NC0044725_NPDES Permit Renewal App_20090128

IDR-FR
DWQ
Beverly Eaves Perdue, Governor
State of North Carolina
Dee Freeman, Secretary
North Carolina Department of Environment and Natural Resources
January 28, 2009
PAUL DAVIS
EXECUTIVE DIRECTOR
LAURINBURG MAXTON AIRPORT COMMISSION
16701 AIRPORT ROAD
MAXTON NC 28364
Dear Mr. Davis:
Coleen H. Sullins, Director
Division of Water Quality
Subject: Receipt of permit renewal application
NPDES Permit NC0044725
Laurinburg Industrial WWTP
Scotland County
The NPDES Unit acknowledges receipt of the permit renewal application for the above
facility on January 28, 2009; however, on initial review it was noted that the required Sludge
Management Plan was notincluded in the submitted paperwork. Please submit to this unit a Sludge
Management Plan. For your convenience, we can accept a faxed copy at [phone] or you can
mail it attention to me at the mail service center address listed below. Upon receipt, a member of
the NPDES Unit will further review your application and will contact you if additional information
is required.
If you have any additional questions concerning renewal of the subject permit, please contact
Gil Vinzani at [phone].
Sincerely,
Dina Sprinkle
Point Source Branch
cc: CENTRAL FILES
Eayettevillex&egional.Office/Surface Water Protection
NPDES Unit
Mailing Address
1617 Mail Service Center
Raleigh, NC 27699-1617
Internet: www.ncwaterqualitv.org
Phone [phone]
Fax [phone]
Location
512 N. Salisbury St.
Raleigh, NC 27604
,Customer Service 1-877-623-6748
One Carolina
Wirral!,
An Equal Opportunity/Affimiative Action Employer— 50% Recycled/10% Post Consumer Paper

J A N 2 8 2009
DENR - WATER QUALITY
NPDES Permit #NC i 44845 BRANCH`
Renewal Application
Laurinburg-Maxton
Airport Commission WWTP
Scotland County
PREPARED FOR
LAURINBURG-MAXTON
AIRPORT COMMISSION
NJ
PREPARED BY
Hobbs, Upchurch & Associates, P.A.
300 S.W. Broad Street
Southern Pines, NC 28387
January 2009

NPDES Permit Renewal Application
(NC0044725)
Laurinburg-Maxton Airport Commission Wastewater Treatment Plant
January 2009
Table of Contents
NPDES Form 2A
Part A Basic Application Information
Part B Additional Application Information (greater than 100,000 gpd)
Part C Certification
Part D Expanded Effluent Testing Data
Part E Toxicity Test Data
Part F Industrial User Discharges
Part G Combined Sewer Systems (Not Applicable)
Attachments
Attachment 1 DMR Data Summary.(September 2005 through September 2008)
Attachment 2 Expanded Effluent Test Results
Attachment 3 Toxicity Test Results and Toxicity Reduction Evaluation Status Reports
Attachment 4 Topographic Map of Laurinburg Maxton Airport Commission WWTP
Attachment 5 Treatment Plant Process Layout
Attachment 6 Current NPDES Permit

NPDES Form 2A

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
FORM
2A
NPDES
APPLICATION OVERVIEW
Form 2A has been developed in a modular format and consists of a "Basic Application Information packet
and a "Supplemental Application Information" packet The Basic Application Information packet is divided
into two parts. All applicants must complete Parts A and. C. Applicants with a design flow greater than or
equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental
Application Information packet.. The following items explain which parts of Form 2A you must complete.
BASIC APPLICATION INFORMATION:
A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works
that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12.
B. Additional Application Information for Applicants with a Design Flow Z 0.1 mgd. All treatment works that have design flows
greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6.
C. Certification. All applicants must complete Part C (Certification).
SUPPLEMENTAL APPLICATION INFORMATION:
D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets
one or more of the following criteria must complete Part D (Expanded Effluent Testing Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to provide the information.
E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing
Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to submit results of toxicity testing.
F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any
significant industrial users (Sills) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges
and RCRA/CERCLA Wastes). SlUs are defined as:
1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and
40 CFR Chapter I, Subchapter N (see instructions); and
2. Any other industrial user that:
a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain
exclusions); or
b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic
capacity of the treatment plant; or
c. Is designated as an SIU by the control authority.
G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer
Systems).
ALL APPLICANTS MUST COMPLETE;PART C.(CERTIFICATION)
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 1 of 22

Part A
Basic Application Information
7

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WVVTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
BASIC APPLICATION INFORMATION
PART A BASIC APPLICATION INFORMATION FOR ALL APPLICANTS:
All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet.
A.1. Facility Information.
Facility Name Laurinburq-Maxton Airport Commission WWTP
Mailing Address 16701 Airport Road
•
Maxton, NC 28364
Contact Person Paul Davis
Title Executive Director
Telephone Number [phone]
Facility Address North Carolina State Road SR1434, East of Laurinburq
•
(not P.O. Box)
A.2. Applicant Information. If the applicant is different from the above, provide the following:
Applicant Name
Mailing Address
Contact Person
Title
Telephone Number ( )
Is the applicant the owner or operator (or both) of the treatment works?
® owner ® operator
Indicate whether correspondence regarding this permit should be directed to the facility or the applicant.
® facility 0 applicant
A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works
(include state -issued permits).
NPDES NC0044725 PSD
UIC Other
RCRA Other
A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each
entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.).
Name Population Served Type of Collection System Ownership
LMAC Airbase 3,500 Separate - Gravity Local Covemment Commission
Town of Wagram 775 Separate - Gravity Municipal
Total population served
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 2 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
A.S. Indian Country.
a. Is the treatment works located in Indian Country?
❑ Yes ® No
b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows
through) Indian Country?
❑ Yes ® No
A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the
average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period
with the 12`h month of "this year" occurring no more than three months prior to this application submittal.
a. Design flow rate 2.0 mgd
Two Years Ago
b. Annual average daily flow rate 0.420 MGD
Last Year This Year
0.743 MGD 0.894 MGD
c. Maximum daily flow rate 0.841 MGD 1.310 MGD 1.322 MGD
A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent
contribution (by miles) of each.
® Separate sanitary sewer 100
❑ Combined storm and sanitary sewer
A.S. Discharges and Other Disposal Methods.
a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes ❑ No
If yes, list how many of each of the following types of discharge points the treatment works uses:
i. Discharges of treated effluent
ii. Discharges of untreated or partially treated effluent
iii. Combined sewer overflow points
iv. Constructed emergency overflows (prior to the headworks)
v. Other
b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments
that do not have outlets for discharge to waters of the U.S.? D Yes
If yes, provide the following for each surface impoundment:
Location:
1
® No
Annual average daily volume discharge to surface impoundment(s) mgd
Is discharge 0 continuous or ❑ intermittent?
c. Does the treatment works land -apply treated wastewater? ❑ Yes ® No
If yes, provide the following for each land application site:
Location:
Number of acres:
Annual average daily volume applied to site: mgd
Is land application ❑ continuous or
❑ intermittent?
d. Does the treatment works discharge or transport treated or untreated wastewater to another
treatment works?
❑ Yes ® No
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 3 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
e.
If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works
(e.g., tank truck, pipe).
If transport is by a party other than the applicant, provide:
Transporter Name
Mailing Address
Contact Person
Title
Telephone Number ( )
For each treatment works that receives this discharge, provide the
following:
Name
Mating Address
Contact Person
Title
Telephone Number ( 1
If known, provide the NPDES permit number of the treatment works
Provide the average daily flow rate from the treatment works into
Does the treatment works discharge or dispose of its wastewater
in A.8. through A.8.d above (e.g., underground percolation, well
If yes, provide the following for each disposal method:
that receives this discharge
the receiving facility. mgd
in a manner not included
injection): ❑ Yes ® No
Description of method (including location and size of site(s) if applicable):
Annual daily volume disposed by this method:
Is disposal through this method ❑ continuous or 0 intermittent?
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 4 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
WASTEWATER DISCHARGES:
If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through
which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question
A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd."
A.9. Description of Outfall.
a. Outfall number 001
b. Location Off of SR1376 near Maxton
(City or town, if applicable) (Zip Code)
Robeson NC
(County)
34° 46' 08"
(State)
79° 19' 58"
(Latitude) (Longitude)
c. Distance from shore (if applicable) 0 ft.
d. Depth below surface (if applicable) 0 ft.
e. Average daily flow rate 0.5703 mgd
f. Does this outfall have either an intermittent or a periodic discharge? ❑ Yes ® No (go to A.9.g.)
If yes, provide the following information:
Number f times per year discharge occurs:
Average duration of each discharge:
Average flow per discharge: mgd
Months in which discharge occurs:
g. Is outfall equipped with a diffuser? ❑ Yes ® No
A.10. Description of Receiving Waters.
a. Name of receiving water Lumber River
b. Name of watershed (if known) Lumber
United States Soil Conservation Service 14-digit watershed code (if known):
c. Name of State Management/River Basin (if known): Lumber River Basin
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
d. Critical low flow of receiving stream (if applicable)
acute 61 (Summer)
cfs
chronic 183 (Winter) cfs
e. Total hardness of receiving stream at critical low flow (if applicable): mg/I of CaCO3
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 5 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinbur-Maxton Airport Commission WWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
A.11. Description of Treatment
a. What level of treatment are provided? Check all that apply.
® Primary ® Secondary
❑ Advanced ® Other. Describe: Tertiary
b. Indicate the following removal rates (as applicable):
Design BOD5 removal or Design CBOD5 removal 90
Design SS removal 86 %
Design P removal 30 %
Design N removal 40
Other
c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe:
Year -Round Chlorination
If disinfection is by chlorination is dechlorination used for this outfall? ® Yes ❑ No
Does the treatment plant have post aeration? ❑ Yes ® No
A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following
parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is
discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data
collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of
40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a
minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart.
Outfall number: 001
PARAMETER
MAXIMUM DAILY VALUE
AVERAGE DAILY VALUE
Value
Units
Value
Units
Number of Samples
pH (Minimum)
7.40
s.u.
pH (Maximum)
8.33
s.u.
Flow Rate
2.422
MGD
0.638
MGD
1,095
Temperature (Winter)
20.4
°C
15.41
°C
180
Temperature (Summer)
29.7
°C
23.39
°C
252
* For pH please report a minimum and a maximum daily value
POLLUTANT
MAXIMUM DAILY
DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MUMDL
Conc.
Units
Conc.
Units
Number of
samples
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
BIOCHEMICAL OXYGEN
DEMAND (Report one)
BOD5
34.00
mg/I
4.07
mg/I
468
0405
15/12
CBOD5
FECAL COLIFORM
>6,000
#/100 ml
25.22
MOO468
9222
200/100
•
TOTAL SUSPENDED SOLIDS (TSS)
389
mg/I
5.97
mg/1
468
0160
15
END OF PART A.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 6 of 22

Part B
Additional Application Information

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
BASIC APPLICATION INFORMATION
PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR
EQUAL TO 0.1 MGD (100,000 gallons per day). .
All applicants with a design flow rate z 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification).
B.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration.
377,000 gpd
•
Briefly explain any steps underway or planned to minimize inflow and infiltration.
The Commission will conduct a detailed analysis of the existing wastewater collection system to locate sources of
extraneous flows. The analysis is expected to be initiated during the winter of 2009.
B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This
map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire
area.)
a. The area surrounding the treatment plant, including all unit processes.
b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which
treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable.
c. Each well where wastewater from the treatment plant is injected underground.
d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within''/4 mile of the property boundaries of the treatment
works, and 2) listed in public record or otherwise known to the applicant.
e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed.
f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail,
or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed.
B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and at
backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g.,
chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow
rates between treatment units. Include a brief narrative description of the diagram.
B.4. Operation/Maintenance Performed by Contractor(s).
Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a
contractor? ❑ Yes ® No
If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional
pages if necessary).
Name: "
Mailing Address:
Telephone Number: ( )
Responsibilities of Contractor:
B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or
uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the
treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5
for each. (If none, go to question B.6.)
a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule.
b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies.
❑Yes ®No
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 7 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WVVTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable).
d. Provide dates imposed
applicable. For improvements
applicable. Indicate
Implementation Stage
- Begin Construction
- End Construction
- Begin Discharge
- Attain Operational
e. Have appropriate
Describe briefly:
by any compliance schedule
planned independently
dates as accurately as possible.
Level
permits/clearances concerning other
or any actual dates of completion for the implementation steps listed
of local, State, or Federal agencies, indicate planned or actual completion
Schedule Actual Completion
MM/DD/YYYY MM/DD/YYYY
below, as
dates, as
Yes 0 No
/ / / /
/ / / /
/ / / /
/ / / /
Federal/State requirements been obtained? 0
B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD
Applicants that discharge to waters of the US must
effluent testing required by the permitting authority
on combine sewer overflows in this section. All information
using 40 CFR Part 136 methods. In addition, this data
QA/QC requirements for standard methods for analytes
based on at least three pollutant scans and must be
Outfall Number: 001
ONLY).
provide effluent testing data for the following parameters. Provide
for each outfall through which effluent is discharged. Do not include
the indicated
information
conducted
other appropriate
data must be
reported must be based on data collected through analysis
must comply with QA/QC requirements of 40 CFR Part 136 and
not addressed by 40 CFR Part 136. At a minimum effluent testing
no more than four and on -half years old.
POLLUTANT
MAXIMUM DAILY
DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MUMDL
Conc.
Units
Conc.
Units
Number of
Samples
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
AMMONIA (as N)
15.2
mg/I
0.43
mg/I
468
0350
8 mg/I
CHLORINE (TOTAL
RESIDUAL, TRC)
57
ug/I
21
ug/I
468
0330
28 ug/I
DISSOLVED OXYGEN
25.2
mg/I
7.31
mg/I
468
0360
Monitor
TOTAL KJELDAHL
NITROGEN (TKN)
NITRATE PLUS NITRITE
NITROGEN
OIL and GREASE
PHOSPHORUS (Total)
24
mg/1
7.53
mg/I
36
0356
Monitor
TOTAL DISSOLVED SOLIDS
(TDS)
OTHER
END OF PART B.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 8 of 22

Part C
Certification

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVVVTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
BASIC APPLICATION INFORMATION
PART C. CERTIFICATION
All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this
certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which
parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm t the • d
Form 2A and have completed all sections that apply to the facility for which this application i sut�mrt ec�„
f q'
Indicate which parts of Form 2A you have completed and are submitting:
E Basic Application Information packet Supplemental Application Inform n onac et:
E Part D (Expanded Effluent Testing Data) f,AAl1 2 s 2009
E Part E (Toxicity Testing: Biomonitoring Data) •
E Part F (Industrial User Discharges and RCRA/CERCLA Wastes)
❑ Part G (Combined Sewer Systo�}^I p , WATER QUALM/CI`11`
NCH
ALL APPLICANTS MUST COMPLETE THE FOLLOWING=CERTIFICATION. POINT: S�t1i�CE �3f�A
SOURCE
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment
for knowing violations.
Name and official title Paul Davis, ExecutivetipDirector
Signature _ ` IY1)C,.,...-•.
Telephone number [phone]
Date signed / '„9- 0-- Oy .
Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment
works or identify appropriate permitting requirements.
SEND COMPLETED FORMS TO:
NCDENR/ DWQ
Attn: NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 9 of 22

Part D
Expanded Effluent Testing Data

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION INFORMATION
PART D. EXPANDED EFFLUENT TESTING DATA
Refer to the directions on the cover page to determine whether this section applies to the treatment works.
Effluent Testing: 1.0 mgd
to have) a pretreatment program,
pollutants. Provide the indicated
effluent is discharged. Do
and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0
or is otherwise required by the permitting authority to provide the data, then provide effluent
effluent testing information and any other information required by the permitting authority
not include information on combined sewer overflows in this section. All information reported must
using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements
for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the
pollutants not specifically listed in this form. At a minimum, effluent testing data must be based
than four and one-half years old.
(Complete once for each outfall discharging effluent to waters of the United States.)
mgd or it has (or is required
testing data for the following
for each outfall through which
be based on data collected
of 40 CFR Part 136 and
blank rows provided below
on at least three pollutant
through analyses conducted
other appropriate QA/QC requirements
any data you may have on
scans and must be no more
Outfall number: 001
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL.
METHOD
MUMDL
Conc.
Units
Mass
Units
Conc.
` Units
Mass
-Units
Number
of.
Samples
METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS.
ANTIMONY
.013
mg/I
0.02
mg/I
3
200.7
ARSENIC
.02
mg/I
0.002
mg/I
3
200.7
BERYLLIUM
.002
mg/I
0.005
mgll
3
200.7
CADMIUM
.005
mg/I
0.01
mg/I
3
200.7
CHROMIUM
.01
mg/I
0.02
mgll
3
200.7
COPPER
.02
mg/I
0.005
mg/I
3
200.7
LEAD
.005
mg/I
0.0002
mg/I
3
200.7
MERCURY
.0002
mg/I
0.02
mg/I
3
245.1
NICKEL
.02
mg/I
0.02
mg/I
3
200.7
SELENIUM
.02
mg/I
0.01
mgll
3
200.7
SILVER
.01
mg/I
0.001
mgll
3
200.7
THALLIUM
.001
mg/I
0.031
mg/I
3
200.8
ZINC
.034
mg/I
0.006
mg/I
3
200.7
CYANIDE
.0082-
mg/I
0.048
mg/I
3
200.7
TOTAL PHENOLIC
COMPOUNDS
.064
mg/I
30
mg/I
3
420.1
HARDNESS (as CaCO3)
30
mgll
0.02
mg/I
1
130.1
Use this space (or a separate sheet) to provide information on other metals requested by the permit writer
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 10 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVVVTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT.,
MAXIMUM ,DAILY <DISCHARGE -
_ ; ,;AVERAGE DAILY •DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Conc
;Units„
Mass'
Units
Conc
Units;
Mass'
Units.
Number
of
Samples
VOLATILE ORGANIC COMPOUNDS
ACROLEIN
.05
mg/I
.05
mg/I
1
624
ACRYLONITRILE
BENZENE
.001
mg/I
.001
mg/I
3
624
BROMOFORM
.001
mg/I
.001
mgll
3
624
CARBON
TETRACHLORIDE
.001
mg/I
.001
mg/I
3
624
CHLOROBENZENE
.001
mg/I
.001
mgll
3
624
CHLORODIBROMO-
METHANE
.001
mgll
.001
mg/I
3
624
CHLOROETHANE
.005
mg/I
.005
mg/I
3
624
2-CHLOROETHYLVINYL
ETHER
05
mgll
.05
mg/I
3
624
CHLOROFORM
.0052
mg/I
.005
mgll
3
624
DICHLOROBROMO-
METHANE
1,1-DICHLOROETHANE
.001
mg/I
.001
mg/I
3
624
1,2-DICHLOROETHANE
.001
mgll
.001
mgll
3
624
TRANS-1,2-DICHLORO-
ETHYLENE
.001
mgll
.001
mg/I
3
624
1,1-DICHLORO-
ETHYLENE
.001
mg/I
.001
mg/I
3
624
1,2-DICHLOROPROPANE
.001
mg/I
.001
mgll
3
624
1,3-DICHLORO-
PROPYLENE
.001
mg/I
.001
mg/I
3
624
ETHYLBENZENE
.001
mg/I
.001
mgll
3
624
METHYL BROMIDE
METHYL CHLORIDE
METHYLENE CHLORIDE
.005
mgll
.005
mgll
3
624
1,1,2,2-TETRA-
CHLOROETHANE
.001
mg/I
.001
mg/I
3
624
.
TETRACHLORO-
ETHYLENE
.001
mgll
.001
mgll
3
624
TOLUENE
.005
mg/I
.005
mg/I
3
624
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 11 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Outfall number: (Complete
once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
°MAXIMUM,DAILY DISCHARGE
AVERAGE DAILY -DISCHARGE.
ANALYTICAL
METHOD
ML/MDL
= Conc.
'
Units :.
Mass
Units,'
Conc,
Units :
Mass.;_
Units
Number
of
Samples
1,1,1-
TRICHLOROETHANE
.001
mg/I
.001
mg/I
3
624
1,1,2
TRICHLOROETHANE
.001
mg/I
.001
mg/I
3
624
TRICHLOROETHYLENE
.001
mg/I
.001
mg/I
3
624
VINYL CHLORIDE
.001
mg/I
.001
mg/I
3
624
Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer
ACID -EXTRACTABLE COMPOUNDS
P-CHLORO-M-CRESOL
2-CHLOROPHENOL
.01
mg/I
.01
mg/I
3
625
2,4-DICHLOROPHENOL
.01
mg/I
.01
mg/I
3
625
2,4-DIMETHYLPHENOL
.01
mg/I
.01
mgll
3
625
4, 6- D I N I T R O-O-C R E S O L
2,4-DINITROPHENOL
.01
mg/I
.01
mg/I
3
625
2-NITROPHENOL
.01
mg/I
.01
mg/I
3
625
4-NITROPHENOL
.01
mg/I
.01
mg/I
3
625
PENTACHLOROPHENOL
.01
mg/I
.01
mg/I
3
625
PHENOL
.01
mg/I
.01
mg/I
3
625
2,4,6-
TRICHLOROPHENOL
.01
mg/I
.01
mg/I
3
625
Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer
BASE -NEUTRAL COMPOUNDS
ACENAPHTHENE
.001
mg/I
.001
mg/I
3
625
ACENAPHTHYLENE
.001
mg/I
.001
mg/I
3
625
ANTHRACENE
.001
mg/I
.001
mg/I
3
625
BENZIDINE
.05
mg/I
.05
mg/I
3
625
BENZO(A)ANTHRACENE
.001
mg/I
.001
mg/I
3
625
BENZO(A)PYRENE
.001
mg/I
.01
mg/I
3
625
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 12 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Outfall number: 001 (Complete
once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Conc.
Units
Mass
`:Units
Conc.:`,.
Units
Mass
Units -
Number
of
Samples
3,4 BENZO-
FLUORANTHENE
.001
mg/I
.001
mgll
3
625
BENZO(GHI)PERYLENE
.001
mg/I
.001
mg/I
3
625
BENZO(K)
FLUORANTHENE
.001
mg/I
.001
mg/I
3
625
BIS (2-CHLOROETHOXY)
METHANE
,01
mg/I
.01
mg/I
3
625
BIS (2-CHLOROETHYL)-
ETHER
01
mg/I
.01
mg/I
3
625
BIS (2-CHLOROISO-
PROPYL) ETHER
.01
mg/I
.01
mg/I
3
625
BIS (2-ETHYLHEXYL)
PHTHALATE
.0029
mg/I
.002
mg/I
3
625
4-BROMOPHENYL
PHENYL ETHER
.01
mg/I
.01
mg/I
3
625
BUTYL BENZYL
PHTHALATE
.001
mg/I
.001
mg/I
3
625
2-CHLORO-
NAPHTHALENE
.01
mg/I
.01
mg/I
3
625
4-CHLORPHENYL
PHENYL ETHER
,01
mg/I
.01
mg/I
3
625
CHRYSENE
.01
mg/I
.01
mg/I
3
625
DI-N-BUTYL PHTHALATE
.001
mg/I
.001
mg/I
3
625
DI-N-OCTYL PHTHALATE
.001
mg/I
.001
mg/l
3
625
DIBENZO(A,H)
ANTHRACENE
.01
mg/I
.01
mg/I
3
625
1,2-DICHLOROBENZENE
.001
mg/I
.001
mg/I
3
624
1,3-DICHLOROBENZENE
.001
mg/I
.001
mg/I
3
624
1,4-DICHLOROBENZENE
.001
mg/I
.001
mg/I
3
624
3,3-DICHLORO-
BENZIDINE
.011
mg/l
.011
mg/I
3
625
-
DIETHYL PHTHALATE
.001
mg/I
.001
mg/I
3
625
DIMETHYL PHTHALATE
.001
mg/1
.001
mg/I
3
625
2,4-DINITROTOLUENE
.01
mg/I
.01
mg/I
3
625
2,6-DINITROTOLUENE
.01
mg/I
.01
mg/I
3
625
1,2-DIPHENYL-
HYDRAZINE
.011
mg/I
.011
mg/I
2
625
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 13 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVWTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MLIMDL
Conc.
Units
Mass
'> Units
Conc...
Units
Mass
Units
Number
of
Samples
FLUORANTHENE
.001
mg/I
.001
mg/I
3
625
FLUORENE
.001
mg/I
.001
mg/I
3
625
HEXACHLOROBENZENE
.01
mg/I
.01
mg/I
3
608
HEXACHLORO-
BUTADIENE
.011
mg/I
.011
mg/I
3
625
HEXACHLOROCYCLO-
PENTADIENE
01
mgll
.01
mg/I
3
625
HEXACHLOROETHANE
.01
mg/I
.01
mg/I
3
625
INDENO(1,2,3-CD)
PYRENE
.001
mg/I
.001
mg/1
3
625
ISOPHORONE
.01
mgll
.01
mg/I
3
625
NAPHTHALENE
.001
mgli
.001
mg/I
3
625
NITROBENZENE
.01
mgll
.01
mg/I
3
625
N-NITROSODI-N-
PROPYLAMINE
.01
mg/I
.01
mg/I
3
625
N-NITROSODI-
METHYLAMINE
.05
mg/I
.05
mg/I
3
625
N-NITROSODI-
PHENYLAMINE
.01
mg/l
.01
mg/I
3
625
PHENANTHRENE
.001
mg/I
.001
mg/I
3
625
PYRENE
.001
mg/I
.001
mg/I
3
625
1,2,4-
TRICHLOROBENZENE
.01
mg/I
.01
mg/I
3
625
Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer
Use this space (or a separate sheet) to provide information on other pollutants (e.g , pesticides) requested by the permit writer
END OF PART D.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS.
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 14 of 22

Part E
Toxicity Test Data

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION INFORMATION'
PART E. TOXICITY TESTING` DATA .
POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the
facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are
required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters.
• At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two
species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results
show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include
information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC
requirements for standard methods for analytes not addressed by 40 CFR Part 136.
• In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test
conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a
toxicity reduction evaluation, if one was conducted.
• If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information
requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods.
If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E.
If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to
complete.
E.1. Required Tests.
Indicate the number of whole effluent
® chronic ❑ acute
E.2. Individual Test Data. Complete the
column per test (where each species
toxicity tests conducted in the past four and one-half years.
following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one
constitutes a test). Copy this page
Test number: See Attached
if
more than three tests are being reported.
Test number: See Attached
Test number: See Attached
a. Test information.
Test Species & test method number
Age at initiation of test
•
Outfall number
Dates sample collected
Date test started
Duration
b. Give toxicity test methods followed.
Manual title
Edition number and year of publication
Page number(s)
c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used.
24-Hour composite
Grab
d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each.
Before disinfection
After disinfection
After dechlorination
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 15 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Test number: Test number: Test number:
e. Describe the point in the treatment process at which the sample was collected.
Sample was collected:
f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both
Chronic toxicity
Acute toxicity
g. Provide the type of test performed.
Static
Static -renewal
Flow -through
h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source.
Laboratory water
Receiving water
i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used.
Fresh water
Salt water
j. Give the percentage effluent used for all concentrations in the test series.
•
k. Parameters measured during the test. (State whether parameter meets test method specifications)
pH
Salinity
Temperature
Ammonia
Dissolved oxygen
I. Test Results.
Acute:
Percent survival in 100%
effluent
LC50
95% C.I.
%
%
Control percent survival
Other (describe)
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 16 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Chronic:
NOEC
OA
IC25
OA
Control percent survival
Ok
Other (describe)
m. Quality Control/Quality Assurance.
Is reference toxicant data available?
Was reference toxicant test within
acceptable bounds?
What date was reference toxicant test
run (MM/DD/YYYY)?
Other (describe)
E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation?
® Yes ❑ No If yes, describe: The cause of the failed toxicity tests is being evaluated by Meritech Inc. The study is
ongoing; however it is believed that waste from Industrial users is the cause for the failed toxicity tests. Additional information is included with
the attached test results.
E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the
cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary
of the results.
Date submitted:
/ / (MM/DD/YYYY)
Summary of results: (see instructions)
END OF PART E.
TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINEFWHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 17 of 22

Part F
Industrial User Discharges
and RCRA/CERCLA Wastes

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VWVfP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL- APPLICATION INFORMATION
PART F.INDUSTRIAL`USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,
complete part F.
GENERAL INFORMATION:
F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program?
® Yes ❑ No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (ClUs). Provide the number
industrial users that discharge to the treatment works.
a. Number of non -categorical SIUs. 4
or other remedial wastes must
of each of the following types of
questions F.3 through F.8 and
b. Number of Gills.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: Umicore Cobalt Products
Mailing Address: 17180 Airport Road
Maxton, NC 28364
F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Chemical Processing
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): Cobalt Carbonate and Cobalt Salts
Raw material(s): Cobalt, Sodium, and Chloride
F.6. Flow Rate.
a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the
day (gpd) and whether the discharge is continuous or intermittent.
16,000 gpd (X continuous or intermittent)
collection system in gallons per
into the collection system
•
b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
750 gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ® Yes ❑ No
b. Categorical pretreatment standards ❑ Yes ❑ No
If subject to categorical pretreatment standards, which category and subcategory?
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 18 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
❑ Yes ® No If yes, describe each episode.
RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE:
F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?
❑ Yes ® No (go to F.12)
F.10. Waste transport. Method by which RCRA waste is received (check all that apply):
❑ Truck ❑ Rail 0 Dedicated Pipe
F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units).
EPA Hazardous Waste Number Amount Units
CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
❑ Yes (complete F.13 through F.15.) ® No -
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in
the next five years).
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if
known. (Attach additional sheets if necessary.)
F.15. Waste Treatment.
a. Is this waste treated (or will be treated) prior to entering the treatment works?
❑ Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
b. Is the discharge (or will the discharge be) continuous or intermittent?
❑ Continuous ❑ Intermittent If intermittent, describe discharge schedule.
END OF PART F.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS.
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 19 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VWVfP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION INFORMATION
PARTF.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,
complete part F.
GENERAL INFORMATION:
F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program?
® Yes ❑ No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number
industrial users that discharge to the treatment works.
c. Number of non -categorical Sills. 4
or other remedial wastes must
of each of the following types of
questions F.3 through F.8 and
d. Number of CIUs.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: Scotland Manufacturing
Mailing Address: Laurinburg-Maxton Airport Road (P.O. Box 1067)
Maxton, NC 28353
F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Forming and cleaning of deep drawn steel
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): Stamped Metal Products
Raw material(s): Steel and various solvents '
F.6. Flow Rate.
c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into
day (gpd) and whether the discharge is continuous or intermittent.
54,000 gpd (X continuous or intermittent)
the collection system in gallons per
into the collection system
d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
8,000 gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ® Yes ❑ No
b. Categorical pretreatment standards ❑ Yes ❑ No
If subject to categorical pretreatment standards, which category and subcategory?
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 20 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
. Lumber
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
❑ Yes E No If yes, describe each episode.
RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE:
F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?
❑ Yes E No (go to F.12)
F.10. Waste transport. Method by which RCRA waste is received (check all that apply):
❑ Truck 0 Rail ❑ Dedicated Pipe
F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units).
EPA Hazardous Waste Number Amount Units
CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
❑ Yes (complete F.13 through F.15.) E No
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in
the next five years).
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if
known. (Attach additional sheets if necessary.)
F.15. Waste Treatment.
c. Is this waste treated (or will be treated) prior to entering the treatment works? ,
❑ Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
d. Is the discharge (or will the discharge be) continuous or intermittent?
❑ Continuous 0 Intermittent If intermittent, describe discharge schedule.
END OF PART F.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO.DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 21 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION INFORMATION
PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES ,
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,
complete part F.
GENERAL INFORMATION:
F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program?
® Yes ❑ No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (ClUs). Provide the number
industrial users that discharge to the treatment works.
e. Number of non -categorical SIUs. 4
or other remedial wastes must
of each of the following types of
questions F.3 through F.8 and
f. Number of ClUs.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: Railroad Friction Products Corporation
Mailing Address: 13601 Airport Rd.
Maxton, NC 28364
F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Manufacture brake pads and other products for railroad use.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): Equipment for Railway Use
Raw material(s):
F.6. Flow Rate.
e. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the
day (gpd) and whether the discharge is continuous or intermittent.
6,000 gpd (X continuous or intermittent)
collection system in gallons per
.
into the collection system
.
f. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
4,000 gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits IZI Yes 0 No
b. Categorical pretreatment standards 0 Yes ❑ No
If subject to categorical pretreatment standards, which category and subcategory?
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 22 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
❑ Yes ® No If yes, describe each episode.
RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE:
F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?
❑ Yes ® No (go to F.12)
F.10. Waste transport Method by which RCRA waste is received (check all that apply):
❑ Truck ❑ Rail ❑ Dedicated Pipe
F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units).
EPA Hazardous Waste Number Amount Units
CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
❑ Yes (complete F.13 through F.15.) ® No
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in
the next five years).
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if
known. (Attach additional sheets if necessary.)
F.15. Waste Treatment.
e. Is this waste treated (or will be treated) prior to entering the treatment works? •
❑ Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
f. Is the discharge (or will the discharge be) continuous or intermittent?
❑ Continuous 0 Intermittent If intermittent, describe discharge schedule.
END OF PART F.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 23 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WWTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION INFORMATION
PART F. INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatmentpworks receivingdischarges from significant industrial users or which receive RCRA,CERCLA, or other
9 9 remedial wastes must
complete part F.
GENERAL INFORMATION:
F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program?
® Yes ❑ No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (ClUs). Provide the number
industrial users that discharge to the treatment works.
g. Number of non -categorical SIUs. 4
of each of the following types of
h. Number of ClUs.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: House of Raeford Chicken Division
Mailing Address: 21501 Charles Craft Rd.
Maxton, NC 28364
F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Meat Processing
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the-SIU's
discharge.
Principal product(s): Processed Meat Products
Raw material(s):
F.6. Flow Rate.
g. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per
day (gpd) and whether the discharge is continuous or intermittent.
32,000 gpd (X continuous or intermittent)
h. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged
into the collection system
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
1,750 gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ® Yes 0 No
b. Categorical pretreatment standards 0 Yes 0 No •
If subject to categorical pretreatment standards, which category and subcategory?
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 24 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission WVVTP, NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
❑ Yes ❑ No If yes, describe each episode.
RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE:
F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe?
❑ Yes ® No (go to F.12)
i
F.10. Waste transport. Method by which RCRA waste is received (check all that apply):
❑ Truck 0 Rail ❑ Dedicated Pipe .
F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units).
EPA Hazardous Waste Number Amount Units
CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
❑ Yes (complete F.13 through F.15.) ® No
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in
the next five years).
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if
known. (Attach additional sheets if necessary.)
F.15. Waste Treatment.
g. Is this waste treated (or will be treated) prior to entering the treatment works?
❑ Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
h. Is the discharge (or will the discharge be) continuous or intermittent?
❑ Continuous 0 Intermittent If intermittent, describe discharge schedule.
END OF PART F.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 25 of 22

Part G
Combined Sewer Systems
(Not Applicable)

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VWUTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN: ,
Lumber
SUPPLEMENTAL APPLICATION INFORMATION
PART G. COMBINED SEWER SYSTEMS
If the treatment works has a combined sewer system, complete Part G.
G.1. System Map. Provide a map indicating the following: (may be included
a. All CSO discharge points.
b. Sensitive use areas potentially affected by CSOs (e.g., beaches,
outstanding natural resource waters).
c. Waters that support threatened and endangered species potentially
G.2. System Diagram. Provide a diagram, either in the map provided in G.1
includes the following information.
a. Location of major sewer trunk lines, both combined and separate
b. Locations of points where separate sanitary sewers feed into the
c. Locations of in -line and off-line storage structures.
d. Locations of flow -regulating devices.
e. Locations of pump stations.
CSO OUTFALLS:
with Basic Application Information)
drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and
affected by CSOs.
or on a separate drawing, of the combined sewer collection system that
sanitary.
combined sewer system. •
Complete questions G.3 through G.6 once for each CSO discharge point.
G.3. Description of Outfall.
a. Outfall number
'
b. Location
(City or town, if applicable) (Zip Code)
(County) (State)
(Latitude) (Longitude)
c. Distance from shore (if applicable) ft.
d. Depth below surface (if applicable) ft.
e. Which of the following were monitored during the last year for this
❑ Rainfall 0 CSO pollutant concentrations
❑ CSO flow volume 0 Receiving water quality
f. How many storm events were monitored during the last year?
G.4. CSO Events.
a. Give the number of CSO events in the last year.
events (0 actual or 0 approx.)
CSO?
0 CSO frequency
•
b. Give the average duration per CSO event.
hours (0 actual or ❑ approx.)
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22.
Page 26 of 22

FACILITY NAME AND PERMIT NUMBER:
Laurinburg-Maxton Airport Commission VVVVTP,
NC0044725
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
c. Give the average volume per CSO event.
million gallons (❑ actual or ❑ approx.)
d. Give the minimum rainfall that caused a CSO event in the last year
Inches of rainfall
G.5. Description of Receiving Waters.
a. Name of receiving water:
b. Name of watershed/river/stream system:
United State Soil Conservation Service 14-digit watershed code (if known):
c. Name of State Management/River Basin:
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
G.6. CSO Operations.
Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent or intermittent beach closings, permanent or
intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any applicable State water quality standard).
END OF PART G.
THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 27 of 22

Attachments

I
Attachment 1
DMR Data Summary
(September 2005 through September 2008)

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Attachment 2
Expanded Effluent Test Results

Environmental Laboratory
2401 W. 5th St. PO Box 589
Lumberton, NC 28358
Phone: [phone]
Lumberton, NC 28359
FAX: [phone]
Email: [e-mail]
/Of! `Cf
LAURINBURG MAXTON AIRPORT
16701 AIRPORT ROAD
MAXTON, NC 28364-
SAMPLE NUMBER- 38416
DATE SAMPLED- 09/21/06
DATE RECEIVED- 09/21/06
TIME RECEIVED- 1200
Page 1 of 1
FINAL REPORT OF ANALYSES
SAMPLE ID- EFFLUENT
PROJECT NAME: 17369
REPORT DATE: 10/16/06
SAMPLER- CHARLES VANDENBERG
DELIVERED BY- JOHNNY HESTER
SAMPLE MATRIX- WW
TIME SAMPLED- 0850
RECEIVED BY- THK
ANALYSIS
ANALYSIS METHOD DATE BY RESULT UNITS
OIL & GREASE (GRAVIMETRIC) SM5520B 10/02/06 THK
NITROGEN, AMMONIA, NH3/4 SM4500F 09/28/06 THK
LABORATORY DIRECTOR / '»
6.4 MG/L
0.1 MG/L
QUAL DET.
CODE LIMIT
NCDENR DWQ # 37, NCDENR DW #37781
1.0
0.1.

ENVIRONMENTAL
SCIENCE CORP.
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
12065 Lebanon Rd.
Mt. Juliet, TN 37]22
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Report Summary
Monday October 02, 2006
Report Number: L2 6 2161
Samples Received: 0 9/ 2 2/ 0
Client Project: TBL-17369
Description: LMAC
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Reviewed By:
Laboratory Certification Numbers
Z'h 11 �ouchr, SC Rep�tative
A2LA - 1461-01, AIHA - 09227, AL - 40660, CA - I-2327, CT - PH-0197, FL - E87487
GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140
NJ - TN002, SC - 84004, TN - 2006, VA - 00109, WV - 233
AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910
This report may not be reproduced, except in full, without written approval from Environmental Science Corp.

ENVIRONMENTAL
SCIENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received September 22, 2006
Description 17369 - LMAC
Sample ID EFFLUENT
Collected By Charles Vandenberg
Collection Date : 09/21/06 08:50
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5659
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 02, 2006
ESC Sample # : L262161-01
Site ID .
Project # : TBL-17369
Parameter Result Det. Limit Units Method Date Dil.
Cyanide 0.0082 0.0050 mg/1 335.3 09/27/06 1
Hardness BDL 30. mg/1 130.1 09/25/06 1
Nitrate -Nitrite 16. 0.10 mg/1 353.2 09/26/06 1
Total Phenol by 4AAP 0.064 0.040 mg/1 420.2 09/26/06 1
Phosphorus,Total 24. 1.0 mg/1 365.1 09/26/06 10
Kjeldahl Nitrogen, TKN BDL 0.50 mg/1 351.2 09/27/06 1
Dissolved Solids 440 1.0 mg/1 160.1 09/28/06 1
Thallium BDL 0.0010 mg/1 200.8 09/30/06 1
ercury BDL 0.00020 mg/1 245.1 09/25/06 1
Antimony BDL 0.020 mg/1 200.7 09/29/06 1
Arsenic BDL 0.020 mg/1 200.7 09/29/06 1
Beryllium BDL 0.0020 mg/1 200.7 09/29/06 1
Cadmium BDL 0.0050 mg/1 200.7 09/29/06 1
Chromium BDL 0.010 mg/1 200.7 09/29/06 1
Copper BDL 0.020 mg/1 200.7 09/29/06 1
Lead BDL 0.0050 mg/1 200.7 09/29/06 1
Nickel BDL 0.020 mg/1 200.7 09/29/06 1
Selenium BDL 0.020 mg/1 200.7 09/29/06 1
Silver BDL 0.010 mg/1 200.7 09/29/06 1
Zinc 0.030 0.030 mg/1 200.7 09/29/06 1
PP Volatile Organics
Acrolein BDL 0.050 mg/1 624 09/29/06 1
Acrylonitrile BDL 0.010 mg/1 624 09/29/06 1
Benzene BDL 0.0010 mg/1 624 09/29/06 1
Bromodichloromethane 0.0010 0.0010 mg/1 624 09/29/06 1
Bromoform BDL 0.0010 mg/1 624 09/29/06 1
Bromomethane BDL 0.0010 mg/1 624 09/29/06 1
Carbon tetrachloride BDL 0.0010 mg/1 624 09/29/06 1
Chlorobenzene BDL 0.0010 mg/1 624 09/29/06 1
Chlorodibromomethane BDL 0.0010 mg/1 624 09/29/06 1
Chloroethane BDL 0.0010 mg/1 624 09/29/06 1
2-Chloroethyl vinyl ether BDL 0.050 mg/1 624 09/29/06 1
Chloroform 0.0052 0.0050 mg/1 624 09/29/06 1
Chloromethane BDL 0.0010 mg/1 624 09/29/06 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 1 of 6

ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received . September 22, 2006
Description 17369 - LMAC
Sample ID EFFLUENT
Collected By Charles Vandenberg
Collection Date : 09/21/06 08:50
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 02, 2006
ESC Sample # : L262161-01
Site ID .
Project # : TBL-17369
Parameter Result Det. Limit Units Method Date Dil.
1,1-Dichloroethane BDL 0.0010 mg/1 624 09/29/06 1
1,2-Dichloroethane BDL 0.0010 mg/1 624 09/29/06 1
1,1-Dichloroethene BDL 0.0010 mg/1 624 09/29/06 1
trans-1,2-Dichloroethene BDL 0.0010 mg/1 624 09/29/06 1
1,2-Dichloropropane BDL 0.0010 mg/1 624 09/29/06 1
cis-1,3-Dichloropropene BDL 0.0010 mg/1 624 09/29/06 1
L trans-1,3-Dichloropropene BDL 0.0010 mg/1 624 09/29/06 1
Ethylbenzene BDL 0.0010 mg/1 624 09/29/06 1
Methylene Chloride BDL 0.0050 mg/1 624 09/29/06 1
1,1,2,2-Tetrachloroethane BDL 0.0010 mg/1 624 09/29/06 1
Tetrachloroethene BDL 0.0010 mg/1 624 09/29/06 1
Toluene BDL 0.0050 mg/1 624 09/29/06 1
1,1,1-Trichloroethane BDL 0.0010 mg/1 624 09/29/06 1
1,1,2-Trichloroethane BDL 0.0010 mg/1 624 09/29/06 1
Trichloroethene BDL 0.0010 mg/1 624 09/29/06 1
Vinyl chloride BDL 0.0010 mg/1 624 09/29/06 1
Surrogate Recovery
Toluene-d8 83.2 % Rec. 624 09/29/06 1
Dibromofluoromethane 80.2 % Rec. 624 09/29/06 1
4-Bromofluorobenzene 98.4 % Rec. 624 09/29/06 1
625 Base/Neutrals w/ TIC
Acenaphthene BDL 0.010 mg/1 625 09/25/06 1
Acenaphthylene BDL 0.010 mg/1 625 09/25/06 1
Anthracene BDL 0.010 mg/1 625 09/25/06 1
Benzidine BDL 0.050 mg/1 625 09/25/06 1
Benzo(a)anthracene BDL 0.010 mg/1 625 09/25/06 1
Benzo(k)fluoranthene BDL 0.010 mg/1 625 09/25/06 1
Benzo(k)fluoranthene BDL 0.010 mg/1 625 09/25/06 1
Benzo(g,h,i)perylene BDL 0.010 mg/1 625 09/25/06 1
Benzo(a)pyrene BDL 0.010 mg/1 625 09/25/06 1
Bis(2-chlorethoxy)methane BDL 0.010 mg/1 625 09/25/06 1
Bis(2-chloroethyl)ether BDL 0.010 mg/1 625 09/25/06 1
Bis(2-chloroisopropyl)ether BDL 0.010 mg/1 625 09/25/06 1
4-Bromophenyl-phenylether BDL 0.010 mg/1 625 09/25/06 1
2-Chloronaphthalene BDL 0.010 mg/1 625 09/25/06 1
4-Chlorophenyl-phenylether BDL 0.010 mg/1 625 09/25/06 1
Chrysene BDL 0.010 mg/1 625 09/25/06 1
Dibenz(a,h)anthracene BDL 0.010 mg/1 625 09/25/06 1
1,2-Dichlorobenzene BDL 0.010 mg/1 625 09/25/06 1
1,3-Dichlorobenzene BDL 0.010 mg/1 625 09/25/06 1
1,4-Dichlorobenzene BDL 0.010 mg/1 625 09/25/06 1
3,3-Dichlorobenzidine BDL 0.010 mg/1 625 09/25/06 1
1,2-Diphenylhydrazine BDL 0.010 mg/1 625 09/25/06 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 2 of 6

i
1
IfrEnvironmental Science Corp.
` Laboratory Services
SEMI—VOLATILES ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Name: TBL Laboratory
SAMPLE ID.
L262161-01
Matrix: WATER ESC Sample NO: L262161-01
Date Collected: 09/21/2006
Date Analyzed: 09/25/2006
Lab File ID: 0925 11
Dilution Factor: 1
Tentatively Identified compounds (TIC) refers to substances not present in the
list of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards . TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist . Quantitation is accomplished by
relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram . TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number Of TICs Found: 4
CONCENTRATION UNITS:
mg/1
CAS NO.
COMPOUND
RT
EST. CONC.
QF
QA
000141-79-7
3—Penten-2—one, 4—methyl—
3.52
0.07
J
91
000127-18-4
Tetrachloroethylene
3.58
0.01
J
99
026456-76-8
2—Hexene, 3,5,5—trimethyl—
3.7
0.02
J
87
001576-87-0
2—Pentenal, (E)—
4.3
0.05
J
62
1

3
Company Name/Address:
Alternate billing information:
Ana
vsis/ e.o .
er/ereservati e
Chain of Custody
TBL Laboratory
Lumberton Box 589
- Lumberton .NC 28359
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12065 Lebanon Road
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TBL Laboratory
P.O. Box 589
- Lumberton NC 28359
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12065 Lebanon Road .
Mt Juliet, TN 37122
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Date Results Needed:
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1 NCF:

i of-; -Po /rrc-
ENVIRONMENTAL
SCIENCE CORP.
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
The analytical results in this report are based upo information su•plied
by you, the client, and are for your exclusive use. ,f you h
questions regarding this data package, please do noesit t-I c-E1.
Entire Report Reviewed By:
Laboratory Certification Numbers
-A2LA - 1461-01, AIHA - 09227, AL - 40660, CA - I-2327,, CT - PH-0197, FL - E87487
• GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140
NJ - TN002, SC - 84004, TN - 2006, VA - 00109., WV - 233
AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910
This report may not be reproduced, except in full, without written approval from Environmental Science Corp.
2 Samples Reported: 02/18/08 13:10 Printed: 02/18/08 13:19
Page 1 of 6
John
ac
epresen a ive

ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received February 08, 2008
Description
Sample ID EFFLUENT
Collected By Charles Vandenberg
Collection Date : 02/07/08 09:40
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814209__
Est. 1970
February 18, 2008
ESC Sample # : L331067-01
Site ID .
Project # : TBL-18936
Result Det. Limit Units Method Date Dil.
Nitrate 25. 0.20 mg/1 300.0 02/09/08 2
Nitrite BDL 0.10 mg/1 300.0 02/08/08 1
Cyanide 0.0051 0.0050 mg/1 4500CN-E 02/12/08 1
Hardness BDL 30. mg/1 130.1 02/12/08 1
Total Nitrogen 30. 0.50 mg/1 Calc. 02/11/08 1
Oil & Grease (Hexane Extr) BDL 5.6 mg/1 1664A 02/16/08 1
Total Phenol by 4AAP BDL 0.040 mg/1 420.1 02/13/08 1
Phosphorus,Total 11. 0.50 mg/1 365.1 02/14/08 5
Kjeldahl Nitrogen, TKN 4.8• 0'.50 mg/1 351.2 02/11/08 1
Dissolved Solids 1600 10. mg/1 2540C 02/13/08 1
Mercury BDL 0.00020 mg/1 7470A 02/11/08 1
Antimony 0.013 0.010 mg/1 6010B 02/09/08 1
Arsenic BDL 0.020 mg/1 6010B 02/09/08 1
Beryllium BDL 0.0020 mg/1 6010B 02/09/08 1
Cadmium BDL 0.0050 mg/1 6010B 02/09/08 1
Chromium BDL 0.010 mg/1 6010B 02/09/08 1
Copper BDL 0.020 mg/1 6010B 02/09/08 1
Lead BDL 0.0050 mg/1 6010B 02/09/08 1
Nickel BDL 0.020 mg/1 6010B 02/09/08 1
Selenium BDL 0.020 mg/1 6010B 02/09/08 1
Silver BDL 0.010 mg/1 6010B 02/09/08 1
Thallium BDL 0.020 mg/1 6010B 02/09/08 1
Zinc 0.034 0.030 mg/1 6010B 02/09/08 1
PP Volatile Organics
Benzene BDL 0.0010 mg/1 8260B 02/09/08 1
Bromodichloromethane BDL 0.0010 mg/1 8260B 02/09/08 1
Bromoform BDL 0.0010 mg/1 8260B 02/09/08 1
Bromomethane BDL 0.0050 mg/1 8260B 02/09/08 1
Carbon tetrachloride BDL 0.0010 mg/1 8260B 02/09/08 1.
Chlorobenzene BDL 0.0010 mg/1 8260B 02/09/08 1
Chlorodibromomethane BDL 0.0010 mg/1 8260B 02/09/08 1
Chloroethane BDL 0.0050 mg/1 8260B 02/09/08 1
2-Chloroethyl vinyl ether BDL 0.050 mg/1 8260B 02/09/08 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 2 of 6

ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
Sample ID
Collected By
Collection Date :
Parameter
February 08, 2008
EFFLUENT
Charles Vandenberg
02/07/08 09:40
Chloroform
Chloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethee
trans-1,2-Dichloroethee
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Surrogate Recovery
Toluene-d8
Dibromofluoromethane
4-Bromofluorobenzene
Base/Neutral Extractables
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis (2-chlorethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
REPORT OF ANALYSIS
Result
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
100.
108.
95.1
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Limit(PQL)
. Det. Limit .Units
0.0050
0.0025
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0050
0.0010
0.0010
0.0050
0.0010
0.0010
0.0010
0.0010
0.0011
0.0011
0.0011
0.056
0.0011
0.0011
0.0011
0.0011
0.0011
0.011
0.011
0.011
0.011
0.011
0.011
0.0011
0.0011
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-08142'89
Est. 1970
February 18, 2008
ESC Sample # : L331067-01
Site ID .
Project # : TBL-18936
Method
•
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 82605
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
mg/1 8260B
% Rec. 8260B
% Rec. 8260B
% Rec. 8260B
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
mg/1 625
Date Dil.
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/09/08 1
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
02/12/08 1.11
Page 3 of 6

ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
Sample ID
Collected By
Collection Date :
February 08, 2008
EFFLUENT
Charles Vandenberg
02/07/08 09:40
REPORT OF ANALYSIS
Parameter Result
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
1,2-Diphenylhydrazine
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocy-clopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
Nitrobenzene-d5
2-Fluorobiphenyl
p-Terphenyl-d14
Phenol-d5
2-Fluorophenol
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
0.0029
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
75.2
70.4
82.0
29.2
45.0
Limit(PQL)
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289.
Eat. 1970
February 18, 2008
ESC Sample # : L331067-01
Site ID .
Project # : TBL-18936
Det. Limit Units Method
0.011 mg/1 625
0.011 mg/1 625
0.011 . mg/1 625
0.011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.0011 mg/1 625
0.011 mg/1 625
0.0011 mg/1 625
0.011 mg/1 625
0.056 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.0011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
0.011 mg/1 625
% Rec
% Rec
% Rec
% Rec
% Rec
625
625
625
625
625
Date Dil.
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
02/12/08
Page 4 of 6

ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
Sample ID
Collected By
Collection Date
February 08, 2008
EFFLUENT
Charles Vandenberg
02/07/08 09:40
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
'Tax I.D. 62-08142$9..
Est. 1970
February 18, 2008
ESC Sample # : L331067-01
Site ID .
Project # : TBL-18936
Parameter Result Det. Limit Units Method
Date Dil.
2,4,6-Tribromophenol 78.6
% Rec. 625
02/12/08 1.11
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 02/18/08 13:10 Printed: 02/18/08 13:41
Page 5 of 6
i

ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received February 08, 2008
Description
Sample ID TRIP BLANK
Collected By Charles Vandenberg
Collection Date : 02/07/08 00:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax Z.D. 62-0814'2.89
Est. 1970
February 18, 2008
ESC Sample # : L331067-02
Site ID .
Project # : TBL-18936
Result Det, Limit Units Method Date Dil.
PP Volatile Organics
Benzene BDL 0.0010 mg/1 8260B 02/10/08 1
Bromodichloromethane BDL 0.0010 mg/1 8260B 02/10/08 1
Bromoform BDL 0.0010 mg/1 8260B 02/10/08 1
Bromomethane BDL 0.0050 mg/1 8260B 02/10/08 1
Carbon tetrachloride BDL 0.0010 mg/1 8260B 02/10/08 1
Chlorobenzene BDL 0.0010 mg/1 8260B 02/10/08 1
Chlorodibromomethane BDL 0.0010 mg/1 8260B 02/10/08 1
Chloroethane BDL 0.0050 mg/1 8260B 02/10/08 1
2-Chloroethyl vinyl ether BDL 0.050 mg/1 8260B 02/10/08 1
Chloroform BDL 0.0050 mg/1 8260B 02/10/08 1
Chloromethane BDL 0.0025 mg/1 8260B 02/10/08 1
1,2-Dichlorobenzene BDL 0.0010 mg/1 8260B 02/10/08 1
1,3-Dichlorobenzene BDL 0.0010 mg/1 8260B 02/10/08. 1
1,4-Dichlorobenzene BDL 0.0010 mg/1 8260B 02/10/08 1
1,1-Dichloroethane BDL 0.0010 mg/1 8260B 02/10/08 1
1,2-Dichloroethane BDL 0.0010 mg/1 8260B 02/10/08 1
1,1-Dichloroethene BDL 0.0010 mg/1 8260B 02/10/08 1
trans-1,2-Dichloroethene BDL 0.0010 mg/1 8260B 02/10/08 1
1,2-Dichloropropane BDL 0.0010 mg/1 8260B 02/10/08 1
cis-1,3-Dichloropropene BDL 0.0010 mg/1 8260B 02/10/08 1
trans-1,3-Dichloropropene BDL 0.0010' mg/1 8260B 02/10/08 1
Ethylbenzene BDL 0.0010 mg/1 8260B 02/10/08 1
Methylene Chloride BDL 0.0050 mg/1 8260B 02/10/08 1
1,1,2,2-Tetrachloroethane BDL 0.0010 mg/1 8260B 02/10/08 1
Tetrachloroethene BDL 0.0010 mg/1 8260B 02/10/08 1
Toluene BDL 0.0050 mg/1 8260B 02/10/08 1
1,1,1-Trichloroethane BDL 0.0010 mg/1 8260B 02/10/08 1
1,1,2-Trichloroethane BDL 0.0010 mg/1 8260B 02/10/08 1
Trichloroethene BDL 0.0010 mg/1 8260B 02/10/08 1
Vinyl chloride BDL 0.0010 mg/1 8260B 02/10/08 1
Surrogate Recovery
Toluene-d8 98.3 % Rec. 8260B 02/10/08 1
Dibromofluoromethane 110. % Rec. 8260B 02/10/08 1
4-Bromofluorobenzene 101. W Rec. 8260B 02/10/08 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 02/18/08 13:10 Printed: 02/18/08 13:41
Page 6 of 6

Alternate billing information:
TBL Laboratory
P.O. Box 589
Lumberton,NC 28359
Report:
LM
Phone(910) 718_6190
FAX [phone]
Collected by:
(print):
Collected by (signal re):
C6.42)
•
Sample ID
Project name:
Client Project #:
/__-- ('9-1
/A.
Site/Facility ID#:
ESC Key:
Rush? ( Lab MUST Be Notified)
Same Day 200%
Next Day 100%
Two Day 50%
Comp/Grab '
Matrix
Date Results Needed:
FAX? No Yes
1111"1"11111111
i ,} kg
Eminnumm-.1..Millinglal
11611111111.1.1111111111111111
MUM 111111111111BIIIMME
.1111111111111111111111111111
11111111111111111111111111111.11111111111111
11.111011■111111111111111111111m1
No.
Cntrs
Analysis/Container/Preservative
••'.'"A• " OIV5oflj GW- Pm, r••••• • •
Remarks:
Relin tjished by: (Signature)
--atead
Relinquished by:
Relinquis
(Signij
Date:
Date:
a:71-6-7
Dale:
6
Depth
Time: Receive
D:3T—
Timp: Re *v
/?)-5 .>7)
Time:
Date
Time
water DT other
y: ( Ignature)
Receiv f
(Signet
Iab
1--
Date:
i•
Chain of Custod
Page of
Prepared by:
4* ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Road
Mt Juliet, TN 37122
Phnne [phone]
Phone [phone]
FAX [phone]
0:4tWii?.--OLLAB
fg-ITifittplate:/Prelogin
-4Cdolerr#:
•-j.L.:tilpped Via:
•
Remarks/Contaminant
o C
L
(lab use only
Sample A (Iab only:
to67,
z
PH Temp
Flow Other
Bottles R
Time:
_
Condition:
pH Checked:
(".
(lab use only)
NCF:
EMI

T' lD�b /k4.P
ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Report < S;ummar
Thursday:October
Report :Number: .:L3.6765`6
Sample.s:>.:Receved::::::1.0:;:/;0:11.08
Client Project:.TBL-19602
Description: TBL-1:96O2
The analytical results in this report are based upon r.t' supplied
by you, the client, and are for your exclusive use. a =n
questions regarding this data package, please do not --it- ;,�to all.
Entire Report Reviewed By:
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327
GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC
NJ - TN002, SC - 84004, TN - 2006, VA - 00109, WV - 2 3
AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910
John
epresen a ive
H-0197, FL - E87487
,DW21704, ND - R-140
This report may not be reproduced, except in full, without written approval from Environmental
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
1 Samples Reported: 10/09/08 14:05 Printed: 10/09/08 14:06
Page 1 of 7
Science Corp.

ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 09, 2008
ESC Sample # : L367656-01
Date Received October 01, 2008
Description TBL-19602
Site ID
Sample ID EFF
Project # : TBL-19602
Collected By Mickey D.
Collection Date : 09/30/08 10:30
Parameter Result Det. Limit Units Method Date Dil.
Nitrate 11. 0.10 mg/1 300.0 10/01/08 1
Nitrite BDL 0.10 mg/1 300.0 10/01/08 1
Cyanide BDL 0.0050 mg/1 4500CN-E 10/02/08 1
Oil & Grease (Hexane Extr) BDL 5.0 mg/1 1664A 10/03/08 1
Total Phenol by 4AAP BDL 0.040 mg/1 420.1 10/07/08 1
Phosphorus,Total 11. 0.50 mg/1 365.1 10/02/08 5
Kjeldahl Nitrogen, TKN 2.0 0.10 mg/1 351.2 10/06/08 1
Thallium BDL 0.0010 mg/1 200.8 10/08/08 1
Mercury BDL 0.00020 mg/1 245.1 10/03/08 1
Antimony BDL 0.020 mg/1 200.7 10/08/08 1
Arsenic BDL 0.020 mg/1 200.7 10/08/08 1
Beryllium BDL 0.0020 mg/1 200.7 10/08/08 1
Cadmium BDL 0.0050 mg/1 200.7 10/08/08 1
Chromium BDL 0.010 mg/1 200.7 10/08/08 1
Copper BDL 0.020 mg/1 200.7 10/08/08 1
Lead BDL 0.0050 mg/1 200.7 10/08/08 1
Nickel BDL 0.020 mg/1 200.7 10/08/08 1
Selenium BDL 0.020 mg/1 200.7 10/08/08 1
Silver BDL 0.010 mg/1 200.7 10/08/08 1
Zinc BDL 0.030 mg/1 200.7 10/08/08 1
PP Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0050 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0050 mg/1 624 10/05/08 1
BDL 0.050 mg/1 624 10/05/08 1
BDL 0.0050 mg/1 624 10/05/08 1
BDL 0.0025 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL 0.0010 mg/1 624 10/05/08 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
L367656-01 (PESTICIDES/PCBS) - Dilution due to matrix
Page 2 of 7

410
ENVIRONMENTAL
SCIENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
Sample ID
October 01, 2008
TBL-19602
EFF
Collected By Mickey D.
Collection Date : 09/30/08 10:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 09, 2008
ESC Sample # : L367656-01
Site ID .
Project # : TBL-19602
Parameter Result Det. Limit Units Method Date Dil.
1,1-Dichloroethane BDL 0.0010 mg/1 624 10/05/08 1
1,2-Dichloroethane BDL 0.0010 mg/1 624 10/05/08 1
1,1-Dichloroethene BDL 0.0010 mg/1 624 10/05/08 1
trans-1,2-Dichloroethene BDL 0.0010 mg/1 624 10/05/08 1
1,2-Dichloropropane BDL 0.0010 mg/1 624 10/05/08 1
cis-1,3-Dichloropropene BDL 0.0010 mg/1 624 10/05/08 1
trans-1,3-Dichloropropene BDL 0.0010 mg/1 624 10/05/08 1
Ethylbenzene BDL 0.0010 mg/1 624 10/05/06 1
Methylene Chloride BDL 0.0050 mg/1 624 10/05/08 1
1,1,2,2-Tetrachloroethane BDL 0.0010 mg/1 624 10/05/08 1
Tetrachloroethene BDL 0.0010 mg/1 624 10/05/08 1
Toluene BDL 0.0050 mg/1 624 10/05/08 1
i 1,1,1-Trichloroethane BDL 0.0010 mg/1 624 10/05/08 1
1,1,2-Trichloroethane BDL 0.0010 mg/1 624 10/05/08 1
Trichloroethene BDL 0.0010 mg/1 624 10/05/08 1
Vinyl chloride BDL 0.0010 mg/1 624 10/05/08 1
Surrogate Recovery
Toluene-d8 97.1 % Rec. 8260B 10/05/08 1
Dibromofluoromethane 103. % Rec. 8260B 10/05/08 1
a,a,a-Trifluorotoluene 97.6 % Rec. 8260B 10/05/08 1
4-Bromofluorobenzene 97.9 % Rec. 8260B 10/05/08 1
Pesticide/PCBs
Aldrin BDL 0.0050 mg/1 608 10/03/08 10
Alpha BHC BDL 0.0050 mg/1 608 10/03/08 10
Beta BHC BDL 0.0050 mg/1 608 10/03/08 10
Delta BHC BDL 0.0050 mg/1 608 10/03/08 10
Gamma BHC BDL 0.0050 mg/1 608 10/03/08 10
Chlordane BDL 0.050 mg/1 608 10/03/08 10
4,4-DDD BDL 0.0050 mg/1 608 10/03/08 10
4,4-DDE BDL 0.0050 mg/1 606 10/03/08 10
4,4-DDT BDL 0.0050 mg/1 608 10/03/08 10
Dieldrin BDL 0.0050 mg/1 608 10/03/08 10
Endosulfan I BDL 0.0050 mg/1 608 10/03/08 10
Endosulfan II BDL 0.0050 mg/1 608 10/03/08 10
Endosulfan sulfate BDL 0.0050 mg/1 606 10/03/08 10
Endrin BDL 0.0050 mg/1 608 10/03/08 10
Endrin aldehyde BDL 0.0050 mg/1 608 10/03/08 10
Endrin ketone BDL 0.0050 mg/1 608 10/03/06 10
Heptachlor BDL 0.0050 mg/1 606 10/03/08 10
Heptachlor epoxide BDL 0.0050 mg/1 608 10/03/08 10
Hexachlorobenzene BDL 0.0050 mg/1 608 10/03/08 10
Methoxychlor BDL 0.0050 mg/1 608 10/03/08 10
Toxaphene BDL 0.10 mg/1 608 10/03/08 10
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
L367656-01 (PESTICIDES/PCBS) - Dilution due to matrix
Page 3 of 7
i

410
ENVIRONMENTAL
S C I ENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
Sample ID
October 01, 2008
TBL-19602
EFF
Collected By Mickey D.
Collection Date : 09/30/08 10:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 09, 2008
ESC Sample # : L367656-01
Site ID .
Project # : TBL-19602
Result Det. Limit Units Method Date Dil.
PCB 1016 BDL 0.0050 mg/1 608 10/03/08 10
PCB 1221 BDL 0.0050 mg/1 608 10/03/08 10
PCB 1232 BDL 0.0050 mg/1 608 10/03/08 10
PCB 1242 BDL 0.0050 mg/1 608 10/03/08 10
PCB 1248 BDL 0.0050 mg/1 608 10/03/08 10
PCB 1254 BDL 0.0050 mg/1 608 10/03/08 10
PCB 1260 BDL 0.0050 mg/1 608 10/03/08 10
Pest/PCBs Surrogates
Decachlorobiphenyl 57.3 % Rec. 608 10/03/08 10
Tetrachloro-m-xylene 54.4 % Rec. 608 10/03/08 10
PP Base/Neutral Extractables
Acenaphthene BDL 0.0010 mg/1 625 10/02/08 1
Acenaphthylene BDL 0.0010 mg/1 625 10/02/08 1
Anthracene BDL 0.0010 mg/1 625 10/02/08 1
Benzidine BDL 0.050 mg/1 625 10/02/08 1
Benzo(a)anthracene BDL 0.0010 mg/1 625 10/02/08 1
Benzo(b)fluoranthene BDL 0.0010 mg/1 625 10/02/08 1
Benzo(k)fluoranthene BDL 0.0010 mg/1 625 10/02/08 1
Benzo(g,h,i)perylene BDL 0.0010 mg/1 625 10/02/08 1
Benzo(a)pyrene BDL 0.0010 mg/1 625 10/02/08 1
Bis(2-chlorethoxy)methane BDL 0.010 mg/1 625 10/02/08 1
Bis(2-chloroethyl)ether BDL 0.010 mg/1 625 10/02/08 1
Bis(2-chloroisopropyl)ether BDL 0.010 mg/1 625 10/02/08 1
4-Bromophenyl-phenylether BDL 0.010 mg/1 625 10/02/08 1
2-Chloronaphthalene BDL 0.010 mg/1 625 10/02/08 1
4-Chlorophenyl-phenylether BDL 0.010 mg/1 625 10/02/08 1
Chrysene BDL 0.010 mg/1 625 10/02/08 1
Dibenz(a,h)anthracene BDL 0.010 mg/1 625 10/02/08 1
3,3-Dichlorobenzidine BDL 0.010 mg/1 625 10/02/08 1
2,4-Dinitrotoluene BDL 0.010 mg/1 625 10/02/08 1
2,6-Dinitrotoluene BDL 0.010 mg/1 625 10/02/08 1
Fluoranthene BDL 0.0010 mg/1 625 10/02/08 1
Fluorene BDL 0.0010 mg/1 625 10/02/08 1
Hexachlorobenzene BDL 0.010 mg/1 625 10/02/08 1
Hexachloro-1,3-butadiene BDL 0.010 mg/1 625 10/02/08 1
Hexachlorocyclopentadiene BDL 0.010 mg/1 625 10/02/08 1
Hexachloroethane BDL 0.010 mg/1 625 10/02/08 1
Indeno(1,2,3-cd)pyrene BDL 0.0010 mg/1 625 10/02/08 1
Isophorone BDL 0.010 mg/1 625 10/02/08 1
Naphthalene BDL 0.0010 mg/1 625 10/02/08 1
Nitrobenzene BDL 0.010 mg/1 625 10/02/08 1
n-Nitros?dimethylamine BDL 0.050 mg/1 625 10/02/08 1
n-Nitrosodiphenylamine BDL 0.010 mg/1 625 10/02/08 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
L367656-01 (PESTICIDES/PCBS) - Dilution due to matrix
Page 4 of 7

•r:
ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
Sample ID
October 01, 2008
TBL-19602
EFF
Collected By Mickey D.
Collection Date : 09/30/08 10:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 09, 2008
ESC Sample # : L367656-01
Site ID .
Project # : TBL-19602
Result Det. Limit Units Method Date Dil.
n-Nitrosodi-n-propylamine BDL 0.010 mg/1 625 10/02/08 1
Phenanthrene BDL 0.0010 mg/1 625 10/02/08 1
Benzylbutyl phthalate BDL 0.0010 mg/1 625 10/02/08 1
Bis(2-ethylhexyl)phthalate 0.0014 0.0010 mg/1 625 10/02/08 1
Di-n-butyl phthalate BDL 0.0010 mg/1 625 10/02/08 1
Diethyl phthalate BDL 0.0010 mg/1 625 10/02/08 1
Dimethyl phthalate BDL 0.0010 mg/1 625 10/02/08 1
Di-n-octyl phthalate BDL 0.0010 mg/1 625 10/02/08 1
Pyrene BDL 0.0010 mg/1 625 10/02/08 1
1,2,4-Trichlorobenzene BDL 0.010 mg/1 625 10/02/08 1
PP Acid Extractables
4-Chloro-3-methylphenol BDL 0.010 mg/1 625 10/02/08 1
2-Chlorophenol BDL 0.010 mg/1 625 10/02/08 1
2,4-Dichlorophenol BDL 0.010 mg/1 625 10/02/08 1
2,4-Dimethylphenol BDL 0.010 mg/1 625 10/02/08 1
4,6-Dinitro-2-methylphenol BDL 0.010 mg/1 625 10/02/08 1
2,4-Dinitrophenol BDL 0.010 mg/1 625 10/02/08 1
2-Nitrophenol BDL 0.010 mg/1 625 10/02/08 1
4-Nitrophenol BDL 0.010 mg/1 625 10/02/08 1
Pentachlorophenol BDL 0.010 mg/1 625 10/02/08 1
Phenol BDL 0.010 mg/1 625 10/02/08 1
2,4,6-Trichlorophenol BDL 0.010 mg/1 625 10/02/08 1
Surrogate Recovery
2-Fluorophenol 16.9 % Rec. 8270C 10/02/08 1
Phenol-d5 13.9 % Rec. 8270C 10/02/08 1
Nitrobenzene-d5 23.1 % Rec. 8270C 10/02/08 1
2-Fluorobiphenyl 34.0 % Rec. 8270C 10/02/08 1
2,4,6-Tribromophenol 54.7 % Rec. 8270C 10/02/08 1
p-Terphenyl-d14 55.9 % Rec. 8270C 10/02/08 1
BDL - Below Detection Limit
Det. Limit -, Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/09/08 14:05 Printed: 10/09/08 14:06
L367656-01 (PESTICIDES/PCBS) - Dilution due to matrix
Page 5 of 7

Attachment A
List of Analytes with QC Qualifiers
Sample Work
Number Group
Sample
Type Analyte
Run
ID
Qualifier
L367656-01 WG386558 SAMP Cyanide R486104 W
WG386708 SAMP Aldrin R489305 0
WG386708 SAMP Alpha BHC R489305 0
WG386708 SAMP Beta BHC R489305 0
WG386708 SAMP Delta BHC R489305 0
WG386708 SAMP Gamma BHC R489305 0
WG386708 SAMP Chlordane R489305 0
WG386708 SAMP 4,4-DDD R489305 0
WG386708 SAMP 4,4-DDE R489305 0
WG386708 SAMP 4,4-DDT R489305 0
WG386708 SAMP •Dieldrin R489305 0
WG386708 SAMP Endosulfan I R489305 0
WG386708 SAMP Endosulfan II R489305 0
WG386708 SAMP Endosulfan sulfate R489305 0
WG386708 SAMP Endrin R489305 0
WG386708 SAMP Endrin aldehyde R489305 0
WG386708 SAMP Endrin ketone R489305 0
WG386708 SAMP Heptachlor R489305 0
WG386708 SAMP Heptachlor epoxide R489305 0
WG386708 SAMP Hexachlorobenzene R489305 0
WG386708 SAMP Methoxychlor R489305 0
WG386708 SAMP Toxaphene R489305 0
WG386708 SAMP PCB 1016 R489305 0
WG386708 SAMP PCB 1221 R489305 0
WG386708 SAMP PCB 1232 R489305 0
WG386708 SAMP PCB 1242 R489305 0
WG386708 SAMP PCB 1248 R489305 0
WG386708 SAMP PCB 1254 R489305 0
WG386708 SAMP PCB 1260 R489305 0
WG386515 SAMP Di-n-butyl phthalate R485986 J4
Page 6 of 7

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J4 The associated batch QC was outside the established quality control range
for accuracy.
0 (ESC) Sample diluted due to matrix interferences that impaired the ability
to make an accurate analytical determination. The detection limit is
elevated in order to reflect the necessary dilution.
W (ESC)-The laboratory analysis was from a sample collected in an improper
container
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected).
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the .group of analytes that are' chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 7 of 7

TBL Laboratory
P.O. Box 589
Lumberton,NC 28359
Report:
Phone[phone]
FAX: [phone]
Collected
(print):
Collected by (signatua):
Alternate billing information:
Project name:
Client Project #:
a/lc/Site/Facility ID#:
1157
Rush?
ESC Key:
( Lab MUST Be Notified )
Same Day 200%
Next Day. 100%
Two Day 50%
Date Results Needed:
FAX? No Yes
Sample ID
Comp/Grab
Matrix'
Depth
Date
9-16-aff
Time
No.
of
Cntrs
Analysis/Container/Preservative
•
Chain of Custody
Page of
Prepared by:
ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Road
Mt. Juliet, TN 37122
Phone [phone]
Phone [phone]
FAX [phone]
tr'sC,r3tair:;•'1.7BI3LAB
. •
,
i',1.1.1Template/Prelogin
?.400.110#:
(lab use only)
Remarks/Contaminant
Sample P (lab only)
•..
.•••;
•
• • •
\ion.
C E
p 13
0
'k; 0 I:1 EJ b
Z 13
0
11
C
9/0
d
'Matrix: SS - Soil/Solid GW Groundwater
Remarks:
Relinquish
•
.qui ed by:
Reit d by: (SIgntii
WN - WasteWa ter DW - Drinking Water OT - Other
Date:
260
Date:
trivbt,
Time:
//: f
Time:
UV, ID
Time:
Receics1 by: ( nature
Rece
ignatu
Reoa Ned: for•lab by:
(Signature)
pH Temp
Flow Other
--Samples returned via:0 UPS
FedEx C) Courier
Date:
cr•COndltion:
Bottles'RedelVed:i
Time:
pH Checked: NCF:
(lab use only)

Attachment 3
Toxicity Test Results
and
Toxicity Reduction Evaluation
Status Reports

01/16/2009 13:22 1336341522
MARTHA
PAGE 02/05
Paul Davis
Executive Director
Laurinburg Maxton Airport Commission
P.O. Box 31
Laurinburg, NC 28352
RE: LMAC Whole Effluent Toxicity investigation
August 27, 2008
Mr. Davis,
The following is a project update and a summary of our findings as well as an outline of proposed
further investigation.
introduction
Laurinburg Maxton Airport Commission (LMAC) retained Meritech, Inc. in June of 2008 to
investigate the repeated failures of quarterly Whole Effluent Toxicity (WET) Tests required for
compliance with the State environmental self -monitoring regulations. The pattern of consistent
failures began in 2007 and continues with several exceptions to the present moment.
Meritech personnel has reviewed the existing laboratory data, compliance records, and the
physical conditions of the LMAC waste water treatment system in order to determine the most
probable causes of high toxicity exhibited by the effluent from that facility. Major industrial
facilities discharging into LMAC plant were also visited by Meritech personnel in order to better
understand on -site wastewater management practices (see enclosed field notes).
Based nn this review several possible dues and areas of concern were identified_ We have
developed a specific investigation plan in order to identify possible avenues or toxicity reduction.
Summary of Findings
1. Based on the review of existing laboratory data it appears that elevated concentrations of
metal contaminants are the main reason for LMAC effluent toxicity. Relatively high
concentrations of various metals are routinely present in LMAC effluent. Meritech
performed a detailed WET study comparing the toxicity of the normal effluent and toxicity .
of the effluent treated with a chelating agent (EDTA) to remove metals. The results of this
study (see enclosed attachments) show that without metals, LMAC effluent exhibits low
toxicity, easily passing the standard WET test even at a concentration twice as high as
required by the State for this facility.

el/1b/2009 13:22 1336341522
MARTHA
HAUL b:V 05
2. Preliminary influent laboratory toxicity data shows that influent as collected from the North
Manhole is significantly Tess toxic than the South Manhole influent. We are suspecting
that industrial dischargers in that part 0f the LMAC wastewater collection system may be
significant contributors to LMAC WET problems.
3. LMAC compliance records show that operation and maintenance factors in the past, may
have at times contributed to the elevated effluent toxicity. An example would be the
broken bar screen, which in January of 2008 that the state said led to ammonia issues.
The failed January toxicity test was taken during the same week of high ammonia
readings.
Proposed Action Plan
1. Isolation of high toxicity factors.
Meritech will sample VINVTP Influent throughout the collection system in order to
isolate individual major Industrial dischargers in terms of their impact on toxicity. We
propose a multilevel sampling event targeting the north and south wings of the
system in addition to the four permitted industries, along with effluent from the
WWTP. We will run a metals scan and a toxicity analysis at each of these sites. If any
prove toxic we then may run a chelated analysis and perhaps organics analysis on
some of those samples also. From this we will try to identify the direction of the
toxicity sources within the LMAC collection system.
2. Additional review of both historical and current operation and maintenance
factors at the LMAC facility and those of industrial dischargers.
We would like to look more into the past O&M practices, when LMAC apparently had
much fewer problems with passing their quarterly WET tests.
Regards,
Kris Pawlak
Laboratory Manager
Meritech, Inc.
Ph: 336 342 4748
Fax: [phone]
Cell: 336 706 0287
Web: www.meritech-labs.com
Attachments

wir lo, Luu7 J. . LL lddbJ41b11
MARTHA
PAGE 04/05
Paul Davis
Executive Director
Laurinburg Maxton Airport Commission
16701 Airport rd.
Laurinburg, NC 28364
RE: LMAC Whole Effluent Toxicity Investigation
October 28, 2008
Mr. Davis,
The following is a current project update and a summary of our findings as well as an outline of
proposed further action.
Introduction
Laurinburg Maxton Airport Commission (LMAC) retained Meritech, Inc. in June of 2008 to
investigate the repeated-faiiures-0E-gaarterlp--Whelc Effluent Toxicity —WET). Thsts required for
compliance with the State environmental self -monitoring regulations. The pattem of failures
started in 2007 and continues with several exceptions to the present moment.
During the month of September Meritech personnel collected several 24-hour composite samples
from various points in the LMAC wastewater systcm. These samples ware subsequently
analyzed for a wide range of organic and inorganic contaminants, as well as Chronic Toxicity.
Analytical data was then reviewed by the Meritech team of specialists.
Based on the sample results and data review, several possible clues and areas of concem were
identified. Wo have developed a specific investigation plan in order to further narrow down the
sources of toxicity and Identify possible avenues of toxicity reduction.
Summary of Findings
1. Based on the review of the current Datch of laboratory data it appears that organic
contaminants as found in the LMAC collection system do not play a significant role in
the effluent toxicity. Organic contaminants of concern were found, especially in the
House of Raeford sample, yet that sample showed no toxicity as evident from the
enclosed test results. Testing for organics may not be used to a great extent in the
future Investigations.
2. Elevated concentrations of metal contaminants appear to be the main reason for
LMAC effluent toxicity. Relatively high concentrations of various metals were found in
all samples which exhibited high toxicity. High sulfate levels from the Umicore
sampling site are also a possible source of toxicity in the LMAC effluent.

01/16/2009 13:22 1336341522
MARTHA
PAGE 05/05
3. Um(core (Site 1) and RR (Railroad Friction) & Scotland (Site 3) samples 'showed high
toxicity and will be subject to additional testing. LMAC effluent (Site 7) as well as both
influent sites - South (Site 6) and North (Site 2) Manholes show significant toxicity.
These sites will continue to be tested.
4. House of Raeford (Site 4) and Butler (Site 5) samples showed no toxicity. These sites
will no longer be targeted in our investigation.
5. We have analyzed certain influent and effluent samples for sulfate and silica content.
At this point we am not sure how significant their presence is in samples showing
high toxicity. We will continue to evaluate this possibility and perform a series
chetatiOln tests on these Samples.
Proposed Action Plan
Continued isolation of high toxicity factors.
Meritech is currently investigating the role high sulfate levels may be playing in L IAC
effluent toxicity results. Sulfate laden waste is generated at the Umicore site and is
not likely be removed by their current pretreatment process. We are also looking at
other inorganic parameters, such as silica, as a possible contributing factor. Siiica
laden waste is generated at tha RR & Scotland site.
The picture which emerges at this time is that metals are the key toxicity factor,
primarily those discharged from Umicore and RR/Scotland sites.
From this point we are suggesting breaking down the RR & Scotland and the
Northern leg of the collection system into smaller segments to isolate the sources of
maximum toxicity. Although it appears that Umicore and Railroad Friction may be the
main contributor to the toxicity problem. we propose to monitor other elements in that
part of the system to eliminate them as possible sources of toxicity.
Regards,
Kris Pawlak
Laboratory Manager
Meritech, inc.
Ph: 336 342 4748
Fax: [phone]
CeII: 336 706 0287
Web: www.meritech-Iabs.com
Attachments

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/21/05
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
X i
Signatur of�tor 4in Responsible Charge
X /'
Signature of 'I0\ tory Supervisor
Comments:
* PASSED: -5.94% Reduction *
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
14
10
18
21
19
21
18
18
22
19
21
18
Adult (L) ive (D) ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
12
19
20
20
21
21
22
22
19
18
20
18
Adult (L)ive (D)ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = -5.94
% Mortality
Avg.Reprod.
0.00
Control
18.25
Control
8.33
Treatment 2
19.33
Treatment
2
Control CV
18.416%
% control orgs
producing 3rd
brood
83.3%
PASS FAI
Check One
pH
Control
Treatment 2
1st sample 1st sample 2nd sample
7.84
7.84
7.67
7.87
s
P1 t
a
H,
1st sample
I D.O.
Control
Treatment 2
e
n
d
7.75
7.12
7.15
7.17
8.03
7.90
7.89
7.78
7.89
7.84
7.81
7.78
s s
t e t e
a n a n
✓ d r d
t t
1st sample 2nd sample
7.44
6.75
7.40
7.15
7.20
7.40
7.60
7.38
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates
Complete This For Either Test
Test Start Date: 09/14/05
Collection (Start) Date
Sample 1: 09/12/05 Sample 2: 09/15/05
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 23.8 hrs L A A
U M M
Sample 2 X 23.8 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
46
179
489
497
<0.1
<0.1
1.4
1.3
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 = %
95% Confidence Limits
%
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Meritech ‹61--
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodaphnia dubia Incubator #:
Pipe #: 00 / County: aco.1' (CU'1a p� --
Date Start: �� f� Date End: q T;,Z J-Q 5
Time / Date of Culture Transfer: q•/3 • P C la'r 7W Time Start: // "1 Time End: 1c/A�,,t
Dilution Water: Lake Reidsville Time / Date Neonates Born: •) 3.. cl .5-- , ,,,►4—.A,Tel/l st Renewal Date: 1 -11D 'CS' Time: an a ..4
Test Organism Source: ir / Age of Neonates at Tes art: /. 1_ i/ape� 2nd Renewal Date:'; lei -0 5.--Time: 7; 30 AM
1 Randomized: QY ' N Culture Tray Temp: �C ; Analyst: ,,c_ Reviewed by: A c)-743,1,
Client: LvV14C
NPDES #:NGooqq-726—
Stirred / Aerated for D.O.: Y /
Control Organism Reproduction
Day #3 1 2 3
# Young Produced
C
c
C
-
-
C
•+ i
6 n,
♦v
e
11
67
1L
v
Adults Live / Dead
1-___ _Elf
Z
L.
L
L
L
L.
L
L_. L .
t_ __
C
2
6
1v 11
1L
# Young Produced
L
317
U
1,17-
t:i
-31 Q
j/7
0,
Vf
'.7
y f7
qp
Adults Live / Dead
L
L
i_
L
t_
L.
L
L ._
L-
L
C
L_
T _ /1-, •
1
2
7
9
# Young Produced
10
c'
-
9
to
/ci 1 D
7
C
/ y
iv
F
11
0
1L
r
Adults Live / Dead
L
L
L-
L-
L, (-
L.
1,--
U.
L_
Total Produced
l if
ID
11
�i
/'9
,2./
)
'
/
2_2
I q
,.1
he
ercent Control Producing 3rd Brood: 3, 3%
Treatment 2 Organism Reproduction
Effluent %:
a,6
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
O
C'
D
6,
c,
0
C,
e)
o
el
c,
tv
Adults Live / Dead
T__. 11f
L-
L
- .
L
L
L
L.
i_
L
C
L
# Young Produced
3
'•
%/6
Iflg
57-
`flf
V]7 .r//
10
46
3/i
L v
Adults Live / Dead
L
L
L
L.
L_
.L._
L.. t—
L.
i_
_ L
L
2
# Young Produced
¶
,
J v
-
' / d
_
9 r (
,
1 o '
10 11
/ q
1L
S
Adults Live / Dead
I
L
L_
L. L.
L_ C__
L___ C.-
L,_ L.
L
LTotal Produced 1)-
(9
),a
)0
o7.J
ai
.2-
,72-
•r?
/g
A
/f
Collection (Start) Dates:
Samplel: -1a_t5
Sample Type / Duration
Sample 1
Sample 2
13
Sample2: V/,57/0s
Test Transferred Fed
By:�By:
Day 0 / .-/i7y
,t Day I /IL
Day 2 AA- ft,4}
Day 3
Day 4 (v‘c
Day 5 rift ���LL
Terminated by: 1 `A--
100
pH.
tp . rl
Grab
151 Sample
Control
17, 84
7,gs 1
Treatment 2
r, 6 7
7•cf7
D.O.
l st Sample
Control
1], 15
-?.IL
Treatment 2
ri.1,5
7,13
Temp.
151 Sample
Control
A5.'1
'L7:1
Treatment 2
, 3
ZS•�
Start End
Comp
X
Duration
23.5
15t Sample
q,03
Igo
'1.70
1S1 Sample
(0. 7'
7,q0
1.15
151 Sample-
.0
2�
46.1
Start End
Day 6
2nd Sample
)T 81
7si
n,q8
2nd Sample
7.2
1.40
"TA,
MIS 2nd Sample
2C-b
A.
211. c-019 5
Start End
Comments:

�--1 (4,QL/v
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
91`9"
Contact:
Address:
City:
PO #
NPDES #: 1\1(40 44 72s
Phone:
Pipe Number:
County: Sc644,fi ,a State: 1\fG Zip: ig364
Type of Facility Generating Effluent:
Client Information
Client: Lo.vr;nburg-MaX }on
Qta ry Arne,•!-1-
1&7o I A�ro,•-�- .
Nckx+on
Sample Information
Sampling Site:
Sample Type:
Sampling Time:
LMA C, �F
Grab
START Date:
END Date:
Sample Chilled (Covered with Ice): Yes
Collector's Name (Print):
A i rper<k-
Collector's Signature:
✓ Composite # of Containers 2
G -1/-OS Time:
Time:
No
iirla✓� QS Van c e✓/ \e,(cF
1 A U J
Toxicity Test Information U
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Pimephales promelas:
Mysidopsis bahia:
Acute:
IWC:
i oxicity Test Concentration(s):
List Any Special Requirements:
Shipping Information
Relinquished By: 1R _ _ , , Date:
�� �A
Received By: d. 411 ate:
Relinquished :y 4, 7 ,,t,� R � ilate:
Received By: _ ,r's'fl �`� �, r? e:
Sample Temperature (C' Met
Sample Recciv
Received From:
* j.,- j , story
Received By: `'\(\�
Sample Temperature (C°):
91-1 - Time: q:3
Time:
Time:
Time:
ent: WT (p/u) UPS
PM
PM
ed-Ex
Date: C `13 Time:')` 4CAM
• 11 / i • `( Sample Condition: \ CccAQ
Re). by,

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
(�3
Client Information
Client: L MA C
Contact: C ,r A A r„ -+
Address: � -7�p ; r
City: M x%c4-ors
County: Sc/34-1,and State: C
Zip:
Type of Facility Generating Effluent: W -r- P
PO #
NPDES #: NCOO4y-1�5
Phone: $y y - cOt{ I
Pipe Number:
28'364
Sample Information
Sampling Site: LhIAC- e.
Sample Type: Grab V Composite
Sampling Time: START Date: q,- 5 _ps Time:
END Date: 9 - 16-05 Time:
Sample Chilled (Covered with Ice): Yes v/' No
Collector's Name (Print): C ,4-,r„rle s Va,nclenbP r5
Collector's Signature: actA,240 v -
# of ContainQrs 2
'• SD CAN1 PM
X;4b• AI PM
Toxicity Test Information
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
2 , 6%
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Samplp Tempera
Time: //'b °
Time:
Time:/,, eir AM
Time:A l:06'AM 1M
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circ1 %yg/ Other: "Q%.
ate:
Date:
Date:
Date:
Sample Receiving (Laboratory Use Only)
Received From: %)
Received By: C Daft_ Date:
Sample Temperature (C ): / Sampl
q_ti6.05
0 Time: 3-33 AM Pl3Tv
Condition: \ C/)

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 09/21/05
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
Reduction: -5.94%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 11'
Adult Male 0 0
Adult Dead 0 1
Adult Mortality 0.00% 8.33%
# Neonates 219 232
Mean # Neonates 18.250 19.333
Standard Deviation 3.361 2.674
Coefficient of Variation 18.416%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 0.92
Success is: survival
Critical b value = 8
11 > B
b = 11
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 C 10-8.2500 13 E 20 0.6667
2 E 12-7.3333 14 E 20 0.6667
3 C 14-4.2500 15 C 19 0.7500
4 E 18-1.3333 16 C 19 0.7500
5 E 18-1.3333 17 E 21 1.6667
6 E 19-0.3333 18 E 21 1.6667
7 E 19-0.3333 19 E 22 2.6667
8 C 18-0.2500 20 E 22 2.6667
9 C 18-0.2500 21 C 21 2.7500
10 C 18-0.2500 22 C 21 2.7500
11 C 18-0.2500 23 C 21 2.7500
12 E 20 0.6667 24 C 22 3.7500

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
n
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 3.7500 -8.2500 0.4493 12:0000
2 2.7500 -7.3333 0.3098 10.0833
3 2.7500 -4.2500 0.2554 7.0000
4 2.7500 -1.3333 0.2145 4.0833
5 2.6667 -1.3333 0.1807 4.0000
6 2.6667 -0.3333 0.1512 3.0000
7 1.6667 -0.3333 0.1245 2.0000
8 1.6667 -0.2500 0.0997 1.9167
9 0.7500 -0.2500 0.0764 1.0000
10 0.7500 -0.2500 0.0539 1.0000
11 0.6667 -0.2500 0.0321 0.9167
12 0.6667 0.6667 0.0107 0.0000
1
W X 167.8397
202.9167
Calculated W = 0.827 Critical W = 0.884
0.827 < 0.884
The reproduction data is not normally distributed
evaluated at a 99% confidence interval
Test Failed!
Wilcoxon Rank Sum Test
Rank Sum - Effluent Group(treatment): 167 Control Group: 133
Mann -Whitney U = 89.0
nl(treatment) = 12 n2(control) = 12
The critical value from TABLE A.15 (0.01 Level of T) for the above n values:
Critical .T = 109
167 > 109
The Sum of the Ranks of the effluent group is greater than the significant
value from the table. Therefore there is no significant difference between
the means of the effluent and control groups and the test passes.
TEST PASSES
Chronic Test PASSES
The reduction was less then 20%

Tk_
Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/14/05
Facility: LMAC
Laboratory
X //i�
NPDES#: NC0044725 Pipe#: 001 County:
erforming Test: MERITECH LABS, INC.
Signature o Ope
or in Responsible Charge
Signature of La or
y Supervisor
Comments:
* PASSED: 4.80% Reduction *
flWork Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Iri CONTROL ORGANISMS
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
20
17
19
19
17
19
21
20
19
20
18
20
Adult (L)ive (D)ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
19
18
16
20
16
19
19
20
16
20
18
17
Adult (L)ive (D)ead
Chronic Test Results
Calculated t = 1.577
Tabular t = 2.508
% Reduction = 4.80
% Mortality
Avg.Reprod.
0.00
Control
19.08
Control
0.00
Treatment
2
18.17
Treatment
2
Control CV
6.498%
% control orgs
producing 3rd
brood
100%
PASS FAIL
Check One
" pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample 1st sample 2nd sample
7.97
7.93
7.90
7.89
s
t
a
r
t
1st sample
e
n
d
7.74
7.65
7.65
7.78
7.92
7.90
7.95
7.86
7.80
7.89
7.83
7.81
s s
t e t e
a n a n
✓ d r d
t t
1st sample 2nd sample
7.78
7.65
7.83
7.60
7.82
7.65
7.83
7.66
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates
Complete This For Either Test
Test Start Date: 12/06/05
Collection (Start) Date
Sample 1: 12/05/05 Sample 2: 12/08/05.
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 24.1 hrs L A A
U M M
Sample 2 X 23.9 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
46
195
626
468
0.35
<0.1
0.5
0.5
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
% -- %
Method of Determination
Moving Average Probit
Spearman Karber - Other
start/end
1
Note: Please
Complete This
Section Also
start/end
Control
High
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 12/14/05
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
Reduction: 4.80%
CONTROL 2.6W Effluent
# Replicates 12 12
Female Live 12 12
Adult Male 0 0
Adult Dead 0 0
Adult Mortality 0.00% 0.00%
# Neonates 229 218
Mean # Neonates 19.083 18.167
Standard Deviation 1.240 1.586
Coefficient of Variation 6.498%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 E 16-2.1667 13 C 19-0.0833
2 E 16-2.1667 14 E 19 0.8333
3 E • 16 -2.1667 15 E 19 0.8333
4 C 17 -2.0833 16 E 19 0.8333
5 C 17-2.0833 17 C 20 0.9167
6 E 17-1.1667 18 C 20 0.9167
7 C 18-1.0833 19 C 20 0.9167
8 E 18-0.1667 20 C 20 0.9167
9 E 18-0.1667 21 E 20 1.8333
10 C 19-0.0833 22 E 20 1.8333
11 C 19-0.0833 23 E 20 1.8333
12 C 19-0.0833 24 C 21 1.9167

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 1.9167 -2.1667 0.4493 4.0834
2 1.8333 -2.1667 0.3098 4.0000
3 1.8333 -2.1667 0.2554 4.0000
4 1.8333 -2.0833 0.2145 3.9166
5 0.9167 -2.0833 0.1807 3.0000
6 0.9167 -1.1667 0.1512 2.0834
7 0.9167 -1.0833 0.1245 2.0000
8 0.9167 -0.1667 0.0997 1.0834
9 0.8333 -0.1667 0.0764 1.0000
10 0.8333 -0.0833 0.0539 0.9166
11 0.8333 -0.0833 0.0321 0.9166
12-0.0833 -0.0833 0.0107 0.0000
1
W = X 39.7522
44.5833
Calculated W = 0.892 Critical W = 0.884
0.892 a 0.884
The reproduction data is normally distributed
evaluated at a 99%- confidence interval.
Test Passes!
F test for Homogeneity of Variance
Effluent variance 2.5152
F = -
Control variance 1.5379
- 1.64
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
1.64 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
19.1 - 18.2-•
t - = 1.577
0.581
Degrees of freedom = 22
Critical t = 2.508
1.577 < 2.508
Test passed. There is not a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test PASSES

Meritech
113.
Pipe #: oo f County: .5 co+ 1cu' cL Date Start: I a - ( -05
NPDES #: j jc Op Time /Date of Culture Transfer: Date End: is-) 3.-p3�
Dilution Water: Lake Reidsville Time / Date Neonates Born: / _ `7„� �I`,',cg'4 Time Start: ,�)fS"rR? Time End: ,o ' ySifrr
�� • .S-� r%.3� g1 ir(//9,1 —,g'ispicAst Renewal Date: IA-8- 05 Time: (OLD Ain
Age of Neonates at Test Start: ,
Stirred / Aerated for D.O.: Y / o vg.,s 2nd Renewal Date: Ia- ► I - 05 Time: & y V)�-
d N Culture Tray Temp: Z 5°C Analyst: Reviewed by: F'Zdtc_
Collection (Start) Dates:
Incubator #:
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodaphnia dubia
Client: L_ IAA AC-
Test Organism Source: -2
Control Organism Reproduction
Da v #3 1
Randomized:
' u / 25 9 10 11 12
# Young Produced
0
0 0 OP
d&
c
0
O
d
O
Adults Live / Dead
*
t _
L.- Lr.
r L.
L
L_
L
t
L
I t--
1
Day #i , - -
5
# Young Produced
//L
S`�
1797
2/g
' f/I'
. ig
rfr
If
Adults Live / Dead
T ,, 4+-7
L
-
1_-.
-
L-
L.
L
L
L
L
3
10 11 12
3 // ait I
L. L t1
# Young Produced
f D
q
g
9
f
,
10
o y
yl� gli
L.. 1—
10
'//
Adults Live / Dead
L-
L—
c_.
I,
ig
L L
C_.
Total Produced
. 0'
/ 7
Pt
/ 9
1/7-
1
/
"go
/9 I. -0 I
ercent Control Producing 3rd Brood:
Treatment 2 Organism Reproduction
Effluent %:
11 12
2.G1%
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
6
O
()
(j
©
016
d-
D
I)0
Adults Live / Dead
1____
L_
L
L.--
L
L_
t
`
L
(—
1.0
Day #ii , - - -
# Young Produced
`9/7
4f ft
, $/
t f.
u
3/ /
,
L§
6
3(
y
' f/
Adults Live / Dead
L.
. L_
L
(__
L
L
I
L
3
10 11
L
12
3I7-
L
# Young Produced
g
g
-' o
0101
/
Plc6v
u
9 10
11 12
r/cOrAdults
//_
Live / Dead
L
L
L.,
(- . L
L
L
L—
L___
ITotal Produced
PI I IgI/b II.I!I5-oIrd I ©I!Y I/ I
.Comments:
Sample 1: .I- 6- 05
Sample Type / Duration
Sample 1
Sample 2
p
100%
pH
1158
7..2�
Grab
A 1st Sample
Control
Treatment 2
D.O.
Control
`1. 9'7
1.90
?,93
7.89
15t Sanple
11,1,4
Treatment 2
Temp.
Control
Treatment 2
'1.65
7 '18
15` Sample
a4.3
4 ,5
a4.a-
ALI.6
Start End
Sample 2: l - .-
Test Transferred
By:
Comp
Duration
2k..1
3, di
15` Sample
7.90
7,95
151 Sample
1.'78
I.83
7 60
151 Sample
a4.5
a4.3
as•o
Start
End
Fed
By:
Day 0 Nit -
Day l
Day 2 f -tp.
Day 3 /lb—
Day4 12%%"
Day 5
Day 6
Terminated by:
2nd Sample
)ram69
So
7 83
t &I
2nd Sample
78a
783
2nd Sample
a4. 9
Start
a(-1.3
a.7
End

Client Information
Client:
Contact:
Address: 1(o -Ai P; rfar-}- R
City: Max+ -oh Pipe Number:
County: Sce+lcne State: NC Zip: ?g a 6
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Laorinbvr - M ix4nn fa;f1tor+-
Type of Facility Generating Effluent: WW-rp
I aocpq (1
1BL- l U34y
PO #
NPDES #:
Phone: $ 41..E - 5 ng 1
Sample Information
Sampling Site: L IAACr Q
Sample Type: Grab Composite • # of Containers
Sampling Time: START Date: l 2 465 Time:PM
END Date: Time: $ : 3 5 (AM)PM
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): C a rl ,e 6 1J,r j p nbe,
Collector's Signature: Ja.14
Toxicity Test Information
Test Required: Chronic: t/ Test Organism: Ceriodaphnia Dubia: ✓
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
i oxicity Test Concentration(s):
List Any Special Requirements:
2.&QTo
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperature (C
ate: 1 Time: //:/ 6 AM PM
Date: % , Time: I l I 0 PM
Date: 1_. er Tim4:2Q IPM
Date: Time/Joy,
Method of SI3ienl: TC(p/u) Jp -.
Tx
Circ1I Tn 'Other: "
Sample Receiving (Laboratory Use Only)
Received From: hoiLp tck-
Received By: M.c (15L Date: \a J to Time: ^1 . / DAM
Sample Temperature (C°): Oc / O.c Sample Condition: \ C tea/

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: LMA L
Contact: G,, /4 e
Address: I jin A
-1 City: M
County: Srl,+10.1 State: 1,,Ic
Type of Facility Generating Effluent:
Zip:
W'ilTP
PO #
NPDES #:
Phone:
Pipe Number:
2R-z6u
Sample Information
Sampling Site: L 4AA<. e
Sample Type: Grab ' omposite # of Containers 2_
Sampling Time: START Date: 12-g - os Time: -g,35 (i$PM
END Date: 12-q -0 5 Time: ' g : -30 PM
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): artrieA e_n e
wn
Collector's Signature: e-)pc
Toxicity Test Information
Test Required: Chronic: f l'est Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Shipping Information
Relinquished By: • t_ ! _ V- L Date: 12 4 D S Time: 6 PM
Received By: 4111NNIIIK. ' Date: h. e Time: AD.' e' ' -- ; PM
Relinquished B �' R Date: Time:i2C069 PM
Received By: 4W��1Ji.�,0 Date: / 2/7/vs Time: 3 o s-•I • I PM
Sample Temperature (C'): (Of ethod of Shipment: WT 64 UPS ed-Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
' v � s Date: C4R,.1
Sample Temperature (C ): OSample Condition:

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/16/06
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory P rforming Test: MERITECH LABS, INC.
X
Signet r o Operator/ % n Responsible Charge
, I,
Signature of Laborato ?Supervisor
Comments:
* PASSED: 7.81% Reduction *
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
19
20
24
24
22
26
23
18
23
23
23
24
Adult (L) ive (D) ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
22
19
22
22
25
24
21
17
13
20
22
21
Adult (L)ive (D)ead
Chronic Test Results
Calculated t = 1.535
Tabular t = 2.508
% Reduction = 7.81
% Mortality
Avg.Reprod.
8.33
Control
22.42
Control
0.00
Treatment 2
20.67
Treatment
2
Control CV
10.324%
% control orgs
producing 3rd
brood
100%
PASS FAI
Check One
1st sample
pH
Control
Treatment 2
D.O.
Control
Treatment 2
7.83
7.96
7.93
7.88
s
t
a
r
t
1st sample
e
n
d
7.93
7.48
7.98
7.46
1st sample
7.92
7.97
7.83
7.86
2nd sample
7.89
7.91
7.75
7.80
s s
t e t e
a n a n
✓ d r d
t t
1st sample 2nd sample
7.70
7.60
7..68
7.50
7.84
7.71
7.80
7.67
LC50/Acute Toxicity Test
(Mortality expressed
as %, combining
replicates
Complete This For Either Test
Test Start Date: 03/08/06
Collection (Start) Date
Sample 1: 03/06/06 Sample 2: 03/09/06
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 03 hrs L A A
U M M
Sample 2 X 05 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
46
175
388
362
<0.1
<0.1
0.3
0.5
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
% -- %
Method of Determination
Moving Average Probit
Spearman Karber - Other -
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
pH
Organism Tested: Ceriodaphnia dubia Duration(hrs.):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Meritech -r ,i.
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodaphnia dubia
Client: L
Incubator #:
Pipe #: oo / County: S t.,?-riciANA Date Start:3 - k'p(P Date End: 3 -/$ OG
NPDES #: NL oc, try 7 2-5 Time / Date of Culture Transfer: 3, 7.e 1.2: /SP,ti Time Start: I (;w,t.,,. Time End: 8: Lis--,
:3
Dilution Water: Lake Reidsville Time / Date Neonates Born: , 7.0 6 y 1/S-pfr., ._. )ij ild., l st Renewal Date:` -10 -% Time: 7. 9S },,,1
Test Organism Source: # 1 Age of Neonates at Test Start: / - - 1.1njj 3 2nd Renewal Date: 3 - 1s-ot, Time: 8; 3p/4")
Stirred / Aerated for D.O.: Y 10 Randomized: ©/ N Culture Tray Ten4: Z5°C Analyst: ,yam Reviewed by: A//d-r----
Control Organism Reproduction
Day #3 1 2 3
# Young Produced
0
0
.00
0
D
0
0
0
O
D
O
Adults Live / Dead
L
I--
L
1.-
L
L
L
L_
L.
L
L
2
4
# Young Produced
of /
/7-
f
ry
LY6
Y/9
V.
0
W9
9/9
LilI,
VS
Adults Live / Dead
1-
t—
L.
L.
L
L
L-
L
L
t____
L
C
a
1
2
1L
# Young Produced
8"'
9
l-L.
I"1
11-
13
I b
7
, 0
10
C?
1-z
Adults Live / Dead _
t^
I--
L
L
L-
U
L-
0
1,
t✓
L
L
Total Produced
(t
,D
ztt
24
-2;2-
-2,(Q
74
) C
23
Z3
211
ercent Control Producing 3r° Brood:_%
Treatment 2 Organism Reproduction
Effluent %:
a.6
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
0
Q•
0
O
0
O
0
p
0
0
0
0
Adults Live / Dead
L
L
L,
(_
L
L
L
L
L
L
a
1
# Young Produced
41/9
1//7
ifj?-3m
y1 ?
`tl1
if/9
s/6
s%
=c/ej
If/5
Adults Live / Dead
L.
L
L L.
G
L-
L
L
L
L
L
L
1
2
4
7
9
11
# Young Produced
q
$
1 I
10
13
12-
6
(O
��o
g
/6
Adults Live / Dead
L.
L
L
L
L.
L
L
L,
(f
L
L.
Total Produced
Z2
11
7-2
2,2
Z;
2'4
).._ (
l 7
l ?)
ZD
IZ
tI
Comments:
Sample Type / Duration
Sample 1
Sample 2
H
Collection (Start) Dates:
Sample 1: j ' " (o S
Test Transferred
By:
Day 0 riA
Day 1
Day 2 M
Day3 �C
Day4
Day5/11-
Day.6 /}J�
Terminated by: 407
✓
1 °°%
pH
7, 33
7.2_0
Grab
1" Sample
Control
7 3..S
q. cite
Treatment 2
1.93
r(, e8
D.O.
1" Sample
Control
r(, q 3
7 43
Treatment 2
rf , 918
rl. 4(D
Tema.
1" Sample
Control
24,9
24. ri
Treatment 2
25. 2
25. 0
Start End
Comp
•x
Duration
„23.$
.1y. 3
Fed
By:
FLL
1`t Saxple 2nd Sanajole
ci qr
1" Sample
r1/10
I. to8
q. too
150
1st Sample
2 5. 0
25. 2-
24}.8
25.1
Start
End
rE 89
`7.'15
?SD
2nd Sample
�l. e4
7.71
`7, 80
7.(0i
2nd Sample
25.0
25.0
25:0
25,0
Start
End

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
-TIC L-I l� 1p 7 S
U� 3/a-7/4%,
Client Information
Client: LM4C
Contact:
Address:
City: Mew- +n
County:
State: 1JG
PO#
NPDES #: gG00 44 -f 25
Phone: CgIn) gH4.sag f
Pipe Number:
Zip: 28 34,4
Type of Facility Generating Effluent: Wk.'rip
Sample Information
Sampling Site:
L t-AA G
Sample Type: Grab ✓Composite
Sampling Time: START Date: 3- (,.p(, Time:
END Date: 3 - 6 Time:
Sample Chilled (Covered with Ice): Yes ti/ No
C,
Collector's Name (Print): wle.5 VohdoINhal
Collector's Signature: Olfu;.
# of Contai rs 2.
2.40 t,AM PM
9:05
PM
Toxicity Test Information
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Acute:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
2.6f'70
Shipping Information
Relinquished By:
Received By:
Relinquished By.��►� _ y�
Received By:
Sample Temperature (C
IeJ. h
"3- 7-4, Time: AN PM
Time: Jp;3b 60 PM
Time: 1 I J du PM
(, Time: I I I (u '
Method of Shipment: WTC(6) UPS Fed -Ex
her:
SamplenReceivin ( aboratay�se Only)
Received From:
M
it -
Received By: 4M5-C�p_x_ Date: ,�j11/O Cp Time: i_:5OAM l�
Sample Temperature (C°): b,3/ p. Sample Condition: lc

IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
luca-75
03(039
Client Information
Client: t_M q L
Contact: P.Avk flw„S
Address: 16-1 e t
City: IA, .Y-t-con
County: Scekla,,,d
PO#
NPDES #:
Phone:
Pipe Number:
State: [J G Zip: 2133 6 y
Type of Facility Generating Effluent:
Sample Information
Sampling Site: L.lµq_ r,F.P
Sample Type: Grab V Composite
Sampling Time: START Date: 3 _ ct-44, Time:
END Date: 3 _ to. 6 Time:
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): Ctlark-s 1/.,,, l er,b€54rj
Collector's Signature: C ,,,,p,,„ 11 z.
# of Containers 2
8:r5 al
( PM
Toxicity Test Information
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished B
Received By:
Sample Temp rature
Re-
Date: 3 -to _a, Time: 9 : Lio
Date: 3.-16 - 04 Time: '
Date: 3 _ 1 a.. 0 c- Time:
Date: 3 -/U - C. Time: f j :` 3U
Method of Shipment: WTC(p/u) UPS
cle O Other:
PM
PM
AM PM
M
-Ex
Sample Receiving (Laboratory Use Only)
Received From: _ter
Received By: \\ � Date: [ b Time: ..SAM( V�1
Sample Temperature (C°): /c,S Sample Condition:

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 03/16/06
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
Reduction: 7.81*
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 11 12
Adult Male 0 0
Adult Dead 1 0
Adult Mortality 8.33% 0.00%
# Neonates 269 248
Mean # Neonates 22.417 20.667
Standard Deviation 2.314 3.200
Coefficient of Variation 10.324%
A = 12
Fisher's Exact Test
B = 12 a = 11
a/A = 0.92 b/B = 1.00
Success is: survival
Critical b value = 6
12 > 6
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 E 13-7.6667 13 C 23 0.5833
2 C 18-4.4167 14 C 23 0.5833
3 E 17-3.6667 15 E 22 1.3333
4 C 19-3.4167 16 E 22 1.3333
5 C 20-2.4167 17 E 22 1.3333
6 E 19-1.6667 18 E 22 1.3333
7 E 20-0.6667 19 C 24 1.5833
8 C 22-0.4167 20 C 24 1.5833
9 E 21 0.3333 21 C 24 1.5833
10 E 21 0.3333 22 E 24 3.3333
11 C 23 0.5833 23 C 26 3.5833
12 C 23 0.5833 24 E 25 4.3333

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 4.3333 -7.6667 0.4493 12.0000
2 3.5833 -4.4167 0.3098 8.0000
3 3.3333 -3.6667 0.2554 7.0000
4 1.5833 -3.4167 0.2145 5.0000
5 1.5833 -2.4167 0.1807 4.0000
6 1.5833 -1.6667 0.1512 3.2500
7 1.3333 -0.6667 0.1245 2.0000
8 1.3333 -0.4167 0.0997 1.7500
9 1.3333 0.3333 0.0764 1.0000
10 1.3333 0.3333 0.0539 1.0000
11 0.5833 0.5833 0.0321 0.0000
12 0.5833 0.5833 0.0107 0.0000
1
W = X 156.2069
171.5833
Calculated W = 0.910 Critical W = 0.884
0.910 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
F
Test Passes!
F test for Homogeneity of Variance
Effluent variance 10.2424
- 1.91
Control variance 5.3561
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
1.91 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
22.4 - 20.7
t = - 1.535
1.140
Degrees of freedom = 22
Critical t = 2.508
1.535 < 2.508
Test passed. There is not a significant difference in reproduction.
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test PASSES

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/15/06
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
X
Signatu, of Operator in Responsible Charge
Signature oatory Supervisor
Comments:
* PASSED: 10.39% Reduction *
Work Order: Environmental Sciences Branch
- MAIL ORIGINALORIGI„L ...,. Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
26
25
26
27
29
32
25
25
31
7
25
30
Adult (L) ive (D) ead
Effluent %: 2.6%
1TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
23
26
23
26
24
22
23
15
25
21
23
25
Adult (L)ive (D)ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = 10.39
% Mortality
Avg.Reprod.
0.00
Control
25.67
Control
0.00
Treatment 2
23.00
Treatment
2
Control CV
24.938%
% control orgs
producing 3rd
brood
91.7%
ASS FAI
Check One
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample 1st sample 2nd sample
8.04
7.89
8.04
8.01
s
t
a
r
t
1st sample
e
n
d
7.92
7.55
7.90
7.53
8.00
7.90
8.08
7.95
s
t
a
r
t
1st sample
e
n
d
7.68
7.59
7.69
7.60
7.95
7.94
7.94
7.82
s
t
a
r
t
2nd sample
e
n
d
7.83
7.61
7.77
7.43
LC50/Acute Toxicity Test
(Mortality expressed as %,
combining replicates
Complete This For Either Test
Test Start Date: 06/07/06
Collection (Start) Date
Sample 1: 06/05/06 Sample 2: 06/08/06
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 24.8 hrs L A A
U M M
Sample 2 X 23.5 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
48
179 575
514
<0.1
<0.1
1.0
0.4
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
--
Method of Determination
Moving Average Probit
Spearman Karber - Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
pH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
' Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Meritech
Client:
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodaphnia dubia
AC
NPDES #: /UC. 60 y y 7oZ5
Dilution Water: Lake Reidsville
Test Organism Source: 3
Stirred / Aerated for D.O.: Y
Control Organism Reproduction
Day #3 1 2
Incubator #:
Pipe #: 06 f County: S --A1Ay,J Date Start: jo 7-0(, Date End:Z., -)y—pe,
Time / Date of Culture Transfer: 7! 36,*M/ 4-7' )4, Time Start: //'i.5 i Time End: /:O&.9 ,,.1
Time / Date Neonates .Born:%',30,4,„ ff:t n-, /b -7 e6 1st Renewal Date: fa - -tl6, Time: S :/ A}/Y7
Age of Neonates at Test Start: 3.7.5 j-,ri 2nd Renewal Dater -.42. _v/0 Time: 7 a.2 ,q,v.)
Randomized: Vp N Culture Tray Temp: . -°Z.` Analyst: /17I-- Reviewed by:(v,2-
3
4
5
# Young Produced
t-3
D
0
t
6
p
Q
L
©
O
0
Adults Live / Dead
1
L
L
L
L
L
L
L
L
L
ay
2
3
4
5
# Young Produced
c
L
3
it
5
L.
L/
ii
3
0
Li-
Ltl
Adults Live / Dead
L
1_
L
L_
L.
L
L
1__
L
1_
L
ay
1
2
3
4
5
6
7
# Young Produced
V/3
/3
9/LJ.
1%,;'
R
1
f4
9-3
/��
inioL
/41
Adults Live / Dead
L
L.
L_
L
L
L
L
L-
L
L
L
Total Produced
Treatment 2 Organism Reproduction
Effluent %:
a.
1
2
3
7 19 AS-1 31 7
Percent Control Producing 3rd Brood:
4
5
6
7
# Young Produced
b
0
no
0
b
Oa
©
0
0
0
Adults Live / Dead
I
L
L
L_
L-
L_
L
L_
L
U
L
L
ay
2
3
4
5
# Young Produced
Li
4
3
4
9
L
'7,
5
LI
L f
5
4
Adults Live / Dead
L
L-
L
1-
L
L-
L
L
L_
L—
L
L—
ay
2
3
4
# Young Produced
�
�j
�Q
1 a
/Q
1
�l'o
16
/o
S
l
cif
/.�
! o
1D
/�
el
1�
Ts
f d
I t�
//
L
Adults Live / Dead
L_
L
L.
L_
L_
L-
L
L__-.
L_
L-
Z.__
Total Produced
,93
/5
2l
Collection (Start) Dates:
Sample 1:6—S
Sample Type / Duration
Sample 1
Sample 2
Sample
Test Transferred Fed
By: By:
Day 0 / L
100'/
pH
7.3/
ef7
Grab
Hardness m/I
Spec. Cond. (umhos/cm) 17
Chlorine (mg/1)
Sample Temp. at Receipt
H
IS` Sample
Comp
X
Duration
S
57S5)L/
6.1 <6,1
).b b 14
l
Control
a,BL}
7 SI
Treatment 2
'', ai
01
D.O.
1" Sample
Control
7!9 2\
7 s3
Treatment 2
710
7 5'3
Temp.
1" Sample
Control
Aro
2670
Treatment 2
, c-D
2 D
Start End
1" Sample
7.(4
7 (09
759
760
1" Sample
l�r0
c2.52'
Start
End
Day 1
Day 2
Day 3
Day 4
Day 5
Day.6
/»2.,
/rE- ME
fin -
Pt_
/y�
Terminated by: /' ' e
2nd Sample
7,96
%qt/
79(t
`7. 82..
2nd Sample
7 ,3
777
7. 43
2nd Sample
)5=t7
Start
24.9
24.9
End
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Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: Lt4AG
Contact:
Address:
City:
County:
PO #
Garry Arn& " NPDES #: 14C nnto Lriz5
%i d! trier . Q41. Phone: g 4L{ . 5 Os/
1-1tvvitir Pipe Number:
ScJ.1-i-karState: NC.- Zip: 2836u
Type of Facility Generating Effluent:
\v,/'f 'P
Sample Information
Sampling Site: L.M c. Q.c?
Sample Type: Grab t/ Composite
Sampling Time: START Date: (g,o, Time:
END Date: (o • 9-0 r, Time:
Sample Chilled (Covered with Ice): Yes ✓ No
Collector's Name (Print):
Collector's Signature:
avr
of Containers Z
Toxicity Test Information
Test Required: Chronic: _✓ Test Organism: Ceriodaphnia Dubia:
Acute:
IWC:
i oxicity Test Concentration(s): ? , 0aj0
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By
Received By:
Sample Tempera re (C
K OWE �iti`w
ate: 6,-9-0 6 Time:
ate: --. Time:,.:1 AIyI PM
Date: C -?-o �- Time: AM
Date: C -9-O C Time: j aSCJ AM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle oOther:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Sample Temperature (C°): 0, /
Date: lop 0 h Time:
Sample on ition:

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 06/15/06
Facility: LMAC NPDES#: NO0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
Reduction: 10.39%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 12
Adult Male 0 0
Adult Dead 0 0
Adult Mortality 0.00% 0.00%
# Neonates 308 276
Mean # Neonates 25.667 23.000
Standard Deviation 6.401 2.954
Coefficient of Variation 24.938%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 C 7-18.6667 13 C 26 0.3333
2 E 15-8.0000 14 C 26 0.3333
3 E 21-2.0000 15 E 24 1.0000
4 E 22-1.0000 16 C 27 1.3333
5 C 25-0.6667 17 E 25 2.0000
6 C 25-0.6667 18 E 25 2.0000
7 C 25-0.6667 19 E 26 3.0000
8 C 25-0.6667 20 E 26 3.0000
9 E 23 0.0000 21 C 29 3.3333
10 E 23 0.0000 22 C 30 4.3333
11 E 23 0.0000 23 C 31 5.3333
12 E 23 0.0000 24 C 32 6.3333

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
f
COEFFICIENTS AND DIFFERENCES
x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 6.3333 -18.6667 0.4493 25.0000
2 5.3333 -8.0000 0.3098 13.3333
3 4.3333 -2.0000 0.2554 6.3333
4 3.3333 -1.0000 0.2145 4.3333
5 3.0000 -0.6667 0.1807 3.6667
6 3.0000 -0.6667 0.1512 3.6667
7 2.0000 -0.6667 0.1245 2.6667
8 2.0000 -0.6667 0.0997 2.6667
9 1.3333 0.0000 0.0764 1.3333
10 1.0000 0.0000 0.0539 1.0000
11 0.3333 0.0000 0.0321 0.3333
12 0.3333 0.0000 0.0107 0.3333
1
W =
X 395.8132
546.6667
Calculated W = 0.724 Critical W = 0.884
0.724 < 0.884
The reproduction data is not normally distributed
evaluated at a 99% confidence interval'
Test Failed!
Wilcoxon Rank Sum Test
Rank Sum - Effluent Group(treatment): 104 Control Group: 196
Mann -Whitney U = 26.0 nl(treatment) = 12 n2(control) = 12
The critical value from TABLE A.15 (0.01 Level of T) for the above n values:
Critical T = 109
104 5 109
The Sum of the Ranks of the effluent group is less than or equal to the
significant value from the table. Therefore there is a significant
difference between the means of the effluent and control groups and the:
TEST FAILS
Chronic Test PASSES
The reduction was less then 20%

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/20/06
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory P rfor�jmiin'g� Test: MERITECH LABS, INC.
X lei .�' 1--a
Signature of Oper- or iResponsible Charge
Signature of Laboratory Supervisor
Comments:
* PASSED: 19.24% Reduction *
'Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
;CONTROL ORGANISMS
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
26
27
23
25
22
24
25
26
25
24
22
22
Adult (L)ive (D)ead
Effluent %: 2.6%
(TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
21
22
16
17
16
18
20
22
22
20
21
20
Adult (L)ive (D)ead
Chronic Test Results
Calculated t = 5.678
Tabular t = 2.508
% Reduction = 19.24
% Mortality
Avg.Reprod.
0.00
Control
24.25
Control
0.00
Treatment 2
19.58
Treatment
2
Control CV
7.061%
% control orgs
producing 3rd
brood
100%
PASS FAIL
Check One
n
. )pH
Control
Treatment 2
-D.O.
Control
Treatment 2
1st sample 1st sample 2nd sample
7.96
7.94
7.96
8.08
8.05
7.88
8.06
8.05
7.97
7.91
8.01
8.02
s s s
t e t e t e
a n a n a n
✓ d r d r d
t t t
lst sample lst sample 2nd sample
8.10
7.47
8.14
7.52
7.65
7.63
7.69
7.60
7.85
7.62
7.75
7.60
1
,
LCSO/Acute Toxicity Test
(Mortality expressed as %, combining replicates
Complete This For Either Test
Test Start Date: 09/13/06
Collection (Start) Date
Sample 1: 09/11/06 Sample 2: 09/14/06
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 23.8 hrs L A A
U M M
Sample 2 X 23.8 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
46
168
675
895
<0.1
<0.1
0.3
1.0
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 = %
95% Confidence Limits
% -- %
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
n.,.,
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

OctIe 5-3
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: LMf�L
Contact: Poo t Dekv i 6
Address: '1 (,7 D i IS%;1Dtro'�}- Qa,
City: Mnx-1 t> 1
County: ScIA-63-\ -IU State: t•l
Po# ► 8 L-- l 7-23 )
NPDES #:
Phone: Ogta)gyH -50 F
Pipe Number:
�- Zip: 263614
Type of Facility Generating Effluent: WWTP
Sample Information
Sampling Site:
Sample Type:
Sampling Time:
LIAR G per+
Grab / Composite
START Date: 9_11_ p (o Time:
END Date: ci I b Time:
Sample Chilled (Covered with Ice): Yes v No
Collector's Name (Print):„ Les
Collector's Signature:�� p 9
Toxicity Test Information
Test Required: Chronic:
Acute:
IWC:
Toxicity Test Concentration(s): 2. ,%
List Any Special Requirements:
# of Containers 7
R'.05 AM PM
:55PM
Test Organism: Ceriodaphnia Dubia:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperature C°):
4.1
Date: G..i, -n'_ Time: /1 066PPM
Date: 9_ 1 _ eC Time: ajtoKOPPM
Date: , . o Time: ra :d o AM(ek
Date: T- la-1 Time: I a: too AM
Ex
Method of Shipment: WTC(p/u) UPS Fed -Ex
I a : o oCircle One Other:
Si m e Reiving (Lab ra Usel illy) y Rd
Received From:
Received By: Date: Time: .21 v� AM��
Sample Temperature C°): a.3 /�3 Sample C n ition:
asp

Data Sheet for Mini Chronic Pass / Fail Test: Ceriadaphnia dubia
Client:
NPDES #: OO /'7ZS
Dilution Water: Lake Reidsville
Test Organism Source:
Stirred / Aerated for D.O.: Y /
Control Organism Reproduction
Day #3
2
.eritech 7 L
i
Date Start: q - 13- O(p Date End: ct /zo&
Time /Date Neonates Born: � -
/
Time Start: / •. �, Time End: s:2p�q,z...
SF^' 9' . / - zt!, 1st Renewal Date: ti,/,,; �ctv Time: g : cQ,
Age of Neonates at Test Start: L f ir.s 2nd Renewal Date: f�
Randomized • N Culture Temp:" ° VI Time: $.•),S—,�}�,
Tray 2S . C Analyst: , ,tit, f� Reviewed by: ,,,,wL
Collection (Start) pates:
3 4 5 6 7 8 9 10 11 12 Sample 1: q/i /p
Pipe #: County: S (-Oft
Time / Date of Culture Transfer: 9: 5--4„,
# Young Produced
Adults Live / Dead
Day #5
# Young Produced
Adults Live / Dead
Day #7
# Young Produced
Adults Live / Dead
O
2
3
0
L1/io L1io f
L L. L
0
4
6
e)
d
cD
5
9/9
L I 1_
6
7
I LI
L 1
Total Produced
/A
L.
.076
2
/3
3
(1
L
.23
['reatment 2 Organism Reproduction
Effluent %:
2 • G 1 2 3
Young Produced
adults Live / Dead
>ay #5
Young Produced
Ldults Live / Dead
)ay #7
Young Produced
.dults Live / Dead
otal•Produced
.mments:
l0
L.
7
1
4
1,2
L
5
10
L
6
L
7
10
10
// it /�
3/0
,/ '
110
9/61
L
L
L
L
1...
L
8
9
10
11
Percent Control Producing 3 ° Brood. 1
4 5 6
L.-
0
7
L
8
10 11
CO)
149
0
C_
(__ (._ L.
L
9 10
y937t
73/�
L,
L
1.,
L
L
L_
gb
8
9
t_
9
I;
L
10
/I
11 12
L
/d
L
Sample Type / Duration
Sample 1
Sample 2
p
Incubator #:
Sample 2: `r.loderz
c00%
pH Grab Comp
7. 1(
-)•�IS�
H 1st Sample
Control
Treatment 2
D.O.
Control
Treatment 2
Temp.
Control
Treatment 2
7.96
7qb
11.94
8.08
1' Sample
S./ 0
•7, SZ.
1 S' Sample
va q
1,a (k
2.5.0
2670
Start End
Duration
23.8
23.8
lst Sample
8, O(o
1st Sample
24.1
2,9.9
Start
Test Transferred
By:
25,0
SCD
End
Day 0
Day I
Day 2
Day 3
Day 4
Fed
By:
%It L
Day 5 fyi—
Day 6
Terminated by: fig--
2nd Sample
7,ci 7
Y,bl
``t l
2nd Sample
7.75"
-7 (0 0
2nd Sample
•7 0
ZS.D
Start
75 O
25�• �
End

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: Laurie -I e—Mourft,
Contact: pa,,, naii
Address: ,6--70I A;�, ai - 1.
ri: PM,,,ei-f,,1
County: State: WC, Zip:
Type of Facility Generating Effluent: \t‘i 1Arr P
PO#
NPDES #: PC601-14-7 SZ
Phone: c{y -50$1
Pipe Number:
21,3‘,1-t
Sample Information
Sampling Site: LMAC, e 1.Yen+
Sample Type: Grab ✓ Composite
Sampling Time: START Date: 9 - l4 _ ), , Time:
END Date: 9- (5-6(0 Time:
Sample Chilled (Covered with Ice): Yes t— No
Collector's Name (Print): C ri V�'1c�.Pr),bp.trq
Collector's Signature: C� D e�
# of Containers 2
PM
PM
Toxicity Test Information
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
2.6`77n
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Samp
ate:
ct -K-D(o Time: 2 AM PM
ate: .. O C Time: ` �'(,Q-AM PM
ate: .f._, t rdi Time: ! 0,4-4 411*1 PM
Date: -(S-v -i Time: j 0 % 1.6 PM
Temperature°) :Method of Shipment: WTC(p/u) UPS Fed -Ex
`� ' ` Circle Ope Other:
V J
Sample Receiving (Laboratory Use Only)/Zr/ 00 g/isyc,,, 35SP
Received From: ! (.L :30ii
Received By: t`-k _
Sample Temperature (C°): , D/
( -0 Sample p itton.
Date: ndti Time:'J<-

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 09/20/06
—1
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
Reduction: 19.24%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 12
Adult Male 0 0
Adult Dead 0 0
Adult Mortality 0.00% 0.00%
# Neonates 291 235
Mean # Neonates 24.250 19.583
Standard Deviation 1.712 2.275
Coefficient of Variation 7.061%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered
i Group Neonates Centered
1 E 16 -3.5833 13 E 20 0.4167
2 E 16 -3.5833 14 C 25 0.7500
3 E 17-2.5833 15 C 25 0.7500
4 C 22-2.2500 16 C 25 0.7500
5 C 22 -2.2500 17 E 21 1.4167
6 C 22-2.2500 18 E 21 1.4167
7 E 18 -1.5833 19 C 26 1.7500
8 C 23-1.2500 20 C 26 1.7500
9 C 24 -0.2500 21 E 22 2.4167
'` 10 C 24 -0.2500 22 E 22 2.4167
11 E 20 0.4167 23 E 22 2.4167
12 E 20 0.4167 24 C 27 2.7500

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 2.7500 -3.5833 0.4493 6.3333
2 2.4167 -3.5833 0.3098 6.0000
3 2.4167 -2.5833 0.2554 5.0000
4 2.4167 -2.2500 0.2145 4.6667
5 1.7500 -2.2500 0.1807 4.0000
6 1.7500 -2.2500 0.1512 4.0000
7 1.4167 -1.5833 0.1245 3.0000
8 1.4167 -1.2500 0.0997 2.6667
9 0.7500 -0.2500 0.0764 1.0000
10 0.7500 -0.2500 0.0539 1.0000
11 0.7500 0.4167 0.0321 0.3333
12 0.4167 0.4167 0.0107 0.0000
1
W = X 82.6341
89.1667
Calculated W = 0.927 Critical W = 0.884
0.927 a 0.884
The reproduction data is normally distributed
evaluatedat a 99confidence interval.
F =
Test Passes!
F test for Homogeneity of Variance
Effluent variance 5.1742
- 1.76
Control variance 2.9318
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
1.76 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
24.3 - 19.6
t = - 5.678
0.822
Degrees of freedom = 22
Critical t = 2.508
5.678 a 2.508
Test
roduction
between the 1Control eand lthe effluent aevaluatedeate
a199%nt ifferncn econfidence interval.
Chronic Test PASSES
The reduction was less then 20%

Meritei h, Inc.
Bioassay Sample.Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: L M A i.
Contact: , ,)
Address: I F, .--, ; + n : , < < . 4 Ld_.
City: M, -•,. -1,r,
County: r State: N
PO# T L-^1-72?
NPDES #:
Phone: (9 t01-:. t. . e = u
Pipe Number:
Zip: -2 . = -
Type of Facility Generating Effluent: \n/ err.
Sample Information
Sampling Site: L MR (. �.i k-
Sample Type: Grab i j Composite
Sampling Time: START Date: )1 r i Time:
END Date: rI .. { �, r (- Time:
# of Containers
c (Aa PM
PM
Sample Chilled (Covered with Ice): Yes ✓ No
Collector's Name (Print): ' '
Collector's Signature: ;. ;
Toxicity Test Information
Test Required: Chronic:
Acute:
Test Organism: Ceriodaphnia Dubia: v
IWC:
Toxicity Test Concentration(s): 2 G
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
.1
fI
Shipping Information
Relinquished By: .- ;; L.. . Date:
Received By: '• Date:
Relinquished By:
Received By:
Date:
Date:
+ _ (' (: Time: AM PM
Time: -AM PM
Time: AM PM
Time:- AM PM
Sample Temperature.(C°): Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Sample Temperature (C°):
Date:
Time: AM PM
Sample Condition:

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client' L -ko(A) r - Mc kx-h. v-
Contact: Pn.0 1 QU,
Address: , t,-r; A, i ✓ ; n , —
City: Mrxl-'G n
County: +-trzr,c+
State:
Type of Facility Generating Effluent:
i r r . PO#
NPDES #: 1\C/10 t-1 ►-j-152
Phone: - Sod 1
NC Zip:
WWmP
Pipe Number: •
Sample Information
Sampling Site: L MAC -c-_---C 104_, + .
Sample Type: Grab Composite
Sampling Time: START . Date: q - _ ne: Time:
END Date: 1- i 5 - et, Time:
Sample Chilled (Covered with Ice): Yes ✓ No
Collector's Name (Print):
Collector's Signature:
Toxicity Test Information
Test Required: Chronic:
Acute:
# of Containers 'i_.
PM
PM
Test Organism: Ceriodaphnia Dubia: ✓`
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
2.6 I(.
Shipping Information Relinquished By:� Date: Ci -15-OL Time: 9 . r )JAM PM
Received By: Date: 2_ 1 r_ . L Time: `3.'/ I AM PM
Relinquished By: ; Date: Time: AM PM
Received By: Date: Time: AM PM
Sample Temperature (C°): Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By: Date: Time: AM PM
Sample Temperature (C°): / Sample Condition:

NPDES#:
est: MERITECH,LABS, INC.
ley
ig Op-ratt.r Jin1Re o s le C arge
X Signature of Laborat r 'Supervl or
Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/14/06
Facility: LMAC
Laboratory Pe rmin
hit r o
NC0044725 Pipe#: 001 County:
Comments:
* PASSED: 0.36% Reduction *
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
18
23
24
24
25
24
18
24
23
24
26
26
Adult (L) ive (D) ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
22
22
22
26
22
22
24
24
24
22
24
24
Adult (L)ive (D)ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = 0.36
% Mortality
Avg.Reprod.
0.00
Control
23.25
Control
0.00
Treatment 2
23.17
Treatment
2
Control CV
11.324%
% control orgs
producing 3rd
brood
100%
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample 1st sample 2nd sample
7.95
7.85
7.95
7.55
s
t
a
r
t
1st sample
e
n
d
8.00
7.02
7.98
6.60
7.96
7.90
7.90
7.88
s
t
a
r
t
1st sample
e
n
d
8.26
8.08
8.29
8.08
7.95
8.01
8.02
8.05
s
t
a
r
t
2nd sample
e
n
d
8.15
7.73
8.23
7.80
LC50/Acute Toxicity Test
(Mortality expressed
as %,
combinin
PASS
FAIL
Check One
Complete This For Either Test
Test Start Date: 12/06/06
Collection (Start) Date
Sample 1: 12/04/06 Sample 2: 12/07/06
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 24.4 hrs L A A
U M M
Sample 2 X 23.8 hrs T P P
Sample
replicates)
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
temp. at receipt(°C)
-42
162
418
595
<0.1
<0.1
3.0
0.8
Concentration
Mortality
LC50 =
95% Confidence Limits
% -- $
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
r,,,,
•
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs) :
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Meritech T6L.
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodap/inia dubia
Client: L : Pipe #: 00i County: „-Han
NPDES #: NC Doti -17 z 5- Time / Date of Culture Transfer: %•; in i��
Dilution Water: Lake Reidsville Time / Date Neonates Born: • .,
Test Organism Source: 4tZ ▪ i
g Age of Neonates at Test St.
Stirred / Aerated for D.O.: Y /® Randomized: Y / N Culture Tray Temp: Z.' °C
Control Organism Reproduction
Day #3 1 2 3 4 5 6
7 0 9
# Young Produced
D
o
b•
0
0
0
0
0
0
Adults Live / Dead
L
L
L
L.
L
L,
L
L,
L
# Young Produced
37
/
`1/q
ylg
$,/7
3
1--/`//2
400
4
Adults Live / Dead
Tl ., , , 4'7
L
L
(--
L
L
LLLL
# Young Produced
$
iID
(2-
I z
r%
1 is
/LI
<
/0
f(
Adults Live / Dead
L
L
L.
L
L
LLL
ITotal Produced
10
0
L
10
L
10
IL
L
1�-
11
0
12
11
12
,5-
9
L
11
12
1ck
L,
io�L
L
1� IZIZy I2q 125124 118 Izy 123 IzLl I z.01
Percent Control Producing 31.d Brood: /(37) %
Treatment 2 Organism Reproduction
Effluent %:
_, u / o V 1U 11 12
# Young Produced G
0
0
0
0
0
0
0
0
0
o
0
Adults Live / Dead L_,
L,
L
L.
L
L,
L
L
L
L
L
L
lavfc • -
# Young Produced
Adults Live / Dead
Day in
-!$
3
34 LI
1,
4
�11p
L
5
Lr
6
Lik
7
8
9
10
11 12
L- L_
L
# Young Produced
1 2 3 4
►0
Adults Live / Dead I L
1(
L_
L
5 6 7 8 9 10 11
L L
ITotal Produced
IZ-?-iZz12(pI
10
L
/L
S`!0
IZ
12
1 Z.-
7z
Comments:
ZZ
ZLf
ZZ
L4
Lg
Incubator #:
Date Start: Date End: i 2-434 to
Time Start: !o'.3a,..„ Time End: it): y gap,
1st Renewal Date: i z1Fs/a Time: 7: 3
2nd Renewal Date: Time:
Analyst/re-AP/mi. Reviewed by: 7' ��
Collection (Start) Dates:
Sample 1: 1 Z/9/oto Sample 2: 12/7/
Sample Type / Duration
Sample 1
Sample 2
Test Transferred
By:
100%
pH
7,5q
7.1138
Grab
Comp
X
Duration
ZL1, `i/
Z3 ,8
Hardness m /I)
z
TIIIIIIIIMI
?'. `' •
I r •` "�
GO,
„t F i Fi
S • ec. Cond. (unrhos/cm)
•G0. (
Chlorine m: I
Sam •IeTem•. atRecei•t
3.0
O.4S
15` Sam I^
Control
785
7. $5
Treatment 2
7.`6-
7,55
D.O.
151 Sample
Control
c•Cc'7,02.
Treatment 2
?, CIS
6.0
Tema.
lst Sample
Control
•2.50
2'{,'
Treatment 2
2 0
2.5
Start End
15' Sample
g0$
15t Sample
25 )
25.o
ZSo
Start
End
Day 0
Day 1
Day 2 /t fi1L
Day 3
Day 4 4
Day 5 M2 jYJL-
Day 6 j1lJ�
Terminated by: -g
Fed
By:
16"
2nd
Sr,
ampic
7,75
gD/
Si o 5-
2nd Sample
2S: 0
ZS. I
2-0
Start
End
r

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client:
Contact:
Address:
Client information
LMAC
Paul D4+f'S
% i-1b I A;rpoi-A Rd.
City: �11�x4n n
PO#f3L-1\0
NPDES #:
Phone: Ow) gy y-sag t
Pipe Number:
County: S (do .1..1Q,r-,a State: %y L Zip: Zg 3 e, t}
Type of Facility Generating Effluent: vAn.f r'P
Sample Information
LtU C
Sampling Site:
Sample Type: Grab Composite
Sampling Time: START Date: 11-4 _116, Time:
END Date: 12 - s -0 h Time:
Sample Chilled (Covered with Ice): Yes I/ No
Collector's Name (Print): rle s Vav,d,�,,,, �'�9
Collector's Signature: C
Toxicity Test Information /
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia: ✓
Acute:
# of Containers 2
PM
PM
Pimephales promelas:
Mysidopsis bahia:
IWC•
Toxicity Test Concentration(s): 2. Vio
List Any Special Requirements:
Shipping Information
Relinquished By:
Received By:
Relinquished By.
Received By.
Sae Tempe Are (C°):
Date: 12-5 -0 b Time:
Date: f z_ 'o (, Time: //?go
Date: S d Time: AM PM
Date: p_- S =0C Time: I IS A (�
Method of Shipment: WTC(p/u) UPS Fed -Ex
U(, Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From: 1
Received By Date:
Sample Temperature (C°): ,,Q Sample
06 Time: 32E-AM(
/c..4
ondition:

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
n (n
Client Information
Client: L,[a►uri',n b,,,rrj,-M,,,c1.r,►)
Contact: Paul Dew i5
Address: 16761 kr©,..l. RA.
City: Ma..x-hf)n
County: 5c i-\ ,j State:
Type of Facility Generating Effluent:
A; r,Po r� PO#
NPDES #: 1gC_O6i- l-r?_5
Phone: (410) 844 - 5691
Pipe Number:
NC_ Zip:
W wT-P
Sample Information •
Sampling Site: L-MAL e I ven4
Sample Type: Grab 1/ Composite
Sampling Time: START Date: 12-j -ot„ Time:
END Date:
Sample Chilled (Covered with Ice): Yes
Collector's Name (Print):
Collector's Signature: ('
12-e-06
# of Containers 2
$ : a041,,,, 7 PM
Time: g •. 20
No
I0,A4
PM
Toxicity Test Information
Test Required: Chronic:
Acute:
Test Organism: Ceriodaphnia Dubia: ✓
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By: r1i, / . , , 1
Received By:�,��...
Relinquished By:? ill ly,,,�,i
Received By: A•�
Sample Tempera re (<°):
r"1 I
Date: 12 _ R - „ Time: ' ; 6 AM PM
Date: 12 _g-o 4 Time: t9 PM
Date: /2_ e 4 Time: 11 =06 * u' PM
Date: /a-Ir'° 6 Time: ! I1 PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
114-0 Q Circle One _ Other:
Sample Receiving (Laboratory Use Only) (NJ_
Received From:
Received By: \-t(`c\C:,_}-' �� . Date:
Sample Temperature (C°): (�.2,/ C'�.g�', Sample Con
mUon:
1 a -- "—OCc. qc. )
Time:

Effluent'Toxicity Statistical Results - Chronic Pass/Fail Date: 12/14/06
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratory Performing Test: MERITECH LABS, INC.
Reduction: 0.36%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 12
Adult Male 0 0
Adult Dead 0 0
Adult Mortality 0.00% 0.00%
# Neonates 279 278
Mean # Neonates 23.250 23.167
Standard Deviation 2.633 1.337
Coefficient of Variation 11.324%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12 .
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered
i Group Neonates Centered
1 C 18-5.2500 13 C 24 0.7500
2 C 18-5.2500 14 C 24 0.7500
3 E 22-1.•.1667 15 C 24 0.7500
4 E 22-1.1667 16 E 24 0.8333
5 E 22-1.1667 . 17 E 24 0.8333
6 E 22-1.•1667 18 E 24 0.8333
7 E 22'-1.1667 19 E 24 0.8333
8 E 22-1.1667 20 E 24 0.8333
9 C 23-0.2500 21 C 25 1.7.500
10 C 23-0.2500 22 C 26 2.7500
11 C 24 0.7500 23 C 26 2.7500
12 C 24 0.'7500 24 E 26 2.8333

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 2.8333 -5.2500 0.4493 8.0833
2 2.7500 -5.2500 0.3098 8.0000
3 2.7500 -1.1667 0.2554 3.9167
4 1.7500 .-1.1667 0.2145 2.9167
5 0.8333 -1.1667 0.1807 2.0000
6 0.8333 -1.1667 0.1512 2.0000
7 0.8333 -1.1667 0.1245 2.0000
8 0.8333 -1.1667 0.0997 2.0000
9 0.8333 -0.2500 0.0764 1.0833
10 0.7500 -0.2500 0.0539 1.0000.
11 0.7500 0.7500 0.0321 0.0000
} 12 0.7500 0.7500 0.0107 0.0000
1
W = X 80.7311
95.9167
Calculated W = 0.842 Critical W = 0.884
0.842 < 0.884
The reproduction, data is not normally distributed
evaluated at a 99% confidence interval
Test Failed!
Wilcoxon Rank Sum Test
Rank Sum - Effluent Group(treatment): 134 Control Group: 167
Mann -Whitney U = 55.5 nl(treatment) = 12 n2(control) = 12
The critical value from TABLE A.15 (0.01 Level of T) for the above n values:
Critical T = 109
I •
134 > 109
The Sum of the Ranks of the effluent group is greater than the significant
value from the table. Therefore there is no significant difference between
the means of the effluent and control groups and the test passes.
TEST PASSES
•Chronic Test PASSES
The reduction was less then 20%

Meritech, Inca
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: LMAC
Contact: f , -
Address: I (\.
City: KA,' 4-t;
County: • -�
State; N (.
Type of Facility Generating Effluent: kiyP
PO# IIL-\C
NPDES #:
Phone: f:Au, i Lf I
Pipe Number:
Zip:
Sample Information
Sampling Site:
Sample Type:
Sampling Time:
Grab
START Date: �•�.
END Date: }- c r, (-
Sample Chilled (Covered with Ice): Yes ;i No
Collector's Name (Print):
Collector's Signature: (�; /.
Composite
Time:
Time:
# of Containers
PM
PM
Toxicity Test Information
Test Required: Chronic: 4 . Test Organism: Ceriodaphnia Dubia: _
Acute:
IWC:
Toxicity Test Concentration(s): 2. L`lo
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By: t,�i:,,.t,,,1f , V .t, ��_ Date:
Received By: \, ; �. . R. ) Date:
Relinquished By: \::..\ ... ,C; Date:
Received By: Date:
-c Time: PM
Time: // ' r.- A PM
Time: AM PM
Time: AM PM
Sample Temperature (C°): Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Sample Temperature (C°): /
Date:
Sample Condition:
Time: AM PM

City:
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: Lou, • . Ni,.x+<
Contact: per, ,1 p,,;, ;
Address: I � 7c1 A;,11e RA
M n x`1- c v1
County: 5r. e•-i 1„A
f1,r1 ,-f
PO#
NPDES #: N c. c n y 1l- 2. 5
Phone: (q \(,) - 565
Pipe Number:
State: NC_ Zip: 2 p; y
Type of Facility Generating Effluent: `A/,n/TP
Sample Information
Sampling Site:
e-C- ven4
Sample Type: Grab v Composite
Sampling Time: START Date: 12 - -� -Cj� Time:
END Date: i 2 - e .06, Time:
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print):
Collector's Signature:
# of Containers 2
g•
�„�,
PM
PM
Toxicity Test Information
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
2.6-74-
Shipping Information
Relinquished By: l .fir. .c..,v r1-1 ,, Date: 12 - -O6 Time:
Received By: �, \-, , 4,-t,..,,"�_ /\ Date: , : . Time:
Relinquished By: ,i 1, ..., .:.=,.:,1;,._` Date: i., . - Time:
Received By: Date: Time:
Sample Temperature (C°):
PM
M PM
AM PM
AM PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Sample Temperature (C°): /
Date: Time:
Sample Condition:
AM PM

n
IX
r---
'Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:
Laboratorry Performing Test: MERITECH LABS, INC.
k ` Y
Signatu e o peratoespo ble harge
Ft -fluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/14/07
Signature of Laboratory Supervisor
Comments: Lots of aborted embryos
in the 2.6;‘test concentration.
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
23
22
21
12
23
22
24
24
15
14
20
19
Adult (L)ive (D)ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
16
14
18
20
7
19
10
2
8
6
17
9
Adult (L) ive (D) ead L L L L D L L D L L L L
Chronic Test Results
Calculated t = 3.734
Tabular t = 2.508
% Reduction = 38.91
% Mortality
Avg.Reprod.
0.00
Control
19.92
Control
16.67
Treatment 2
12.17
Treatment
2
Control CV
20.586%
% control orgs
producing 3rd
brood
91.7%
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
8.05
7.99
8.04
7.92
s
t
a
r
t
1st sample
e
n
d
7.95
7.99
7.96
8.01
1st sample
8.02
8.03
7.97
7.95
s
t
a
r
t
1st sample
e
n
d
8.25
7.98
8.22
7.99
2nd sample
PASS FAI
Check One
8.03
7.98
7.98
8.01
s
t
a
r
t
2nd sample
e
n
d
8.22
7.83
8.26
7.97
LC50/Acute Toxicity Test
(Mortality expressed
as %,
combinin
Complete This For Either Test
Test Start Date: 03/07/07
Collection (Start) Date
Sample 1: 03/05/07 Sample 2: 03/08/07
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 24.7 hrs L A A
U M M
Sample 2 X 24.2 hrs T P p
Sample
replicates)
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
temp. at receipt(°C)
40
180
514
657
<0.1
<0.1
0.4
0.2
Concentration
Mortality
LC50 = %
95% Confidence Limits
%
Method of Determination
Moving Average Probit
Spearman Karber - Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
cnnr
pH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Client:
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodap/rnia rhihia
_� CM
Meritech T8L
NPDES #: o 7 Z � ---- County•
Dilution Water: Lake Reidsville
Test Organism Source:
Time Pipe #:
Time / Date of Culture Transfer: �3 : -- ci ee Date
/ Date Neonates Born: Date me E a�-�y
2 •••-`Time Start: .��1, m _.�
Age of Neonates at Test .�
Stirred /Aerated for D.O.: Start.
y /(� Randomized:
Control Organism Re roduction N Culture Tray Temp:Z
Day #3
# Young Produced
Adults Live / Dead
Day #5
# Young Produced
Adults Live / Dead
Day #7
# Young Produced
Adults Live / Dead
i'otal Produced
I 2
'reatment 2 Organism Re roduction
Effluent %:
Z:(
Young Produced
dults Live / Dead
ay #5
Young Produced
cults Live / Dead
Ly#7
(oung Produced
ults Live / Dead
:al Produced
10 11 12
10 11 12
Percent Control Producing3`
Brood:7%
Z
Parmannign ristimirAnn
7,K ,0 „ 12
©©�o1N�v
rnmet:
MIN
Incubator #:
1st Renewal Dat . Time:
End:
Renewal Date: 3 - Time: i�
°C ,� m,
Analyst;
_ Reviewed by:
Collection (Start) Dates:
Sample 1: 3-.S_
Sample Type / Duration
Sample 2: 3- g -
Tet
0=
Transferred Fed
By: By:
Day 0
Day 1
!r
at -
Day 2
Day 3,�
Day 4 -�
Day 5 /'t:f m
Day 6
Terminated by: 4e—
r—

Client Information
Client:
Contact:
Address:
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
-GVtin� .� -Mood- r. rl � � r"r
Q-ari V-Andef Y'
I6--bI Air?or} ) .
City: l -i-en
County: 5c2,41o,r, j State: Nc. Zip:
Type of Facility Generating Effluent:
W,w-r-P
PO#
NPDES #:
Phone:
Pipe Number:
?B3 64
Sample Information
Sampling Site:
l-l✓ c (2.P.e
Sample Type: Grab Composite # of Containers
Sampling Time: START Date: 3_5-07 Time: $:30 AI PM
2—
END Date: 3 -,-o Time: c : Io ei PM
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): . rl V. , , _ r.
Collector's Signature:
Toxicity Test Information
Test Required: Chronic: j7Test Organism: Ceriodaphnia Dubia: t/
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Samp e Temperature
Nee
Sample Receiving (L
ate: -07 Time: AM PM
Date: 3-(Q-01 Time: (D PM
Date: 3 —1'4
Time: i (:Jo • TA PM
• PM
Date: —'' Time: WriT A
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
hof story Use Only) (k1�
Received From: ,MYa .s
Received By.1/411" J Date: 3-C, G 7 Time:k4S qN
Sample Temperature (C°): O,y / %,'_ Sample Condition: 1c c c�
3-(;-07
I� S��

1
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
C) 3OCi l o 5--
Client Information
Client:
Contact:
Address:
City:
Lurirburg-MaYe6r1 4irrorT
0.-�arI iimad i t r49 I
16701 a i rPe r - Rd,
County: State: NjL Zip:
Type of Facility Generating Effluent:
PO#
NPDES #: tk O6'147Z5
Phone: (9v)) if 44 -6ogt
Pipe Number:
2$?,6 y
Sample Information
Sampling Site:
1-MAC. c�4 LJQ '-%-
Sample Type: Grab Composite
Sampling Time: START Date: 3 .g .o7 Time:
END Date: 3 -q-07 Time:
Sample Chilled (Covered with Ice): Yes - No
Collector's Name (Print):
Collector's Signature:
# of Contai a -rs Z
PM
al : 00 Am AM PM
d,mg E c.ne-te4
(-)n, :3-1.�- v ub 1"COAM
Toxicity Test Information
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
c-w,dtsVO4,10A0,-
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperature (C°):
Sample Receiving (Laboratory Use Only)
Received From: Gr p i N r.\, c S
Date: o Time: 'J /*s� M
Date: 07 Time: ": PM
Date: Time: AM P
Date: 3 _ 44 07 Time: ;),') AM t"_J
Method of Shipment: WTC(p/u) UPS Fed -Ex
ircle One Other:
v r
tee'
Received By: i\ra,/t^- Date: 3 - I- 01 Time: U0 CCn AM.�I
Sample Temperature (C°): 0 / 0 Sample Condition: Lcc, c>

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 7.8333 -10.1667 0.4493 18.0000
2 6.8333 -7.9167 0.3098 14.7500
3 5.8333 -6.1667 0.2554 12.0000
4 4.8333 -5.9167 0.2145 10.7500
5 4.0833 -5.1667 0.1807 9.2500
6 4.0833 -4.9167 0.1512 9.0000
7 3.8333 -4.1667 0.1245 8.0000
8 3.0833 -3.1667 0.0997 6.2500
9 3.0833 -2.1667 0.0764 5.2500
10 2.0833 -0.9167 0.0539 3.0000
11 2.0833 0.0833 0.0321 2.0000
12 1.8333 1.0833 0.0107 0.7500
1
W = X 543.5449
568.5833
Calculated W = 0.956 Critical W = 0.884
0.956 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
F =
Test Passes!
F test for Homogeneity of Variance
Effluent variance
Control variance
34.8788
- 2.07
16.8106
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
2.07 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
19.9 - 12.2
t - - 3.734
2.075
Degrees of freedom = 22
Critical t = 2.508
3.734 a 2.508
Test fails. There is a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test FAILS
The mean # of young produced by each group is dissimilar

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/14/07
[Facility: LMAC
Laboratory Performing Test: MERITECH LABS, INC.
X !
Signature o Operat rb�e
NPDES#:
osible harge
NC0044725 Pipe#: 001 County:
Signature of Laboratory Supervisor
Comments: Lots of aborted embryos
in the 2.6xtest concentration.
Work Order:
MAIL ORIGINAL TO:
j North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
23
22
21
12
23
22'
24
24
15
14
20
19
Adult (L)ive (D)ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
16
14
18
20
7
19
10
2
6
17
9
Adult (L)ive (D)ead
Chronic Test Results
Calculated t = 3.734
Tabular t = 2.508
% Reduction = 38.91
% Mortality
Avg.Reprod.
0.00
Control
19.92
Control
16.67
Treatment 2
12.17
Treatment
2
Control CV
20.586%
% control orgs
producing 3rd
brood
91.7%
PASS FAIL
Check One
pH
1st sample
Control
Treatment 2
D.0
Control
Treatment 2
8.05
7.99
8.04
7.92
s
t
a
r
t
1st sample
e
n
d
7.95
7.99
7.96
8.01
1st sample 2nd sample
8.02
8.03
7.97
7.95
s
t
a
r
t
1st
8.03
7.98
7.98
8.01
s
e t e
n a n
d r d
t
sample 2nd sample
8.25
7.98
8.22
7.99
8.22
7.83
8.26
7.97
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates
Complete This For Either Test
Test Start Date: 03/07/07
Collection (Start) Date
Sample 1: 03/05/07 Sample 2: 03/08/07
Sample Type/Duration
Sample 1
Sample 2
Grab
Comp.
Duration
24.7 hrs
24.2 hrs
D
I
L
U
T
2nd
1st P/F
S S
A A
M M
P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
40
180
514
657
<0.1
<0.1
0.4
0.2
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
%
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs`:
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Mierh ech T6L
Data Sheet for Mini Chronic Pass / Fail Test: Ceriodaphnin (labia
;lient: LAMA-
,IPDES #: K)Lo yi-{ 7z:;
)ilution Water: Lake Reidsville
'est Organism Source:
tirred / Aerated for D.O.: Y /(EP
:ontrol Organism Reproduction
lay #3 1 2
Incubators:
Date End: 3-0/-o?
Time / Date Neonates Born: , 1 �/. 7 v st Renewal Da 3 0')
Pipe #: County: �Gp- -la„� co. Date Start: 3 - 7-6)
Time / Date.of Culture Transfer: q : ! ;. / '�. ;• 7'Time Start: •CEO. f
7 — .�i - 1-
Age of Neonates at Test Start: yvr-y 2nd Renewal Date: 3 /2--0'
3
Randomized: N Culture Tray Temp:2,5 °C
4
Young Produced
0
0
0
U
0
0
0
0
0
0
0
C.)
.dults Live / Dead
L
L
L
.
L
i,
L
L
L
L
L
L
2
10
L.
Young Produced
3
-3A
y
7—/
/g
Mo
Li
Li*
'7'
4
1/2.1v
V
.dults Live / Dead
L
L.
_
L
L
L
L
L
i_
L
L
L
2
Young Produced
;9' o
9
0Je'
/%
'
/
/o/tb
S
6h
/a
6f /l
dults Live / Dead
L
L
L
L
L
L
L
I
L
L
L
L
Dtal Produced
2-3
-eatment 2 Organism Reproduction
Effluent %:
1 2
3
)51
Percent Control Producing 3rd Brood:
iia
19
>, %
Young Produced
0
CU
0
0
0
0
0
0
0
0
`G
0
clults Live / Dead
L
1—
L
L
L
L.
L
L
L
L
L
L.
2
Young Produced
3
'Z
14
!
3
3
Z
2.
't{
Z
1
lults Live / Dead
L
L
L
L
L
(.._
L
L_
L
L
L
L.
•
Young Produced
S�
.,
,fir.
iv.�
11
1L•
cults Live / Dead
L
L
L
)tal Produced
i6 14 1 g ao . l� i o g I 1 �
)mmel : I-- I'I c 3 �1� % 1 �- 5r1 0'1.611 L'_.04_4 9L) F
Sample Type / Duration
Sample 1
t00%
pH
7.51
Grab
Comp
X
Duration
2 14.7
Sample 2
Control
Treatment 2
rig
151 Sample
8.c6
tf,gc
r1,q2
D.O.
1' Sample
Control
rf• 95
7,q9
Treatment 2
ft 1L
q. o I
Temp.
Control
151 Sample
25.0
Treatment 2
25.0
24.9
Start End
zy•2
151 Sample
25.1
25.0
25,0
25.0
Start
End
Analyst: ehE
Collection (Start) Dates:
Sample 1: 3-5-07 Sample 2: 3- $- 0`1
Test Transferred Fed
By: By:
Day 0 'fib'— i L-
Time End:it) :00 q..-,
Time:
Time:
Reviewed by:_
Day I
Day 21re
Day 3
Day 4
Day 5 iir&�
Day 6
Terminated by: /!/L
2"d Sample
8, 03
1.98
8•01
2nd Sample
8.22
rj.83
S. 2(0
1.� 1
2nd Sample
z5.
25. 0
241
24. q
Start
End

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address:
Lao6nbu'� -Moil-en A irp9,4 PO#
C el as V�ndem6r NPDES #:
1 b i A eo r-i- j, Phone:
City: FAa.,,,-Een
County: 30,41,,,,, d State: c. Zip:
Type of Facility Generating Effluent:
1N,wTP
crs,o(A)
-i21v6--
Pipe Number:
2'636`t
Sample Information
Sampling Site:
Sample Type:
Sampling Time:
L-Mflc a,F�
Grab Composite
START Date:
END Date: 3
Sample Chilled (Covered with Ice): Yes
Collector's Name (Print): C,1-,arle,s VON-.dexbpf
Collector's Signature: e \J' u
3-5- in
# of Containers
Time: $;30
Time:
No
q:I0
2—
PM
®i PM
Toxicity Test Information
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample T m erature
Sample Receiving (L
bof story Us
Method of Shipment: WTC(p/u) UPS
Circle One Other:
e Only) R,_1
Received From:. 1 *V& s 0(L vas
Received By. ' I
Sample Temperature (C°): ()/ Cj,,L Sample Condition: le ec
ate: -07 Time: AM PM
Date: 3-4-01 Time: /0;4° Se PM
Date: 3 '"a —) Time: J I :Jo . 1t PM
Date: ?''-' Time: ir .1� A • PM
Fed -Ex
3-6 0 7 1-4 . �S
Date: 3`C -G 7 me: . c AM)

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address:
City:
County:
Cl- 1�a.+clitvlbt•r
16 701 A rFe r4- a�,
Ma„t-E-,n
State: hic_
Type of Facility Generating Effluent:
PO#
NPDES #: Nc oa 1-147Z5
Phone: (qb) $ 444 -S0RI
Pipe Number:
Zip: 22836 LI
Sample Information
Sampling Site:
L,MAG eaClvQ.h4-
Sample Type: Grab ✓Composite
Sampling Time: START Date: 3 -g _07
END Date: 3 -q _67
Sample Chilled (Covered with Ice): Yes .�
Collector's Name (Print):
Collector's Signature:
# of Contai m -rs Z
Time: $: S'D AM PM
Time: :Oc. AM PM
No
Tme EA\
3-0-q as i-'IUOAM
Toxicity Test Information
4S
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
re'r ClAcvele-S VoivicAvr,
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperature (C°):
Date: a Time: $ i M
Date: . q+-07 Time: "I'14zirOPM
�-- Date: Time: AM P
Date: 3._ 4.- 07 Time: 13 41 AM
Method of Shipment: WTC(p/u) UPS Fed -Ex
ircle One Other:
Sample Receiving (Laboratory Use Only)
Received From: Grp►.IC' N t\\�
Received By: av1^ rr Date: 3 -I- 01 Time: l Can AM i'84�..
Sample Temperature (C°): O t 2 / 0 ,a Sample Condition:
Lcc.c.

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 7.8333 -10.1667 0.4493 18.0000
2 6.8333 -7.9167 0.3098 14.7500
3 5.8333 -6.1667 0.2554 12.0000
4 4.8333 -5.9167 0.2145 10.7500
5 4.0833 -5.1667 0.1807 9.2500
6 4.0833 -4.9167 0.1512 9.0000
7 3.8333 -4.1667 0.1245 8.0000
8 3.0833 -3.1667 0.0997 6.2500
9 3.0833 -2.1667 0.0764 5.2500
10 2.0833 -0.9167 0.0539 3.0000
11 2.0833 0.0833 0.0321 2.0000
12 1.8333 1.0833 0.0107 0.7500
1
W = X 543.5449
568.5833
Calculated W = 0.956 Critical W = 0.884
0.956 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
F =
Test Passes!
F test for Homogeneity of Variance
Effluent variance 34.8788
- 2.07
Control variance
16.8106
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
2.07 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

1
EQUAL VARIANCE t TEST
19.9 - 12.2
t = - 3.734
2.075
Degrees of freedom = 22
Critical t = 2.508
3.734 a 2.508
Test fails. There is a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test FAILS
The mean # of young produced by each group is dissimilar

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia Tc�
Facility LOA C._
NPDES#: NC oc) LI 72 5" Pipe#c / County Se tictric/
Laboratory Performing Test 6-1 vtc•
Signature of O.R.C.
Signature of Lab Supervisor
Sample Information
Sample 1
Sample 2
Control
Collection Start Date
Grab
Composite
(Duration)
Hardness(mg/I
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receipt
y /t,c-?
y do'?
r-.
!,
_ y
z3•r`i
2.3, b
Onage
Li Z'
f, 01 L)
I b 5
c,Iy
e:33
1:, ,
_
-.'
c.y °c
p �•
°C,
Comments Adel4 • 1,�,�I� t,-,erActl; -3 /
11((1v�51�e��5 - :yet~ tae,.ck
-CDC AC*A;(k7
Control
Effluent%
Effluent%
1 .3
Effluent%
Z.(
Effluent%
Effluent%
, y
# Young
Adult
(L)ive (D)ead
# Young
Adult
(L)ive (D)ead
# Young
zz-
L
Test
Information'
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
Start Date
End Date
/707
Start
Renewl
Renew2
Start Time
I . I SF:',
Start
End Time
9:zr
Renewl
Renew2
c.'i
tc.y
Control
Control
Control
€.a-1
e,It
7.E E.
p.07
.c3
7.�7
7.Q&
Iw.c I
7,q 5'
e.cz
7.q8
7.9'z_
F,cI
e. c3
7.9 `i
7.91-
7.91
7.(oL
2.7 ,
2 -i .0
7, 7 5
ZS.c
7,97
I
27�L
•7, $ .3
z5,o
Z5, o
7.78
Zy.S
7_5,0
7.5y
Z7•I
Z.>.0
Organism#
2 3 4 5 6 7 8 9 10 11 12 Mean
z.
1 2
ZL
11
LC
ZL
L
25
Z5
L
L
2'-1
L.
27
ZI
L
3 4 5 6 7 8 9 10 11 12 Mean
2C
L
2C
L
15
L
2 3 4 5
Itt
I-1
ly
21
2.I
L_
10
L
L-
6 7 8 9 10
IrV
(
l '3
19
Mean
f5i
Adult
(L)ive (D)ead
L
L
L
L
L
L
L
L
% Red
35.7
# Young
Li
_
'-‘
..
11
-
5
v
17
♦♦
Z
1
8
L
4
J
4
I V
Adult
(L)ive (D)ead
L
L
L
L
L
L
L-
L
D
L
%Red
75..7
# Young
6
_
3
..
7--
-
3
v
8
v
Z
,
3
lJ
3
A
8
I V
.........
Adult
(L)ive (D)ead
L
L
D
L
L-
t_
L
L
L
Mean
Chronic Test Results
Final Control Mortality %
% Control 3rd Brood
Control Repro CV
U
1 pc)
7•U.')
48 Hour Mortality
Control IWC
Cof IC
Significant?
ality Significant
r
No Conc.
Reproduction Analysis:
Repro. LOEC= 1.2 %; NOEC=0.6J %
Method: 0..),,c115
Normal Distrib? Yc5 Method: l!c_jelc c.
Statistic: c •`IS j Critical: t.cl 2
Equal Variances? Ye-5Method:L jcIts
Statistic: 11, B Critical: 15.CI
Non -Parametric Analysis (if applicable):
Method:
Effluent % Rank Sum Critical Sum
# Young
3
Z
Z
Z
3
4.;
Adult
(L)ive (D)ead
L
L
L
D
L
1 z. 8
% Red
L EfrI
Overall Analysis:
Result = PASS/FAIL or /
Test LOEC= I • %; NOEL= (? . b6'
Chronic Value= O. qz %
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
t% Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95

Client: LVAA-C-
NPDES#: NCO° q--/z5
% Effluent Dav #
Control
3
5
7
Total
3
C�. (a.S% 5
7
Total
1.2)
5
3
7
Total
3
Z.% 5
7
Total
5-.Z
3
5
7
Total
3
/O. % 5
7
Total
Meritech, Inc.
Ceriodaphnia dubia Reproduction Data Sheet
Start Date:
End Date:
'Hz Flo,
Replicates
2 3 4 5 6
7
8
Start Time:
End Time:
Reviewed by:
9
I'.
qyw5-
10
0
0
0
0
0
0
0
y//Q
y//d
Yl$
34/
No
y/S
� Q
3%1A
5
8
11
12-
i 1
11
12
tb
12-
5"8
8
Zz
•2$'
"2.-'-)
zS'
25'
2y
zq
2,5'
21
20
O
O
O
O
O
O
O
L
9/g
Y/
'�/�s
y/7
s
��
3/7
3O9 .
3fe
a
8
8
8
A
8
6
6
Zo
-Lc)
20
2u _
15
z/
00
!cam
-zo
6
O
o
O
O
o
O
O
o
0
0
3//e9
A
9
y/-
y/&
i q
9
y1&
9
//f
6
6
7
7/6,
6
'
li
6
6
1 !
16
17
P1
2/
! ii
/6
/0
/3
/9
b
O
o
0
o
O
o
0
O
o
1
9
4
q
346
`f
tt`
.2)
5.--
o
ox
o
I
Y
o
y
D
—
0
'i
9
`!
c
1-7
Z.
F
q
y D
5
(3
(7
O
O
O
O
O
o
00
3
3
a
3
'I
.2
3
:
V
3
11
0
b D
O
y
0
0 4t-
0
`I
O D
6)
-3
z D
3
13
2.
3
3
8
3 p
0
0
0
0
O
0
0
0
0
0
23)
0
3,7)
Z
0*
a
GD
0
4'
7
0
1
3rd Brood
!t0
C.V.
7.E3
% RED.
% RED.
eqvc �
c't - b1Ji5
aeac1
% RED.
4
% RED.
% RED.
Mean
Reproduction
Z3, 1
18.7
6.-I
35,7
5.7
7-.7
52,
2,6

ifitiAffilTI774E-C7fric I,Vc0
ENVIRONMENTAL LABORATORIES
.4 Division of VVA rcr Technology, and Controls. Inc.
T i3L
trsr
Incubator #:
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
!Client: (.YYI
;Dilution Water: Lake Reidsville
Collection Start Dat
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine (mgil)
Temperature (°C)
100% pH
Temp. of Stock:
Randomization:
NPDES#: on44725
Batch #
58S
Hardness (mg/I)
y2
Conductivity (umhos)
185
1st Sample
2nd Sample
`1 , ,
Li 9I
G 23 ,g
NM
to93
Mill
0.1
0.33
IMMINII
rl. Io:
BMIll
No
D.O. Adjustment:
Stirred Aerated
one
Neonates:
Tray #: 3
Transfer: Date/Time Li '1 T D�-1 $; 30,4M
Born: Date/Time9"t7 7r 1 v
Age at Start of Test: ,• hours
Test Start, Renewal, and End Dates / Times:
Start Date: Ilijfrip7 Time:
1st Renewal Date: ` /2.047
2nd Renewal Date: (-1/23/07
Time:
Time:
End Date: ' 1j�0-7 Time: TA SC'
Test Transfer:
Start: 00-
Day2: ►ir(—
Day 5: 1�1
Terminated:
Feeding:
Start: (vl.t_
Day 1: Ivlli
Day 2:
Day 3:
Day;:
Day 5:
Day 6:
rnL
Mk_
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Start- -
- End--
- Start
End ---
Start End
pH
D.O.
Temp.
Control
High Conc.
Control
High Conc.
Control
High Conc.
8.02
8.04
r(, 92,
25.0
26.0
8,11
7,(QZ
ZS. o
2S,o
g, G 1
7
7.icj
3-.o3
1 • 03
7.78'
7.7s
25'. a
'2.q6 91
2'sf 2?.D
25,E

Client Information
Client:
Contact:
Address: 16.7 c 4;pr,r1-
City: Mc,x 4v
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
C .-,-eSv 3 U4 ndrxcbery
County: e-f 1,nr1 State: ik
6(4
iBL- t8o33
PO #
NPDES #: lff ' ' )25
Phone: (c 318 - sz-
Pipe Number:
Zip: 2?3b K
Type of Facility Generating Effluent: jitk„rl"S
Sample Information
Sample Type: Grab ✓ Composite
Sampling Time: START Date: 141 b -a-) Time: $ 3-s
END Date: 1 -r ies , Time:
Sample Chilled (Covered with Ice): Yes -ram' No
Collector's Name (Print): Gi►cw la,s Varva e)n ba t3
Collector's Signature: th,, `7
# of Containers .2
$: yd
PM
PM
Toxicity Test Information
Test Required: Chronic:
Acute:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Test Organism: Ceriodaphnia Dubia:
Pimephales promelas:
Mysidopsis bahia:
M 14:51,,
u4';btll
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Teme C°):
!4
Date: Lien -d) Time:
Date: _ \ Time: b PM
Date: `/- /f7 sJ 2•r' 7-c7 Time: A
Date: L -/ % -07 Time: ,, o_? A M
Method of Shipment: WTC(p/u) UPS Fed -Ex
`c piplsOne Other:
Sample Receiving (Laboratory Use Only)
Received From: bU5
Received By:
AM PM
Date: L -A1 - CSC Time: (o 10 AM P�
Sample Temperatur/(C°): 0 / t1, Lk Sample Condition: T e c

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address:
City:
IWC: Mu
Toxicity Test Concentration(s): 10
List Any Special Requirements:
END Date: 14 -20. 07
Sample Chilled, (Covered with Ice): Yes �✓
Collector's Name (Print): Cj.�,�)���
Collector's Signature: tdlj,
L ctv rt.Au hrg - A rpi r 4-'
CirI46 Vane,lier
1 11-70A; rpbr4- .1A_
Maw} -on
County: Sc,714c, - c4 State: NC. Zip:
Type of Facility Generating Effluent: 'wWT P
PO#
NPDES #: NCoe 1-iyi 2J
Phone:
Pipe Number:
21,364
Sample Information
Sampling Site: L,MC- e k)Q.
Sample Type: a/
p Grab Composite
Sampling Time: START Date: Time:
Time:
No
# of Containers ' -
q.s-tp GPM
q;Ito1 PM
Toxicity Test Information
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia: ✓
Acute: Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Tempe - . e (C°):
Oc..oa: -1
Sample Receiving (Laboratory Use Only) Qc.1
^
Received From:��—
Received By:/CA
Sample Temperature (C°): ("�, �,� /
ate: 4-20 _n7 Time: MI 2p ,i52 PM
ate: 4,2 .4 Time: /-0;2i PM
ate: 1'J-0 . Time: II e A PM
Date: 'i - a '' `1 Time: ff.() PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
1-11/Z6.
Sample Condition:
Date:
`t-4_0-0--) (1, LiS 1 r\
Time: AM
1Cc'G

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D=
D* =
0.1213
0.9514
(p-value = 0.0283)
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data PASS normality test (alpha = 0.01). Continue analysis.

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 11.8241 (p-value = 0.0373)
Data PASS Bl homogeneity test at 0.01 level. Continue analysis.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)

Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
0.65% 10 0 10
TOTAL 20 0 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 10.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL'ANIMALS
CONTROL 10 0 10
1 . 3 % 10 0 10
TOTAL 20 0 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 10.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL
10 0 10
2.6% 9 1 10

TOTAL
19 1 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 9.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
5.2% 8 2 10
TOTAL 18 2 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 8.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
10 .4 0 6 4 10
TOTAL 16 4 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 6.
Since b is less than or equal to 6.0 there is a significant difference
between CONTROL and TREATMENT at the 0.05 level.
Summary of Fisher's Exact Tests

NUMBER NUMBER SIG
GROUP IDENTIFICATION EXPOSED DEAD 0.05
CONTROL 10 0
1 0.65% 10 0
2 1.3% 10 0
3 2.6% 10 1
4 5.2% 10 2
5 10.4% 10 4

Title: lmac
File: lmac Transform: NO TRANSFORMATION
ANOVA Table
SOURCE
DF SS MS F
Between
5 3785.2833 757.0567 99.4915
Within (Error) 54 410.9000 7.6093
Total
59 4196.1833
(p-value = 0.0000)
Critical F = 3.3769 (alpha = 0.01, df = 5,54)
= 2.3861 (alpha = 0.05, df = 5,54)
Since F > Critical F REJECT Ho: All equal (alpha = 0.05)

Ol N aN W N I-,
I Q I
Q I
I 1-' OI
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I • • • Ol Fi I H I U] I-. I-'
I 1A N al W N Q 1 I rt 9 1 (] I H I rt 5
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IMWHWJCOIW I ( t t I I rt
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1 1 1 K 1 F-'NNONO 1 I
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1 1 1 ;S 1 0 0 0 0 0 0 1 H 1
1 1 1 Co 1 000000 1 '',' 1
1 1 1 Hi 1 0 0 0 0 0 0 I 1
1 F-' NSA W 1-'F' I 1 0 1 000000 I I
1 co W N as VD W I tJ I 5 I ,
I FJWsAHCNIA t 1 •• I 1 1
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ro
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:U1.1ojSLIP 1y

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Dunnett's Test - TABLE 1 OF 2 Ho:Control<Treatment
TRANSFORMED MEAN CALCULATED IN SIG
GROUP IDENTIFICATION MEAN ORIGINAL UNITS T STAT 0.05
1 control 23.5000 23.5000
2 0.65% 19.1000 19.1000 3.5667 *
3 1.3% 15.1000 15.1000 6.8092 *
4 2.6% 5.7000 5.7000 14.4289 *
5 5.2% 4.1000 4.1000 15.7259 *
6 10.4% 2.8000 2.8000 16.7797 *
Dunnett critical value = 2.3100 (1 Tailed, alpha = 0.05, df [used] = 5,40)
(Actual df = 5,54)
Title: lmac
File: lmac Transform: NO TRANSFORMATION
Dunnett's Test - TABLE 2 OF 2
Ho:Control<Treatment
NUM OF MIN SIG DIFF % OF DIFFERENCE
GROUP IDENTIFICATION REPS (IN ORIG. UNITS) CONTROL FROM CONTROL
1 control 10
2 0.65% 10 2.8497 12.1 4.4000
3 1.3% 10 2.8497 12.1 8.4000
4 2.6% 10 2.8497 12.1 17.8000
5 5.2% 10 2.8497 12.1 19.4000
6 10.4% 10 2.8497 12.1 20.7000

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility LMAG
NPDES#: NC 0044 725
.1.• 11
Laboratory Performing Test 1L t l 1'\tt.; C (� , ). rlc
Signature of Lab Supervisor
C-60^41•^At
Signature of O.R.C.
Sample Information
IMMIII
5/7
k T
Sample 2
Control
Collection Start Date
Grab
Composite
(Duration)
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receip
;
it 7
'{
{
�
r .
Z 1.
7
2-5
,",.<r.aH�
- 4rLR**.
;;--
ilHardness(mg/I
r' 41
L(
1- C.
i„E,.'
r'Y'
'c
r
" °c
r'z. „
.'r• >{
Control
Effluent%
0 . (0 6
Effluent%
1.3
Effluent%
2. Co
Effluent%
5.2
Effluent%
N0.4
Organism#
Pipe# County
6/Le t lard
Comments
Test
Information'
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
Start Date
s49 7
IStart
CA
10.9
End Date
7
Renewl
IC.Y
Renew2
Oki
Start Time
Start
Control
End Time
9 :e6A,M
Renewl
Control
Renew2
Control
7.y�1
i•c7
7.7C:
7.�
�. 3
7. c/'t
7. ?�/
7.7
•1.c.0
?.-rl
J
'• 7
2 S. (;
I
2 .L
—
_
_
..
.
-
.i
r J
.. .. ....._..
# Young
1-.- i
,711
,r3
.),3
jz .3
,-4,.2tS
..)
l e(,
.r,
Adult
r•- .n.
(L)ive (D)ead
L
L_
L.
L.
L.
L L.
L.
L
L.':'.
1
# Young
Adult
(L)ive (D)ead
1
# Young
Adult
(L)ive (D)ead
1.
2
L-
3
L-
4
5 6 7 8 9 10 11 12 Mean
r*
L
2 3 4 5
L.
L.
�i.
L.
6
I �s
L
.2..'S
L
7 8 9 10
!/
L_
•).L.
L.
L.
l;>1
Moan
# Young
•
,2t
10
.
ICI
13
.1
) 1
1!
g5
1
V
it
J
i_3
I V
/ 5—
,moomoo_
u.7-
Adult
(L)ive (D)ead
L.
L
L
L
L
i'_.
L.-
L.
L.
L
Red
x�
# Young
G
7
,,
iv
,.,
(U
,..11
/('.
/6
u
I?
a
iy
1 v
S
All
Adult
%Red
(L)ive (D)ead
L
(
L
L-
L
L_
L..
._
L
L-21
# Young
Adult
(L) ive (D)ead
3
L
2
vl
L_
3 4 5 6 7 8 9 10 wean
L
L
7
17
L-
Chronic Test Results
Final Control Mortality %
Ta Control 3rd Brood
Control Repro CV
1(c:
48 Hour Mortality
Control IWC
0of1L'
Significant?' y
Final Mortality
Reproduction Analsis: L�
Repro. LOEC=j_.._7 %; NOEC=L� J%
Method:
Normal Distrib? Le-c Method: o 1} ."'
Statistic: l_- Critical:1_n
Equal Variances?P Method£rertkjf
Statistic:)-3 .
Non -Parametric Analysis (if ap licable):
Method:s$1; 1r�rrtX D, �Jia�:il'a/
Effluent % Rank Sum Critical Sum
C.(as _ _ 7S u_
cs'S- o 1S;b
T
_5 77, 0 7 S`V _
cc, Q J}:i
`. a- -
Overall Analysis:
Result = PASS/FAIL or
Test LOEC= / 3 %,• NOEC=O.(> %
Chronic Value=__‘1, 90. %
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/l
t% Reduction from Coned Renroducbon Mean
DWQ form AT-3 (8/91) Rev. 11/95

ENVIRONMENTAL LABORATORIES
n viv;s�nn oe w.vrc•r Tech r polcs9), ..nn' Contra's.
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
Client: Lin A
Dilution Water: Lake Reidsville
Collection Start Date
Sample Type / Duration
Conductivity (ur�hos/cm)
Residual Chlorinell(mg/I)
Temperature (°C)
100% pH
NPDES #: NG00441725
Batch #
Hardness (mg/l)
Conductivity (umhos)
yy
180
1st Sample
2nd Sample
-/74 7
5tiol&r(
/zq.?
C/z3.t0
[a4O
k 301
Lo .1
z 0 .1
0.Li
0.S
7. 99
$. 0(,
Incubator #:
Temp. of Stock: 25 °C
Randomization:
No
D.O. Adjustment:
Stirred Aerated
Neonates:
Tray #: .5
Transfer: Date/Time S- S't l/ L! 4/r,
Born: Date/Time S= 2--/.7 I
Age at Start of Test: oZ.3 hours
Test Start, Renewal, and End Dates / Times:
Start Date: '// 4?
1st Renewal Date:
2nd Renewal Date:
End Date: 5/iGrt 7
qpi
Time: I (:
Time: ?,..c -k--
Time: 3. CU 6—
Time: q AD,
Test Transfer:
Start: M (L
Day2:
Day 5:
Terminated:
/r(1
Feeding:
Start:
Day 1:
Day 2:
Day 3:
Day 4:
Day 5:
Day 6:
1/f
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Start
End
Start
End
Start
End
pH
D.O.
Temp.
Control
High Conc.
Control
High Conc.
Control
7, 9
"7. 79
7.7L
LLI
7.y8
6.07
7,119
?.3U
25 . U
7,13
3
7.0
"2 y .c1
7,gr1
8 10
�. Co(o
25.
7 q(c.
8.05
r1.88
'M 3
25.1
Ei cc
C.., 13
'7.60
High Conc.
Z7,()
25.1
2.5, ►

Client: L
NPDES#: NC 00-1/025
% Effluent Day #
3
Control 5
7
Total
O . (Q S%
3
5
7
Total
3
5
7
Total
3
5
7
Total
3
5, 2_.% 5
7
Total
3
5
7
Total
2
3
Meritech, Inc.
Ceriodaphnia dubia Reproduction Data Sheet
Start Date: 7/ /0 7
4
End Date: S /(�/O i
Replicates
5 6
Start Time: I I'•00�
End Time: . :0 A�
Reviewed by: /.N*_
o
v
J
v
O
o
-3/4
y /
3f
9
`//�
/ 8
1/8
`//, c7
`i/' 0
L/o/
r /z
Y/ o
G
-7
1/
11
/r
1v
1/
q
/U
. .)
a1
,q?
��
a3
:�,-/
-s—
_21
/6/
ao
Y/ q
//
1/
0
0
/()
0
p
0
`14,,
0
y/3
/1
0
3/9
//
v23
O
Vic
o
0
0
O
0
0
0
0
0
I
/(9
q
yil 1
Y/
`i/ I D
V76
y%y
01
YA 0
,a
`Y v
3
v
//
/ 0
7
3
7
/�
la
L.
:
�a
A
�'
11
o
Z
0
y/ ,
IC)
2,0
2
O
-376
0
IC
0
y�Z
1/
0
Y/L/
0
O
y�y
0
0
0
y�y
O
y/ec.
s—
O
0
0
0
0
0
0
0
0
a
Vi
y
ti
i/
IVY
` I
4
Y
.3
/v
F
_5.
s-
7
/9
6
k
f 6
267
1 V
s
.O
v
3
0
y
0
0
0
yf3
L
0
yfZ
O
3
3
.3
v
0
8'
O
7lo
7
/7
O
t2
3rd Brood
0
C.V.
Vo RED.
Mean
Reproduction
a,01
C..orgA)C� L431w�
a
IS £%b
% RED.
Vo RED.
% RED.
% RED.
72771
5,2 , 7

City: Mo.-NA-or-1
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
00°6
eL - / °LO
Client Information
Client: LaJr;,,bor - t4wc4arr krpopr- PO#
Contact: C ries Va,,,4Q,s,60,4-
Address: 167Di Air�r+
County: Scx+V r.,Gf State: N L
Zip:
Type of Facility Generating Effluent: \ vnl P
NPDES #:
Phone: (ql,)
Pipe Num`6er:
2S36y
318-5?2$Z,
Sample Information
Sampling Site: LvAe
Sample Type: Grab Composite
Sampling Time: START Date:
END Date: S - 43 -67
Sample Chilled (Covered with Ice): Yes v
Collector's Name (Print): Cjwle,b V,,nelextke rg
Collector's Signature:M,,
Time:
Time:
No
of Containers 2-
Toxicity Test Information / L%
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Mysidopsis bahia:
M0144 te, DAL.7 4- a►-15
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Te.
Date: S- B -07
Date: S7-r-c7
Date: S - f -b 7
Time: AM PM
Time: /J; d . PM
Time: AM
Time: /J'Ipe A
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only) , ,".,
Received From 6'\ 1 C"1`t"✓`
Received By: 1 'ter-- Date: S-- ---0 7 Time: 4c AM
Sample Temperature (C°): O. `i/ 0,1 Sample Condition: S (-*

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tarnco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address:
City:
County:
,_wI taivr4
State:
PO#
NPDES #: Nu-A1-1H-725
Phone: 1910)
Pipe Number:
Nc_ Zip: 2-8,3!
Type of Facility Generating Effluent: iiv1nTF
Sample Information
Sampling Site: L-MAC
Sample Type: Grab ✓ Composite
Sampling Time: START Date: S - b -67 Time:
# of Containers Z
la:o 5
END Date: 5 -11-67 Time: U•,4tp
Sample Chilled (Covered with Ice): Yes ✓ No
Collector's Name (Print): CLaAe...skke
Collector's Signature: (`,,14,o jf J
Toxicity Test Information
Test Required: Chronic:
Acute:
V
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Test Organism: Ceriodaphnia Dubia:
Pimephales promelas:
Mysidopsis bahia:
M deg_
PM
PM
Shipping Information
Relinquished By: ate: S - II -07 Time: '0-0 AM 'M
Received By: Date:
�M_;, „ • -II_ 0-1 Time: // c5"AM PM
Relinquished B;�� �, , Date: 5-/i - 0 7 Time: AM
Received By: Date: S II -07 Time: (JOS`A
Sample Tem - ure (C°): Method of Shipment: WTC(p/u) UPS Fed -Ex
j- ie._ 5 -.I1 _6 7 `(, [isle One Other:
Sample Receiving (Laboratory Use Only)
Received From: 17L-
13y: if
' ��-t Date: /( C I ime::(ul Am`l
Sample •l'emperaKue (C°): 0. c% Q.5= Sample Condition:
(

Title: LMAC
File:
lmac
Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D = 0.0740
D' = 0.5804
(p-value > 0.100)
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data PASS normality test (alpha = 0.01). Continue analysis.

r-�
Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 23.2033 (p-value = 0.0003)
Data FAIL B1 homogeneity test at 0.01 level. Try another transformation.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)

Title: LMAC
File:
lmac Transform:
NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX MEAN
1 control 10 19.0000 25.0000 22.0000
2 0.65 10 21.0000 26.0000 23.8000
3 1.3 10 4.0000 26.0000 17.2000
4 2.6 10 8.0000 20.0000 12.7000
5 5.2 10 5.0000 16.0000 10.4000
6 10.4 10 3.0000 17.0000 7.5000
Title: LMAC
File:
lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE 1 SD SEM C.V. %
1 control 3.5556 1.8856 0.5963 8.5710
2 0.65 2.8444 1.6865 0.5333 7.0863
3 1.3 51.9556 7.2080 2.2794 41.9071
4 2.6 17.7889 4.2177 1.3337 33.2101
5 5.2 26.4889 5.1467 1.6275 49.4878
6 10.4 19.8333 4.4535 1.4083 59.3795

Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05
1 control 22.0000
2 0.65 23.8000
3 1.3 17.2000
4 2.6 12.7000
5 5.2 10.4000
6 10.4 7.5000
130.50 ' 75.00 10.00
85.00 75.00 10.00
57.00 75.00 10.00
55.00 75.00 10.00
55.00 75.00 10.00
Critical values are 1 tailed ( k = 5 )

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address:
City:
i.
PO#
NPDES #:
Phone:
Pipe Number:
County: - State: Zip: -
Type of Facility Generating Effluent:
Sample Information
Sampling Site:
Sample Type: Grab Composite # of Containers
Sampling Time: START Date: Time: .Q,M' PM
END Date: Time: AM)PM
Sample Chilled (Covered with Ice): Yes No
Collector's Narne (Print):
Collector's Signature:
Toxicity Test Information
Test Required: Chronic: - Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
1WC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Shipping Information
Relinquished By: _.t ; , Date: Time: AM PM
Received By: �.�_-.. ,Date: Time: • AM%PM
Relinquished By: ';:` Date: -� - ,; 0 7 Time: AM PM
Received By: Date: Time: AM PM
Sample Temperature (C°): Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By: Date: Time: AM PM
Sample Temperature (C°): / Sample Condition:

Effluent Toxicity Report Form -
• Laborator:y Performing Test: MERI'1'ECH, INC
nn
•Siggnatuie oIes onsTiT .C�iarg
P ' I)
/ e
Signature of Laboratory > ervlsor
Chronic Pass/Fail and Acute LC50
Date: 06; _'.ff .p
NPDESi: NC0044725 Pipe{►: 001 County SCOTLAND
pe. rator
Comments:
* PASSED: 8.84% Reduction
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
Chronic Test Results
Calculated t = 2.182
Tabular t = 2.508
% Reduction = 8.84
Young Produced
22
24
21
20
20
20
22
24
16
18
21
21
Adult (L)ive (D)ead
L
L (L
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
Young Produced
20
18
18
20
14
19
18
20
20
21
20
19
Adult (L) ive (D) ead
L
L
L
L
L
L
L
L
L
L
L
L
pH
1st sample 1st sample 2nd sample
Control (8.03
treatment 2 18.03
.:.0.
Control
Treatment 2
8.01
8.08
s
a
1"
t
1st sample
7.85
7.44
7.70
7.50
8.08
8.07
8.14
8.13
s
e t e
n a n
d r d
t
1st sample
7.56
7.25
7.57
7.32
8.12
7.99
8.22
8.15
s
a
r
2nd sample
e
n
d
7.60
7.33
7.67
7.35
LC50/Acute Toxicity Test
.Mortality expressed as %,
combining replicate
% Mortality
Avg.Reprod.
0.00
Control
20.75
Control
0.00
Treatment 2
18.92
Treatment
Control CV
10.898%
% control orgs
producing 3rd
brood
100%
PASS FAIL
X
L_
Check One,
{
Complete This For Either Test
Test Start Date: 06/06/07
Collection (Start) Date
Sample 1: 06/04/07 Sample 2: 06/07/07
Sample Type/Duration
Sample 1
Sample 2
Grab
Comp.
Duration
23.6 hrs
23.9 hrs
2rd
1st P�•F
D
I 5
L
U M
T P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
42
18311030 ,21]H
0 1
<0.
0.5
%
%
%
%%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 = %
95% Confidence Limits
%
Method of Determination
Moving Average Probit
Spearman Karber - Other
start/end
1
Note: Please
Complete This
Section Also
Control
High
Conc.
start/end
J
pH D.O
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)

Merutech
Data Sheet for Mini Chronic Pass / Fail Test: Cerrodonhrrrn rhrhin
Client: (_�_
C"PDES Pipe #:_c2 h (_ County: .-J`c:o+1 / /
� �- or) Li y 7 z=_ Titrie / Date of Culture Transfer: , � a'�'�� Date Star(:
rN0! q Date End: ��i3� _1__
Dilution Water: rake Reidsville Time / Date Neonates Born: p ! Ol `�`�` "`/ Time End:
` Time Start: �f
Test Organism Source: -I / 'S 'C 1st Renewal Date: G
Age of Neonates at Test Start:1) ,�; s -_—_ l��/t? 7 Time: d 5 �. �`
Stirred /Aerated for D.O.: Y / L�__2nd Renewal Date: 6///p7 Time: S� /s'rirfl
Randomized: D N Culture Tray Temp: L5 °C Anal st;h" h� „�
Control Organism Re roduction Y /� Reviewed by:
2 3 a 5 6 Collection (Sta-t)-Dates:
8 9 10 11 12 Sample l: 6)/'% 7
o
L
Day #3
# Young Produced 1 0
Adults Live / Dead
Day #5
# Young Produced
Adults Live / Dead
Day #7
R Young Produced
Adults Live / Dead
Total Produced
Treatment 2 Orrlanism Re
Effluent %:
Young Produced
dults Live / Dead
)ay #5
Young Produced
.dults Live / Dead
ay
Young Produced
dults Live / Dead
nal Produced
)mments:
�L
Incubator
roduction
Percent Control Producing 3' I Brood: / CD ° �°
ti
,o
20
21
Sample Type / Duration
Sample 1
Sample 2
Hardness (mg/I)
I00%
pH
g,oz
g. 5S
Grab
LI 2—
Spec. Cond. (umhos/cm) 183
Chlorine (mg/1)
Sample Temp. at Receipt
p
H
Control
Treatment 2
D.O.
Control
l s' Sample
Sample 2: 6/7/C7
Comp
X
to30
Duration
�3,G
Z 3 . C1
tirtt
Z10-0
8.0 y3.01
6, 0 S,05
Is'
Sample
Treatment 2
7, 70
7.50
Temp. 15t Sample
Control
Treatment 2
9.G
z 0
2 5r0
Start End
I.0.)
0.5
L01l
0.8
1' Sample
a l `i
Test Transferred
B. O'7
5.13
Is' Sample
.S6
757
• -5 25
15f Sample
zs .3
25.3
Start
25.1
25.1
End
Day 0
Day I
Day 2
Day 3
Day 4
Day 5'1ll\
Day 6
Terminated by
Fed
By: By:
a/1
i
OIL
2nd Sample
2nd Sample
25.0 •25.0
c.
Start
25.0
End

IMeritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
0CQ0S cos
Client Information
Client: I__ OP\C
Contact: (,\.,,,,L < \rI II
Address:
County: -
State:
Type of Facility Generating Effluent:
City:
Relinquished By.
Received By:
Sample T
PO# T�L-
NPDES #: L�ir `I� t 7 2
Phone: MO i ; i . * ��i 2
Pipe Number:
Zip: -k -2./. rr
Sample Information
Sampling Site:
Sample Type:
Sampling Time: START
END
Sample Chilled (Covered with Ice): Yes
Collector's Name (Print): (' i.- .l \ f ,t
Collector's Signature: j ' s , �t.� ` t
I. Composite # of Containers
Time: •1 l (AM PM
Time: ;; :.; ANT. pm
No
LTA RI
Grab
Date:
Date:
•
Y
Toxicity Test Information
1
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
1 • I 1
- r•.
v
Shipping Information
Relinquished Bye (�,
e ^ jlA ?". \) L +, t Date: (....r_ _n� Time: /l) 1 AM PM
Recei v d.By: .,� ,'.` �; :i.r Date: is - ��'1 Time: %tr • ARPM
Date: (, - S• ° 7 Time/Z.e-, AM PM
Date: 6 Time/Zed AM PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Cir4-7Other: ape
Sample Receiving (Laboratory Use Only)
Received From:
Received 13y:
Sample Temp
VjALAix_
Date: (� —�- 61 _ Time:•1{C° AM
azure (C°): 0_'j_/p S' Sample Condition: ��r�
LIMP

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Talmo Rd
Reidsville, NC 27320
[phone]
Client Information
Client: OA C
Contact:
Address:
City:
County:
CANc.r1e.5 ,dphbP.�
Mot
State: 11L,
Sample Type: Grab
Sampling Time: START Date:
END Date:
Sample Chilled (Covered with Ice): Ye
Collector's Name (Print):
Collector's Signature:
CXCU`6 131
PO#
NPDES #: n(G004H3
Phone: (9 i0) 318 -$ 22 ?—
Pipe Number:
Zip: 2•�-��4
Type of Facility Generating Effluent: \A/ v/1--T
Sample Information
Sampling Site: 1.—t\Atp,ell
JPn�
Toxicity Test Information
Composite
6 -$
Time:
Time:
t
d of Containers Z_
cI,SO AM PM
9'.45 PM
s / No
Test Required: Chronic: Test Organism:
Acute:
[WC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Ceriodaphnia Dubia:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
SampTemperatu
ate: (a-g_ p-7 Time: /p; t53-- PM
Date: 11-...07 Time: PM
Date: 6-- —7 Time: (As PM
Date: 6- b' •-° Time: 7PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
iving (Laboratory Use Only)
Receives From: Q,II films_
Sample Tempo ire (C°): D. 3'/ (,
Received ( y:
Date: (41--67 _ Time: 336 AME&
Sample Condition:

n
Effluent Toxicity Statistical Results - Chronic Pass/Fail
Date: 06/28/07
Facility: LMAC
NPDES#: NC0044725 Pipe#: 001 County:SCOTLAND
Laboratory Performing Test: MERITECH, INC
Reduction: 8.84%
CONTROL 2.6% Effluent
# Replicates 12
12
Female Live 12
12
Adult Male 0
0
Adult Dead 0
0
Adult Mortality 0.00%
0.00%
# Neonates 249
227
Mean # Nonates 20.750 I
18.917
Standard Deviation 2.261
1.832
Coefficient of Variation 10.898%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered
i Group Neonates Centered
1 E 14-4.9167
2 C 16-4.7500 13 C 21 0.2500
3 C 18-2.7500 E 21 0.2500
14
4 E 18-0.9167 16 E 20 1.0833
5 E 18-0.9167 20 1.0833
6 E 18-0.9167 18 E 20 1.0833
19 E 20 1.0833
7 C 20-0.7500
1
8 C 20-0.7500E 20 1.0833
9 C 20-0.7500 20 C 22 1.2500
10 E 19 0.0833 21 21 2.0833
E
11 E 19 0.0833 2223 E 214 33.2.2500
12 C 21 0.2500 24 C C 24 500
24 3.2500

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x n-i-1) - x ( (i)
1 3.2500-4.9167
2 3.2500 -4.7500 0.4493 8.1667
0.3098
3 2.0833 -2.7500 0.1807 2.10.2154 4.8667333
.8000
4 1.2500 -0.9167 1
5 1.2500 -0.9167
0.1807 2.1667
6 1.0833 -0.9167 0.1512 2.0000
7 1.0833-0.7500 0.1245 1.8333
8
1.0833 -0.7500 0.0997 1.8333
9 1.0833 -0.7500 0.0764
10 1.0833 0.0833 1.0000
11 0.2500 0.0539 1.0000
12 0.0833 0.0321 0.1667
0.2500 0.2500 0.0107
0.0000
W =
93.1667
X 83.7434 I
Calculated W = 0.899 Critical W = 0.884
0.899 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
F =
Effluent variance 3.3561
Test Passes!
F test for Homogeneity of Variance
Control variance 5.1136
= = 1.52
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
1.52 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
20.8 - 18.9
t = - 2.182
0.840
Degrees of freedom = 22
Critical t = 2.508
2.182 < 2.508
Test passed. There is not a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test PASSES

Effluent Toxicity Report Form Chronic Pass/Fail and Acute LC50 Date: 09/21/07
Facility: LMAC
Laboratory Performing Test: MERITECH, INC
X
Signature ot Opera or in s nsible Charge
X
Signature ot Laboratory Supervisor
NPDES#: NC0044725 Pipe#: 001 County: SCOTLAND
Comments: *Dilution Water Batch
#614 & 615 Used*
* PASSED: -4.03% Reduction *
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
22
25
24
20
26
22
24
20
22
26
22
20
Adult (L)ive (D)ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
22
26
24
28
26
26
26
26
14
25
20
21
Adult (L) ive (D) ead
Chronic Test Results
Calculated t = -0.712
Tabular t = 2.508
% Reduction = -4.03
% Mortality
Avg.Reprod.
0.00
Control
22.75
Control
0.00
Treatment 2
23.67
Treatment
2
Control CV
9.762%
% control orgs
producing 3rd
brood
100%
PASS FAIL
Check One
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
7.95
7.93
7.96
8.06
s
t
a
r
t
1st sample
e
n
d
7.80
7.35
7.80
7.56
1st sample
8.09
8.10
7.89
7.93
s
t
a
r
t
1st sample
e
n
d
7.76
7.65
7.74
7.69
2nd sample
8.03
7.99
8.00
7.91
s
t
a
r
t
2nd sample
e
n
d
8.03
7.63
8.00
7.56
LC50/Acute Toxicity Test
(Mortality expressed
as %,
combining
Complete This For Either Test
Test Start Date: 09/12/07
Collection (Start) Date
Sample 1: 09/10/07 Sample 2: 09/13/07
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 23.4 hrs L A A
U M M
Sample 2 X 23.8 hrs T P P
Sample
replicates
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Hardness(mg/1)
Spec. Cond.(pmhos)
Chlorine(mg/1)
temp. at receipt(°C)
40
164
589
625
<0.1
<0.1
1.1
1.5
Concentration
Mortality
LC50 =
95% Confidence Limits
% -- %
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
Cnn n
pH
1 Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Client: L
NPDES #: NC ri- '.j72. 5--
Dilution Water: Lake Reidsville
Test Organism Source: Tray #
Stirred / Aerated for D.O.: Y /(N
Meritech, Inc. •l-tgL
Mini Chronic Pass/Fail Test: Ceriodaphnia dubia
Pipe #: 00 / County: Scot/civic/
Date / Time of Culture Transfer: cf - )/- L>_ l S-; -;e:) A,,1
Date / Time Neonates born: 9' )I - l j /2-- .S5vn 1st Renewal Date:
.11 Age of Neonates at Test Start: <23.7 hours 2nd Renewal Date:
RandomizedcN Culture Tray Temp: ZS °c ' Analyst(s):
Control Organism Reproduction
Day #2
1 2 3
Date Start:
Time Start:
8
10
# Youn. Produced
D
0
0
0
0
-
0
0
0
0
0
11
0
,L
0
Adults Live / Dead
L-
L-
L
L
L
L
L
L
L
L.
L.
1---
Day #5
1
# YoungProduced
`i
3 Z
`) /b
`t
L4
710
cif
"
L 1
a18 1 1
3/7
Adults Live / Dead
L
L
L
L_
L_
L
L
L
L-
L
L
L
Day #7
1
2
3
7
# Young Produced
10
to
to
B
11
i O
10
la
i;
)2 -
/0
1;
Adults Live / Dead
L
1--
L
L
tv
L-
L
L
L
L
L
L
I Total Produced
2 -
ZS
?A
20
2.6
22
Z`)
ZO
22.
Ztv
Z.
20
Test Sample Organism Reproduction
Effluent %: , 6
Day #2
1
2
Percent of Control producing third brood: 16.0 %
# Young Produced
0
Ci
0
C)
C)
0
0
0
D
0
Cj
d
Adults Live / Dead
L
L
L
L.
i-
1-
1-
1-
L-
L
L
L
Day #5
1
2
# Young Produced
44
1/i0
`//iD
��2
4//0
SAD
1 lZ
`II,•o
1
3//0
VB
1/2
Adults Live / Dead
L
L
L,
V_
iL
,L
L•
L_
'L
L
L
av #7
# Young Produced
ti 0
i 2
-
ID
(2-
► Z-
_
'��
,
16
u
1-2—Y93
.
lu
12
I I
8
IL
/p
Adults Live / Dead
L
i.._
L
L
L-
,‘._
U
L
L
L
L
L_
Total Produced
2
2t7
2fp
ZS
10
Cc- rents:
2-k.7
Incubator #:-'
Date End: y q AC 7
r\r) Time End: Y 36-,-
Q/r Lik7 Time:
c(l/?%b) Time: `� !i,vc•
ye, , t t., MP- Reviewed by:
Collection (Start) Dates:
Sample 1: 4/ 7
Sample Information
Sample 2: 1// 347
100% pH
G / C?
Duration
Sample 1
7, I ei
C•
2, 3, t-/ hours
Sample 2
7, 5 9
C..
'131° r Alhours
Batch #
0 Li 1
6i5
--.
Sami ple
Samplez
Transfer Day
0
2
5
'{ -...
= "'q
Hardness
(mg/L)
Lit)
q 0
-^'y
:5 -
'{r r,
pec. Cond.
(umhoslcm)
161
i ii%K
Q
.6
625
Chlorine
(mg/L)
^ras
n 1
`,
Receipt Sample
Temp. (C)
t nt
sr ,,i,
! r> ,.-
s u "1' ,
�''s R—�7
, '
1
1st Sample
Control
%`is
7,93
Sample
7'7 6
8, of
D.O.
1st Sam le
Control
7301,
Sample
7,,
<i6-6
Temp.
1st Sample
Control
Z .3j
2C u
Sample
-2,-1,LS•u
�
Transferred by: Fed by.
Day 0 14))2'
Day 1 r vlL
Day AK- :41L,
Day 3 � .--
Day 4
Day 5 it../
Day 6
Terminated by: !G
1st Sample
8. /0
7,y3
1st Sample
7($)
7,1,9
1st Sample
2C
f
'
2nd Sample
S"s
7.Y5
7,9)
2nd Sample
7, ta3
2nd Sample
si0
- -1
7.5•.

fl
END Date: q-11_07 Time: 10.-10
Sample Chilled (Covered with Ice): Yes / No
Collector's Name (Print): G riez
Collector's Signature: ,o V
Toxicity Test Information
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: LM6C
Contact: G-a.las Vcolc€
Address: tg.7p1 r+
City: Max -Eon
County: Sc. e}k,.ina State:
cy\1\<
('?tut,i0
tNtC . Zip:
Type of Facility Generating Effluent: W NA/TF`P
PO#
NPDES #: FJGO6LfL 725
Phone: (q tel gt44 -5og i
Pipe Number:
2836 4
Sample Information
Sampling Site: LM'AC, ac-FjJer4
Sample Type: Grab ✓ Composite # of Containers 2.
Sampling Time: START Date: q _:4Q _0-7 Time: Ip•. y 5 AM PM
PM
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
2.6°C,
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperat
1. ure
(q°):
Or
R-1,.�1
9-AN -07 Time:
9^((-o1 Time: OLt1) T►PM
9 - I (-fl' Time: IV, I SAM
`J - I f v Th Time: t1-1_13—AM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Date:
Date:
Date:
Date:
Sample Receiving (Laboratory Use Only) ckt-c—
Received From:CJAPE, c S S
Received By:
Sample Tempera re (C°): \ .1 / 1I Sample Condition: _Ltd
7j/`6
y��d
Date: qj -il-o1 Time: 14)C-

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
MIL( 97
Client Information
Client: tA(1/4(.,
Contact: CA,arAa.S
Address: Eb'D6 Aze-Fewa- g&
City:
Mo,�c+trr
County: +L,,,,a, State: NC, Zip:
Type of Facility Generating Effluent: W`f-r?
PO#
NPDES #: I4cd Q y 1.4-15
Phone: (c 10) 31Ag2`t32
Pipe Number:
113bu
Sample Information
Sampling Site: LMict( P,
Sample Type: Grab Composite # of Containers 2
Sampling Time: START Date: q_Is _o7 Time: q; SS i PM
END Date: q-114-D1 Time: q•,yp PM
Sample Chilled (Covered with Ice): Yes ✓ No
Collector's Name (Print): �� rjG-s �a►�b ��l�q
Collector's Signature: V
Toxicity Test Information
U
Test Required: Chronic: Test Organism(Ceriodaphnia Dubia
Acute: rtmepnales prome
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
746
as:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sam le Te pwrat ure (C°):
Date: .y Time: /D16S
Date: ' o'( Time: /a PM
Date: 9-CI Time: I ' :3a t1 PM
Date: S IK41 Time: .61 PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
, A_.Circle O „.O her:
ample ' eceiving aborator rse Only)
Received From: Nu I4'
Received By:
Sample Tempe
an S
- ri
Date: Time: y •/ AM F
ure (C°): is . 5 /4 Sample ondition: a
M

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 09/21/07
Facility: LMAC NPDES#: NO0044725 Pipe#: 001 County:SCOTLAND
Laboratory Performing Test: MERITECH, INC
Reduction: -4.03% CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 12
Adult Male 0 0
Adult Dead 0 0
Adult Mortality 0.00% 0.00%
# Neonates 273 284
Mean # Neonates 22.750 23.667
Standard Deviation 2.221 3.869
Coefficient of Variation 9.762%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 1.00
Success is: survival
Critical b value = 8
12 > 8
b = 12
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 E 14-9.6667 13 C 24 1.2500
2 E 20-3.6667 14 C 24 1.2500
-, 3 C 20 -2.7500 15 E 25 1.3333
4 C 20 -2.7500 16 C 25 2.2500
5 C 20 -2.7500 17 E 26 2.3333
6 E 21-2.6667 18 E 26 2.3333
7 E 22 -1.6667 19 E 26 2.3333
8 C 22-0.7500 20 E 26 2.3333
9 C 22 -0.7500 21 E 26 2.3333
10 C 22 -0.7500 22 C 26 3.2500
11 C 22-0.7500 23 C 26 3.2500
12 E 24 0.3333 24 E 26 4.3333

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 4.3333 -9.6667 0.4493 14.0000
2 3.2500 -3.6667 0.3098 6.9167
3 3.2500 -2.7500 0.2554 6.0000
4 2.3333 -2.7500 0.2145 5.0833
5 2.3333 -2.7500 0.1807 5.0833
6 2.3333 -2.6667 0.1512 5.0000
7 2.3333 -1.6667 0.1245 4.0000
8 2.3333 -0.7500 0.0997 3.0833
9 2.2500 -0.7500 0.0764 3.0000
10 1.3333 -0.7500 0.0539 2.0833
11 1.2500 -0.7500 0.0321 2.0000
12 1.2500 0.3333 0.0107 0.9167
1
W = X 194.6365
218.9167
Calculated W = 0.889 Critical W = 0.884
0.889 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
Test Passes!
F test for Homogeneity of Variance
Effluent variance 14.9697
F = _ - 3.04
Control variance 4.9318
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
3.04 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
22.8 - 23.7
t = _ -0.712
1.28E
Degrees of freedom = 22
Critical t = 2.508
-0.712 < 2.508
Test passed. There is not a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test PASSES

Client Information
Client: L1)ajc,
Contact:
Address:
City:
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
0-ar (Qs Vanden
lb?Ol AZ~.
Mcxxkon
County: $�. ,,r,d State: • Jc, Zip:
Type of Facility Generating Effluent: W WIMP
PO#
NPDES #: fJ Goev-14 5
Phone: ) 844 -5o11 t
Pipe Number:
2834
Sample Information
Sampling Site:
LN,AC, ec-Ploerrr
Sample Type: Grab V Composite # of Containers 2
Sampling Time: START Date: q -in _p- Time: 10•, 4 5 PM
END Date: q.11_07 Time: 10'.lo PM
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): Ci6ari �
Collector's Signature: •
Toxicity Test Information
Test Required: Chronic: Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
2 -bcin
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperature (
Date: 9-,11 -07
Date: 9.1-0/
Date: - 11 -151
Date: ¶ - I ► ex)
Time: CQ.15-- ' M
Time: /o:fo '1% PM
Time: W. I S-AM
Time: ('e;,s--AM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Date:
Time: AM PM
Sample Temperature (C°):
Sample Condition:

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: LtAAL
Contact:
Address:
City: Mo„ non
61pl A;iQo,• - R
County: Sccerkx,,,d, State: NG
PO#
NPDES #: I,iG o y 4-t25
Phone: [phone].gz432
Pipe Number:
Zip: 1136y
Type of Facility Generating Effluent: W-VV- f
Sampling Site:
Sample Type: Grab Composite # of Containers )
Sampling Time: START Date: q.13_07 Time: q ; 55 PM
END Date: 01-14-b1 Time: 01%46 PM
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): C� � _ CANme `ia6 �1q
Collector's Signature: ,,,A,� 'V LJ
Sample Information
LMifiU �.
Toxicity Test Information
Test Required: Chronic: Test Organism Ceriodaphnia Dubia.
Acute: imep a es prome
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
7_Co')
as:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample TFmp� ure (C°):
Date: 41 Time: co*5
Date: ` o1 Time: /6 : !g,' PM
Date: 9-f i - 1 Time: ! i :vs a PM
Date: l'i -,1 1 Time: 11', a d fag PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Date:
Time: AM PM
Sample Temperature (C°): / Sample Condition:

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/14/07
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County: SCOTLAND
Laboratory Performing Test: MERITECH, INC
X Signature eo er o in esetA4T yes
sible Char e
Signature of Laboratory Supervisor
Comments: Dilution Water Batch
#631 & 632 Used
** Mann -Whitney U = 0.0 **
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
23
24
27
25
14
24
23
24
21
23
27
23
Adult (L)ive (D)ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
11
12
11
13
12
11
4
9
12
13
13
13
Adult (L)ive (D)ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = 51.80
% Mortality
Avg.Reprod.
0.00
Control
23.17
Control
8.33
Treatment 2
11.17
Treatment
2
Control CV
14.473%
% control orgs
producing 3rd
brood
91.7%
PASS FAIL
Check One
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample 1st sample
7.95
8.00
8.01
8.00
s
t
a
r
t
1st sample
e
n
d
8.09
7.80
8.03
7.75
7.94
7.85
7.94
7.95
s
t
a
r
t
1st sample
e
n
d
8.20
7.48
8.04
7.33
2nd sample
7.98
8.01
7.98
8.01
s
t
a
r
t
2nd sample
e
n
d
7.65
7.60
7.59
7.36
LC50/Acute Toxicity Test
(Mortality expressed
as %, combining
Complete This For Either Test
Test Start Date: 12/05/07
Collection (Start) Date
Sample 1: 12/03/07 Sample 2: 12/06/07
Sample Type/Duration 2nd
1st P/F
Grab Comp. Duration D
I S S
Sample 1 X 23.7 hrs L A A
U M M
Sample 2 X 23.9 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
46
171
1582
1400
<0.1
0.14
1.3
1.3
replicates)
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
% -- $
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
r �
Note: Please
Complete This
Section Also
start/end
Control
High
•
pH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Meritech, Inc. tr3
Mini Chronic Pass/Fail Test: Ceriodaphnia dubia
Client: Lvm P L Pipe #: po j County: S -Hc ;1d Date Start:
NPDES #: NC cc Y 44'12 S Date / Time of Culture Transfer: C 7 / ;, .> [` s Time Start:
Dilution Water: Lake Reidsville Date / Time Neonates born: i a_ - S - i77 /y. ; , I•, 3i7,\\ 1st Renewal Date:
Test Organism Source: Tray # 3 Age of Neonates at Test Start: S' :,1-5—hours 2nd Renewal Date:
Stirred / Aerated for D.O.: Y / 6 Randomized:6)/ N Culture Tray Temp: 2`I .q °C
Control Organism Reproduction
Day #2
1
2
3
4
5
6
8 9 10 11 12
# Young Produced
C.
0
0
0
00 C)
0
0
0
0
d
Adults Live / Dead
Lr
L_
L
L
LLL
L
L
(-
L
L
Day #5
1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
,S
`-F
&
'
)---.
9
`
3
9--
5
3
Adults Live / Dead
L
L
L
L
L
LLL
L
(-_
L
L
Day #7
1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
yet)(:
%
10 f
l%
]D
)6l0.
1/1G
%
Va
71b
rir1g
XY(D
Adults Live / Dead
L
i
/
L ,
l__.
i.._
Z.__
/_
L
L
L
1---
Total Produced
),3
29
93
,2S
iy
zi
a.3
'-'i-
a 1
a.3
27
3
Test Sample Organism Reproduction
Effluent %:
Day #2
1
Percent of Control producing third brood: ' / %
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
)
00
U
0
0
0
0
C
C
0
0
Adults Live / Dead
L.
L
L
L
L
L
L
L
L
(__
_.r
�._
Day #5
1
2 3 4 5 6 7 8 9 10 11
# Young Produced
L/
7
Li
zi
it
:Z
y
9
5-`
5
Adults Live / Dead
L
L—
(.._
L
L
L
L
L.
C__, L
(--
L
Day #7
1
2 3 4
# Young Produced
.
R
6
9
-
,:
s
'9
,9
g
Adults Live / Dead
I,_.
L
L.
L
L
L
I
:7)
L_
L.
L
i_
Total Produced
i J
21 j)
' I
)
/i
1
'1
)).
1 -,
'3
t3'
07
Incubator #:
Date End: / 2_// z / , ?
Time End: : i S- �n
Time: '! L/ ()0..
Time: Cr: O ro--
Analyst(s): , /"L%'2, Reviewed by:
Collection (Start) Dates:
Sample 1: / 1/3/67
Sample Information
Sample 2: 1214
100% pH
G / C?
Duration
Sample 1
r(, cf Z,
C
2.3.7 hours
Sample 2
7, 9 S
G.
23 ,q hours
BatchSample
L3 1
613z
1
Sample
2
Transfer Day
0
2
5
Hardness
(mg/L)
II�
Li llr
„�
,•
I (J
_
Spec. Cond.
t I
.....3.(umhos/cm)
l�1
(jr�`
U yo
Chlorine
(mg/L)
L.G.I
C,I9
Receipt Sample
Temp. (°C)
'i�
1 /
r23
Comments: uv ,�}� hop W- ,^ rL� r: �'1,:,niti��5 r r�U
'4-2.rdl
1st Sample •
Control
IT cis
53o
Sample
',l) (
5.CC.
D.O.
1st Sample
Control
g,oi
-7,S
Sample
6.0.3
7, 75
Tern .
1st Sample
Control
2 6
? j L'
Sample
25. (
1,') .C`
Transferred by: Fedby:
Day 0 1 /H
Day 1
Day2 it4.11'114L.
Day 3
Day 4
Day 5 h111----1,1.1 L
Day 6 .je!'
Terminated by:
1st Sample
7,4'
7? LI
7. gs
1st Sample
7,08
7,33
1st Sample
ZS�
2nd Sample
r
,7 i5
8.CI
2nd Sample
T.6D
5`,
9
2nd Sample
CO
J J�
2 'J

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address: c„-74,
City: __Mca.,+,5n
County: 5co4-1L,�
State: N r
Type of Facility Generating Effluent: \are„,
Zip:
PO#
NPDES #: NCto44725
Phone: AD) RyW-c,OR1
Pipe Number:
Sample Information
Sampling Site: I_MAL cz
Sample Type:
Sampling Time: START
END
Sample Chilled (Covered with 1 )
Collector's Name (Print): mfie.s
Collector's Signature:
Grab ✓Composite # of Containers 2
Date: 1Z- 3_o-t Time:
Date: 12- ti - -i Time:
ce :Yes No
%N.Aonb12-iro,
Toxicity Test Information
Test Required: Chronic:
Acute:
Test Organism: Ceriodaphnia Dubia:
IWC:
Toxicity Test Concentration(s): 24.76
.76
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By -
Received By:
Sapl Temper
Ak' -- - -
Date: 12-4-(37 Time: /p. of I j PM
Date: Time: 16O
Date: l;)- v/-•o7 Time: Ia'.15-AM te
Date: la•1 -in Time: /3:4)---AM(10
e (): Method of Shipment: WTC(p/u) UPS Fed -Ex
;� Circle One Other:
.0-1 ,
Sample Receiving (Laboratory Use Only)/?e )/ A 5) e J : y%L.-f-�1� �— %2- /- G i -7 : o -, P/'
Received From:
LcaJ✓��nb4 -3 �1n�-c�q A i rno.-t-
Rd.
Received By: .�
Sample Temperature (C°):
Date: 1 -< -C 1 Time: 1I °' )PM
Sample Condition: A i ,.d

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: LMt1L.
Contact:
Address:
Sampling Time: START
END
Sample Chilled (Covered with Ice): Yes
Collector's Name (Print):
Collector's Signature:
Druvr
+kz'
nrle S YowAQ.vibpX
I�o'iei Airpert— FA
City: M�..X+c n 1
County: at:A-1m
State:
Type of Facility Generating Effluent:
Pt �
1n► vvr-P
PO#
NPDES #: I' C4644725
Phone: Mid) S 4y -Sods 1
Pipe Number:
Zip: 1 3 64
Sample Information
Sampling Site: LM A(,
Sample Type: Grab t/ Composite # of Contain s
Date: 11.6„_0.7 Time: C�PM
Date: 12-2_ 61 Time: I N 6 o AM PM
No
N%a►a�6a r9
Toxicity Test Information
Test Required: Chronic:
Acute:
—Test Organism: Ceriodaphnia Dubia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sample Temperature (
Date: ►-Z,_-t_on Time: j}.' PM
Date: 1„2,,-2-67 Time: /a:, PM
Date: a -?-a-7 Time: I1',ao KM PM
Date: Time: 11,7.a AM PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
-1., Circle One Other:
•
R � c 'd : � � f-�-- 1 — 7 — v 7 /. 3o PNt
Sample Receiving (Laboratory use Only)
Received From:
Received By: Date:
Sample Temperature (C°): /,',/ /, 3 Sample Condition:
nx,t.sAed : Jx,,
_ /.Z-7-07 5:I5Pr
430Am.
ced-

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 12/14/07
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:SCOTLAND
Laboratory Performing Test: MERITECH, INC
Reduction: 51.80%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 11
Adult Male 0 0
Adult Dead 0 1
Adult Mortality 0.00% 8.33%
# Neonates 278 134
Mean # Neonates 23.167 11.167
Standard Deviation 3.353 2.552
Coefficient of Variation 14.473%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 0.92
Success is: survival
Critical b value = 8
11 > 8
b = 11
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 C 14-9.1667 13 C 24 0.8333
2 E 4-7.1667 14 C 24 0.8333
3 C 21-2.1667 15 E 12 0.8333
4 E 9-2.1667 16 E 12 0.8333
5 C 23-0.1667 17 E 12 0.8333
6 C 23-0.1667 18 C 25 1.8333
7 C 23-0.1667 19 E 13 1.8333
8 C 23-0.1667 20 E 13 1.8333
9 E 11-0.1667 21 E 13 1.8333
10 E 11-0.1667 22 E 13 1.8333
11 E 11-0.1667 23 C 27 3.8333
12 C 24 0.8333 24 C 27 3.8333

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 3.8333 -9.1667 0.4493 13.0000
2 3.8333 -7.1667 0.3098 11.0000
3 1.8333 -2.1667 0.2554 4.0000
4 1.8333 -2.1667 0.2145 4.0000
5 1.8333 -0.1667 0.1807 2.0000
6 1.8333 -0.1667 0.1512 2.0000
7 1.8333 -0.1667 0.1245 2.0000
8 0.8333 -0.1667 0.0997 1.0000
9 0.8333 -0.1667 0.0764 1.0000
10 0.8333 -0.1667 0.0539 1.0000
11 0.8333 -0.1667 0.0321 1.0000
12 0.8333 0.8333 0.0107 0.0000
1
W = X 151.3687
195.3333
Calculated W = 0.775 Critical W = 0.884
0.775 < 0.884
The reproduction data is not normally distributed
evaluated at a 99% confidence interval
Test Failed!
Wilcoxon Rank Sum Test
Rank Sum - Effluent Group(treatment): 78 Control Group: 222
Mann -Whitney U = 0.0 nl(treatment) = 12 n2(control) = 12
The critical value from TABLE A.15 (0.01 Level of T) for the above n values:
Critical T = 109
78 s 109
The Sum of the Ranks of the effluent group is less than or equal to the
significant value from the table. Therefore there is a significant
difference between the means of the effluent and control groups and the:
TEST FAILS
Chronic Test FAILS
One or both of the groups do not have an Normal Distribution

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
(61—0?�-3(
Client Information
Client:
Contact:
Address:
City:
County:
-c,.,rtin6,x9 - Mrt>e+Aln
Chnrle3 Ya,r)de n 64,r
14.-Tnl I;frAri- i d.
Mc.Y�nn
CEAA
State:
Type of Facility Generating Effluent:
NC
Zip:
WW1 •)
PO#
NPDES#: NCpO44725
Phone: (qv))R4ti- 5/R
Pipe Num er:
Sample Information
Sampling Site:
l._MAC, c6.4'
Sample Type: Grab
Sampling Time: START Date: IZ- 3-o l
END Date: 12- B 7 1
Sample Chilled (Covered with Ice): Yes
Collector's Name (Print): CA" exele.5
Collector's Signature:
✓Composite # of Containers Z
Time: 1dt�sa.� M
Time: q;45 ar,., AM PM
No
VGAnA b cc
Toxicity Test Information
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute:
IWC:
Toxicity Test Concentration(s): 2.6076
List Any Special Requirements:
Pimephales promelas:
Mysidopsis bahia:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sa ple Temper re
):
Date: 12-4_07 Time: !pp PM
Date: 12 ,_4 ( Time: 1 00 P
Date: 1,7). vl--o1 Time: la •,'1.I7AM
Date: ta•1 -dm Time: )):V—AM4la
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Sample Temperature (C°):
Date: Time: AM PM
Sample Condition:

713 L
Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility LVf
Laboratory Performing Test
x
Signature of O.R.C.
NPDES#: NC (20 N 4 7 25 Pipe# pal County 5c_cif/4 ✓t d
IN\ cist �j1 �n r_ Comments 1/4d/on In.+
# 637 ; 673 8', 63q
/r) -►-�i $ j
x
/ i'
Signature of Lab Supervis
Sample Information
Collection Start Date
Grab
Composite
(Duration)
Hardness(mg/I
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receip
Control
Effluent%
0.(0-5-
Effluent%
1,3
Effluent%
Effluent%
Effluent%
/o. y
# Young
Adult
(L)ive (D)ead
n'-l2 dr
# Young
Adult
(L)ive (D)ead
# Young
Adult
(L)ive (D)ead
< o.1
/,
1
1?
L
6,)
Test
Information'
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
I Start
Start Date End Date Start Time End Time
/� 40 1 /VOX U
li /01:/l9 AlRenew
Renewl
Renew2
Start
Renewl
8, Q3
gs
Organism#
2 3 4 5 6 7 8 9 10 11 12
-w
L
zl
L
L
1 2 3 4
L
1 2
l.�
1
L
21
L
26
L
o
io,y
%qo
7.q Lt
7193
7.71
25:3
7-z-To
Moan
18.$
5 6 7 8 9 10 11 12 Moan
� Iril�l��io
�I
L
L-L
3 4 5
5-
9
6 7
Z
L
5
L
5
L_
/0
L
/0
8 9 10
3
,17
3
Mean
# Young
6
to
-*
�j
g
u
.z,
7
a
y
1 u
S
Mean
j.
Adult
(L)ive (D)ead
0
L
L
L_
L.
i__
J
L"%Red
# Young
`
g
"
3
.t
/
:)
3
D
)
/
I
ti
oZ
9
(a
10
R
Mean
Adult
(L)ive (D)ead
L
I!
L
L
L L_D
L
D
L%
9 10 Mean
a
/6.
7.9S
7g3
730
Control
7.q I
7 %7
7,A9
Control
7,q1
.7so
z�0
Control
798
7 ci
7.CSA
77 5"
20
Chronic Test Results
Final Control Mortality %
% Control 3rd Brood
Control Repro CV
O
0/0
/9,1
48 Hour Mortality
Control IWC
I_j of )oI
Significant?
Final Mortality
0
I %I
I-0ofjQl
Reproduction Analysis: L
Repro. LOEC=O45%; NOEC=_012,0 %
Method:
Normal Distrib?FPS Methodtatavxroyd
Statistic:a 5 g Critical: f. 'S'
Equal Variances? _D_ Method.11
Statistic:. Cf_ Critical:J,L_
Non -Parametric Analysis (if applicable :
JK��
Effluent % Rank um Critical Sum
.s757Q 7s
55,v 75.
# Young
Adult
(L)ive (D)ead
)
L
1
L
0
3
L
L
3
2
L
% Red
L 93.
Overall Analysis:
Result = PASS/FAIL r 0'6
S
Test LOEC= %; NOEC= %
Chronic Value=_<..O4 4 %
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
t% Reduction from Control Roproducllon Moan
DWQ form AT-3 (8/91) Rev. 11/95

ER® T E 0E'I I f4JC
ENVIRONMENTAL LABORATORIES
R Uivisiwi r>/ VWir•-r Ti.•chr, o/c, v and G.n Crc Is, /na
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
NPDES #: MC CO Li y 72
Collection Start Date
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine(mg/I)
Temperature (°C)
100% pH
1st Sample
2nd Sample
t �y
%/i%%!
'r' i ;G.G'� / r-
Cf23,10
C 7. ,;;
r c5 t1cJ
t%%O
<d;r
Lc,/
L2
,
7,59
ii9?,
Incubator*:
Temp. of Stock: 2.5- °C
Randomization: No
Dilution Water: Lake Reidsville
Batch #
Transfer
Day
Hardness
(mg/L CaCO3)
Conductivity
(umhos/cm)
637
0
W6
I67
63'6
2
Li
i68'
(�- 1-
5
1_-1 r
7l-
i cl
I /
Sample D.O. Adjustment:
Stirred Aerated None'',
Neonates:
Tray #: 5
Transfer Date/Time: / - " fJ S / 4 M
Born Date/Time: -
Age at Start of Test: hours
Test Start, Renewal, and End Dates / Times: Test Transferred by:
Start Date: 14/hi Time: j Start: /PP--
1st Renewal Date: la( Time: T:35 Day 2: !/'r""
1
2nd Renewal Date: /air Time: �' �( %fix, Day 5: �'; ��—
End Date: rhAS Time: / L ID \ Terminated: 1"e-
I
Test Fed By:
Start:
Day 1: t}yi
Day 2: Day 3:
Day 4: N1,11,L,
Day5: Ili L.
Day 6: Ay.
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Start
End
Start
End
Start
End
pH
Control
$ Ipti
71Q i
�• S�'
7,9i(
7, y�
7 a 1
High Conc.
I 0-3
s I O7
-%q 0
7,7 /
791�
d
7,rol
-J,iC
D.O.
Control
•7 .57
-2. -9
7,SD
7.CoZr
7,SZ
High Conc.
7p,5"
7,sy
-2,63
/,7%I
1,05
7,S0
Temp.
Control
2.5,0
zsio
ZS,'�I
. CD
ZS^ 0
Z5•°
High Conc.
//'
Z7•r%
ZS�L
% Y 3
Z✓rJ
�: 0
� 5,0
✓ LJ
5 L

Client: L_.t41 J C_
control
NPDES #: NC CX >-I 4 ? le-5-
Day #
2
5
7
Total
2
Ci. (v.5 % 5
7
Total
2
).3 % 5
7
Total
7
Total
2
% 5
7
Total
2
/0' % 5
7
Total
IVIerutech, Inc.
Ceriodaphnia dubia Chronic Multidilutional Reproduction
Start: Date: (( (O5
End Date: r' (D 10 5
Start Time: V1-.00.711./
End Time: 11.1 \u Qf
Analyst(s): i"{1- M..) ri1E Reviewed by:
Replicates
2 3 4 5 6
7
8
9
10
O
O
0
.O
a
'0
0
0
o
l0i
./
/9
9- 49
!,
7 /7-
6/9
7 o
1
` &
G= g-
1
2/
9
/ er
/q
l
0
O
0
0
0
6
cO
O.
O
v
y
9�7
`i
3
.-7
g
q.
/6
1
) r
7-
2
/0
b
/0
o
o
o
a
O
O
O
o
o
c,
1
3
`I
Li
1
y
3
3
3 :)
v
1
A
6--Ai
sr-
3
-2
6 j)
--
—
/,'?
`i
`-
3.0
3 :D
`/
,S---
3"
O
o
O
O
O:
0
O
co
o
p
o�
3
/
o
4
3
/
g-
3
/
L7
b:
E
6
3
.3
.5-
2
1
5
0
p
0
Q
O
O
p
o
o
,o
o
O
3
0
0
0
O
d
0
v
I
D
3
3
l
1)-2j
49 D
.),
l
2
'A
ti
1
I
I D
O 7D,
o
o
o
o
O
O
O
0
0
a
O
D
o
v
0
0
0
O
0
C3
!
p
6i
3
b D
ti
3D
2
l
i
/
)
0 7=
v
f
.3')
/
1
% 3rd Brood
io
C.V.
% RED.
A neAri
% RED.
I Ded
% RED.
1
% RED.
%RED.
1
Mean
Reproduction
� .? 1
7
3.9
7 9 . ?�

IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client:
Contact:
Address:
City:
L
C erf(e.s enl rq ,
t W1 A�{per+ d
County: S ar.. State: NL
Type of Facility Generating Effluent:
/3 L
PO #
NPDES #: Ne_pO 44725
Phone: NO 3 ig -g 2g 2_
Pipe Number:
Zip: 2-126Lt
Sample Information
Sample Type: Grab •t/ Composite
Sampling Time: START Date: ;,: up �„os Time:
# of Container Z
ID: 4D cirr,
END Date: ev • l-g.o8 Time: to ; l 50.,M
Sample Chilled (Covered with Ice): Yes No
Collector's Name (Print): r10_4 rwienber
Collector's Signature: g
Toxicity Test Information
Test Required: Chronic: ✓ Test Organism: Ceriodaphnia Dubia:
Acute: Pimephales promelas:
Mysidopsis bahia:
Ntu t4- e. c,► lv o n 5
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
Sam le Temper tune (C"):
Date: 1 _ g - og Time: 1 •
Date: —o Time: //: D0"
Date: 1 _ Y - Time: ( ‘M
Date: t
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
6
Sample Receiving (Laboratory Use On1y)RLG'd ' i ---J /— 7-0
Rehr, 55— /— r o 7
Received From:
Received By:
Sample Temp
ure (C'): /o a
Date: 1
Sample
G <r Time: M 7 S (
on• ition: Jc Cr-(
g ►�
PM
3 :So th
7 .: ov Pvr

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
(336) 3424748
Client Information
Client: LMq L PO#
Contact: �1»r1 e S \rar► e.eq
Address: 16,1e, q;rp(A- .
City: i�1a x.t.vn
County: State: NC,
NPDES #: 2c
Phone:
Pipe Number:
Zip: 2S ,4
Type of Facility Generating Effluent: J w T?
Sample Information
Sampling Site: LµRC- ¢ 'tP
Sample Type: Grab Composite # of Containers 2
Sampling Time: START Date: 1.0 _oy Time: q. sS .
END Date: i _St -off Time: c ;yo
Sample Chilled (Covered with Ice): Yes Y No
Collector's Name (Print): -A2s ‘kw‘AA,,,69,,r5
Collector's Signature:
PM
PM
Toxicity Test Information
Test Required: Chronic:
Acute:
Test Organism: Ceriodaphnia Dgbia:
Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
le `O\ 4-Dins
Shipping Information
Relinquished By: ;, ,, --,'
Received By: 411;�,,,,�
Relinquished Bye‘_ A_M,�
Received By: `r, ii.
Samp;e Temperaturp (C°):
1)4
Date: k Time: j(:0 PM
Date: 1-.4 _ Time: /l . 0 e A PM
Date: - !I -° Time: 1II pM
Date: I-!l"" Time: ii'.s-o lPM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)Re
y�
Received From:
Received By:
Sample Temperaturei{C°): j (} //0
'/
Date: / Z�Y Time:
Sample Condition: . /Ce
PM
3 ; 331'h
6:3af/L1

Title: LMAC
File:
lmac
Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
ID =
D* =
0.1244
0.9759
(p-value = 0.0218)
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data PASS normality test (alpha = 0.01). Continue analysis.

II
Title: LMAC
File:
lmac
Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 18.7975 (p-value = 0.0021)
Data FAIL B1 homogeneity test at 0.01 level. Try another transformation.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)

Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX MEAN
1 control 10 9.0000 21.0000 18.8000
2 0.65 10 7.0000 16.0000 9.7000
3 1.3 10 2.0000 13.0000 5.6000
4 2.6 10 0.0000 8.0000 3.9000
5 5.2 10 0.0000 3.0000 1.5000
6 10.4 10 0.0000 3.0000 1.2000
Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE SD SEM• C:V. %
1 control 12.8444 3.5839 1.1333 19.0634
2 0.65 6.4556 2.5408 0.8035 26.1936
3 1.3 10.9333 3.3066 1.0456 59.0457
4 2.6 5.6556 2.3781 0.7520 60.9780
5 5.2 1.1667 1.0801 0.3416 72.0082
6 10.4 1.2889 1.1353 0.3590 94.6077

,Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05
1 control 18.8000
2 0.65 9.7000 60.50 75.00 10.00 *
3 1.3 5.6000 56.50 75.00 10.00 *
4 2.6 3.9000 55.00 75.00 10.00 *
5 5.2 1.5000 55.00 75.00 10.00 *
6 10.4 1.2000 55.00 75.00 10.00 *
Critical values are 1 tailed ( k = 5 )

Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
.65 10 0 10
TOTAL 20 0 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 10.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
1.3 8 2 10
TOTAL 18 2 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 8.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL
10 0 10
2.6 9 1 10

TOTAL
19 1 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 9.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
IDENTIFICATION
NUMBER OF
ALIVE
DEAD TOTAL ANIMALS
CONTROL 10 0 10
5.2 8 2 10
TOTAL 18 2 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 8.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
10.4 7 3 10
-1
TOTAL 17 3 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 7.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Summary of Fisher's Exact Tests

NUMBER NUMBER SIG
, GROUP IDENTIFICATION EXPOSED DEAD 0.05
CONTROL 10 0
1 .65 10 0
2 1.3 10 2
3 2.6 10 1
4 5.2 10 2
5 10.4 10 3
1
1
)

L��p•C� F-�-C'
Collector's Name (Print): L- -- •,1 E
Collector's Signature: U.c„..t.P, \J,,
Toxicity Test Information
Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: t (I.
L
Contact: ,� 1 �. Vr: L.-1; ? cxr
Address: IL,1 c I 4 ; , o ? 4- 9.,1.
City: M
County: State: Nc ; Zip: 2S f 4
Type of Facility Generating Effluent: W w T
PO#
NPDES #: kic.004-9-125
Phone:
Pipe Number:
Sample Information
Sampling Site:
Sample Type: Grab ✓ Composite.
Sampling Time: START Date: 1- is - c:s1 Time: 9' SS
END Date: ti--og Time: 9'.HO
Sample Chilled (Covered with Ice): Yes Y No
VonA6e,r)
t_
T..)
Test Required: Chronic: V Test Organism: Ceriodaphnia Dlibia: t�
Acute: Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
;fly 1 \j rT.) �n s
# of Containers 2
PM
PM
Shipping Information
Relinquished By:
Received By:
Relinquished By c.
Received By:
Sample Temperature (C°):
Date: 1- 1 - o . Time: r f : bd AM PM
Date: 1-11 -a4 Time: //: - ° AM PM
Date: ' ' ' Time: ' • : AM PM
Date: Time: • AM PM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
Sample Temperature (C°): /
Date: Time:
Sample Condition:
AM PM

,
-,3L
Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility L.W\pt-C_
Laboratory Performing Test
x C rkaLA Vf'llnt12 ,Al
Signature of O.R.C.
NPDES#: NC OO 4 q -7 is" Pipe# 00 ( County Scotia •ttc/
ANA e e ,*P 6,1 . I'vtc •
X
Signature of Lab Supervisor
Comments
Sample Information
Sample 1
Sample 2
Control
Collection Start Date
Grab
Composite
(Duration)
Hardness(mg/I�
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receipt
2_4_oe
2-r1_ a
,.. .`.1
tr
�-
L .._ .. _ 1
2 9
-Mv: r I
._
2� 2
r .
k ai
0
B 52
2580
183
40.1
<0.1
E.'i
d .0 °c
0.8 °c
u
Control
Effluent%
O. (05
Effluent%
I.3
Test
Information'
Start Date
2//68
End Date
2//3/08
Start Time
End Time
9 :3cArn
Start
Renewl
Renew2
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
ot
io.4%
Start
Renewl
Renew2
Control
Control
Control
e,12,
0.18
�]rll0
8 13
B.18
g.G2�
'1,99
rr. 84
'1.32
'1.88
'7. '75
8, 05
7.83
7.25
r1.4A
�7.56,
Qin
q. 5o
24.9
24.g
24.9
2�.
24.8
24,9
26.0
25.0
25.0
25.0
25.0
25.0
Organism#
4 5 6 7 8 9 10 11 12 Mean
# Young
20
25
2,1
2r-i
2,4
25
23
2'-I
21
24
!�1
Adult
(L)ive (D)ead
L
L
L
L
L.
L-
L
L
L
hrn 3
,:.��i
1
2
3
4 5 6 7 8 9 10 11 12 Mean
Chronic Test Results
Final Control Mortality °n
% Control 3rd Brood
Control Repro CV
J
J o0
# Young
4
II
I0
S
5
19
13
to
`7
48 Hour Mortality
Control IWC
0of10_
Significant?
_.Q_of
©i p
Adult
(L)ive (D)ead
# Young
Adult
(L)ive (D)ead
1J LLLLLLL
1 2 3 4 5 6 7 8 9 10
i
14
L
14
3.
L
3
L
3
L
4
4
1
Mean
Mean
Effluent%
# Young
1i
4
3
14
1
3
3
3
4
3
_
. (o
l
Adu(Dt)ead
(L)ive
`D
L
-h%
1^
b
L
L
L
L_
Mean
Effluent%
# Young
4
I
0
0
3
3
3
0
0
i
51 Z•
l
(L)iveAdu(Dt)ead
I
/
I
b
L
I
D
D
T.
._V
Ir
Effluent%
/04y
1
2
3
4 5 6 7 8 9 10 Mean
% Red
5.9
F
/
3 %
5
ty Significant @
r
No Conc.
Reproduction Analysis:
Repro. LOEC=O. /°; NOEC=‘k
Method:
Normal Dist/rib? Method: ) 4 f'
Statistic:) • Critical: _;_t)
Equal Variances?ga_ Methost -H
Critical: R..3 —
Non -Par etric Anal sis (if applicable):
Method: `)
Effluent % Rank Sufn Critical Sum
# Young
D
0
0
0
0
0
0
0
0
Adult
(L)ive (D)ead
1
3
Overall Analysis:
Result = PASS/FAA, or «6�
Test LOEC= D, /.; NOEc=_ /o
Chronic Value=_<ab %
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
tx Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95

_l
11/1 ER/ TI'cy, /Nc_ ENVIRONMENTAL LABORATORIES
R Oivislon q/ W.arrr ry.chno/cagY and Ccantru/s, rnc.
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sh
Test Effluent Information: eet
Client:
NPDES
Collection Start Date
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine (mg/I)
Temperature (°C)
100%pHI
Incubator #:
Temp. of Stock: 2q,
Randomization:
Test Start, Renewal, and End Dates / Times:
Start Date: 2 6.p8_ Time:lj
1st Renewal Date: 2,- . _Q8
2nd Renewal Date: 2- J I-0B
End Date: 2 S
Chemical and Physical Determinations:
Control
�'•3�
Time: $' L/b
Hardness
(mg/L CaCO3)
Neonates:
Tray #: _
Transfer Date/Time: 2_� g
Born Date/Time:
Age at Start of Test: Pt ST hours
Test Transferred by:
Start: mi
Test Fed By:
Start: /211*
Day 1:
Day 2: 731
Day 3: mg.
Day 4:
Day 5: t_
Day 6:
2nd Renewal

n
11
I
Client Information
Client: L
Contact:
Address:
City:
County:
Meritech, Inc.
Bioassay Sample Chain of
642 Tamco Rd Custody
Reidsville, NC 27320
[phone]
State:
Type of Facility Generating Effluent:
Sample Information
Sampling Site:
Sample Type:
Sampling Time:
PO#
NPDES #: •
Phone: low ,
Pipe Number:
Zip:
Grab
Date., 2 Composite # of Containers
Date: Time: td: 0 5
Sample Chilled (Covered with Ice : 2� ��¢ Time: to
Time:
Collector's Name (Print): )Yes No
Collector's Signature:
Toxicity Test Information
Test Required: Chronic:
Acute:
START
END
IWC:
Toxicity Test Concentration(s):
List Any Special Requirements:
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
:i S ��., Sampl Temperature
Sample Receiving (Laboratory Use Only)
S' .' Received Frnn,• /I/I.a_ .. r.
Test Organism: Ceriodaphnia Dubia: t
Pimephales promelas:
Mysidopsis bahia:
ate:
ate: Time: AM
ate: T a Time:
C-�ti� Date: i Time: �.( ANj
)' Method of Shipment: ETC /u �PS AM
! ^e—IG Circle One (p )UPS Fed -Ex
Other:
2
PM
PM
PM

Title: LMAC
File: lmac Transform:
Kolmogorov Test for Normality
NO TRANSFORMATION
D =
D* =
0.1594
1.1448
(p-value = 0.0028)
Critical D* = 1.035 (alpha = 0.01 , N = 50)
= 0.895 (alpha = 0.05 , N = 50)
Data FAIL normality test (alpha = 0.01). Try another transformation.
Warning
- The first three homogeneity tests are
o non -normality
and should not be performed with this data lasvis.

Title: LMAC,
File: lmac Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 31.5772 (p-value = 0.0000)
Data FAIL B1 homogeneity test at 0.01 level. Try another transformation.
Critical B = 13.2767 (alpha = 0.01, df = 4)
= 9.4877 (alpha = 0.05, df = 4)

I
1
3
Client: L WIh
NPDES
>ntrol
Day #
2
5
Total
% 5
7
Total
5
7
Total
n� I3-e Sr
2
5
7
Total
Cerioda
hnia dubia Chronic Multidilutional Re roduction
Start Date: " O
End Date: a_ 3 - o
Analyst(s):
Re !icates
5 6
10
Sr/L1111161111WAIIIMINVAIIIMI
UMW 11121111M1
o
Start Time: D', IC2 /Arn
End Time: (�
Reviewed by:
5
7
Total
5
7
Total
% 3rd Brood
C.V.
3
% RED.
% RED.
Mean
Reproduction

__ J
Client:
Contact Person:
Address:
City:
County:
Sample Site:
Sample Type:
Sampling Time:
Bloassa Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax:[phone]
Email: txmrtechCo�bellsouth net Web Site: www.meritech-Iabs.com
CLIENT INFORMATION
MERITECH, INC.
Sample ID #:
PO#:
-70 j J NPDES#: NCOo441z
Phone:_‘110l 318 - 2 8
Pipe #:
State:JG
❑ Grab
. Composite
SAMPLE INFORMATION
—► CHRONIC TESTS MUST BE
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICTAKEN AFTER E T. o O
Collector's•Name: Print: �s
Test Required:
Comments:
Relinquished by:
Received by:
Relinquished by:
Received by:
Start Date: _� _ i O
End Date:.,g•
Chronic (7 days)
0 Acute (24-48 hours)
IWC: %
8-Or Ps,
Method of Shipment: ❑ UPS 0 Fed EXFi97,
r� Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ••
itech Pick-up
—0 a' .5; Li _5-
# of containers:__
Start Time: _g_Lk _ CO PM
End Time:-g=a_ PM
Signature:
TOXICITY TEST INFORMATION
Test Organism: LY Cerioda hnia dubia
p (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
SHIPPING INFORMATION
Date:
Date:
Time: /t' : O PM
Time: % Q a PM
Time:
Time: / , i T— AM1
Date:
Date: 3-- b "Oa—
. a- '--0/ h a : io PA,
Sample Temperature (°Cf_
SAMPLE RECEIVING
,elinquished
Laboratory Use On!

Meritech, Inc.
Bioassay Sample Chain of Custody
642 Tamco Rd
Reidsville, NC 27320
[phone]
Client Information
Client: i.,µflc.
Contact: G,,,l fis Va„ dih1{-
Address: 1 &,-►p t Al era
City: Netx-},n r�
County: Scoi-6144, State: Mc,
Type of Facility Generating Effluent:
PO#
NPDES #:Gpoyy-1ZS
Phone: 010 sZC?y
Pipe Number:
Zip: 2'3644
wW-rP
Sample Information
Sampling Site: LMAG e_Alc
Sample Type: Grab ✓ Composite
# of Containers 2
Sampling Time: START Date:. 2_4-01/ Time: lb: p s PM
END Date: 2- S,pg Time: [O:On (1& PM
Sample Chilled (Covered with Ice): Yes ✓ No
Collector's Name (Print):CANe,ri niorAl
Collector's Signature:
Toxicity Test Information
Test Required: Chronic:
Acute:
Test Organism: Ceriodaphnia Dubia:
Pimephales promelas:
Mysidopsis bahia:
IWC:
Toxicity Test Concentration(s): tzgr,
List Any Special Requirements: Moy. v4-:ons �1
Shipping Information
Relinquished By:
Received By:
Relinquished By:
Received By:
dimmimmin
Sample Temperature C ):
r art I Lec.t
Sample Receiving (Laboratory Use Only)
Received From:
Received By:
ate: z."S _p$ Time:
ate: S d' Time:
ate: y Time:
Date: � . S ^o Y Time: ► ): a AM
Method of Shipment: WTC(p/u) UPS Fed -Ex
Circle One Other:
Date:
Time: AM PM
Sample Temperature (C°): / Sample Condition:

Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX MEAN
1 control 10 20.0000 25.0000 23.1000
2 0.65 10 4.0000 19.0000 9.5000
3 1.3 10 3.0000 6.0000 3.9000
4 2.6 10 1.0000 4.0000 3.2000
5 5.2 10 0.0000 4.0000 1.2000
Title: LMAC
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE SD SEM C.V.
1 control 3.2111 1.7920 0.5667 7.7574
2 0.65 18.5000 4.3012 1.3601 45.2754
3 1.3 0.7667 0.8756 0.2769 22.4512
4 2.6 0.8444 0.9189 0.2906 28.7168
5 5.2 2.4000 1.5492 0.4899 129.0994

Title: LMAC
File:
lmac
Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05
1 control 23.1000
2 0.65 9.5000 55.00 76.00 10.00 *
3 1.3 3.9000 55.00 76.00 10.00 *
4 2.6 3.2000 55.00 76.00 10.00 *
5 5.2 1.2000 55.00 76.00 10.00 *
Critical values are 1 tailed ( k = 4 )

Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE
CONTROL
DEAD
TOTAL ANIMALS
10 0 10
.65 9
1 10
TOTAL 19
1 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 9.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
IDENTIFICATION
NUMBER OF
ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
1.3 6 4 10
TOTAL 16 4 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 6.
Since b is less than or equal to 6.0 there is a significant difference
between CONTROL and TREATMENT at the 0.05 level.
1 Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL
10 0 10
2.6 7 3 10

TOTAL
17 3 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 7.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
IDENTIFICATION
NUMBER OF
ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
5.2 3 7 10
TOTAL 13 7 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 3.
Since b is less than or equal to 6.0 there is a significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
IDENTIFICATION
NUMBER OF
ALIVE
DEAD TOTAL ANIMALS
CONTROL 10 0 10
10.4 1 9 10
TOTAL 11 9 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 1.
Since b is less than or equal to 6.0 there is a significant difference
between CONTROL and TREATMENT at the 0.05 level.
Summary of Fisher's Exact Tests
NUMBER
NUMBER SIG

GROUP IDENTIFICATION EXPOSED DEAD 0.05
CONTROL 10 0
1 .65 10 1
2 1.3 10 4
3 2.6 10 3
4 5.2 10 7
5 10.4 10 9

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/12/08
Facility: LMAC
Laboratory Perf •, mL"i c st: MEECH, INC
NPDES#: NC0044725 Pipe#: 001 County: SCOTLAND
ignature • 4)perator RespoFisible Charge
Signature of Laboratory Supervisor
Comments: Dilution Water Batch
#649, 650 & 651 Used
- Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
- CONTROL ORGANISMS
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
15
17
22
25
23
20
16
18
21
16
20
25
Adult (L) ive (D) ead
- Effluent %: 2.6%
;TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
14
9
10
8
15
15
3
9
16
11
16
11
Adult (L)ive (D)ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = 42.44
% Mortality
Avg.Reprod.
0.00
Control
19.83
Control
41.67
Treatment 2
11.42
Treatment
2
Control CV
17.576%
% control orgs
producing 3rd
brood
81.3%
PASS FAI
Check One
pH
Control
- Treatment 2
D.O.
Control
Treatment 2
1st sample 1st sample 2nd sample
8.03
7.99
8.03
8.05
s
t
a
r
t
1st
8.10
7.94
8.06
7.95
s
e t
n a
d r
t
sample 1st
7.60
7.35
7.72
7.47
8.09
7.98
8.11
8.17
s
e t e
n a n
d r d
t
sample 2nd sample
7.66
7.47
7.77
7.37
7.68
7.40
7.80
7.69
LC50/Acute Toxicity Test
1
-!(Mortality expressed as %, combining replicates
-1
Complete This For Either Test
Test Start Date: 03/05/08
Collection (Start) Date
Sample 1: 03/03/08 Sample 2: 03/06/08
Sample Type/Duration
Sample 1
Sample 2
Sample
Grab
Comp.
Duration
25.5 hrs
24.0 hrs
D
I
L
U
T
2nd
1st P/F
S
A
M
P
S
A
M
P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
temp. at receipt(°C)
48
188
1608
2570
<0.1
<0.1
0.7
1.6
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
r'.,n
pH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
•
D.O.

Meritech, Inc. T3 L
Mini Chronic Pass/Fail Test: Ceriodaphnia dubia
client: L f r l/ Pipe*: OO( County: .S ct/a n
VPDES #: NC 0 y i-/ ?2.5"-- Date / Time of Culture Transfer:
Date Start:
Time Start:
Dilution Water: Lake Reidsville Date /Time Neonates born: 3- -OS- 121st Renewal Date: 3 7 /p
rest Organism Source: Tray # 1 Age of Neonates at Test Start: . S hours
I� Culture Tray Temp: Z�{q 2nd Renewal Date:
Stirred / Aerated for D.O.: Y / Randomize °C
Control Organism Reproduction
Day #2
# Young Produced
Adults Live / Dead
Day #5
# Young Produced
Adults Live / Dead
1 2 3 4 5 6 7 8 9 10 11 12
0
O
O
L
0
L
0
L
O
O
L
0
L
O
L
O
L
Day #7
# Young Produced
Adults Live / Dead
1.
1
Gj
2
go-
3
$%B
L
L,
5 6 7 8 9 10 11
LIA tilto j/k
L_
/7
L--
L
3/7
L.
2 3 4 5 6 7 8 9 10 11 12
L
L
l--
1I
1D
L_
7
L^
1-2
j1
Co
L
w
L.
/1
L
Total Produced
10-17
ash 23
Test Sample Organism Reproduction
Effluent %: Z . („
Day #2
# Young Produced
Adults Live / Dead
Day #5
# Young Produced
Adults Live / Dead
Day #7
# Young Produced
Adults Live / Dead
1
L
a0
Ib
)'' I a )
20
Percent of Control producing third brood: (8713 0/0
2 3 4 5 6 7 8 9 10 11 12
O
L
0
L
0
0
L
0
L
O
L^
0
L
0
L
0
L
0
1
1
5
L
1L!
Total Produced 5
/riz 3
lents:
2
L_
3
L_
4
q
Lr
L//5-4--
L.
7
3
8 a
L
2/3
10 11 12
11/y
1/�
Lr
2 3 4 5 6 7 8 9 10 11 12
L.-
0
ll
D
do
17
6
L_
T)
)53
L_
9
6
H.0
11
L_
/�
L
11
Analyst(s): M L/M e�
Incubator #: 1
Date End: 3//.2_/c2 3
Time End:
Time:
Time:
Reviewed by: yy�
Collection (Start) Dates:
Sample 1: 3 /3/03 Sample 2: 3f (o /0 8
Sample Information
100% pH
G / C?
Duration
Sample 1
8, 02_
C-
'2,55 hours
Sample 2
8, 21
C.
Z hours
Batch #
% Li
`�
6✓J
Sample
Sample
Transfer Day
0
2
5
;.r, ...9"'
.»"•fi.r'_`,,"tt'��°..
Hardness
(mg/L)
Wei�
e
q(0
�
4 , .:
.
(pea Cond.
umhos/cm
)
I $o
I$6
f ��
1b68
25e
Chlorine
(mg/L)
yy•
';;'vdx�''�,:i
ii tj<5;
''• .1
:`:r:a
e;
a.�t-ij
���tb�c
' i
.40.'
Receipt Sample
Temp. (°C)
��
is i",'•
�i' r�tr
i` 3>;''t
z
� .,�fr.,
'_s''4ti
0 7
Lb
1st Sample
Control
$.03
731
Sample
$,03
SOS
D.O.
1st Sample
Control
7•(D
7,35
Sample
7r'11-
7,L17
Temp. 1st Sample
Control
2L1, g
z�•o
Transferred by: Fed by:
Day 0 iiiA ismL
Day 1 fiL
Day 2 ,Mt- Y11 V
Day 3
Day 4 l `--
Day 5 %1/1/1' 65
Day 6
Terminated by: 497
1st Sample
1,91
go (0
7�f's
1st Sample
sic
7 r?7
7, 37
r
td-
3%r0
2nd Sample
go1
7,95
e�
2nd Sample
7,ND
(; go
7•(.9
1st Sample 2nd Sample
z�l,g
1,0
z�l•8
-AA

Client:
Contact Person:
Address:
City:
County:
MERITECH, INC.
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Sample ID #: O O'v 3
Email: txmrtechcbeilsouth.net Web Site: www.meritech-labs.com
CLIENT INFORMATION
Lwonnberg 410ti-h9h Air rt
14761 A :ere fi—
f
f" `a5c-6:51
Sc -t r 4 State: 1\t(
PO#:
NPDES#: NCQO H y-12,r
Phone:
Pipe #:
Zip: 2 3(
Sample Site:
LIAll G o .:
Sample Type: ❑ Grab Q/(Composite
Sampling Time: Start Date:
End Date: 3.4-6$
SAMPLE INFORMATION
# of containers:
Start Time: .&: 36 . AM PM
End Time: as•aa:,
PM
_•,. CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE "•
Collector's Name:
Print:
Test Required: Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 2.6 %
Signature:
TOXICITY TEST INFORMATION
Test Organism: CR Cerlodaphnla dubla (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysldopsis bahla (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
:
Relinquished by: C�
Received bG: J / Date: 3 - C -
SHIPPING INFORMATION
Date:
Date:
Date:
Date: 0)
Sample Temperature (°C):
3— —17f /:3o PR -I
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
Time:
Time:
Time: %a .S d
Time: /a1. 3 4
/P o°
�IiJO
Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery**
3--L/-0 R S: IO Pri
SAMPLE RECEIVING (Laboratory Use Only)
k
PM
PM
AM
AM
Time: 010 S PM
Sample Temperature C): 0 . / / 0.1 / / Sample Condition: IS e-C/
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC. Sample ID#:630ir)0
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech(@.bellsouth.net Web Site: www.meritech-Iabs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
Qur.:3301-41%4-0,n AirFAA-
I� eA `Gielenbez_nb�
11010t Airrrf- Q ,.
'v o r� 1
S CD o.r A State: Mc,
Zip:
PO#:
NPDES#: NC 0644 -1 zS
Phone:
Pipe #:
Z$364
Sample Site:
LMAr, e,PD
Sample Type: ❑ Grab cgl Composite
Sampling Time:
Start Date: 3 4e -ag
End Date:
SAMPLE INFORMATION
Start Time:
3 -1 .p$ End Time:
# of containers: 2
I CM0 AM PM
PM
CHRONIC TESTS MUST BE
TAKEN AFTER t9784)-A �". p0
•" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE `•'
Collector's Name: Print:
Signature:
Test Required: _ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 2.(0 %
TOXICITY TEST INFORMATION
Test Organism: g Cerlodaphnla dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsls bahla (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
SHIPPING INFORMATION
Date:
Date:
Date:
Date:
3
Sample Temperature (°C):
3-"7'-0�
/"/, _- - _A Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
**Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ..
�- 7 - o $
Time:
Time: `D .' r� AM
Time:
` n
Time: l ir , 3u r1
/o,"'3-- a
1(r.7c) e�n
lY
PM
PM
PM
PM
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by: R. ,(..Q.Q i\.n,5
Received by: M La, ) ft(c_e- Date: 3 �j- ()FS
Sample Temperatures (°C): I , `p / / / Sample Condition: J
Time: ) 1 AM
PM
WHITE = Laboratory copy
YELLOW = Client copy

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 03/12/08
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:SCOTLAND
Laboratory Performing Test: MERITECH, INC
Reduction: 42.44%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 7
Adult Male 0 0
Adult Dead 0 5
Adult Mortality 0.00% 41.67%
# Neonates 238 137
Mean # Neonates 19.833 11.417
Standard Deviation 3.486 3.942
Coefficient of Variation 17.576%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 0.58
Success is: survival
Critical b value = 8
7 s 8
b = 7
The test concludes that the proportion of survival is signif-
icantly different for the control and the effluent groups.
Test Failed!
Chronic Test FAILS
The survival proportions of the two groups are dissimilar

Client:
Contact Person:
Address:
City:
County:
MERITECH, INC. Sample ID#:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtechc bellsouth.net Web Site: www.meritech-labs.com
CLIENT INFORMATION
L.Avrlyd3urg -gctacitinPurrr+
Gh jrla6 V nzia"b are-
14070 I A ; ermi—
fkaxkit�
State: NC Zip:
, POW
NPDES#: NCCO y 4.725
Phone:
Pipe #:
Sample Slte: LIP*
Sample Type: El Grab [Composite
Sampling Time:
Start Date: N' -tt8
End Date: 3-4-68
SAMPLE INFORMATION.
# of containers:
Start Time: $:31) . CI PM
End Time: tokoks. PM
—i CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE ***
Collector's Name: Print: C krk. lL - -(
Signature:
Test Required: 54 Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 21) %
TOXICITY TEST INFORMATION
Test Organism: ( Ceriodaphnia dubla (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysldopsls bahla (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
SHIPPING INFORMATION
Date:
Date:
Date:
Date: �! -tT
3 -&f 4"
Sample Temperature (°C):
Time:
Time:
Time:
Time:
/Irao
1I:JP
/a :') D AM
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
•• Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery'•
AM
PM
PM
SAMPLE RECEIVING (Laboratory Use Only1
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC. Sample ID #:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone] _
Email: txmrtechAbeIlsouth.net Web Site: www.meritech-labs.com
CLIENT INFORMATION
Client: ' n r ; n'h,.. r� ~ hAr:.x i e n A t r��r r+ PO#:
Contact Person: � ,.�r� K,.< \L - . : n6 G v1) trei NPDES#: NC (:':. Li 4 -7 ;. 5
Address: I (.,.7€7; i fi i v r,^ r+ f� � .. Phone:
City:rtn(c. r Pipe #:
t- ll
County: f I--.o t • -°• vim., Al State: N C Zip: •) . 36 !
SAMPLE. INFORMATION
Sample Site:��,(j
Sample Type: ❑ Grab Composite
Sampling Time: Start Date: 3 t: - C
End Date:
# of containers:
Start Time: i (. - tr: :• 651.M) PM
1
—r CHRONIC TESTS MUST BE
TAKEN AFTER 10:00-AM
•" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE "•
r f )
End Time: /.+• f `) AM) PM
Collector's Name: Print: Signature:
Test Required: ,j2 Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 2. G` %
• TOXICITY TEST INFORMATION
Test Organism: Cerlodaphnla dubla (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysldopsls bahla (shrimp)
Test Concentrations (if multiple dilutions): ..
SHIPPING INFORMATION
Relinquished by: i ! /, t. Date: - t Time: Ajut) PM
f
Received by: • ;� i : .. _ Date: ' r_- ., Time: AM PM
Relinquished by: ' ,•..., i,,..-,,',; o_,____ Date: _ Time: AM PM
Received by: Date: Time: AM PM
Sample Temperature (°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
**Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ••
SAMPLE RECEIVING (Laboratory Use Onlyl
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

-re L
Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility L v1AC-.
Laboratory Perf
Signature O.R.C.
NPDES#: NC Oil 4`I7Z5 Pipe# 00i County SCOW(10
e'��eG�t �nr`-
Sample Information
Sample 1
Sample 2
Control
Collection Start Date'
Grab
Composite
(Duration)
Hardness(mg/1
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receip
y7 >5
.
- ' =
i__ �i
.' is d
i:
L1 1
aii 2
r"= ...
{ .. , , ,•;1
i1V y�nS'.H�r�#t fill
1a1t 0,,,,+4i 1°t�
r,�tCo`1�'f' .�!99rrI
i.n„'_{y itz. '.cr
L%
/
L
3(1,6
MIMI
C fi),)
_)r 1
°C
1.1
°C
c,
WI
...
Control
Effluent%
Effluent%
1,3
1
Organism#
Comments
Test
Information'
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
Start Date
/q�0g
Start
End Date
114/03
Renewl
Renew2
Start Time
Start
End Time
101)4
Renewl
Renew?
(°I°
L, �{
It 4
%
rail
Control
Control
Control
7qL
7,9t
7 74,
•7,9`t
7, 87
7,
796
iS-t�3
7.S1
q7
71S
7.�5
%s.�
7: y;
;7e1q
79.S
3
.2.C, 0
7..55
»l,a
1So
7b3
,ZS �
zy9
7, c3
J
,,L
S.0
,D
I5.v
2 3 4 5 6 7 8 9 10 11 12 Mean
# Young
2_ 7
r
9
sal
A
37
:\7
,r
-A,.,
Adult
(L)ive (D)ead
L.
L-
L
L
L.
L
L-
L
L
_�,
5
9 10 11 12 Mean
# Young
Adult
(L)ive (D)ead
L
L
Ic
L
iI
L
3 /1
l.,
Iq
L_
L
# Young
Adult
(L)ive (D)ead
1 2 3 4 5 6 7 8 9 10
4
L
l
L<
L_
7
L_
L
to
L--
7
L
r."3
L_
ll
L
Mean
% Red
Mean
Effluent%
# Young
I
0
-7
-7
il
7
ID
/c
t
7,2
%Redr
ILL
Z. (
Adult
(L)ive (D)ead
L-
L
L
L-
L
L-
L
L_
L
D
Mean
Effluent%
# Young
7
S
17
LI),
p
3
0
7
IS-
5. Z'
(L)ive (D)ead
L
L
D
L
D
D
L-
a)
L
La
Effluent%
7 ar `l
# Young
Adult
(L)ive (D)ead
1
a-
2 3 4 5 6 7 8 9 10 Mean
3
7
L
L
1)
1,
Lf
1
J
Chronic Test Results
Final Control Mortality %
% Control 3rd Brood
Control Repro CV
48 Hour Mortality
Control IWC
_ofJc�_
Significant?
Reproductio --
Repro. LOEC=Qb(r�-�%; NOEL=44 /e
Method:___
Normal Distrib? KS Method:(; Ica\
Statistic: Qt(1)_ Critical:
Equal Variances? j U Method ' }I,
Statistic:___ Critical:_
_CofJ_
ty Significant
No Conc.
Non -Parametric
Method:S+er'.(� J1iru.
Analysis (if applicable):
Da 2.anli-r
Effluent % Rank Sum
/r-l-
5r� _
Critical Sum
O
Z- -U --
- r-
Overall Analysis:
Result = PASS/FAIL or
Test LOEC= cujcS%; NOEC=
Chronic Value= < QS %
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
t% Reduction from Control Roproduction Moan
DWQ form AT-3 (8/91) Rev. 11/95

MER/ TECH
ENVIRONMENTAL LABORATORIES
A Oiviaior, LVairr Tr: chrrology wnr/ C'o r.[ral . /r.c.
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
Client: L_v A-C_
NPDES #: QC 1 L fZ5
Collection Start Date
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine (mg/I)
Temperature (°C)
100% pH
1st Sample
2nd Sample
`1/7 /,S
VOA'
c./aq,/
Gjzq. L
*Nob
‘octtp
zD,1
40.
' ?, (D I
g, b3
4-i-ofr
Incubator #: "4- 3
Temp. of Stock: ZS °c
Randomization:(i9No
Dilution Water: Lake Reidsville
Batch #
Transfer
Day
Hardness
(mg/L CaCO3)
Conductivity
(umhos/cm)
(055
0
yio
18 z-
(oS(o
2
46
178
Co,c7
5
Li 2_
178r
Sample D.O. Adjustment:
Stirred Aerated
Neonates:
Tray #: I
Transfer Date/Time: i- 9- 0 g/ g AM
Born Date/Time: `i"D / 1p� L%fn
Age at Start of Test: 2.1 hours
Test Start, Renewal, and End Dates / Times:
Start Date: "//Q/tiTime: /0: ODA/n
1st Renewal Date:
2nd Renewal Date: /' q !O'
y/,dc, ,
End Date:
Time: -r-3 '-
Time: 'F60 Am
Time: I0GD on
Test Transferred by:
Start:
Day 2: 14/114—
Day 5: /►1V'`
Terminated:
0
Test Fed By:
L-
Start:
Day 1:
bN II —
Day 2: /1
Day 3:
Day 4:
Day 5: /n L'
Day6: r
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Start
End
Start
End
Start
End
pH
Control
~737
• 7_9?
7-9'q
"? 45
7,6i2-
fla f
High Conc.
-,Q(D
') c1(
-2,9c/
7,07
7l%
$,03
D.O.
Control
"7, 7�
-),(03
7.k3
7, 63
-7/%'(
High Conc.
7,7 (0
7. (07
7 V
7,55
7, 8 7
_3,S3
750
Temp.
Control
Z5,0
Sc0
Zq<<I
7,5 ()
-Zgigd
2S•0
High Conc.
2.5. 0
2S.0
Z'1/.`i'
2 5 . 0
71I. g
7.--(1

Client: L1MA-C
Meritech, Inc.
Ceriodaphnia dubia Chronic Multidilutional Reproduction
Start Date: q (q l0$
NPDES#: NC 664-H7.2.-
control
Day #
2
5
7
Total
2
7
Total
2
1,3 % 5
7
Total
2
5
Total
2
7
Total
2
10 % 5
7
Total
Start Time: I0 OD ,.,,
End Date: q 1 l ioLOW End Time: 1 b : :1>
Analyst(s): / /nt-//1n1C
Replicates
1 2 3 4 5 6
Reviewed by:
8 9 10 % 3rd Brood
0
0
0
0
0
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7
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9
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9
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2
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d D
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—
4
7
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o
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-7. .
0
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30
:3
it D
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i D
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.--
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61
--
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=3
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OC )
C.V. Mean
Reproduction
% RED.
% RED.
% RED.
(0 DoA
0/0 RED.
;1 ' 1
73.1

MERITECH, INC. Sample ID #: v 9U \
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech aa..bellsouth.net Web Site: www.meritech-labs.com
id -(�IIS
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
g3ev,,-/ ik/4
ge...67/} ? d
State: 4/,,X'_, Zip:
PO#:
NPDES#: NC
Phone:
Pipe #:
836 1-
Sample Site:
Sample Type:
Sampling Time:
SAMPLE INFORMATION
❑ Grab a Composite
Start Date:
End Date:
# of containers: 2
Start Time: /e-;ed c9 PM
End Time: ye:4S' 2 PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"` SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED
Collector's Name: Print: 7-
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: %
Signature:
TH ICE "'
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnla dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsls bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
HIPPING INFORMATION
Ct- _ e.
tc.
Date:
Date:
Date: "0-
Date:
,Sample Tem erature S°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
amples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery**
Time: i, : hI ® PM
AtiT a& PM
Ito
,a•'16
Time:
Time:
Time:
/ SAMPLE RECEIVING (Laboratory Use Onlv1
Relinquished by: l> �eV `' (�
Receivedb k(
Date: 9 fq fo ' Time: 0 7� J
n
Sample Temperatures (°C): 1 , I / l • I / / Sample Condition: k r (
AM CDI
AM r
PM
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC. Sample ID#: 04 r 17
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech a(�bellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
�✓TL L'�t�f' C9'mt1 Ji/a
/(a o i �,Am7
//142x Tv-y
State:
Zip:
PO#:
NPDES#: NC
Phone:
Pipe #:
,7? 3S-
Sample Site:
Sample Type: ❑ Grab ,Composite
Sampling Time: Start Date:
End Date:
SAMPLE INFORMATION
# of containers:
Start Time: /6:00 AM PM
End Time:
/O f /vim PM
—r CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
`* SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WI _ 1
Collectors Name: Print:
Signature:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: OA
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
r
Relinquished by:
Received b
Relinquished by:
Received by:
SHIPPING INFORMATION
Date:
Date: (%_ i l
Date: ' if
Date: I/-o if
q-//-a$ 6:151'
Sample Temperature (°C):
Time: .Al ! PM
Time: / /.`, G d CNIDPM
Time: o?: 1710 AM
Time: 2: L/ o AM El
Method of Shipment: 0 UPS ❑ Fed EX ❑ Meritech Pick-up
.. Samples shipped on Friday must be FedEz and must be clearly labeled for Saturday delivery**
Relinquished by: 1� IC.e e n J
Received by:
SAMPLE RECEIVING (Laboratory Use Only)
L1-Iz-oU
Date: Time: gigs AM PM
Sample Temperatures (C): Q . Z / O. Z / / Sample Condition: LQ_
M l -tee n�-
WHITE = Laboratory copy YELLOW = Client copy

I
r-,
Client:
Contact Person:
Address:
City:
County:
MERITECH, INC. Sample ID #: 69U�
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech(a�belisouth.net Web Site: www.meritech-labs.com
CLIENT INFORMATION•
067/
State: 4/,e Zip:
PO#:
NPDES#: NC
Phone:
Pipe #:
Sample Site:
Sample Type:
Sampling Time:
SAMPLE INFORMATION
❑ Grab Composite
Start Date:
End Date:
e
vif
# of containers:
Start Time: /O•;del PM
End Time: JO:OS" PM
a
—► CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
•** SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED ITH ICE ***
Collector's Name: Print rrfZ?V,,,' Peoriici,y/2„0 Signature:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC:
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by: I!L ✓J
Received by: -L
Relinquished by:
Received by: CA, re— I e.
HIPPING INFORMATION
Date:
Date:
Date: t(-2? -E=r?
Date:
kfr
• Sam le Tem erature S°C :
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
amples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery •*
(1•K 7 3v7%1
Time:
Time:
Time:
Time:
SAMPLE RECEIVING (Laboratory Use Only)
�
Relinquished by: ��� l
Received. y� K/�� fQ/0 Date: 1 YSample Temperatures CC): 1 ,1 / k. ` / / Sample Condition: L ('C
ice) ® PM
or: i PM
t7 Lip AM CD
1�1,Li6 AM Cam'
Time: 07 JJ
PM
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC. samplelD#: v`T /1
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech4bellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
Po#:
State:
Zip:
NPDES#: NC
Phone:
Pipe #:
Sample Site:
Sample Type: ❑ Grab ,_Composite
Sampling Time: Start Date:
End Date:
SAMPLE INFORMATION
-- O Y
t- — o
# of containers:
Start Time: /c O AM PM
End Time:
/d ` /vd PM
—► CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"` SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WI •1 I
Collectors Name: Print:
Signature:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC:
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
�, SH'PING INFORMATION )
Relinquished by: pp �" Date: �/"0 b Time: Cam% A PM
Received b Date: L/- / / --Cr?Time: / i', O d AM PM
Relinquished by: Date: 1/` // -6)4- Time: o? 47/0 AM
Received by: /` Date: j'/r0 Time: . , L1 o AM Pll
Xe1,:, : "/1 _.7sample Temperature (° 6 : ! 5 Pit"'
Method of Shipment: ❑ UPS ❑ Fed EX 0 Meritech Pick-up
**Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery **
Relinquished by: 1� ILe e n J
Received by:
SAMPLE RECEIVING (Laboratory Use Only)
M La,i-o'e n c�
Date: L - 12 - 0 8
Time: ' I ; t/5
Sample Temperatures (°C): Q • Z / 0. Z / / Sample Condition:
•AM PM
WHITE = Laboratory copy YELLOW = Client copy

Title: lmac
File: LMAC Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D=
D* =
0.0793
0.6222
(p-value > 0.100)
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data PASS normality test (alpha = 0.01). Continue analysis.

In
Title: lmac
File: LMAC Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 18.8123 (p-value = 0.0021)
Data FAIL B1 homogeneity test at 0.01 level. Try another transformation.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)
T

Title: lmac
File: LMAC Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX MEAN
1 CONTROL 10 21.0000 29.0000 26.8000
2 0.65 10 8.0000 24.0000 16.2000
3 1.3 10 4.0000 16.0000 8.8000
4 2.6 10 0.0000 18.0000 7.2000
5 5.2 10 0.0000 8.0000 4.5000
6 10.4 10 1.0000 7.0000 2.8000
Title: lmac
File: LMAC Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE SD SEM C.V. %
1 CONTROL 5.2889 2.2998 0.7272 8.5812
2 0.65 40.1778 6.3386 2.0044 39.1271
3 1.3 13.7333 3.7059 1.1719 42.1119
4 2.6 27.2889 5.2239 1.6519 72.5538
5 5.2 7.3889 2.7183 0.8596 60.4056
6 10.4 3.5111 1.8738 0.5925 66.9213

Title: lmac
File: LMAC Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DP 0.05
1 CONTROL 26.8000
2 0.65 16.2000 58.50 75.00 10.00 *
3 1.3 8.8000 55.00 75.00 10.00 *
4 2.6 7.2000 55.00 75.00 10.00 *
5 5.2 4.5000 55.00 75.00 10.00 *
6 10.4 2.8000 55.00 75.00 10.00 *
Critical values are 1 tailed ( k = 5 )

MERITECH, INC. Sample ID#:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech(a�bellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
/d 7 / /7 1I/' /
State: /-f/�' Zip:
PO#:
NPDES#: NC
Phone:
Pipe #:
Sample Site: f'- !—
Sample Type: ❑ Grab
SAMPLE INFORMATION
© Composite # of containers:
Sampling Time: Start Date: Start Time: aro AM' PM
End Date: y - Y,- : ' End Time: /64,;Q...5` AM PM
—� CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
*" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE "'
Collector's Name: c2,
Print: �,. /T( q ;•; /Cf,, i� Signature: ,. • j �� , -�am
TOXICITY TEST INFORMATION
Test Required: ❑ Chronic (7 days) Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Acute (24-48 hours) ❑ Pimephales promelas (fathead minnow)
❑ Mysldopsis bahia (shrimp)
1WC: % Test Concentrations (if multiple dilutions):
Comments:
SHIPPING INFORMATION
/
l
Relinquished by: / :.�. if , 4'i . �: .. Date: f - -6/- — % Time: AM PM
Received by: \/. Date: Time: AM PM
Relinquished by: Date:
c I . % 'G Time: /`.• AM .PM
Received by: �? e• ,L j Date: I 1� Time: ' AM PM
�) 1�•, t Sample Temperature (°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
•• Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery "
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC. Sample ID it:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech bellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
/c 70/ - 4v7 f 4
State: /1/;.11
PO#:
NPDES#: NC
Phone:
Pipe #:
Zip: '37 c
SAMPLE INFORMATION
Sample Site:
Sample Type: ['Grab Composite
Sampling Time: Start Date: 4— /0 o
End Date:
Start Time:
# of containers:
/r') .<)O iD PM
End Time: /6 ` /.J c j PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
•ff SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WIT I
Collector's Name: Print: �7.Z(` y 9 /74/. Signature: J
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC:
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnla dubla (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
SHIPPING INFORMATION
Date:
Date: L/. /'
Date: ! / • /
Time:
Time:
Time:
AM PM
AM )PM
AM PM
Date: Time: AM PM
Sample Temperature (°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
•• Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery •.
SAMPLE RECEIVING (Laboratory Use OnIY)
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 05/16/08
Facility: LMAC CLARIFIER
Laborator1y Performin• Test: MERITECH, INC
Signature
-; Work Order:
NPDES#: NC
Operator in Responsible Charge
of Laboratory Supervisor
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
Pipe#:
County: SCOTLAND
Comments: Dilution Water Batch
#662 & 663 Used
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
20
21
18
22
18
16
24
23
23
17
14
19
Adult (L) ive (D) ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
5
0
1
0
7
2
2
4
3
2
0
3
Adult (L) ive (D) ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = 87.66
% Mortality
Avg.Reprod.
0.00
Control
19.58
Control
33.33
Treatment 2
2.42
Treatment
2
Control CV
15.920%
% control orgs
producing 3rd
brood
100%
PASS FAIL
Check One
pH
Control
-1 Treatment 2
D.O.
Control
Treatment 2
1st sample
8.01
7.93
8.00
7.97
s
t
a
r
t
1st sample
e
n
d
7.77
7.28
7.69
7.59
lst sample 2nd sample
7.98
7.93
8.04
7.99
s
t
a
r
t
1st
8.04
7.89
8.05
7.99
s
e t e
n a n
d r d
t
sample 2nd sample
7.64
7.52
7.72
7.43
7.74
7.16
7.72
7.28
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates
Complete This For Either Test
Test Start Date: 05/07/08
Collection (Start) Date
Sample 1: 05/05/08 Sample 2: 05/08/08
Sample Type/Duration 2nd
lst P/F
Grab Comp. Duration D
I S S
Sample 1 X 24.6 hrs L A A
U M M
Sample 2 X 25.0 hrs T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
44
167
745
1605
<0.1
<0.1
0.8
0.5
96
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 = %
95% Confidence Limits
% --
Method of Determination
Moving Average Probit
Spearman Karber - Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
('nn n
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Client: L.MA--. CGf iTter
Meritech, Inc.
Mini Chronic Pass/Fail Test: Ceriodaphnia dubia
Pipe #: County: Ovid Date Start: 5- r% 08
NPDES #: NC Date / Time of Culture Transfer: S- S
Dilution Water: Lake Reidsville Date / Time Neonates born: .S - 0
Test Organism Source: Tray # I Age of Neonates at Test Start: / q.
Stirred / Aerated for D.O.: Y /
tel Time Start: `0 : 3')4,, ,n
(0 it 1st Renewal Date: 5- - 08
hours 2nd Renewal Date: 5- /2- 03
Incubator #: 3
Date End:
Time End:
Time:
Time:
Randomized/ N Culture Tray Temp: 2-5•D °C Analyst(s): fat/ 1 ../rn E Reviewed by:
5-141-68
12:45"pi
q.,
�Oc
-1Z
Control Organism Reproduction
Day #2 1 2 3 4
5 6 7 8 9 10 11 12
# Young Produced
0
0
0
0
0
p
0
0
0
O
0
0
Adults Live / Dead
L
L-
L-
1-
1-
1,
U.
L-
L-
L.-
L-
L
Day #5
1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
T
4//7"
ii Y
Lt.
3
,--
Y-
-3
2
Adults Live / Dead
1,
L.
LIL
L
L
L
L
L
Z_
L
Dav #7
1
2
3
5
8 9 10 11 12
# Young Produced
Yg
/2
4=1 8.
S/D
7/7
6%
i&z
V/6
`�f D
y$
6/6
Adults Live / Dead
L-
L
L
L
L--
L.
L
L
L.
L.
L-
1—
TotalProduced
120
o
167.a.
/g
/6
2I
t)..
3.31l 7.1 1 L
1
Test Sample Organism Reproduction
Effluent %:
Da v #2
1
Percent of Control producing third brood: / OQ %
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
0
0
0
0
0
O
0
0
0
O
O
O
Adults Live / Dead
l.,
t-
L<
l-
)--
L
L-
L-
L-
L-
L...-
Da #5
1
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
2
0
/
0
,z
,a
9-
0.a
0
3
Adults Live / Dead
L.
.
L
L_
L
L
V
L
L
L
Da #7
# Young Produced
Adults Live / Dead
1
3
L
2 3 4 5 6 7 8 9 10 11 12
0
L_
1)
L
S.
L
L
L
17
L
Total Produced
,iments:
5-
0
1
0
7
a
3
2
6
3
Collection (Start) Dates:
Sample 1: 5-5-08
Sample Information
Sample 2: O`y
100% pH
G / C?
Duration
Sample 1
7. `i (7
G
Z i{. (D hours
Sample 2
7,8Y
C
ZS hours
Batch #
/' ^7
ICD L
"_�
�(r�
Sample
1
Sample
2
Transfer Day
0
2
5
Ha(rdnes
mg/L)
4a
1s L!
Spec. Cond.
(umhos/cm)
) /,
1 W�
'—�
t7
rms.Ii��(,'J�
Chlorine
(mg/L)
4.z,
;
..
.... _..
's0.I
L0� i
Receipt Sample
Temp. ('C)
? °',
0. 8
O,
1st Sample
Control
3..0/
.7,C1-5
Sample
',0)
7,c17
D.O.
1st Sample
Control
177
7:Z'6
Sample
7.0
I,S9
TemD.
1st Sample
7't.(
-7-'(-)Control
Sample
Transferred by: Fed by:
Day 0 flA- /nC
Day 1
Day2 VIA(1- y
Day 3
Day 4
Day 5
Day 6
Terminated by:"‹..
1st Sample
7,;3
7,9?
1st Sample
7,(04
�r�rl
�Iv
?cj3
1st Sample
2nd Sample
v'I
('fi.
7.9c1
2nd Sample
7,7`1
7,7Z
7; .
2nd Sample
1,5, 0
2 -:()
2

MERITECH, INC.
',toaster SanwIM Chain of Custody
642 Tamco Rd, Reidsvile NC 27320
Phone: [phone] Fax [phone]
Email: Web no: www.mariteth-labs.can
CLIENT INFORMATION
C8.nt Lr7,7i'
Contact Person: 1/Ap, 1�X Al1LL. ice/ !'
Address: /' 74/
Pet
County: _S'e, 2)71/,9wi stator ,�_ zip: a Pj ‘ SL
Sample LINE Clatind ,-
SAMPLE INFORMATION
Sample Type: ❑ Grab UcCamposite d of containers:
sampling Time: Start Data: ,f �= - [) Start Time: .)'d CAI�i PM
End Date: (9 ` End Time: Al) `Q S ( PM
--. CHRONIC TESTS MUST ISE
TAKEN AFTER 10:00 AM
1 "' SAMPLE CONTAINERS ARE TO BE C rEt YijtXCHILLED L (no air space), AND COHERED
Collector's Name: Print /�'X,/ )i�d,SJ/n Signature:
TOXICITY TEST INFORMATION
Test Requited: ❑ Chronlc (7 deye) Teat Organism: ❑ Cerbdaphnla deign (water flea)
0 Acute (2448 hours) ❑ Plargphelee pranwias (fathead minnow)
❑ Nysidopsls Mhla (gip)
IWC: x Teat Coeuntrs0ens (If multiple dliudons):
Comments:
POdti
NPDESt: NC
Phone:
NG INFORMA
Data: 'Ti ._. g( /J G( Time: /1. I Si)Pm
r/
Date: ,r" G- O y Time: r I, it a PM
Data: S-- (�" 2S" Time: i -? b AM llc)
[
Data 5 — o - v Time: 1'a ,1 AM RM-�
I" L.• d , Sample Temperatta+9 rc):
6—op 3=3or"
ci ; M'ethorafShipment
drawee
0 UPS ElFed EElX titerdadrh Pl-up
SAMPLE tECIP/ING IL*bomtory !!eta Only)
Relinquished by:
Received by
Relinquished by.
Received by
Relinquished by
Received by:
Sample Temperatures ('C): 1)Ti
Date:
Tom' AM PM
Sample Condition:

MERITECH, INC.
&loissatl Simla Chan of Custody
642 Mince Rd, Reidsville NC 27320
Phone: [phone] Fs>c 1-336 342-1522
Email: gagggibabgaggIUSI. Web Slice: wt w.mottec-labs.cvrn
Client
Contact Person:
Address:
County:
CLIENL INFORMATION
ion
State: /,�,._
POA
NPOESIP: NC
Phone:
Pipe S:
Semple sib:
Sample Type:
sampling Time:
SAMPLE INFORMATION
❑ Grab ta-Composite
e of containers:
Start Dale: gc) Start Time: 920 AM Pt#
End Date: ,5 9 " )) End Time: fb:02) AM PM
SAMPLE CONTAINERS ARE TV BE COAT
Cali.ctoes Naar.: Print;
1
—► CHRONIC TESTS MUST SE
TAKEN AFTER 10:00 AM
(no airspore), CHILLED AND C
Signature:
TOXICIJY TEST INFORMATION
Test Required: ❑ Chronic (7 days) Test Organism: 0 C.dodaphnia dmWa (water Rae)
❑ Acad. (24-48 hours) ❑ Pia: phd s premiums (fathead minnow)
❑ Nysldopsfr battle (shrimp)
Test Concentrations ($ multiple (Muttons):
Comments:
Relinquished by:
Received by:
Relinquished by
Received by:
Date:
Dee:
Data:
Date:
Time:
Time:
Time:
I!` °�W) PM
/ f b AAA' PM
'CI.0D AM i
,! 1. 1 G mple Temperature My
Method of Shipment 0 UPS 0 Fed EX ❑ Uard.d+ Pick-up
re.
/,;,i f / -/ ` p se Pbc134y Fdd�Y Pz 6 '.MrSb Pb Gtsarlab ly el., for words/ seaway ••
E��/ISAMPLGNO (Leabrl ofyM lite On)v)
Relinquished by
Received by:
Sample Temperatures CC): ifl • 5 I
rQ (\CL
Date: 5-4 0— O S
Time: 9, 3o Pit
Sample Condition: -1 (.Q-d

Effluent Toxicity Statistical Results - Chronic Pass/Fail
Date: 05/16/08
Facility: LMAC CLARIFIER
Laboratory Performing Test: MERITECH, INC
Reduction: 87.66%
# Replicates
Female Live
Adult Male
Adult Dead
Adult Mortality
# Neonates
Mean # Neonates
Standard Deviation
Coefficient of Variation
A = 12
NPDES#: NC
CONTROL
12
12
0
0
0.00%
235
19.583
3.118
15.920%
Fisher's Exact Test
B = 12
a/A = 1.00
Success
a = 12
b/B = 0.67
is: survival
Critical b value = 8
8 s 8
Pipe#: County:SCOTLAND
2.6% Effluent
12
8
0
4
33.33%
29
2.417
2.151
b = 8
The test concludes that the proportion of survival is signif-
icantly different for the control and the effluent groups.
Test Failed!
Chronic Test FAILS
The survival proportions of the two groups are dissimilar

Clint
Contact Person:
MERITECH, INC.
Disaster Smote Chain of Cssfodk+
642 Tamco Rd, Reidwas NC 27320
Phone: [phone] Far 1-336-342-1522
Email: QkmrtedumboflsoiM.net Web BNa: www.meetech-laba.ccrq
CLIENT INFORMATIpN
sample w r.
PM
?-1,G 4' )) fr' 1,-t , i-7.l' NPOES*: NC
Address: , / 74, � .2--- ,eve .,1 Phone
C4 ./1-14G2Fl o :
• County: se'2 /94r4/ mot.: 7-7,40' ; X Pi 6 4-
SAMPLE INFORMATION
Semple She:
Sample Type:
sampling Tin.:
a of containers: 1
PLI
—0. Mitotic TESTS MUST BE
TANEN AFTER 10:00 AM
6" SAMPLE CONTAINERS ARE TO BE CIC �1 C� (no airspace), CHILLED AND COVERED
Coltectar'. Name: Print /i7 y > G:9 �!� Signature:
❑ Grab IS\Composita
Start IDaie: � 6 fr start Time: 9_'
End Dale: 4 - Q Yj End TM.: /4
Test Required: 0 Chronic (7 days)
CI Acute (24-4a hours)
Corttrf>•i
!WC:
TOXICITY TEST INFORMATION
Taft Omani..: ❑ Cgrfpdip/n1a *bin (water flea)
❑ Plarephaies peoseel&s (fathead minnow)
0 *sidopaafa kohl& (shrimp)
96 bet Concentrations (If mukipto airtime):
PM
Relinquished by-.
Received by:
Relinquished by
Received by:
INFORM%
Date:
Del):
Date: e
Date:
Sample T.mperatkre ('C):
The:
Tints:
Time:
Method of Shipment 0 UPS ❑ Fed EX ❑ Mentedk Pick-up
eem#w ehlNped es Frrtrey JINN& be Feast cad must he Weedy le6s sd ter Sr heeay defter),
IhlS
if:(1- aPM
! 2r �•? b AM IQ
t"�•.3J AM
Relinquished by:
Received by:
Sample Temperatures ('G): 1
t3AMPL1; RECHWIN6 fLobortofy Use
I
1
Date:
Time:
AM PM
Sample Condition:

MERITECH, INC. sample in st
pioneer Santo& Chain o f Custody
842 Tenn= Rd, Reidsville NC 27320
Phone: [phone] Far 1-336-342-1522
Emelt 91131=0216111811121. Web Sk:MELLIMCksthAaiscm
Cleat
Contact Penson:
Addles*:
City:
County:
CUENT INFORMATION
Jes27-T/
cl
1140-,4"e5
Sc,97z-
Stain:
Sample $SE
Sample Type:
Sampling Tana:
,e4„4/P:A"df
0 Grab aComposits
SAMPLE INFORMATION
So( containers:
Stan Dale: R-4) (tr Shut rime: AM PM
End Deb: 9 '"D End Ttrie:1„e,C).6 AM PM
POR
NPDESO: NC
PS*
Afgle0-51—
"• SAMPLE CONTAINERS ARE PO BE CON TY (no airspace), CHILLED AND
Callectoes Name: Print •
Mgr:Mum:
Test Required: 0 Meade days)
Amity (24-48 hours)
Cantmeata:
I WC:
CHRONIC TEt3T8 MUST BE
TAKEN AFTER 10:00 AR
TOWItY TEST INFORMATION
Test Orani.m 0 CeriochpIinia dubla (water fles)
El Plasepheies protest= (fathead minnow)
0 Mysideeals halals (shrimp)
Test Caraintratiows (It maple diutons):
Rettnquehed by.
Received by:
Relinquished by:
Received by:
Date:
Deis:
Date:
Date:
1/4c-9-0 r
• .....---"Zsempis Tlimpecatize CC):
Method &Shipment 0 UPS 0 Fed EX D metal' di pick...up
••• Samples shipped an Way iamb, Fuse: Ind mob usury Imbed ser Sitenies &Aveiro
Time:
rime:
rime:
" WPM
bb a) pm
fI•Db AM 1615
Time:
Asi
Relinquished br.
Rsabrad by:
SAMPLE RIMMING (Litbamitoly L. Onhl
Sample Temperatures (4C):
I I
1
Deb:
Trims:
AM PLI
Sample Conditto:

TL
Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility L
Laboratory Perfor
Signature o O '.C.
NPDES#: NC cc-4-17zS Pipe# 00(County 5-cot/civic'
Sample Information
Sample 1
Sample 2
Control
Collection Start Date
Grab
Composite
(Duration)
Hardness(mg/I
Spec.Cond.(pmhos/cny
Chlorine(mg/I
Sample temp. at receipt
5-5-oe
5 -8-cF
L /•
� -y, i
p3
�.,
f' res. '
%
4q `tf
-1 35-
1, .5153
173
, 7 Ilq
.. C, 1
LC' . /
C Ft oc
(',.S c
.'..=
Control
Effl u e nt%
b.(cS
Effluent%
1.3
Organism#
2 3 4 5 6 7 8
Comments 1x: -tlN
(1; L' I
1 5 -te.sfi
Test
Information*
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
Start Date
•5 /7 %o
End Date
Start Time
Co
End Time
Start
Renewl
Renew2
Start
Renew
Renew2
IC,1
Control
Control
Control
7, 49
7.43
7, 99
c•.3
7,c/9
53. &(,
7,90
7.v3
7.77
-7.7C•
'7, 7/
7, LJ
7, ?V
7. (-/C
zl
72
7LL
7.5L
?Jr.:
7y•g
-Z4.
z•S:C
z.>.e
Z5:I
9 10 11 12 Mean
#Young
[?
1.)
I(,
1cl
i$
1$
-Li
IF'
IS
1.7
t7,ta
Adult
(L)ive (D)ead
t-
L-
L
L_
L
l_
L_
L
L.
...
2 3 4 5 6 7 8 9 10 11 12 Mean
Chronic Test Results
Final Control Mortality %
% Control 3rd Brood
Control Repro CV
C
ci C
q,1)
# Young
15
Iy
15
/•S
rf
16
2)
F
I CI
(k�
48 Hour Mortality
Control IWC
C; of /0
of /L
Significant?n ( h
ality Significant @
or
Adult
(L)ive (D)ead
# Young
L.
L-
1_
1_
L-
L
1 2 3 4 5 6 7 8 9 10
17
IZ
►-
N;
IS
3
Mean
NIMIIMINEW
Adult
(L)ive (D)ead
1~-
t_
L
0
L
/c. 7
% Red
Mean
Effluent%
# Young
`l
7
.c
(;
7
5-
9.
I (v
q
-2 1-
Z Z. (v
Adult
(L)ive (D)ead
L
L
L
L
1_
1 _
L
L
%Re
17,
Mean
Effluent%
# Young
q
/C
G
'L
%
0
Li
,5-
5.1
Adult
1
% Red
5". 2-(L)ive
(D)ead
l�
-
L
i%
L
t
7c.7
Effluent%
10
2 3 4 5 6 7 8 9 10 Moan
% Red
No Conc.
Reproduction Analysis:
Repro. LOEC= o.G:S %; NOEC= = 6.6 %
Method:
Normal Distrib? 1'es
Method: 4.,71,,,oce
Statistic: C 73&5 Critical: l.c:i`�
Equal Variances? n:c Method:.,
Statistic: 1,{ . N (i Critical: r 5 . c `r
Non -Parametric Analysis (if applicable):
Method: 5-1-f-8.l s f�4,� c„e }a l=
Effluent % Rank Sum Critical Sum
7Z.G '7•S.�
l.3 4-G -7fC
z • G: • 7 • ti
S. z 55-,
/D.`r .55.0 �•S.0
# Young
0
z
Adult
(L) ive (D)ead
L-
z
L.-
l�
0
It Red
41.1
Overall Analysis:
Result = PASS/FAIL or
TestLOEC= c,�s %°; NOEC= zc-e)
Chronic Value= c e . tv S %
MAIL
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mgll
Y% Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95

l
N1ER/ TECH,. /NC_
ENVIRONMENTAL LABORATORIES
A Division l./ WA frr Tirchno/ogy wnd G'onlro/i, /•,c.
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
Client: L y E 1>
NPDES #: OO L' Lf 7 ZS
Collection Start Dat
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine (mg/I)
Temperature (°C)
100% pH
1st Sample
e
2nd Sample
5 -S--O$
S-$-06
c-/zy,s
GAy, 2.
735
t,55)
7,01
8,7zz
Incubator #: i
Temp. of Stock: 25,0 °C
Randomization: �Y
No
Dilution Water: Lake Reidsville
Batch #
Transfer
Day
Hardness
(mg/L CaCO3)
Conductivity
(umhos/cm)
664
o
%
173
latoz
2
1IL
I67
67(93
5
14(0
I?I%
Sample D.O. Adjustment:
Stirred Aerated
Neonates:
Tray #: 3
Transfer Date/Time: _5-- -Off / �' 3
Born Date/Time: $ & -oe / /( - y�..
Age at Start of Test 2.2.0 hours
Test Start, Renewal, and End Dates / Times:
Start Date: Time: q co .
1 st Renewal Date: S —q -0 Time: q-S, cicA"--
2nd Renewal Date: 5--/ 2--05' Time: Q
End Date: Time: 3D/4f)
Test Transferred by:
Start: "Rd_
Day2: 114/2--
Day 5:
Terminated:
Test Fed By:
Start: /1
Day 1: 1t412-
Day 2:
Day 3: ; r
Day 4: k1Z
Day 5: N.G._
Day 6:
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Start
End
Start
End
Start
End
pH
Control
`?, T1
-2, 90
7, qg
7,93
5,0q
7,
High Conc.
7, q`f
.?',03
7, y3
7.0
8. a3
7 . uG
D.O.
.
Control
.7, ? 1
7, q 7,7
& q
---4.$-2_
7,? 4
?, l (.,
High Conc.
7. 7 -)
7, go
.7v
-)+ Z1
7-(0 `/
7.10
2_ �, U
Tem p.
Control
v./ , r
2.570
2 t-�, 3
-2 5. /
2.,0
T
High Conc.
Z ! .c-1
'1
2,5 ,0
ZLi,
2 .i. i
25 .D
_.C. 0

Meritech, Inc.
Client: LvYM-C
control
NPDES #: NC ry, 4 2 7
Day #
2
5
Total
2
O.I,S % 5
7
Total
2
t , 3 % 5
7
Total
2
.(v % 5
7
Total
2
5Z % 5
7
Total
2
(O. % 5
7
Total
Ceriodaphnia dubia Chronic Multidilutional Reproduction
Start Date: .5 - 7 - OS
End Date: 5- f/Li -06
Analyst(s): Irljt A.
Replicates
2 3 4 5 6
7
8
Start Time: ; (1)o-
End Time: $3[) G,w„
9
Reviewed by:
10
0
0
0
0
c
0
o
C
00
S�
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a-
;
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11011111
C.V. Mean
q.
Reproduction
% RED.
% RED.
% RED.
RED.
% RED.
i1.(.9
14.0
i0.
32.2-
Sg•7
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V c)� We-• % 5
< 6 v 654

MERITECH, INC. Sample0 S O7 O 9
Dfo.sswSanolt Chalet ofGrstodv to r.
642 TIImco Rd, Reidevie NC 27320
Phone: 1-336:342-4748 Far 1-336.342-1 S22
Eman: Qanriedikebetlpouth.net Web Site: www.meritech-latmcorn
Client 11/g r Poi
Contact Person: --7-z r.% ,Q: Vie/&/' NPDEsr. NC
Address:
/t ,/j / ,42T���� ��
Phone:
City .et e .-i) ✓l/ Pipe s;
' County: -7 /.eri State: 1/./ -qC1 V 1
SAMPLE INFORMATION
Sample Slip: C��
Sample Type: ❑ Gab lidomposite
ANT INFORYALTION
1 of containers:
8amprnp Them: Start Data: — y`"— !> Stott Time: R ; 3 j) PM
End Deb: JC "l2 — C7 iK bed This: /p f))) e✓ J- M
o2
-- 0 CHRONIC TESTS MIST BE
TAKEN AFTER 10:00 AM
'' SAMPLE CONTAINERS ARE T O BE COMPLETELYFtJLL. (no air spies)„ CHILLED AND COVERED ...
Coliectoes Nam.: Print��ei4 Signature:
Test Required: 0 Chronic (7 daps)
0 Acids (24-48 hours)
Relinqubahed by:
Raraived by
Relinquished bar.
Received by:
TOXIc!iY TE8T INFO ta1lr�ta
Tint Orvenisrn: 0 Cedodaphnla m,bfa- (water -flea)- - -
❑ Piosephsiss pis, (fathead minnow)
❑ NysSdopsfar Whl. (shrimp)
IWC: '16 Toot Cementations (K mtAgpb dilutions)
NG INFORM
Date:
Deis: _ Y
Date:
Date: 5--
/ - � /fir Samoa
K--6'2•mp.`aturs cr
lr /U �v� Method of BhlPmem 0 ups ,j ��
6!0 Fed EX ❑ Blamer+ Pidc-up
I� atill31264 b• F mid me be qI "wad the ..
7 O/� �Y M4'rM'
AMPLE REFrEIyINa&ftratzzawatl
inquls}aed by Aft kJ ItLe-
fv S
Sample Temperatures ('C): ©' / O rq
f
Tbrne: I L! I b 6 PM
Taw /NS AM PM
Time: I • AM a
Time: AM
6 `7� pi/
c«nCrI(ian: T

MERITECH, INC.
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech a(7bellsouth.net Web Site: www.meritech-Iabs.com
Sample ID #: 6509 q9
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
State:��- Zip:
PO#:
NPDES#: NC
Phone:
Pipe #:
Sample Site:
Sample Type: ❑ Grab
Sampling Time: Start Date:
End Date:
Composite
SAMPLE INFORMATION
# of containers: a
Start Time: 9; v) PM
End Time: /6 ; (6 AA J PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
•" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WIT
Collector's Name: Print: — - -- - _._ .. ..... _.
�i�' � � •i � Signature: ,iyji
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: %
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubla (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysldopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
E •"
Relinquished by:
Received by:
Relinquished by:
Received by:
777
SHIP
ING INFORMATION
i
Date:
Date:
Date:
Date:
Sam le Temperature (°C):
-�'-t-
5 'cr?
r -
to P/N
Method of Shipment: ❑ UPS D Fed EX ❑ Meritech Pick-up
Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ••
S--c7-01? '/S Pr'-,
Time:
Time:
Time:
Time:
,):°v PM
11: 60 ® PM
��.oLi AM
Relinquished by: R.
Received by: vl LJL) CQ.X\Q Date: _5- / 0- 08
SAMPLE RECEIVING (Laboratory Use Only)
Sample Temperatures (°C): 0. 5 / 0 5 /
Time: q: o PM
/ Sample ConditioniUS2-
WHITE = Laboratory copy YELLOW = Client copy

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D=
D* =
0.0939
0.7365
(p-value > 0.100)
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data PASS normality test (alpha = 0.01). Continue analysis.

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 24.4558 (p-value = 0.0002)
Data FAIL B1 homogeneity test at 0.01 level. Try another transformation.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)

Z 1 1
O I I
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Title: lmac
File: lmac Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05
1 control 17.6000
2 .65 14.0000 72.00 75.00 10.00 *
3 1.3 10.7000 64.00 75.00 10.00 *
4 2.6 7.8000 56.50 75.00 10.00 *
5 5.2 5.2000 55.00 75.00 10.00 *
6 10.4 1.4000 55.00 75.00 10.00 *
Critical values are 1 tailed ( k = 5 )

Fisher's Exact Test
IDENTIFICATION
NUMBER OF
ALIVE
DEAD TOTAL ANIMALS
CONTROL 10 0 10
.65 10 0 10
TOTAL 20 0 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 10.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
1.3 9 1 10
TOTAL 19 1 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 9.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION ALIVE DEAD TOTAL ANIMALS
CONTROL
10 0 10
2.6 9 1 10

r-
TOTAL 19 1 20
ritical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 9.
Since b is greater than 6.0 there is no significant difference
between CONTROL and TREATMENT at the 0.05 level.
Fisher's Exact Test
IDENTIFICATION
NUMBER OF
ALIVE
DEAD TOTAL ANIMALS
CONTROL 10 0 10
5.2
8 2 10
TOTAL 18 2 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 8.
Since b is greater than 6.0 there is no significant difference
between CONTROL and 'TREATMENT at the 0.05 level.
Fisher's Exact Test
NUMBER OF
IDENTIFICATION
ALIVE DEAD TOTAL ANIMALS
CONTROL 10 0 10
10.4 4 6 10
TOTAL 14 6 20
Critical Fisher's value (10,10,10) (alpha=0.05) is 6.0. b value is 4.
Since b is less than or equal to 6.0 there is a significant difference
between CONTROL and TREATMENT at the 0.05 level.
Summary of Fisher's Exact Tests -
--------------------------------- ----------------------
NUMBER NUMBER SIG

IDENTIFICATION EXPOSED DEAD 0.05
-
i
i
(
�
(
i
I
2
3
4
5
CONTBOI, 10 0
'65 lO 0
l'3 IO I
2'6 IO l
5'2 lO 2
10.4 IU 6
^

MERITECH, INC.
&wow Santo,* Chan o f Custody
642 Timed Rd, Reidsville NC 27320
Phone: [phone] Fillc 1-336-342-1522
Sample ID It:
Enafl.roitstiadmagigbati Web Silo: wyntitneriledt-tabS.COnt
0
CLIENT INFORMATION
Client
Contact Noon:
//a / iif
AddreSs: ,
CRY:. 4%04).'
• County: Se:471/41/S
State:
P00:
WOES*: NC
Phone:
POPS
-.763/n" •
Sample IN*
SAMPLE INFORMATION
Sample Type: 0 Grab
of oontairiers:
Sampiterg lima: Start Date: q — 0 Stan Time: ci; 3/) 7 P1A
End Doc .5. -/D - End Tkna: /1) ilk) &PM
—• CHRONIC TESTS MUST SE
TAKER AFTER 1000 AM
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY, RAI (no air specs). CURLED AND COVERED
Callectort Memo: Print Signature:
Test Requited: El Cbmfilie(7&Ws)
Mita (24-48 hours)
Commits:
IWC:
TOXICITY TEST INFORMATION
Teat Organism: 0 Codoclophnla dubia Oster flea)
El Plasephakas pawns:as (fathead minnow)
El Ilysidopols kohl, (shrimp)
Teat Cementations Of multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
INFORIAA
Datrr
Sample Temperature (°C):
Method of Shipment D UPS El Fed EX El Maritach Pick-up
flompler aruppert au Friday rem be Fedex sod mist be deem Meshed ear Isherdey dam, •••
/ k ; / ,--
-,-..71 N (,;77— ' i li.
Date: , -..-- -7v nme: It:I. , est 3i4.. ',.......
Cele: Lc:- - 0 (>' Time: ill (4 AT
PM .„_.
Data: , - ' Time: lb.) 4 Am 0 .,,..
FG)
Tlme: AM
SAMPLE R.E.01/3/ING asborptory Use Orgy)
Relinquished by.
Reosived by:
Sample Temperatunte ('C): /
Cole:
NA PIA
Semple Contrition:

MERITECH, INC. Sample ID#:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech(albellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
Sample Slte:
Sample Type: ❑ Grab
Sampling Time: Start Date:
2
AComposite
CLIENT INFORMATION
PO#:
NPDES#: NC
Phone:
Pipe #:
State: /f/,C_ Zip:
SAMPLE INFORMATION
# of containers: a
Start Time: 9; 3'p 6P PM
End Date: 5✓gad End Time:/6f 6
PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"` SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITIl4 E "'
Collectors Name: Print:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 0/0
Signature:
TOXICITY TEST INFORMATION
Test Organism: El Ceriodaphnla dubla (water flea)
❑ Plmephales promelas (fathead minnow)
❑ Mysidopsls bahla (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
SHIP'ING INFORMATION
Date:
Date:
Date:
Date:
S -Y 'aLf
Sample Temperature (°C):
Time: Time: I . ® PM
Time: (j . J LS AM i
Time:
111 °° P PM
/'--:O J AM
Method of Shipment: CIUPS ❑ Fed EX ❑ Meritech Pick-u ' ;1
" Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday de�i rery"
Relinquished by:
Received by:
Sample Temperatures (°C):
SAMPLE RECEIVING (Laboratory Use Onlyl
Date:
Time:
AM PM
/ / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

77
Facility: LMAC
Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Date: 06/19/08
Laboratory Perfo
X
Signature �fOD r in Responsi
X
Signature of Laboratory Supervisor
Test: MEN: ECH, INC
NPDES#: NC0044725 Pipe#: 001 County: SCOTLAND
Comments: Dilution Water Batch
#672 & 673 Used
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
2 3 4 5 6 7 8 9 10 11 12
# Young Produced
Adult (L) ive (D) ead
18 19 20 20 19 21 23 21 20 22 17 19
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1
# Young Produced
15
2 3 4 5 6 7 8 9 10 11 12
15
7
10
14
11
16
7
17
15
14
10
Adult (L) ive (D) ead
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample 1st sample 2nd sample
7.97
7.92
7.93
7.91
s
t e
a n
r d
t
1st sample
7.55
7.41
7.54
7.10
7.96
8.02
7.95
7.91
8.01
7.97
7.96
8.03
s s
t e t e
a n a n
r d r d
t t
1st sample 2nd sample
7.60
7.56
7.35
7.28
7.65
7.69
7.48
7.50
LC50/Acute Toxicity Test
'(Mortality expressed
%
%
as %,
%
%
combining replicates)
Chronic Test Results
Calculated t = 6.623
Tabular t = 2.508
% Reduction = 36.82
% Mortality
0.00
Control
16.67
Treatment 2
Control CV
8.418%
% control orgs
producing 3rd
brood
100%
Avg.Reprod.
19.92
Control
12.58
Treatment 2
PASS
FAIL
X
Check One
Complete This For Either Test
Test Start Date: 06/11/08
Collection (Start) Date
Sample 1: 06/09/08 Sample 2: 06/12/08
Sample Type/Duration 2nd
Grab Comp. Duration D 1st P/F
Sample 1 I S S
P X 24.2 hrs L A A
Sample 2 U M M
P X 25.0 hrs T p p
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
Concentration
Mortality
ILC50 =
95% Confidence Limits
% -- %
Method of Determination
Moving Average Probit
Spearman Karber Other
start/end
pH
rganism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
42
183
1095
1573
<0.1
<0.1
0.6
Note: Please
Complete This
Section Also
start/end
Control
High
Conc.
D.O.
0.4

Ii en t:
TISL
Meritech, Inc.
Mini Chronic Pass/Fail Test: Ceriodaphnia dubia
Pipe #: pp ( County: & +I KC! Date Start:
JPDES #: NC (X Li li-)ZS Date / Time of Culture Transfer: 6 • /C-C bhp,
Dilution Water: Lake Reidsville Date / Time Neonates born: (c • / -c4 / 7- (D
"est Organism Source: Tray # S Age of Neonates at Test Start: & 4 . S-Eours
stirred / Aerated for D.O.: Y / J) Randomized: N Culture Tray Temp: -25.0 °C
Control Organism Reproduction
Day #2
1
2
3
4
5
# Young Produced
C
L•
C
0
C`
-
COCC
-
..
v
IV
1 1
IL
Adults Live / Dead
(_—
L_
L-
L
L
L
L
L
L
L
L
L
2
3
4
7
11
# Young Produced
`tl to
9 /�
` /7
1/i c
ilh
y f g
Lino
Y19
��g
L�'
Yl
14
cif 7-
Adults Live / Dead
L
L
L
t✓
L
L
L-
L_
L_
L
L
2
3
4
# Young Produced
a
k.
"1
R-
9
a1
Iv
Ii
IL
2
Adults Live / Dead
t
L
L
L.
(.._
L.
L__
t_
L
Total Produced
r/9-
ao
0\o
Test Sample Organism Reproduction
Effluent %: a, 6 I
Da #2
3
Percent of Control producing third brood:
4
5
17-119
# Young Produced
C
C
0
O
0
-•..
O
C'
CI
.,
C
,v
C'
1 1
0
IL
C;
Adults Live / Dead
L.
L
L
�
L
L
L
L
L
L
L
L
2
3
4
#Young Produced
q/5-9/
Th11.
//
VI 7t
/S"_VS--
r./L
'14)
VS---j}lt
3/7
Adults Live / Dead
L
L,
L
.D
L
L
L
L
L
L L
L
2
3
4
# Young Produced
fP
6
3
(Q
2
3
Iv
6
11
IL
O
Adults Live / Dead
L.
L
L
p
1---
L
L
L_
L
L_
L
a)
Total Produced
L
/"
11
t(
17-
to
Time Start: 1 5o,/
1st Renewal Date: 6 - j 3 .-CS Time: "'L/,S
2nd Renewal Date: (i- / c -05j Time:
Analyst(s): r7Z-M/mL Reviewed by:
Incubator #:
Date End:
Time End: 9 :) CAM
1;' Gs ---
Collection (Start) Dates:
Sample �v''[i j Sample 2: //Z/oB
Sample Information
1
100% pH
G / C?
Duration
Sample 1
7. (D
t .
lg. 2- hours
Sample 2
-),sp
G
2-5- hours
Batch #
67.1.
673
Sample
Sample
.___•7
Transfer Day
0
2
5 "
W.:
'.''
Hardness
(mg/L)
`�f ' I
Z.
Li 9
"
i.
� r��
l
Spec. Cond.
(umhos/cm)
153
-?
ter?
C1 I
q5 1 1
I'3
Y C�
Chlorine
(mg/L)
k
.p ..
Y
.lj::i l
� 0
zo, ++
Receipt Sample
Temp. (°C)
r .-1
`dam g' -.?`1
7
o, to
01 I
'
1st Sample
Control
?
70,3
Sample
7, Z-7,9)
D.O.
1st Sample
Control
-1;S-�
'2.11(
Sample
75y
7/v
Temp. 1st Sample
Control
zoo
Transferred by: Fed by:
Day 0
Day 1
Day 2
Day3 M
Day4
Day 5 01 f'L VA -
Day Day 6
Terminated by:
1st Sample
7q(0
79s
c,Z.
1st Sample
7.(00
'7.35
Z28
1st Sample
7.
,,
75.0
7f�s
2nd Sample
s,Qi
7197
2nd Sample
769
2nd Sample
2,0
Corr nts:
r
J
Sample _ Z S .� 2S

MERITECH, INC.
Sample ID ft: 0 i; 11 o
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech(aa..belisouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
L17?-4 C
/fM,iid,>i
76.
sc->p.�/17
State: N
Zip:
NPDES#: NC
Phone:
Pipe #:
Sample Site:
Sample Type:
Sampling Time:
❑ Grab
Start Date:
End Date:
SAMPLE INFORMATION
®. Composite # of containers:
Start Time:
/0 sc0 67 PM
End Time: /d ` / CJ.e6) PM
a
—. CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH I
Collectors Name: Print: �j/,�jL e)j0 Signature:
Test Required: Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 0l• Lo %
TOXICITY TEST INFORMATION
Test Organism: Cl Ceriodaphnla dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
SH
PING INFORMATION
Date:
Date:
Date:
Date:
/ : 1/0
€/ --v V
GP-lo -G6
Lc -/D-08
Sample Temperature (°C):
/< 6—/0E Isi
Method of Shipment: 0 UPS ❑ Fed EX ❑ Meritech Pick-up
**Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery'•
Time: Y ! f PM
Time:
Time:
Time: AM PM
m PM
13115 AM G
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by: difirCC.s [L,e-I'__. / c
Received t i Date: /n //'
Sample Temperatures (C 0 •gyp / U • (p / /
Time: 07c) .S
Sample Condition: I:CP
PM
WHITE = Laboratory copy
YELLOW = Client copy

MERITECH, INC.
Sample ID #: D .o I Leg
er'1,
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech at ..bellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
Sample Site:
CLIENT INFORMATION
/l 70 / e;474T �(J
State: ry- Zip:
SAMPLE INFORMATION
PO#:
NPDES#: NC
Phone:
Pipe #:
Sample Type: ❑ Grab gi Composite
Sampling Time:
# of containers:
Start Date: - % •-D b Start Time: 9. 3 D
End Date:_ J D End Time: /d;a0
PM
PM
—+ CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"` SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITHICE "'
Collector's Name:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: OA
Signature:
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
r
Relinquished by: +
Received by: 1 1Q0s/ �—
i
Relinquished by: /' 0-j c
Received by:
IPPING INFORMATION
Date: d— / � `-e-) r
Date:
Date: - I3 -v b
Date: 6 —13 _ v
-/$--ci8 S-oo r,5
Sample Temperature (°C):
Time: ) 1 SO CZ PM
Time: j / S-0 RADII PM
Time: AM PM
Time: / = 5 5 A PM
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery**
Relinquished by:
Received by:
Sample Temperatures (°C):
SAMPLE RECEIVING (Laboratory Use Only)
Date:
Time: AM
Sample Condition: i
WHITE = Laboratory copy YELLOW = Client copy

Effluent Toxicity Statistical Results - Chronic Pass Fail
/ Date: 06/19/08
Facility: LMAC NPDES#: NC0044725 Pipe#: 001 County:SCOTLAND
Laboratory Performing Test: MERITECH, INC
Reduction: 36.82%
CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 10
Adult Male 0 0
Adult Dead 0 2
Adult Mortality 0.00% 16.67%
# Neonates 239 151
Mean # Neonates 19.917 12.583
Standard Deviation 1.676 3.450
Coefficient of Variation 8.418%
A = 12
Fisher's Exact Test
B = 12
a/A = 1.00
a = 12 b = 10
b/B = 0.83
Success is: survival
Critical b value = 8
10 > 8
The test concludes that the proportion of survival is not
significantly different for the control and the effluent groups.
Test Passes!
SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA
ORDERED OBSERVATIONS
i Group Neonates Centered i Group Neonates Centered
1 E 7-5.5833 13 C 20 0.0833
2 E 7-5.5833 14 C 21 1.0833
3 C 17-2.9167 15 C 21 1.0833
4 E 10-2.5833 16 E 14 1.4167
5 E 10-2.5833 17 E 14 1.4167
6 C 18-1.9167 18 C 22 2.0833
7 E 11-1.5833 19 E 15 2.4167
8 C 19-0.9167 20 E 15 2.4167
9 C 19-0.9167 21 E 15 2.4167
10 C 19-0.9167 22 C 23 3.0833
11 C 20 0.0833 23 E 16 3.4167
12 C 20 0.0833 24 E 17 4.4167

SHAPIRO-WILK'S TEST FOR NORMAL DISTRIBUTION OF DATA (cont.)
COEFFICIENTS AND DIFFERENCES
i x(n-i-1) x(i) a(i) x(n-i-1) - x(i)
1 4.4167 -5.5833 0.4493 10.0000
2 3.4167 -5.5833 0.3098 9.0000
3 3.0833 -2.9167 0.2554 6.0000
4 2.4167 -2.5833 0.2145 5.0000
5 2.4167 -2.5833 0.1807 5.0000
6 2.4167 -1.9167 0.1512 4.3334
7 2.0833 -1.5833 0.1245 3.6666
8 1.4167 -0.9167 0.0997 2.3334
9 1.4167 -0.9167 0.0764 2.3334
10 1.0833 -0.9167 0.0539 2.0000
11 1.0833 0.0833 0.0321 1.0000
12 0.0833 0.0833 0.0107 0.0000
1
W = X 155.0551
161.8333
Calculated W = 0.958 Critical W = 0.884
0.958 a 0.884
The reproduction data is normally distributed
evaluated at a 99% confidence interval.
Test Passes!
F test for Homogeneity of Variance
Effluent variance 11.9015
F = - - 4.23
Control variance 2.8106
Numerator degrees of freedom: 11 Denominator degrees of freedom: 11
Critical F = 5.32
4.23 s 5.32 =► The Test PASSES, the variances of the two groups
are significantly the same, homogeneous.

EQUAL VARIANCE t TEST
19.9 - 12.6
t = - 6.623
1.107
Degrees of freedom = 22
Critical t = 2.508
6.623 t 2.508
Test fails. There is a significant difference in reproduction
between the Control and the effluent evaluated at a 99% confidence interval.
Chronic Test FAILS
The mean # of young produced by each group is dissimilar

MERITECH, INC. Sample ID#:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtechbellsouth.net Web Site: www.meritech-labs"com
CLIENT INFORMATION
Client: / . //1 .r
Contact Person: z" P / / K -�• ;�' ; /g, i / 7-
Address: /;!, 74
v L.
City: , •/.��X r.� ,•',/
County: , •l % /-;;5 -3 State:
- Zip:
NPDES#: NC
Phone:
Pipe #:
,3 r
Sample Site:
SAMPLE INFORMATION
Sample Type: 0 Grab 0 Composite
Sampling Time: Start Date:
End Date:
//% - %i (7')
# of containers:
Start Time: / i) " ; �j AM PM
End Time: //) • / J `AM> PM
—. CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"` SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH -*!*
/ Signature: Cam`
Collector's Name: Print: ; i� .(•` /�/� �-�1r, if �'%," .; 9 s" / �� r/ c;‹-/• 1,
' TOXICITY TEST INFORMATION
Test Required: Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 9, /( %
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:'' /^
Received by: !�
PPING INFORMATION
Cis
, i. '4 • 1E'; i—•
Date:
Date:
Date:
4 — / • 3 L ?•
Date:
Time:
Time:
Time:
Time:
13L1
Sample Temperature (°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
**Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery "
PM
PM
AM G
AM PM
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / - / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC.
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Sample ID #:
Email: txmrtech[a)bellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
PO#:
/ 4-ir NPDES#: NC
Jl 70 - o4 A
State: /VC Zip:
Phone:
Pipe #:
e 44-
Sample Site:
SAMPLE INFORMATION
Sample Type: ❑ Grab g Composite
Sampling Time: Start Date:
End Date:
Start Time:
End Time:
# of containers:
9:3L0cPM
* :sV ( ) PM
--► CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH E •'•
Collectors Name: Print:di/Er ,r,C.4",70,(1)--zezi Signature:
TOXICITY TEST INFORMATION
Test Required: ❑ Chronic (7 days) Test Organism: ❑ Ceriodaphnia dubia (water flea)
0 Acute (24-48 hours) ❑ Plmephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Comments:
Relinquished by:
r
Received by: Z oo0s 14 9—
Relinquished by: / 001-c
Received by:
IPPING INFORMATION
Date: d- / `5 0 V- Time: ) 1 c 1 PM
Date: (o - I �' i Time: ) / sty `ANI PM
Date: (4 -I3'Cl d Time: AM PM
Date: Time: AM PM
Sample Temperature (°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
.• Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery .•
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility k %
Laborat ry Performing Test
x
S g ture of
NPDES#: NC rjp /1Jg.
Signature of Lab Supervisor
Pipe# County —51t)
Comments lTfitkoh \NI
•W lo7g k/ 1) 1,,524r1 . Sfihbs-,-iC; ,'ndic44e ks
/.3 % F)l ), /.3' i s c .2c) R�
Sample Information
1
Sample 2
Control
Collection Start Date
Grab
Composite
(Duration)
Hardness(mg/I
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receipt
_Sample
7./j
7: i 7-�7g��
4.41
{ `#} "v
1^-�'L}„�
' , I
-'1,
.., z ; i ; `
'`.I.
{*i °
;,4 v._ is
,r
"1
-.
17S Cl
/rye Ill
0, j
.0 a, i
I 9 'c
0, 5
c
, ,,
Control
Effluent%
i.- ( 5
Effluent%
I �
1
Organism#
2 3 4 5 6
Test
Information'
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
Start Date
7i6-6P
End Date
72.3/0&
Start Time
l /:40a4
End Time
9
Start
Renewl
Renewl
Start
Renewl
Renewl
°!0
/U.i
Control
Control
Control
8.00
is,03
7'1 G
7 2-3
g. rxt
75—q
7OD
A a
s.20
c 1z
7.5
707
7.60
7.93
7,G1
7.1/ 2)
oi
7."
7.GS
7.2,2
29.
293
7..3
76C
25. i
2L/4
2 '0
Mean
# Young
ow
aU
i
9-I
),4
AI
23
2/
a)
23
24A
Adult
(L)ive (D)ead
L
t
i._
L.
L-
L
L
t_
L
L
# Young
Adult
(L)ive (D)ead
# Young
Adult
(L)ive (D)ead
1
;b
t_
/9
L
1 2
1g-
L
l3
L_
/7
L
4 5 6 7 8 9 10 11 12 Mean
AS-
L
L_
14
L
C_
12
3 4 5 6 7 8 9 10
Ili
L
t_
I9
1y
L
//
L
15,
L-
19
Mean
/7..1
% Red
Mean
Effluent%
# Young
1
et
(L1
$
0
to
%v2
1
9-
1 .
/v.,i
%Red
CZ,Z
—
Adult
(L)ive (D)ead
L-
L-
L
.P
L
L
L_
L_
L.
Mean
Effluent%
# Young
0
5
1
kg,
v
er
cit.
10
V
A
Gg
SI L
Adult
(L)ive (D)ead
L—
L
L
L-
L
L.
L
L
D
L
%Red
G...,
Effluent%
III, `]
# Young
Adult
(L)ive (D)ead
1
Li
L
2 3 4 5 6 7 8 9 10 Mean
7
L
7
L_
3
1
S
S`
L
L_
0
L_
�y 4
U
Chronic Test Results
Final Control Mortality %
% Control 3rd Brood
Control Repro CV
0
MO
6,
ef
48 Hour Mortality
Control IWC
D _of 1O_
Significant?
Final Mortality
Y
�_of 10
No Co
Reproduction Analysis:
Repro. LOEC=L13_%; NOEL=0./.C%
Method:
Normal Distrib?�t3 Method:: jc QY
Statistic:A,�7¢ __ Critical:_
Equal Variances? Q method:RicLUeff
Statistic:L7.�_____ Critical:��i__
Non -Parametric Analy� (if app icable):
Method �f) �Q �/eS-
1c.
Effluent % Rank um Critical Sum
S-R, e 7S ; 0
P x-
ss 751 .4
Overall Analysis:
Result = PASS/FAIL or
Test LOECe . &, %' NOEC=1..3
Chronic Value= /1
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mgll
% Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95

MER/ TECH,, /MC_
ENVIRONMENTAL LABORATORIES
A O;v;s;on of WAf.•r TC'Chno/ogy an C.or.f,'o/s. /roc
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
Client:
NPDES #: y L-17Z 5--
Collection Start Date
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine (mg/I)
Temperature (°C)
100% pH
Incubator #:
1st Sample
2nd Sample
7/VA'
77/7/a
.S(o
16
7e 7`-
T'y/
Temp. of Stock: 2-C- °C
Randomization:
No
Dilution Water: Lake Reidsville
Batch #
Transfer
Day
Hardness
(mg/L CaCO3)
Conductivity
(umhos/cm)
6)79
0
yU
lc z--
,(
2
../
.ii
(a div
5
uLI
l R 1
Sample D.O. Adjustment:
Stirred Aerated
Neonates:
Tray*: _I ,
Transfer Date/Time: 7 ^ /r• 1 / Y . I(, - FlP1
Born Date/Time: 7- ) L� /
Age at Start of Test: ?-01 hours
Test Start, Renewal, and End Dates / Times:
Start Date:
1st Renewal Date:
2nd Renewal Date:
End Date:
1/14:4,y Time: 1I0OA,rn
74 I,
-743 /01
Time: ?' / 5144
Time:
Time:
Test Transferred by:
Start:
Day2: 14/112
Day 5:
Terminated: VVi 4—
Test Fed By:
Start: M
Day 1: 411-
Day 2: M
Day 3:
Day 4: AX,
Day 5: __
Day6: A.1
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Starta
End
Start
End
Start
End
pH
Control
-2,c 1
-7 .9 3
?.0 1
7,Q `'
zo3
7. 3
High Conc.
.6,,.
g• 03
',0(:)
sc, i) -2_F
Zv
r. 1 Z
D.O./,
Control
7, (G /
--7, q 3
.--7. 0-
7. 2.2
7, .-
705
High Conc.
/!
7 �llfi
-7.25�
7�Y
7•00
,/
7,s-
�7
07
Temp.
Control
Zki. j
-? `k ,
-`t•c6
-2.c.Z--.
?,5 •t.
High Conc.
ZL1,2;
-LA,(i
7.LI,5
'Zc,0
ZS, /
Z.�v

Client:
control
� YM C
NPDES#: NC 00Uy72.5
Day #
2
5
Total
2
5
7
Total
2
i, 3 % 5
7
Total
2
z.(o % 5
7
Total
2
5, % 5
/O.V %
7
Total
2
5
Total
1
2
Meritech, Inc.
Ceriodaphnia dubia Chronic Multidilutional Reproduction
Start Date: Start Time: l Dc --
3
4
End Date: 7/2 v` /ne End Time: `-r
Analyst(s): ./7t/f— Reviewed by:
Replicates
5 6
7
8
9
10
O
0
p
0
0
o.
O
O
0
O
/7
s'%'
.3/
33
LI/9
Y�,
3//4'
V /7
i/
4//
g
7
3-
/0
8
q
/a
/d
9
.D
.30
,'
-2/
2/
2.1
a-3
:).1
/
2.3
O
O
0
O
O
O
0
O
G
LI/1
'1/4
y y
.s/P.
3/9
4/9
/
Y,/
1
Wg.
0
7
7
F
C
9
5—
;o
/9
/ -
mac—
/ 3
-V
iSy
19
V/
i.
O
0
0
0
0
C')
0
CI)
O.
C)
///�
L//(
17/f 7
VA?'
.3/5—
:c
Y 9-
y7,3
/'
6
3
s
8"
2
".s
/R
/3
ie,
J1
/V
/.
7R*
/ g
(-)
G
0
0
0
O
O
O
o
0
/_3
L
y f 7
D
o
9
Y/7
'1/y
a/ -7
lq
ci
)1
&-ip
0
1O
2
/ '
2
,2
()
O
O
O ..
O
(-)
0
0
0
O
D
3
5/ i,
/:
0
9
y
L//Y
Y .27
=R
D
2
Sr
(7
5—
..
--
0
,4—"
o
.5--
9
/6
0
0,
/a
i.c
-2
C)
0
0.
0
0
0
0
0
0
c•
�
`1
3/3
3
/f
V
3/2
s—
0
0
0
.3
/
oD
0
/
0
3
—
% 3rd Brood
Iw
C.V. Mean
9
Reproduction
% RED.
% RED.
% RED.
% RED.
20 , 1
C. z
17/
g', —
rn.z
1. z_
.a;, I
0/0 RED.

MERITECH, INC. Sample ID#: Of `(-PC s —a
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax [phone]
Email: txmrtechbellsouth.net Web Site: www,meritech-labs.coni
—11 L—
CLIENT INFORMATION
Client L in L PO#:
Contact Person: : GiLe.{ .�; n NPDES#: NC
l' '
Address: I C 0 k�. i.. nor' p.�� Phone:
City: ({\o,.F —D n o_ Pipe #:
County: 5 el State: N L Zip: a`1 j-3 b
Sample Site:
SAMPLE INFORMATION
Sample Type: ❑ Grab ErComposite
Sampling Time: Start Date: - L -f 'v
# of containers:
Start Time: / 0; 00 g PM
End Date: — j S '�� End Time: 1 O'• 0 5 An PM --. CHRONIC TESTS MUST BE
v TAKEN AFTER 10:00 AM
*** SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE'*`
Collectors Name: Print (R : (�k,e y 0Xe."d ; n
Signature:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
twc• a . %
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysldopsls bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:'
Relinquished by:
Received by:
SH PING INFORMATION
Date: 1 ^ ) ,S— Time: \--'..SO AM t
Date: �-' 1 J J Time: 1a, AM
Date: / - Time: AM PM
Date: Time: AM PM
Sample Temperature (°C):
Method of Shipment ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
" Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery "
Relinquished by:
Received by: Date: 1/' (p f O (� Time: 10 00 A6i1 PM
Sample Temperatures (°C): ] e / I . / / Sample Condition: l ( J
SAMPLE RECEIVING (Laboratory Use Onlvl

MERITECH, INC.
pioassaySample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtechabellsouth.net Web Site: www,meritech-labs.corrt
Sample ID #: V 7 194
CLIENT INFORMATION
Client 2,34
Contact Person: 071, / aj4-/-'
Address: / 44 / /j AI.Ij 4 'I'd
City: !/%,q era /f/ !7/C Pipe
County: sl C46 TI-Zi7esVd State: /f/ '� Zip: ,qJ,Tal
PO#:
NPDES#: NC
Phone:
SAMPLE INFORMATION
Sample Site:
Sample Type: 0 Grab .Composite # of containers: Q
Sampling Time: Start Date: 7-47-t 0 Start Time: , 36) ® PM
End Date: 7 •-/ - U S End Time: /d;Q PM —+ CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no airspace), CHILLED AND COVERED ' ICE "'
Collectors Name: Print ..-7/X610j �1l?dA,111/
Signature:
,� TOXICITY TEST INFORMATION
ILj Test Required: 'Chronic (7 days) Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Acute (24-48 hours) ❑ Plmephales promelas (fathead minnow)
❑ Mysidopsls bahla (shrimp)
Test Concentrations (if multiple dilutions):
Comments:
IWC:
iyo
SHIPPING INFORMATION
elfin uished b : ` "
q Y [ 7 Time: I /3 0 � PM
Received by: •i`"j - Date: / `d F ff Time: 1 1 -j D Ci PM
Relinquished by: Date: -7- Id' 9 Time: '1( 1-06 AM Li
Received by: % Date: '7 - ( a' -'Y Time: f '3-. , tJ AM l
Sample Temperature (°C):
Method of Shipment: 0 UPS 0 Fed EX 0 Meritech Pick-up
" Samples shipped on Friday must be FedEa and must be clearly labeled for Saturday delivery "
e 1` SAMPLE RECEIVING (Laboratory Use Onlyl
/4 7\1 Relinquished by: /n� -7- / q -(j : q6 p/A
/( Received by: IV) 1�- Date: Time: ' 6d AM PM
Sample Temperatures (°C): 0 • S / d . Y / Sample Condition: t

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D = 0.1109 (p-value = 0.0638)
D* = 0.8702
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data PASS normality test (alpha = 0.01). Continue analysis.

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 17.5538 (p-value = 0.0036)
Data FAIL B1 homogeneity test at 0.01 level. Try another transformation.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)
_7

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX MEAN
1 control 10 18.0000 23.0000 20.9000
2 .65 10 12.0000 25.0000 19.2000
3 1.3 10 13.0000 20.0000 17.1000
4 2.6 10 0.0000 18.0000 10.2000
5 5.2 10 0.0000 16.0000 6.4000
6 10.4 10 0.0000 8.0000 4.3000
Title: lmac
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE SD SEM C.V. %
1 control 2.1000 1.4491 0.4583 6.9337
2 .65 13.0667 3.6148 1.1431 18.8270
3 1.3 5.2111 2.2828 0.7219 13.3496
4 2.6 25.9556 5.0947 1.6111 49.9476
5 5.2 26.0444 5.1034 1.6138 79.7402
6 10.4 7.5667 2.7508 0.8699 63.9711

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05
1 control 20.9000
2 .65 19.2000 82.00 75.00 10.00
3 1.3 17.1000 60.50 75.00 10.00 *
4 2.6 10.2000 55.50 75.00 10.00 *
5 5.2 6.4000 55.00 75.00 10.00 *
6 10.4 4.3000 55.00 75.00 10.00 *
Critical values are 1 tailed ( k = 5 )

MERITECH, INC. Sample ID#:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtecht bellsouth.net Web Site: www.meritech-labs.com
L- 19'1-1S3
CLIENT INFORMATION
Client L it A L PO#:
Contact Person: 1' 1: c k _e,( o-iC r• .e, NPDES#: NC
i Address: I (D—I O 1 I
. r e.0 �� ��r/� Phone:
City: , ' „''�-+ 0 I-)
U Pipe #.
County: 5 (1, o r\ a State: N L Zip: a`a ?) C LI
Sample Site:
SAMPLE INFORMATION
Sample Type: ❑ Grab ErComposite
Sampling Time: Start Date: -_ - l.1f-o 8
Start Time:
# of containers:
/a.Ogo PM
End Date: - j S " $ End Time: / O,. O 5 PM --. CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
*" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no alrspace), CHILLED AND COVERED WITH ICE "'
Collectors Name: Print in : C,k,e7 C:1)Le.,j; n Signature:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
SH ING INFORMATION
Relinquished by: dj� ` Date: —1 - 1 S Time: \\`.SO AM PM
Received by: 7 Date: 7- I J• a' Time: 1�; S b
�7 AM
Relinquished by: iC(4-- / Date: - /,- Time: AM PM
Received by: Date: Time: --- — AM PM
Sample Temperature (°C): /�\, ;-- = r
Method of Shipment: 0 UPS ❑ Fed EX 0 M11 eritecti.Oick,Lp '�'
" Samples shipped on Friday must be FedEx and must be clearly labeled( Saturda f1ellvery"
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by:
Received by: Date:
Time: AM PM
Sample Temperatures CC): / / / Sample Condition:

V!/ ♦V/ <uVV
s
CW:
MERITECH, INC.
642 Ttma, Rd. Reidevne NC 27320
Phone: [phone]e Fax [phone]
Emdf:
flans Sir
State: ,.
Sample MK =Minutium
O
Ian*, Type: Odab acomposis
• a oont,inerrSempUes
nm.: Start Q,M �..
stmtTime: '6 Pal
End Dri; 7 �-/S� Q End Tine. jt) Psi `-• CHRONIC TESTS N US •BE
... � MPLE CONTAINARE Ito DE COMPLETELY FULL (no al r TAKEN AFTER ladll Al
Consci n's t Print 'SP�1. CtfA' LE
5n:
POt:
MESS: NC
Phone:
Pt•a
r..t+trqutwa: �rnnk
R ) TestOrganism O cododyphnft d (meter
❑ Phi, lro+ndw (farad minnow)
0 bride (stomp)
ANC: 96 tot Concenfrallons (if multiple
Cm,neeraa:
Received by:
Relinquished by;
Rooehod by:
Re Chun/ lad by-
Received by:
SampU Ta,npersturog (
0 Acute (24-4a Imre)
mCm► Tsa. ,
m.Tv,.,
Sample Temperetire (C):
•h,LCJ,R7 lti(Fr'm1 T..�. u
n
Data /9` dt /H' Tire: l� {3 a' ,let
Dote: (d' /3 L da
Dee: -7_rY---�. Tine: -L-`_ AN
Tlme 1.3`_t AM Ft
Mom
Mae od of Shiaent: 0 �❑ Fed EX
Mr lempisa stopped an Miel n�aria moat be plearyWiled for $andq away"
—� Debt: ysr Time: l-?Gd
8an'pa Condition:
I

Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
Facility L1,tv). NPDES#: NC 0 Cite g72 Pipe# County .c.3 f /CuiC
Laboratory Pe
Signatur4 c)f O.R.C.
CiZ
Signature of Lab Supervisor
Sample Information
Sample 1
Sam le 2
Control
Collection Start Date
Grab
Composite
p
(Duration)
Hardness(mg/I
Spec.Cond.(pmhos/cm
Chlorine(mg/I
Sample temp. at receipt
g/y O �
FI7log
__
`.
44
tom. n t,
2r{ ; hr
Z r
y,3
"..,
''•,,01i?,t
����{ .�`��
^. ,..
'' �.-�yY?Qj
4'i Nb yb
mom
i 3 (W
' Z 110
c o, I
L o, /ff-
.. ,s.
J • j °c
o1 °C
�.•;
Control
Effluent%
O•(oS
Effluent%
1.3
# Young
1
1(�
Organism#
2 3 4 5 6 7 8
tq
1q
19
18
Comments 0, ((J.
iv�{2i 6Cst-d, s
(.� 6 3 t;a BS uscd
Test
Information*
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
Start Date
8/ /g
End Date
/r3/o6
Start Time
II :II
End Time
/0 :3t.
Start
Renewl
Renew2
Start
Renewl
Renew2
b/o
/O.y
8:I `(
$,z.3
/D, `1
g,.t)
a/o
6,03
/O,Li
8,15
8,3z
Control
8.z3
Control
7.95
7, n
Control
8,01
7.L3
7. Nl
7.57
7.N6
Z
7, 68
7, 3,
7.2.0
7.1t3
7,35
7•Zz
'7, /D
l-S.0
2S•G
2S'O
zS.o
ZS.0
2 5-
ZOO
zS.0
z S C)
9 10 11 12 Mean
9
Adult
(L)ive (D)ead
L
L
L
L
L
L
L
L_
Chronic Test Results
Final Control Mortality °n
% Control 3rd Brood
Control Repro CV
90
# Young
Adult
(L)ive (D)ead
# Young
1
1q
20
L
2 3 4 5 6 7 8 9 10 11 12 Mean
l(y,q
I,)
L
19
L_
1 2 3 4
1d
13
IQ
zN
10
L
zz
L
Iv
L
1�
IZ
L
)b
L
5 6 7 8 9 10
11
18
17
Iy
z1
17
Mean
Adult
(L)ive (D)ead
L
L
L
L
L
L
L.
i_
% Red
.11,r i
Mean
Effluent%
# Young
VI
17
12.
16,
I L
1 s
19
Is
ZG
IC
11.0
• (0
(L)ive (D)ead
L
L
L
L
L
L
L
L
L
L
Mean
Effluent%
# Young
2.1
t 9
(Z
ILi
LL
Zl
z 1
1 7
11
19
l .S"
s. Z
(L)ive (D)ead
L-
L_
LA`
L
L.
L-
L
L
L
�l4eL
Effluent%
# Young
Adult
(L)ive (D)ead
1
7,3
L
2 3 4 5 6 7 8 9 10 Mean
L
1(0
L
7,1
7.3
L
zl
L
ZU
t'
IO
L
19
L
% Red
-4,3z
48 Hour Mortality
Control IWC
Uof _I 0_
Significant?
Y
0 of IC)
Final Mortality Si. nificant
or
Reproduction Analysis:
Repro. LOEC= y ro L %; NOEC= /0• / %
Method: 5ec.l's ��Cr•��lc-•.k
Normal Distrib? 11) Me od:xU
Statistic:_ I_t .0
Critical:_ i
Equal Variances? 5 Method:ix.41e L _
Statistic:_) . - Critical: iS-e`?
Non -Parametric Analysis (if applicable):
Method: .Sk-e .t •s 111a Cre L1 c
Effluent % Rank Sum Critical Sum
0,65- .J —_ 75-
1.3
z,to
S. 2-
ID.,-1 7X
_
—I 1 z-- -
—� i�-- 75-
Overall Analysis:
Result = PASS/FAIL or
Test LOEC= >/0.9 _%; NOEC= /0•V %
Chronic Value= >/p.N _%
MAIL
TO:
ATT: Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, N.C. 27699-1621
'Should use highest test concentration or
highest concentration with D.O. >5.0 mg/I
t% Reduction from Control Reproduction Mean
DWQ form AT-3 (8/91) Rev. 11/95

T�
/V1ER/ TECH INC_
ENVIRONMENTAL LABORATORIES
' L)i visio,, rnr N41 rrr T.•chrio/c,q :1,1d C:c,n( o%c. Inc
Multi-dilutional Ceriodaphnia dubia Chronic Definitive Test Data Sheet
Test Effluent Information:
Client: L A 1
NPDES #: IUC. (`}o yL/%Z(
Collection Start Dat
Sample Type / Duration
Conductivity (umhos/cm)
Residual Chlorine (mg/I)
Temperature (°C)
100% pH
1st Sample
e
2nd Sample
s-//9/G32
L /7 /68'
G/ .3
6 q.3
130
2114
16,1
Lo,1
I.S
b, I
S', L l
$..Z 6
Incubator #: 3
Temp. of Stock: °C
Randomization:
No
Dilution Water: Lake Reidsville
Batch #
Transfer
Day
Hardness
(mg/L CaCO3)
Conductivity
• (umhos/cm)
(o83
0
.4N
/ s72__
6, g Li .
2
,16
t ec/
(P S
5
WO
1 qZ
Sample D.O. Ad'ustment:
Stirred Aerated orie
Neonates:
Tray #:
9
Transfer Date/Time: ?-5--"0 l_
Born Date/Time: k" /1 -id,S—
Age at Start of Test:23.3 hours
Test Start, Renewal, and End Dates / Times:
Start Date:
1st Renewal Date:
2nd Renewal Date: End Date: i 3 /o(
qdor
q, (oe
Time:
Time:
Time:
Time:
l/%,3eAm
Test Transferred by:
Start: / —
Day 2:
Day 5:
Terminated:
l44(—
/1'2
Test Fed By:
Start:
Day 1:
Day 2:
Day 3: %X-
Day 4:
Days: f
Day 6:
Chemical and Physical Determinations:
Test Start
1st Renewal
2nd Renewal
Start
End
Start
End
Start
End
?.8,r
pH
Control
g`. 0 `1
Z, Z3
7. ? (
7, 7`!
0,01
High Conc.
, f 2
Li_
Q 2
CJ . -2J
K , 7
Q
U 163
i, /5
`
�(
1Jf 3�
D.O.
Control
', L
7, 3 c
�. Li
7, ZZ
7, (o r
7,!o
High Conc.
7 3
--),3(
-).LI)
-2,20
7,.. q
7/e
Temp.
Control
2,c 0
23.0
z(
vc.17
2> ,0
zS (D
zs.F----
High Conc.
ic,0
is ,0
7.6U
VS V
0

Client:
control
Meritech, Inc.
Ceriodaphnia dubia Chronic Multidilutional Reproduction
Start Date: gr.- t •- C
NPDES#: NC Ooy1-17��
Day #
2
5
7
Total
2
5
7
Total
2
5
7
Total
2
% 5
7
Total
2
% 5
7
Total
2
5
7
Total
1
Start Time: 11'/5.—A- n
End Date: Cc -• G 5 End Time: I(:): 3 C /j r7
Analyst(s): (112_/ 'rG Reviewed by:
Replicates
2 3 4 5 6
7
8
10
0
. U
o
0
O
O
0
c.,,
Q,
o
3f�
Q/7
'?/$
9/7
S//$)
-/1
/
V
9
5`"
,5"
.,
R
7-7
/ 6
/
)6,
) i
/(,
/6
/9
/6/
/9
l
i(
q
0,
0
G
o
c,,
G
o
0
0
7, .
V
`/
l,;
c;
_5A--
YA
3/7
d -/'
7/1
, fl>
6/ -
b
• 7j/
6
c?/
-2 0
I
/ S
19�
U
0
o
0
0
0
p
0
C
0
/g
%/
17
If'%n
,5""
V. j
of 5-
6
f0
?-.
7
6/'
7/ 9
7
Pi
l -
/9
.,)-Li
)/
) .
) 7
l/
...l
)7
o
0'
0
G
0
0
0
01(l
/r
/0
5!
�i/ '1
/
1
/7
G=
(.: 7
; 1
c9
7! !7
/
/�
./
�5---
/7
)2
/P
4'7
/9
�
o. ,
o
0
0
0
0
0
o
c,
0
y6
6
Li
9
9/6
.
99
L.
'/
-9 0
/
3
i --
/J
.
Jl
;/
17
i9
iq
^,Z 8-).r•
0)
0
0
0
0
0
o
c,,
c>
0
y/9
`}
6
s
s—
/4
'/&
tj/'
/
s 7
//
7 7
1
119
a)
.Z)
l'
)0
) C
2,
% 3rd Brood
I clo
C.V. Mean
18•�
Reproduction
% RED.
% RED.
% RED.
% RED.
% RED.
Nr ,2-
160
1?. o
►7,0
1 FY. 5

•+cc u-rp
p-1
•
MERITECH, INC. Sample IDAt_ _ O 6O " 03
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax [phone]
Emit bunrtech(dtbellsouth.net Web Site: www.meritech-tabs.com
CLIENT INFORMATION
/6 7.0
She /7)-1. 4,4d
0 Grab .-Composite
Start Date:
End Date:
State: A/<- Zip:
SAMPLE INFORMATION
S-0 V
# of containers:
Start Time: 9:4- ;- V PM
End Time: /1) -ar 6) PM
Client
Contact Person:
Address:
City:
County.
Sample Site:
Sample Type:
Sampling Time:
MEM
POD:
NPDES#: NC
Phone:
Pipe #:
-gig 3/a�
—. CHRONIC T1 3TS MUST BE
TAKEN AF IE . i0:00 AM
"` SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED 177 1 ICE •"
Collector's Name: Print ,2X:CiC j, /X ,4'6(`4;' ' Signature:/. ` ftf`
Test Required: ❑ Chronic (7 days)
❑ Acute 1:24-48 hours)
Comments:
IWC:. 96
TOXICITY TEST INFORMATION
Test Organism: ❑ Cedodaphnia dubla (water flea)
❑ Plmephales promelas (fathead minn w;
❑ Mysldopsls hahla (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by;
Received by:
Relinquished by
Received by:
HIP IN INFORMATION
Date:
Dale:
Date: S '134
Date: s r 0 8
Sample Tempe re (°C):
Method of Shipment ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
" Samples shipped on Frtdsy must be FedEx and muat be clearly labeled for Saturday delivery '-
Time: l a- D-L° AM CFA
Time:
Time:
Time: S - / AM PM
r�� 1 AM PO
5: 15 AM C
0-11 U e PM
Sample Temperatures CC): Lc J / I S j 1
Sample Condition: LC.G��
SAMPLE RECEIVING (Laboratory Use Only,
Relinquished by: Aufte.A.A._ tue..4„-
Recetved•b'/4----- Date:
Time:

I 1.V! II !1\V.
p/oessav Sample Chain of Custody
• 642 Temco Rd, ReIdevtlle NC 27320
Phone: [phone] Fax [phone]
Sample IO f: 6 2-0
Email blmrtachebelleouth.net Web Site: www_meritechJaba.cam
CLIENT INFORMATION
CEent / /7%,44,
Contact Person: /}1,- y ,,.77;,
Address: /6 7,C) ' ( z/,°)Kl % ,rd
County: s/1_01 4 -7 L State: 4,[
POO:
NPDESt: NC
Phone:
Pipe it:
SAMPLE INFORMATION
Sample SIN:
Sample Type: 0 Grab Composite
Sampling Tine: Start Date:
End Date:
# of contalnera:
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no airspace), CHILLED AND COVERED WITH
CoU.ctote Nam: Print /!',l�`l°,1(+ ek4e`l Signature:
8 ` / c9 ) start rim.: 9 . -g Ar PM
93— e--/)s
Test Required: 0 Chronic (7 days)
0 Acute (24.48 hour)
Comments:
End Time:
TOXICITY TEST INFORMATION
Teat Organism: ❑ Carlpdaphnla duble (water flea)
❑ Plmaphates prpmefas (fathead minnow)
❑ Mysfdopsls bahla (shrimp)
IWC: °% Test Concentrations (f multiple dilutions):
PM
Relinquished by:
Received by:
Relinquished by:
Received by:
S, N
Date:
Date:
Date:
_,j
TION
-g
Date: 5 — e
Sample Tenjperature (°C):
Time: 11: 61,
Time: /b Ot� 6
Time: It; 06
Tine: fa-1..•0-0— AM
d. ��f.�-.��� 17— a—oR r.5"A ,r;ys-pi)
GG nMMetthod of Shipment ❑ UPS CI Fed EX CIMeriitech P(dc-up
Z G : /� fie R miser mint t» FedEt Ind meet be chicly labeled far Setae y r.ttwry "
PM
PM
PM
`(� A AMPLE RECEIVING (Laboratory Use Only)
Relinquished by: n _ / ,`�
Received by: /1- p..ea_d_._ Dele: ? —, Time: )034 to
Sample Temperature; CC): 0 ., /jjli / Semple Condition:
PM

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D =
D* =
0.1504
1.1799
(p-value = 0.0017)
Critical D* = 1.035 (alpha = 0.01 , N = 60)
= 0.895 (alpha = 0.05 , N = 60)
Data FAIL normality test (alpha = 0.01). Try another transformation.
Warning - The first three homogeneity tests are sensitive to non -normality
and should not be performed with this data as is.

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated B1 statistic = 1.9402 (p-value = 0.8574)
Data PASS B1 homogeneity test at 0.01 level. Continue analysis.
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705 (alpha = 0.05, df = 5)

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX MEAN
1 control 10 9.0000 19.0000 16.2000
2 .65 10 10.0000 22.0000 16.9000
3 1.3 10 11.0000 24.0000 18.0000
4 2.6 10 12.0000 20.0000 17.0000
5 5.2 10 12.0000 22.0000 18.5000
6 10.4 10 10.0000 23.0000 19.4000
Title: lmac
File: lmac Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE SD SEM C.V. %
1 control 9.2889 3.0478 0.9638 18.8134
2 .65 13.6556 3.6953 1.1686 21.8659
3 1.3 12.0000 3.4641 1.0954 19.2450
4 2.6 6.4444 2.5386 0.8028 14.9329
5 5.2 10.7222 3.2745 1.0355 17.6999
6 10.4 15.3778 3.9215 1.2401 20.2137

Title: lmac
File: lmac Transform: NO TRANSFORMATION
Steel's Many -One Rank Test - Ho: Control<Treatment
MEAN IN RANK CRIT. SIG
GROUP IDENTIFICATION ORIGINAL UNITS SUM VALUE DF 0.05
1 control 16.2000
2 .65 16.9000 113.00 75.00 10.00
3 1.3 18.0000 122.00 75.00 10.00
4 2.6 17.0000 112.00 75.00 10.00
5 5.2 18.5000 129.00 75.00 10.00
6 10.4 19.4000 137.00 75.00 10.00
Critical values are 1 tailed ( k = 5 )

r-'- 1
MERITECH, INC. Sample ID N:
Bioassay Samn/e Chain of Cpsfodv
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax [phone]
Emait psmrtechfdtbelleouth.net Web Stte: www.maritech-Iaba.corrt
CLIENT INFORMATION
Ctie t L.�.f�e
Contact Person: %y r `y', d r�
/6 7' ' . /��.Q.��.�� 4'c/
CRY: /J'l•77
Address:
Coltector's Name: Print "nZ'e./(y /�/. -05•10(il,.4 Signature:
TOXICITY TEST INFORMATION
Teat Required: 0 Chronic (7 days) Teat Organism: 0 Cedodaphnle dubia (water flee)
❑ Acute (24-48 hours) 0 Plmephales promelas (fathead minn •w;
❑ Mysidnpsls bahia (shrimp)
IWC: • % Teat Concentrations (if multiple dilutions):
County. Senil ie
Sample Site:
Sample Type: 0 Grab . -Composite
Sampling Time: Start Data
State: /1/C. Zip:
SAMPLE INFORMATION
# of containers:
Start Time: 9:4- !` ) PM
End Date: •-5-1) Y End Time: //)_ ' 61) PM `. CHRONIC TI STS MUST BE
TAKEN AF rE .10:00 AM
m SAMPLE CONTAINERS ARE TO BE COMPLETELY' FULL (no air space), CHILLED AND COVERED 177 1 ICE "'
•
PO#:
NPDES¢: NC
Phone:
Pipe #:
.a�
Comments:
IN 1 FORMATION .
Relinquished by; 77 Date:
` /. CRt
.) G' -� '�icY Tune: i 2 � '_ AM
Received by: Data:
5 -� Time: (tea tS AM P 4�
Relinquished by: (_-_.__--- Date: j v--
Time: AM PM
Received by: Date: Time
AM PM
Sample Temperature rC):
Method of Shipment ��/ pment ❑ UPS 0 Fed EX ❑ Meritech P1*Aip •
M i
Samples shipped on Friday must ha FwIF....w ....... - clearly labeled for Sat ,
try;
Relinquished by:
Received by: Date:
Sample Temperatures CC): /
SAMPLE RECEIVING (Laboratory Use Only)
Time: AM PM
Sample Condition:

ever -.RI 1 VV<f it It\V.
fiIoassav Samole Chain of Custody
• 642 Tamco Rd, Reidsville NC 27320
Phona: 1-336342-4748 Far 1-338-342-1522
Sample ID t
Email• bander:Mtbeildouth.net Web See: www.meritechAabs.com
Client
Contact Person
City:
county:
CLIENT INFORMATION(
!?.-'p,46f / ,/i d ,`,- i A
/( 7cJ (( �,z� ✓� rd
State: `v
POS:
NPDESI: NC
Phone:
Pipe It:
Z4): 9�
Sample Site;
Sample Type:
. Sampling Time:
❑ Grab
AMPLE INFORMATION
c? # of containers:
y
Start Date: t7 — ! - O.) start -rot 9 - Y/) -,4 APM
End Date:
Composite
9_3-e-/)s
End Time: j/e (0 C�M) PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10110 AM
"" SAME CONTAINERS ARE TO BE COMPLETELY FULL (no air spanC ), HILLED AND COVERED WITH
CoUactozs Nems: Print /! 4i://e(/ C%»/' Signature:
Teat Required: 0 Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC: 96
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodephnla dubia (Water flea)
❑ Piinaphabs promelas (fathead minnow)
❑ Mysldops/s bahia (shrimp)
Teat Concentrations (f multiple dllutions):
Relinquished by:
Received by;
Relinquished by:
Received by:
Time:
Time:
Time:
Time:
Method of Shipment ❑ UPS ❑ Fed EX ❑ Meritpch Pick-up
— semen snipped oa FAday meat be Fades and usual be closely labeled ter eebedq .lwry
//: aC PM
Otr—
if a6—PM
/a %c7-0--- AM
PM
g.
NPLE RECEMNO ILaborwtoty Usa Onlv1
Relinquished by:
Received by:
ssnlpta Tsmparetums rC) l l
Dole:
Time:
Sample Condition:
AM PM

,Effluent. Toxi,city Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/27/08
Facility: LMAC
;Laboratory Perfo
;\
Signature
NPDES#: NC0044725 Pipe#: 001 County: SCOTLAND
est : MER ECH, INC
er t r in Res onsiby-L,C) ge
Signature of Laboratory Supervisor
Comments:
Work Order:
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced
19
23
21
20
15
26
27
17
24
17
21
16
Adult (L)ive (D)ead
Effluent %: 2.6%
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
`# Young Produced
0
0
0
1
0
2
0
0
0
0
0
0
Adult (L)ive (D)ead
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = 98.78
% Mortality
Avg.Reprod.
0.00
Control
20.50
Control
33.33
Treatment 2
0.25
Treatment
2
Control CV
19.120%
% control orgs
producing 3rd
brood
100%
PASS
FAIL
X
Check One
off
Control
Treatment 2
Control
Treatment 2
1st sample 1st sample 2nd sample
7.90
8.10
7.76
7.83
7.69
7.77
7.88
7.80
7.82
7.84
7.97
7.76
s s s
t e t e t e
a n a n a n
✓ d r d r d
t t t
1st sample 1st sample 2nd sample
7.43
7.32
7.39
7.29
7.50
7.41
7.46
7.38
7.50
7.21
7.53
6.86
LC50/Acute Toxicity Test
tMortality expressed as %, combining replicates
Complete This For Either Test
Test Start Date: 09/17/08
Collection (Start) Date
Sample 1: 09/15/08 Sample 2: 09/18/08
Sample Type/Duration
Sample 1
Sample 2
Grab
Comp.
Duration
24.7 hrs
25.2 hrs
2nd
1st P/F
D
I S S
L A A
U M M
T P P
Hardness(mg/1)
Spec. Cond.(µmhos)
Chlorine(mg/1)
Sample temp. at receipt(°C)
50
181
733
1515
<0.1
<0.1
1.6
0.7
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
%
Concentration
Mortality
LC50 =
95% Confidence Limits
% -- %
Method of Determination
Moving Average Probit _
Spearman Karber - Other
start/end
Note: Please
Complete This
Section Also
start/end
Control
High
r.,,,
•
pH
Organism Tested: Ceriodaphnia dubia
Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
D.O.

Meritech, Inc.
I. ,, Mini Chronic Pass/FailTest: eriodaphnia dubia Incubator*:
M
:lient: LA-C-- Pipe #: pOS,
% County: p-t0.lck Date Start: q/17 /0F Date End: eJrL yl08-
IPDES #: NC co4N72 S Date / Time of Culture Transfer: 9- /(-66- 8.:304r, Time Start:
p, oZ,i+r+ Time End: ,3 ; /S �'�
ilution Water: Lake Reidsville Date / Time Neonates born: I r 17-6 �j' -))A,1 t 1st Renewal Date: q/1cj l(� 5� Time:
est Organism Source: Tray# 7c:cc` '
9 Age of Neonates at Test Start: `7. 0 hours 2nd Renewal Date: 91zz/0S�' Time: ,-, %, q
tirred / Aerated for D.O.: Randomized: N Culture Tray Temp: Z7.0°C Analyst(s): L Reviewed by:
Control Organism Reproduction Collection (Start) Dates:
2
Day #2 1
# Young Produced
0
0
0
0
0
0
0
0
v
0
Iv
0
11
0
IL
0
Adults Live / Dead
i--
t,
L
L
L
l�
L
L
L
L.
L
L--
Day #5
1
2
# Young Produced
3
9
9
Y
6
i--/
v
5
Iv
3
11
3
IL
3
Adults Live / Dead
L
L
L
L
L
L
L
LLLLL
Day #7
1
# Young Produced
0
%
/
5! 9
��0
1/
7/t f-
4/ j
04 ‘l 7-
lih
I V
s!/
1/1
0L 8,
1
F
Adults Live / Dead
L
L
L
L_
L.
L/
L
L
L
L
Total Produced
al
2-0
Test Sample Organism Reproduction
Effluent %: Z, (p
Day #2
1
2
I.�
11
(6
Percent of Control producing third brood: / OD %
# Young Produced
0
0
0
0
0
0
0
0
00
0
0
Adults Live / Dead
L.
L
1.-
L
L
L_
L
l__
L
L
L
Day #5
1
2
3
# Young Produced
0
0
6
Q
o
d
n
0©
0
0
Adults Live / Dead
1-.
L
L
L
i
L
L
L
L
P
k.
L
Day #7
1
2
10
# Young Produced
0
0
0
I
a
0
6
0-0
1 1
Q
1 L
0
Adults Live / Dead
L
L.,
i--
L
J7
L
r„_
1)
L
27
D
Total Produced
0
0
0
0
0
Tt
Sample 1: 9/ 0f5
Sample Information
Sample 2: MOM
100% pH
G / C?
Duration
Sample 1
-71 L//
C;
2. y. 7 hours
Sample 2
', / l
G
Z.c. Z hours
Batch #
I II
i0
•--`a
j
Sample
�
Sample
2
Transfer Day
Q
2
5
_''
Hardness
(mg/L)
S0
n�
.,, -.•
,
Spec. Cond.
(umhos/cm)
,1
l 1
_'
7.3,
f515
Chlorine
(mg/L)
p
'' ' F
��
a iiic4CLO
.` :y-'
II
2_0•
Receipt Sample
Temp. CC)
``xK-
5 :2.
`
�r'
.
_
1
'1 (17
017
1st Sam le
Control
7,610
g,'o
Sample
7'Yo
783
D.O.
1st Sam le
Control
7'y3
?-32"
Sample
7.37
7. 29
Temp. 1st Sample
Control
ZS,l7
i5.0
Transferred by: Fed by:
Day 0
Day 1 fig
Day2 Kiri-AIL.
Day 3 t'LU
Day 4
Day 5 VIPi�l-lam
Day 6
Terminated by: /jR--
1st Sample
277
7.06
_7 Bo
1st Sample
753
Z'I
7,LAV
7. 36
1st Sample
i5 0
°
2nd Sample
7g
797
7' 7(2
2nd Sample
h
If/
712I
753
(•Sb
2nd Sample
250
Comments:
Samnip
s•(-) LI;:�

Client:
Contact Person:
Address:
City:
County:
MERITECH, INC. Sample ID #. °S'1 \L
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech aC.belisouth.net Web Site: www.meritech-labs.com
CLIENT INFORMATION
L4U riiv t4fi 1fl,4r�( »v /Q;!70,0i
A / e, dkt gd ,v' .
1 G7d1 R'r j'r r r Rd
i>q s/v ) /Vt 2'3Gi"
5GC./14.1/W
State: .44
Zip:
PO#:
NPDES#: NC
Phone:
Pipe #:
Mit
SAMPLE INFORMATION
Sample Site:
Sample Type: ❑ Grab 2/Composite
Sampling Time: Start Date: 9^ /‘-'0 Start Time: 5,. 3 G.7 PM
End Date:
# of containers:
End Time: /0 ; /
PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
•" SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE "'
Collectors Name: Print: . 411 t4•S M 42d /: N
Signature:
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC:
Ok
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:
Received by:
Relinquished by:
Received by:
Ad
SHIPPING INFORMATION
Date: 9-it -Q ' Time:
Date: q-I, -6,' Time:
Date: - t Time:
icmple
Date:nj - f!/� Time:
Temperature (°C):
%/;bb
In0
Method of Shipment: 0 UPS 0 Fed EX ❑ Meritech Pick-up
•. Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery .•
® PM
0 PM
t PM
PM
Relinquished by:
Received by:
SAMPLE RECEIVING (Laboratory Use Only)
Date:
Time: l�S
Sample Temperatures (°C): / ' (ri / / -V / / Sample Condition: .it~CCA,
PM
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC.
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Sample ID #: �, j It 0-7
Email: txmrtech(@belisouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
/ 4 70 / •
State: /17,e'
Zip:
PO#:
i6L- 5-
NPDES#: NC
Phone:
Pipe #:
SAMPLE INFORMATION
Sample Site:
Sample Type: ❑ Grab Composite
Sampling Time: Start Date:
End Date:
9-/9—Q
# of containers:
Start Time: 9 ; 4-Ji(A18!M
End Time:/0 r PM
—♦ CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
"' SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERE ICE "'
Collector's Name: Print: �Z"-C,/(1)," Signaturee�,,�
TOXICITY TEST INFORMATION
Test Required: ❑ Chronic (7 days) Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Acute (24-48 hours) ❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
IWC: % Test Concentrations (if multiple dilutions):
Comments:
Relinquished by:
Received by:
Relinquished by:
Received by:
S IPPING INFORMATION
T
Date: /-/9-c
Date: q: V l� -G "
Date: '1- 11 —t d
Date: _ - i 1
Sample Temperature (°C):
Time: //•l d d ® PM
Time: // d i PM
Time: 1. '-i 5 At PM
Time: AM PM
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery**
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by: /- 7.2
Received by:
Sample Temperatures (°C): � L • �i C . 7 /
Date:
Time:
Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

Effluent Toxicity Statistical Results - Chronic Pass/Fail Date: 09/27/08
Facility: LMAC NPDES#: NO0044725 Pipe#: 001 County:SCOTLAND
Laboratory Performing Test: MERITECH, INC
Reduction: 98.78% CONTROL 2.6% Effluent
# Replicates 12 12
Female Live 12 8
Adult Male 0 0
Adult Dead 0 4
Adult Mortality 0.00% 33.33%
# Neonates 246 3
Mean # Neonates 20.500 0.250
Standard Deviation 3.920 0.622
Coefficient of Variation 19.120%
A = 12
Fisher's Exact Test
B = 12 a = 12
a/A = 1.00 b/B = 0.67
Success is: survival
Critical b value = 8
8 s 8
b = 8
The test concludes that the proportion of survival is signif-
icantly different for the control and the effluent groups.
Test Failed!
Chronic Test FAILS
The survival proportions of the two groups are dissimilar

MERITECH, INC.
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Sample ID #:
Email: txmrtechbellsouth.net Web Site: www.meritech-labs.com
Client:
Contact Person:
Address:
City:
County:
CLIENT INFORMATION
LAM t^ i ry/NPj %i]A7(71'rN let 171
nisi e dkei✓c>1 •ile
lG7v't Rs
rY xAif roc`. 2 5(3•64i ".
S G o f/,aNd State:
PO#:
NPDES#: NC
• •••Phone:,
.Pipe.#: 1.
Zip: 2 ..$34 y
Sample Site:
Sample Type: ❑ Grab Composite
SAMPLE INFORMATION
# of containers: `/
Sampling Time: Start Date: 9- / b'.- 4 ri Start Time: 9...30 AM o t PM
a
End Date: / - /( - O Fi End Time: /O . / G AI / PM
CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
... SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVERED WITH ICE `••
•
Collector's Name: Print: ;A�✓g MS M a.d / Signature: ;'1444
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC:
TOXICITY TEST INFORMATION
Test Organism: ❑ Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
SHIPPING INFORMATION
-.r•
Relinquished by: /-! :/,. , Date: 9-it -o $ Time: //; by CO PM
Received by: " � � � �1,
Date: nj — /4 - ti Time: 1/ o 9 ® PM
Relinquished by: _ Date: Time: 1 { • At PM
Received by: • —'f ` (A Date: / Time: • r • ') `-) M) PM
y 'Sample Temperature (°C):
Method of Shipment: 0 UPS El Fed EX 0 Meritech Pick-up
•• Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery ••
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by:
Received by: Date: Time: 3 - AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy YELLOW = Client copy

MERITECH, INC. Sample ID#:
Bioassay Sample Chain of Custody
642 Tamco Rd, Reidsville NC 27320
Phone: [phone] Fax: [phone]
Email: txmrtech(belisouth.net Web Site: www.meritech-labs.com
/2; L -
CLIENT INFORMATION
Client: L 1-7.,11_ PO#:
Contact Person: emu'-rXr. a=4'J �'�i�,' NPDES#: NC
Address: / 4) 70 / ..420-/// -- 2)-e% -_%-:f r/ Phone:
City: /y i y j7 .- Pipe #:
County: C407G�j 0/ State: i� Zip: ,2
Sample Site:
SAMPLE INFORMTIO
Sample Type: ❑ Grab [t Composite f coq' iners:
i
Sampling Time: Start Date: 9 - / 9- 0 ,' Start Time:
[� 9 : 4g" ;� AM 1
End Date: C%% - / / --z) End Time: /0:cc (AM' P —► CHRONIC TESTS MUST BE
TAKEN AFTER 10:00 AM
•'• SAMPLE CONTAINERS ARE TO BE COMPLETELY FULL (no air space), CHILLED AND COVEREI W ICE "•
Collector's Name: Print: ,17 y.C. 16;1,• 6'/%d,
Test Required: ❑ Chronic (7 days)
❑ Acute (24-48 hours)
Comments:
IWC:
Signature:
TOXICITY TEST INFORMATION
Test Organism: El Ceriodaphnia dubia (water flea)
❑ Pimephales promelas (fathead minnow)
❑ Mysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
Relinquished by:.,--7-7"
Received by:
Relinquished by:
Received by:
S,HIPPING INFORMATION
Date:
Date:
Date:
Date:
Time: //. U 0 0 PM
Time: 1/,' A�df `� PM
Time: I I . PM
Time: AM PM
Sample Temperature (°C):
Method of Shipment: ❑ UPS ❑ Fed EX ❑ Meritech Pick-up
**Samples shipped on Friday must be FedEx and must be clearly labeled for Saturday delivery**
SAMPLE RECEIVING (Laboratory Use Only)
Relinquished by:
Received by: Date: Time: AM PM
Sample Temperatures (°C): / / / Sample Condition:
WHITE = Laboratory copy
YELLOW = Client copy

Attachment 4
Topographic Map of Laurinburg Maxton
Airport Commission WWTP

--.4
., ....-„t„kt.,,,.
• -.4ir" '4 .`
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. ' Commission WWTP
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Topographic Map
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Attachment 5
Treatment Plant Process Layout

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SITE LAYOUT PLAN

Attachment 6
Current NPDES Permit

Michael F. Easley, Governor
State of North Carolina
William G. Ross, Jr., Secretary
Department of Environment and Natural Resources
Alan W. Klimek P.E., Director
Division of Water Quality
May 6, 2005
Mr. Larry Barnett, Executive Director
The Laurinburg — Maxton Airport Commission (LMAC)
P.O. Box 31
Laurinburg, North Carolina 28353
Subject: Issuance of NPDES Permit NC0044725
LMAC Wastewater Treatment Plant (WWTP)
Scotland County
Dear Mr. Barnett:
The Division of Water Quality (the Division) hereby issues this final permit for the subject facility. This
permit is issued to the LMAC pursuant to the requirements of North Carolina General Statute 143-215.1
and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection
Agency dated May 9, 1994, or as subsequently amended.
BOD5 Limits -- Corrections to the DRAFT. BOD 5-day limits appeared in error in your draft
permit. These have been corrected to read 12.0 and 18.0 mg/L (summer monthly average and weekly
average), and 15.0 and 22.5 mg/L (winter monthly average and weekly average) consistent with your
previous permit.
Concerning Weekly Average Ammonia Limits (NH3 as N). As previously issued, this permit
includes Monthly Average ammonia limits for summer and winter flows to protect the receiving stream
from the chronic affects of ammonia. In cooperation with EPA Region 4, the Division shall add new
Weekly Average ammonia limits to permits across the state to further protect the receiving stream from
the acute toxic effects of ammonia (see Effluent Limitations and Monitoring Requirements). The
Division has therefore included new Weekly Average limits to this permit.
Concerning Mercury. Please note that the Division has removed the mercury limit that appeared in the
draft permit because past data show no reasonable potential to exceed the mercury standard. However,
the Lumber River remains impaired for mercury and quarterly monitoring is required. Furthermore, the
LMAC must conduct all future analyses using EPA low-level mercury test Method 1631. There are
currently 11 commercial labs certified by North Carolina to perform Method 1631.
The attached letters provide general background on the low-level method and required clean sampling
techniques (see correspondence dated August 30, 2002 and August 12, 2003). Although some
information needs updating, these letters contain follow-up contact information, should you have
questions.
ATA
NCDENR
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1 800 623-7748

The Laurinburg — Maxton Airport Commission (LMAC)
Wastewater Treatment Plant
Issuance of NPDES Permit NC0044725
Page 2
The LMAC and 155 other facilities in North Carolina are subject to EPA 1631. Mercury
bioaccumulation in fish tissue from the Lumber River Basin has prompted fish consumption advisories
and impaired waterbody designations. A Phase II, Total Maximum Daily Load (TMDL) is currently in
progress for the Lumber and Waccamaw watersheds. The TMDL will utilize low-level effluent data to
determine current and allowable mercury loadings to surface waters. These Phase II programs are
scheduled for completion by Winter 2006.
Annual Priority Pollutant Analyses. Finally, the permittee must provide Priority Pollutant
Analyses (PPA) annually in compliance with statewide requirement of all municipal discharges [see
permit Special Condition A. (5.)].
Renewal Reasonable Potential Analysis. As part of this renewal, the Division conducted Reasonable
Potential Analyses (RPA) on contaminants of concern. These include potential toxicants and metals
considering Significant Industrial Users (SIUs), previous effluent monitoring, and this facility's
Pretreatment Program. This RPA evaluates "reasonable potential" for parameters to exceed North
Carolina's instream Water Quality Standards. Having concluded its review, the Division offers the
following comments and changes to your previous permit (see table).
Permit Renewal -- Recommended Changes/Add
V1�
Parameter :
1_
�.`:.;
s RP
4�;.,-
F=' Cments s/ Renewal Acton '"
om
.rAi fit �"v .` �.. � ��ia ;% i �� r1�' �r
'� ...
•Ammonia
°` °
-,
Added Weekly Average Limits, per EPA requirement; revised
summer/winter limits
Ch'ronium.,
No
Based on corrected data submitted by the Permittee, deleted from the
permit.
Conductivity
—
Retained effluent monitoring; deleted stream monitoring
Copper ::
Yes
Action Level Standard, no TOX problem therefore no limits; add
monitoring 2/Month
Mercury:
—
Not detected by EPA Method 245.1. Mercury advisory in the Lumber
River requires Quarterly monitoring only using EPA Test Method 1631
Oil & Grease.
No
Considering 15 mg/L (BPJ) — deleted monitoring from the permit.
Selenium-
No
Based on a revised database (11 sample points from June 2001 to present),
selenium was not detected. Therefore no "reasonable potential."
Zinc.
Yes
Action Level Standard, no TOX problem therefore no limits; add
monitoring 2/Month
*RP = "Reasonable Potential" to exceed instream Water Quality Standard.
The Division understands that an error occurred in reporting molybdenum in the sludge, according to
your letter of January 7, 2005. However, occurrence of molybdenum found in final bio-solids appears
not to have occurred as an isolated incident. Therefore, the Division has amended Special Condition
A. (3.), discussed in the draft permit, to require that the Permittee contact the Division's
Pretreatment Unit to establish a plan to evaluate the sources of molybdenum upstream of the
WWTP.

The Laurinburg — Maxton Airport Commission (LMAC)
Wastewater Treatment Plant
Issuance of NPDES Permit NC0044725
Page 3
If any parts, measurement frequencies, or sampling requirements contained in this permit are
unacceptable, you have the right to an adjudicatory hearing upon written request within thirty (30)
days after receiving this letter. Your request must be in the form of a written petition conforming to
Chapter 150B of the North Carolina General Statutes, and must be filed with the office of
Administrative Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless
such a demand is made, this permit shall be final and binding.
This permit is not transferable except after notifying, the Division of Water Quality. The Division may
require modification, or revocation and re -issuance of this permit. Please notice that this permit does
not affect your legal obligation to obtain other permits required by the Division of Water Quality, the
Division of Land Resources, the Coastal Area Management Act, or other federal or local
governments.
If you have questions, or if we can be of further service, please contact Joe Corporon at
[[e-mail]] or call [phone], extension 597.
Respectfully,
Alan W. Klimek, P.E.
Enclosure: Final NPDES Permit NC0044725
Correspondence concerning mercury dated August 30, 2002 and August 12, 2003
cc: Central Files
Fayetteville Regional Office, Water Quality Section
NPDES Unit
Pretreatment Unit
Aquatic Toxicology Unit

Permit NC0044725
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
(NPDES)
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
The Laurinburg — Maxton Airport Commission
is hereby authorized to discharge wastewater from an outfall located at the
The Laurinburg — Maxton Airport Commission (LMAC)
Wastewater Treatment Plant (WWTP)
NCSR 1434, east of Laurinburg
Robison County
to receiving waters designated as the Lumber River within the Lumber River Basin in accordance
with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and
IV hereof.
This permit shall become effective June 1, 2005.
This permit and authorization to discharge shall expire at midnight on July 31, 2009.
Signed this day May 6, 2005.
,e7L,
Alan W. Klimek, PE, Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit NC0044725
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are
hereby revoked, and as of this issuance, any previously issued permit bearing this number is
no longer effective. Therefore, the exclusive authority to operate and discharge from this
facility arises under the permit conditions, requirements, terms, and provisions described
herein.
The Laurinburg — Maxton Airport Commission
is hereby authorized:
1. to continue discharging 2.0 MGD of domestic and industrial wastewater from the existing
wastewater treatment facility consisting of activated sludge wastewater treatment
facilities. The treatment system utilizes
• a mechanical bar screen
• two each, 0.5 MGD oxidation ditches with aerators
• three each, secondary clarifiers
• a 60-foot diameter clarifier
• a tertiary filter
• a 73-foot diameter sludge digester
• a 32-foot diameter sludge digester
• chlorination / de -chlorination facilities
• sludge drying beds
• effluent pump station, and
• a stand-by power generating unit.
located at the Laurinburg — Maxton Airport Commission Wastewater Treatment Plant,
NCSR 1434, east of Laurinburg, Robison County, and
2. to discharge from said treatment facility through Outfall 001 at a specified location (see
attached map) into the Lumber River, a waterbody classified as B, Sw; HQW waters
within the Lumber River Basin.

Upstream
Monitoring Point
(at HWY 71)
Outfall 001
Robeson County
(flows south)
• Downstream Monitoring Point
(south @ NCSR 1303)
Laurinburg — Maxton Airport
Commission WWTP
i Receiving Stream: Lumber River Drainage Basin: Lumber liver
[ Latitude: 3-:" -16. I n" N Imiwitude: 79I QI 57" \V
—State Grid / lISGS Quad: 11 21SE / Wakulla, N.C. Sub -Basin: 03-07-51
'\
Permitted Flow: 2.0 N1GD Stream (lass: li, Sw, IIQW
North
Discharge Line — force
main and gravity flow
• (approximate location)
NPDES Permit NC0044725
Robeson County

1
Li —J L J
J
J
J
NPDES Permit No. NC0044725
A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on June 1, 2005 and lasting until expiration, the Permittee is authorized to discharge through Outfall 001.
Such discharges shall be limited and monitored by the Permittee as specified below:
PARAMETERS
t , .
.EFFLUENT.DavinS t :-* .a.,
MONITORING:REQ.UTIREMENTS
Measurement +=
Frequency
rr Sample
t Type , •
;
Sample
z
Monthly,
Average•
Weekly r
Average'
, , Daily, � r
a Maximum
Flow (MGD)
2.0
Continuous
Recording
I or E
BOD, 5 day, 20°C (April 1 — October 31) 2
12.0 mg/L
18.0 mg/L
3/Week
Composite
I, E
BOD, 5 day, 20°C (November 1_ March 31) 2
15.0 mg/L
22.5 mg/L
3/Week
Composite
I, E
Total Suspended Solids (TSS) 2
15.0 mg/L
22.5 mg/L
3/Week
Composite
I, E
NH3 as N (April 1— October 31)
8.0 mg/L
24.0 mg/L
3/Week
Composite
E
NH3 as N (November 1 — March 31)
10.0 mg/L
30.0 mg/L
3/Week
Composite
E
Fecal Coliform (geometric mean)
200 / 100 ml
400 / 100 ml
3/Week
Grab
E
Total Residual Chlorine (TRC) 3
28 µg/L
3/Week
Grab
E
Dissolved Oxygen 4
3/Week
Grab
E
Temperature (°C)
3/Week
Grab
E
Conductivity
3/Week
Grab
E
pH
> 6.0 and < 9.0 standard units
3/Week
Grab
E
Total Phosphorus
Monthly
Composite
E
Total Nitrogen (NO2-N + NO3-N + TKN)
Monthly
Composite
E
Chloride
8,300 pounds/day
12,450 pounds/day
2/Monthly
Composite
E
Total Sodium
6,800 pounds/day
10,200 pounds/day
2/Monthly
Composite
E
Total Cobalt
3.6 pounds/day
5.4 pounds/day
2/Monthly
Composite
E
Total Copper
2/Monthly
Composite
E
Total Zinc
2/Monthly
Composite
E
Total Mercury 5
Quarterly
Grab
E
Chronic Toxicity 6
Quarterly
Composite
E
Temperature °C
Variable?
Grab
U, D
Dissolved Oxygen
Variable?
Grab
U, D
See next page for Table Footnotes

NPDES Permit No. NC0044725
Table Footnotes:
1. Sample Locations: E — Effluent; I — Influent; U — Upstream monitoring at HWY 71; D — Downstream at NCSR 1303.
2. The monthly average effluent BOD5 and Total Suspended Solids concentrations shall not exceed 15 % of the respective influent
value (i.e., 85% removal is required).
3. Total Residual Chlorine (TRC) shall be monitored only if chlorine is used to disinfect.
4. Daily average dissolved oxygen effluent concentration shall not fall below 5.0 mg/L.
5. Mercury -- To facilitate the Lumber River's Phase 11 TMDL process for mercury, the Permittee shall report mercury using sample -
collection criteria and test methods established by EPA Test Method 1631. This permit is subject to Special Condition A.(2.).
6. Chronic Toxicity (Ceriodaphnia) at 2.6 %; quarterly during March, June, September, December; See Special Condition A. (4.)
7. Variable: instream samples shall be collected upstream and downstream 3/week during the summer months of June, July, August, and
September; samples shall be collected weekly during the rest of the year.
Units:
mg/L = milligrams per liter µg/L = micrograms per liter
BOD = biochemical oxygen demand NH3 as N = ammonia as nitrogen ml = milliliter
Effluent shall contain no floating solids or foam visible in other than trace amounts.
A. (2). MERCURY REOPENER.
The Division may re -open this permit to require mercury load limitations, mercury minimization plans, and/or source -water
characterization following the Division's completion of the Phase 11 Mercury TMDL for the Lumber and Waccamaw River watersheds.
A. (3). PRETREATMENT MANAGEMENT PLAN TO EVALUATE THE SOURCE(S) OF MOLYBDENUM IN BIO-SOLIDS.
The Permittee is required to contact the Division's Pretreatment Unit to establish a plan to evaluate the sources of molybdenum upstream
of the WWTP.
1

NPDES Permit No. NC0044725
SUPPLEMENT OT EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
SPECIAL CONDITIONS
A. (4.) CHRONIC TOXICITY PERMIT LIMIT (QUARTERLY)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 2.6 %.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North Carolina
Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or "North Carolina Phase II
Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. The tests will be performed
during the months of, March, June, September, and December. Effluent sampling for this testing shall be performed at
the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure, performed as the first test of any single quarter, results in a failure or ChV below the permit
limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months, as
described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or
subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest concentration
having no detectable impairment of reproduction or survival and the lowest concentration that does have a detectable impairment
of reproduction or survival. The definition of "detectable impairment," collection methods, exposure regimes, and further
statistical methods are specified in the "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -
February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring
Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the pass/fail results and
THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the following address:
Attention:
NC DENR / DWQ / Environmental Sciences Branch
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30 days after
the end of the reporting period for which the report is made. Test data shall be complete, accurate, include all supporting
chemical/physical measurements and all concentration/response data, and be certified by laboratory supervisor and ORC or
approved designate signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is
employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit
number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the form.
The report shall be submitted to the Environmental Sciences Branch at the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be required
during the following month. Should any test data from this monitoring requirement or tests performed by the North Carolina
Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document (such as minimum control
organism survival, minimum control organism reproduction, and/or appropriate environmental controls)
shall constitute an invalid test and will require immediate follow-up testing, to be completed no later than the
last day of the month following the month of initial monitoring.

NPDES Permit No. NC0044725
A. (5.) ANNUAL PRIORITY POLLUNT ANALYSES
The permittee shall perform effluent Priority Pollutant (PPA) scans in accordance with 40 CFR Part 136 for all parameters listed in the
_ attached table. The Permittee shall sample approximately annually except to provide seasonal variation (perhaps in different calendar
quarters). Unless otherwise indicated, metals shall be analyzed as "total recoverable."
1
Ammonia (as N)
Trans-1,2-dichloroethylene
Bis (2-chloroethyl) ether
Chlorine, total residual (TRC)
1, I -dichloroethylene
Bis (2-chloroisopropyl) ether
Dissolved oxygen
1,2-dichloropropane
Bis (2-ethylhexyl) phthalate
Nitrate/Nitrite _
1,3-dichloropropylene
4-bromophenyl phenyl ether
Kjeldahl nitrogen
Ethylbenzene
Butyl benzyl phthalate
Oil and grease
Methyl bromide
2-chloronaphthalene
Phosphorus
Methyl chloride
4-chlorophenyl phenyl ether
Total dissolved solids
Methylene chloride
Chrysene
Hardness
1,1,2,2-tetrachloroethane
Di-n-butyl phthalate
Antimony
Tetrachloroethylene
Di-n-octyl phthalate
Arsenic
Toluene
Dibenzo(a,h)anthracene
Beryllium
1,1,1-tichloroethane
1,2-dichlorobenzene
Cadmium
1,1,2-trichloroethane
1,3-dichlorobenzene
Chromium
Trichloroethylene
1,4-dichlorobenzene
Copper
Vinyl chloride
3,3-dichlorobenzidine
Lead
Acid' extractable Compounds ti ?
Diethyl phthalate
Mercury
P-chloro-m-creso
Dimethyl phthalate
Nickel
2-chlorophenol
2,4-dinitrotoluene
Selenium
2,4-dichlorophenol
2,6-dinitrotoluene
Silver
2,4-dimethylphenol
1,2-diphenylhydrazine
Thallium
4,6-dinitro-o-cresol
Fluoranthene
Zinc
2,4-dinitrophenol
Fluorene
Cyanide
2-nitrophenol
Hexachlorobenzene
Total phenolic compounds
4-nitrophenol
Hexachlorobutadiene
Vol_atde1Orgamc Compounds . } ` ,ll
Pentachlorophenol
Hexachlorocyclo-pentadiene
Acrolein
Phenol
Hexachloroethane
Acrylonitrile
2,4,6-trichlorophenol
Indeno(1,2,3-cd)pyrene
Benzene
Base -neutral Compounds <
Isophorone
Bromoform
Acenaphthene
Naphthalene
Carbon tetrachloride
Acenaphthylene
Nitrobenzene
Chlorobenzene
Anthracene
N-nitrosodi-n-propylamine
Chlorodibromomethane
Benzidine
N-nitrosodimethylanune
Chloroethane
Benzo(a)anthracene
N-nitrosodiphenylamine
2-chloroethylvinyl ether
Benzo(a)pyrene
Phenanthrene
Chloroform
3,4 benzofluoranthene
Pyrene
Dichlorobromomethane
Benzo(ghi)perylene
1,2,4-trichlorobenzene
1,1-dichloroethane
Benzo(k)fluoranthene
1,2-dichloroethane
Bis (2-chloroethoxy) methane
The Permittee shall report test results within 90 days of sample collection to the Division in DWQ Form- DMR-PPA1 or in a form approved by the
Director. The report shall be submitted to the following address:
NC DENR / DWQ / Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

NPDES Permit Requirements
Page 1 of 16
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events.
3/Week
Samples are collected three times per week on three separate calendar days.
Act or "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended, 33 USC 1251, et. seq.
Annual Average
The arithmetic mean of all "daily'discharges" of a pollutant measured during the calendar year. In the case of fecal
coliform, the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system, which
is not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Quarter
One of the following distinct periods: January through March, April through June, July through September, and
October through December.
Composite Sample
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 ml in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The
Director may designate the most appropriate method (specific number and size of aliquots necessary, the time
interval between grab samples, etc.) on a case -by -case basis. Samples may be collected manually or automatically.
Composite samples may be obtained by the following methods:
(1) Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24 ,hour
period of discharge and combined proportional to the rate of flow measured at the time of individual sample --
collection, or
(3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period
with the time intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow recorder and
totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the
expected total daily flow at the treatment system, or
(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at
a constant time interval. This method may only be used in situations where effluent flow rates vary
less than 15 percent. The grab samples shall be taken at intervals of no greater than 20 minutes apart
during any 24-hour period and must be of equal size and of no less than 100 milliliters. Use of this method
requires prior approval by the Director.
Version 6/20/2003

NPDES Permit Requirements
Page 2 of 16
In accordance with (4) above, influent grab samples shall not be collected more than once per hour.
Effluent grab samples shall not be collected more than once per hour except at wastewater treatment systems
having a detention time of greater than 24 hours. In such cases, effluent grab samples may be collected at
intervals evenly spaced over the 24-hour period that are equal in number of hours to the detention time of the
system in number of days. However, the interval between effluent grab samples may not exceed six hours nor
the number of samples less than four during a 24-hour sampling period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as
the total mass of the pollutant discharged over the day. The "daily discharge" concentration comprises the mean
concentration for a 24-hour sampling period as either a composite sample concentration or the arithmetic mean of all
grab samples collected during that period. (40 CFR 122.3)
Daily Maximum
The highest "daily discharge" during the calendar month.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit. The Division expects that sampling shall be conducted on weekdays except where holidays or other
disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week
for any permit parameter(s), that requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWQ or "the Division"
The Division of Water Quality, Department of Environment and Natural Resources.
EMC
The North Carolina Environmental Management Commission.
Facility Closure
The cessation of wastewater treatment at a permitted facility, or the cessation of all activities that require coverage
under the NPDES. Completion of facility closure will allow this permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N = the number of individual values. For purposes of
calculating the geometric mean, values of "0" (or "< [detection level]") shall be considered =1.
Grab Sample
Individual samples of at least 100 ml collected over a period of time not exceeding 15 minutes. Grab samples can be
collected manually. Grab samples must be representative of the discharge (or the receiving stream, for instream
samples).
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
Instantaneous flow measurement
A measure of flow taken at the time of sampling, when both the sample and flow will be representative of the total
discharge.
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NPDES Permit Requirements
Page 3 of 16
Monthly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal
coliform, the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Quality.
Quarterly Average (concentration limit)
The average of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable,
or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
Upset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by
operational error, improperly. designed treatment facilities, inadequate treatment facilities, lack of preventive
maintenance, or careless or improper operation.
Weekly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of fecal
coliform, the geometric mean of such discharges.
Section B. General Conditions
1. Duty to Comply _
The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation
of the Clean Water Act and is grounds for enforcement action; for permit termination, revocation and reissuance,
or modification; or denial of a permit renewal application [40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants and with standards for sewage sludge use or disposal established under
section 405(d) of the Clean Water Act within the time provided in the regulations that establish these
standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been
modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates section 301, 302, 306, 307, 308, 318 or 405 of the
Act, or any permit condition or limitation implementing any such sections in a permit issued under section
402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8)
of the Act, is subject to a civil penalty not to exceed $25,000 per day for each violation. [40 CFR 122.41 (a)
(2)]
c. The Clean Water Act provides that any person who negligently violates sections 301, 302, 306, 307, 308, 318, or
405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under
section 402 of the Act, or any requirement imposed in a pretreatment program approved under section
402(a)(3) or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a
negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of
violation, or by imprisonment of not more than 2 years, or both. [40 CFR 122.41 (a) (2)]
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NPDES Permit Requirements
Page 4 of 16
g•
d. Any person who knowing violates such sections, or such conditions or limitations is subject to criminal
penalties of $5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In
the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal
penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or both.
[40 CFR 122.41 (a) (2)]
e. Any person who knowingly violates section 301, 302, 303, 306, 307, 308, 318 or 405 of the Act, or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,
and who knows at that time that he thereby places another person in imminent danger of death or serious
bodily injury, shall, upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not
more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment
violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than
30 years, or both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction
of violating the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined
up to $2,000,000 for second or subsequent convictions. [40 CFR 122.41 (a) (2)]
f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes § 143-215.6A]
Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302,
306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are
not to exceed $10,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed
$25,000. Penalties for Class II violations are not to exceed $10,000 per day for each. day during which the
violation continues, with the maximum amount of any Class II penalty not to exceed $125,000. [40 CFR
122.41 (a) (3)]
2. Duty to Mitigate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit which has a reasonable likelihood of adversely affecting human health or the environment
[40 CFR 122.41 (d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II. C. 4), "Upsets" (Part II. C. 5) and "Power
Failures" (Part II. C. 7), nothing in this permit shall be construed to relieve the Permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309
of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as
fish kills, even though the responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor
any infringement of Federal, State or local laws or regulations [40 CFR 122.41 (g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
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7. Severability
The provisions of this permit are severable. If any provision of this permit, or the application of any provision of this
permit to any circumstances, is held invalid, the application of such provision to other circumstances, and the remainder
-7 of this permit, shall not be affected thereby [NCGS 150B-23].
8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the
Permit Issuing Authority upon request, copies of records required by this permit [40 CFR 122,41 (h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit, the
Permittee must apply for and obtain a new permit [40 CFR 122.41 (b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the Permittee shall submit such information, forms, and
fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration date.
Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will subject
the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified
[40 CFR 122.41 (k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation, or (b) the manager of one or more manufacturing, production, or
operating facilities, provided, the manager is authorized to make management decisions which govern the
operation of the regulated facility including having the explicit or implicit duty of making major capital
investment recommendations, and initiating and directing other comprehensive measures to assure long
term environmental compliance with environmental laws and regulations; the manager can ensure that
the necessary systems are established or actions taken to gather complete and accurate information for
permit application requirements; and where authority to sign documents has been assigned or delegated
to the manager in accordance with corporate procedures .
(2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official [40 CFR 122.22].
b.. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a. above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
1. The authorization is made in writing by a person described above;
2. The authorization specified either an individual or a position having responsibility for the overall
operation of the regulated facility or activity, such as the position of plant manager, operator of a well or
well field, superintendent, a position of equivalent responsibility, or an individual or position having
overall responsibility for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position.); and
3. The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.22]
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c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate
because a different individual or position has responsibility for the overall operation of the facility, a new
authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director
prior to or together with any reports, information, or applications to be signed by an authorized
representative [40 CFR 122.22]
d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification [40 CFR 122.22]:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41 (f)].
13: Permit Modification. Revocation and Reissuance. or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules, and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code, Subchapter 2H .0100; and North Carolina General Statute 143-215.1 et. al.
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 2H.0105 (b) (4)
may cause this Division to initiate action to revoke the permit.
Section C. Operation and Maintenance of Pollution Controls
1. Certified Operator
Upon classification of the permitted facility by the Certification Commission, the Permittee shall employ a
certified water pollution control treatment system operator in responsible charge (ORC) of the water pollution
control treatment system. Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the water pollution control treatment system by the Certification Commission. The
Permittee must also employ one or more certified Back-up .ORCs who possess a currently valid certificate of the
type of the system. Back-up ORCs must possess a grade equal to (or no more than one grade less than) the grade
of the system [15A NCAC 8G.0201].
The ORC of each Class I facility must:
> Visit the facility at least weekly
> Comply with all other conditions of 15A NCAC 8G.0204.
The ORC of each Class II, III and IV facility must
➢ Visit the facility at least daily, excluding weekends and holidays
➢ Properly manage and document daily operation and maintenance of the facility
➢ Comply with all other conditions of 15A NCAC 8G.0204.
Once the facility is classified, the Permittee shall submit a letter to the Certification Commission designating the
operator in responsible charge:
a. Within 60 calendar days prior to wastewater being introduced into a new system
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b. Within 120 calendar days of:
> Receiving notification of a change in the classification of the
new ORC and back-up ORC
> A vacancy in the position of ORC or back-up ORC.
2. Proper Operation and Maintenance
The Permittee shall at all times provide the operation and maintenance resources necessary to operate the existing
facilities at optimum efficiency. The Permittee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or used by the Pernuttee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the Permittee to install
and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the
permit [40 CFR 122.41 (e)].
system requiring the designation of a
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.41
(c)]
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations [40 CFR 122.41 (m) (2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not *subject to the
provisions of Paragraphs b. and c. of this section.
b.
Notice [40 CFR 122.41 (m). (3)]
(1) Anticipated bypass. If the Permittee
notice, if possible at least ten days
anticipated quality and effect of the byp
(2) Unanticipated bypass. The Permittee
II. E. 6. (24-hour notice).
knows in advance of the need for a bypass, it shall submit prior
before the date of the bypass; including an evaluation of the
ass.
shall submit notice of an unanticipated bypass as required in Part
c. Prohibition of Bypass
(1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the. use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance; and
(C) The Permittee submitted notices as required under Paragraph b. of this section.
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system -wide collection system
permit associated with the treatment facility.
The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects, if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c.
(1) of this section.
(3)
5. Upsets
a. Effect of an upset [40 CFR 122.41 (n) (2)]: An upset constitutes an affirmative defense to an action
brought for noncompliance with such technology based permit effluent limitations if the requirements of
paragraph b. of this condition are met. No determination made during administrative review of claims that
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noncompliance was caused by upset, and before an action for noncompliance, is final administrative action
subject to judicial review.
b. Conditions necessary for a demonstration of upset: A Permittee who wishes to establish the
affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or
other relevant evidence that:
(1) An upset occurred and that the Permittee can identify the cause(s) of the upset;
(2) The Permittee facility was at the time being properly operated; and
(3) The Permittee submitted notice of the upset as required in Part II. E. 6. (b) (B) of this permit.
(4) The Permittee complied with any remedial measures required under Part II. B. 2. of this permit.
d. Burden of proof [40 CFR 122.41 (n) (4)]: The Permittee seeking to establish the occurrence of an
upset has the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States. The Permittee
shall comply with all existing Federal regulations governing the disposal of sewage sludge. Upon promulgation of
40 CFR Part 503, any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR 503. The
Permittee shall comply with applicable 40 CFR 503 Standards for the Use and Disposal of Sewage Sludge (when
promulgated) within the time provided in the regulation, even if the permit is not modified to incorporate the
requirement. The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 2H.0124 —
Reliability) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures
either by means of alternate power sources, standby generators or retention of inadequately treated effluent.
Section D. Monitoring and Records
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and nature of
the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and time that is
characteristic of the discharge over the entire period the sample represents. All samples shall be taken at the
monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted
by any other wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority [40 CFR 122.41 (j)].
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and reported on a
monthly Discharge Monitoring Report (DMR) Form (MR 1, 1.1, 2, 3) or alternative forms approved by the
Director, postmarked no later than the 28th day following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these, and all other reports required herein, shall be submitted to the following address:
NC DENR / Division of Water Quality / Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
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3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The
devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge
volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once -through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in Part I
of this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to
NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to
Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act (as Amended), and 40 CFR 136; or in
the case of sludge use or disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless
other test procedures have been specified in this permit [40 CFR 122.41].
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must be
reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are
determined capable of achieving minimum detection and reporting levels below permit discharge requirements,
then the most sensitive (method with the lowest possible detection and reporting level) approved method must
be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any
monitoring device or method required to be maintained under this permit shall, upon conviction, be punished by
a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or
by both. If a conviction of a person is for a violation committed after a first conviction of such person under this
paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more
than 4 years, or both [40 CFR 122.41].
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge
use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40
CFR 503), the Permittee shall retain records of all monitoring information, including.
> all calibration and maintenance records
> all original strip chart recordings for continuous monitoring instrumentation
> copies of all reports required by this permit
> copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time [40 CFR
122.41].
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record
the following information [40 CFR 122.41]:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
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e. The analytical techniques or methods used; and
f. The results of such analyses.
8. Inspection and Entry
The Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting
as a representative of the Director), upon the presentation of credentials and other documents as may be required
by law, to;
a. Enter upon the Permittee's premises where a regulated facility or activity is located or conducted, or where
records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices,
or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the Clean Water Act, any substances or parameters at any location [40 CFR 122.41 (i)].
Section E Reporting Requirements
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge
of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall
constitute a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or
additions to the permitted facility [40 CFR 122.41 (1)]. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
122.29 (b); or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to
notification requirements under 40 CFR 122.42 (a) (1). •
c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices,
and such alternation, addition or change may justify the application of permit conditions that are different
from or absent in the existing permit, including notification of additional use or disposal sites not reported
during the permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to.the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit [40 CFR 122.41 (1) (2)].
4. Trans fers
This permit is not transferable to any person except after notice to the Director. The Director may require
modification or revocation and reissuance of the permit to document the change of ownership. Any such action
may incorporate other requirements as may be necessary under the Clean Water Act [40 CFR 122.41 (1) (3)].
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41 (1) (4)].
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II. D. 2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation and reporting of the data submitted on the DMR.
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6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances. The written
submission shall contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the
noncompliance [40 CFR 122.41 (1) (6)].
b. The Director may waive the written report on a case -by -case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at [phone], [phone] or [phone].
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported.under Part II. E. 5 and 6. of this permit at
the time monitoring reports are submitted. The reports shall contain the information listed in Part II. E. 6. of
this permit [40 CFR 122.41 (1) (7)].
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit
such facts or information [40 CFR 122.41 (1) (8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following.
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; or any. other unusual
circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass directly to receiving
waters without treatment of all or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33
USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division of Water Quality. As required by the Act, effluent data shall not be considered confidential.
Knowingly making any false statement on any such report may result in the imposition of criminal penalties as
provided for in NCGS 143-215.1 (b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this permit, including
monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of
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not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both
[40 CFR 122.41].
12. Annual Performance Reports
Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an annual
report to the Permit Issuing Authority and to the users/customers served by the Permittee (NCGS 143-215.1C).
The report shall summarize the performance of the collection or treatment system, as well as the extent to which
the facility was compliant with applicable Federal or State laws, regulations and rules pertaining to water quality.
The report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon
which annual period is used for evaluation.
PART III
OTHER REQUIREMENTS
Section A. Construction
The Permittee shall not commence construction of wastewater treatment facilities, nor add to the plant's treatment
capacity, nor change the treatment process(es) utilized at the treatment plant unless the Division has issued an
Authorization to Construct (AtC) permit. Issuance of an AtC will not occur until Final Plans and Specifications for
the proposed construction have been submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall, upon written notice from the Director of the Division of Water Quality, conduct groundwater
monitoring as may be required to determine the compliance of this NPDES permitted facility with the current
groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR 122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis, of any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the
following "notification levels";
(1) One hundred micrograms per liter (100 µg/L);
(2) Two hundred micrograms per liter (200 µg/L) for acrolein and acrylonitrile; five hundred micrograms
per liter (500 µg/L) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and one milligram per liter
(1 mg/L) for antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine or
infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the
highest of the following "notification levels";
(1) Five hundred micrograms per liter (500 µg/L);
(2) One milligram per liter (1 mg/L) for antimony;
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Evaluation of Wastewater Discharge Alternatives
The Permittee shall evaluate all wastewater disposal alternatives and pursue the most environmentally sound
alternative of the reasonably cost effective alternatives. If the facility is in substantial non-compliance with the terms
and conditions of the NPDES permit or governing rules, regulations or laws, the Permittee shall submit a report in
such form and detail as required by the Division evaluating these alternatives and a plan of action within 60 days of
notification by the Division.
Section E. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system
covered by this permit. The Division may require specific measures during deactivation of the system to prevent
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—1 adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit
continue at the permitted facility.
PART IV
SPECIAL CONDITIONS FOR MUNCIPAL FACILITIES
Section A. Publicly Owned Treatment Works (POTWs)
All POTWs must provide adequate notice to the Director of the following:
1. Any new introduction of pollutants into the POTW from an indirect discharger which would be subject to
section 301 or 306 of CWA if it were directly discharging those pollutants; and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger
as influent to that POTW at the time of issuance of the permit.
3. For purposes of this paragraph, adequate notice shall include information on (1) the quality and quantity of
effluent introduced into the POTW, and (2) any anticipated impact of the change on the quantity or quality
of effluent to be discharged from the POTW.
Section B. Municipal Control of Pollutants from Industrial Users.
• 1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from
industries using the municipal system may be present in the Permittee's discharge. At such time as
sufficient information becomes available to establish limitations for such pollutants, this permit may be
revised to specify effluent limitations for any or all of such other pollutants in accordance with best
practicable technology or water quality standards.
2. Under no circumstances shall the Permittee allow introduction of the following wastes in the waste
treatment system:
a. Pollutants which create a fire or explosion hazard in the POTW, induding, but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees
Centigrade using the test methods specified in 40 CFR 261.21;
b. Pollutants which will cause corrosive structural damage to the POTW, but in no case Discharges
with pH lower than 5.0, unless the works is specifically designed to accommodate such Discharges;
c.. Solid or viscous pollutants in amounts which .will cause obstruction to the flow in the POTW
resulting in Interference;
d. Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a Discharge at a flow
rate and/or pollutant concentration which will cause Interference with the POTW;
e. Heat in amounts which will inhibit biological activity in the POTW resulting in Interference, but in
no case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C
(104°F) unless the Division, upon request of the POTW, approves alternate temperature limits;
f. Petroleum oil, nonbiodegradable cutting oil, or products of mineral oil origin in amounts that will
cause interference or pass through; _
g. Pollutants which result in the presence of toxic gases, vapors, or fumes within the POTW in a
quantity that may cause acute worker health and safety problems;
h. Any trucked or hauled pollutants, except at discharge points designated by the POTW.
3. With regard to the effluent requirements listed in Part I of this permit, it may be necessary for the
Permittee to supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to
ensure compliance by the Permittee with all applicable effluent limitations. Such actions by the Permittee
may be necessary regarding some or all of the industries discharging to the municipal system.
4. The Permittee shall require any industrial discharges sending influent to the permitted system to meet
Federal Pretreatment Standards promulgated in response to Section 307(b) of the Act. Prior to accepting
wastewater from any significant industrial user, the Permittee shall either develop and submit to the
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Division a Pretreatment Program for approval per 15A NCAC 2H .0907(a) or modify an existing
Pretreatment Program per 15A NCAC 2H .0907(b).
5. This permit shall be modified, or alternatively, revoked and reissued, to incorporate or modify an approved
POTW Pretreatment Program or to include a compliance schedule for the development of a POTW
Pretreatment Program as required under Section 402(b)(8) of the Clean Water Act and implementing
regulations or by the requirements of the approved State pretreatment program, as appropriate.
Section C. Pretreatment Programs
Under authority of sections 307(b) and (c) and 402(b)(8) of the Clean Water Act and implementing regulations 40
CFR Part 403, North Carolina General Statute 143-215.3 (14) and implementing regulations 15A NCAC 2H
.0900, and in accordance with the approved pretreatment program, all provisions and regulations contained and
referenced in the Pretreatment Program Submittal are an enforceable part of this permit.
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the Clean
Water Act, the Federal Pretreatment Regulations 40 CFR Part 403, the State Pretreatment Regulations 15A
NCAC 2H .0900, and the legal authorities, policies, procedures, and financial provisions contained in its
pretreatment program submission and Division approved modifications there of. Such operation shall include
but is not limited to the implementation of the following conditions and requirements:
1. Sewer Use Ordinance (SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program.
2. Industrial Waste Survey (IWS)
The Permittee shall update its Industrial Waste Survey (IWS) to include all users of the sewer collection
system at least once every five years.
3. Monitoring Plan
The Permittee shall implement a Division approved Monitoring Plan for the collection of facility specific
data to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of
specific pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required
by Part II, Section D, and Section E.5.).
4. Headworks Analysis (HWA) and Local Limits
The Permittee shall obtain Division approval of a Headworks Analysis (HWA) at least once every five
years, and as required by the Division. Within 180 days of the effective date of this permit (or any
subsequent permit modification) the Permittee shall submit to the Division a written technical evaluation
of the need to revise local limits (i.e., an updated HWA or documentation of why one is not needed) [40
CFR 122.42]. The Permittee shall develop, in accordance with 40 CFR 403.5(c) and 15A NCAC 2H ..0909,
specific Local Limits to implement the prohibitions listed in 40 CFR 403.5(a) and (b) and 15A NCAC 2H
.0909.
5. Industrial User Pretreatment Permits (IUP) & Allocation Tables
In accordance with NCGS 143-215.1, the Permittee shall issue to all significant industrial users, permits for
operation of pretreatment equipment and discharge to the Permittee's treatment works. These permits
shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special
conditions, and compliance schedules as necessary for the installation of treatment and control
technologies to assure that their wastewater discharge will meet all applicable pretreatment standards and
requirements. The Permittee shall maintain a current Allocation Table (AT) which summarizes the results
of the Headworks Analysis (HWA) and the limits from all Industrial User Pretreatment Permits (IUP).
Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA.
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6. Authorization to Construct (A to C)
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable
industrial users for the construction or modification of any pretreatment facility. Prior to the issuance of
an AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to
comply with all Industrial User Pretreatment Permit (IUP) limitations.
7. POTW Inspection & Monitoring of their SIUs
The Permittee shall conduct inspection, surveillance, and monitoring activities as described in its Division
approved pretreatment program in order to determine, independent of information supplied by industrial
users, compliance with applicable pretreatment standards. The Permittee must:
a. Inspect all Significant Industrial Users (SIUs) at least once per calendar year; and
b. Sample all Significant Industrial Users (SIUs) at least twice per calendar year for all permit -
limited pollutants, once during the period from January 1 through June 30 and once during the
period from July 1 through December 31, except for organic compounds which shall be sampled
once per calendar year;
8. SIU Self Monitoring and Reporting
The Permittee shall require all industrial users to comply with the applicable monitoring and reporting
requirements outlined in the Division approved pretreatment program, the industry's pretreatment permit,
or in 15A NCAC 2H .0908.
9. Enforcement Response Plan (ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b) and (c) of the Clean Water Act (40 CFR 405 et. seq.), prohibitive
discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 2H .0909, and specific local limitations.
All enforcement actions shall be consistent with the Enforcement Response Plan (ERP) approved by the
Division.
10. Pretreatment Annual Reports (PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 2H .0908. In lieu of submitting
annual reports, Modified Pretreatment Programs developed under 15A NCAC 2H .0904 (b) may be
required to meet with Division personnel periodically to discuss enforcement of pretreatment requirements
and other pretreatment implementation issues.
For all other active pretreatment programs, the Permittee shall submit two copies of a Pretreatment Annual
Report (PAR) describing its pretreatment activities over the previous twelve months to the Division at the
following address:
NC DENR / DWQ / Pretreatment Unit
1617 Mail Service Center
Raleigh, NC 27699-1.617
These reports shall be submitted according to a schedule established by the Director and shall contain the
following
a.) Narrative
A brief discussion of reasons for, status of, and actions taken for all Significant Industrial
Users (SIUs) in Significant Non -Compliance (SNC);
b.) Pretreatment Program Summary (PPS)
A pretreatment program summary (PPS) on specific forms approved by the Division;
c.) Significant Non -Compliance Report (SNCR)
The nature of the violations and the actions taken or proposed to correct the violations on
specific forms approved by. the Division;
d.) Industrial Data Summary Forms (IDSF)
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Monitoring data from samples collected by both the POTW and the Significant Industrial
User (SIU). These analytical results must be reported on Industrial Data Summary Forms
(IDSF) or other specific format approved by the Division;
e.) Other Information
Copies of the POTW's allocation table, new or modified enforcement compliance schedules,
public notice of SIUs in SNC, and any other information, upon request, which in the
opinion of the Director is needed to determine compliance with the pretreatment
implementation requirements of this permit;
11 Public Notice
The Permittee shall publish annually a list of Significant Industrial Users (SIUs) that were in Significant
Non -Compliance (SNC) as defined . in the Permittee's Division approved Sewer Use Ordinance with
applicable pretreatment requirements and standards duringthe previous twelve month period. This list
shall be published within four months of the applicable twelve-month period.
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results, along
with support information including general records, water quality records, and records of industrial impact
on the POTW.
13. Funding and Financial Report
The Permittee shall maintain adequate funding and staffing levels to accomplish the objectives of its
approved pretreatment program.
14. Modification to Pretreatment Programs.
Modifications to,. the approved pretreatment program including but not limitedto local limits
modifications, POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan
modifications, shall be considered a permit modification and shall be governed by 15 NCAC 2H .0114 and
15A NCAC 2H .0907.
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