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Home My WebLink AboutWQ0034806_Compliance Schedule_20210823oQk isle W U-71-{' 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes E9 no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes X no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for moo` iiv ty, ignitability, and reactivity: Laboratory�� and Date of analysis: -a Passed corrosivity test: 09 yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: '91 yes ❑ no. Flashpoint:*?)qC) OF (> 140°F) Passed reactivity test: W yes ❑no. HCN: L I mg/kg (<250) & H2S: //• mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mgfi) TCLP Parameter Limit (mg/1) Result NO) Arsenic 5.0 41.0 Hexachlorobenzene 0.13 lO,OSa Barium 100.0 41.0 Hexachloro-1,3-Butadiene 0.5 LO,OSD Benzene 0.5 LQ,O( Hexachloroethane 3.0 1D.0So Cadmium 1.0 .41.0 Lead 5.0 41. p Carbon Tetrachloride 0.5 <O, O 1 Lindane 0.4 L Q,{300,1 Chlordane 0.03 �[p, D Z Mercury 0.2 40,0002 Chlorobenzene 100.0 40,01 Methoxychlor 10.0 40,dD0 Chloroform 6.0 4-10,01 Methyl Ethyl Ketone 200.0 L0.05• Chromium 5.0 L/, p Nitrobenzene 2.0 L0.060 m-Cresol 200.0 L O. pS-D Pentachlorophenol 100.0 G b. 25za o-Cresol 200.0 40,V!rV Pyridine 5.0 <o'c5b p-Cresol 200.0 LD o5p Selenium 1.0 .4 /, D Cresol 200.0 [D, DSp Silver 5.0 .4/, O 2,4-D 10.0 -'O'CO3 Tetrachloroethylene 0.7 LO,O( 1,4-Dichlorobenzene 7.5 /-G-V!5b Toxaphene 0.5 L0.05 1,2-Dichloroethane 0.5 L O,.o l Trichloroethylene 0.5 40,0( 1,1-Dichloroethylene 0.7 GOO) 2,4,5-Trichlorophenol 400.0 4 t?!;o 2,4-Dinitrotoluene 0.13 40,010 2,4,6-Trichlorophenol 2.0 LQ,OSO Endrin 0.02 [Q 0006 2,4,5-TP (Silvex) 1.0 40. UO3 Heptachlor and its Hydroxide 0.008 1_0.0005 Vinyl Chloride 0.2 .40.0( FORM: RSC 06-16 Page 2 of 5 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road,. Manteo, NC 27954 • 252.473.5702 Lab/Fax L 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info a)environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Aug 20, 2021 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020D08 Attention: Wesley Wooten Report #: 2021-12892 Project ID: Oak Island Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-32255 Site: Sludge 812/2021 7:30 AM Solid/Sludge Wesley Wooten Test Method Results Date Chlordane (TCLP) SW B45 Method 0081 B/3510 <0.02 mg/L 08/09/2021 Endrin (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 08/09/2021 Heptachlor (TCLP) SW B46 Method 8081B/3510 <0,0005 mg/L 08/09/2021 Heptachlor epoxide (TCLP) SW 046 Method 8081 B1351 0 <0.0005mg/L 08109/2021 Lindane (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 08/09/2021 Methoxychlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 08109/2021 Toxaphene (TCLP) SW 846 Method 80818/351a <0.05 mg/L 08/09/2021 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021 2,4,5-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 08/06/2021 2,4,6-Trichlorophenol(TCLP) SW 846 method 8270/3510 <0.050mg/L 08/06/2021 2,4-Dinitrotoluene (TCLP) SW 846 method 827013510 <0.050 mg/L 08/06/2021 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 08/06/2021 Hexachloro-1,3-butadiene(TCLP) SW 845 method 8270/3510 <0.050mg/L 08/06/2021 Hexachlorobenzene(TCLP) SW 846 method827013510 <0.050mg/L 08/06/2021 Hexachloroethane (TCLP) SW B45 method 8270/3510 <0.050 mg/L 08/0612021 m + p-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 08/06/2021 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021 o-Cresol (TCLP) SW 646 method B270/3510 <0.050 mg/L 08/06/2021 Pentachlorophenol (TCLP) SW 846 method 827CIM510 <0.250 mg/L 08/06/2021 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021 2,4,5-TP(TCLP) SW846 Method 8151A <0.003mg/L 08/10/2021 2,4-D(TCLP) SW846 Method 6151A <0.003mg/L 08/10/2021 1,1-Dichloroethylene(TCLP) SW846 Method 826015030 <0.01mg/L 08/05/2021 1,2-Dichloroethane(TCLP) SW846 Method 826015030 <0.01mg/L 08/05/2021 Benzene (TCLP) SW845 Method 8260/5030 <0.01 mg/L 08/05/2021 Carbon Tetrachloride (TCLP) SW046 Method 8260/5030 <0.01 mg/L 08/05/2021 Report #:: 2021-12892 Pagel or4 71 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Aug 20, 2021 8155 Malpass Corner Road Customer PO M Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report#: 2021-12892 Project ID: Oak Island Chlorobenzene (TCLP) SW846 Method828015030 <0.01 mg/L 08/05/2021 Chloroform (TCLP) SW846 Method0280/5030 <0.01mg/L 08/05/2021 Methyl ethyl ketone (TCLP) SW846 Method 826DIS030 <0.05 mg/L 08/0512021 Tetrachloroethylene (TCLP) SW846 Method 8280/5030 <0.01 mg/L 08/05/2021 Trichloroethylene (TCLP) SW846 MethodB28015030 <0.01 mg/L 08/05/2021 Vinyl Chloride (TCLP) SW645 Method 8260/5030 <0,01 mg/L 08/05/2021 RCI Cyanide Sulfide Ignitability Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc SM 4500 CN D SM 4500 S D SW 046 method 1010 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 2001 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 Nitrate+Nitrite-Nitrogen EPA353.2 Total Solids (°/,) SM 2540 s pH SM 4500 H 8 Result estimated. Analyzed out of 15 minutes hold time. Ammonia Nitrogen SM 4500 NH3 C <1 mg/kg 11.8 mg/kg >190°F 3790 mg/kg <27.4 mg/kg <13.7 mg/kg 43800 mg/kg 17.3 mg/kg 239 mg/kg <13.7 mg/kg 2660 mg/kg <13.7 mg/kg <13.7 mg/kg 2460 mg/kg <13.7 mg/kg 2610 mg/kg 1270 mg/kg 12.6 rri 2.07 % 8.41 units 11900 mg/kg 08/03/2021 08/09/2021 08/05/2021 08/03/2021 08/09/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 08/03/2021 0810312021 08/0512021 08/02/2021 08/0512021 08/05/2021 Report #:: 2021-12892 Page 2 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ^ 910.392.0223 Lab • 910.392.4424 Fax 710 Bow5ertown Road, blanteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Higliway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoLenvironmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Aug 20, 2021 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report#: 2021-12892 Project ID: Oak Island Total Kjeldahl Nitrogen (TKN) SM45000rg0 20200mg/kg 08/05/2021 Total Phosphorus SM4500PF 5310mg/kg 08/09/2021 Mercury SW8467471B 1.30mg/kg 08/06/2021 TCLP Metals Arsenic EPA200.7 <1.Omg/L 08/09/2021 Barium EPA200.7 <1.0mg/L 08109/2021 Cadmium EPA200.7 <1.0mg/L 08/09/2021 Chromium EPA200.7 <1.Omg/L 08/09/2021 Lead EPA 200.7 <1.0 mg/L 08/0912021 Selenium EPA200.7 <1.0mg/L 08/09/2021 Silver EPA200.7 <1.0mg/L 08/09/2021 Mercury EPA 245.1 <0.0002 mg/L 08/06/2021 Lab ID Sample ID: Collect Daterrime Matrix Sampled by 21-32256 Site: 1 8/2/2021 7:35 AM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (% Fecal Density Lab ID Sample ID: 21-32257 Site:2 Test Total Solids (%) Fecal Density SM 2540 B SM 9221C E-2014 Collect Date/Time 8/2/2021 7:36 AM Method SM 2540 B SM 9221 C E-2014 1.39% 08/02/2021 6763MPN/g 08/02/2021 Matrix Sampled by Solid/Sludge Wesley Wooten Results Date Analyze( 1.94 % 08/02/2021 5671 MPN/g 08/02/2021 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-32258 Site: 3 8/2/2021 7:37 AM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) SM2540B 1.75% 08/02/2021 Fecal Density SM 9221C E-2014 20000MPN/g 08/02/2021 Report #:: 2021-12892 Page 3 of 4 Environmental Chemists, Inc. AM" 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(ajenvironmentalchemists.com Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Date of Report: Aug 20, 2021 Customer PO #: Customer ID: 14020008 Report #: 2021-12892 Project ID: Oak Island Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-32259 Site: 4 8/2/2021 7:38 AM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.03 % 08/02/2021 Fecal Density SM 9221C E-2014 8375 MPN/g 08/02/2021 Lab ID Sample ID: 21-32260 Site:5 Test Total Solids (%) Fecal Density Lab ID Sample ID: 21-32261 Site:6 Collect Datefrime 8/2/2021 7:39 AM Method SM 2540 8 SM 9221C E-2014 Collect Date/Time 8/2/2021 7:40 AM Matrix Sampled by Solid/Sludge Wesley Wooten Results Date Analyze) 1.84 % 08/02/2021 5979MPN/g 08/02/2021 Matrix Sampled by Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.71 % 08/02/2021 Fecal Density SM 9221C E-2014 4620MPN/g 08/02/2021 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-32262 Site: 7 8/2/2021 7:41 AM Solid/Sludge Wesley Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.64 % 08/02/2021 Fecal Density SM 9221C E-2014 4818 MPN/g 08/02/2021 Comment: Sludge „ residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. ► Reviewed by: , U�M�Qi�J ReportB:: 2021-12B92 Page of Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Clientl.wt5 Date: Z a/ Report Number. - Ia q Z Receipt of sample: ECHEM Pickup ❑ Client Delivery 111 11PS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO rff N/A I. Were custody seals present on the cooler? ❑ YES ❑ NO JR N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES 10 NO 3. If temperature of coolerexceeded VC, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? 5. Were sample ID's listed on the COC? 6. Weresamples ID's listed on sample containers? 7. Were collection date and time listed on the COC? W 8. Were tests to be performed listed on the COC? 9. Did samples arrive in proper containers for each test? 10Dilve in good condition for each test? 10( YESOON 1. Was adequate sample volume available?' 12. Were samples receved within proper holding time for requested tests? ❑ YES13. Were acid preserved samples received at a pH of <2? ❑ YES14. Were cyanide samples received at a pH >12? ❑ YES15. Were sulfide samples received at a pH >9? ❑ YES16. ❑ YES17. ❑ YES18. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *` Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatilesare pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): HzSO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samp!es Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and lime: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 N 'I 0) CT A W N (p 3 cn i n m y 3 1 v —I N 7 a VI � r A M 1 i C) 0 3 i c I• M o M m o 0 a c N I S a (4 Ci m Sample Type Composite Li C) G) Ci O n G) Ci G) 0 G) 0 O C) O (7) or Grab Container (P or G) 0 o' Chlorine m mg/L 3 I .ti 6'• 4' "� , .. �. J\ LAB to NUMBER — u s j( NONE HCL H2SO4 71 N ; m X HNO3 C NAOH N c' X X X X X X X THIO Z co OTHER ( (D (D (D N (D (D (D C_ 0 t 01 N 0) 01 01 N t (D (D (D CD (D (D (D r t V=i N N N ton N N ( z D o e e r1 (1) U) (n Vl cn (A cn C N N C n 3 m IT 1D m o 9 N m z Z C) 0 G z p 09 0 �000 O r' OM z m m T 1 1 Z p Z a M _0 m D z Z 0 A y= 0r c D Z y O o = "ym V C m f N Mpl i T �\ o z Z N J 0` � IT 'A 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100%non-municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes 9 no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes N no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: ro Laboratory 0-Or^and Date of analysis:el- Passed corrosivity test: 59 yes ❑ no. pH: s.u. (2 <pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint:VC0 OF (> 140°F) Passed reactivity test: 9 yes ❑no. HCN: 41 mg/kg (<250) & H2S: 0.15 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/7) TCLP Parameter Limit (Mg/7) Result (M917l Arsenic 5.0 41.0 Hexachlorobenzene 0.13 ,40'cso Barium 100.0 .41.0 Hexachloro-1,3-Butadiene 0.5 40,0S0 Benzene 0.5 G 0, p 1 Hexachloroethane 3.0 Z0, o SD Cadmium 1.0 41. O Lead 5.0 G 1 .O Carbon Tetrachloride 0.5 ,2,01 Lindane 0.4 e0.D005 Chlordane 0.03 LO,O;L Mercury 0.2 Ca.P0o2 Chlorobenzene 100.0 G D.01 Methoxychlor 10.0 40.00O5r Chloroform 6.0 40.01 Methyl Ethyl Ketone 200.0 <o.05 Chromium 5.0 41.O Nitrobenzene 20 <O,OSO m-Cresol 200.0 LO,p!�D Pentachlorophenol 100.0 40.,2$p o-Cresol 200.0 .4p,0S0 Pyridine 5.0 Gp,psv p-Cresol 200.0 G O, 05 a Selenium 1.0 < 1, D Cresol 200.0 ,fo, pl.5p Silver 5.0 </. O 2,4-D 10.0 4 0, 003 Tetrachloroethylene 0.7 40,01 1,4-Dichlorobenzene 7.5 LO,p50 Toxaphene 0.5 <p,OS 1,2-Dichloroethane 0.5 t0.o1 Trichloroethylene 0.5 .40,01 1,1-Dichloroethylene 0.7 40.01 2,4,5-Trichlorophenol 400.0 < 0,.a!50 2,4-Dinitrotoluene 0.13 < 0.05o 2,4,6-Trichlorophenol 2.0 /-ays0 Endrin 0.02 V. d oos 2,4,5-TP (Silvex) 1.0 4O,op-3 Heptachlor and its Hydroxide 0.008 fq, O 005 Vinyl Chloride 0.2 < O, 01 FORM: RSC 06-16 Page 2 of 5 Environmental Chemists Inc. g gg 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL& CONSULTING CHEMISTS info(Senvironmentalchemists.com Onslow Water & Sewer Authority Date of Report: Jul 20, 2021 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report#: 2021-10651 Project ID: Summer House WRF Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-26545 Site: SH Digestor 6/29/2021 7:23 AM Solid/Sludge Kary Herndon Test Method Results Date Chlordane (TCLP) SW 846 Method 8081 B1351 0 <0.02mg/L 07/09/2021 Endrin (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 07/09/2021 Heptachlor (TCLP) SW 845 Method 8081B/3510 <0.0005 mg/L 07/09/2021 Heptachlor epoxide (TCLP) SW 846 Method 8081B/3510 <0.0005mg/L 07/09/2021 Lindane(TCLP) SW 846 Method 808 1 B/3510 <0.0005mg/L 07/09/2021 Methoxychlor (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 07/0912021 Toxaphene(TCLP) SW 846 Method 8081 B1351 0 <0.05mg/L 07/09/2021 1,4-Dichlorobenzene(TCLP) SW 846 method 8270/3510 <0.050mg/L 07/08/2021 2,4,5-Trichlorophenol(TCLP) SW 046 method 827013510 <0.050mg/L 07/08/2021 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 2,4-Dinitrotoluene(TCLP) SW 846 method827013510 <0.050mg/L 07/08/2021 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 Hexachloro-1,3-butadiene(TCLP) SW 846 method82701351D <0.050mg/L 07/08/2021 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 07/08/2021 Hexachlorcethane (TCLP) SW 046method 8270/3510 <0.050mg/L 07/08/2021 m + p-Cresol (TCLP) SW 846 method 8270/3610 <0.050 mg/L 07/08/2021 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 o-Cresol (TCLP) SW 848 method 8270/3510 <0.050 mg/L 07/08/2021 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 07/08/2021 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 2,4,5-TP(TCLP) SW846 Method 8151A <0.003mg/L 07/1312021 2,4-D(TCLP) SW846Method 8151A <0.003mg/L 07/13/2021 1. 1 -Dichloroethylene (TCLP) SW046 Method 8260/5030 <0.01 mg/L 07/02/2021 1,2-Dichloroethene(TCLP) SW846 Method 8260/5030 <0.01mg/L 07/02/2021 Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021 Report #:: 2021-10651 Page 1 of 2 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 1,- 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info ez.-environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Jul 20, 2021 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2021-10651 Project ID: Summer House WRF Chlorobenzene(TCLP) SW846 Method026015030 <0.01mg/L 07/02/2021 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021 Methyl ethyl ketone (TCLP) SW846 Method8260/5030 <0.05mg/L 07/02/2021 Tetrachloroethylene(TCLP) SW846 Method8260/5030 <0.01mg/L 07/02/2021 Trichlorcethylene(TCLP) SW848 Method 826015030 <0.01mg/L 07/02/2021 Vinyl Chloride (TCLP) SW846 Method826015030 <0.01 mg/L 07/02/2021 RCI Cyanide SM4500CN0 Reporting limit elevated due to matrix interference. <1mg/kg 07/07/2021 Sulfide SM 4500 S D 0.15 mg/kg 07/06/2021 Ignitability SW 846 method 1010 >200 OF 07/20/2021 pH Result estimated. SW 845 Method 90450 Analyzed out of 15 minutes hold time. 6.33 units 06/30/2021 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 07/09/2021 Barium EPA 200.7 <1.0mg/L 07/09/2021 Cadmium EPA200.7 <1.Omg/L 07/09/2021 Chromium EPA 200.7 <1.0mg/L 07/09/2021 Lead EPA 200.7 <1.0 mg/L 07/09/2021 Selenium EPA 200.7 <1.0mg/L 07/09/2021 Silver EPA 200.7 <1.Omg/L 07/09/2021 Mercury EPA245.1 <0.0002mg/L 07/14/2021 Comment: Reviewed by: kw1k,01ri, Report M. 2021-10651 Page 2 or 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington NC 28405 910.392.0223 Sample Receipt checklist Client: VJ rt Date: 1291 Z) Report Number: ZI "I0(c J I Receipt of sample: E HEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES JLJ No N/A 2. If custodyseals were present, were they intact/unbroken? Original temperature upon receipt a,l C Corrected temperature upon receipt How temperature taken` ❑ Temperature Blank Against Bottles R Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor 'co .0 YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date d t' I' YES ❑ NO 8. an ime tsted on the COC? Were tests to be performed listed on the COC? YES ❑ NO 9, Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? L— vrr YEy F _ .. ❑ NO I __ 12. � _yw:_ n_•••�,i� wmio vv ono vm! Were samples received within proper holding time for ❑ YES ❑ NO 13. requested tests? Were acid preserved samples received at a pH of Q? ❑ YES Cl NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ` Cl YES ❑ NO 17. Were Sul fide/Cyanice received at a chlorine residual of co.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? TOC,/Vo�atles are H checf:ed at h P m,� oianalysis and recorded on the benchsh=et " Ba,Leda samples a': check=d fp- Cnlonve at time of analysis and recorded on the b2rch5'1=,t Sample Preservation: Sample(s) by adding (circle one): Time of preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) were received incorrectly preserved and were adjusted accordingly H;50, HNO3 HCl NaOH If more than one preservative is needed notate in comment: hatnw 'V9:=: `.J:�'y i:J'n=` 53: Vi:' i,^Im'] 3re•Y i0' h[J�•�r[ip afei'_'J2j i3l'.'J es cc rain are, 5 —p e.. a, - aate ano arie: 'c C•JSt^T_ _.. 6S i- ._ h?i ❑a:IG?J Volatiles Samples) were received with headspace .iMMEN I r DOC. QA.002 Rev 1 tz ONWASA Sending Facility: Summer House WRF Twining Rose Lane Holly Ridge, NC 28445 Phone: 910.389.8511 Project Manager: Kary Herndon Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Subcontracted Laboratory: SUBCONTRACT ORDER :r LfeJ nu Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-02.23 Fax:(910) 392-4424 NODEMR: DWQ CERT H"MON k 9a NCDHHS: DU CERMUTrOM x 37719 Work Order: Q212701 Summer House WRF Sample ID: Q212701.01 SH Dlgestor S2 Sampled.• 0512912021 07:23 Sampled by: Aram Nemdon Analysis Due Expires EnviroChem Lab ID pH, SW846 07/09/2021 06/29/2021 07:40 Analysis Due Expires EnvlroChem Lab ID Sulfide colorlmetrlc 07/09/2021 07/13/2D21 07:23 Analysis Due Expires EnvlroChem Lab ID Cn-335.4 07/09/2021 07/13/2021 07:23 Analysis Due Expires EnvlroChem Lab ID I ".... Due Expires EnvlroChem Lab ID rnarys's Due Expires EnvlroChem Lab ID Expires EnvlroChem Lab ID Due Expires EnvlroChem Lab ID TCLP Metals 07/09/2021 12/26/2021 07:23 Analysis Due Expires EnvlroChem Lab ID a8260/5030 07J09/2021 12/26/2021 07:23 Analysis An Due Expires EnviroChem Lab ID SW846 8153A Containers Supplied: P 1 liter (A) 07/69/2021 12/26/2021 07:23 AG 1L (B) AG 11. (C) AG 1L (D) EnviroChem Report No: / 6 " s-/ f02r1 21 Is Dv Relinquished By Dale ReZeived By Date I /' Page 1 of 1 2 -5�W a-._ S loro W tzF 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes CS no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes Is no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: 1e0 Laboratoryt%X. and Date of analysis: Passed corrosivity test: PS yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: 91 yes ❑ no. Flashpoint:> M; OF (> 140°F) Passed reactivity test: ® yes Ono. HCN:.7•09 mg/kg (<250) & HrS: a-, `o'`o' mg/kg (<500) TCLP Parameter Limit (m8/1) Result (mSn) TCLP Parameter Limit im%/1) Result (m8/1) Arsenic 5.0 41,p Hexachlorobenzenc 0.13 40.0,50 Barium 100.0 4.O Hexachloro-1,3-Butadiene 0.5 X p,o$D Benzene 0.5 <p, O 1 Hexachloroethane 3.0 < 0.05C Cadmium 1.0 Lead 5.0 E1.0 Carbon Tetrachloride 0.5 <p,0/ Lindane 0.4 <0,0005 Chlordane 0.03 < (), 02 Mercury 0.2 C 0, 0002 Chlorobenzene 100.0 .4'D,01 Methoxychlor 10.0 Chloroform 6.0 <0,01 Methyl Ethyl Ketone 200.0 <O,OS Chromium 5.0 41.0 Nitrobenzene 2.0 <O,D,SO m-Cresol 200.0 40, osv Pentachlorophenol 100.0 < O• aS0 o-Cresol 200.0 <o,o50 Pyridine 5.0 <O,OgO p-Cresol 200.0 <V,Ol�p Selenium 1.0 G1.0 Cresol 200.0 40.o50 Silver 5.0 1,p 2,4-D 10.0 <0.003 Tetmchloroethylene 0.7 <p,o j 1,4-Dichlorobenzene 7.5 40.0sp Toxaphene 0.5 <O.0!5 1,2-Dichloroethane 0.5 <p, p/ Trichloroethylene 0.5 <O, 01 1,1-Dichloroethylene 0.7 S0.01 2,4,5-Trichlorophenol 400.0 <p,050 2,4-Dinitrotoluene 0.13 <O,OSQ 2,4,6-Trichlorophenol 2.0 <O,OSo Endrin 0.02 <0,0p045 2,4,5-TP(Silvex) 1.0 <0,003 Heptachlor and its Hydroxide 0.008 4r, 00 d Vinyl Chloride 0.2 e p, o ) FORM: RSC 06-16 Page 2 of 5 Environmental Chemists, Inc. O 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCa-environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Jul 21, 2021 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report#: 2021-10653 Project ID: Swansboro WRF Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-26548 Site: Digester 6/29/2021 6:30 AM Solid/Sludge Randal Riggs Test Method Results Date Chlordane (TCLP) SW 845 Method 8081B13510 <0.02mg/L 07/09/2021 Endrin (TCLP) SW 846 Method 60818/3510 <0.0005 mg/L 07/09/2021 Heptachlor (TCLP) SW S46 Method 80818/3510 <0.0005 mg/L 07/09/2021 Heptachlor epoxide (TCLP) SW 846 Method 0081B13510 <0.0005 mgll- 07/0912021 Lindane(TCLP) SW 846 Method 8081B/3510 <0.0005mg/L 07/09/2021 Methoxychlor (TCLP) SW 846 Method 8081813510 <6.0005 mg/L 07/09/2021 Toxaphene(TCLP) SW 846 Method80818/3510 <0.05mg/L 07/09/2021 1,4-Dichlorobenzene (TCLP) SW 846 method 02701351a <0.050 mg/L 07/08/2021 2,4,5-Trichlorophenol (TCLP) SW 845 method 8270/3510 <0.060 mg/L 07/08/2021 2,4,6-Trichlorophenol(TCLP) SW 846 method 827013510 <0.050mg/L 07/08/2021 2,4-Dinitrotoluene (TCLP) SW 846 method E27013510 <0.050 mg/L 07/08/2021 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 07/08/2021 Hexachloro-1,3-butadiene(TCLP) SW 846 method 8270/3510 <0,050mg/L 07/08/2021 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 07/08/2021 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/0812021 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 07/08/2021 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021 2,4,5-TP(TCLP) SW846 Method8151A <0.003mg/L 07/1312021 2,4-D (TCLP) SW845 Method 8151A <0.003 mg/L 07/13/2021 1,1-Dichloroethylene(TCLP) SW846 Method826015030 <0.01mg/L 07/02/2021 1,2-Dichloroethane (TCLP) SW848 Method 826015030 <0.01 mg/L 07/02/2021 Benzene (TCLP) SW846 Method826015030 <0.01mg/L 07/02/2021 Carbon Tetrachloride (TCLP) SW846 Method 028015030 <0.01 mg/L 07/02/2021 Report #:: 2021-10553 Page 1 of 2 Environmental Chemists Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax v- ANALYTICAL & CONSULTING CHEMISTS info a.environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Jul 21, 2021 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2021-10653 Project ID: Swainsboro WRF Chlorobenzene(TCLP) SW846 Method825015030 <0.01mg/L 07/02/2021 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 07/02/2021 Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021 Trichloroethylene(TCLP) SW046 Method 826015030 <0.01mg/L 07/02/2021 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021 RCI Cyanide SM 4500 CN D 2.05 mg/kg 07/07/2021 Sulfide SM4500SD 22.8mg/kg 07/06/2021 Ignitability SW 646 method 1010 >195'F 07/20/2021 pH Result estimated. SW 646 Method 9045D Analyzed out of 15 minutes hold time. 7.53 units 06/30/2021 TCLP Metals Arsenic EPA200.7 <1.0mg/L 07/09/2021 Barium EPA200.7 <1.Omg/L 07/09/2021 Cadmium EPA200.7 <1.Omg/L 07/09/2021 Chromium EPA200.7 <1.0mg/L 07/09/2021 Lead EPA 200.7 <1.0 mg/L 07/09/2021 Selenium EPA200.7 <1.0mg/L 07/09/2021 Silver EPA200.7 <1.0mg/L 07/09/2021 Mercury EPA245.1 <0.0002mg/L 07/14/2021 Comment: Reviewed by: QI �p� QWW-J A Report #:: 2021-10653 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmirwton, NC 28405 910.3 92.0223 1'11II/nt Sample Receipt Checklist Client: WYTS Date: Re �Zqq Zi port Number: Q 21 — I o53 Receipt of sample: ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. 4Vere custody seals present on the cooler? ❑ YES ❑ fd0 I N/A Original temperature upon 2. If custody seals were present, were they intact/unbroken? receipt I °C Corrected temperature upon receipt_ How temperature taken: ❑ 7emperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor `C: 0.0 YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample IO's listed on the C0C? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test) YES ❑ NO 10. Did samples arrive in good condition for each test? Yt5 ❑ NO 12. Were samples received within proper holding time for YES ❑ NO requested tests? 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received ❑ YES ❑ NO at a pH >12? 15. Were sulfide samples received at a pH >9? YES ❑ ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? " YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <O.S m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the fiend within 15 minutes? TOC/Volafiles are pH checked at time of analysis and recorded on the ben chsheet Bacteria ,ample; a•e checked for Cnlonne at hme of analys,; and recorded on the b=,ct�;:�__;. Sample Preservation: (Must be completed for any samples) incorrectly preserved or with headspace) 53mple(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H.SO, HNOs HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Vote- ho =� ._s,:DT'er,, . ,e mmediateV fT in^C:-ectI% ores=_-,ej s=_-rp es Oe:a n a • saw rare_` to anz'iz=- by the cds: -" PC v.as nourad Cate a" ante: VOlatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 renuing racuity: Swansboro WWTF 228 Georgetown Road Jacksonville, NC 28540 Phone: 910.389.8511 Project Manager: Randal Riggs Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Subcontracted Laboratory: SUBCONTRACT ORDER Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone:(910) 392-0223 Fax:(910) 392-4424 NCOENR: DWQ aRnFICAnON a M NCDHHS: DU CERnHaWON 137729 Work Order: S212701 Swainsboro WRF Sample ID: S212701-01 Swansboro Digestor 001 SL Sampled,' 0612912021 06:30 Sampled by: Randal Rioas Analysis Due Expires EnviroChem Lab ID PH, SW846 07/09/2021 06/29/2021 06:47 Analysis Due Expires EnviroChem Lab ID Sulfide colorlmetric 07/09/2021 07/13/2021 06:30 Analysis Due Expires EnviroChem Lab ID Cn-335.4 07/09/2021 07/13/2021 06:30 Analysis Due Expires EnvlroChem Lab ID SW 846 Mtd 8270/3510 07/09/2021 07/27/2021 06:30 Analysis Due Expires EnviroChem Lab ID SW 846 808113/3510 07/09/2021 07/27/2021 06:30 Analysis Due Expires EnviroChem Lab ID Ignitability 1030 07/09/2021 07/27/2021 06:30 Analysis Due Expires EnviroChem Lab ID Hg 245.1 07/09/2021 07/27/2021 06:30 Analysis Due Expires EnviroChem Lab ID TCLP Metals 07/09/2021 12/26/2021 06:30 Analysis Due Expires EnviroChem Lab ID SW846 8260/5030 07/09/2021 12/26/2021 06:30 Analysis SW846 B151A Due 07/09/2021 Expires 12/26/2021 06:3n EnviroChem Lab ID Containeasuppl"d AG 1L(A) AG IL AG IL(C) 1L Plastic EnvlroChem Report No: Z 1 — I �� -� Rehngwshed By Dale eceivetl ByBy Page 1 of t 6.2q- Z/ Date