj u lili uu anan r Q SCASSCAS ClieP al n i g i ualual r QQ O 19 t- RT c itit O 30 O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10347023521611034702352162 e o O 44 PDPD . m Y pt o 1 RR W on i t C 70 %% a acce r 4 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal r s 90 w e MM e o 8 it f Vf V 4 mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q 88 mm ii 120120 S 11 H PL // MC 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 8080 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e ds ECEC in 102100 RR ee m c r %% x e t e ge e 39 nn d a o f ri o t tit KgKg //o a d m gg on i m ie r s L i mm 00 at u alal f n 30 n n o o s:s: ntit f Vf V o tt e ii a c cti atine g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o ReactReact iuo e,, l 253p c ueue s a ee e ll . e ) Oh dada VManuaSR w 3310 ii 48004800 , vv 90349034 ff s w ll hnologil 330 ( uWuW al ec : //w SSSS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y.0.0 ns stst 8 TT QLQL u 55 - o b ee 22 PP C r 3 i TT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu n T M ss o m d i 4890 SD4820 l e ReRe y MSR103470MR103470 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah aat r n nn PD u y AANoR SD 0844-0010844-001 hQChQC J BR 99 ND tctc 00 veve ii aa tt 99 cc 1B1B : s IDID ReaRea D:D:er t: ,, ee i II ll c tete f t: tt pp yy e dede ll n ii ff ali malmal enen oj u lili uu anan r Q SCASSCAS ClieP al n i g i H ualual r QQ O 19 t- RT c 5 itit O O - mm ii LL 19090846 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10373223655561037322365558 e .3 o O PDPD 0 m Y pt o RR W on i t C 32 %% a acce r 7 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal .2 r s w e 6 MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q .4 66 mm ii S 22 H PL // MC 101 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa .6 se m8m n ss pp ii ii o 9 ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e ds ECEC in 100 RR ee m c r %% x 9C4C e ..t e ge e 00 39 nn d 22 a o f ri o t tit @@ o .. a d m on uu i m ie .. r s L i ss 0 at u alal f n 31 n n o o s:s: ntit f Vf V o tt e ii a c cti atine g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e(450(450 r te nd Wi o t o iuo e WW l 253.0 p c ueue s a e ll .7 e )PP Oh aa VManuaSR w 3310 , vv 9045D9045D s w_N_N hnologil 330 ( WW HH al ec : //w pSpS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst 8 TT QLQL u - o b ee PP C r 3 i TT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E .0.2 its uu n T M 76 ss o m d i l e CS ReRe y LR103732DUPR103732 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e DUP t ro eeut e A tt am o g yy D ll ah aat r n nn PD u y AANoR SD 103732 R 1702-001 hQC - J BR 9 ND SSW tc 0 a CC 9 LL1B : s IDID D:D:er t: ee i II ll c tete f t: tt pp yy e ll n ali mama enen oj u lili anan r Q SCApHSCApH ClieP al n i g i ualualual r QQQ O 19 t- RT c ititit O O - mmm iii LLL 19090846 01 P DDD PPP y E ov l RRR c a e n r R und a o #: d r p 103732236556910373223655741037322366527 e o O PDPDPD m Y pt o RRR W on i t C 32 %%% a acce r 7 m a eqNo:eqNo:eqNo: u 3 AR p SSS RunNo:RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alalal r s w e MM e o it f Vf Vf V mov el m c b i ti e D: ReReRe L s g I SU i R DDD it e e din ch u PPP m l l t r a RRR epik C HoVPS Ba 201920192019 ititit /// Q 666 mmm iii 110110110 S 222 H PL /// MC 999 hLhLhL ggg iii HHH e:e:e: e:e:e: ttt ttt ititit DaDaDa DaDaDa se 909090 mmm n sss ppp iii iii o eee LLL sss rrr p yyy s www lll PPP e aaa r LoLoLo nnn a AAA e r a e ds ECECEC in 101101101 RRR ee m c r %%% x 9C7C4C e ...t e ge e 999 39 nn d 111 a o f ri o t tit @@@ o ... a d m on uuu i m ie ... r s L i sss 000 at u alalal f n 32 n n o o s:s:s: ntit f Vf Vf V o ttt e iii a c cti atine g ReReRe t r qu UnUnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o (9045(9045(9045 iuo e l 253.0.0.0 p c LLL ueueue s a e IlIlIl .777 e ) Oh aaa VManuaSR w 3310 OOO , vvv 9045D9045D9045D s w hnologil 330 ( H_WH_WH_W al ec : //w PSPSPS P E M F: T RL SPKSPKSPK FAX http No:No:No: ntal : e ststst ahoga Code:Code:Code: m eee 211 ite y ns ststst 8 TTT QLQLQL u - o b eee PPP C r 3 i TTT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltltlt E .0.0.0 its uuu n T M 777 sss o m d i l e CSCSCS ReReRe y LR103732LR103732LR103732 itati r t e ciat n v o a e:e:e: o D:D:D:s u ppp s c I I I q yyy e a hhh r TTT e ppp tctctc d h ow e aaa t mmm el n BBB pt aaa b ie SSS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 7 7 7 KKK CCC J BR EEE ND SWSWSW CCC CHLCHLCHL : s IDIDID D:D:D:er t: eee i III lll c tetete f t: ttt ppp yyy e lll n ali mamama enenen oj u lilili ananan r Q SCApHSCApHSCApH ClieP al n i g i ual r Q O 19 t- RT c it O 10 O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1037322365571 e .4 o O PD 0 m Y pt o R W on i t C 32 % a acce r 7 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y al .6 r s w e 7 MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it 0 / Q 6 m i S 2 H PL / MC 9 hL g i H e: e: t t it 0 Da Da se m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e 0 ds EC in R ee m c r % x 8C e .t e ge e 9 39 nn d 1 a o f ri o t tit @ o . a d m on u i m ie . r s L i s 0 at u al f n 33 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) (9045D) Oh a VManuaSR w 3310 S , v 9045D s w_ hnologil 330 ( W H al ec : //w pS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E .6 its u n T M 7 s o m d i l e Re y DUPR103732 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e DUP t ro eeut e A tt am o g yy D ll ah aat r n nn PD u y AANoR SD 0844-001 hQC J BR 9 ND tc 0 a 9 1B : s ID D:er t: e i I l c te f t: t p y e l n ali ma en oj u li an r Q SCApH ClieP al n i g i SS ualualual r QQQ O 19 t- RT c ititit O O - mmm iii LLL 19090846 01 P DDD PPP y E ov l RRR c a e n r R und a o #: d r p 103755236679310375523667941037552366795 e o O PDPDPD m Y pt o RRR W on i t C 55 %%% a acce r 7 m a eqNo:eqNo:eqNo: u 3 AR p SSS RunNo:RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alalal r s w e MM e o it f Vf Vf V mov el m c b i ti e D: ReReRe L s g I SU i R DDD it e e din ch u PPP m l l t r a RRR epik C HoVPS Ba 201920192019 ititit /// Q 555 mmm iii 130141144130105106130 S 222 H PL /// MC 999 hLhLhL ggg iii HHH e:e:e: e:e:e: ttt ttt ititit DaDaDa DaDaDa .5.3 se 7070373870 mm08m n sss ppp iii iii o 66 eee LLL sss rrr p yyy s www lll PPP e aaa r LoLoLo nnn a AAA e r a e 00 .3.3.7.3.0 ds ECECEC in 144114 RRR ee 9386615747 m c r %%% x e t e ge e 39 nn d a o f ri o t tit /L/L/L o a d m ggg on i m ie r s L i mmm 000000 at u alalal f n 34 n n o o s:s:s: ntit f Vf Vf V o ttt e iii a c cti atine g ReReRe t r qu UnUnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPK b 4223 , 4489 C-C-C- c l - s 4 tin a ek.c e OOO r te nd Wi o t o iuo e l 253p c ueueue s SVSVSV a e lll . e ) --- Oh aaa VManuaSR w 3310 PPP 5000300075003000300075003000 , vvv 8321A8321A8321A .... s w LLL 000 hnologil 330 .0.00.0 ( WWW CCC 000 al ec : //w TSTSTS P E M F: T RL SPKSPKSPK FAX http No:No:No: ntal : e ststst ahoga Code:Code:Code: m eee 211 ite y ns ststst T 8 TT QLQLQL u - o b eee PPP C r 3 01000100 0100010001000100 i TTT ...... v We 00 0000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltltlt E its uuu n T M NDND LK sss o 342259185175 m ....d i 072007000430 B l e CS .0.00.0 ReReRe y 000 MR103755LR103755MSR103755 itati r t e ciat n v o a e:e:e: o D:D:D:s u ppp s c I I I q yyy e a hhh r TTT e ppp tctctc d h ow e aaa t mmm el n BBB pt aaa b ie ididid SSS dd ccc ee aaa acc ct ct ccc e ee iii ed t t ttt eeid eee ct s dd e MS ccc t ro eeut aaa e A tt lll am o g yy yyy D ll ah aat r n nn PD u y AANoR SD ophenophenophen rrr 1306-001 ooo hQC J lll BR 9 ND hhh SS tc 0 ccc a BS iii CSC 9 MBPLL1B 4-D4-D4-D : ,,, s IDIDID 222 D:D:D:er t: ::: eee i III lll TPTPTP c tetete f t: ttt ppp yyy e urrurrurr lll n 5-5-5- ,,,ali mamama enenen oj 4-D44-D44-D4 u lilili ananan ,,, ,,, r Q SCA22 SSCA22 SSCA22 S ClieP al n i g i S ual r Q O 19 t- RT c 0 it O 3030 O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r 0 p 1037552366796 e o O 7774 PD .. m Y pt 56 o R W on i t C 55 % a acce r 7 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y al r s w e MM e o it f V 1850 mov el . m c 04300 b i 0. ti e D: Re L s 0 g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 5 m i 150150130 S 2 H PL / MC 9 hL g i H e: e: t t it Da Da se 101070 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .3.3.3 ds EC in R ee 656151 m c r % x e t e ge e 39 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 00 at u al f n 35 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C- c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - Oh a VManuaSR w 3310 P 300075003000 , v 8321A .. s w L 0 hnologil 330 0.0 ( W C 0 al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 01000100 i T .. v We 00 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M s o 196188 m .d .i 0460 SD l e 0.0 Re y 0 MR103755 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie id S dd c ee a acc ct ct c e ee i ed t t t SD eeid e ct s dd e M c t ro eeut a e A tt l am o g yy y D ll ah aat r n nn PD u y AANoR SD ophen r 1306-001 o hQC J l BR 9 ND h tc 0 c a i 9 1B 4-D : , s ID 2 D:er t: : e i I l TP c te f t: t p y e urr l n 5- ,ali ma en oj 4-D4 u li an , , r Q SCA22 S ClieP al n i g i ual r Q O 19 t- RT c it O O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r p 1037962368919 e o O PD m Y pt o R W on i t C 96 % a acce r 7 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 7 m i 102 S 2 H PL / MC 9 hL g i H e: e: t t it Da Da se 98 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .2 ds EC in R ee 98 m c r % x e t e ge e 39 nn d a o f ri o t tit o a d m on i m ie r s L i °F 0 at u al f n 36 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l (10 - s 4 tin a ek.c e r S te nd Wi o t o iuo e t_l 253.4 p c ue s a e l . e )P Oh a VManuaSR w h 3310 , v 1010 135 s w hnologil 330 as ( W l al ec : //w FS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M s o 133 m d i l e CS Re y LR103796 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 103796 R - J F) BR ° ND SSS 0 CC 4 LL 1 ( : t s n ID i D:er t: e i I l c te f t: t p y e hpo l n ali s ma en oj a u li an r Q SCAFl ClieP al n i g i ual r Q O 19 t- RT c it O 20 O - m i L 19090846 01 P D P y E ov l R c a e n r R und a o #: d r 0 p 1038272370078 e o O PD m Y pt o R W on i t C 27 % a acce r 8 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y 0 al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 7 m i S 2 H PL / MC 9 hL g i H e: e: t t it Da Da se m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e ds EC in R ee m c r % x e t e ge e 39 nn d a o f ri o t tit o a d m on i m ie r s L i at u al f n 37 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223_S , 4489 c l - s 4 tin d a ek.c e i r te nd Wi o t o iuo e l 253p c qu ue s a e l i . e ) Oh a L VManuaSR w 3310 , v 9095 s w hnologil 330 ee ( W r al ec : //w FS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its ss u n T M s o m d i pa l e Re y DUPR103827 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e DUP t ro eeut e A tt am o g yy D ll ah aat r n nn PD u y AANoR SD 1577-001 hQC J BR 9 ND tc 0 a 9 1B : id s ID D:qu er t: i e i I l c te f t: L t p y e l n ali ma en oj u li an ree r Q SCAF ClieP 1 f o 1 age P 39 f o 38 e g Pa SummitEnvironmentalTechnologies,Inc. 3310 WinSt. CuyahogaFalls,Ohio44223 SampleLog-InCheckList TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com ClientName:WorkOrderNumber:RcptNo: SYN-NC-27028190908461 Loggedby:9/12/201910:10:00AM JohnA.Semenik Completed By:9/12/20199:54:33 PM JacquelineRasile Reviewed By:9/13/201910:31:04AM JenniferWoolf ChainofCustody IsChainofCustodycomplete?YesNoNotPresent 1. Howwas the sampledelivered? UPS 2. Log In Coolersarepresent?YesNoNA 3. Shippingcontainer/cooleringood condition?YesNo 4. Custodysealsintacton shipping container/cooler?YesNoNotPresent No.Seal Date:SignedBy: Wasanattemptmade to cool the samples?YesNoNA 5. Wereallsamplesreceivedata temperatureof>0°C to6.0°CYesNoNA 6. Sample(s)inproper container(s)?YesNo 7. Sufficientsamplevolume forindicated test(s)?YesNo 8. Are samples(except VOAandONG)properlypreserved?YesNo 9. Waspreservativeadded tobottles?YesNoNA 10. Is theheadspacein the VOAvialsless than1/4inchor6mm?YesNoNo VOAVials 11. Wereanysample containersreceivedbroken?YesNo 12. Doespaperworkmatchbottlelabels?YesNo 13. (Notediscrepancieson chainof custody) ArematricescorrectlyidentifiedonChainofCustody?YesNo 14. Isit clearwhatanalyseswererequested?YesNo 15. Wereallholding timesable tobemet?YesNo 16. (Ifno,notify customer forauthorization.) Special Handling(if applicable) Was clientnotifiedofalldiscrepancieswiththisorder?YesNoNA 17. PersonNotified: Date ByWhom:Via:eMailPhoneFaxIn Person Regarding: ClientInstructions: Additionalremarks: 18. CoolerInformation CoolerNoTempºCConditionSealIntactSeal NoSeal DateSigned By 15.5GoodNot Present Page39of39 State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section’sNon-Discharge Permitting Unit General – This certification provides detailed information of residuals source generating facility and its residuals quality for land . Do not submit this certification for review without application, distribution, or disposal in accordance with 15A NCAC 02T .1100 a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit a separate certification for each source facility. For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source-Generating Facility Information: For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the “Map Guidance for Residuals Land Application Permits”. Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan -A detailed sampling plan for the residuals source-generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division-certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: For each source facility, attach the following: Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 1 Page 900 600 42123580 Proposed s Per Year Dry Ton b 900600 42123580 Maximum Current 10(B) 0 - 0023841 32010(A) 32 - - NCNC0047597 03 03 Permit Number D (Deleted) County DurhamDurhamDurhamDurham M (Modified) ent reatment ham WRF PlantPlant Durham WRF h Dur Facility Name R (Renewed) NortSouth Brown Water T Williams Water Treatm N (New) 16 - 06 hamhamhamham are: RSC : facility FORM City Of Durham City Of DurCity Of DurCity Of DurCity Of Dur source Facility Permit Holder a RRRR Status Code UMMARY FOR Status Code for RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: a S of 5 2 ge Pa (i.e, not applicable to new facility). distribution, land application, or disposal for permitted currently 16 - residuals 06 he amount of T b FORM: RSC State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE-GENERATING FACILITY INFORMATION (See Instruction B.): 1.FacilityName: SouthDurhamWRF 2. Facility permit holder is: Federal, State, Local Government, or Private. Facility permit issued by:Div. of Water Resources,Div. of Environmental Health, or Other (explain: ). 3. Facility contact person and title: Charles Cocker WWTP Superintendent Complete mailing address: 6605 Farrington Road City: Durham State: NC Zip: 27517- Telephone number: (919) 560-4336E-mail address: charles.cocker@durhamnc.gov 4.Facility physical address: 6605 Farrington Road City: Durham State: NC Zip: 27517- Coordinates: Latitude: 35 5417 Longitude: 78 5838 Datum: NAD 84 Level of accuracy: Second Method of measurement: Map 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water,treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes No 7.Facility permitted/design flow: 20MGD and facility average daily flow: 9.07MGD 8.Average amount of residuals being generated at this facility 2270.78dry tons per year. 9.Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 4 Million Gallon Anaerobic Digester Type and volume of residuals storage (i.e., outside of residuals treatment units): 1.75 Acre Covered Storage Pad II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6)as: Biological Non-Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-hazardous under RCRA:(Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non-municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: yes no. If yes, list the number(s): b.Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR§261.21- 261.24: yes no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental Technologies and Date of analysis: 10/01/2019 Passed corrosivity test: yes no. pH: 7.6 s.u. (2 < pH < 12.5) oo Passed ignitability test: yes no. Flashpoint: >140 F (> 140F) Passed reactivity test: yes no. HCN: ND mg/kg (<250) & HS: ND mg/kg (<500) 2 TCLP Parameter Limit Result TCLP Parameter Limit Result (mg/l) (mg/l) (mg/l) (mg/l) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 1/27/2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mg/kg) (mg/kg) (mg/kg) Arsenic 75 41 4.00 Cadmium 85 39 0.753 Copper 4,300 1,500 335 Lead 840 300 15.0 Mercury 57 17 0.355 Molybdenum 75 n/a 15.9 Nickel 420 420 16.0 Selenium 100 100 4.61 Zinc 7,500 2,800 2690 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Arsenic Chromium Nickel Unit to Boundary to Closest Property Line (meters, check one) (mg/kg) (mg/kg) (mg/kg) > 0 but < 25 30 200 210 34 220 240 50 but < 75 39 260 270 46 300 320 53 360 390 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 16.6 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 1/27/2020 Parameter Result (mg/kg) Aluminum 26,500 Ammonia-Nitrogen7,950 Calcium 18,100 Magnesium 5,660 Nitrate-Nitrite Nitrogen295 pH (Standard Unit) 7.3 Phosphorus 34,800 Potassium 3,190 Sodium 813 Total Kjeldahl Nitrogen 63,900 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): .55 \[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth\]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This rate is a (check one): default value, or actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: st ) Year PAN Application Method First (1Five-Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 15,460 24,070 Injection/Incorporation 19,435 28,045 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp.density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non-biological residuals): Alternative 1 \[15A NCAC 02T.1106(b)(3)(A)\] - Time/Temperature Compliance. Alternative 2 \[15A NCAC 02T.1106(b)(3)(B)\] - Alkaline Treatment. Alternative 3 \[15A NCAC 02T.1106(b)(3)(C)\]-Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 \[15A NCAC 02T.1106(b)(3)(D)\] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 \[15A NCAC 02T.1106(b)(3)(E)-(K)\] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, gamma ray irradiation, or pasteurization. b. For Land Application of Class B: Alternative 1 \[15A NCAC 02T.1106(c)(1)\] - Fecal Coliform Density Demonstration. Alternative 2 \[15A NCAC 02T.1106(c)(2)\] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, air drying, anaerobic digestion, composting, or lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt - If Daily Cover Alternative is chosen in Item II.8. below \[15A NCAC 02T.1106(a)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 \[15A NCAC 02T.1107(a)(1)\] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 \[15A NCAC 02T.1107(a)(2)\] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 \[15A NCAC 02T.1107(a)(3)\] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 \[15A NCAC 02T.1107(a)(4)\] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 \[15A NCAC 02T.1107(a)(5)\] - 14-Day Aerobic Processes. Alternative 6 \[15A NCAC 02T.1107(a)(6)\] - Alkaline Stabilization. Alternative 7 \[15A NCAC 02T.1107(a)(7)\] - Drying of Stabilized Residuals. Alternative 8 \[15A NCAC 02T.1107(a)(8)\] - Drying of Unstabilized Residuals. Alternative 9 \[15A NCAC 02T.1107(a)(9)\] - Injection. Alternative 10 \[15A NCAC 02T.1107(a)(10)\] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover \[15A NCAC 02T.1107(b)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Residuals Sampling Plan City of Durham Land Application Program South Durham WRF Nutrients and Metals Analysis Sampling Point:Dewatered Residuals Storage Shed Sampling Frequency: 6/yr Sample Type: Composite Lab: Waypoint Analytical Pathogen Reduction (Fecal Coliform Density Demonstration) Sampling Point: Dewatered Residuals Storage Shed Sampling Frequency: 6/yr Sample Type: Grab – Fecal Coliform tests Lab: In house Vector Attraction Reduction (38% Volatile SolidsReduction) Sampling Point: Digester Influent & Effluent & Dewatered Residuals Storage Sampling Frequency: 6/yr Sample Type: Composite Lab: In house TCLP Sampling Point: Dewatered Residuals Storage Shed Sampling Frequency: Annually Sample Type: Composite Lab: Summit Environmental Technologies, Inc 203803131! Tzobhsp!Dfousbm!MMD0!Evsibn! Nbsz!Csfxfs! 395!Cphfs!Spbe! Npdltwjmmf-!OD-!38139! Sfg;!Bobmzujdbm!Uftujoh! Sfqpsu!Ovncfs;!31.128.111:! Qspkfdu!Eftdsjqujpo;!Evsibn!Tpvui! Efbs!Nbsz!Csfxfs;! 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ZftOp Tbnqmft!xfsf!dpotjefsfe!bddfqubcmf!bt!dppmjoh! qspdftt!ibe!cfhvo/ ZftOpO0B Xbufs!.!Tbnqmf!dpoubjofst!qspqfsmz!qsftfswfe OpO0B Xbufs!.!WPB!wjbmt!gsff!pg!ifbetqbdfZft ZftOpO0B Usjq!Cmbolt!sfdfjwfe!xjui!WPBt ZftOpO0B Tpjm!WPB!nfuipe!6146!€!dpnqmjbodf!dsjufsjb!nfu Ijhi!dpodfousbujpo!dpoubjofs!)59!is*Mpx!dpodfousbujpo!FoDpsf!tbnqmfst!)59!is* Ijhi!dpodfousbujpo!qsf.xfjhife!)nfuibopm!.25!e*Mpx!dpod!qsf.xfjhife!wjbmt!)Tpe!Cjt!.25!e* Tqfdjbm!qsfdbvujpot!ps!jotusvdujpot!jodmvefe@ZftOp Dpnnfout; Tjhobuvsf;Csboej!XbutpoEbuf!'!Ujnf;1202803131!22;45;56 Qbhf!6!pg!7 Qbhf!7!pg!7 SummitEnvironmentalTechnologies,Inc. 3310 WinSt. CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com October 01, 2019 RyanCopeland Synagro 284BogerRd. Mocksville,NC27028 TEL:(336) 998-7150 FAX: (336) 998-8450 RE: Durham OrderNo.:19090844 DearRyanCopeland: Summit Environmental Technologies,Inc.received 1 sample(s) on 9/12/2019forthe analyses presentedinthefollowingreport. Therewere no problemswiththeanalyticaleventsassociatedwiththisreport unless noted intheCaseNarrative. Qualitycontrol dataiswithinlaboratory defined ormethod specifiedacceptancelimits exceptwhere noted. Ifyou haveany questionsregardingthesetestsresults, pleasefeelfreetocallthe laboratory. Sincerely, Jennifer Woolf ProjectManager 3310 WinSt. CuyahogaFalls,Ohio 44223 Arkansas88-0735,California07256CA,Colorado,ConnecticutPH-0108,Delaware,FloridaNELACE87688,GeorgiaE87688,IdahoOH00923,Illinois 200061,IndianaC-OH-13,KansasE-10347,Kentucky(UndergroundStorageTank)3,Kentucky90146,Louisiana04061, Maryland339, Minnesota 409711,NewHampshire2996,New JerseyOH006,NewYork11777,NorthCarolina39705and631,NorthDakotaR-201,OhioDW,OhioVAP CL0052,Oklahoma9940,OregonOH200001,Pennsylvania010,RhodeIslandLA000317,SouthCarolina92016001,Texas T104704466-11-5,Utah OH009232011-1,VirginiaVELAP9456,WashingtonC891 Page1of37 Page1of38 SummitEnvironmentalTechnologies,Inc. CaseNarrative 3310 WinSt. CuyahogaFalls,Ohio44223 WO#: 19090844 TEL:(330)253-8211FAX:(330)253-4489 Date: 10/1/2019 Website:http://www.settek.com CLIENT:Synagro Project:Durham WorkOrderNarrative: 19090844: Thisreportinitsentiretyconsists ofthefollowing documents:CoverLetter,CaseNarrative, AnalyticalResults,QCSummaryReport,ApplicableAccreditationInformation,Chain-of-Custody, CoolerReceiptForm,and otherapplicableformsas necessary.All documentscontaintheSummit Environmental Technologies,Inc.,WorkOrderNumberassignedtothisreport. Summit EnvironmentalTechnologies,Inc., holdstheaccreditations/certificationslistedatthe bottom of thecoverletterthatmay ormay not pertaintothisreport.Pleaserefertothe"AccreditationProgram AnalytesReport"foraccreditedanalyteslist. Theinformationcontainedinthisanalyticalreportisthe sole property ofSummit Environmental Technologies,Inc.andthat ofthecustomer.Itcannot bereproducedinanyformwithouttheconsent of Summit EnvironmentalTechnologies,Inc. orthecustomerforwhichthisreportwasissued. Theresults containedinthisreportare onlyrepresentative ofthe samplesreceived.Conditionscan varyat different timesandat different samplingconditions.Summit Environmental Technologies,Inc.is notresponsible for use orinterpretation ofthe dataincluded herein. AllresultsforSolidSamplesarereported on an"asreceived" or"wetweight" basis unlessindicatedas "dryweight" usingthe"-dry" designation on thereporting units. Thisreportis believedtomeetall oftherequirements oftheaccreditingagency,whereapplicable.Any comments or problemswiththeanalyticaleventsassociatedwiththisreportare noted below. PrepSampleComments: 19090844-001A 475817:PrepCommentsfor MtlPrep_TCLP(3010A),Sample 19090844-001A: Samplewasfilteredafter digestion. AnalyticalSequenceSampleNotes: 19090844-001ATCLP-SVOC_8270E:Surrogateoutsiderecoverylimits.Minimummethodcriterion of one surrogatewithinestablishedrecoverylimitswasmet. 19090844-001a TCLP-SVOC-CPest(8081B):CCVexhibited high biasedrecoveriesfor several analytes;associatedsampleresultsareN.D. 19090844-001ATCLP-SVOC-Herb_TCLP(8321):Sampleexhibited outlyingrecovery ofSurrogate: DCAA. Original Page2of37 Page2of38 SummitEnvironmentalTechnologies,Inc. QualifiersandAcronyms 3310 WinSt. CuyahogaFalls,Ohio44223 WO#: 19090844 TEL:(330)253-8211FAX:(330)253-4489 Date: 10/1/2019 Website:http://www.settek.com ThesecommonlyusedQualifiersandAcronymsmayormaynotbepresentinthis report. Qualifiers Thecompoundwasanalyzedforbutwasnotdetected. U ThereportedvalueisgreaterthantheMethodDetectionLimitbutlessthantheReportingLimit. J HTheholdtimeforsamplepreparationand/oranalysiswasexceeded. Theresultisreportedfromadilution. D Theresultexceededthelinearrangeofthecalibrationorisestimatedduetointerference. E Theresultisbelowthe MinimumCompound Limit. MC *TheresultexceedstheRegulatoryLimitorMaximumContaminationLimit. Manualintegrationwasusedtodeterminethearearesponse. m Manualintegrationinwhichpeakwasdeleted d TheresultispresumptivebasedonaMassSpectrallibrarysearchassuminga1:1response. N PThesecondcolumnconfirmationexceeded25%difference. TheresulthasbeenconfirmedbyGC/MS. C TheresultwasnotconfirmedwhenGC/MSAnalysiswasperformed. X Theanalytewasdetectedintheassociatedblank. B/MB+ GTheICBorCCBcontainedreportableamountsofanalyte. TheCCVrecoveryfailedlow(-)orhigh(+). QC-/+ TheRPDwasoutsideofacceptedrecoverylimits. R/QDR TheLCSorLCSDrecoveryfailedlow(-)orhigh(+). QL-/+ QLRTheLCS/LCSDRPDwasoutsideofacceptedrecoverylimits. TheMSorMSDrecoveryfailedlow(-)orhigh(+). QM-/+ TheMS/MSDRPDwasoutsideofacceptedrecoverylimits. QMR TheICVrecoveryfailedlow(-)orhigh(+). QV-/+ SThespikeresultwasoutsideofacceptedrecoverylimits. Deviation;Adeviationfromthemethodwasperformed; PleaserefertotheCaseNarrativefor Z additionalinformation Acronyms NDNotDetectedRLReportingLimit QualityControlMethodDetectionLimit QCMDL MBMethodBlankLODLevelofDetection LaboratoryControl SampleLevelofQuantitation LCSLOQ LaboratoryControl SampleDuplicatePracticalQuantitationLimit LCSDPQL QualityControl SampleContractRequiredQuantitationLimit QCSCRQL DUPDuplicatePLPermitLimit Matrix SpikeRegulatoryLimit MSRegLvl Matrix SpikeDuplicateMaximumContaminationLimit MSDMCL RelativePercentDifferentMinimumCompoundLimit RPDMinCL InitialCalibrationVerificationReanalysis ICVRA ICBInitialCalibrationBlankREReextraction ContinuingCalibrationVerificationTentativelyIdentifiedCompound CCVTIC CCBContinuingCalibrationBlankRTRetentionTime ReportingLimitCheckCalibration Factor RLCCF DilutionFactorResponseFactor DFRF Thislist of QualifiersandAcronymsreflects themostcommonlyutilizedQualifiersandAcronyms forreporting. Pleaserefer to theAnalyticalNotesin theCaseNarrativeforanyQualifiersorAcronyms thatdonotappearin this list or foradditionalinformationregarding theuseof theseQualifiersonreporteddata. Original Page3of37 Page3of38 SummitEnvironmentalTechnologies,Inc. Workorder 3310 WinSt. SampleSummary CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 19090844 Website:http://www.settek.com 01-Oct-19 CLIENT:Synagro Project:Durham TagNo Lab SampleIDClient SampleIDDateCollectedDateReceivedMatrix 19090844-001SouthDurham9/11/20199:40:00AM9/12/201910:10:00AMSludge Page4of37 Page4of38 te l a PMPMPMPMPM AMAMAM AMAM a 37 D n 19 i s -0000004200 4500000000 i :::::of t ::::: g s RT i c r5 1717224737 90844 3546122555 ::::: ::::: 0 aly -O 55433 e O O 93 g 101011 19 01 An a P 999 P 111 20192019201920192019 00020192019 ///// E // 222 88776 58 11111 21 ///// // R 99999 #:99 9/27/9/26/9/25/ O S W A A PMAMPM 0041 TE :: 000000 ::: 0330 :: 450200 ::: 1111195 DA te a 20192019201920192019 D ///// 76865 p 11111 ///// re 9M99M99 P PMPMPMPM 0000 0000 :::: 00000000 te :::: a 5555 D 9999 e 1111 t 0000 a 2222 h c a 9/15/9/15/9/15/9/15/ Le LP id C ol T - s )-S e 1311/8081) 2 11/6010) d . s .21311/7470) i 3i 3W 4 010) c s . 1 . i S W 1 y 3 ( 3 bl ( . S . r a ( s 7 7 e n i / /n s (SW s is o ) 4 i H As y 4s s l iy 1 y 38 s a s l al 901 n y ale inati f ( l 903n n A ( a 832 m e o ati A rn A s : e e s e ol tA y id nid D)5 r e le f s a l u 846l -V D i y- c u ati ticid e rta l S sm ee CW me 9045 g ee int ee S a o MMPSVo vv W N C PPPPP 1311/8270) hp c.t (S Pa sLLLLL St. sactiacti nom W a Iee CCCCC l H n 4223 , 4489 FpRRSVOTTTT(ST Te - s 4 ek.c e t Wi o t i e 253 s . ) Oh w 3310 , ix s w ge hnologil 330 r ( t al ec :aud //w l F: T S M FAX http ntal : e ahoga m 211 ite y ns 8 u - ob C r 3 i v We 25 AM n te ) E 00 Da it: 330 n ( 40 : mm io 9 t L: Su 9 E ec 1 T 0 oll 2 C 9/11/ ID e l p am ro h m r am g a u ah S r D n u y nt SD uth lie o S C 1A 0 0 - t: ID c t: le e n p oj m r a 19090844 ClieP S SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 19090844 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 10/1/2019 TagNumber: CLIENT:Synagro CollectionDate:9/11/20199:40:00AM Matrix:SLUDGE LabID:19090844-001A Project:Durham ClientSampleIDSouthDurham AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW7470ASW7470AMJM TCLPMERCURYANALYSIS(SW1311/7470) TCLPMercuryND0.00500mg/L19/17/20194:22:00PM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW6010DSW3010AEAM TCLPMETALSANALYSIS(SW1311/6010) TCLP Arsenic(As)ND1.25mg/L19/17/20193:47:42PM TCLP Barium(Ba)ND12.5mg/L19/17/20193:47:42PM TCLPCadmium(Cd)ND0.250mg/L19/17/20193:47:42PM TCLPChromium(Cr)ND0.500mg/L19/17/20193:47:42PM TCLPLead(Pb)ND1.25mg/L19/17/20193:47:42PM TCLP Selenium(Se)ND0.125mg/L19/17/20193:47:42PM TCLP Silver(Ag)ND1.25mg/L19/17/20193:47:42PM Analyst: FLASHPOINT DETERMINATION (1010)SW1010TAH Flashpoint(140°F)>140°F19/27/201910:35:45 AM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8270SW3510CSFG TCLP SEMI-VOLATILESANALYSIS (SW1311/8270) 1,4-DichlorobenzeneND0.200mg/L29/18/20193:55:00AM 2,4,5-TrichlorophenolND0.500mg/L29/18/20193:55:00AM 2,4,6-TrichlorophenolND0.500mg/L29/18/20193:55:00AM 2,4-DinitrotolueneND0.100mg/L29/18/20193:55:00AM Cresols,TotalND10.0mg/L29/18/20193:55:00AM Hexachloro-1,3-butadieneND0.0400mg/L29/18/20193:55:00AM HexachlorobenzeneND0.100mg/L29/18/20193:55:00AM HexachloroethaneND0.200mg/L29/18/20193:55:00AM NitrobenzeneND0.200mg/L29/18/20193:55:00AM PentachlorophenolND0.500mg/L29/18/20193:55:00AM PyridineND0.500mg/L29/18/20193:55:00AM Surr:2-Fluorophenol15.010-109%Rec29/18/20193:55:00AM Surr: Phenol-d620.610-109%Rec29/18/20193:55:00AM Surr:Nitrobenzene-d59.9419-120S%Rec29/18/20193:55:00AM BAnalytedetected in the associatedMethod BlankEValueabovequantitationrange Qualifiers: HHoldingtimesforpreparationor analysisexceededMManualIntegrationused todetermine arearesponse MCValueisbelowMinimum CompoundLimit.NTentativelyidentified compounds NDNotDetectedPSecond column confirmationexceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal < MDL Page6of38 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 19090844 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 10/1/2019 TagNumber: CLIENT:Synagro CollectionDate:9/11/20199:40:00AM Matrix:SLUDGE LabID:19090844-001A Project:Durham ClientSampleIDSouthDurham AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8270SW3510CSFG TCLP SEMI-VOLATILESANALYSIS (SW1311/8270) Surr:2,4,6-Tribromophenol24.110-120%Rec29/18/20193:55:00AM Surr:2-Fluorobiphenyl11.022-117S%Rec29/18/20193:55:00AM Surr:p-Terphenyl-d1414.134-116S%Rec29/18/20193:55:00AM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8081SW3510CRIS TCLP PESTICIDESANALYSIS (SW1311/8081) Chlordane, totalND0.0250mg/L109/25/20199:25:00AM ToxapheneND0.500mg/L109/25/20199:25:00AM EndrinND0.00200mg/L109/25/20199:25:00AM gamma-BHCND0.00200mg/L109/25/20199:25:00AM HeptachlorND0.00200QC+mg/L109/25/20199:25:00AM HeptachlorepoxideND0.00200mg/L109/25/20199:25:00AM MethoxychlorND0.00200dQC+mg/L109/25/20199:25:00AM Surr:TCMX63.610-119%Rec109/25/20199:25:00AM Surr:DCB73.910-119%Rec109/25/20199:25:00AM Analyst: TCLP HERBICIDES (SW846:1311/8321)SW8321ABJH SVOC SW-846:8321HERBICIDES-TCLP 2,4-DND0.0100mg/L19/25/201911:12:00 AM 2,4,5-TPND0.0100mg/L19/25/201911:12:00 AM Surr:2,4-Dichlorophenylaceticacid0.22070-130S%Rec19/25/201911:12:00 AM Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8260SW1311MRMT TCLP VOLATILESANALYSIS 1,1-DichloroetheneND0.250mg/L509/16/20193:37:00PM 1,2-DichloroethaneND0.250mg/L509/16/20193:37:00PM MEKND5.00mg/L509/16/20193:37:00PM BenzeneND0.250mg/L509/16/20193:37:00PM Carbon tetrachlorideND0.250mg/L509/16/20193:37:00PM ChlorobenzeneND2.50mg/L509/16/20193:37:00PM ChloroformND0.250mg/L509/16/20193:37:00PM TetrachloroetheneND0.250mg/L509/16/20193:37:00PM BAnalytedetected in the associatedMethod BlankEValueabovequantitationrange Qualifiers: HHoldingtimesforpreparationor analysisexceededMManualIntegrationused todetermine arearesponse MCValueisbelowMinimum CompoundLimit.NTentativelyidentified compounds NDNotDetectedPSecond column confirmationexceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal < MDL Page7of38 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 19090844 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 10/1/2019 TagNumber: CLIENT:Synagro CollectionDate:9/11/20199:40:00AM Matrix:SLUDGE LabID:19090844-001A Project:Durham ClientSampleIDSouthDurham AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC,BNA,PEST, HERB-SOLIDSW8260SW1311MRMT TCLP VOLATILESANALYSIS TrichloroetheneND0.250mg/L509/16/20193:37:00PM Vinyl chlorideND0.100mg/L509/16/20193:37:00PM Surr:4-Bromofluorobenzene98.270-130%Rec509/16/20193:37:00PM Surr:Dibromofluoromethane98.770-130%Rec509/16/20193:37:00PM Surr:Toluene-d898.270-130%Rec509/16/20193:37:00PM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9014MS REACTIVE CYANIDE(9014/7.3.3.2)-SOLID Cyanide,ReactiveND0.500mg/Kg19/18/20195:17:00PM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9045DDHC PH (SW9045D) pH7.6s.u.@19.8C19/26/201910:46:00 AM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9034MS REACTIVE SULFIDE(9034)/7.3.4.2 Sulfide,ReactiveND25.0mg/Kg19/18/20195:17:00PM BAnalytedetected in the associatedMethod BlankEValueabovequantitationrange Qualifiers: HHoldingtimesforpreparationor analysisexceededMManualIntegrationused todetermine arearesponse MCValueisbelowMinimum CompoundLimit.NTentativelyidentified compounds NDNotDetectedPSecond column confirmationexceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal < MDL Page8of38 SummitEnvironmentalTechnologies,Inc. AccreditationProgram 3310 WinSt. AnalytesReport CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 19090844 Website:http://www.settek.com 01-Oct-19 Client:SynagroState:NW Project:DurhamProgramName:NC_WW_SCM SampleIDMatrixTestNameAnalyteStatus SludgeFlashpointDetermination(1010)Flashpoint(140°F)A 19090844-001A SludgepH(SW9045D)HydrogenIon(pH)A SludgeReactive Cyanide(9014/7.3.3.2)-SolidCyanide, ReactiveU SludgeReactiveSulfide(9034)/7.3.4.2Sulfide, ReactiveU SludgeSVOCSW-846:8321Herbicides-TCLP2,4,5-TPN SludgeSVOCSW-846:8321Herbicides-TCLP2,4-DN SludgeTCLPMercuryAnalysis(SW1311/7470)MercuryA SludgeTCLPMetalsAnalysis(SW1311/6010)ArsenicA SludgeTCLPMetalsAnalysis(SW1311/6010)BariumA SludgeTCLPMetalsAnalysis(SW1311/6010)CadmiumA SludgeTCLPMetalsAnalysis(SW1311/6010)ChromiumA SludgeTCLPMetalsAnalysis(SW1311/6010)LeadA SludgeTCLPMetalsAnalysis(SW1311/6010)SeleniumA SludgeTCLPMetalsAnalysis(SW1311/6010)SilverA SludgeTCLPPesticidesAnalysis(SW1311/8081)Chlordane, totalA SludgeTCLPPesticidesAnalysis(SW1311/8081)EndrinA SludgeTCLPPesticidesAnalysis(SW1311/8081)gamma-BHCA SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorA SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorepoxideA SludgeTCLPPesticidesAnalysis(SW1311/8081)MethoxychlorA SludgeTCLPPesticidesAnalysis(SW1311/8081)ToxapheneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)1,4-DichlorobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,5-TrichlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,6-TrichlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4-DinitrotolueneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)Cresols,TotalA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobutadieneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachloroethaneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)NitrobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PentachlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PyridineA KeyKeyKey NC_WW_SCMAAccreditedNC_WW_SCMNNotAccreditedNC_WW_SCMUUnavailable Page1of 2 Original#1 Page9of38 SummitEnvironmentalTechnologies,Inc. AccreditationProgram 3310 WinSt. AnalytesReport CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 19090844 Website:http://www.settek.com 01-Oct-19 Client:SynagroState:NW Project:DurhamProgramName:NC_WW_SCM SampleIDMatrixTestNameAnalyteStatus SludgeTCLPVolatilesAnalysis1,1-DichloroetheneA 19090844-001A SludgeTCLPVolatilesAnalysis1,2-DichloroethaneA SludgeTCLPVolatilesAnalysis2-ButanoneA SludgeTCLPVolatilesAnalysisBenzeneA SludgeTCLPVolatilesAnalysisCarbon tetrachlorideA SludgeTCLPVolatilesAnalysisChlorobenzeneA SludgeTCLPVolatilesAnalysisChloroformA SludgeTCLPVolatilesAnalysisTetrachloroetheneA SludgeTCLPVolatilesAnalysisTrichloroetheneA SludgeTCLPVolatilesAnalysisVinyl chlorideA KeyKeyKey NC_WW_SCMAAccreditedNC_WW_SCMNNotAccreditedNC_WW_SCMUUnavailable Page2of 2 Original#1 Page10of38 al 37 n f i o g i ual r 1 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1032572340758 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 25 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 56 m i 130130130 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se 707070 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .8.5.6 ds EC in R ee 949695 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m at u al f n 11 n n o o s: ntit f V o t 1311M e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s 4 tin a C-M ek.c e r te nd Wi o t o O iuo e l 253.0.0.0 p c ue s V a e l . e ) - Oh a VManuaSR w 3310 P , v 8260 500500500 s w L hnologil 330 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 500 e 1. P C r 3 05000500050005000500050005000200 i T ....0.... v We 00000000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDNDNDNDNDNDNDND LK s o 474483478 m d i B l e Re y M39425 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro ene eeut e tt am z hane o g yy t D ll ah e aat r n nn PD u m y AANoR SD oroben u de uoro il l d8 f r f J nene BR - ne o o o ND ea le e B-39425 hh n BSh m m tt h ne ne t c e o o MPee r er a u de l he r i z b oeB t t: i r o r - s orooro e rm llo ID o 4DT l l t o hh D:er t: ::: h f eh i I cc l c te f t:iioroe c ene t l c p y e l urrurrurr lz n h orobenoro ray ali ll ma tc en oj i n 1-D2-D u EK li eni an er ,, r Q SCA11MBCarbonChChTTV S S S ClieP al 37 n f i o g i ual r 2 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1032782344117 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 25 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 6 m i 131137163132139139129187138147126125117 S 1 H PL / MC 9 hL g i H e: e: t t it Da Da .4.6.1.1.7.3.3.2.1.1.4.3 se 82 m935332964200 n s p i i o 775767756287 e L s r p y s w l P e a r Lo n a A e r a e .4.7.3 ds EC in 103112102107111111107110117102 R ee 809999 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 0000000000 at u al f n 12 n n o o s: ntit f V o t 1311M e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s 4 tin a C-M ek.c e r te nd Wi o t o O iuo e l 253p c ue000000 s V a e l .... e ) - 100 Oh a .VManuaSR w 3310 P 020002000200020002000200020002000200 , v 8260 ..0.......505050 s w L hnologil 330 000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b 100 e . P C r 3 0500 i T 0. v 0050000500005000050000500005000050000200 We ........ 0 25nk n a 00000000 ) l E it B 330 d ( its o mm m th L: i e l Su lt E .1.8.6 its u n T M ND s o 102 m .514949 d i 02070224021402230213021902340161 l e CS ..0...... Re y 00000000 L39425 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro ene eeut e tt am z hane o g yy t D ll ah e aat r n nn PD u m y AANoR SD oroben 03278 u de uoro 1il l d8 f r -f J nene BR - ne o o o ND ea SSS le e hh n h m CCm tt h ne ne t c e o o LLee r er a u de l he r i z b oeB t t: i r o r - s orooro e rm llo ID o 4DT l l t o hh D:er t: ::: h f eh i I cc l c te f t:iioroe c ene t l c p y e l urrurrurr lz n h orobenoro ray ali ll ma tc en oj i n 1-D2-D u EK li eni an er ,, r Q SCA11MBCarbonChChTTV S S S ClieP al 37 n f i o g i S ual r 3 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349918 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 109109120120117116 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se 101019102234 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .2.1.5.0.7.2 ds EC in R ee 384421552135 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m at u al f n 13 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 000000000000000 000 Oh a C-BN ......VManuaSR w 3310 , v 8270 111111 s O w hnologil 330 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5.... P C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDNDNDNDNDNDNDNDNDND LK s o 382441215550217352 m ......d i B l e 000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n u enolenolol e z J b pb BR ene i e bd6 z hhn ne n ND r neoo - z- h nl ppaerr B-39428e e 3 T n BS p e o oo,hoo h - b u r rrt lal MPbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i S SSSSS ualm r 4 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349919 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 130 132133130130130130130130130130130130130130130130130 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da .4.7.1.3.9.7.4.1.5.5.1.6.8.4 se 34101043 m611321136972.16 n s p i i o 333433343313443 e L s r p y s w l P e a r Lo n a A e r a e .6.2.1.0.8.3.1.6.4.4.0.6.0.0.2.9.0.3 ds EC in R ee 326060634749315230415437434824622135 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 14 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 600000000000000000 000 Oh a C-BN .......VManuaSR w 3310 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s O w hnologil 330 00000000000 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5... P. C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M ND s o 261481481504383249420243331432301430480242629210353 m .................d i l e CS 00000000000000000 Re y L39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad 9428 o ty nephen henolene-d5ri 3 n u enolenolol e -z J b pb BR ene i e bd6 z hhn ne n ND r neoo SSS- z- h nl ppaerr e e 3 T n CCp e o oo,hoo h - b u r rrt lal LLbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i S ualm r 5 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349926 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 126 144153155148148126134132158176130130130154130130156 S 11 H PL // MC 99 hL g i H e: e: t t it 5 Da Da .8.7.8.4.7.8.5.5.4 se 1010292010103986 m382032.494. n s p i i o 32123331138 e L s r p y s w l P e a r Lo n a A e r a e .5.2.6.6.4.1.1.4.4.2.4.6.0.8.2.4.6.8 ds EC in R ee 397373785760376835516043515728722643 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 15 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 600000000000000000 000 Oh a C-BN .......VManuaSR w 3310 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s O w hnologil 330 00000000000 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1..... P C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDND s o 316586589628297547283409510578282724266438 m ..............d i l e 00000000000000 Re y MS39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e MS t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i SS ualm r 6 Q 1 O 19 e t- RT g c a it O 303030303030303030303030 P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r 00000000 p 1034232349938 e .5.6.5.0 o O 839915166141 PD ...... m Y pt 29105111061188 o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y 00 al r s w e MM e o it f V 3156586058926284459629685472283240924832 mov el .......... m c b i 0000000000 ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 126 144153155148148126134132158176130130130154130130156 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da .8.7.8.4.7.8.5.5.4 se 101029201010391086 m382032.494. n s p i i o 32123331138 e L s r p y s w l P e a r Lo n a A e r a e .4.0.8.7.6.5.4.8.7.8.7.6.9.4.1.2.4.1 ds EC in R ee 388181826467337231556542546230742844 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 16 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n _T SPK b 4223 , 4489 c l - s A 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) 600000000000000000 000 Oh a C-BN .......VManuaSR w 3310 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s O w hnologil 330 00000000000 ( W al ec : //w SVS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1.... P. C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDND s o 307648654662516267582254446526549624301742284441 m ..........d ......i SD l e 0000000000000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t SD eeid ct s dd e M t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i S ual r 7 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349964 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 109109120120117116 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se 101019102234 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .2.1.5.0.7.2 ds EC in R ee 384421552135 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m at u al f n 17 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 000000000000000 000 Oh a ......VManuaSR w 3310 P , v 8270 111111 s w L hnologil 330 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5.... P C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDNDNDNDNDNDNDNDNDND LK s o 382441215550217352 m ......d i B l e 000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n u enolenolol e z J b pb BR ene i e bd6 z hhn ne n ND r neoo - z- h nl ppaerr B-39428e e 3 T n BS p e o oo,hoo h - b u r rrt lal MPbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i S SSSSS ualm r 8 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349965 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 67 m i 130 132133130130130130130130130130130130130130130130130 S 11 H PL // MC 99 hL g i H e: e: t t it Da Da .4.7.1.3.9.7.4.1.5.5.1.6.8.4 se 34101043 m611321136972.16 n s p i i o 333433343313443 e L s r p y s w l P e a r Lo n a A e r a e .6.2.1.0.8.3.1.6.4.4.0.6.0.0.2.9.0.3 ds EC in R ee 326060634749315230415437434824622135 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 18 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 600000000000000000 000 Oh a .......VManuaSR w 3310 P 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s w L hnologil 330 00000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y 00 ns st 8 T QL u . - o b 100250250250100100250250 e ....5... P. C r 3 050002000500 i T 000.0..0000 v We 000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M ND s o 261481481504383249420243331432301430480242629210353 m .................d i l e CS 00000000000000000 Re y L39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad 9428 o ty nephen henolene-d5ri 3 n u enolenolol e -z J b pb BR ene i e bd6 z hhn ne n ND r neoo SSS- z- h nl ppaerr e e 3 T n CCp e o oo,hoo h - b u r rrt lal LLbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t lll i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aaa n d 5-6- s i ,,ali xxx maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i S ualm r 9 Q 1 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1034232349966 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q .2 67 m i 124 152150141132132156142131135134146130156183153154 S 11 H 64 PL // MC 99 hL g i H e: e: t t it Da Da .2.6.6.9.6.3.3.4.7.9.3.4.8 .3 se 58922177 m507674.7.03714 50 n s p i i- o 13222514921225 1 e L s - r p y s w l P e a r Lo n a A e r a e .5.2.6.6.4.1.1.4.4.2.4.6.0.8.2.4.6.8 ds EC in R ee 397373785760376835516043515728722643 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 19 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 600000000000000000 000 Oh a .......VManuaSR w 3310 P 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s w L hnologil 330 00000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1..... P C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDNDNDND s o 316586589628297547283409510578282724266438 m ..............d i l e 00000000000000 Re y MS39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e MS t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i S ualm r 0 Q 2 O 19 e t- RT g c a it O 303030303030303030303030 P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r 00000000 p 1034232349967 e .5.6.5.0 o O 839915166141 PD ...... m Y pt 29105111061188 o R W on i t C % a acce r m a eqNo: u AR p 28 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y 00 al r s w e MM e o it f V 3156586058926284459629685472283240924832 mov el .......... m c b i 0000000000 ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q .2 67 m i 124 152150141132132156142131135134146130156183153154 S 11 H 64 PL // MC 99 hL g i H e: e: t t it Da Da .2.6.6.9.6.3.3.4.7.9.3.4.8 .3 se 58922177 m507674.7.03714 50 n s p i i- o 13222514921225 1 e L s - r p y s w l P e a r Lo n a A e r a e .4.0.8.7.6.5.4.8.7.8.7.6.9.4.1.2.4.1 ds EC in R ee 388181826467337231556542546230742844 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 000000000000 at u al f n 20 n n o o s: ntit f V o t 3510C e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C_ c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - 600000000000000000 000 Oh a .......VManuaSR w 3310 P 80008000800080008000800080008000800080008000 , v 8270 .....1......111111 s w L hnologil 330 00000000000 ( W C al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y.0 ns st 8 T QL u 0 - o b 200500500100500100200200500500 e .....1..... P C r 3 0400 i T 00000.00000 v We 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M NDND s o 307648654662516267582254446526549624301742284441 m ..........d ......i SD l e 0000000000000000 Re y M39428 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t SD eeid ct s dd e M t ro eeut e A tt am o g yy D ll ah aat r n yl nn PD u ene y ophenol i AANoR SD -d14 m l ad o ty nephen henolene-d5ri n 0150-001u enolenolol hQCe z J b pb BR ene i e 9bd6 z hhn ne n ND r neoo - z- tc 0h nl ppaerr e e 3 T n a p 9e o oo,hoo h - b u r rrt lal 1Bbn p uu 6 o t lle -1bee oo, o neer llo t o t oooFFT 4 : i h e hh -,-- rrr s T oro or z l ccro IDl ooo2N22p ii t ll l i hrr h D:er t: :: P:::: ol s, e i Ihhh cnl lc TT c tesne f t:ii ccc i t o p a y e urrurrurrurrurrurr lt aa n a d 5-6- s i ,,ali xx x maroben r en oj t 4-D444-D u lii eny an ,,,, r Q SCA1222o-CreCreHeHeHeNPP S S S S S S ClieP al 37 n f i o g i ualual r 1 2 O 19 e t- RT g c itQitQ a O P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10326023412421032602341243 e o O PDPD m Y pt o W RR on i t C %% a acce r m a eqNo:eqNo: u AR p 40 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alal r s w e MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I i SU R DD it e e din ch u PP m l l t r a RR epik C HoVS Ba 2019201920192019 itit //// Q 6666 mm ii S 1111 H PLP //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 80120 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .9 ds ECEC in 104801201078012010680120109801201058012010880120 RR ee 95 m c r %% x e t e ge e 38 nn d a o f ri o t tit /L/L o a d m on gg i m ie r s L i mm 0000000 at u alal f n 21 n n o o s:s: ntit f Vf V o tt 3010A3010A e ii a c cti atine g WW ReRe t r qu UnUn e m SS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a -7(6-7(6 ek.c e r t end Wi o t PP o io u e l 253p LL c ueue s a e ll . e ) 000000000000000 CC000000 Oh aa .......VS w 3310 , TT vv 6010D6010D 2222222 s-- w ll hnologil 330 tt ( WW al ec : //w MSMS P MManua F: T RLR SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211ite y 0000 ns stst T 8 T QLQL u .. - o b 500100200500500500100200500500 ee .5...5.... P..P C r 3 05000500 i TT 0000.00000.0 v We 00 25nkE n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu 089212181116 n T M ...... NDNDNDNDNDNDNDND LK ss o m 212222 d i B l e CS ReRe y M39440L39440 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ctct e ee ed tt eeid ct s dd e t ro eeut e tt am o g yy D ll ah at r a n n nPD u y AA SD 9440 e)e) 3 Cd)(Cr)Cd)(Cr) - SS J BRR s)s) (( a)(a)( NDNo SSS mm AA BB g)g) mm B-39440 (( mm BSuu b)b) (( CC ii uu cAcA uu ii ii MPPiLLPi (( mm mrmr nn mm uu ee oo ii: enen ee rlrl s vv ss IDID raeilraeil D:D:er t: eCadChrLead(eCadChrLead(i II ll c tete f t: tt pp yy e P AP BPPPP SP SP AP BPPPP SP S ll n ali mama enen oj u lili anan CLCLCLCLCLCLCLCLCLCLCLCLCLCL r Q SCATTTTTTTSCATTTTTTT ClieP al 37 n f i o g i ualual r 2 QQ 2 O 19 e t- RT g c a itit O 20202020202020 P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r 0 p 10332023468751033202346876 e o O 199695935256 PDPD ...... m Y pt 111122 o RR W on i t C %% a acce r m a eqNo:eqNo: u AR p 40 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y 0 alal r s w e MM e o 280962058048344258 it ...... f Vf V mov el 212222 m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 2019201920192019 itit //// Q 6767 mm ii 130130 130130130130130130130130130130130130 S 1111 H PL //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 7070707070707070707070707070 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .9.8.8 ds ECEC in 114103102117113115102105104120116 RR ee 989799 m c r %% x e t e ge e 38 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 0000000000 at u alal f n 22 7474 n n o 88 o s:s: .. ntit f Vf V o tt 3010A3010A e ii a 22 c cti atine g WW ReRe t 005326005326 r qu .. UnUn e m SS g e 00 e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a -7(6-7(6 ek.c e r te nd Wi o t PP o iuo e l 253p LL c ueue s a e ll . e ) 000000000000000000000000000000 C000000C000000 Oh aa ..............VManuaSR w 3310 , TT vv 6010D6010D 22222222222222 s-- w ll hnologil 330 tt ( WW al ec : //w MSMS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y 0000 ns stst T 8 T QLQL u .. - o b 500100200500500500100200500500 ee .5.....5.... PP C r 3 0500 0500 i TT 0000.00000.0 v We 0 0 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu 289606053426310010094032 n T M ............ NDND ss o m 212222222222 d i SD l e ReRe y MS39440M39440 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah aat r n nn PD u y AANoR SD e)e) 0818-0120818-012 hQChQC Cd)(Cr)Cd)(Cr) SS J BR s)s) (( 99 a)(a)( ND tctc mm 0A0A BB g)g) mm (( mm aa uu b)b) (( 99 ii uu cAcA uu ii ii 1BPi1BPi (( mm mrmr nn mm uu ee oo ii: enen ee rlrl s vv ss IDID raeilraeil D:D:er t: eCadChrLead(eCadChrLead(i II ll c tete f t: tt pp yy e P AP BPPPP SP SP AP BPPPP SP S ll n ali mama enen oj u lili anan CLCLCLCLCLCLCLCLCLCLCLCLCLCL r Q SCATTTTTTTSCATTTTTTT ClieP al 37 n f i o g i ualualualual r 3 QQQQ 2 O 19 e t- RT g c a itititit O 20 P O - mmmm iiii LLLL 19090844 01 P DDDD PPPP y E ov l RRRR c a e n r R und a o #: d r p 1033592346192103359234619310335923462001033592346201 e o O 75 PDPDPDPD . m Y pt 2 o RRRR W on i t C %%%% a acce r m a eqNo:eqNo:eqNo:eqNo: u AR p 61 SSSS RunNo:RunNo:RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alalalal r s w e MM e o it f Vf Vf Vf V 0111 mov el . m c b i 0 ti e D: ReReReRe L s g I SU i R DDDD it e e din ch u PPPP m l l t r a RRRR epik C HoVPS Ba 20192019201920192019201920192019 itititit //////// Q 77777777 mmmm iiii 120125125 S 11111111 H PL //////// MC 99999999 hLhLhLhL gggg iiii HHHH e:e:e:e: e:e:e:e: tttt tttt itititit DaDaDaDa DaDaDaDa se 807575 mmmm n ssss pppp iiii iiii o eeee LLLL ssss rrrr p yyyy s wwww llll PPPP e aaaa r LoLoLoLo nnnn a AAAA e r a e ds ECECECEC in 112111108 RRRR ee m c r %%%% x e t e ge e 38 nn d a o f ri o t tit o a d m on i m ie r s L i PPMPPMPPMPPM 000 at u alalalal f n 23 n n o o s:s:s:s: ntit f Vf Vf Vf V o tttt 7470A7470A7470A7470A e iiii a c cti atine g WWWW ReReReRe t r qu UnUnUnUn e m SSSS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPKSPK b 4223 , 4489 c l - s (74(74(74(74 4 tin a ek.c e r te nd Wi PPPP o t o iuo LLLL e l 253p c ueueueue s a e llll . CCCC e ) Oh aaaa VManuaSR TTTT w 3310 040001000100 , vvvv 7470A7470A7470A7470A .. ____ s w 0 hnologil 330 .00 ( GGGG WWWW 0 al ec : //w HSHSHSHS P E M F: T RL SPKSPKSPKSPK FAX http No:No:No:No: ntal : e stststst ahoga Code:Code:Code:Code: m eeee 211 ite y ns stststst T 8 TTT QLQLQLQL u - o b eeee PPPP C r 3 i TTTT v 00200002000050000500 We .... 25nk n a 0000 ) l E it B 330 d ( its o mm m th L: i e l Su ltltltlt E its uuuu n T M ND LK ssss o m d i 044601110108 BSD l e CS .. 0 ReReReRe y .00 M39461L39461MS39461M39461 itati r t 0 e ciat n v o a e:e:e:e: o D:D:D:D:s u pppp s c I I I I q yyyy e a hhhh r TTTT e pppp tctctctc d h ow e aaaa t mmmm el n BBBB pt aaaa b ie SSSS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah aat r n nn PD u y AANoR SD 9461 3 0845-0010845-001 hQChQC - J BR 99 ND SSS tctc 00 B-39461 aa BS CC 99 ryryryry MPLL1B1B uuuu cccc : rrrr s IDIDIDID eeee D:D:D:D:er t: eMeMeMeM i IIII llll c tetetete f t: tttt pppp yyyy e PPPP llll n ali mamamama enenenen oj u lililili anananan CLCLCLCL r Q SCATSCATSCATSCAT ClieP al 37 n f i o g i ual r 4 Q 2 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1033592346201 e o O PD m Y pt o R W on i t C % a acce r m a eqNo: u AR p 61 S RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 20192019 it // Q 77 m i S 11 H PL // MC 99 hL g i H e: e: t t it Da Da se m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e ds EC in R ee m c r % x e t e ge e 38 nn d a o f ri o t tit o a d m on i m ie r s L i PPM at u al f n 24 n n o o s: ntit f V o t 7470A e i a c cti atine g W Re t r qu Un e m S g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s (74 4 tin a ek.c e r te nd Wi P o t o iuo L e l 253p c ue s a e l . C e ) Oh a VManuaSR T w 3310 , v 7470A _ s w hnologil 330 ( G W al ec : //w HS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M s o m d i SD l e Re y M39461 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t SD eeid ct s dd e M t ro eeut e A tt am o g yy D ll ah aat r n nn PD u y AANoR SD 0845-001 hQC J BR 9 ND tc 0 a 9 1B : s ID D:er t: e i I l c te f t: t p y e l n ali ma en oj u li an r Q SCA ClieP al 37 n f i o g i C+C+C+C+ ualual r 5 QQQQ 2 O 19 e t- RT g c itQitQ a O 3030303030 P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r 00 p 10368223767551036822376756 e .4.8.7 o O 2523 PD..PD m Y pt o W RR on i t C %% a acce r m a eqNo:eqNo: u AR p 80 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alal r s w e MM e o it f Vf V 01101001171201889 mov el ... m c 0075210009659 b i 0.0.0 ti e D: Re Re L s 00 g I i SU R DD it e e din ch u PP m l l t r a RR epik C HoVS Ba 2019201920192019 itit //// Q 8585 mm ii S 1212 H PLP //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 102241019210208101571019410192102081015710194 mm n ss p p ii ii o e e LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .0.5.0.2.2.2.5.6.9 ds ECEC in 1031019717210251110102241171019718810251 R R ee 996788596975966569 m c r %% x e t e ge e 38 nn d a o f ri o t tit /L/L o a d m on gg i m ie r s L i mm 0000000000 at u alal f n 25 n n o o s:s: ntit f Vf V o tt 3510C3510C e ii a c cti atine g WW ReRe t r qu UnUn e m SS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 C-C- c l - s 4 tin a ek.c e OO r t end Wi o t o io u e l 253p c ue0000ue0000 s SVSV a e ll ... ..e ) -- Oh aa VS w 3310 PP 0100010001000100010001000100010001000100 , vv 8081 8081 ....2020....2020 .. s w LL hnologil 330 0000000000 ( WW CC al ec : //w TST S P MManua F: T RLR SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211ite y ns stst 8 TT QLQL u - o b ee PP C r 3 i TT v 00500005000050000500005000050000500005000050000500 We ...... .... 25nkE n a 0000000000 ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E .8.8.1.0 its uu n T M ss o m 1314 d 1113 i 0990067501030880017201100752011709650188 SD l e ..... 00000 ReRe y ..0.00.0.0 M39480MS 39480 itati r t 00000 e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a h h r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ctct e ee ed tt sd eeid ct s dd e mms t ro eeut e tt am o g yy D ll ah amam at r a n n nPD u y AA urhurh SD DD 0844-001ah0844-001ah dede J tt ii BRR 99 NDNo xx uu 00 oo oo 99 pp 1S1S ee oror MXMX ll : HCHC hh CC s orororor llcllc BB IDID TDCBTDCB yy hhhh D:D:er t: :::: ee i Ia-Ia- xx cccc ll c tete f t: tt inaainaa pp yy e tturrurrtturrurr ll n hoho ali tt mama enen mmmm oj u ee lili ndrndr anan r Q SCAEgaHepHepM S SSCEgaHepHepM S S A ClieP al 37 n f i o g C+C+ i C+C+ d ualual r 6 QQ QQ QQ 2 dd O 19 e t- RT g c a itit O P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10368223767571036822376758 e o O PDPD m Y pt o RR W on i t C %% a acce r m a eqNo:eqNo: u AR p 80 SS RunNo:RunNo: ide em 4 rs 9 p ut r 3 o o Mini f y alal r s w e MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 2019201920192019 itit //// Q 8585 mm ii 130 130130130178130130119119 S 1212 H PL //// MC 9999 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 101010101010101010 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .6.0.8.9.8.9.6.7 ds ECEC in 130 RR ee 5938574732513253 m c r %% x e t e ge e 38 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 00000 at u alal f n 26 n n o o s:s: ntit f Vf V o tt 3510C3510C e ii a c cti atine g WW ReRe t r qu UnUn e m SS g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 C-C- c l - s 4 tin a ek.c e OO r te nd Wi o t o iuo e l 253p c ue0000ue0000 s SVSV a e ll ... ..e ) -- Oh aa VManuaSR w 3310 PP 01000100010001000100 , vv 80818081 ....20202020 . s w LL hnologil 330 00000 ( WW CC al ec : //w TSTS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst T 8 T QLQL u - o b ee PP C r 3 i TT v 0025000500 We .. 25nk n 000500000500 000500000500000500000500000500000500000500000500 a .....00..... ) l E 00 00000000 it B 330 d ( its o mm m th L: i e l Su ltlt E .4.7 its uu 5551 n T M .. NDNDNDNDNDNDND LK ss o m 610610 d i 05960380057804790130 B l e CS . 0000 ReRe y ....0 L39480M39480 itati r t 0000 e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD dede J ii 39480 BR 39480 - ND -xx SS bal soo BS t C cpp o lLmP t ee oror MXMX ll , : HCHC hh CC s orororor llcllc BB IDID TDCBTDCB yy hhhh D:D:er t: :::: ee i Ia-Ia- xx cccc ll c tete f t: tt inaainaa pp yy e tturrurrtturrurr ll n hoapheneho ordane ali tt l mama x enen mmmm oj u ee lili ndrndr anan o r Q SCAEgaHepHepM S SSCAChTEgaHepHepM S S ClieP al 37 n f i o g i ualual r 7 QQ 2 O 19 e t- RT g c 5 a itit O P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10346323517351034632351736 e o O PDPD m Y pt 275 .o RR W on i 0 t C 63 %% a acce r 4 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal r s w e MM e o 156 it . f Vf V mov el 9 m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q 88 mm ii 122122 S 11 H PL // MC 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa .6.6 se m1m1 n ss pp ii ii o 88 ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e .5.7 ds ECEC in RR ee 9090 m c r %% x e t e ge e 38 nn d a o f ri o t tit KgKg //o a d m gg on i m ie r s L i mm at u alal f n 27 9292 n n o o s:s: ntit f Vf V o tt 1010 e ii a .. c cti atine 00 g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r ReaRea te nd Wi o,, t o iuo e ee l 253p c ue00ue00 s a e ll .d.d. e ) ii Oh aa VManuaSR w 3310 , nn vv 90149014 1010 s w aa hnologil 330 ( yy WW al ec : //w CSCS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst 8 TT QLQL u - o b 495481 ee . PP. C r 3 i TT 00 v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu 1618 n T M .. ss o m 99 d i SD l e ReRe y MSR103463MR103463 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah amam aat r n nn PD u y AANoR urhurh SD DD 0844-001h0844-001h J tt BR 9ve9ve ii ND uu tt 00 oo cc 99 aa 1S1S ee : RR s IDID ,, D:D:er t: ee i II ll dede c tete f t: ii tt pp yy e ll n ali mama enen oj u lili anan r Q SCACyanSCACyan ClieP al 37 n f i o g i ualualual r 8 QQQ 2 O 19 e t- RT g c a ititit O P O - mmm iii LLL 19090844 01 P DDD PPP y E ov l RRR c a e n r R und a o #: d r p 103463235172010346323517211034632351723 e o O PDPDPD m Y pt o RRR W on i t C 63 %%% a acce r 4 m a eqNo:eqNo:eqNo: u 3 AR p SSS RunNo:RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alalal r s w e MM e o it f Vf Vf V mov el m c b i ti e D: ReReRe L s g I SU i R DDD it e e din ch u PPP m l l t r a RRR epik C HoVPS Ba 201920192019 ititit /// Q 888 mmm iii 115150 S 111 H PL /// MC 999 hLhLhL ggg iii HHH e:e:e: e:e:e: ttt ttt ititit DaDaDa DaDaDa se 8550 mmm n sss ppp iii iii o eee LLL sss rrr p yyy s www lll PPP e aaa r LoLoLo nnn a AAA e r a e .9 ds ECECEC in 109 RRR ee 93 m c r %%% x e t e ge e 38 nn d a o f ri o t tit /L/L/L o a d m ggg on i m ie r s L i mmm 00 at u alalal f n 28 n n o o s:s:s: ntit f Vf Vf V o ttt e iii a c cti atine g ReReRe t r qu UnUnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r ReaReaRea te nd Wi o,,, t o iuo e eee l 253p c ueue00ue s a e lll .dd.d e ) iii Oh aaa VManuaSR w 3310 5000 , nnn vvv 901490149014 10. s w aaa hnologil 330 0 ( yyy WWW al ec : //w CSCSCS P E M F: T RL SPKSPKSPK FAX http No:No:No: ntal : e ststst ahoga Code:Code:Code: m eee 211 ite y ns ststst TT 8 T QLQLQL u - o b 485495495 eee ... PPP C r 3 i TTT 000 v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltltlt E its uuu 39 n T M . ND LK sss o 543 m 9.d i B l LC e CS 0 ReReRe y MR103463LR103463RR103463 itati r t e ciat n v o a e:e:e: o D:D:D:s u ppp s c I I I q yyy e a hhh r TTT e ppp tctctc d h ow e aaa t mmm el n BBB pt aaa b ie SSS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD hQC J BR veveve LK iii ND SW tc ttt B LCa BW ccc CSC aaa MPLLRB eee : RRR s IDIDID ,,, D:D:D:er t: eee i III lll dedede c tetete f t: iii ttt ppp yyy e lll n ali mamama enenen oj u lilili ananan r Q SCACyanSCACyanSCACyan ClieP al 37 n f i o g i ualual r 9 QQ 2 O 19 e t- RT g c a itit O P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10347023521491034702352150 e o O PDPD m Y pt o RR W on i t C 70 %% a acce r 4 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal r s w e MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q 88 mm ii 115 S 11 H PL // MC 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 85 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e ds ECEC in 101 RR ee m c r %% x e t e ge e 38 nn d a o f ri o t tit /L/L o a d m gg on i m ie r s L i mm 0 at u alal f n 29 n n o o s:s: ntit f Vf V o tt e ii a c cti atine g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o ReactReact iuo e,, l 253p c ueue s a ee e ll . e ) Oh dada VManuaSR w 3310 ii 4800 , vv 90349034 ff s w ll hnologil 330 ( uWuW al ec : //w SSSS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y.0.0 ns stst T 8 T QLQL u 55 - o b ee 22 PP C r 3 i TT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu n T M ND LK ss o m d i 4830 B l e CS ReRe y MR103470LR103470 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 103470 R - J BR ND SSW veve B-R103470ii BW tCCt cc MPLL : s IDID ReaRea D:D:er t: ,, ee i II ll c tete f t: tt pp yy e dede ll n ii ff ali malmal enen oj u lili uu anan r Q SCASSCAS ClieP al 37 n f i o g i ualual r 0 QQ 3 O 19 e t- RT g c a itit O 30 P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10347023521611034702352162 e o O 44 PDPD . m Y pt o 1 RR W on i t C 70 %% a acce r 4 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal r s 90 w e MM e o 8 it f Vf V 4 mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q 88 mm ii 120120 S 11 H PL // MC 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa se 8080 mm n ss pp ii ii o ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e ds ECEC in 102100 RR ee m c r %% x e t e ge e 38 nn d a o f ri o t tit KgKg //o a d m gg on i m ie r s L i mm 00 at u alal f n 30 n n o o s:s: ntit f Vf V o tt e ii a c cti atine g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o ReactReact iuo e,, l 253p c ueue s a ee e ll . e ) Oh dada VManuaSR w 3310 ii 48004800 , vv 90349034 ff s w ll hnologil 330 ( uWuW al ec : //w SSSS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y.0.0 ns stst 8 TT QLQL u 55 - o b ee 22 PP C r 3 i TT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E its uu n T M ss o m d i 4890 SD4820 l e ReRe y MSR103470MR103470 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t SD eeid ct s dd e MSM t ro eeut e AA tt am o g yy D ll ah amam aat r n nn PD u y AANoR urhurh SD DD 0844-001h0844-001h J tt BR 99 ND uu 00 veve ii oo tt 99 cc 1S1S : s IDID ReaRea D:D:er t: ,, ee i II ll c tete f t: tt pp yy e dede ll n ii ff ali malmal enen oj u lili uu anan r Q SCASSCAS ClieP al 37 n f i o g i H ualual r 1 QQ 3 O 19 e t- RT g c 5 a itit O P O - mm ii LL 19090844 01 P DD PP y E ov l RR c a e n r R und a o #: d r p 10373223655561037322365558 e .3 o O PDPD 0 m Y pt o RR W on i t C 32 %% a acce r 7 m a eqNo:eqNo: u 3 AR p SS RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alal .2 r s w e 6 MM e o it f Vf V mov el m c b i ti e D: ReRe L s g I SU i R DD it e e din ch u PP m l l t r a RR epik C HoVPS Ba 20192019 itit // Q .4 66 mm ii S 22 H PL // MC 101 99 hLhL gg ii HH e:e: e:e: tt tt itit DaDa DaDa .6 se m8m n ss pp ii ii o 9 ee LL ss rr p yy s ww ll PP e aa r LoLo nn a AA e r a e ds ECEC in 100 RR ee m c r %% x 9C4C e ..t e ge e 00 38 nn d 22 a o f ri o t tit @@ o .. a d m on uu i m ie .. r s L i ss 0 at u alal f n 31 n n o o s:s: ntit f Vf V o tt e ii a c cti atine g ReRe t r qu UnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e(450(450 r te nd Wi o t o iuo e WW l 253.0 p c ueue s a e ll .7 e )PP Oh aa VManuaSR w 3310 , vv 9045D9045D s w_N_N hnologil 330 ( WW HH al ec : //w pSpS P E M F: T RL SPKSPK FAX http No:No: ntal : e stst ahoga Code:Code: m ee 211 ite y ns stst 8 TT QLQL u - o b ee PP C r 3 i TT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltlt E .0.2 its uu n T M 76 ss o m d i l e CS ReRe y LR103732DUPR103732 itati r t e ciat n v o a e:e: o D:D:s u pp s c I I q yy e a hh r TT e pp tctc d h ow e aa t mm el n BB pt aa b ie SS dd ee acc ct ct e ee ed t t eeid ct s dd e DUP t ro eeut e A tt am o g yy D ll ah aat r n nn PD u y AANoR SD 103732 R 1702-001 hQC - J BR 9 ND SSW tc 0 a CC 9 LL1B : s IDID D:D:er t: ee i II ll c tete f t: tt pp yy e ll n ali mama enen oj u lili anan r Q SCApHSCApH ClieP al 37 n f i o g i ualualual r 2 QQQ 3 O 19 e t- RT g c a ititit O P O - mmm iii LLL 19090844 01 P DDD PPP y E ov l RRR c a e n r R und a o #: d r p 103732236556910373223655741037322366527 e o O PDPDPD m Y pt o RRR W on i t C 32 %%% a acce r 7 m a eqNo:eqNo:eqNo: u 3 AR p SSS RunNo:RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alalal r s w e MM e o it f Vf Vf V mov el m c b i ti e D: ReReRe L s g I SU i R DDD it e e din ch u PPP m l l t r a RRR epik C HoVPS Ba 201920192019 ititit /// Q 666 mmm iii 110110110 S 222 H PL /// MC 999 hLhLhL ggg iii HHH e:e:e: e:e:e: ttt ttt ititit DaDaDa DaDaDa se 909090 mmm n sss ppp iii iii o eee LLL sss rrr p yyy s www lll PPP e aaa r LoLoLo nnn a AAA e r a e ds ECECEC in 101101101 RRR ee m c r %%% x 9C7C4C e ...t e ge e 999 38 nn d 111 a o f ri o t tit @@@ o ... a d m on uuu i m ie ... r s L i sss 000 at u alalal f n 32 n n o o s:s:s: ntit f Vf Vf V o ttt e iii a c cti atine g ReReRe t r qu UnUnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o (9045(9045(9045 iuo e l 253.0.0.0 p c LLL ueueue s a e IlIlIl .777 e ) Oh aaa VManuaSR w 3310 OOO , vvv 9045D9045D9045D s w hnologil 330 ( H_WH_WH_W al ec : //w PSPSPS P E M F: T RL SPKSPKSPK FAX http No:No:No: ntal : e ststst ahoga Code:Code:Code: m eee 211 ite y ns ststst 8 TTT QLQLQL u - o b eee PPP C r 3 i TTT v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltltlt E .0.0.0 its uuu n T M 777 sss o m d i l e CSCSCS ReReRe y LR103732LR103732LR103732 itati r t e ciat n v o a e:e:e: o D:D:D:s u ppp s c I I I q yyy e a hhh r TTT e ppp tctctc d h ow e aaa t mmm el n BBB pt aaa b ie SSS dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 7 7 7 KKK CCC J BR EEE ND SWSWSW CCC CHLCHLCHL : s IDIDID D:D:D:er t: eee i III lll c tetete f t: ttt ppp yyy e lll n ali mamama enenen oj u lilili ananan r Q SCApHSCApHSCApH ClieP al 37 n f i o g i ual r 3 Q 3 O 19 e t- RT g c a it O 10 P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1037322365571 e .4 o O PD 0 m Y pt o R W on i t C 32 % a acce r 7 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y al .6 r s w e 7 MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it 0 / Q 6 m i S 2 H PL / MC 9 hL g i H e: e: t t it 0 Da Da se m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e 0 ds EC in R ee m c r % x 8C e .t e ge e 9 38 nn d 1 a o f ri o t tit @ o . a d m on u i m ie . r s L i s 0 at u al f n 33 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l - s 4 tin a ek.c e r te nd Wi o t o iuo e l 253p c ue s a e l . e ) (9045D) Oh a VManuaSR w 3310 S , v 9045D s w_ hnologil 330 ( W H al ec : //w pS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E .6 its u n T M 7 s o m d i l e Re y DUPR103732 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e DUP t ro eeut e A tt am o g yy D ll ah am aat r n nn PD u y AANoR urh SD D 0844-001h J t BR 9 ND u 0 o 9 1S : s ID D:er t: e i I l c te f t: t p y e l n ali ma en oj u li an r Q SCApH ClieP al 37 n f i o g i SS ualualual r 4 QQQ 3 O 19 e t- RT g c a ititit O P O - mmm iii LLL 19090844 01 P DDD PPP y E ov l RRR c a e n r R und a o #: d r p 103755236679310375523667941037552366795 e o O PDPDPD m Y pt o RRR W on i t C 55 %%% a acce r 7 m a eqNo:eqNo:eqNo: u 3 AR p SSS RunNo:RunNo:RunNo: 0 ide em rs 1 p ut r R o o Mini f y alalal r s w e MM e o it f Vf Vf V mov el m c b i ti e D: ReReRe L s g I SU i R DDD it e e din ch u PPP m l l t r a RRR epik C HoVPS Ba 201920192019 ititit /// Q 555 mmm iii 130141144130105106130 S 222 H PL /// MC 999 hLhLhL ggg iii HHH e:e:e: e:e:e: ttt ttt ititit DaDaDa DaDaDa .5.3 se 7070373870 mm08m n sss ppp iii iii o 66 eee LLL sss rrr p yyy s www lll PPP e aaa r LoLoLo nnn a AAA e r a e 00 .3.3.7.3.0 ds ECECEC in 144114 RRR ee 9386615747 m c r %%% x e t e ge e 38 nn d a o f ri o t tit /L/L/L o a d m ggg on i m ie r s L i mmm 000000 at u alalal f n 34 n n o o s:s:s: ntit f Vf Vf V o ttt e iii a c cti atine g ReReRe t r qu UnUnUn e m g e e u c. D St. nom Pa ntol ov Ig I n SPKSPKSPK b 4223 , 4489 C-C-C- c l - s 4 tin a ek.c e OOO r te nd Wi o t o iuo e l 253p c ueueue s SVSVSV a e lll . e ) --- Oh aaa VManuaSR w 3310 PPP 5000300075003000300075003000 , vvv 8321A8321A8321A .... s w LLL 000 hnologil 330 .0.00.0 ( WWW CCC 000 al ec : //w TSTSTS P E M F: T RL SPKSPKSPK FAX http No:No:No: ntal : e ststst ahoga Code:Code:Code: m eee 211 ite y ns ststst T 8 TT QLQLQL u - o b eee PPP C r 3 01000100 0100010001000100 i TTT ...... v We 00 0000 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su ltltlt E its uuu n T M NDND LK sss o 342259185175 m ....d i 072007000430 B l e CS .0.00.0 ReReRe y 000 MR103755LR103755MSR103755 itati r t e ciat n v o a e:e:e: o D:D:D:s u ppp s c I I I q yyy e a hhh r TTT e ppp tctctc d h ow e aaa t mmm el n BBB pt aaa b ie ididid SSS dd ccc ee aaa acc ct ct ccc e ee iii ed t t ttt eeid eee ct s dd e MS ccc t ro eeut aaa e A tt lll am o g yy yyy D ll ah aat r n nn PD u y AANoR SD ophenophenophen rrr 1306-001 ooo hQC J lll BR 9 ND hhh SS tc 0 ccc a BS iii CSC 9 MBPLL1B 4-D4-D4-D : ,,, s IDIDID 222 D:D:D:er t: ::: eee i III lll TPTPTP c tetete f t: ttt ppp yyy e urrurrurr lll n 5-5-5- ,,,ali mamama enenen oj 4-D44-D44-D4 u lilili ananan ,,, ,,, r Q SCA22 SSCA22 SSCA22 S ClieP al 37 n f i o g i S ual r 5 Q 3 O 19 e t- RT g c 0 a it O 3030 P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r 0 p 1037552366796 e o O 7774 PD .. m Y pt 56 o R W on i t C 55 % a acce r 7 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y al r s w e MM e o it f V 1850 mov el . m c 04300 b i 0. ti e D: Re L s 0 g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 5 m i 150150130 S 2 H PL / MC 9 hL g i H e: e: t t it Da Da se 101070 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .3.3.3 ds EC in R ee 656151 m c r % x e t e ge e 38 nn d a o f ri o t tit /L o a d m g on i m ie r s L i m 00 at u al f n 35 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 C- c l - s 4 tin a ek.c e O r te nd Wi o t o iuo e l 253p c ue s SV a e l . e ) - Oh a VManuaSR w 3310 P 300075003000 , v 8321A .. s w L 0 hnologil 330 0.0 ( W C 0 al ec : //w TS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 01000100 i T .. v We 00 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M s o 196188 m .d .i 0460 SD l e 0.0 Re y 0 MR103755 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie id S dd c ee a acc ct ct c e ee i ed t t t SD eeid e ct s dd e M c t ro eeut a e A tt l am o g yy y D ll ah aat r n nn PD u y AANoR SD ophen r 1306-001 o hQC J l BR 9 ND h tc 0 c a i 9 1B 4-D : , s ID 2 D:er t: : e i I l TP c te f t: t p y e urr l n 5- ,ali ma en oj 4-D4 u li an , , r Q SCA22 S ClieP al 37 n f i o g i ual r 6 Q 3 O 19 e t- RT g c a it O P O - m i L 19090844 01 P D P y E ov l R c a e n r R und a o #: d r p 1037962368919 e o O PD m Y pt o R W on i t C 96 % a acce r 7 m a eqNo: u 3 AR p S RunNo: 0 ide em rs 1 p ut r R o o Mini f y al r s w e MM e o it f V mov el m c b i ti e D: Re L s g I SU i R D it e e din ch u P m l l t r a R epik C HoVPS Ba 2019 it / Q 7 m i 102 S 2 H PL / MC 9 hL g i H e: e: t t it Da Da se 98 m n s p i i o e L s r p y s w l P e a r Lo n a A e r a e .2 ds EC in R ee 98 m c r % x e t e ge e 38 nn d a o f ri o t tit o a d m on i m ie r s L i °F 0 at u al f n 36 n n o o s: ntit f V o t e i a c cti atine g Re t r qu Un e m g e e u c. D St. nom Pa ntol ov Ig I n SPK b 4223 , 4489 c l (10 - s 4 tin a ek.c e r S te nd Wi o t o iuo e t_l 253.4 p c ue s a e l . e )P Oh a VManuaSR w h 3310 , v 1010 135 s w hnologil 330 as ( W l al ec : //w FS P E M F: T RL SPK FAX http No: ntal : e st ahoga Code: m e 211 ite y ns st 8 T QL u - o b e P C r 3 i T v We 25nk n a ) l E it B 330 d ( its o mm m th L: i e l Su lt E its u n T M s o 133 m d i l e CS Re y LR103796 itati r t e ciat n v o a e: o D:s u p s c I q y e a h r T e p tc d h ow e a t m el n B pt a b ie S dd ee acc ct ct e ee ed t t eeid ct s dd e t ro eeut e tt am o g yy D ll ah aat r n nn PD u y AANoR SD 103796 R - J F) BR ° ND SSS 0 CC 4 LL 1 ( : t s n ID i D:er t: e i I l c te f t: t p y e hpo l n ali s ma en oj a u li an r Q SCAFl ClieP Page37of38 SummitEnvironmentalTechnologies,Inc. 3310 WinSt. CuyahogaFalls,Ohio44223 SampleLog-InCheckList TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com ClientName:WorkOrderNumber:RcptNo: SYN-NC-27028190908441 Loggedby:9/12/201910:10:00AM JohnA.Semenik Completed By:9/12/20199:44:05 PM JacquelineRasile Reviewed By:9/13/201910:24:09AM JenniferWoolf ChainofCustody IsChainofCustodycomplete?YesNoNotPresent 1. Howwas the sampledelivered? UPS 2. Log In Coolersarepresent?YesNoNA 3. Shippingcontainer/cooleringood condition?YesNo 4. Custodysealsintacton shipping container/cooler?YesNoNotPresent No.Seal Date:SignedBy: Wasanattemptmade to cool the samples?YesNoNA 5. Wereallsamplesreceivedata temperatureof>0°C to6.0°CYesNoNA 6. Sample(s)inproper container(s)?YesNo 7. Sufficientsamplevolume forindicated test(s)?YesNo 8. Are samples(except VOAandONG)properlypreserved?YesNo 9. Waspreservativeadded tobottles?YesNoNA 10. Is theheadspacein the VOAvialsless than1/4inchor6mm?YesNoNo VOAVials 11. Wereanysample containersreceivedbroken?YesNo 12. Doespaperworkmatchbottlelabels?YesNo 13. (Notediscrepancieson chainof custody) ArematricescorrectlyidentifiedonChainofCustody?YesNo 14. Isit clearwhatanalyseswererequested?YesNo 15. Wereallholding timesable tobemet?YesNo 16. (Ifno,notify customer forauthorization.) Special Handling(if applicable) Was clientnotifiedofalldiscrepancieswiththisorder?YesNoNA 17. PersonNotified: Date ByWhom:Via:eMailPhoneFaxIn Person Regarding: ClientInstructions: Additionalremarks: 18. CoolerInformation CoolerNoTempºCConditionSealIntactSeal NoSeal DateSigned By 15.5GoodNot Present Page37of37 Page38of38 State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section’sNon-Discharge Permitting Unit General – This certification provides detailed information of residuals source generating facility and its residuals quality for land . Do not submit this certification for review without application, distribution, or disposal in accordance with 15A NCAC 02T .1100 a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit a separate certification for each source facility. For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source-Generating Facility Information: For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the “Map Guidance for Residuals Land Application Permits”. Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan -A detailed sampling plan for the residuals source-generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division-certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: For each source facility, attach the following: Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 1 Page 900 600 42123580 Proposed s Per Year Dry Ton b 900600 42123580 Maximum Current 10(B) 0 - 0023841 32010(A) 32 - - NCNC0047597 03 03 Permit Number D (Deleted) County DurhamDurhamDurhamDurham M (Modified) ent reatment ham WRF PlantPlant Durham WRF h Dur Facility Name R (Renewed) NortSouth Brown Water T Williams Water Treatm N (New) 16 - 06 hamhamhamham are: RSC : facility FORM City Of Durham City Of DurCity Of DurCity Of DurCity Of Dur source Facility Permit Holder a RRRR Status Code Status Code for RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: a SUMMARY FOR of 5 2 Page (i.e, not applicable to new facility). distribution, land application, or disposal for permitted currently 16 - residuals 06 he amount of T b FORM: RSC State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE-GENERATING FACILITY INFORMATION (See Instruction B.): 1.FacilityName: Brown Water Treatment Plant 2. Facility permit holder is: Federal, State, Local Government, or Private. Facility permit issued by:Div. of Water Resources,Div. of Environmental Health, or Other (explain: ). 3. Facility contact person and title: Tom Lucas Assistant WTP Superintendent Complete mailing address: 101 City Hall Plaza City: Durham State: NC Zip: 27701- Telephone number: (919) 560-4362E-mail address: 4.Facility physical address: 1615 Infinity Road City: Durham State: NC Zip: 27712- Coordinates: Latitude: 36 0528 Longitude: 78 5220 Datum: NAD 84 Level of accuracy: Second Method of measurement: Map 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water,treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes No 7.Facility permitted/design flow: 30MGD and facility average daily flow: 27.3 (Both WTPs)MGD 8.Average amount of residuals being generated at this facility 611.39 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Water Treatment Process Type and volume of residuals storage (i.e., outside of residuals treatment units): Lagoon (½ Acre) II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6)as: Biological Non-Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-hazardous under RCRA:(Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non-municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: yes no. If yes, list the number(s): b.Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR§261.21- 261.24: yes no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental Laboratories and Date of analysis: 02/28/2018 Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) oo Passed ignitability test: yes no. Flashpoint: F (> 140F) Passed reactivity test: yes no. HCN: mg/kg (<250) & HS: mg/kg (<500) 2 TCLP Parameter Limit Result TCLP Parameter Limit Result (mg/l) (mg/l) (mg/l) (mg/l) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 DN FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 4/15/2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mg/kg) (mg/kg) (mg/kg) Arsenic 75 41 <12.5 Cadmium 85 39 2.99 Copper 4,300 1,500 354 Lead 840 300 <7.50 Mercury 57 17 <0.0740 Molybdenum 75 n/a <6.25 Nickel 420 420 31.6 Selenium 100 100 <12.5 Zinc 7,500 2,800 76 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Arsenic Chromium Nickel Unit to Boundary to Closest Property Line (meters, check one) (mg/kg) (mg/kg) (mg/kg) > 0 but < 25 30 200 210 34 220 240 39 260 270 46 300 320 53 360 390 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 20 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 4/15/2020 Parameter Result (mg/kg) Aluminum 9050 Ammonia-Nitrogen1200 Calcium <625 Magnesium 302 Nitrate-Nitrite Nitrogen<23.8 pH (Standard Unit) 5.4 Phosphorus 815 Potassium 171 Sodium <625 Total Kjeldahl Nitrogen 12700 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.30 \[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth\]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): default value, or actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: st ) Year PAN Application Method First (1Five-Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 5,224 7,700 Injection/Incorporation 5,824 8,300 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp.density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non-biological residuals): Alternative 1 \[15A NCAC 02T.1106(b)(3)(A)\] - Time/Temperature Compliance. Alternative 2 \[15A NCAC 02T.1106(b)(3)(B)\] - Alkaline Treatment. Alternative 3 \[15A NCAC 02T.1106(b)(3)(C)\]-Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 \[15A NCAC 02T.1106(b)(3)(D)\] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 \[15A NCAC 02T.1106(b)(3)(E)-(K)\] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, gamma ray irradiation, or pasteurization. b. For Land Application of Class B: Alternative 1 \[15A NCAC 02T.1106(c)(1)\] - Fecal Coliform Density Demonstration. Alternative 2 \[15A NCAC 02T.1106(c)(2)\] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, air drying, anaerobic digestion, composting, or lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt - If Daily Cover Alternative is chosen in Item II.8. below \[15A NCAC 02T.1106(a)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 \[15A NCAC 02T.1107(a)(1)\] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 \[15A NCAC 02T.1107(a)(2)\] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 \[15A NCAC 02T.1107(a)(3)\] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 \[15A NCAC 02T.1107(a)(4)\] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 \[15A NCAC 02T.1107(a)(5)\] - 14-Day Aerobic Processes. Alternative 6 \[15A NCAC 02T.1107(a)(6)\] - Alkaline Stabilization. Alternative 7 \[15A NCAC 02T.1107(a)(7)\] - Drying of Stabilized Residuals. Alternative 8 \[15A NCAC 02T.1107(a)(8)\] - Drying of Unstabilized Residuals. Alternative 9 \[15A NCAC 02T.1107(a)(9)\] - Injection. Alternative 10 \[15A NCAC 02T.1107(a)(10)\] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover \[15A NCAC 02T.1107(b)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 is pumped to Sanitary Sewer System. is Wasted to Lagoon 2. Lagoon 2 Liquid Sludge is Wasted to Thickener. It is sent to Synagro Belt Press. Filtrate Filters and Flows to Leaves Basins Settled Water Flocculators and Sedimentation Basins Water and sent through Coagulant is added to Raw Raw Water Enters Plant Filtered BROWN WATER TREATMENT PLANT PROCESS FLOW DIAGRAM Water Flows to Clearwells Finished Water is City from Clearwells Pumped to Residuals Sampling Plan City of Durham Land Application Program Brown WTP Nutrients and Metals Analysis Sampling Point:Dewatering Press Sampling Frequency: 4/yr Sample Type: Composite Lab: Waypoint Analytical Pathogen Reduction Sampling Point: Dewatering Press Sampling Frequency: 4/yr Sample Type: Grab – Fecal Coliform tests Lab: Meritech TCLP Sampling Point: Dewatering Press Sampling Frequency: Annually Sample Type: Composite Lab: Summit Environmental Technologies, Inc Mbcpsbupsz(t!mjbcjmjuz!jo!boz!dmbjn!sfmbujoh!up!bobmztft!qfsgpsnfe!tibmm!cf!mjnjufe!up-!bu!mbcpsbupsz(t!pqujpo-!sfqfbujoh!uif! bobmztjt!jo!rvftujpo!bu!mbcpsbupsz(t!fyqfotf-!ps!uif!sfgvoe!pg!uif!dibshft!qbje!gps!qfsgpsnbodf!pg!tbje!bobmztjt/! ! 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ZftOp Tbnqmft!xfsf!dpotjefsfe!bddfqubcmf!bt!dppmjoh! qspdftt!ibe!cfhvo/ ZftOpO0B Xbufs!.!Tbnqmf!dpoubjofst!qspqfsmz!qsftfswfe OpO0B Xbufs!.!WPB!wjbmt!gsff!pg!ifbetqbdfZft ZftOpO0B Usjq!Cmbolt!sfdfjwfe!xjui!WPBt ZftOpO0B Tpjm!WPB!nfuipe!6146!—!dpnqmjbodf!dsjufsjb!nfu Ijhi!dpodfousbujpo!dpoubjofs!)59!is*Mpx!dpodfousbujpo!FoDpsf!tbnqmfst!)59!is* Ijhi!dpodfousbujpo!qsf.xfjhife!)nfuibopm!.25!e*Mpx!dpod!qsf.xfjhife!wjbmt!)Tpe!Cjt!.25!e* Tqfdjbm!qsfdbvujpot!ps!jotusvdujpot!jodmvefe@ZftOp Dpnnfout; Tjhobuvsf;Csboej!XbutpoEbuf!'!Ujnf;1501703131!21;42;61 Qbhf!7!pg!8 Qbhf!8!pg!8 SummitEnvironmentalTechnologies,Inc. 3310 WinSt. CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com May 06, 2020 RyanCopeland Synagro 284BogerRd. Mocksville,NC 27028 TEL:(336) 998-7150 FAX: (336) 998-8450 RE: DurhamBrown OrderNo.:20041280 DearRyanCopeland: Summit EnvironmentalTechnologies,Inc.received 1 sample(s) on 4/24/2020forthe analyses presentedinthefollowingreport. Therewere no problemswiththeanalyticaleventsassociatedwiththisreport unless noted intheCaseNarrative. Qualitycontrol dataiswithinlaboratory definedormethod specifiedacceptancelimits exceptwhere noted. Ifyou haveany questionsregardingthesetestsresults, pleasefeelfreetocallthe laboratory. Sincerely, Jennifer Woolf ProjectManager 3310 Win St. Cuyahoga Falls,Ohio44223 Arkansas88-0735,California2943,Colorado,ConnecticutPH-0108,FloridaNELACE87688,IdahoOH00923,Illinois200061,IndianaC-OH-13,Kansas E-10347,Kentucky(UndergroundStorageTank)3,Kentucky90146, Maryland339,Michigan9988, Minnesota1780279,NevadaOH009232020-1,New Hampshire2996,New JerseyOH006,NewYork11777,NorthCarolina39705and631,NorthDakotaR-201,OhioDW,OhioVAPCL0052,Oklahoma 2019-155,OregonOH200001,Pennsylvania011,RhodeIslandLA000317,SouthCarolina92016001,TexasT104704466-19-16,UtahOH009232020-12, VirginiaVELAP10381,WestVirginia9957C Page 1 of 31 SummitEnvironmentalTechnologies,Inc. CaseNarrative 3310 WinSt. CuyahogaFalls,Ohio44223 WO#: 20041280 TEL:(330)253-8211FAX:(330)253-4489 Date: 5/6/2020 Website:http://www.settek.com CLIENT:Synagro Project:DurhamBrown Thisreportinitsentiretyconsists ofthefollowingdocuments:CoverLetter,CaseNarrative,Analytical Results,QCSummaryReport,ApplicableAccreditationInformation,Chain-of-Custody,Cooler ReceiptForm,and otherapplicableformsas necessary.All documentscontaintheSummit Environmental Technologies,Inc.,WorkOrderNumberassignedtothisreport. Summit Environmental Technologies,Inc., holdstheaccreditations/certificationslistedatthe bottomof thecoverletterthatmay ormaynot pertaintothisreport.Pleaserefertothe"AccreditationProgram AnalytesReport"foraccreditedanalyteslist. Theinformationcontainedinthisanalyticalreportisthesole property ofSummitEnvironmental Technologies,Inc.andthat ofthecustomer.Itcannot bereproducedinanyformwithouttheconsent of Summit Environmental Technologies,Inc. orthecustomerforwhichthisreportwasissued. Theresults containedinthisreportare onlyrepresentative ofthesamplesreceived.Conditionscan varyat different timesandat different samplingconditions.SummitEnvironmental Technologies,Inc.is notresponsible for useorinterpretation ofthe dataincluded herein. AllresultsforSolidSamplesarereported on an"asreceived" or"wetweight" basis unlessindicatedas "dryweight" usingthe"-dry" designation on thereportingunits. Thisreportis believedtomeetall oftherequirements oftheaccreditingagency,whereapplicable.Any comments or problemswiththeanalyticaleventsassociatedwiththisreportare noted below. PrepCommentsforHGPrep_(7470),Samplemb2-43232: 22.5 ml ofKMnO4added. Original Page 2 of 31 SummitEnvironmentalTechnologies,Inc. QualifiersandAcronyms 3310 WinSt. CuyahogaFalls,Ohio44223 WO#: 20041280 TEL:(330)253-8211FAX:(330)253-4489 Date: 5/6/2020 Website:http://www.settek.com ThesecommonlyusedQualifiersandAcronymsmayormaynotbepresentinthis report. Qualifiers Thecompoundwasanalyzedforbutwasnotdetected. U ThereportedvalueisgreaterthantheMethodDetectionLimitbutlessthantheReportingLimit. J HTheholdtimeforsamplepreparationand/oranalysiswasexceeded. Theresultisreportedfromadilution. D Theresultexceededthelinearrangeofthecalibrationorisestimatedduetointerference. E Theresultisbelowthe MinimumCompound Limit. MC *TheresultexceedstheRegulatoryLimitorMaximumContaminationLimit. Manualintegrationwasusedtodeterminethearearesponse. m Manualintegrationinwhichpeakwasdeleted d TheresultispresumptivebasedonaMassSpectrallibrarysearchassuminga1:1response. N PThesecondcolumnconfirmationexceeded25%difference. TheresulthasbeenconfirmedbyGC/MS. C TheresultwasnotconfirmedwhenGC/MSAnalysiswasperformed. X Theanalytewasdetectedintheassociatedblank. B/MB+ GTheICBorCCBcontainedreportableamountsofanalyte. TheCCVrecoveryfailedlow(-)orhigh(+). QC-/+ TheRPDwasoutsideofacceptedrecoverylimits. R/QDR TheLCSorLCSDrecoveryfailedlow(-)orhigh(+). QL-/+ QLRTheLCS/LCSDRPDwasoutsideofacceptedrecoverylimits. TheMSorMSDrecoveryfailedlow(-)orhigh(+). QM-/+ TheMS/MSDRPDwasoutsideofacceptedrecoverylimits. QMR TheICVrecoveryfailedlow(-)orhigh(+). QV-/+ SThespikeresultwasoutsideofacceptedrecoverylimits. Deviation;Adeviationfromthemethodwasperformed; PleaserefertotheCaseNarrativefor Z additionalinformation Acronyms NDNotDetectedRLReportingLimit QualityControlMethodDetectionLimit QCMDL MBMethodBlankLODLevelofDetection LaboratoryControl SampleLevelofQuantitation LCSLOQ LaboratoryControl SampleDuplicatePracticalQuantitationLimit LCSDPQL QualityControl SampleContractRequiredQuantitationLimit QCSCRQL DUPDuplicatePLPermitLimit Matrix SpikeRegulatoryLimit MSRegLvl Matrix SpikeDuplicateMaximumContaminationLimit MSDMCL RelativePercentDifferentMinimumCompoundLimit RPDMinCL InitialCalibrationVerificationReanalysis ICVRA ICBInitialCalibrationBlankREReextraction ContinuingCalibrationVerificationTentativelyIdentifiedCompound CCVTIC CCBContinuingCalibrationBlankRTRetentionTime ReportingLimitCheckCalibration Factor RLCCF DilutionFactorResponseFactor DFRF ThislistofQualifiersandAcronymsreflects themostcommonlyutilizedQualifiersandAcronyms forreporting. Pleasereferto theAnalyticalNotesintheCaseNarrative foranyQualifiersorAcronymsthatdonotappearin this list orforadditionalinformationregarding theuseof theseQualifiersonreporteddata. Original Page 3 of 31 SummitEnvironmentalTechnologies,Inc. Workorder 3310 WinSt. SampleSummary CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 20041280 Website:http://www.settek.com 06-May-20 CLIENT:Synagro Project:DurhamBrown TagNo Lab SampleIDClient SampleIDDateCollectedDateReceivedMatrix 20041280-001Durham BrownWTP4/23/202011:30:00AM4/24/202010:10:00AMSludge Page 4 of 31 te a PMPMPMPMPMPMPM AMAM AMAMAM al D 0 n 0000 20 i s 000045460000 -0 0000 00 i ::::::: :: g y s RT i 0:9:9: a y r 00074931273809 l 30732 00 ::::::: ::::: a 312173 M 1 O O 86 99 - 10 0000000 0 20041280 An 2222222 P 2 06 0000000 0 2222222 2 ////// E / 111144 2 ///// / / 555555 5 R 4/30/ 4/29/20204/27/20204/27/2020 #: 4/30/2020 O S W PMAMPMPMPM AM TE 0000000000 ::::: 00 : 0040000000 ::::: 55 2:9112 DA 9 te a D p re 4/29/20205/1/20204/30/20204/30/20204/30/20204/29/2020 P PMPMPMPMPM 0000000000 ::::: te0000000000 ::::: a 22222 D e t a 20202020202020202020 5) h ///// 9 c 99999 a 22222 ///// 90 44444 : Le id 846 ol - W )-S 1030) 1311/8081) 2 : . (S s 1311/7470) i W 3 t s . 1311/6010)1311/6010) s W y 3 846e(S 8321B l . - WW a (S T s i A n /7.3.4.2 s Ws (S(S s is ) i P s A y 4sss id l (S E iiy y 3s a u ss l s e y 0 al 9014/7 n q al d ( ilyly bi 9n i n t A ( aa l L e s a A Ann o s e e d e is e Sol dd AA0) ey ie i d n r f 7l fi ss c a l u Fr -V o 2 c i y i c u rbiati t rtaltal y l r S e sm eee C t it e me 9045D) ee l l ee i a HMMMPSVo vv age 5 of 31 FW bi N a PPPPPPP 1311/8 c. t (S P ntLLLLLLL 23 sactiacti nom W nit 2 I ee CCCCCCC ai H g ,4 in St.4489 PpRRTTTTTT(ST TeI - s 4 e W 0 ettek.c 253 hio 1 s ) 3 O 3 , ix s ge hnologi 330 r ( t all ec : aud //www. l F: T X S M l A a t F http n : e ahoga te m i y s 8211 u - onb C r vi WeAM 253 n te ) E 00 : itDa 330 n ( :30 mm 1 io t L: 1 Su E ec0 T 2 0 oll 2 C 4/23/ wn TP W ro ID n B le w p o rom r m a g a B ah S r m n t u a y n h e r SD i u l D C 001A - t: ID t: 280 le ec n 1 p e 4 oj i m 0 r a 0 ClP S2 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 20041280 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 5/6/2020 TagNumber: CLIENT:Synagro CollectionDate:4/23/202011:30:00AM Matrix:SLUDGE LabID:20041280-001A Project:DurhamBrown ClientSampleIDDurhamBrownWTP AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW7470ASW7470AMJM TCLPMERCURYANALYSIS (SW1311/7470) TCLPMercuryND0.00200mg/L15/1/20201:07:00 PM Analyst: TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW6010DEAM TCLPMETALSANALYSIS (SW1311/6010) TCLP Arsenic(As)ND0.500mg/L15/1/20201:31:46 PM TCLP Barium(Ba)ND5.00mg/L15/1/20201:31:46 PM TCLPCadmium(Cd)ND0.100mg/L15/1/20201:31:46 PM TCLPChromium(Cr)ND0.200mg/L15/1/20201:31:46 PM TCLPLead(Pb)ND0.500mg/L15/1/20201:31:46 PM TCLP Selenium(Se)ND0.0500mg/L15/1/20201:31:46 PM TCLP Silver(Ag)ND0.500mg/L15/1/20202:49:45 PM Analyst: TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW8270SW3510CSFG TCLPSEMI-VOLATILESANALYSIS(SW1311/8270) 1,4-DichlorobenzeneND0.200mg/L25/4/20203:38:00 PM 2,4,5-TrichlorophenolND0.500mg/L25/4/20203:38:00 PM 2,4,6-TrichlorophenolND0.500mg/L25/4/20203:38:00 PM 2,4-DinitrotolueneND0.100mg/L25/4/20203:38:00 PM Cresols,TotalND10.0mg/L25/4/20203:38:00 PM Hexachloro-1,3-butadieneND0.0400mg/L25/4/20203:38:00 PM HexachlorobenzeneND0.100mg/L25/4/20203:38:00 PM HexachloroethaneND0.200mg/L25/4/20203:38:00 PM NitrobenzeneND0.200mg/L25/4/20203:38:00 PM PentachlorophenolND0.500mg/L25/4/20203:38:00 PM PyridineND0.500mg/L25/4/20203:38:00 PM Surr:2-Fluorophenol85.610-109%Rec25/4/20203:38:00 PM Surr: Phenol-d685.210-109%Rec25/4/20203:38:00 PM Surr:Nitrobenzene-d572.719-120%Rec25/4/20203:38:00 PM Surr:2,4,6-Tribromophenol11610-120%Rec25/4/20203:38:00 PM Surr:2-Fluorobiphenyl86.122-117%Rec25/4/20203:38:00 PM Surr:p-Terphenyl-d1412334-116S%Rec25/4/20203:38:00 PM BAnalytedetectedinthe associatedMethod BlankEValue abovequantitationrange Qualifiers: HHolding timesforpreparationor analysisexceededMManualIntegrationusedtodetermine arearesponse MCValue isbelowMinimum CompoundLimit.NTentatively identified compounds NDNotDetectedPSecond column confirmation exceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal<MDL Page 6 of 31 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 20041280 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 5/6/2020 TagNumber: CLIENT:Synagro CollectionDate:4/23/202011:30:00AM Matrix:SLUDGE LabID:20041280-001A Project:DurhamBrown ClientSampleIDDurhamBrownWTP AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW8081SW3510CMES TCLPPESTICIDESANALYSIS(SW1311/8081) Chlordane, totalND0.125mg/L55/4/20207:27:00 PM ToxapheneND0.250mg/L55/4/20207:27:00 PM EndrinND0.0125mg/L55/4/20207:27:00 PM gamma-BHCND0.0125mg/L55/4/20207:27:00 PM HeptachlorND0.0125mg/L55/4/20207:27:00 PM HeptachlorepoxideND0.0125mg/L55/4/20207:27:00 PM MethoxychlorND0.0125dmg/L55/4/20207:27:00 PM Surr:TCMX19.610-119%Rec55/4/20207:27:00 PM Surr:DCB18.210-119%Rec55/4/20207:27:00 PM Analyst: TCLPHERBICIDES BY EPA8321BSW8321ASW1311MBJH 2,4-DND0.500mg/L505/2/20206:32:00 AM 2,4,5-TPND0.500mg/L505/2/20206:32:00 AM Surr:2,4-Dichlorophenylaceticacid10570-130%Rec505/2/20206:32:00 AM Analyst: TCLPMETALS, VOC, BNA, PEST,HERB-SOLIDSW8260SW1311MRMT TCLPVOLATILESANALYSIS 1,1-DichloroetheneND0.250mg/L504/30/20201:09:00 PM 1,2-DichloroethaneND0.250mg/L504/30/20201:09:00 PM MEKND5.00mg/L504/30/20201:09:00 PM BenzeneND0.250mg/L504/30/20201:09:00 PM Carbon tetrachlorideND0.250mg/L504/30/20201:09:00 PM ChlorobenzeneND2.50mg/L504/30/20201:09:00 PM ChloroformND0.250mg/L504/30/20201:09:00 PM TetrachloroetheneND0.250mg/L504/30/20201:09:00 PM TrichloroetheneND0.250mg/L504/30/20201:09:00 PM VinylchlorideND0.100mg/L504/30/20201:09:00 PM Surr:4-Bromofluorobenzene91.270-130%Rec504/30/20201:09:00 PM Surr:Dibromofluoromethane10270-130%Rec504/30/20201:09:00 PM Surr:Toluene-d899.970-130%Rec504/30/20201:09:00 PM BAnalytedetectedinthe associatedMethod BlankEValue abovequantitationrange Qualifiers: HHolding timesforpreparationor analysisexceededMManualIntegrationusedtodetermine arearesponse MCValue isbelowMinimum CompoundLimit.NTentatively identified compounds NDNotDetectedPSecond column confirmation exceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal<MDL Page 7 of 31 SummitEnvironmentalTechnologies,Inc. AnalyticalReport 3310 WinSt. (basereport) CuyahogaFalls,Ohio44223 WO#: 20041280 TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com DateReported: 5/6/2020 TagNumber: CLIENT:Synagro CollectionDate:4/23/202011:30:00AM Matrix:SLUDGE LabID:20041280-001A Project:DurhamBrown ClientSampleIDDurhamBrownWTP AnalysesResultQualUnitsDFDateAnalyzed RL Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9014MS REACTIVE CYANIDE (9014/7.3.3.2)-SOLID Cyanide,ReactiveND0.490mg/Kg14/27/20209:09:00 AM Analyst: PAINTFILTERFREELIQUIDSTEST (SW-846:9095)SW9095DHC FreeLiquidpass14/29/20208:30:00 AM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW1030AJT IGNITABILITYOF SOLIDS (SW-846:1030) Ignitabilitynon-flammablemm/sec15/1/20203:00:00 PM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9045DDHC PH (SW9045D) pH6.1s.u.@21.9C14/30/202010:07:00 AM Analyst: RCI-SOLID-W/ IGNITABILITY1030SW9034MS REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide,ReactiveND25.0mg/Kg14/27/20209:09:00 AM BAnalytedetectedinthe associatedMethod BlankEValue abovequantitationrange Qualifiers: HHolding timesforpreparationor analysisexceededMManualIntegrationusedtodetermine arearesponse MCValue isbelowMinimum CompoundLimit.NTentatively identified compounds NDNotDetectedPSecond column confirmation exceeds PLPermitLimitRRPDoutside acceptedrecoverylimits Original RLReportingDetectionLimitUSampleswith CalcVal<MDL Page 8 of 31 SummitEnvironmentalTechnologies,Inc. AccreditationProgram 3310 WinSt. AnalytesReport CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 20041280 Website:http://www.settek.com 06-May-20 Client:SynagroState:NW Project:DurhamBrownProgramName:NC_WW_SCM SampleIDMatrixTestNameAnalyteStatus SludgeIgnitabilityofSolids(SW-846:1030)IgnitabilityA 20041280-001A SludgePaintFilterFreeLiquidsTest(SW-846:9095)FreeLiquidN SludgepH(SW9045D)HydrogenIon(pH)A SludgeReactive Cyanide(9014/7.3.3.2)-SolidCyanide, ReactiveN SludgeReactiveSulfide(9034)/7.3.4.2Sulfide, ReactiveN SludgeTCLPHerbicidesbyEPA8321B2,4,5-TPA SludgeTCLPHerbicidesbyEPA8321B2,4-DA SludgeTCLPMercuryAnalysis(SW1311/7470)MercuryA SludgeTCLPMetalsAnalysis(SW1311/6010)ArsenicA SludgeTCLPMetalsAnalysis(SW1311/6010)BariumA SludgeTCLPMetalsAnalysis(SW1311/6010)CadmiumA SludgeTCLPMetalsAnalysis(SW1311/6010)ChromiumA SludgeTCLPMetalsAnalysis(SW1311/6010)LeadA SludgeTCLPMetalsAnalysis(SW1311/6010)SeleniumA SludgeTCLPMetalsAnalysis(SW1311/6010)SilverA SludgeTCLPPesticidesAnalysis(SW1311/8081)Chlordane, totalA SludgeTCLPPesticidesAnalysis(SW1311/8081)EndrinA SludgeTCLPPesticidesAnalysis(SW1311/8081)gamma-BHCA SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorA SludgeTCLPPesticidesAnalysis(SW1311/8081)HeptachlorepoxideA SludgeTCLPPesticidesAnalysis(SW1311/8081)MethoxychlorA SludgeTCLPPesticidesAnalysis(SW1311/8081)ToxapheneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)1,4-DichlorobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,5-TrichlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4,6-TrichlorophenolA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)2,4-DinitrotolueneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)Cresols,TotalA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachlorobutadieneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)HexachloroethaneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)NitrobenzeneA SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PentachlorophenolA KeyKey NC_WW_SCMAAccreditedNC_WW_SCMNNotAccredited Original#1 Page 9 of 31 SummitEnvironmentalTechnologies,Inc. AccreditationProgram 3310 WinSt. AnalytesReport CuyahogaFalls,Ohio44223 TEL:(330)253-8211FAX:(330)253-4489 WO#: 20041280 Website:http://www.settek.com 06-May-20 Client:SynagroState:NW Project:DurhamBrownProgramName:NC_WW_SCM SampleIDMatrixTestNameAnalyteStatus SludgeTCLPSemi-VolatilesAnalysis(SW1311/8270)PyridineA 20041280-001A SludgeTCLPVolatilesAnalysis1,1-DichloroetheneA SludgeTCLPVolatilesAnalysis1,2-DichloroethaneA SludgeTCLPVolatilesAnalysis2-ButanoneA SludgeTCLPVolatilesAnalysisBenzeneA SludgeTCLPVolatilesAnalysisCarbon tetrachlorideA SludgeTCLPVolatilesAnalysisChlorobenzeneA SludgeTCLPVolatilesAnalysisChloroformA SludgeTCLPVolatilesAnalysisTetrachloroetheneA SludgeTCLPVolatilesAnalysisTrichloroetheneA SludgeTCLPVolatilesAnalysisVinyl chlorideA KeyKey NC_WW_SCMAAccreditedNC_WW_SCMNNotAccredited Original#1 Page 10 of 31 al n i g i ual r Q O 80 20 - RT y a it 412 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r p 1124312758003 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43209 o o M f y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 20202020 it // Q m i 130130130 S 2930 H PL // L MC 44 gh i H e:e: t t it DaDa se 707070 m s i i on L s rep p y w s l P e r Lo na a A e r a e .2 ds EC in 100100 R ee 97 m c r % x e t e ge e n n d a o r o it t /L ati n dm g o i em r s L m i ati al u f n n n o o f V ntit o ts: 1311M i a c u atinecti W Re t r q Un e m S g age 11 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPK ,4b in St.4489 l - s 4 tin a C-M e W r end o O 0o u ettek.c 253 l p hioc 1 ue000000 s V l a e ... ) e - 3 O a VManuaSR 3 P , v 8260 505050 s L hnologi 330 ( K W C all ec : //www. P TS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y s s 8211 T QL u - onb 100 e . C P r 0500 T 0. vi 0050000500005000050000500005000050000200 We . ...0.... 253 nk n 00000000 a ) El B it 330 d ( its o mm m th L: i e l Su lt E .6.1.2 its u Tn M NDNDNDNDNDNDNDNDNDND s LK o m 485050 d i e B l e ati R y M43209 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd ne t e t rom ene eeu e tt a z ha o g yy t D ll ah e aat r n nn PD u m y AANoR SD deuoroben uoro il l f f J BR o or ND o l B-43209 henehane BSh m m tt hene t c MP ro ene uene-d8 de l hene ra i z bro B t t: i o s D: oroeoroe e llor oroe 4-DT l en Il oe t orm hh D: t: ::: r h bf eneh ier n cc l te f t:iio oorrrrrr c e t I l o c p ec y l uuu lza n DD h oror ry --ali rbll n m e entc SSS oj i n i u 12 EK liahh anaei er ,, r Q SCA11MBCCCTTV ClP al n i g i ualualualual r Q QQQ O 80 20 - RT y a itititit 412 20 0 O M mmmm iiii - 20 P 06 DLDLDLDL P PPP E y ov l R RRR c a e n R r und a o #: d r p 1124432759120112443275912111244327599281124432759929 e o O 32 PDPDPDPD m pt 2 n . o RRRR e W o o:o:o:o:o:o:o:o: 0 C NNNN NNNN% %%% ati qqqq nnnn r m acc a eeee e u ARY p SSSS RuRuRuRu id em rs ni p i ut r 43214 o o M f y alalalal r s w e MM e 722 o v it .l f Vf Vf Vf V mo e 1 i m b U ti ReReReRe D: L s I S i Rec DDDD it h e e PPPP ding c u m l l t r RRRR a epik C HoVPS Ba 2020202020202020 itititit //// Q 2020202020202020 //// mmmm iiii 120130130 S 301301301301 H PL //////// LLLL MC 45454545 ghghghgh iiii HHHH e:e:e:e:e:e:e:e: tttt tttt itititit DaDaDaDaDaDaDaDa se 807070 mmmm ssss iiii iiii on LLLL ssss reprepreprep p yyyy wwww s llll PPPP e r LoLoLoLo nananana a AAAA e r a e .0.2 ds ECECECEC in 104 RRRR ee 8686 m c r %%%% x e t e ge e n n d a o r o it t /L/L/L/L ati n dm gggg o i em r s L mmmm i 0 ati alalalal u f n n n o o f Vf Vf Vf V ntit o ts:ts:ts:ts: 3010A3010A3010A3010A iiii a c u atinecti WWWW ReReReRe 001200001200 t r q .. Un UnUnUn e m SSSS g age 12 of 31 00 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPKSPKSPK ,4b in St.4489 l - s 4 tin a -7(6-7(6-7(6-7(6 e W r end PPPP o 0o u ettek.c 253 l p hio LLLL c 1 ueue00ue00ue00 s llll a e ) e 3 000 O CCCC aaaa ... VManuaSR 3 , TTTT vvvv 6010D6010D6010D6010D 222 s ---- hnologi llll 330 tttt ( KKKK WWWW all ec : //www. PPPP MSMSMSMS P E M F: T RL X SSSS l A e:e:e:e: a t F http dddd No:No:No:No: n oooo : e stststst ahoga CCCC te m eeee tttt i y s ssss T 8211 TTT QLQLQLQL u - onb 500500500500 eeee ... . C PPPP r TTTT 0000 vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt ltltlt E its uuuu 077273 Tn M ... ND ssss LK o m 211 d i eeee BSD l e CS ati RRRR y M43214L43214MS43214M43214 r e ciat ntit o a D:D:D:D: ov pe:pe:pe:pe: ss c I I I I yyyy qu e hhhh a r TTTT e cccc w ptptptpt d h o e aaaa t mmmm el n BBBB pt aaaa ib e SSSS c dd wn ee tt o ac r e ecec ed tt d B SD eei ct s dd t e MSM t rom eeu e AA tt a o g yy D ll ah aat r n nn PD u y AANoR SD hQChQC -43214 J BR ND SSS g)g)g)g) B-43214 BS CC AAAA MPLL20041350-004Batc20041350-004Batc er(er(er(er( : s D:vD:vD:vD:v ilililil I I I I D:D:D:D: t: eSeSeSeS ier llll tetetete f t: t It It It I pppp ec yyyy PPPP llll n ali LLLL mmmm e enenenen oj i u lililili anaanaanaana CCCC r Q SCATSCATSCATSCAT ClP al n i g i ual r Q O 80 20 - RT y a it 412 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r p 1124432759929 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43214 o o M f y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 2020 it / Q 2020 / m i S 301 H PL // L MC 45 gh i H e:e: t t it DaDa se m s i i on L s rep p y w s l P e r Lo na a A e r a e ds EC in R ee m c r % x e t e ge e n n d a o r o it t /L ati n dm g o i em r s L m i ati al u f n n n o o f V ntit o ts: 3010A i a c u atinecti W Re t r q Un e m S g age 13 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPK ,4b in St.4489 l - s 4 tin a -7(6 e W r end P o 0o u ettek.c 253 l p hio L c 1 ue s l a e ) e 3 O C a VManuaSR 3 , T v 6010D s - hnologi l 330 t ( K W all ec : //www. P MS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y s s 8211 T QL u - onb e C P r T vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt E its u Tn M s o m d i e SD l e ati R y M43214 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B SD eei ct s dd t e M t rom eeu e A tt a o g yy D ll ah aat r n nn PD u y AANoR SD hQC J BR ND 20041350-004Batc : s D: I D: t: e ier l te f t: t I p ec y l n ali m e en oj i u li ana r Q SCA ClP al n i g i C+ ual r Q Q O 80 20 - RT y a it 412 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r p 1124392758485 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43218 o o M f y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 2020 it / Q 2020 / m i 109109120120117116 S 301 H PL // L MC 45 gh i H e:e: t t it DaDa se 101019102234 m s i i on L s rep p y w s l P e r Lo na a A e r a e .3.6.8.9 ds EC in 107113 R ee 78756777 m c r % x e t e ge e n n d a o r o it t /L ati n dm g o i em r s L m i ati al u f n n n o o f V ntit o ts: 3510C i a c u atinecti W Re t r q Un e m S g age 14 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c _TSPK ,4b in St.4489 l - s 4 A tin a e W r end o 0o u ettek.c 253 l p hioc 1 ue000000000000 s l a e ) e 3 000000 O a ...... C-BN VManuaSR 3 , v 8270 111111 s O hnologi 330 ( K W all ec : //www. P SVS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y 00 s s 8211 T QL u . - onb 100250250250100100250250 e . ...5.... C P r 050002000500 T 000.0..0000 vi We 000 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt E its u 835678077913 Tn M .. NDNDNDNDNDNDNDNDNDNDNDND s LK o 7767 m ...1.1 d i e B l e 0000 ati R y M43218 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e ol t rom eeu e tt a o g yy D ll ah aat r n yl nn PD u ene y iophen AANoR SD -d14 m l ad ty phen ene-d5i ene J z bro BR ene i z ND r z-d6 l B-43218 3-bu T BS , hane uene t lal MP uorophenoluorob 6- t erphen orophenolorophenol , o roben ll to t FlFlT 4 : i eneheno hh , s D:T oroben orophenol z lccro l oro-1orobenoroe2-PN22-p- ii t I lll i hrr h D: t: ol:::::: s, ehhh ier l cnen lc TT ne tes f t:ii rrrrrrrrrrrr ccc t Ii -- o pb a ec y e uuuuuu lt n aaa DDd 56 s o i -,,-ali xxx n mr e enr SSSSSS e oj t i u 4444 lieeei anaey ,,,,-Cr r Q SCA1222oCrHHHNPP ClP al n i g i C+ ual r Q Q O 80 20 - RT y a it 412 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r p 1124392758486 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43218 o o M f y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 2020 it / Q 2020 / m i 130 132133130130130130130130130130130130130130130130130 S 301 H PL // L MC 45 gh i H e:e: t t it DaDa .4.7.1.3.9.7.4.1.5.5.1.6.8.4 se 43 341010 m . s i i 36313143323131433639173244136 on L s rep p y w s l P e r Lo na a A e r a e .2.4.6.8.4.2.1.0.6.1.6.6.3 ds EC in 101102104120118 R ee 53997979539649735385836881 m c r % x e t e ge e n n d a o r o it t /L ati n dm g o i em r s L m i 000000000000 ati al u f n n n o o f V ntit o ts: 3510C i a c u atinecti W Re t r q Un e m S g age 15 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c _TSPK ,4b in St.4489 l - s 4 A tin a e W r end o 0o u ettek.c 253 l p hioc 1 ue000000000000000000000000000000000000 s l a e ) e 3 000006000000000000 O a ....... C-BN VManuaSR 3 88888888888 , v 8270 .....1......111111 s O hnologi 330 00000000000 ( K W all ec : //www. P SVS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y 00 s s 8211 T QL u . - onb 100250250250100100250250 e . ...5.... C P r 050002000500 T 000.0..0000 vi We 000 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt E its u 2609961837276993843428513686201318 Tn M .. ND s o 487864735848868 m ..............1.1 d i e l e 000000000000000 CS ati R y L43218 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e ol t rom eeu e tt a o g yy D ll ah aat r n yl nn PD u ene y iophen AANoR SD -d14 m l ad ty phen ene-d5i ene -43218 J z bro BR ene i z ND r SSS z-d6 l 3-bu T CC , hane uene t lal LL uorophenoluorob 6- t erphen orophenolorophenol , o roben ll to t FlFlT 4 : i eneheno hh , s D:T oroben orophenol z lccro l oro-1orobenoroe2-PN22-p- ii t I lll i hrr h D: t: ol:::::: s, ehhh ier l cnen lc TT ne tes f t:ii rrrrrrrrrrrr ccc t Ii -- o pb a ec y e uuuuuu lt n aaa DDd 56 s o i -,,-ali xxx n mr e enr SSSSSS e oj t i u 4444 lieeei anaey ,,,,-Cr r Q SCA1222oCrHHHNPP ClP al n i C+g i S ual r Q Q m O 80 20 - RT y a it 412 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r p 1124392760532 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43218 o o M f y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 2020 it / Q 2020 / m i 126 144153155148148126134132158176130130130154130130156 S 301 H PL // L MC 45 gh i H e:e: t t it 5 DaDa .8.7.8.4.7.8.5.5.4 se 3986 101029201010 m .. s i i 33281220333231419348 on L s rep p y w s l P e r Lo na a A e r a e .7.4.0.0.5.6.8.0.6.7.8 ds EC in 113115114114109134128 R ee 6994936667846193947993 m c r % x e t e ge e n n d a o r o it t /L ati n dm g o i em r s L m i 000000000000 ati al u f n n n o o f V ntit o ts: 3510C i a c u atinecti W Re t r q Un e m S g age 16 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c _TSPK ,4b in St.4489 l - s 4 A tin a e W r end o 0o u ettek.c 253 l p hioc 1 ue000000000000000000000000000000000000 s l a e ) e 3 000006000000000000 O a ....... C-BN VManuaSR 3 88888888888 , v 8270 .....1......111111 s O hnologi 330 00000000000 ( K W all ec : //www. P SVS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y.0 s s 8211 T QL u - onb 200500500100500100200200500500 e . ....10..... C P r 0400 T 00000.00000 vi We 0 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt E its u 58002114552813407671304697343828 Tn M .. NDND s o 59997595689979 m .............1.1 d i e l e 00000000000000 ati R y MS43218 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e MS ol t rom eeu e A tt a o g yy D ll ah aat r n yl nn PD u ene y iophen AANoR SD -d14 m l ad ty phen ene-d5i hQCene J z bro BR ene i z ND r z-d6 l 3-bu T , hane uene t lal 20041350-002Batc uorophenoluorob 6- t erphen orophenolorophenol , o roben ll to t FlFlT 4 : i eneheno hh , s D:T oroben orophenol z lccro l oro-1orobenoroe2-PN22-p- ii t I lll i hrr h D: t: ol:::::: s, ehhh ier l cnen lc TT ne tes f t:ii rrrrrrrrrrrr ccc t Ii -- o pb a ec y e uuuuuu lt n aaa DDd 56 s o i -,,-ali xxx n mr e enr SSSSSS e oj t i u 4444 lieeei anaey ,,,,-Cr r Q SCA1222oCrHHHNPP ClP al n i C+g i ualm r Q Q m O 80 20 - RT y a it 412 303030303030303030303030 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r 00000000 p 1124392760533.9.0.1.6.1.6 e o O 65069785 PD .... m pt n 1511146117812410 o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43218 o o M f 00 y al r s w e MM e o v it l f V 5576900492089140754852809128540067648708 mo e .......... i m b U ti 0000000000 Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 2020 it / Q 2020 / m i 126 144153155148148126134132158176130130130154130130156 S 301 H PL // L MC 45 gh i H e:e: t t it DaDa .8.7.8.4.7.8 .5.5.4 se 39 1010292010101086 m .. s i i 3328122033323 1419348 on L s rep p y w s l P e r Lo na a A e r a e .4.9.0.0.5.8.6.9.0.1.1.2.6 ds EC in 101107104 125118 R ee 59998483615980974887887484 m c r % x e t e ge e n n d a o r o it t /L ati n dm g o i em r s L m i 000000000000 ati al u f n n n o o f V ntit o ts: 3510C i a c u atinecti W Re t r q Un e m S g age 17 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c _TSPK ,4b in St.4489 l - s 4 A tin a e W r end o 0o u ettek.c 253 l p hioc 1 ue000000000000000000000000000000000000 s l a e ) e 3 000006000000000000 O a ....... C-BN VManuaSR 3 88888888888 , v 8270 .....1......1 11111 s O hnologi 330 00000000000 ( K W all ec : //www. P SVS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y.0 s s 8211 T QL u - onb 200500500100500100200200500500 e . .....10.... C P r 0400 T 00000.00000 vi We 0 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt E its u 76079955729234784483 T 718142254618 n M .. NDND s o 4878648467 8878 m .......... ...1.1 d i e SD l e 00000000000000 ati R y M43218 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B SD eei ct s dd t e M ol t rom eeu e A tt a o g yy D ll ah aat r n yl nn PD u ene y iophen AANoR SD -d14 m l ad ty phen ene-d5i hQCene J z bro BR ene i z ND r z-d6 l 3-bu T , hane uene t lal 20041350-002Batc uorophenoluorob 6- t erphen orophenolorophenol , o roben ll to t FlFlT 4 : i eneheno hh , s D:T oroben orophenol z lccro l oro-1orobenoroe2-PN22-p- ii t I lll i hrr h D: t: ol:::::: s, ehhh ier l cnen lc TT ne tes f t:ii rrrrrrrrrrrr ccc t Ii -- o pb a ec y e uuuuuu lt n aaa DDd 56 s o i -,,-ali xxx n mr e enr SSSSSS e oj t i u 4444 lieeei anaey ,,,,-Cr r Q SCA1222oCrHHHNPP ClP al n i g i S ualualualual r QQQQ O 80 20 - RT y a itititit 412 0 O M mmmm iiii - 20 P 06 DLDLDLDL PPPP E y ov l RRRR c a e n R r und a o #: d r p 1124452758965112445275896711244527589691124452758994 e o O PDPDPDPD m pt n o RRRR e W o o:o:o:o:o:o:o:o: C NNNN NNNN %%%% ati qqqq nnnn r m acc a eeee e u ARY p SSSS RuRuRuRu id em rs ni p i ut r 43232 o o M f y alalalal r s w e MM e o v it l f Vf Vf Vf V mo e i m b U ti ReReReRe D: L s I S i Rec DDDD it h e e PPPP ding c u m l l t r RRRR a epik C HoVPS Ba itititit Q 20202020202020202020202020202020 //////// mmmm iiii 120125 S 11111111 H PL //////// LLLL MC 55555555 ghghghgh iiii HHHH e:e:e:e:e:e:e:e: tttt tttt itititit DaDaDaDaDaDaDaDa se 8075 mmmm ssss iiii iiii on LLLL ssss reprepreprep p yyyy wwww s llll PPPP e r LoLoLoLo nananana a AAAA e r a e .0 ds ECECECEC in 128 RRRR ee 99 m c r %%%% x e t e ge e n n d a o r o it t ati n dm o i em r s L PPMPPMPPMPPM i 00 ati alalalal u f n n n o o f Vf Vf Vf V ntit o ts:ts:ts:ts: 7470A7470A7470A7470A iiii a c u atinecti WWWW ReReReRe t r q UnUnUnUn e m SSSS g age 18 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPKSPKSPK ,4b in St.4489 l - s 4(74(74(74(74 tin a e W r end PPPP o 0o u ettek.c LLLL 253 l p hioc 1 ueue00ueue00 s llll a e ) CCCC e 3 44 O aaaa VManuaSR TTTT 3 , vvvv 7470A7470A7470A7470A ____ s 0000 hnologi 330 .. ( KKKK GGGG WWWW 00 all ec : //www. PPPP HSHSHSHS P E M F: T RL X SSSS l A e:e:e:e: a t F http dddd No:No:No:No: n oooo : e stststst ahoga CCCC te m eeee tttt i y s ssss 8211 TTTT QLQLQLQL u - onb eeee C PPPP r TTTT vi 00200002000020000200 We .... 253 nk n 0000 a ) El B it 330 d ( its o mm m th L: i e l Su ltltltlt E its uuuu T 9614 n M NDND ssss LKLK o 35 m d i eeee BB l e CS ati 0000 RRRR y .. M43232L43232M43232MS43232 r 00 e ciat ntit o a D:D:D:D: ov pe:pe:pe:pe: ss c I I I I yyyy qu e hhhh a r TTTT e cccc w ptptptpt d h o e aaaa t mmmm el n BBBB pt aaaa ib e SSSS c dd wn ee tt o ac r e -2 ecec ed tt d B eei ct s dd t e MS t rom eeu 4-30 e A tt a o g yy D ll ah aat r n NK nn PD u y A AANoR SD L B hQC -43232 J P BR ND SSS L B-43232 BSBS CC C MPLLTP20041350-004Batc uryuryuryury cccc : s D:D:D:D: erererer I I I I D:D:D:D: t: eMeMeMeM ier llll tetetete f t: t It It It I pppp ec yyyy PPPP llll n ali LLLL mmmm e enenenen oj i u lililili anaanaanaana CCCC r Q SCATSCATSCATSCAT ClP al n i g i S ualualualual r Q QQQ O 80 20 - RT y a itititit 412 20 0 O M mmmm iiii - 20 P 06 DLDLDLDL P PPP E y ov l R RRR c a e n R r und a o #: d r p 1124452758994112445275899611244527590031124452759005 e o O 94 PDPDPDPD m pt 1 n . o RRRR e W o o:o:o:o:o:o:o:o: 0 C NNNN NN%NN %%% ati qqqq nnnn r m acc a eeee e u ARY p SSSS RuRuRuRu id em rs ni p i ut r 43232 o o M f y alalalal r s w e MM e o v it l f Vf Vf Vf V 0514 mo e i m 0 b U ti . ReReReRe D: L s 0 I S i Rec DDDD it h e e PPPP ding c u m l l t r RRRR a epik C HoVPS Ba itititit Q 20202020202020202020202020202020 //////// mmmm iiii 125 S 11111111 H PL //////// LLLL MC 55555555 ghghghgh iiii HHHH e:e:e:e:e:e:e:e: tttt tttt itititit DaDaDaDaDaDaDaDa se 75 mmmm ssss iiii iiii on LLLL ssss reprepreprep p yyyy wwww s llll PPPP e r LoLoLoLo nananana a AAAA e r a e ds ECECECEC in 129 RRRR ee m c r %%%% x e t e ge e n n d a o r o it t ati n dm o i em r s L PPMPPMPPMPPM i 0 ati alalalal u f n n n o o f Vf Vf Vf V ntit o ts:ts:ts:ts: 7470A7470A7470A7470A iiii a c u atinecti WWWW ReReReRe t r q Un UnUnUn e m SSSS g age 19 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPKSPKSPK ,4b in St.4489 l - s 4(74(74(74(74 tin a e W r end PPPP o 0o u ettek.c LLLL 253 l p hioc 1 ueue00ueue s llll a e ) CCCC e 3 4 O aaaa VManuaSR TTTT 3 , vvvv 7470A7470A7470A7470A ____ s 00 hnologi 330 . ( KKKK GGGG WWWW 0 all ec : //www. PPPP HSHSHSHS P E M F: T RL X SSSS l A e:e:e:e: a t F http dddd No:No:No:No: n oooo : e stststst ahoga CCCC te m eeee tttt i y s ssss T 8211 TTT QLQLQLQL u - onb eeee C PPPP r TTTT vi 002000020000200 We .. . 253 nk n 000 a ) El B it 330 d ( its o mm m th L: i e l Su lt ltltlt E its uuuu T 15 n M NDND ssss LKLK o 5 m d i eeee SDBB l e ati 00 RRRR y . MS43232M43232M43232M43232 r 0 e ciat ntit o a D:D:D:D: ov pe:pe:pe:pe: ss c I I I I yyyy qu e hhhh a r TTTT e cccc w ptptptpt d h o e aaaa t mmmm el n BBBB pt aaaa ib e SSSS c dd wn ee tt o ac r e ecec 1-1-ed tt d B SD eei ct s 5-5- dd t e MSM t rom eeu 12 e AA tt a o g yy D ll ah aat r n NKNK nn PD u y AA AANoR SD LL BB hQChQC J PP BR ND LL BSBS CC 20041350-004Batc20041350-004BatcTPTP uryuryury ccc : s D:D:D:D: ererer I I I I D:D:D:D: t: eeMeMeM ier llll tetetete f t: t It It It I pppp ec yyyy PPP llll n ali LLL mmmm e enenenen oj i u lililili anaanaanaana CCC r Q SCASCATSCATSCAT ClP al n i g i ual r Q O 80 20 - RT y a it 412 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r p 1124452759012 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs ni p i ut r 43232 o o M f y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba it Q 20202020 // m i S 11 H PL // L MC 55 gh i H e:e: t t it DaDa se m s i i on L s rep p y w s l P e r Lo na a A e r a e ds EC in R ee m c r % x e t e ge e n n d a o r o it t ati n dm o i em r s L PPM i ati al u f n n n o o f V ntit o ts: 7470A i a c u atinecti W Re t r q Un e m S g age 20 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPK ,4b in St.4489 l - s 4(74 tin a e W r end P o 0o u ettek.c L 253 l p hioc 1 ue s l a e ) C e 3 O a VManuaSR T 3 , v 7470A _ s hnologi 330 ( K G W all ec : //www. P HS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y s s 8211 T QL u - onb e C P r T vi 00200 We . 253 nk n 0 a ) El B it 330 d ( its o mm m th L: i e l Su lt E its u Tn M ND s LK o m d i e B l e ati R y M43232 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e t rom eeu e tt a o g yy D ll ah aat r n nn PD u y AANoR SD J BR ND B2-43232 BS MP ury c : s D: er I D: t: eM ier l te f t: t I p ec y P l n ali L m e en oj i u li ana C r Q SCAT ClP al n i g i ual r Q O 80 20 - RT y a it 412 20 0 O M m i - 20 P 06 DL P E y ov l R c a e n R r und a o #: d r 0 p 1123102753993 e o O PD m pt n o R e W o o:o: C N N % ati q n r m acc a e e u ARY p S Ru id em rs 112310 ni p i ut r R o o M f 0 y al r s w e MM e o v it l f V mo e i m b U ti Re D: L s I S i Rec D it h e e P ding c u m l l t r R a epik C HoVPS Ba 2020 it / Q m i S 29 H PL / L MC 4 gh i H e:e: t t it DaDa se m s i i on L s rep p y w s l P e r Lo na a A e r a e ds EC in R ee m c r % x e t e ge e n n d a o r o it t ati n dm o i em r s L i ati al u f n n n o o f V ntit o ts: i a c u atinecti Re t r q Un e m g age 21 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPK ,4b in St.4489_S l - s 4 tin d a e W i r end o 0o u ettek.c 253 l p hioc 1 quue s l a e i ) e 3 O a L VManuaSR 3 , v 9095 s hnologi 330 ee ( K W all ec : //www. P FrS P E M F: T RL X S l A e: a t F http d No: n o : e st ahoga C te m e t i y s s 8211 T QL u - onb e C P r T vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt E its uss Tn M s o m d i e pa l e ati R y DUPR112310 r e ciat ntit o a D: ov pe: ss c I y qu e h a r T e c w pt d h o e a t m el n B pt a ib e S c dd wn ee tt o ac r e ecec ed tt d B eei ct WT s dd t e DUP t rom eeu n e A tt a o g yy w D ll ah aat r n ro nn PD u y B AANoR SD m a J BR ND urh 20041280-001D : id s D: I D:qu t: i e ier l te f t: L t I p ec y l n e ali m e en oj e i u li ana r r Q SCAF ClP al n i g i ualualualual r QQQQ O 80 20 - RT y a itititit 412 0 O M mmmm iiii - 20 P 06 DLDLDLDL PPPP E y ov l RRRR c a e n R r und a o #: d r p 1123232754426112323275442711232327544291123232754434 e o O PDPDPDPD m pt n o RRRR e W o o:o:o:o:o:o:o:o: C NNNN NNNN %%%% ati qqqq nnnn r m acc a eeee e u ARY p SSSS RuRuRuRu id em rs 112323 ni p i ut r R o o M f y alalalal r s w e MM e o v it l f Vf Vf Vf V mo e i m b U ti ReReReRe D: L s I S i Rec DDDD it h e e PPPP ding c u m l l t r RRRR a epik C HoVPS Ba 2020202020202020 itititit //// Q mmmm iiii 115135125 S 27272727 H PL //// LLLL MC 4444 ghghghgh iiii HHHH e:e:e:e:e:e:e:e: tttt tttt itititit DaDaDaDaDaDaDaDa se 856575 mmmm ssss iiii iiii on LLLL ssss reprepreprep p yyyy wwww s llll PPPP e r LoLoLoLo nananana a AAAA e r a e .4.0.8 ds ECECECEC in RRRR ee 948189 m c r %%%% x e t e ge e n n d a o r o it t /L/L/L/L ati n dm gggg o i em r s L mmmm i 000 ati alalalal u f n n n o o f Vf Vf Vf V ntit o ts:ts:ts:ts: iiii a c u atinecti ReReReRe t r q UnUnUnUn e m g age 22 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPKSPKSPK ,4b in St.4489 l - s 4 tin a e W r ReaReaReaRea end ,,,, o 0o u ettek.c 253 eeee l p hioc 1 ueue00ue00ue00 s llll a e .. )dddd e 3 0 iiii O aaaa VManuaSR 3 5 , nnnn vvvv 9014901490149014 10.10 s aaaa hnologi 330 0 ( KKKK yyyy WWWW all ec : //www. PPPP CSCSCSCS P E M F: T RL X SSSS l A e:e:e:e: a t F http dddd No:No:No:No: n oooo : e stststst ahoga CCCC te m eeee tttt i y s ssss 8211 TTTT QLQLQLQL u - onb 485495500485 eeee .... C PPPP r TTTT 0000 vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su ltltltlt E its uuuu 4498 Tn M .. ND ND ssss LK o m 98 d i eeee B l LC e CS ati RRRR y MR112323LR112323RR112323MSR112323 r e ciat ntit o a D:D:D:D: ov pe:pe:pe:pe: ss c I I I I yyyy qu e hhhh a r TTTT e cccc w ptptptpt d h o e aaaa t mmmm el n BBBB pt aaaa ib e SSSS c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e MS t rom eeu e A tt a o g yy D ll ah aat r n nn PD u y AANoR SD eck hQChQC h J BR veveveve nk iiii ND SWC a lL BW ctctctct CSC BPLLRBatc20041299-001Batc : ReaReaReaRea s D:D:D:D: ,,,, I I I I D:D:D:D: t: eeee ier llll dededede tetetete f t: iiii t It It It I pppp ec yyyy llll n nnnn ali mmmm e enenenen oj i u lililili anaanaanaana r Q SCACyaSCACyaSCACyaSCACya ClP al n i g i ualual r Q Q O 80 20 - RT y a itit 412 10 0 O M mm ii - 20 P 06 DLDL P P E y ov l R R c a e n R r und a o #: d r p 11232327544341123232754435 e o O 97 PDPD . m pt n 3 o RR e W o o:o:o:o: C NN NN% % ati qq nn r m acc a ee e u ARY p SS RuRu id em rs 112323 ni p i ut r R o o M f y alal r s w e MM e 984 o v it .l f Vf V mo e 8 i m b U ti ReRe D: L s I S i Rec DD it h e e PP ding c u m l l t r RR a epik C HoVPS Ba 20202020 itit // Q mm ii 125 S 2727 H PL // LL MC 44 ghgh ii HH e:e:e:e: tt tt itit DaDaDaDa se 75 mm ss ii ii on LL ss reprep p yy ww s ll PP e r LoLo nana a AA e r a e .5 ds ECEC in RR ee 93 m c r %% x e t e ge e n n d a o r o it t /L/L ati n dm gg o i em r s L mm i 0 ati alal u f n n n o o f Vf V ntit o ts:ts: ii a c u atinecti ReRe t r q Un Un e m g age 23 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPK ,4b in St.4489 l - s 4 tin a e W r ReaRea end ,, o 0o u ettek.c 253 ee l p hioc 1 ueue00 s ll a e . )dd e 3 ii O aa VManuaSR 3 , nn vv 90149014 10 s aa hnologi 330 ( KK yy WW all ec : //www. PP CSCS P E M F: T RL X SS l A e:e: a t F http dd No:No: n oo : e stst ahoga CC te m ee tt i y s ss T 8211 T QLQL u - onb 490 ee . C PP r TT 0 vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt lt E its uu 35 Tn M . ss o m 9 d i ee SD l e ati RR y MSR112323MR112323 r e ciat ntit o a D:D: ov pe:pe: ss c I I yy qu e hh a r TT e cc w ptpt d h o e aa t mm el n BB pt aa ib e SS c dd wn ee tt o ac r e ecec ed tt d B SD eei ct s dd t e MSM t rom eeu e AA tt a o g yy D ll ah aat r n nn PD u y AANoR SD hQChQC J BR ve i ND ct 20041299-001Batc20041299-001Batc : Rea s D:D: , I I D:D: t: ee ier ll de tete f t: i t It I pp ec yy ll n n ali mm e enen oj i u lili anaana r Q SCASCACya ClP al n i g i ualual r QQ O 80 20 - RT y a itit 412 0 O M mm ii - 20 P 06 DLDL PP E y ov l RR c a e n R r und a o #: d r p 11233627550231123362755024 e o O PDPD m pt n o RR e W o o:o:o:o: C NN NN %% ati qq nn r m acc a ee e u ARY p SS RuRu id em rs 112336 ni p i ut r R o o M f y alal r s w e MM e o v it l f Vf V mo e i m b U ti ReRe D: L s I S i Rec DD it h e e PP ding c u m l l t r RR a epik C HoVPS Ba 20202020 itit // Q mm ii 115 S 2727 H PL // LL MC 44 ghgh ii HH e:e:e:e: tt tt itit DaDaDaDa se 85 mm ss ii ii on LL ss reprep p yy ww s ll PP e r LoLo nana a AA e r a e .1 ds ECEC in RR ee 95 m c r %% x e t e ge e n n d a o r o it KgKg t // ati n dm gg o i em r s L mm i 0 ati alal u f n n n o o f Vf V ntit o ts:ts: ii a c u atinecti ReRe t r q UnUn e m g age 24 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPK ,4b in St.4489 l - s 4 tin a e W r end o ReactReact 0o u ettek.c ,, 253 l p hioc 1 ueue s elel a e ) e 3 O aa dd VManuaSR 3 ii3280 , vv 90349034 ff s ll hnologi 330 ( KK uWuW all ec : //www. PP SSSS P E M F: T RL X SS l A e:e: a t F http dd No:No: n oo : e stst ahoga CC te m ee tt i y.0.0 s ss 8211 TT QLQL u - onb ee 2525 C PP r TT vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su ltlt E its uu Tn M ND ss LK o m d i ee 3120 B l e CS ati RR y MR112336LR112336 r e ciat ntit o a D:D: ov pe:pe: ss c I I yy qu e hh a r TT e cc w ptpt d h o e aa t mm el n BB pt aa ib e SS c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e t rom eeu e tt a o g yy D ll ah aat r n nn PD u y AANoR SD -R112336 J BR ND SSS veve B-R112336ii BS CC ctct MPLL : s D:D: ReaRea I I D:D: t:,, ee ier ll ee tete f t: t It I pp ec yy dd ll n ii ff ali ll mm e enen oj i u lili anauanau r Q SCASSCAS ClP al n i g i ualual r QQ O 80 20 - RT y a itit 412 30 0 O M mm ii - 20 P 06 DLDL PP E y ov l RR c a e n R r und a o #: d r p 11233627550291123362755030 e o O 19 PDPD . m pt n 3 o RR e W o o:o:o:o: C NN NN %% ati qq nn r m acc a ee e u ARY p SS RuRu id em rs 112336 ni p i ut r R o o M f y alal r s w e MM e o v it l f Vf V 3080 mo e i m b U ti ReRe D: L s I S i Rec DD it h e e PP ding c u m l l t r RR a epik C HoVPS Ba 20202020 itit // Q mm ii 125125 S 2727 H PL // LL MC 44 ghgh ii HH e:e:e:e: tt tt itit DaDaDaDa se 7575 mm ss ii ii on LL ss reprep p yy ww s ll PP e r LoLo nana a AA e r a e .9.0 ds ECEC in RR ee 9397 m c r %% x e t e ge e n n d a o r o it t /L/L ati n dm gg o i em r s L mm i 00 ati alal u f n n n o o f Vf V ntit o ts:ts: ii a c u atinecti ReRe t r q UnUn e m g age 25 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPK ,4b in St.4489 l - s 4 tin a e W r end o ReactReact 0o u ettek.c ,, 253 l p hioc 1 ueue s elel a e ) e 3 O aa dd VManuaSR 3 i3280i3280 , vv 90349034 ff s ll hnologi 330 ( KK uWuW all ec : //www. PP SSSS P E M F: T RL X SS l A e:e: a t F http dd No:No: n oo : e stst ahoga CC te m ee tt i y.0.0 s ss 8211 TT QLQL u - onb ee 2525 C PP r TT vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su ltlt E its uu Tn M ss o m d i ee 3080 3180 SD l e ati RR y MSR112336MR112336 r e ciat ntit o a D:D: ov pe:pe: ss c I I yy qu e hh a r TT e cc w ptpt d h o e aa t mm el n BB pt aa ib e SS c dd wn ee tt o ac r e ecec ed tt d B SD eei ct s dd t e MSM t rom eeu e AA tt a o g yy D ll ah aat r n nn PD u y AANoR SD hQChQC J BR ND veve ii ctct 20041299-001Batc20041299-001Batc : s D:D: ReaRea I I D:D: t:,, ee ier ll ee tete f t: t It I pp ec yy dd ll n ii ff ali ll mm e enen oj i u lili anauanau r Q SCASSCAS ClP al n i g i ualualual r QQQ O 80 20 - RT y a 5 ititit 412 0 O M mmm iii - 20 P 06 DLDLDL PPP E y ov l RRR c a e n R r und a o #: d r p 11237727565681123772756570.41123772756616 e o O PDPDPD 0 m pt n o RRR e W o o:o:o:o:o:o: C NNN NNN %%% ati qqq nnn r m acc a eee e u ARY p SSS RuRuRu id em rs 112377 ni p i ut r R o o M f y alalal .8 r s w e 7 MM e o v it l f Vf Vf V mo e i m b U ti ReReRe D: L s I S i Rec DDD it h e e PPP ding c u m l l t r RRR a epik C HoVPS Ba 202020202020 ititit /// Q .4.4 mmm 11 iii S 303030 H 00 PL /// LLL MC 11 444 ghghgh iii HHH e:e:e:e:e:e: ttt ttt ititit DaDaDaDaDaDa .6.6 se mmm sss iii iii 9898 on LLL sss repreprep p yyy www s lll PPP e r LoLoLo nanana a AAA e r a e .6 ds ECECEC in 100 RRR ee 99 m c r %%% 9C0C9C x e ...t e ge e n n d a o r o it @21@22@21 t ... ati n dm o uuu i em ... r s L sss i 00 ati alalal u f n n n o o f Vf Vf V ntit o ts:ts:ts: iii a c u atinecti ReReRe t r q UnUnUn e m g age 26 of 31 e e c.u D l 23 nom P o nt 2 Iov g 0-0- I c SPKSPKSPK ,4b in St.4489 l - s 4 tin a e W r end o (4500 (450(450 0o u ettek.c 253.0.0 l p hioc 1 ueueue s lll a e 77 ) W e WW 3 O aaa VManuaSR 3 , vvv 9045D9045D9045D s hnologi 330 ( KKK WWH_DW H_DH_D all ec : //www. PPP pSpSPS P E M F: T RL X SSS l A e:e:e: a t F http ddd No:No:No: n ooo : e ststst ahoga CCC te m eee ttt i y s sss 8211 TTT QLQLQL u - onb eee C PPP r TTT vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su ltltlt E .8 .0.0 its uuu Tn M 777 sss o m d i eee l e CSCS ati RRR y LR112377DUPR112377LR112377 r e ciat ntit o a D:D:D: ov pe:pe:pe: ss c I I I yyy qu e hhh a r TTT e ccc w ptptpt d h o e aaa t mmm el n BBB pt aaa ib e SSS c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e DUP t rom eeu e A tt a o g yy D ll ah aat r n nn PD CK u y E AANoR SD CH hQC -R112377 J BR 7 ND SSWSW H CCC LL20041481-001BatcPL : s D:D:D: I I I D:D:D: t: eee ier lll tetete f t: t It It I ppp ec yyy lll n ali mmm e enenen oj i u lilili anaanaana r Q SCApHSCApHSCApH ClP al n i g i ualual r QQ O 80 20 - RT y a itit 412 0 O M mm ii - 20 P 06 DLDL PP E y ov l RR c a e n R r und a o #: d r p 11243827583351124382758336 e o O PDPD m pt n o RR e W o o:o:o:o: C NN NN %% ati qq nn r m acc a ee e u ARY p SS RuRu id em rs 112438 ni p i ut r R o o M f y alal r s w e MM e o v it l f Vf V mo e i m b U ti ReRe D: L s I S i Rec DD it h e e PP ding c u m l l t r RR a epik C HoVPS Ba itit Q 20202020 // mm ii 130130130130130130 S 11 H PL // LL MC 55 ghgh ii HH e:e:e:e: tt tt itit DaDaDaDa se 707070707070 mm ss ii ii on LL ss reprep p yy ww s ll PP e r LoLo nana a AA e r a e .9.1.0 ds ECEC in 129102106 RR ee 989997 m c r %% x e t e ge e n n d a o r o it t /L/L ati n dm gg o i em r s L mm i 000000 ati alal u f n n n o o f Vf V ntit o ts:ts: ii a c u atinecti ReRe t r q UnUn e m g age 27 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPK ,4b in St.4489 l - s PWPW 4 tin a e W r end o 0o u _N_N ettek.c 253 l p hioc 1 ue0000000000ue00 s PlPl a e ) e 3 600600 O aa VManuaSR CC 3 , II vv 6010D6010D s -- 0102010404 hnologi ll 330 .... . tt ( KK 004 WW 00.000 all ec : //www. PP MSMS P E 0 M F: T RL X SS l A e:e: a t F http dd No:No: n oo : e stst ahoga CC te m ee tt i y s ss 8211 TT QLQL u - onb ee C PP r 02000200020001500250 TT ..... vi 00500 We 00.000 253 nk n 0 a ) El B it 330 d ( its o mm m th L: i e l Su ltlt E its uu 072588 Tn M NDNDND ss o 243 m d i ee 000 l LCLC e ... ati RR y 000 RR112438RR112438 r e ciat ntit o a D:D: ov pe:pe: ss c I I yy qu e hh a r TT e cc w ptpt d h o e aa t mm el n BB pt aa ib e SS c dd wn ee tt o ac r e ecec ed tt d B eei ct s dd t e t rom eeu e tt a o g yy D ll ah aat r n nn PD u y AANoR SD e) hQChQC (Cr) 2 J S BR s) (Cd) a)( ND C m A B m (m LCL ub) ( i u c u i i RBatcRBatci P m m m u i: en en l s D:D: s rare I I D:D: t: eABCadChroLead(eS ier ll tete f t: t It I pp ec yy PPPPPP ll n ali LLLLLL mm e enen oj i u lili anaana CCCCCC r Q SCATTTTTSCAT ClP al n i g i ualualualual r Q QQQ O 80 20 - RT y a itititit 412 202020 0 O M mmmm iiii - 20 P 06 DLDLDLDL P PPP E y ov l R RRR c a e n R r und a o #: d r 000 p 1124572759305112457275930711245727593091124572759310 e o O PDPDPDPD m pt n o RRRR e W o o:o:o:o:o:o:o:o: C NNNN NNN%N %%% ati qqqq nnnn r m acc a eeee e u ARY p SSSS RuRuRuRu id em rs 112457 ni p i ut r R o o M f 000 y alalalal r s w e MM e o v it l f Vf Vf Vf V mo e i m b U ti ReReReRe D: L s I S i Rec DDDD it h e e PPPP ding c u m l l t r RRRR a epik C HoVPS Ba itititit Q 2020202020202020 //// mmmm iiii 130 S 1111 H PL //// LLLL MC 5555 ghghghgh iiii HHHH e:e:e:e:e:e:e:e: tttt tttt itititit DaDaDaDaDaDaDaDa se 70 mmmm ssss iiii iiii on LLLL ssss reprepreprep p yyyy wwww s llll PPPP e r LoLoLoLo nananana a AAAA e r a e ds ECECECEC in 110 RRRR ee m c r %%%% x e t e ge e n n d a o r o secsecsecsec it t ati n dm o i em r s L mm/mm/mm/mm/i 0 ati alalalal u f n n n o o f Vf Vf Vf V ntit o ts:ts:ts:ts: iiii a c u atinecti ReReReRe t r q Un UnUnUn e m g age 28 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPKSPKSPK ,4b in St.4489 _S_S_S_S l - s 4 tin yyyy a e W r tttt end o 0o u ettek.c 253 iliiliiliili l p hioc 1 ue40ueueue s llll a e )bbbb e 3 2 O aaaa . VManuaSR 3 , tatatata vvvv 1030103010301030 7 iiii s hnologi 330 ( KKKK WWWW all ec gngngngn : //www. PPPP ISISISI P S E M F: T RL X SSSS l A e:e:e:e: a t F http dddd No:No:No:No: n oooo : e stststst ahoga CCCC te m eeee tttt i y s ssss T 8211 TTT QLQLQLQL u - onb eeee C PPPP r TTTT vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su lt ltltlt E le .2.2 its uuuu 96 Tn M .22 ssss o m ab 7 >>d i eeee l e CS ati RRRR y LR112457DUPR112457DUPR112457DUP R112457 r mm e ciat ntit a l o a f D:D:D:D: ov pe:pe:pe:pe: ss c I I I I yyyy qu e hhhh a r TTTT e cccc w ptptnon-ptpt d h o e aaaa t mmmm el n BBBB pt aaaa ib e SSSS c dd wn ee tt o ac r e ecec IP ed tt d B eei R ct s dd t e DUPDUPT t rom eeu e AAA tt a o g yy D ll ah aat r n nn PD u y AANoR SD hQChQChQC -R112457 J BR ND SSS CC LL20041479-002Batc20041479-005BatcBatc 20041479-005 : s D:D:D:D: tytytyty iiii I I I I D:D:D:D: t: ilililil eeee ier llll tetetete f t:bbbb t It It It I pppp ec yyyy aaaa llll n tttt iiii ali mmmm e enenenen oj i u nnnn lililili anaanaanaana r gggg Q SCAISCAISCAISCAI ClP al n i g i ualualualual r QQQ Q O 80 20 - RT y a itititit 412 202020 0 O M mmmm iiii - 20 P 06 DLDLDLDL PPP P E y ov l RRR R c a e n R r und a o #: d r 000 p 1124572759310112457275931211245727593141124572759316 e o O PDPDPDPD m pt n o RRRR e W o o:o:o:o:o:o:o:o: C NNNN NN%N%N% % ati qqqq nnnn r m acc a eeee e u ARY p SSSS RuRuRuRu id em rs 112457 ni p i ut r R o o M f 000 y alalalal r s w e MM e o v it l f Vf Vf Vf V mo e i m b U ti ReReReRe D: L s I S i Rec DDDD it h e e PPPP ding c u m l l t r RRRR a epik C HoVPS Ba itititit Q 2020202020202020 //// mmmm iiii S 1111 H PL //// LLLL MC 5555 ghghghgh iiii HHHH e:e:e:e:e:e:e:e: tttt tttt itititit DaDaDaDaDaDaDaDa se mmmm ssss iiii iiii on LLLL ssss reprepreprep p yyyy wwww s llll PPPP e r LoLoLoLo nananana a AAAA e r a e ds ECECECEC in RRRR ee m c r %%%% x e t e ge e n n d a o r o secsecsecsec it t ati n dm o i em r s L mm/mm/mm/mm/i ati alalalal u f n n n o o f Vf Vf Vf V ntit o ts:ts:ts:ts: iiii a c u atinecti ReReReRe t r q UnUnUn Un e m g age 29 of 31 e e c.u D l 23 nom P o nt 2 Iov g I c SPKSPKSPKSPK ,4b in St.4489 _S_S_S_S l - s 4 tin yyyy a e W r tttt end o 0o u ettek.c 253 iliiliiliili l p hioc 1 ueueueue s llll a e )bbbb e 3 O aaaa VManuaSR 3 , tatatata vvvv 1030103010301030 iiii s hnologi 330 ( KKKK WWWW all ec gngngngn : //www. PPPP ISISISIS P E M F: T RL X SSSS l A e:e:e:e: a t F http dddd No:No:No:No: n oooo : e stststst ahoga CCCC te m eeee tttt i y s ssss TTT 8211 T QLQLQLQL u - onb eeee C PPPP r TTTT vi We 253 nk n a ) El B it 330 d ( its o mm m th L: i e l Su ltltlt lt E lelele its uuuu Tn M ssss o m ababab d i eeee l e ati RRRR y DUPR112457DUPR112457DUPR112457DUPR112457 r mmmmmm e ciat ntit aaa lll o a fff D:D:D:D: ov pe:pe:pe:pe: ss c I I I I yyyy qu e hhhh a r TTTT e cccc w ptptnon-ptnon-ptnon- d h o e aaaa t mmmm el n BBBB pt aaaa ib e SSSS c dd wn ee tt o ac r e ecec IP ed tt d B eei R ct WT s dd t e TDUPDUPDUP t rom eeu n e AAAA tt a o g yy w D ll ah aat r n ro nn PD u y B AANoR SD m a hQChQChQC J BR ND urh 20041479-005Batc20041278-001Batc20041280-001D20041282-001Batc : s D:D:D:D: tytyty iii I I I I D:D:D:D: t: ililil eeee ier llll tetetete f t:bbb t It It It I pppp ec yyyy aaa llll n ttt iii ali mmmm e enenenen oj i u nnn lililili anaanaanaana r ggg Q SCASCAISCAISCAI ClP om c . a r a m m a . ww w on i t a u l a v E x i P DB Page 30 of 31 SummitEnvironmentalTechnologies,Inc. 3310 WinSt. CuyahogaFalls,Ohio44223 SampleLog-InCheckList TEL:(330)253-8211FAX:(330)253-4489 Website:http://www.settek.com ClientName:WorkOrderNumber:RcptNo: SYN-NC-27028200412801 Loggedby:4/24/202010:10:00AM JacquelineRasile Completed By:4/24/20202:34:37PM JacquelineRasile Reviewed By:4/24/20203:54:08PM Sara E. Kidd Chainof Custody IsChainofCustody complete?YesNoNot Present 1. Howwas the sampledelivered? UPS 2. LogIn Coolersarepresent?YesNoNA 3. Shipping container/cooleringood condition?YesNo 4. Custody sealsintactonshipping container/cooler?YesNoNot Present No.Seal Date:SignedBy: Wasanattemptmadetocool the samples?YesNoNA 5. Wereall samplesreceivedata temperatureof>0°Cto6.0°CYesNoNA 6. Sample(s)inpropercontainer(s)?YesNo 7. Sufficient samplevolumeforindicated test(s)?YesNo 8. Are samples(exceptVOAandONG)properlypreserved?YesNo 9. Waspreservativeaddedtobottles?YesNoNA 10. Is theheadspaceintheVOAvialsless than1/4inchor6mm?YesNoNo VOA Vials 11. Wereany sample containersreceivedbroken?YesNo 12. Doespaperworkmatchbottlelabels?YesNo 13. (Notediscrepancieson chainof custody) Arematrices correctlyidentifiedonChainofCustody?YesNo 14. Isit clearwhatanalyseswererequested?YesNo 15. Wereallholding timesable tobemet?YesNo 16. (Ifno,notifycustomer forauthorization.) Special Handling(ifapplicable) Was clientnotifiedofalldiscrepancieswith thisorder?YesNoNA 17. PersonNotified: Date: ByWhom:Via:eMailPhoneFaxInPerson Regarding: Client Instructions: Additionalremarks: 18. Cooler Information CoolerNoTempºCConditionSealIntactSeal NoSeal DateSigned By 11.4GoodNot Present Page 31 of 31 State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section’sNon-Discharge Permitting Unit General – This certification provides detailed information of residuals source generating facility and its residuals quality for land . Do not submit this certification for review without application, distribution, or disposal in accordance with 15A NCAC 02T .1100 a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit a separate certification for each source facility. For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source-Generating Facility Information: For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the “Map Guidance for Residuals Land Application Permits”. Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan -A detailed sampling plan for the residuals source-generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division-certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: For each source facility, attach the following: Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 1 Page 900 600 42123580 Proposed s Per Year Dry Ton b 900600 42123580 Maximum Current 10(B) 0 - 0023841 32010(A) 32 - - NCNC0047597 03 03 Permit Number D (Deleted) County DurhamDurhamDurhamDurham M (Modified) ent reatment ham WRF PlantPlant Durham WRF h Dur Facility Name R (Renewed) NortSouth Brown Water T Williams Water Treatm N (New) 16 - 06 hamhamhamham are: RSC : facility FORM City Of Durham City Of DurCity Of DurCity Of DurCity Of Dur source Facility Permit Holder a RRRR Status Code Status Code for RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: a SUMMARY FOR of 5 2 Page (i.e, not applicable to new facility). distribution, land application, or disposal for permitted currently 16 - residuals 06 he amount of T b FORM: RSC State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE-GENERATING FACILITY INFORMATION (See Instruction B.): 1.FacilityName: WiliamsWater Treatment Plant 2. Facility permit holder is: Federal, State, Local Government, or Private. Facility permit issued by:Div. of Water Resources,Div. of Environmental Health, or Other (explain: ). 3. Facility contact person and title: Bobby Whisnaut Assistant WTP Superintendent Complete mailing address: 101 City Hall Plaza City: Durham State: NC Zip: 27701- Telephone number: (919) 560-4362E-mail address: 4.Facility physical address: 1405 HillandaleRoad City: Durham State: NC Zip: 27705- Coordinates: Latitude: 36 0142 Longitude: 78 5133 Datum: NAD 84 Level of accuracy: Second Method of measurement: Map 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water,treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes No 7.Facility permitted/design flow: 22MGD and facility average daily flow: 27.3 (Both WTPs)MGD 8.Average amount of residuals being generated at this facility 29.26dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Water Treatment Process Type and volume of residuals storage (i.e., outside of residuals treatment units): 2 Storage Tanks (65,000 Gal Each) II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6)as: Biological Non-Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-hazardous under RCRA:(Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non-municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: yes no. If yes, list the number(s): b.Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR§261.21- 261.24: yes no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental Laboratoris and Date of analysis: 02/28/2018 Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) oo Passed ignitability test: yes no. Flashpoint: F (> 140F) Passed reactivity test: yes no. HCN: mg/kg (<250) & HS: mg/kg (<500) 2 TCLP Parameter Limit Result TCLP Parameter Limit Result (mg/l) (mg/l) (mg/l) (mg/l) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 DN FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 4/15/2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mg/kg) (mg/kg) (mg/kg) Arsenic 75 41 <12.5 Cadmium 85 39 2.99 Copper 4,300 1,500 354 Lead 840 300 <7.50 Mercury 57 17 <0.0740 Molybdenum 75 n/a <6.25 Nickel 420 420 31.6 Selenium 100 100 <12.5 Zinc 7,500 2,800 76 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Arsenic Chromium Nickel Unit to Boundary to Closest Property Line (meters, check one) (mg/kg) (mg/kg) (mg/kg) > 0 but < 25 30 200 210 34 220 240 39 260 270 46 300 320 53 360 390 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 20 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 4/15/2020 Parameter Result (mg/kg) Aluminum 9050 Ammonia-Nitrogen1200 Calcium <625 Magnesium 302 Nitrate-Nitrite Nitrogen<23.8 pH (Standard Unit) 5.4 Phosphorus 815 Potassium 171 Sodium <625 Total Kjeldahl Nitrogen 12700 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.30 \[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth\]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): default value, or actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: st ) Year PAN Application Method First (1Five-Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 5,224 7,700 Injection/Incorporation 5,824 8,300 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp.density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non-biological residuals): Alternative 1 \[15A NCAC 02T.1106(b)(3)(A)\] - Time/Temperature Compliance. Alternative 2 \[15A NCAC 02T.1106(b)(3)(B)\] - Alkaline Treatment. Alternative 3 \[15A NCAC 02T.1106(b)(3)(C)\]-Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 \[15A NCAC 02T.1106(b)(3)(D)\] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 \[15A NCAC 02T.1106(b)(3)(E)-(K)\] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, gamma ray irradiation, or pasteurization. b. For Land Application of Class B: Alternative 1 \[15A NCAC 02T.1106(c)(1)\] - Fecal Coliform Density Demonstration. Alternative 2 \[15A NCAC 02T.1106(c)(2)\] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, air drying, anaerobic digestion, composting, or lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt - If Daily Cover Alternative is chosen in Item II.8. below \[15A NCAC 02T.1106(a)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 \[15A NCAC 02T.1107(a)(1)\] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 \[15A NCAC 02T.1107(a)(2)\] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 \[15A NCAC 02T.1107(a)(3)\] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 \[15A NCAC 02T.1107(a)(4)\] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 \[15A NCAC 02T.1107(a)(5)\] - 14-Day Aerobic Processes. Alternative 6 \[15A NCAC 02T.1107(a)(6)\] - Alkaline Stabilization. Alternative 7 \[15A NCAC 02T.1107(a)(7)\] - Drying of Stabilized Residuals. Alternative 8 \[15A NCAC 02T.1107(a)(8)\] - Drying of Unstabilized Residuals. Alternative 9 \[15A NCAC 02T.1107(a)(9)\] - Injection. Alternative 10 \[15A NCAC 02T.1107(a)(10)\] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover \[15A NCAC 02T.1107(b)(2)\]. Not Applicable - Non-Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 CźƌƷĻƩƭ .ğƭźƓƭ ğƓķ CƌƚǞƭ Ʒƚ {ĻƷƷƌĻķ ‘ğƷĻƩ \[ĻğǝĻƭ tǒƒƦĻķ Ʒƚ /źƷǤ ŅƩƚƒ /ƌĻğƩǞĻƌƌƭ CźƓźƭŷĻķ ‘ğƷĻƩ źƭ wğǞ ‘ğƷĻƩ 9ƓƷĻƩƭ tƌğƓƷ {ĻķźƒĻƓƷğƷźƚƓ .ğƭźƓƭ ƭĻƓƷ ƷŷƩƚǒŭŷ CƌƚĭĭǒƌğƷƚƩƭ ğƓķ /ƚğŭǒƌğƓƷ źƭ ğķķĻķ Ʒƚ wğǞ ‘ğƷĻƩ ğƓķ /ƌĻğƩǞĻƌƌƭ CźƌƷĻƩĻķ ‘ğƷĻƩ CƌƚǞƭ Ʒƚ WILLIAMS WATER TREATMENT PLANT PROCESS FLOW DIAGRAM ƷǞƚ ƷğƓƉƭ ŅƚƩ ƭƷƚƩğŭĻ͵ ŅƩƚƒ ƷŷĻ ķĻĭğƓƷ ƷğƓƉƭ źƭ ŷĻ ƩĻƭƷ źƭ ƭĻƓƷ Ʒƚ ƷŷĻƭĻ źƭ ƦƩƚĭĻƭƭĻķ ĬǤ {ǤƓğŭƩƚ͵ {ǤƓğŭƩƚ ŷğǒƌƭ Ʒŷźƭ ƭƌǒķŭĻ {ƌǒķŭĻ źƭ ǞğƭƷĻķ Ʒƚ {ĻƷƷƌĻ {ƚƌźķƭ .ǒźƌķźƓŭ͵ {ǒƦĻƩƓğƷĻ ƭĻƓƷ Ʒƚ ƷŷĻ ƭğƓźƷğƩǤ ƭĻǞĻƩ͵ Ʒƚ ƷŷĻ .ƩƚǞƓ tƌğƓƷ ǞŷĻƩĻ źƷ Residuals Sampling Plan City of Durham Land Application Program Williams WTP All material transferred to Brown WTP where it is dewatered for land application. All sampling will be performed at the Brown WTP. Nutrients and Metals Analysis Sampling Point: Dewatering Press at Brown WTP Sampling Frequency: 4/yr Sample Type: Composite Lab: Waypoint Analytical Pathogen Reduction Sampling Point: Dewatering Press at Brown WTP Sampling Frequency: 4/yr Sample Type: Grab – Fecal Coliform tests Lab: Meritech TCLP Sampling Point: Dewatering Press at Brown WTP Sampling Frequency: Annually Sample Type: Composite Lab: Summit Environmental Technologies, Inc Biosolids Handling City Of Durham , North Carolina – Permit WQ0003504 Biosolids from the City of Durham Williams WTP (NPDES 03-32-010(B)) are transferred to City of Durham Brown WTP as a liquid where they are then dewatered and land applied or taken to a compost facility . CITY OF DURHAM PERMIT RENEWAL QUANTITATIVE JUSTIFICATION FOR RESIDUALS PRODUCTION RATE The following is a record of the annual land application volume for the City of Durham’s wastewater & water treatment plants, for the period of the current, expiring permit: Dry Tons Land Applied YearNorth South Brown Williams 20192,882.07 1,813.96549.35 20191,054.41 2,164.52594.48 20172,077.45 2,340.79846.69 105.6 20162,474.30 2,820.291,274 29.4 20151,858.75 2,565 40.53 20142,430.19 1,920.12403.83 The current permitted volume (9292 dry tons per year) is greater than the anticipated need for the coming years. Over the six years shown above the average number of dry tons land applied was 5040.96, which is well within reason of the permitted dry tonnage. These plants have stayed consistent through the past 6 years and consistent results are expected for 2020 and the following years. State of North Carolina Department of Environmental Quality Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONSFOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section’s Non-Discharge Permitting Unit General – This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Application Site Certification (FORM: LASC 06-16): Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit the requested information for all land application sites. For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes are as follows: New (N) Renewed (R) Modified (M) Transferred (T) Deleted (D) Attach the following in accordance with each status code: Status Code Required Item N RT M County Board Notification.doc * Land Owner Agreement (If applicable) Setback Waiver Agreement An updated vicinity/setback map in accordance with the “MapGuidance * for ResidualsLand Application Permits” A soils and agronomic evaluation in accordance with the “Soil Scientist * Evaluation Policy” INSTRUCTIONS FOR FORM: LASC 06-16 Page 1 of 3 An updated accounting of the land application site’s cumulative pollutant loading rates (CPLRs) Status Code Required Item NRTM For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly indicate the location of the land application site and in accordance with the soil map requirements in the “SoilScientist Evaluation Policy” Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same time period) * This item may be required for land application site with a status code “M”, please contact the Division if you need assistant in determining attachment requirements. Crop Type should include the most likely crop types for the life of the permit (five years). Predominant Soils Series Name must be either the name of the soil indicated in Attachment “B” of the existing permit, or name of the soil series as provided by the licensed soil scientist. Predominant SoilMapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil-mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: Digital or Raw Photo Extraction (EXT) Address Matching (ADD) Aerial Photography with Ground Control (AER) Geodetic Quality GPS Survey (GEO) Cadastral Survey (SUR) LORAN-C Navigation Device (LOR) Conversion from Coordinate Plane (CP) Navigation Quality GPS (GPS) Conversion from Township-Section-Range (TSR) Remote Sensing (RS) Conversion from Universal Trans Merc (UTM) Zip Code Centroid (ZIP) Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. Surface water body classifications information may be found at: http://deq.nc.gov/about/divisions/water- resources/planning/classification-standards/classifications Any questions concerning the waterbody and its classification, please contact the Division’s regional offices. A list of the Division’s regional offices, their county coverage, and their contact information may be downloaded at: http://deq.nc.gov/contact/regional-offices General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link http://deq.nc.gov/about/divisions/water-resources/planning/classification-standards/classifications. Stream Classification Process: One of the options below may be used depending on the known initial project information. KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2.Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. Notes on index number and unnamed streams: Unnamed Streams15A NCAC 02B .0301(i). Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case-by-case reclassification proceedings are conducted. The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River BasinStreams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah Basin And Savannah River drainage area entering South Carolina shall be classified "B Tr." River Drainage Area French Broad River Streams entering Tennessee will be classified "B." Basin Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River BasinStreams entering South Carolina are classified "C." New River BasinStreams entering the State of Tennessee are classified "C." Catawba River BasinStreams entering South Carolina are classified "C." Yadkin-Pee Dee River Streams entering Virginia are classified "C," and such streams entering South Carolina are Basin classified "C." Lumber River BasinStreams entering South Carolina are classified "C Sw." Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or Roanoke River Basin described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar-Pamlico River All drainage canals not noted in the schedule are classified "C Sw." except the main drainage Basin canals to Pamlico Sound and its bays which shall be classified "SC." Pasquotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 1 c Page BBBB B 323223 nB Geb HrHrBHrBHrB E VaVaVaVaBGeBGeBGeGeBGeB CeB2 or Rep. Slope Mapping Unit b le l Predominant Soil ville ng e ce don eorgevilleer Series Name EnonGeorgevilleGeorgevilleGAppliApplingVancVanVanceEnonHerndonVanceCecilHGeorgeHerndonGeorgevilleGeorgevilleGeorgevilleGeorgevilleHerndonGeorgevi ue scue FescueFescueFescueFescueFescueFescueFescueFescueFescueFescueFeFescueFescFescueFescueFescueFescueFescueFescueFescueFescueFescue Crop(s) e e nge angeangeangeangeange rangerr anvillanvilleanville PersonPerson County OrangeOrangeOOrangeOraOrangeOrangOrOOrOrO GranvilleGranvilleGranvilleGranvilleGrGrGr Alamance 59 3 .7.6 9.5 3 40 5.98.68.4.14.34.48.9 Net 44 3533.12.841.337.516.99648.526.117.557.6 Acres net acres. 1.5 76 2 alker . W me Vanhook ame K. Walker SameSameSameSameSameSameSameSameSameSameSameSaSameSSameSameSame Operator(s) Lessee(s) or David PopeDavid Pope ichal R David KDavid nce r ue Flore ker alkerlker horpehorpehorpehorpehorpehorpehorpe a TTTTTTT WalkeWalkerWalkerWalker net acres and Total to be certified: Walker . . W N. N. N. N. N. N. N. K. K. Walker k Carrie S F. ed Gentry ry id K. Wal lfred Gentrylfr 631.5 vid on 2 John F. PopeJohn F. Pope Landowner(s)Kirby Trust 1a AA DDon F Henry Henry Henry Henry Henry HenHenry DavDavid KDavid K. David K. WDDavid K. David Vanhoo . SITE CERTIFICATION m Richal 237 1 112 - 01020304050607000405060080102 --- 56 ---------------- -- 555 10 33 158787 ty Of Durha - --05005050505050505000505050606 --- ---------------- RRR Ci PSPS 16 -- OROROR AM GGRGRGGRGRGROROROROROROROOROR- --- - ---------------- C CC NCNC PLICATION SITE INFORMATION (See Instruction B): NCNNC NC Site/Field ID NNCNCNCNCNCNCNCNCNCNCNCNCNNCNC P D A a : LASC 06 AN L N RRRRRRRRRRRRRRRR NN MMM Code Status LAND APPLICATION Applicant's name: Land application sites currently certified: I.FORM 2 Page 3 BBBB C fB pB aB3 C HrBHr ToB GaBGaBGeBGeGeBGeBGeBGeBGeBGeBGeBGeBGeBGeBGeGeGeBGeGeBGeB ApBA HwB FaBF llelle illeilleilleilleilleilleilleilleilleille g oneville iew geviing rg rview orgevorgevorgevorgevorgevorgevorgevorgevorgevorgev i oast airv HerndGeorgevilleGeorgeviCecilGeorgevilleGeorgevilleGeorgevilleGeorgevilleGeorgevilleGeorGeorgevilleApplApplinGeoGeGeGeGeGeGeGeHerndonGeGeGeLloydFTFa opop e Crop cue escue escueescue F FescueFescueFescueFescuFescueFescueFescueFescueFescueFescueFFesFescueFescueFescueFescueFescueFescueFescueFFescue Row Row CropRow CropRow CropRow CrRow CrRow Crop gege n son angeaangeangeangeangeangeangeangeangeangeangeangeangeangeangeangeangeangeange ran erson PersonPPer OrOrOrangeOrangeOrOrOOrOrOrOrangeOrOrOrOrOrOrOrangeOrOrOrOrOrOrOrangeOr 52 9.6.3 0 4.9.79.38.96.77.37.2.24.3 16.312.517.816.918.82912.911.110.610.515.320.011.114.17.2115.265.420.4 134.1 a e ta tta . Parkere Latta Pope LatLattaLaLatta me . W. Parker dd ame Sa SameSameSameSamSameSameSSame vid Popevid Pope vid vid Latta as W avid David PopeDaDavid PopeDDavid PopeDavid PopeDavid PopDaDavid PopeDavid Pope DaviDavidDaviDaDavid LattDaDavid Latta David homas ThomT zeze eeeeze Parker crescres illiams Walker hompson hompson t A H. BreeH. BreezeH. Breeze h Walker Thompson ah Walker ra sett Acressett Asett Acressett Acressetsett Acressett Acressett Acres m as W. r am H. Breeze liam H. Br san P. W DorDorDorDoDorDorDorsett AcresDorsett AcresDorDor idney T u hom Deborah WalkerDeboDeborah WalkerDeborDeborah Joseph Lee Pope SidneySSidney T S TWilWilliam William William H. BreezeWilliWilliaWilliam H. BrWilliam H. Breeze SITE CERTIFICATION 297 1 02030100304050607080910060701012131410102030405 0 010203 ------------------------- ---- 6 0909121212121212121212127677676767676769191919191 09 010101 ------------------------- - --- R R 16 PSPSPS 0 OROROOROROROROROROROROROROROROROROROROROROROROROR- --- - ------------------------- C NCNCNC NC NCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNNC : LASC 06 RRRRRRRRRRRRRRRRRRRRRRRRRRRRR LAND APPLICATION FORM 3 Page 3 B BBBB B BB B2C2 B eb bCdB mB db aB3 HHeb HrBHrHr To GeBGeGeGeBGeHeHeB HdBHA CmBCmCmBCmBC FaB3FaFaB3FFaB3 AAAdB2 w a ing ord fordf if eorgevilleeorgevilleelena FairviewFairviewToastFairviewCliffordCliffordCliffordClifClFairvieFairviewGHerndon HerndonGGeorgevilleGeorgevilleGeorgevilleApplingHHelenaHelenaHelenaHelenApplApplingHelenaApplingHerndon opopopopopop ue Crop cue escue w Crop FescueFescueFescueFescueFescueFescueFescueFescueFFesFescueFescFescueFescueFescueow FescueFescueFescueFescueFescueow Crop RRow CrRow CrRoRow CrRRow CrRow CrRow Cr nce onon mancemance ersonerson lamance PPersonPersonPersonPersonPersonPersonPersonPersPersonPPersonPersPersonPersonPersonPersonPerson Orange AlamanceAlamaAlamanceAlamanceAlamanceAlamanceAlaAlaAAlamance 74 .2.7.6.0 3.00 8.08.63.8 37.22333.321.740.368.934.630.816.928.410.39.411.915.6155221.12.212.717.914.414.630.713 104.2 ynch ynch Lynch H ude H Lynchude H L mememe aamea Claude SameSameSSameSameSameSaSameSameSameSameSameSameSameSameSSameSameSameSSameSameClaClaude H LynchClaude H LynchClaClaude H LSame rr n so nchnchnchnch try rland mpsonk Hunterk Huntek Hunterk Hunterk Huntek Hunter ons Dairy, INC cc ompson cfarland Gentry hompsonhomphohompsonhompsonhompsonhompson hompsonhompson Mcfa ThThompson& S d Gen y y T red ie M ta lfred Gentry ottie AlfAlfred GentryAlfreA Lat idney T . Claude H. LyClaude H. LyClaude H. LyClaude H. Ly Scottie McfarlandScScott Sidney TSidney TSidney TSidney TSidneSidneSidney TSidney TSSidney TSidney JoAnne AmicJoAnne AmiJoAnne AmicJoAnne AmicJoAnne AmiJoAnne Amic SITE CERTIFICATION Milton A 425 49 01020300100304006 01 0050607080101112131401020301020304 ---------- - ------------------ 3 1 2222222222323232323 01 01010101010100101010102020203030303 ---------- - ------------------ S MMM 16 PSPSPSPSPSPPSPSPSPSPSPSPSPSPSPSPSPS OR- AAMAMAMAAMAMAMAAM ------------------ - ---------- C C NCNCNCNCNCNCNCNCNCNNCNCNCNCNCNCNCNC NC NCNCNCNCNNCNCNCNCNC : LASC 06 RRRRRRRRRRRRRRRRRRRRRRRRRRRRR LAND APPLICATION FORM 4 Page B Hr B BBBBBBB BB eBrB fB GeGeBEnBHrLgGeBHrBHrBHrBHrBApBHeBHeHeHCGeApBHeApHeBGeHHrHeBHeHeBVaB n ville on dond na rgeville ndon lena elenaelena HernGerogeGeorgevilleEnonHerndonLignumGeoHerndonHerHerndonHerndonApplingHeHHelenaHelena CecilGeorgevilleApplingHApplingHelenaGeorgevilleHernHerndoHelenaHeleHelenaVance opopopopopopop rop ue CropCCrop cuecue scuescue FescueFesFescueFescueFescueFescueFescueFescueFeFescFescueFescueFescueFeFesow Crop Row CrRow CrRow CrRow CrRowRow CropRow CropRow Row CrRow CropRowRow CrRRow Cr e gege ngen angeangeangeangea rang OOrangeOrangeOrOrOrangeOrOrOranOrangeOrangeOrangeOrangeOrangeOraOrangeOrangeOrangeOrangeOrangeOrangeOrangeOrangeOrangeOrangeOrangeOrOrangeOrange 1 6 6.55.84.47.24.55.14.46.28.68.59.74.05.77.87.6 15.319.311.113.611.010.514.426.626.930.733.21.335.7 gers w a ope Carreow in Carreowd Pope tin Carreo vivid P avid Latta MartMarMartin Martin CarreowDaDaDavid PopeWilliam F. RoWilliam F. RogersWilliam F. RogersWilliam F. Rogers SameSameSameSameSameSameSameSameDDavid LattDavid LattaSameSameSameSameSameSameSame n airy, INC rs rrisoz ok s Dairy, INC otz o oge h LLot Chandler ons Dons Dairy, INCons Dairy, INCons Dairy, INCons Dairy, INCons Dairy, INConons Dairy, INC klin Popeklin Popeklin Pope is Chandler ng Lotz VanhookVan land Harrisonland Haland Harrison & S& S& S& S& S& S& S& S e ran gange Lotz y R. R tatatatatatatata at LLatLatLatLatLatLatLat e Freee Free Free WolfgaWolfgangWolfgang RichalRichal Wolf James T. WilsonJames T. WilsonJames T. WilsonJames T. WilsonJames T. Wilson . . . . . . . . Nanc John FranJohn FranJohn F ettiettietti Robert CurtRobert Curtis ChandlerRobert Curtis SITE CERTIFICATION BBB Milton AMilton AMilton AMilton AMilton AMilton AMilton AMilton A 37 A 1234523 020040506008090102030102030403040507 -------8B 9 ------------------- 08A - - - 4 3 14141414141515 0101010101010101040047070707087878793 -------93 9 ------------------- 93 - - - RR 16 OROROROROROROR OROROROROOROROOROROROROROROROROROROR- -------OR OR ------------------- OR - - - C NCNCNCNNCNCNC NCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNC NC NC NC : LASC 06 R RRRRRRRRRRRRRRRRRRRRRRRRRRR LAND APPLICATION FORM R 5 Page A BBB fB pBneB fB C AVaBHeBVaBHeBVaBHeVaBVaBApBApBHeBHeOrBOnAOSmBRaBHWeBWeBCVaBHeBVaBHeBHeVaB a nge ena pling lenance oam ApplingVanceHelenaVanceHelenaVanceHelVanceVanceApApplingHeHelenOrangeOraOrangeSilRasaloHelenaWedoweeWedoweeCecilCecilVanceHelenaVanceHelenaHelenaVa p opoop Crop cuecue sscue es w Crop FescueFescueFescueFescueFescueFescueFescueFeFFescueFeFescueFescueFescueFescueFescueow Crop Row CrRow CrRow CropRow CrRow CropRow CropRow CropRow CropRoRow CropRRowRow Crop e ge on ngen son rsrson ange range erson PersonPersonPersonPersonPersonPePPersonPersonPerPersonPersonPersonPersonPePerson OrangOOrangeOraOrangeOrangeOrangeOrOrangeOrangeOrangeOrangeOra 959 2.5.8 .1 34.49.5 7.53.82.36.19.94.45.19.54.47.1 16.24.30.531.2136.6223319.818.730.223.319.016.13.427.116.6 ddddddddddd ogers Rogers atterfiel F. Rogers D. S me illiam F. R mes D. Satterfielmes D. Satterfielmesmes D. Satterfielmes D. Satterfielmes D. Satterfielmes D. Satterfielmes D. Satterfielmes D. Satterfielmes D. Satterfielmes D. Satterfiel ameaame aaaaaaaaaaa William F. RogersWilliam F. RogersWilliam F. RogersWilliam F. RogersWWilliam F. RogersWilliam F. RogersWilliam F.William F. RogersWilliam F. RogersWilliam SSSameSameSameSameSJJJJJJJJJJJ ler dler eld ield ry ogers er t handler rvrver terfi ChandChan GenGentry Carver is C Larry Rogers S. Carver urtis Chandler M. Satterfield Curtis ChandlerCurtis Chandler iam Larry R ancy R. Rogers Roy S. CaRoy S.Roy Roy S. CarverRoy S. Ca san san M. Satterfieldsan M. Satterfieldsan M. Satterfieldsan M. Satterfieldsan M. Satterfsan M. Satterfieldsan M. Satterfieldsan M. Satsan M. Satterfieldsan M. Satterfield TommyTommy NNancy R. Rogers uuuuuuuuuuu SSSSSSSSSSS WillWilliam Robert CurtRobert Curtis Robert Curtis Robert CRobert Curtis ChandlerRobertRobert SITE CERTIFICATION 11121314151617180102 9B 0102030405010203040507080910 10B---------- 10A - -------------- 06B 06A - - - - 9 93939393939396969494 93 070707070422929292929292929 ---------- 9393 - ----------29---- 29 -- - - R 16 S PSPSPSPSPSPSPSPSPSPSPSPSPSPS OROROROROROROROROROR- O ----------P---- PS OR---------- OR - - - - - C NCNCNCNCNCNCNNCNCNCNCNCNCNC NCNCNCNCNCNCNCNCNCNC NC NC NC NC NC : LASC 06 RRRRRRRRRRRRRRRRRRRRRRRRRRRRR LAND APPLICATION FORM 6 Page Class EnBEnB Current and Proposed EnonEnon scue is CeB2) Stream Index No. FescueFe Waterbody Subbasin and unit (Deleted) D sonson Accuracy ) PerPer Nearest SecondNearest SecondNearest SecondNearest SecondNearest SecondNearest SecondNearest SecondNearest Second 6 . Location 8.9 19 T (Transferred dd 8% slope Cecil in Anson County the mapping - ruction C): field on the same page. ADDADDADDADDADDADDADD ADD Inst the same mes D. Satterfielmes D. Satterfiel Location Method Code M (Modified) aa JJ of Datum NAD 83NAD 83NAD 83NAD 83NAD 83NAD 83NAD 83NAD 83 Location R (Renewed) Satterfield Longitude N (New) an M. ssan M. Satterfield uu ) SS : SITE CERTIFICATION , etc. Cecil Latitude 1112 -- Appling, 2929 -- 16 PSPS - -- NCNC : LASC 06 Site/Field ID WATERBODY AND CLASSIFICATIONS INFORMATION (See RR Soil Series Name (i.e. Status Code for land application sites areMapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2 LAND APPLICATION a bc II.Note: Please keep the site information (I.) and waterbody information (II.) FORM 0 VICINITY MAP cc III Oro ! ................. I V) J11" 100111 GRAPHIC SCALE V = 2, 000' 2,000' 0 2,000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within NC-PS-29 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1-12