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HomeMy WebLinkAboutWI0400575_Permit (Issuance)_20210823NC Department of Environmental Quality — Division of Water Resources (DWR) NOTIFICATION OF INTENT (NOI) TO CONSTRUCT OR OPERATE INJECTION WELLS The following are `permitted by rule" and do not require an individual permit when constructed in accordance with the rules of 15A NCAC 02C.0200 (NOTE: This form must be received at least 14 DAYS prior to injection) AQUIFER TEST WELLS (15A NCAC 02C .0220) These wells are used to inject uncontaminated fluid into an aquifer to determine aquifer hydraulic characteristics. IN SITU REMEDIATION (15A NCAC 02C .0225) or TRACER WELLS (15A NCAC 02C .0229): 1) Passive Injection Systems - In -well delivery systems to diffuse injectants into the subsurface. Examples include ORC socks, iSOC systems, and other gas infusion methods (Note: Injection Event Records (IER) do not need to be submitted for replacement of each sock used in ORC systems). 2) Small -Scale Injection Operations — Injection wells located within a land surface area not to exceed 10,000 square feet for the purpose of soil or groundwater remediation or tracer tests. An individual permit shall be required for test or treatment areas exceeding 10,000 square feet. 3) Pilot Tests - Preliminary studies conducted for the purpose of evaluating the technical feasibility of a remediation strategy in order to develop a full scale remediation plan for future implementation, and where the surface area of the injection zone wells is located within an area that does not exceed five percent of the land surface above the known extent of groundwater contamination. An individual permit shall be required to conduct more than one pilot test on any separate groundwater contaminant plume. 4) Air Injection Wells - Used to inject ambient air to enhance in -situ treatment of soil or groundwater. 5) In -Situ Thermal Wells (IST) — Used to `heat' contaminated groundwater to enhance remediation. Print Clearly or Type Information. Illegible Submittals Will Be Returned as Incomplete. DATE: July 16 , 2021 PERMIT NO. W 10400575 (to be filled in by DWR) NOTE- If this NOI is being submitted as notification of a modification of a previously issued NOI for this site (e.g., different injection wells, plume, additives, etc.) and still meets the deemed permitted by rule criteria, provide the previously assigned permit tracking number and any needed relevant information to assess and approve injection: A. B. Permit No. WI Issued Date: WELL TYPE TO BE CONSTRUCTED OR OPERATED (1) Air Injection Well Complete sections B through F, J, M (2) Aquifer Test Well . Complete sections B through F, J, M (3) Passive Injection System Complete sections B through F, H-M (4) X Small -Scale Injection Operation Complete sections B through M (5) Pilot Test Complete sections B through M (6) Tracer Injection Well Complete sections B through M (7) In -Situ Thermal (IST) Well Complete sections B through M STATUS OF WELL OWNER: Choose an item. Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 1 C. WELL OWNER(S) — State name of Business/Agency, and Name and Title of person delegated authority to sign on behalf of the business or agency: Name(s): L&L Food Stores / Dan Daly Mailing Address: PO Box 699 — 706 E Church St. City: Nashville State: NC Zip Code: 27856 County: Nash Day Tele No.: 252-459-3146 Cell No.: 252-903-8432 EMAIL Address: gddaly@embargmail.com Fax No.: 252-459-2675 D. PROPERTY OWNER(S) (if different than well owner/applicant) Name and Title: L&L Roses, LLC / Trey Watkins Company Name Mailing Address: 613 US HWY 158 Bypass City: Henderson State: NC Zip Code: 27537 County: Vance Day Tele No.: 252-438-7141 Cell No.: 919-610-1033 EMAIL Address: treyw@roseoilco.com Fax No.: E. PROJECT CONTACT (Typically Environmental Consulting/Engineering Firm) Name and Title: Ryan Kerins Company Name Terraquest Environmental Consultants, P.C. Mailing Address: 100 East Ruffin Street City: Mebane State: NC Zip Code: 27302 County: Alamance Day Tele No.: 919-563-9091 Cell No.: 919-906-0960 EMAIL Address: rdkerins@terraquestpc.com Fax No.: 919-563-9095 F. PHYSICAL LOCATION OF WELL SITE (1) Facility Name & Address: L&L Food Store #6 1765 Red Oak Road City: Nashville County: Nash Zip Code: 27856 (2) Geographic Coordinates: Latitude**: 35 ° 59 ' 33.36 " or ° Longitude**: -77 ° 56 ' 1.176 " or °. Reference Datum: WG584 Accuracy: +/- 2cm Method of Collection: Google **FOR AIR INJECTION AND AQUIFER TEST WELLS ONLY: A FACILITY SITE MAP WITH PROPERTY BOUNDARIES MAY BE SUBMITTED IN LIEU OF GEOGRAPHIC COORDINATES. G. TREATMENT AREA Land surface area of contaminant plume: 11,000 square feet Land surface area of inj. well network: 800 square feet (< 10,000 ft2 for small-scale injections) Percent of contaminant plume area to be treated: 7 (must be < 5% of plume for pilot test injections) Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 2 H. INJECTION ZONE MAPS — Attach the following to the notification. (1) Contaminant plume map(s) with isoconcentration lines that show the horizontal extent of the contaminant plume in soil and groundwater, existing and proposed monitoring wells, and existing and proposed injection wells; and (2) Cross-section(s) to the known or projected depth of contamination that show the horizontal and vertical extent of the contaminant plume in soil and groundwater, changes in lithology, existing and proposed monitoring wells, and existing and proposed injection wells. (3) Potentiometric surface map(s) indicating the rate and direction of groundwater movement, plus existing and proposed wells. I. DESCRIPTION OF PROPOSED INJECTION ACTIVITIES AT THE SITE — Provide a brief narrative regarding the cause of the contamination, and purpose, scope, goals of the proposed injection activity: Small scale injection of 4,000 gallons (1 pound OBC per gallon) broken up as 500 gallons into each of 8 points. J. WELL CONSTRUCTION DATA (1) No. of injection wells: 8 Proposed Existing (provide NC Well Construction Record (GW-1) for each well) (2) Appx. injection depths (BLS): 5, 10, 15, 20, 25 (3) For Proposed wells or Existing wells not having GW-ls, provide well construction details for each injection well in a diagram or table format. A single diagram or line in a table can be used for multiple wells with the same construction details. Well construction details shall include the following (indicate if construction is proposed or as -built): (a) Well type as permanent, Geoprobe/DPT, or subsurface distribution infiltration gallery (b) Depth below land surface of casing, each grout type and depth, screen, and sand pack (c) Well contractor name and certification number K. INJECTION SUMMARY NOTE: Only injectants approved by the epidemiology section of the NC Division of Public Health, Department of Health and Human Services can be injected. Approved injectants can be found online at http: //deq.nc. gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/ground-water- protection/ground-water-approved-injectants. All other substances must be reviewed by the DHHSprior to use. Contact the UIC Program for more info if you wish to get approval for a different additive. However, please note it may take 3 months or longer. If no injectants are to be used use N/A. Injectant: Oxygen Biochem Total Amt. to be injected (gal)/event: 4,000 gallons Injectant: Total Amt. to be injected (gal)/event: Injectant: Total Amt. to be injected (gal)/event: Injectant: Total Amt. to be injected (gal)/event: Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 3 Injectant: Total Amt. to be injected (gap/event: Total Amt to be injected (gal/event): No. of separate injection events: Total Amt. to be injected (gal): Source of Water (if applicable): L. MONITORING PLAN — Describe below or in separate attachment a monitoring plan to be used to determine if violations of groundwater quality standards specified in Subchapter OM result from the injection activity. VOC Monitoring will be regulated by NCDWM-UST. Semi-annual sampling of monitoring wells for 6200E analysis is anticipated. M. SIGNATURE OF APPLICANT AND PROPERTY OWNER Well Owner/Applicant: "I hereby certify, under penally of law, that I am familiar with the information submitted in this document and all attachments thereto and that, based on my inquiry of those individuals immediately responsible for obtaining said information, I believe that the information is true, accurate and complete. I am aware that there are significant penalties, including the possibility of fines and imprisonment, for submitting false information. I agree to construct; operate, maintain, repair, and if applicable, abandon the r)rj'tion w anjf all related appurtenances in accordance with the 1 SA NCAC 02C 0200 Rules." Signature of Abplieant Print or Type Full Name and Title Property Owner (if the property is not owned by the Well Owner/Applicant): "As owner of the property on which the injection well(s) are to be constructed and operated I hereby consent to allow the applicant to construct each injection well as outlined in this application and agree that it shall be the responsibility of the applicant to ensure that the injection well(s) conform to the Well Construction Standards (15A NCAC 02C .0200)." "Owner" means any person who holds the fee or other property rights in the well being constructed. A well is real property and its coon on Iand shall be deemed to vest ownership in the land owner, in the absence of contrary agreement ' Ling)E1 tkaaser; Signature* of Property Owner (if different from applicant) Print or Type Full Name and Title *An access agreement between the applicant and property owner may be submitted in lieu of a signature on this form. Please send 1 (one) bard color copy of this NOI along with a copy on an attached CD or Flash Drive at least two (2) weeks prior to injection to: DWR -- UIC Program 1636 Mail Service Center Raleigh, NC 27699-1636 Telephone: (919) 707-9000 Deemed Permitted OW Remediation NOI Rev. 2-17-2020 Page 4 002726 ESTIMATED EXTENT OF 2L STANDARD VIOLATION 004147 6 •a r 1 Dar II* p� hi mvl = cwxxmv s 5 N t „ v _ WW1 MWZ_ MW3 !WWI_ MW6 MVO.__ MAT_ MW9 MW1a MW11 14W 12 44W13 MW1 4 3J13j71 3,P1321 3113/11 3J13/21 3,P13/21 3f1 221 3J13/21 3,P13/21 3f13221 3J13j71 3,P13/21 3f13221 3/13/21 3 21 3J20 ..0.330 0 3aa r0 330 50.330 a 330 33411 0 -_423 0 .133 0 -Yy0 5E1 429 0 `10 1243 m ..0410 0110 148 .0 410 0110 1o�u .0430 0110 .0410 162 444 : .0300 259 LAZE .0 300 : 01a0 67.3 .0100 ▪ 01a0 7.371 0 .i00 . 01a0 .0300 5-13 3.71 c 1.60 7.3170 5.9531 _40 140 773 160 724 14,1113 _40 t 1.60 150 56.9 93 .0140 370 9E.E t0==0 :07 .0 10 0-=0 '0710 ESs 0-=0 .0 740 .0?40 .0 40 0710 350 ■47 ..07(0 c07a0 c0 T00 .0'(0 ▪ 0 7a0 3E3 .0'(0 ▪ 0 700 .0 700 119 . 0300 910 1216 ..0 820 . 0110 515 ..0320 7 42 7.1111 ..0320 . 0320 <0320 1E2 9.67 ..0360 356 355 .0360 -:.a350 164 .0360 0279 571 .0190 =0160 .0190 635 336 '.0530 154 692 Y0130 .0130 17_5 .0130 0320 15.5 .0530 :as10 .0530 .0330 0130 200 104 256 '100 100 65.E 300 100 SEE 100 1.00 1.00 217 253 690 33.3 15 < 0 69] < 0 69) 33.6 .01. ▪ 171 '0190 ▪ 069) <0 69] Y0 690 < 0593 215nntla rd 600 -400 300 20 70 400 400 70 6 70 GCL 3000 29)0)] 34.530 3 -.0 20600 7. ..0 2- .0 25..0 25..0 6A00 ] 00 LEGEND MONITORING WELL a SOLE -SOURCE SUPPLY WELL 0 Proposed injection point UST LEGEND Current: TA1: 10,000-GAL GASOLINE TA2: 6,000-GAL GASOLINE TA3: 1 ,000-GAL KEROSENE Removed: T1: 8,000-GAL GASOLINE T2: 8,000-GAL GASOLINE T3: 4,000-GAL GASOLINE GRAPHIC SCALE 0' 20' 40' 1" = 40' 80' 0 z 0 z NASHVILLE L&L FOOD STORES FIGURE NO. CO 2 CD CC CHECKED BY: co O 0 PROJECT NO: 0 J H DRAWN BY: /.//// // ESTIMATED EXTENT OF, / ,ESTIMATED EXTENT OF 2L STANDARD VIOLATION 0'-10' BGL Lean Clay (CL) Mostly medium stiff reddish —orange —tan clay, few to trace fine sand. 10' — 20' BGL Sandy Lean Clay (CL) Medium stiff, red to orange to tan to white mostly clay, with some silt and some fine—grained sand. Some gravel noted from 14-15' BGL in MW8,9,10,11. 20' — 30' BGL Silt (ML) Medium stiff to soft, red to white to tan, mostly silt with some clay and trace sand. Estimated extent of STG MSCC violation Elevations are referenced to an arbitrary datum plane of 100.00'. A detailed discussion of site geology along with boring logs ore included in the CSA Report. This drawing is a fence diagram. The distances between wells do not correlate with a straight line between the first and last well of the cross section. Some features have been projected onto the traces. *Depth to water measurements were collected during sampling on 7/17/19 and on 4/15/20 only for the wells sampled as pre —approved by the NCLUST TF. A complete set of water levels was not collected at one time. The difference in water table elevations is shown here accordingly. ESTIMATED EXTEN OF STG MSCC VIOLATION HORIZONTAL: 1" = 30' VERTICAL: 1" = 10' ESTIMATED EXTENT OF 2L STANDARD VIOLATION LEGEND MONITORING WELL SOLE —SOURCE SUPPLY WELL The groundwater elevations as measured on 2/16/21 are listed in feet. The Type III monitoring well MW1 2 was not used in the construction of this map. The interpreted groundwater flow direction is indicated by the arrows placed perpendicular to the contour lines. Samples collected on 2/16/21 were lost in transit to the lab in Texas due to the winter weather event of 2021. The wells were resampled on 3/13/21. MP Well IUD Groundwater Elevation (ft_j MW1 98.35 MW2 94.77 MW3 95.53 N1W4 96.45 MW5 99.27 MW6 97.09 MW7 96.37 MVTh 96.10 1N1W9 95.78 MW 10 94.63 MW11 96.45 MW12 95.82 MW 13 95.11 MW14 96.83 UST Current: TA1: 10,000 TA2: 6,000— TA3: 1 ,000— Removed: T1 : 8,000— T2: 8,000— T3: 4,000— LEGEND —GAL GASOLINE GAL GASOLINE GAL KEROSENE GAL GASOLINE GAL GASOLINE GAL GASOLINE GRAPHIC SCALE 0' 20' 40' 1" = 40' 80' CD 0 W U Q CC 'OTENTIOMETRIC 0) z CD O H QZ O L,J 0 O Y O (3O 0O ow z o� 0_ w J CO J_ J � _ 0) z z NASH ILL , NC L&L FOOD STORES rr) FIGURE NO. N 0) CO CD Ct CHECKED BY: 0 J H DRAWN BY: co 0 0 PROJECT NO: 0 II 0 U z w 25' TYPICAL INJECTION POINT DETAIL LAND SURFACE GENERAL INFORMATION Well Driller: Terraquest Environmental Consultants, Jonathan R. Grubbs #3001 TEMPORARY BORING FOR INJECTION POINT BOTTOM TM. RRACII ENVIRONMENTAL CONSULTANTS, P.C. P.C. — _MATERIAL SAFETY DATA SHEET Oxygen BioChem (OBC)® M.SDS Ref. No.: 1,18.44-8 Date Approved: 04/30/2006 Revision No.: 2 This document has been prepared to meet the rerluimments of the U.S. OSHA Hazard Communication Standard, 29 CFR 1910.1200; the Canada's Workplace Ha2ardous Materials Information System (WHMIS) and, the EC Directive, 2001/58/EC. 1. PRODUCT AND COMPANY IDENTIFICATION PRODUCT NAME: C:FYIRAL USE: MANUFACTURER FMC CORPORATION FMC Pcroxygcns 1735 Market Street Philadelphia, PA 19103 (215) 299-6000 (General Information) Oxygen BioChem (OBC)S For chemical oxidation and aerobic biorcrnediation, petroleum hydrocarbon remediation, creosote rentndiation and partially halogenated hydrocarbon mmediation. EMERGENCY TELEPHONE NUMBERS (303) 595.9048 (Medical U.S. - C'ill Collect) For leak, fire, spill, or accident cinnrgcncics, call: (800) 4244300 (CHEMTREC - U.S.A. Sc Canada) 2. HAZARDS IDENTIFICATION EMERGENCY OVERVIEW: m Odorless ofltwhitcfine granular solid (cony bavcseparatarn or noticcahlc. ix o-toncappcaratucc). a> Oxidizer m Contact with combustibles may cause fin:. m Decomposes in storage under conditions of moisture (water/water vapor) and/or excessive heal causing release of oxides of sulfur and oxygen that supports combustion. Decomposition could form a high temperature melt_ See Section 10("Stabilityand Reactivity"). Deluge container with water at safe distance or in protected area. co May he severely irritating to the ayes. POTENTIAL HEALTH EFFECTS: Airborne dust may be irritating to eyes, no. I throat and skin upon contact. Exposum to high Icvels of dust may cause difficulty in breathing insem persons. No significant long tcmu inhalation hazard; in-itation usually subsides alter exposure ceases. Page 1 of 10 Oxygen BioChent (OBC)® (F18-44-8) Date: 04/30/2006 3. COMPOSITION / INFORMATION ON INGREDIENTS Chemical Name CAS# Wt. % EC No. EC Class Proprietary Mixture None Not classified 4. FIRST AID MEASURES EYES: Immediately flush with water for at least 15 minutes, lifting the upper and lower eyelids intermittently. See a medical doctor or ophthalmologist immediately. SKIN: Wash with plenty of soap and water. Get medical attention if irritation occurs and persists. INGESTION: Rinse mouth with water. Dilute by giving 1 or 2 glasses of water. Do not induce vomiting Never give anything by mouth to an unconscious person. See a medical doctor immediately. INHALATION: Remove to fresh air. If breathing difficulty or discomfort occurs and persists, obtain medical attention. NOTES TO MEDICAL DOCTOR: Modest irritation is the only expected effect. No serious consequences are expected, except perhaps in the case of direct eye contact. Contaminated external surfaces should be flooded with water, and direct eye contact deserves ophthalmologic evaluation. If ingested, gastrointestinal irritation but not caustic burns are to be expected; dilution with water indicated as may be gastric evacuation via emesis or lavage if large doses or severe irritation is evident. Demulcents should be helpful. No systemic effects are expected though human toxicity data is sparse. 5. FIRE FIGHTING MEASURES EXTINGUISHING MEDIA: Deluge with plenty of water. FIRE / EXPLOSION HAZARDS: Product is non-combustible. Under fire conditions, may decompose and release oxygen gas, which may intensify fire. Presence of water accelerates decomposition. Mixtures with polysulfide polymers may ignite, FIRE FIGHTING PROCEDURES: Use flooding quantities of water. Use water spray to keep fire exposed containets cool. Do not use carbon dioxide or other gas filled fire extinguishers; they will have no effect on decomposition. Wear full protective clothing and self-contained breathing apparatus. Page 2 of 10 Oxygen BioChem (OBC)® (F18-44-8) Date: 04/30/2006 FLAMMABLE LIMITS: Non-combustible SENSITIVITY TO IMPACT: Oxidizable materials can be ignited by grinding and may become explosive. SENSITIVITY TO STATIC DISCIIARGE: Not available 6. ACCIDENTAL RELEASE MEASURES RELEASE NOTES: Confine and collect spill, put into an approved DOT container (do not return to original container) and isolate for disposal. Isolated material should be monitored for signs of decomposition (fuming / smoking). If spilled material is wet, dissolve with large quantities of water and dispose as a hazardous waste. Runoff to sewer may create fire or explosion hazard (do not flush powdered material into sewer). Dispose of wastes according to the method outlined in Section 13, "Disposal Considerations". 7. HANDLING AND STORAGE HANDLING: Avoid contact by using personal protective equipment. Use respiratory protective equipment when release of airborne dust is expected. If compounded with organics or combustible materials be sure to exclude moisture. Use clean plastic or stainless steel scoops only. STORAGE: Keep dry (reacts with moisture). Use first in, first out storage system. Store unopened in a cool, clean, dry place away from point sources of heat (e.g. steam pipes, radiant heaters, hot air vents or welding sparks). Keep container tightly closed when not in use. Avoid contamination of opened product. Avoid contact with reducing agents. In case of fire or decmpositoin (fuming / smoking) deluge with plenty of water to control decomposition. Fore storage, refer to NFPA Bulletin 430 on storage of liquid and solid oxidizing materials. COMMENTS: VENTILATION: Provide mechanical general and/or local exhaust ventilation to prevent release of dust into work environment. Spills should be collected into suitable containers to prevent dispersion into the air. If ventilation is inadequate or not available, use dust respirator and eye protection. 8. EXPOSURE CONTROLS / PERSONAL PROTECTION EXPOSURE LIMITS Chemical Name ACGIH OSHA Supplier Proprietary Ingredient 0.1 mg/m3 (TWA) Page 3 of 10 Oxygen BioChem (OBC)® (F18-44-8) Date: 04/30/2006 10. STABILITY AND REACTIVITY CONDITIONS TO AVOID: Heat (decomposes at 275°C), moisture, reducing agents. Grinding with organics, STABILITY: Stable (decomposition could occur when exposed to heat or moisture) POLYMERIZATION: Will not occur INCOMPATIBLE MATERIALS• Grinding mixtures with organics (oxidizable materials can be ignited by grinding and may become explosive); heavy metals. Acids, alkalis, halides (fluorides, chlorides, bromides and iodides), combustible materials, most metals and heavy metals, oxidizable materials, other oxidizers, reducing agents, cleaners, and organic or carbon containing compounds. Contact with incompatible materials can result in a material decomposition or other uncontrolled reactions. HAZARDOUS DECOMPOSITION PRODUCTS: Oxygen that supports combustion and oxides of sulfur, nitrogen, and calcium hydroxide. COMMENTS. PRECAUTIONARY STATEMENT: Use of persulfates in chemical reactions requires appropriate precautions and design considerations for pressure and thermal relief. Decomposing persulfates will evolve large volumes of gas and/or vapor, can accelerate exponentially with heat generation, and create significant and hazardous pressures if contained and not properly controlled or mitigated. Use with alcohols in the presence of water has been demonstrated to generate conditions that require rigorous adherence to process safety methods and standards to prevent escalation to an uncontrolled reaction. 11. TOXICOLOGICAL INFORMATION EYE EFFECTS' No data available for the mixture. Proprietary Component* Non -irritating (rabbit) Proprietary Component Severely irritaitng (unwashed); Minimally irritating (washed) SKIN EFFECTS: No data available for the mixture. Expected to be non-irritating.(rabbit) DERMAL LD50' No data available for the mixture. Proprietary Components: > 10 g/kg (rat) ORAL LD50' No data available for the mixture. Proprietary Component: 895 mg/kg (rat) Proprietary Component: 5 g/kg (rat) Page 5 of 10 Oxygen BioChem (OBC)® (F18-44-8) Date: 04/30/2006 13. DISPOSAL CONSIDERATIONS DISPOSAL METHOD: Dissolve in water to allow the release of oxygen and dispose via a treatment system in accordance with governmental agencies regulations. Contact appropriate regulatory agency prior to disposal. 14. TRANSPORT INFORMATION U.S. DEPARTMENT OF TRANSPORTATION (DOT) PROPER SHIPPING NAME: Oxidizing solid, n.o.s. (sodium persulfate, calcium peroxide) PRIMARY HAZARD CLASS/DIVISION: 5.1 (Oxidizer) UN/NA NUMBER: UN 1479 PACKING GROUP: II LABEL(S): 5.1 (Oxidizer) PLACARD(S): 5.1 (Oxidizer) MARKING(S): Oxidizing solid, n.o.s. (sodium persulfate, calcium peroxide), UNi479 ADDITIONAL INFORMATION: Hazardous Substance/RQ: Not applicable 49 STCC Number: 4918733 This material is shipped in 55 Ib. polyethylene pail with vented screw -on lid (approx 6.5 gallon) INTERNATIONAL MARITIME DANGEROUS GOODS (IMDG) PROPER SHIPPING NAME: Oxidizing solid, n.o.s. (sodium persulfate, calcium peroxide) INTERNATIONAL CIVIL AVIATION ORGANIZATION (ICAO) / INTERNATIONAL AIR TRANSPORT ASSOCIATION (IATA) PROPER SHIPPING NAME: ADDITIONAL INFORMATION: Page 7 of 10 Oxidizing solid, n.o.s. (sodium persulfate, calcium peroxide) Combination packaging is recommended for air transport. Oxygen BioChem (OBC)® (F18-44-8) Date: 04/30/2006 OTHER INFORMATION: Place spilled product in suitable container and wash residue with plenty of water. See Section 6 (Accidental Release Measures) above for additional instructions. 15. REGULATORY INFORMATION UNITED STATES SARA TITLE III (SUPERFUND AMENDMENTS AND REAUTHORIZATION ACT) SECTION 311 HAZARD CATEGORIES (40 CFR 370): Fire Hazard, Inmtediate (Acute) Health Hazard SECTION 312 THRESHOLD PLANNING QUANTITY (40 CFR 370): The Threshold Planning Quantity (TPQ) for this product, if treated as a mixture, is 10,000 lbs; however, this product contains the following ingredients with a TPQ of less than 10,000 lbs.: None SECTION 313 REPORTABLE INGREDIENTS (40 CFR 372): Not listed CERCLA (COMPREHENSIVE ENVIRONMENTAL RESPONSE COMPENSATION AND LIABILITY ACT) CERCLA DESIGNATION & REPORTABLE QUANTITIES (RQ) (40 CFR 302.4): Proprietary component: Unlisted, RQ = 100 lbs., Ignitability TSCA (TOXIC SUBSTANCE CONTROL ACT) TSCA INVENTORY STATUS (40 CFR 710): Listed (components) RESOURCE CONSERVATION AND RECOVERY ACT (RCRA) RCRA IDENTIFICATION OF HAZARDOUS WASTE (40 CFR 261): Waste Number: D001 CANADA WHMIS (WORKPLACE HAZARDOUS MATERIALS INFORMATION SYSTEM): Chemical Name: Proprietary Component Product Identification Number: 1505 Hazard Classification / Division: Class C (Oxidizer), Class D, Div. 2, Subdiv. B. (Toxic) Ingredient Disclosure List: Listed Chemical Name: Proprietary Component Product Identification Number: 1457 Hazard Classification / Division: Class D, Div 2, Subdiv. B, Class C (Oxidizer) Ingredient Disclosure List: Listed Page 8 of 10 Oxygen BioChem (OBC)® (F18-44-8) Date: 04/30/2006 INTERNATIONAL LISTINGS Proprietary Component Australia (AICS): Listed China: Listed Japan (ENCS): (1)-1131 Korea: KE-12369 Philippines (PICCS): Listed Proprietary Component Australia (AICS): Listed China: Listed Japan (ENCS): (1)-181 Korea: KE-04518 Philippines (PICCS): Listed Proprietary Component Australia (AICS): Listed China: Listed Japan (ENCS): (1)-190 Korea: ICE-04597 Philippines (PICCS): Listed HAZARD, RISK AND SAFETY PHRASE DESCRIPTIONS: EC Symbols: (Not classified as hazardous) EC Risk Phrases: (Not classified as hazardous) EC Safety Phrases: (Not classified as hazardous) 16. OTHER INFORMATION HMIS Health 2 Flammability 0 Physical Hazard 1 Personal Protection (PPE) J Protection = J (Safety goggles, gloves, apron & combination dust & vapor respirator) HMIS = Hazardous Materials Identification System Degree of Hazard Code: 4 = Severe 3 = Serious Page 9 of 10 Oxygen BioChem (OBC)® (F18-44-8) Date: 04/30/2006 2 = Moderate 1 = Slight 0 = Minimal NFPA Health 2 Flammability 0 Reactivity 1 Special OX SPECIAL = OX (Oxidizer) NFPA = National Fire Protection Association Degree of Hazard Code: 4 = Extreme 3 = High 2 = Moderate 1 = Slight 0 = Insignificant REVISION SUMMARY: This MSDS replaces Revision #I, dated December 12, 2005. Changes in information are as follows: Section 1 (Product and Company Identification) Section 16 (Other Information) FMC Logo - FMC Corporation Trademark Oxygen BioChem (OBC) - Trademark of Redox Tech, LLC © 2006 FMC Corporation. All Rights Reserved. FMC Corporation believes that the information and recommendations contained herein (including data and statements) are accurate as of the date hereof. NO WARRANTY OF FITNESS FOR ANY PARTICULAR PURPOSE, WARRANTY OF MERCHANTABILITY, OR ANY OTHER WARRANTY, EXPRESSED OR IMPLIFD, IS MADE CONCERNING THE INFORMATION PROVIDED HEREIN. The information provided herein relates only to the specific product designated and may not be applicable where such product is used in combination with any other materials or in any process. It is a violation of Federal law to use this product in a manner inconsistent with its labeling. Further, since the conditions and methods of use are beyond the control of FMC Corporation, FMC Corporation expressly disclaims any and all liability as to any results obtained or arising from any use of the product or reliance on such information. Page 10 of 10