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Home My WebLink AboutWQ0032016_Monitoring - 07-2021_20210826DWR - NonDischarge Monitoring Report Submittal NORTH CAROLINA Ertrlranmrrttat Quaffty Monitoring Report Submittal Permit Number #* Name of Facility:* Month:* July Report Information Type* GW-59 WQ0032016 Rose Hill Plantation Year:* 2021 Upload Document* Rose Hill (WQ0032016) GW- 3.46MB 59 (with lab results) July 2021.pdf FDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* kreese@rpbsystenns.com Name of Submitter:* Kimber Reese Signature: Date of submittal: 8/26/2021 This will be filled in automatically Initial Review Reviewer: Giri, Poonam a Is the project number correct?* WQ0032016 Is the monitoring report accepted? * r Yes r No Regional Office * Asheville Accepted Date: 8/30/2021 GW-59A COMPLIANCE REPORT FORM Permit # WQ0032.O1 CA (Submit one each monitoring period with GW 59 forms.) I Enter date monitoring results be submitted after the established were due. ( BT51/2.j ) Will this monitoring report (GW-59 and GW-59A) YES ,NOO due date? 2 Was any required information missing on the GW-59 report forms? VES NO/ V IF the answer to question 1 or 2 is "YES'', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. YES NO 4 Are any monitored constituents equal to or above the established standards? YES i, If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). Welt#I - p H (p.2. Wei 14-2- fN5.G 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO', monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO If the answer to question 7 is "YES', If the answer to question 7 is required to determine the impact describe those actions in the space provided below. "NO'; contact the Regional Office within 90 days; an evaluation may be the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this form with GW-59 forms for required I hereby acknowledge that the report (Compliance Report GW-59A) portion (GW-59A) of the monitoring report should sign below and submit this wells to the address provided at the top of the current GW-59 form. above information was evaluated and the information submitted in this is true and complete to the best of my know edge. r Signature of Permitteo (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Rose Hill Plantation Development, LLC Mail original and 1 copy to: Permit Name (if different): Facility Address: 3041 New Leicester Highway Leicester NC 28748 Contact Person: Bob Barr Well Location/Site Name: Well # 1(MW A on GW-lb) County Buncombe Telephone#: (828) 251-1900 No. of wells to be sampled: 3 (from Permit) DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Non -Discharge NPDES Expiration Date: 2/28/2022 UIC Other W00032016 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑■ Other: Surface Irrigation SAMPLING INFORMATION WELL ID NUMBER (from Permit): Weil Depth: 69 ft, Depth to Water Level 82546: 32.28 Well # 1 Upgradient ft. below measuring point Measuring Point is 2.5 ft. above land surface Date sample collected: 7/29/2021 Well Diameter: 2 in. Screened Interval: 49 ft. Relative M.P, Elevation: to 69 ft. ft. Volume of water pumped/bailed before sampling: gallons Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: 0 YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 8/11/2021 Laboratory Name: Pace Analytical PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 Coliform: MF Fecal 31s1s <1 /100mL Nitrate (NO3J as N oos2o <0.040 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.074 (Note. Use MPN method for highly turbid samples) Dissolved Solids:Total 70soo 50.0 pH (Lab) 00403 TOC 00680 <1.0 Chloride 00940 1.3 Arsenic 01002 Grease and Oils 00552 Phenol 32730 Sulfate 00945 Specific Conductance 00095 Total Ammonia 00510 <0.10 (Ammonia Nitrogen: NH3as N', Ammonia Nitrogen, Total) TKN as N 00625 mg/L units mg/L mg/L ug/L mg/L ug/L mg/L µMhos mg/L mg/L Orthophosphate 70507 Ai -Aluminum o1105 Ba - Barium 01007 Ca - Calcium 00916 Cd - Cadmium 01027 Chromium: Total 01034 Cu - Copper 01042 Fe - Iron 01045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 00927 Mn - Manganese 01055 Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L uglL mg/L ug/L ug1L mg/L mg/L uglL uglL FIELD ANALYSES: pH 00400: 6.2 units Temp. 00010: 19.1 °C Spec. Cond. 00094: 48.6 µMhos Odor 00085: Appearance Pb - Lead 01051 Zn - Zinc a1092 Slight Musty Clear Certification No. 40 ug/L mg1L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑■ No (0) VOC 7873 , method # , method # , method # , method # If WELL WAS DRY at time of sampling, check here. For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg1L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Fri 4 Robert P. Barr / Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 06-07-2018 Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Pnnt Clearly or Type Facility Name: Rose Hill Plantation Development, LLC Mail original and 1 copy to: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Permit Name (if different): Facility Address: 3041 New Leicester Highway Leicester NC 28748 Contact Person: Bob Barr Well Location/Site Name: Well # 2(MW B on GW-1 b) County Buncombe Telephone#: (828) 251-1900 No. of wells to be sampled: 3 (from Permit PERMIT Number: Non -Discharge NPDES Expiration Date: 2/28/2022 U!C Other WQ0032016 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Spray Field ❑ Remediation: Infiltration Gallery ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑■ Other: Surface Irrigation SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 30 ft, Depth to Water Level 82546: 12.10 Well # 2 downgradient ft. below measuring point Measuring Point is 2.5 ft. above land surface Volume of water pumped/bailed before sampling: Samples for metals were collected unfiltered: • YES Date sample collected: 7/29/2021 Well Diameter: 2 in. Screened Interval: 10 ft- Relative M.P. Elevation: gallons ❑ NO and field acidified: ❑■ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 8/11/2021 Laboratory Name: Pace Analytical PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 Coliform: MF Fecal 31616 <1 /100mL Coliform: MF Total 31504 (Note: Use MPN method for highly turbid samples) Dissolved Solids:Total 70300 <25.0 pH (Lab) 00403 TOC oo68o <1.0 Chloride oo940 1.8 Arsenic 01002 Grease and Oils 00552 Phenol 32730 Sulfate 00945 Specific Conductance 00095 Total Ammonia o0610 <0.10 (Ammonia Nitrogen; NH3as N, Ammonia Nitrogen, Total) TKN as N 00625 /100mL mg/L units mg/L mg/L ug/L mg/L ug/L mg/L ttMhos mg/L mg/L Nitrate (NO3) as N 00620 0.39 Phosphorus: Total as P 00665 0.056 Orthophosphate 70507 Al -Aluminum 011os Ba - Barium 01007 Ca - Calcium 00918 Cd - Cadmium 01027 Chromium: Total 01034 Cu - Copper 01042 Fe - Iron o1045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 00927 Mn - Manganese 01055 Ni - Nickel 01067 to 30 ft. ft. mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug!L mg/L mg/L ug/L uglL FIELD ANALYSES: pH o0400: 5.6 units Spec. Cond. 00094; 33 Temp. 00010: 18.6 °c MMhos Odor 00085: Slight Appearance Pb - Lead 01051 Zn - Zinc 01092 Clear Certification No. 40 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) 0 No (0) VOC 7873 , method # , method # , method # , method # If WELL WAS DRY at time of sampling, check here: For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Robert P. Barr / Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 06-07-2018 ar- Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Rose Hill Plantation Development, LLC Mail original and 1 copy to: Permit Name (if different): Facility Address: 3041 New Leicester Highway Leicester NC 28748 Contact Person: Bob Barr Well Location/Site Name: Well # 3 County Buncombe Telephone#: (828) 251-1900 No. of wells to be sampled: 3 (from Permit) DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Non -Discharge NPDES Expiration Date: 2/28/2022 UIC Other WQ0032016 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Spray Field ❑ Remediation: ❑ Remediation: Infiltration Gallery ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑■ Other: Surface Irrigation SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: 14 ft. Depth to Water Level 82546: 5.00 Well # 3 Date sample collected: 7/29/2021 Well Diameter: 2 ft. below measuring point Screened Interval: 4 Measuring Point is 0 ft. above land surface Volume of water pumped/bailed before sampling: Samples for metals were collected unfiltered: ❑■ YES FIELD ANALYSES: in. pH [loam 6.6 units Temp. ooalo: 22•2 °C ft. to 14 ft. Spec. Cond. 00094: 102.7 µMhos Relative M.P. Elevation: ft. gallons El NO and field acidified: ❑■ YES ❑ NO Odor 00085: Sulfur Appearance cloudy If WELL WAS DRY at time of sampling, check here. n LABORATORY INFORMATION Date sample analyzed: s/11/2021 Laboratory Name: Pace Analytical PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 Coliform: MF Fecal 31616 <1 mg/L Nitrite (NO2) as N oos15 /100mL Nitrate (NO3) as N 00620 <0.040 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.68 (Note: Use MPN method for highly turbid samples) Dissolved Solids:Total 70300 81.0 pH (Lab) 00403 Orthophosphate 70507 mg/L Al - Aluminum 01105 units Ba - Barium 01007 TOC 00680 <1.0 mg/L Ca - Calcium oasis mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 Chloride 00940 5.1 Specific Conductance 00095 Total Ammonia o0610 <0.10 (Ammonia Nitrogen; NH3as N: Ammonia Nitrogen, Total) TKN as N 00625 µMhos K - Potassium 00937 mg/L Mg - Magnesium 00927 Mn - Manganese 01ass Ni - Nickel 01067 mglL mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead 01os1 Zn - Zinc o1092 Certification No. 40 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑■ No (0) VOC 7873 , method # , method # , method # , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory, I am aware that there are significant penalties for submitting false information, including the possibility of tines and impriso trn •nt for knowing violations. Robert P. Barr / Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 06-07-2018 ,'I Signature of Permittee (or Authorized Agent) 9 t?T u (Date) aceAnalytfical www.yacelabs.conr ANALYTICAL RESULTS Project: Rose Hill MWs Pace Project No.: 92552398 Pace Analytical Services, LLC 2226 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-1 Lab ID: 92552398001 Collected: 07/29/21 12:00 Received: 07/29/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 08/04/21 08:31 Collected By Ryan Byes 1 08/04/21 08:31 Collected Date 7/29/21 1 08/04/21 08:31 Collected Time 12:00 1 08/04/21 08:31 pH 6.2 Std. Units 1 08/04/21 08:31 Temperature 19.1 deg C 1 08/04/21 08:31 Static Water Level 32.28 feet 1 08/04/21 08:31 Specific Conductance 48.6 umhos/cm 1 08/04/21 08:31 Turbidity 7.9 NTU 1 08/04/21 08:31 Odor Sllight 1 08/04/21 08:31 musty Appearance Clear 1 08/04/21 08:31 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 50.0 mg/L 25.0 1 08/03/21 11:03 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.7 Std. Units 0.10 1 08/09/21 15:06 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services -Asheville Fecal Coliforms ND CFU/100 mL 1.0 1 07129/21 17:11 07/30/21 15:48 350.1 Ammonia Analytical Method: EPA 350,1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/10/21 13:55 7664-41-7 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Nitrate ND mg/L 0.040 1 07/30/21 01:08 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.074 mg/L 0.050 1 08/09/21 13:03 08/10/21 00:47 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 1.3 mg/L 1.0 1 08/10/21 16:22 16887-00-6 5310E TOC Analytical Method: SM 5310B-2011 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 08/03/21 12:29 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/11/2021 12:24 PM without the written consent of Pace Analytical Services, LLC. H3 Page 4 of 20 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Rose Hill MWs Pace Project No.: 92552398 Pate Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-2 Lab ID: 92552398002 Collected: 07/29/21 12:15 Received: 07/29/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 08/04/21 08:40 Collected By Ryan Byas 1 08/04/21 08:40 Collected Date 7/29/21 1 08/04/21 08:40 Collected Time 12:15 1 08/04/21 08:40 pH 5.6 Std. Units 1 08/04/21 08:40 Temperature 18.6 deg C 1 08/04/21 08:40 Static Water Level 12.10 feet 1 08/04/21 08:40 Specific Conductance 20.7 umhos/cm 1 08/04/21 08:40 Turbidity 30.9 NTU 1 08/04/21 08:40 Odor None 1 08/04/21 08:40 Appearance Slightly 1 08/04/21 08:40 cloudy 2540C Total Dissolved Solids Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville ND mg/L 25.0 1 08/03/21 18:46 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 5.7 Std. Units 0.10 1 08/09/21 15:09 H3 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 92220-2006 Pace Analytical Services - Asheville Fecal Coliforms ND CFU/100 mL 1.0 1 07/29/21 17:11 07/30/21 15:48 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/10/21 12:56 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 0.39 mg/L 0.040 1 07/30/21 01:20 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.056 mg/L 0.050 1 08/09/21 13:03 08/10/21 00:48 7723-14-0 4500 Chloride Chloride 5310E TOC Total Organic Carbon Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville 1.8 mg/L 1.0 1 08/10/21 16:12 16887-00-6 Analytical Method: SM 5310B-2011 Pace Analytical Services -Asheville ND mg/L 1.0 1 08/03/21 12:46 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/11/2021 12:24 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Rose Hill MWs Pace Project No.: 92552398 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-3B Lab ID: 92552398003 Collected: 07/29/21 12:40 Received: 07/29/21 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 08/04/21 0B:42 Collected By Ryan Byes 1 08/04/21 08:42 Collected Date 7/29/21 1 08/04/21 08:42 Collected Time 12:40 1 08/04/21 08:42 pH 6.6 Sid. Units 1 08/04/21 08:42 Temperature 22.2 deg C 1 08/04/21 08:42 Static Water Level 5.00 feet 1 08/04/21 08:42 Specific Conductance 102.7 umhos/cm 1 08/04/21 08:42 Turbidity 572 NTU 1 08/04/2108:42 Odor Sulfur 1 08/04/21 08:42 Appearance Cloudy 1 08/04/21 08:42 2540C Total Dissolved Solids Total Dissolved Solids 9040 pH pH at 25 Degrees C Analytical Method: SM 2540C-2011 Pace Analytical Services - Asheville 81.0 mg/L 25.0 1 08103/21 18:46 Analytical Method: EPA 9040C Pace Analytical Services -Asheville 6.5 Std. Units 0.10 1 08/09/21 15:16 H3 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Asheville Fecal Coliforms ND CFU/100 mL 2.0 2 07129/21 17:11 07/30)21 15:48 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia NO mg/L 0.10 1 08/10/21 12:59 7664-41-7 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate ND mg/L 0.040 1 07/30)21 01:22 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.68 mg/L 0.050 1 08/09/21 13:03 08/10/21 00:49 7723-14-0 4500 Chloride Chloride 5310B TOC Total Organic Carbon Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville 5.1 mg/L 1.0 1 08/10/21 16:13 16887-00-6 Analytical Method: SM 5310B-2011 Pace Analytical Services -Asheville ND mg/L 1.0 1 08/03/21 13:02 7440- 44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/11/2021 12:24 PM without the written consent of Pace Analytical Services, LLC. 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