WQ0039181_Modification_20210823

Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0039181
Applicant/Permittee Carolina Malt House, Inc.
Applicant/Permittee Address 12969 statesville blvd cleveland nc 27013
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Organization
Facility Name Carolina Malt House WWTF
County Rowan
Fee Category Major
Is this a complete
application?*
c Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $395
Complete App Date 08/23/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff
Name * mark van wagenberg
Email Address*
[e-mail]
electronic subntttal, confirmation of receipt, and other correspondence.
Phone Number*
7042139334
Project Information
........ ..................................................................................................................................................... ......... ......... ... .... ........ ... ... .... .... .... ... ... ... .... .... .... ... .... .... ......... ......
Application/Document Type* r New (Fee Req ui red)
c Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation
r High -Rate Infiltration
r Other Wastewater
r Reclaimed Water
r Closed -Loop Recycle
r Residuals
r Single -Family Residence Wastewater
r Other
Irrigation
Permit Number:*
W00039181
Has Current Existing permt number
Applicant/Permittee *
Carolina Malt House, Inc.
Applicant/Permittee Address*
12969 statesville blvd cleveland nc 27013
Facility Name *
Carolina Malt House WWTF
Please provide comments/notes
on your current submittal below.
Hello,
Please see attached engineering computations, water balance, nutrient management plan,
Agri -Waste Technology, Inc. memorandum, addendum to soil evaluation that support the
revision. Permit application will be for an average 12,520 gallons per day. This is based on
the maximum water that can be spread and still not over apply nitrogen on the application
fields. Our current permit is for an average of 6,053 gallons for the two steeping lines.
Thanks!
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Etc.)
Carolina Malt House waster water revision 8_13_21.pdf 23.01 MB
Upload only 1 PCFdocurrent (less than 250 M3). Miltiple docurrents must be combined into one RDFfile unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center

Raleigh, NC 27699-1617
Signature
00wa' Mr�z.�x�
Submission Date 8/13/2021

CAROLINA MALT HOUSE, INC.
%Aaron Goss
Waste Management System
ROWAN COUNTY, NORTH CAROLINA
ADDRESS: 12969 Statesville Blvd.
Cleveland, NC 27013
PHONE: [phone]
LOCATION: 12969 Statesville Blvd
Near Third Creek
LONGITUDE - 800 42'52.6"
LATITUDE - 350 44'20.4 it
operation Type: Barley Malting House
PLANNED BY: Aaron Goss, Carolina Malt House, Inc.
Samuel C. Bingham, PE, Engineer
APPROVED BY:
DATE:
�Ss 9
SEAL
t0355
Carolina Malt House, Inc
Waste Plan

Modification to Permit
Carolina Malt. House, Inc. (CMH) contacted Jeff Vaughan,.
Ph.D, Senior Agronomist/Soil Scientist with Agri -Waste
Technology, Inc. (AWT) located at 502 N. Salem Street, Suite
203, Apex, North Carolina 27502 about the methodology for
properly computing the plant available nitrogen when
applying their wastewater to the waste application fields.
See AWTr s Memorandum dated February 3, 2021 attached.
The plant available nitrogen factor for CMH wastewater
is 50% of the total nitrogen expressed as Total Kjehdahl
Nitrogen. (TKN) based. on AWT"s evaluation of CMH treatment
system.
Based can this new information, CMH want to apply for as
.large a permit as their current waste application system.
will justify in order to not have to worry about possible
fees and penalties for exceeding their current operating
capacity.
The current permit is limited by nitrogen loading rate
based on 100% of the nitrogen being available to crops when
applied. Engineering calculations, water balance and
nutrient management plan are revised reflecting the maximum
nitrogen and wastewater volume that can be applied using the
actual plant -available nitrogen factor of 50%.
Carolina Malt Mouse, Inc
Waste Plan

INDEX
Part 1 - Engineer Calculations, 2/27/2021
Engineering Calculations and Plans
I.
Waste
Production
II.
Waste
Management Overview
A.
Waste Storage Pond
B.
Glean Water Exclusion
C.
Plant Available Nutrients for Waste
Utilization Plan
D.
Operation and Maintenance Plans
E.
Emergency Action Plans
III.
Waste
Storage Pond.
IV.
Clean
Water Exclusion
A.
Diversions & Waterways
V.
Waste
Nutrients
A.
Waste Volumes
B.
Nutrient. Computations
C.
Spray Irrigation Water Balance
Part 2 - Water Balance, 2/27/202_1
Part 3 - Nutrient Management Plan, 3/1/2021
Part 4 - Agri -Waste Technology, Inc. Memorandum, 2/3/2021
Part 3 - Adendum to Soil Evaluation, 6/12/2017
2 Carolina Malt House, Inc.
Waste flan

_..
ENGINEEERII' G CALCULATIONS, 2/ 7/2021

ENGINEERING CALCULATIONS
T. Waste Production
The Carolina Malting House produces malted barley by
steeping barley seeds, germinating them and then drying down
and/or roasting to the final product. The calculations
herein regarding wastewater production have been obtained
from 2 years of malting experience at the Carolina Malt
House. The Carolina Malt House steeps 22-ton batches of
barley; the calculations begin here.
The canonical bulk density of "raw" barley ("raw"
meaning barley straight from the field) is 48 lb/bushel,
which is 38.57 lb per ft3. Prior to malting, the raw barley
is cleaned using a series of screens, blowers, and density
sifters to remove debris, light grain and other undesirable
matter. The cleaned barley bulk density is 43.94 lb per
ft3. The volume of 22 tons of cleaned barley is 1,001 ft3.
Most of the wastewater generated by a malt house comes
from the steeping process, during which the barley is
submerged and then drained three times over the course of
two days. During steeping, the barley takes up water and
the individual kernels increase in size, and the bulk volume
consequently increases. A typical increase in volume of
1.62 times is expected with the steeping process with
moderate agitation. The final volume of the cleaned barley
after steeping will be 1,622 ft3.
Volume of Steeping tank and bowl is:
[ (ri (14 ) 2/ 4) (10' ) + fi (7) 1 (7')/ 31 + [ (Tq (6. 5) 1/4) (3. 25'
ri(3.25 )2 (3.25')/31 = 1,970 cu ft
Based on measurements by Carolina Malt House, the
steeping water volume is 8,400 gallons in first steep.
Carolina Malt House have determined that using 8,400
gallons' water in first steep gives them a volume that they
are comfortable using in the steeping process (i.e. Barley
is submerged a couple feet with water the first steep).
Second and third steeps use less water. It is estimated that
7,400 gallons are used in the second and third steeps,
respectively.
Total steep water per 22-ton batch for three steep
cycles is 23,200 gallons'.
Additional water is used for flushing the barley from
the steeping vessel to the germination vessel and for
washing down the steeping vessel after the third steep is
Carolina Malt House, Inc
Waste Plan

completed. The total water used for this conical steeping
operation includes the 23,200 gallons (3 steeps) noted
above, plus an additional 3,000 gallons estimated by
Carolina Malt House. That brings the total water used per
22-ton batch to 26,200 gallons.
This water is not all sent to the subject wastewater
system, however. Much of the water is taken up by the
barley during steeping, and this water is evaporated during
the germination, withering and kilning phases. Based on
Carolina Malt Houses experience (moisture content before and
after) 3,500 gallons will be evaporated during steeping
process. Thus the total wastewater generated per steeping
cycle will be approximately 26,200 gallons minus 3,500
gallons or 22,700 gallons.
Even though the steeping process takes two days, the
Carolina Malt House have a process bottleneck at the
germination and kilning phase that will limit steeping to
occurring only every seven and half days. This means the
Malt House steeps barley no more often than every 7.5 days
for each kiln. Two kilns will be used in phase II so
anticipated water use is 22,'700 gallons' x 2 or 45,400
,gallons every 7.5 days so the wastewater produced will
average around 6,053 gallons every day.
To allow more flexibility, Carolina Malt House want the
permit volume based on their current wastewater irrigation
system capability. Permit application will be for an
average of 12,520 gallons per day. See engineering
calculations, water balance and nutrient management plan
justifying this capacity.
11. Waste Management Overview
The waste management system will economically as
possible handle all the waste production described above in
a manner that does not degrade air, soil or water resources.
The system will prevent discharge of pollutants to surface
and ground water by recycling waste through soil and plants,.
The waste management system includes the following
comDonents:
A. Waste Storage Pond
The waste storage pond is located south of the malting
facility and collects all wastewater from the steeping
operation.
Waste storage pond stores the following volumes of
liquid waste:
1) Wastewater from steeping operation
4 Carolina Malt House, Inc.
Waste Plan

2) 0.51 of residue solids
3) Rainfall minus evaporation on pond
4) 21 freeboard which includes 25 year - 24 hour
direct rainfall
USDA -MRCS conservation standard practice 313 "Waste
Storage Facility" and other requirements from State and
Federal agencies were used to design the waste pond. This
pond will provide temporary storage for organic wastewater
generated by agricultural processing. USDA -MRCS
conservation standard practice 521A "Pond Sealing or Lining -
Flexible Membrane" was used to design the synthetic Liner.
The Waste storage pond is located over 100 feet from
the nearest well and over 50 feet from nearest property
line. The waste storage pond is located no closer than 750
feet from any residence.
B. Clean Water Exclusion
Clean water was excluded from the waste storage pond
and irrigation area to the fullest extent possible.
Diversions, culverts and guttering are used.
Diversions and waterways were used to divert clean
water around waste storage pond.
C. Plant Available Nutrients for Waste Utilization Plan
Estimate of Plant Avail -able Nitrogen to collect and
spread each year will be determined.
D. operation and Maintenance Plan
The owner shall be responsible for operating and
maintaining the system. See Operation and Maintenance Plan.
E. Emergency Action Plan
The emergency action plan describes emergency
conditions and immediate steps to take to gain control.
III. Waste Storage Pond
A. Design Volumes
1. The wastewater is mostly water with low nutrient
content. A storage period is planned to allow management
flexibility in irrigating wastewater.
Carolina Malt House, Inc
Waste Plan

No drainage area enters the waste pond. Only direct
rainfall storage and evaporation will be considered in the
design.
Rainfall and Temperature data from Salisbury Station 7615
(gears 1900-1993)
80th percentile annual rainfall from Salisbury Station 7615
(1900-1993) - 52.36"
Evaporation data from Table Tl of NOAA TR34. NOAA data will
be used in design since several years used in evaluation.
AVERAGE
80th
AVERAGE,
MONTH
RAINFALL,
Perc.
TEMP.
PAN EVAP. NORMAL
EVAP.
from NOAA TR34
0.7(PAN)
Greensboro, NC
JAN.
3.71
4.21
41.0
1.82
1.27'
FEB.
3.92
4.45
43.0
2.21
1.55
MAR.
4.31
4.90
50.9
3.95
2.77
APR.
3.62
4.11
59.7
5.25
3.68
MAY
3.91
4.44
68.2
6.41
4.49
JUN.
4.18
4.75
75.5
6.72
4.70
JUL.
4.81
5.46
78.7
6.69
4.68
AUG.
4.41
5.01
77.4
6.21
4.35
SEP.
3.55
4.03
71.7
4.64
3.25
OCT.
3.16
3.59
60.6
3.49
2.44
NOV.
2.75
3.12
50.1
2.47
1.73
DEC.
3.76
4.27
42.0
1.86
1.30
2. 25 yr - 24 hr rainfall on pond surface
From NOAA Atlas 14 Point Precipitation Frequency
Estimated 25 yr Rainfall - 5.79" = .5 ft
3. Freeboard
NC requires 2.0 for freeboard below lowest. outlet (i.e.
Top of dam since fill height is less than 3'). This volume
will include the 25-year storage.
4. Steeping, Flushing and Wash Water
Volume - 12,520 gallons/days
S. Residue volume
Per waste facility standard, 0.5' in bottom of pond
shall be provided for residual solids after liquid is
removed. Residual solids will, be removed by agitation and
irrigated when needed.
6 Carolina Malt Mouse, Inc:.
Waste Ilan

6. Estimate Pump -Out Volume each Year
A. Based on 12,520-gallon average volume/day produced
Storage
Storage
Rain-
Evap.
R-E
R-E
Wastewater
Total Vol
Fall
Inch
inch
Vol
Vol. from
Gallons
Inch
Gallons
Plant
Gallons
Dec -Feb
12.93
4.12
1 8.81
70,122
1, 142, 450
1,212,572
Mar -May
13.45
10.94
2.51
19,978
1,142,450
1,162.,428
Jun -Aug
15.22
13.7
1.52
12,098
1,142,450
1,154,548
� �N ov
-
10.74
7.42
3.32
26.,425
1,142,450
1,168,875
Yearly
4,698,423
Total—
***Each three-month period represents a ji.ZD-Udy pt--LIUU
Note: This estimated pump -out volume is based on a surface
area of 113' x 113' or 0.29 acres for estimating rainfall
minus evaporation. The spray irrigation water balance
attached shows a total 4,697,014 gallons for the year. Use
spray irrigation water balance in the waste utilization
plan.
B. Summary of Design Volumes
1. Steeping and Wash Volume 12,869 gallons/day
2. Unpumpable Volume (residue storage) 0.5 ft
3. Additional freeboard & 25 yr - 24 hr rainfall 2.0 ft
TOTAL 2.5 ft
C. Size of Waste Storage Pond
113' X 113'
2. 0'
101' X101,
3:1 \ 18.0'
53x53' / 3: 1
Wastewater Storage
Volume = 8.0/6[53 X 53 -1- 101 X 101 +4(77 X 77)]
� 48,968 cu ft = 366,281 gallons
Top of Dam
Total Volume = 10.5/'6[50 X 50 +113 X 113 +4(81.5 X 81.5)]
73,216.5 ou It- 547,659 gallons
7 Carolina Malt House, Inc
Waste Plan

Depth
Gallons of
Storage
0.5
9,922
Residue Storage
1.0
21,034
2.0
47,094
3.0
78,719
4.0
116,448
5.0
160,82.0
6.0
212,372
7.0
271,644
8.0
339,173
8.5
376,203
Maximum Capacity
10.5
547,559
Top of Dam
Carolina Malt House Waste Storage Pond Capacity
D. Waste Storage Period
The storage period for waste storage pond for liquids
is approximately 0.94 month for the permitted average
wastewater volume for the plant (4,697,014 gallons/12
month).
Storage Period = 366,281 gallons/4,697,014 gallons/12 month
0.94 months
E. Pump -Gut Elevation and ESW Elevation
Maximum pump out level
2.0' below Emergency Spillway
The waste storage pond should be irrigated before the
water level reaches the freeboard storage volume. This
elevation is 2.0 ft below the Top of Dam elevation.
F. Pond Maker
Marker is installed in pond. Foot and tenths of foot
increments are identified. Lowest point on top of dam,
maximum level at top of temporary liquid storage volume.
which shows the 2' freebrord and minimum liquid level at.
bottom of temporary liquid storage volume will. be .boldly
marked.
G. Agitation/Mixing
The irrigation system should handle small solids. It
r,n°+- ar,ti r-i pater- -t it a ciae and duckweed growth will be
Carolina Malt House, Inc.
Waste Mau

problem if it can be mixers and routinely reeved from the
waste pond. The irrigation pump shall be designed to allow
mixing of the wastewater especially in the bottom of the
pond. An aerator can easily be added at later date if algae
or duckweed problem is not manageable.
H. Large Solids in Waste Pond.
It maybe necessary to remove large solids which
accumulates in bottom of pond that cannot be irrigated such
as dead :birds, trash from weed eating, etc. These items
shall be removed with shovel and bucket and disposed of at
county landfill,
IV. Clean Water Exclusion
A. Diversions & Waterways
Clean water diversions shall be maintained around the
waste storage pond. ]diversions shall be designed to carry
the 25 year - 24 hour runoff plus capacity to store some
sediment. Typical diversion is 1.0 feet deep on 0.5% slope
for small drainage areas.
V. Waste Nutrients
A. Waste Volume
The table below shows the estimated storage to spread
each year based on average rainfall and evaporation rates
and 12,520 gallons/day of wastewater from malting house.
Waste
Normal Capacity
I volume to
Estimated
' Percent.
Pump _.
Storage
of Pond
Spread each
Storage
Gai]ection
Level
Pond
@ Pump -Out
Year
Period
Feet Below
Level
Gallons/Year
morxths
Top of Daze
Gallons
Gal
Source
o
4,697,019
0.94
7.00s
�•Q"
B. Nutrient computations
a. Source - Waste Storage Pond
Briggs reference indicates that waste steep water is
yellow -brawn, readily putrescible, contains microbes (but
few or no pathogens), suspended organic matter, colloidal.
materials and a range of low -molecular weight substances:
dissolved salts, hexose and pentose sugars, amino acids,
organic acids (including phenolic acid) and phosphates
dissolved from surface of the grains and from the interiors
of broken grains. The liquid is prone to froth." Carolina
Malt Douse pre -cleans grain to remove small. grains, broken
grain, awns, rachises, etc. as much as practical.
9 Carolina Malt House, Inc
Waste Plan

Wastewater samples have been collected in the waste
pond. The following samples are representative of the
nutrient content that is expected in the pond.
Sample Date
TKN (mg/L)
3/12/201.9
24.30
3/17/2020
26.99
11/23/2020
26.9
78.19
Average TKN = 78.19/3 or 26.07 mg/L
The average total nitrogen (TKN) test value of 26.07
mg/l will be used to compute plant available nitrogen.
Based on evaluation by Agri -Waste Technology, Inc. a 50°
nitrogen factor should be used for the wastewater. The
plant available nitrogen (PAN) calculation is shown below.
TKN in Sample
PAN
26.07 ppm
TKN*0.5
= 26.07 ppm *0.5
= 13.035 ppm or
.109 lbs/1000 gal
Application field will allow application of 512 lbs of
Plant Available Nitrogen to be applied per year..
(0.109 lb/1000 gallons) and the 4,697,014 gallons`/year
wastewater volume are used to estimated nutrient content to
spread each year.
Nitrogen Volume = 4,697,014 gal/year x 0.1.09 lb N/1000 gal.
512 lbs
Michael Shepherd, Environmental Senior specialist, of
NCDA & CS, completed the nutrient management plan based on
the nitrogen nutrient amount, the soil fertility analysis,
irrigation design and crap planned at the site. The
nitrogen crop uptake value for fescue hay on Pacolet soil is
1.60 lb/acre..
Wastewater application shall be based on wastewater
volume and waste analysis to prevent overloading nitrogen on
the waste application fields.
NOTE: The irrigation system was designed with an
additional .irrigation zone that can he installed in future
if application fields need to be expanded to handle nutrient
loading. Permit would need to be updated to include
additional application fields if needed in future.
10 Carolina Malt House, Inc.
Waste Plan

C. Spray Irrigation Water Balance
See water balance computed by the "NC DENR Division of
Water Quality Water Budget excel program (versions)"" for
checking the size of the irrigation fields and waste pond
needed to handle an average 12,520 gal/day wastewater
production from malting house.
Summary of Water Balance Below:
Maximum Allowable Irrigation based on Ksat of 0.109
in/hr for the soil unit in application fields and drainage
factor of 0.1 is computed in the water balance.
Max. Allowable Irrig. Field 1 (Soil 1) 76.48 in/yr
Max. Allowable Irrig. Field 2A (Soil 1) 76.48 in/yr
Max. Allowable Irrig. Yield 23 (Soil 1) 76.48 in/yr
Design Irrigation - Field 1 54.06 in/yr
Design irrigation - Field 2A 54.06 in/yr
Design Irrigation - Field 2B 54.05 in/yr
Larry Thompson, soil scientist, evaluation recommends a
maximum loading rate not to exceed 1.1 in/week for soil I or
57.2 in/yr. 54.06 in/yr application rate from water balance
for the 12,520 gallons'/day wastewater volume is less than
the maximum allowable by Soil Scientist. See Soil Scientist
addendum to soil scientist evaluation dated June 12, 2017.
Flow to Field 1 (zone 1)- 1,614,160 gal/yr 1.1 acre
Flow to Field 2A (zone 2)- 1,614,760 gal/yr 1.1 acre
Flow to Field 2B (zone 3)- 1,467,665 gal/yr 1.0 acre
Soil Scientist also recommended an instantaneous
loading rate of 0.1 in/hr with a max. application rate of
0.25 in/hr not to exceed 0.25 hour/event. Irrigation system
was designed for this application rate.
Minimum Storage period recommended is 13.1 days in the
water balance. Carolina Malt House have a waste pond with
0.94 months of storage for the 12,520 gallon/day of
wastewater to ease management of irrigation system since
irrigation cannot occur during inclement weather conditions
or during crop maintenance periods. Storage will likely
help with managing greater amounts of wastewater in future
expansions.
Carolina Malt House, Inc
Waste Plan

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NUTRIENT MANAGEMENT PLAN, /1/2021

31112,021
Carolina Malt
Aaron Goss
12969 Statesville Blvd
Cleveland, NC 27013
704-412-9962
Owner/Manager/Producer Agreement
This plan has been developed by:
NCDA&CS DSWC
Michael Shepherd
191 S. Main St
Mocksville, NC 27028
336-940-8901
Developer Signature
I (we) understand and agree to the specifications and operation and maintenance procedures
established in this nutrient management plan for the farm named above. I have read and
understand the Required Specifications that are included with this plan.
Signature (owner)
Signature (manager or producer)
Date
This plan meets the minimum standards and specifications of the U.S.Department of Agriculture -
Natural Resources Conservation Service or the standard of practices adopted by the Soil and Water
Conservation Commission.
23M���
11 =1 MM
Technical Specialist Signature
Date
31212021

Carolina Malt House Waste Utilization Plan
3.1.2021 Plan Update
Wastewater samples have been collected in the waste pond and the following samples are
representative of the nutrient content that is expected in the pond after phase 11 is completed.
Sample Date
TKN (mg/L)
3/12/2019
24.30
3/17/2020
2639
11/23/2020
26.9
7&19
Average TKN = 78.19/3 or 26.07 mg/L
The average total nitrogen (TKN) test value of 26.07 mg/l will be used to compute plant available
nitrogen. Based on evaluation by Agri -Waste Technology, Inc. the 0.5 nitrogen factor should be used for
the Carolina Malt House wastewater. The plant available nitrogen (PAN) calculation is shown below.
TKN in Sample = 26.07 ppm
PAN = TKN*0,5
= 26.0,7 ppm *0.5
= 13.035 ppm or.109 lbs/1000 gal
Application fields will allow application: of 512 lbs of Plant Available Nitrogen to be applied per year.
(0.109 lb/1000 gallons) and the 4,697,014 gallons'/year wastewater volume are used to estimated
nutrient content to spread each year.
Nitrogen Volume = 4,697,014 gal/year x 0.109 lb N/1000 gal. = 512 lbs

Michael Shepherd,, Environmental Senior specialist, of NCDA&CS, completed the nutrient management
plan update based on the nitrogen nutrient amount,, the soil fertility analysis, irrigation design and crop
planned at the site. The nitrogen crop uptake value for fescue hay on Pacolet soil is 160 lb/acre.
Wastewater application shall be based on wastewater volume and waste analysis to prevent
overloading nitrogen on the waste application fields.
The table below shows the estimated storage to spread each year based on average rainfall and
evaporation rates and 12,520 gallons/day of wastewater from malting house.
Waste
Normal Capacity
Volume to
Estimated
Percent
Pump Level
Storage
of Pond
Spread each
Storage
Collection
Feet Below
Pond
Year
Period
@ Pump -Out
Top, of Dam
Months
Level.Gallons/Year
Gallons
Source
366,281
4,697,014
O94
100%
2.0'
3.27.2017 Plan
This plan was designed to address the waste water created during the malting process of grains at
Carolina Malt House, Waste water will be stored in a storage pond with a 90 day storage capacity of
366,000 gallons. The storage pond will have a total depth of 3-0.5' with O.S' designed for residua I
storage in the bottom, 8' designed for liquid storage, and 2' freeboard and will be equipped with a
synthetic liner.
This plan was developed based on the assumed nitrogen concentration of 0.36 lbs N/1000 gal. At this
time no coefficient of nitrogen mineralization and volatilization rate is known so the plan was designed
assuming all nitrogen will be available for uptake by the crop. In order to obtain this value in the NM
software, we entered a N value of 107.78 ppm with an operation type of dairy milk cow slurry. The
software uses a first year nitrogen coefficient of 0.4 for dairy milk cow slurry resulting in the 0.36 lbs N
/1000 gal value. After the operation is up and running and several waste samples have been collected
from the storage pond, a reevaluation of the nitrogen concentration should be conducted to determine
if the waste plan needs to be amended. Carolina Malt House will be working with NCDA&CS agronomist
to come up with a more realistic reduction for nitrogen mineralization and volatilization rates in the
future,
This plan shows that nutrients will not limit the application of waste water on irrigation fields. A total of
3.2 acres will be irrigated such that nutrients are not over applied to any field. The limiting factor on the
irrigation fields will be the hydraulic loading rates of the Pacolet soils. The soils evaluation report from
Thompson Environmental Consulting indicated a maximum instantaneous application rate of 0.2S in/hr
with a maximum irrigation duration of 0.2S hours in order for the amount of applied wastewater not to

exceed O.1in/hr. Please refer to the soil evaluation report and the, irrigation design for more in-depth
details an irrigation setup, events, and application fields.
All of the irrigation fields are made up of Pacolet soils with a fescue hay crop. Each field in the plan
corresponds to the irrigation zones detailed in the irrigation design. This fescue hay crop has a
Phosphorus remove rate of 57 lbs P205/acre. With the low soil Phosphorus index and low waste
nutrient Phosphorus measurement, the nutrient plan is based on Nitrogen utilization. Historically the
irrigation fields were fescue pastureland for beef cattle and has not previously received any waste
water.
The fescue hay crop for all irrigation fields should be properly maintained and harvested to ensure
adequate Nitrogen uptake is achieved.Refer to the crop notes section of this plan or consult your local
agronomist for proper fescue hay care,
I. The collection and storage facilities shall be properly maintained and operated at all times; this
also includes the irrigation equipment.
I A suitable vegetative cover shall be maintained on all land application sites and buffers in
accordance with the Waste Utilization Plan. No waste may be applied on fields not approved by or
prepared in accordance with the Waste Utilization Plan.
An acceptable pH of the soil shall be maintained on all land application sites to insure an
optimum yield for the crop(s) being grown.
4. The plant available nitrogen (PAN) application rates and hydraulic loading rates identified in the
Waste Utilization Plan shall not be exceeded.
5. Application of wastewater on land which is used to grow crops for direct human consumption
(e.g., strawberries, melons, lettuce, cabbage, etc.) shall not occur within 30 days prior to or during the
planting of the crop or at any time during the growing season, or in the case of fruit bearing trees, 30
days prior to breaking dormancy. For fiber and food crops, which undergo further processing,
application of wastewater shall not occur within 30 days of harvesting. If waste is to be applied to bare
soil, the waste shall be incorporated into the soil within, 24 hours after the application on land.
6. Domestic wastewater from showers, toilets, etc. shall not be discharged into the waste
management system. Wash -water may be added to the wastewater as long as detergents and
disinfectants are used which have been labeled as readily biodegradable by the manufacturer.

7Solid materials such as, but not limited to, bottles, gloves or any other solid waste from the
malting operation, shall be prevented from entering the waste management system and shall be
disposed of properly.
9. irrigation equipment must be capable of applying the wastewater on the application site
specified in the Waste Utilization Plan and at rates not to exceed agronomic and hydraulic loading for
the sites.
10. Wastewater shall not be applied to wetlands or surface water or shall not reach wetlands or
surface waters of the state by runoff, drift, manmade conveyances (pipes or ditches), direct application,
or direct discharge during operation or Irrigation. Any discharge of wastewater, which reaches surface
water, is prohibited. Illegal discharges are subject to the assessment of civil penalties for every day the
discharge continues.
11. Wastewater shall not be applied to saturated soils, during rainfall events, or when the soil
surface is frozen. When wastewater is to be applied on acres subject flooding in grassland, the
wastewater may be irrigated, provided the application does not occur when flooding is predicted.
12. Wastewater shall not be applied closer than 100 feet to surface water. This distance may be
reduced to 25 feet for waters that are not perennial provided adequate vegetative filter strips are
present.
13. Wastewater shall not be applied closer than 100 feet to wells,
14. Wastewater shall not be applied closer than 150 feet to property lines other than those owned
by the landowner.
IS. Wastewater shall not be applied closer than 50 feet to public right-of-ways.
16. Wastewater shall be tested within 60 days of utilization and soil shall be tested at least annually
at crop sites where waste products are applied. Nitrogen shall be the, rate -determining element. Zinc
and copper levels in the soils shall be monitored and alternative crop sites shall be used when these
metals approach excess levels. Soil test and waste analysis records shall be kept for 5 years.

17. Wastewater shall be applied at rates not to exceed the soil infiltration rate. No ponding shall
occur.
18. Records of waste application shall be maintained to establish actual application rates. The
records will include date of application, amount of wastewater applied per acre by hydrant or field
number, most recent waste analysis and soil test report, and the realistic yield expectation (RYE)
nitrogen rate. Waste application records shall be maintained for 5 years.
19. Proper calibration of application equipment should be done to ensure uniformity and accuracy
of spreading rates.
20, it is the responsibility of the owner to secure an update of the, waste utilization plan when there
is a change in the operation, method of utilization or available land.

[W. Me W I LTI WE
Nutrients applied in accordance with this plan will be supplied from the following
source(s):
Commercial Fertilizer is included in this plan.
U 1021
Carolina Malt House waste water generates 4,697,014 gaislyear. This production facility has
waste water storage capacities of approximately 30 days.
Estimated Pounds of Plant Available Nitrogen Generated per Year
Injected
613
Incorporated44 wks or less
following application
613
Incorporated-5 wks to 3 mos
following application
511
Broadcast
511
Irrigated
511
Max. Available
PAN (lbs)
Actual PAN
Applied (lbs)
PAN Surplus I
Deficit (lbs)
Actual Volume
Applied (Gallons)
Volume Surplus/ Deficit
(Gallons)
Year 1
511
512
(1)
4,706,877
(9,863)
31212021 8:42!53 AM 1 11

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The table shown below provides a summary of the crops or rotations included in the plan for each field. Realistic Yield estimates
and Plant Available Nitrogen (PAN) recommendations are also provided for each crop as well as the crop's P205 Removal Rate.
The Leaching Index (LI) and the Phosphorous Loss Assessment Tool (PLAT) Rating are also provided for each field, where
available.
Notes: 1. In the tract column, - symbol means leased, otherwise, owned.
--------- ----
Ll Potential Lepching Technkzd,Gulqaoce
Low potential to contribute to soluble nutrient None
<2 leaching below the root zone.
Moderate potential to contribute to soluble nutrient Nutrient Management (590) should be planned.
> 2 & < = 10 leaching below the root zone.
High potential to contribute to soluble nutrient Nutrient Management (590) should be planned. Other conservation
leaching below the root zone. practices that improve available water holding capacity of soil and
improve nutrient use efficiency should be considered. Examples are
> 10 Cover Crops (340) to scavenge nutrients, Sod -Based Rotations (328),
Long -Term No -Till (778), and edge -of -field practices such as Filter
Strips(393) and Riparian Forest Buffers (391).
3/212021 &43:09 AM 1/ 2

The Following crop note applies to field(s): 1, 2A, 2B
Fescue: Piedmont
Adaptation: Well -adapted.
In Lhe Picdm.onl, tall rescue can be plaritcd A u& 20 to Oct. 10(bcst)and Feb. 15 to Mar, 20. Foi-
pure-stand broadcast seedings use 20 to 30 1 b/ac., for drilled use 15 to 20 lb/ac. seed. Use cerfiriedwed
to avoid hilroducing weeds or annual ry-egrass. Plant seed 0.25" to 0.5" deep for pure stands, 0.25" fil
mixture with clovers. Soil test, for preplant and mainlenance lime, phosphorus, and potassium
reconuilendation.s. Apply 40 to 60 lb/sac nitrogen at planting for pure stands only. Do not apply N l'or
mixtures with clovers but: use proper legume inoculation techniques. Apply 150 to 200 lb/ac, N to
pure -stand fescue for hay production, reduce N rates by 25'X0 to 50%0 for grazing Apply N r Feb, I to Mar,
20 and Aim, 20 to Sept. 30, with equal arrIOLUILS in each window. Reller to NCSLJ Technical Bulletin 305
Production and Uti Ii/ation of Pastures and Forages in Nordi Carolina for additional information or
consult your regional agronomist or extension agent for assistance,

■ 1 a A
AGRI-''VIIA►STE TECHNOLOGY, INC MEMORANDUM,
2/3/2021

MEMORANDUM
PREPARED FOR: Mr. Aaron Cross, Carolina Malt House, .Inc.
PREPARED BY: Jeff Vaughan, Ph.D.
Senior Agronomist/Soil Scientist
DATE: February 3, 2021
As requested, the following details methodology for properly computing plant -available nitrogen.
(PAN) from land applied organic materials such as manure, biosolids, lagoon liquid, compost,
etc. In general, only a portion of the total nitrogen in land applied organic materials is plant -
available. This is because a portion of the total nitrogen is lost, generally to the atmosphere, via
various pathways or remains bound in unavailable nitrogen forms in. the soil. The portion of
total nitrogen in land applied organic materials that is plant -available can range from 40-1000/o
(of the total nitrogen) and is based on the type of material, the land application method, and
tillage practices after land application.
We have reviewed the infornnation that you provided to us for the wastewater treatment system
at the Carolina Malt House. The wastewater treatment system appears to use an anaerobic
lagoon to collect, treat, and store the wastewater, The wastewater is then land applied to tall
fescue as a plant nutrient source via surface irrigation. Based on the attached document from the
North Carolina Department of Agriculture and Consumer Services, this type of wastewater
would be best classified as Lagoon Liquid, Anaerobic, Other ("'Waste Code ALO) with surface
irrigation application. The plant -available nitrogen factor for this type of land applied organic
material would then be 0.5, or 50% of the total nitrogen (page 10, Table 3) expressed as Total
Kjehdahl Nitrogen (TKN). As example calculation is below for reference:
TKN in sample = 30ppm
PAN = TKN * 0.5
30ppm *0.5
15ppm or 0, 125lbs/1 000gal
We appreciate the opportunity to assist you. Please contact us with any questions, concerns, or
comments,

Waste and Compost Analysis Guide
Plant/Waste/Solution/Media Analysis Section
Agronomic Division
N.C. Dept. of Agriculture & Consumer Services
[phone]
Michelle McGinnis, Ph.D., Agronomist
Jan Queen, Chemist
Mark Buchanan, Chemistry Supervisor
Catherine Stokes, Communication Specialist
Brenda Cleveland, Section Chief
July 2013 revision

������ Contents
"�oxm^evxus
1. Overview of Agronomic Division
Z.Overview mfWaste Analysis and Nutrient Management ---------__
Waste application rate -limiting factors ................................... .............................. .......................... 2
Additional resources ................................................................ ................. ... ___ .......................... 3
3. Anayltes, Measures, 8bCalculations onWaste Analysis Report —__--------_
Standard analysis: Tests conducted for basic fee ($5)............................................. _................. '4
Additional analysis upon request: Tests conducted for additional fee ($l8) ..................................... 4
Nutrients available for first crop .................................. .... ................................... ...... ................ 5
4.Methods for Waste Analysis ....................... ... —..................................................... ---_........ lR
Solid Waste Analysis Methodology -----------_
Liquid Waste Analysis Methodology ... ... --... ........................................................................ 20
List nfTables
Table 1. Analytes & measures included with standard and additional lab analysis ................................6
Tabke2. Lab tests associated with standard analysis bpwaste code ............................. ........ ................ 7
Table 3. cncffickents--------------------------.. 10
Table 4. ICP wavelengths used to quantify total elemental concentrations .......................................... 19
Julyzco Nczmu&csWamomuCo^nx~/A.^ly,�Gmudc i

1. Overview of Agronomic Division
The Agronomic Division Mission is to provide N,C. residents with site -specific diagnostic and
advisory services to increase agricultural productivity, promote responsible land management and
safeguard environmental quality. The Agronomic Division is comprised of four sections: (1) Field
Services, (2) Soil Testing; (3) Nematode Assay; and (4) Plant, Waste, Solution and. Media Analysis.
The Field Services Section has a staff of 13
regional agronomists to advise and educate
farmers, agriculture consultants, fertilizer
dealers, homeowners and other state residents
regarding agronomic sampling techniques,
responsible and cost-effective fertilization
practices, interpretation of agronomic lab results
and the implementation of agronomic
recommendations. For further information, see
www.ncagr..gov/agronomi/rahome.htm-
Soil Testing provides soil nutrient indexes as
well as weight per volume, pH., acidity, percent
humic matter, soil class and soluble salt levels
as described in Crop Fertilization Based on
North Carolina Soil Tests. The Soil Test Report
provides precise lime and fertilizer
recommendations for specific crops and soil
classes. For further information, see
www.ncagr.gov/agronomi/sthome.htm.
Nematode Assay identifies plant -parasitic
nematodes and estimates population size and
relative hazard to the crop. The Nematode
Assay Report provides recommendations for
control of plant -parasitic nematodes. For further
information, see
www.ncagr.gov/agronomi/nemhome.htm.
Plant Tissue Analysis measures nutrient levels
within crop tissue and identifies nutrient
deficiencies and toxicities. The Plant Analysis
Report provides recommendations for
adjustment of crop fertilization programs. For
further information, see
www.ncagr.gov/agronomi/uyrplant.htm.
Waste Analysis determines nutrient levels in
farm (such as animal manure), industrial,
municipal and composted waste materials. The
Waste Analysis Report provides estimates of
first -crop nutrient availability and
recommendations for the environmentally sound
use of waste material as a plant nutrient source.
For further information, see
www.ncagr.gov/a.gronomi/uyrwaste.htm.
Solution Anatysi5 measures nutrient
concentrations as well as pH, electrical
conductivity (soluble salts) and total alkalinity
levels of water used in agricultural production,
such as irrigation water, nutrient solutions and
livestock drinking water. The Solution Analysis
Report provides an assessment of potential
problems and recommendations for their
management. For further information, see
www.ncagr.gov/agronomi/uyrso9n.htm,
Media Analysis measures nutrient
concentrations as well as pH Lind electrical
conductivity (soluble salts) of soilless media
used for containerized crop production. The
Media Analysis Report helps growers
troubleshoot problems and. fine-tune fertilization
programs. For further infonnation, see
www.ncagr.-gov/agronomi/uVrmedia.htm.
.Dine 2012 lvCDA&C's WaAe and, Compost AT)alysis Gtide;

2. Overview of Waste Analysis and Nutrient Management
The Agronomic Division's Waste Analysis Lab
analyzes liquid and solid waste samples from
farm, municipal and industrial sources to assess
their use in agriculture. Analyses of animal
waste from liquid management systems for
total Kjeldahl nitrogen (TKN), total
phosphorus, copper and zinc are certified by
the N.C. Department of Environment and
Natural Resources (NCDENR) Division of
Water Quality.
The Waste Analysis Lab also analyzes compost
samples. Commercial cornposters of waste
products may be required to test the chemical
properties of the compost in order to comply
with NCDENR regulations. Compost samples
are also submitted by compost users to
determine how chemical properties might limit
use or impact application rates in gardens or
landscapes.
The Waste Analysis Report provides total
nutrient concentrations (nitrogen, phosphorus,
potassium, calcium, magnesium, sulfur, iron,
manganese, zinc, copper, boron) as well as
estimates of first -year, plant -available nutrient
concentrations (nutrients available to the first
crop grown in units of lb/ton or lb/1000 gal.).
Additional chemical measures may also be
provided on the waste report, such as levels of
sodium; pH; electrical conductivity (soluble
salts); carbon; carbon -to -nitrogen ratio (C:N);
calcium carbonate equivalence (CCE%);
agricultural time equivalent (ALE); heavy
metals (lead, nickel, cadmium); chloride; and
inorganic nitrogen (ammonium and nitrate
nitrogen).
Nutrients -available -for -first -crop values are
based on estimates of mineralization rates for
the specific waste type (e.g., anaerobic lagoon
liquid) and source (e.g., swine) as well as
application method (e.g,, irrigation). These
estimated values are influenced by factors such
as the specific nature of the waste material, soil
physical properties (i.e., texture, soil moisture),
soil chemical properties (i.e., pH, cation
exchange capacity), soil and air temperature,
and weather. Mineralization rates used to
calculate nutrient availability arc reviewed and
revised periodically using current scientific
literature.
Knowledge of available nutrients and other
chemical properties associated with waste
applied to land, in conjunction with site -
specific factors, is the basis for efficient
nutrient management and responsible land
stewardship. Waste application rates are
usually limited by levels of nitrogen,
phosphorus, zinc, copper, boron, sodium or
CCE% as discussed below.
Waste application rate -limiting factors
Nitrogen (N)
Generally, the available N in the waste
determines the rate of application, unless
another element or chemical property is more
restrictive. N can be applied at rates dctennined
by the realistic yield expectation (RYE) of a
specific crop by soil type. Rates using the RYE
approach are available online at
nutrients.soil.ncsu.edu/yield.s/. Contact the N.C.
Interag-cricy NqLri.cLIt Management Committee
for guidelines when a specific RYE is not
available.
Phosphorus (P)
Rates of waste application should be based on
estimated available P when the site is
vulnerable to off -site P movement. The N,C.
Phosphorus Loss Assessment Tool (PLAT) is
used to assess the potential for P transport from
fields to surface water. When animal manure or
organic by-products are used in crop
production, this software toot can identify
whether N or P is the application -rate -
determining nutrient. PLAT ratings are
July 2012 NCDA&CS Wzistc and Compost Amlysis Guide

interpreted as follows: lore or medium, the
manure or organic by-product can be applied
based on the crop's N requirement; high,
application rate is limited to P removal from
the site; very high no additional P should be
applied.
Zinc (Zn) and copper (Cu)
For sites receiving animal waste, monitoring
soil Zn and. Cu levels is required by Animal
Waste Management Rules (l 5A NCAC 2T).
Application rates should be limited when soil
Zn and/or Cu levels are excessively high and/or
the waste product has a high Zn and/or Cu
concentration. Under these conditions, it is also
advisable to monitor crop nutrient
concentrations with tissue analysis. These
practices will help prevent excess Zn and/or Cu
accumulation in the soil.
For all crops except peanuts, the NCDA&CS
soil -test Zn-index (Zn-1) and. Cu-index (Cu-1)
caution level is 2000 (-142 lb Zn/acre and —72
lb Cu/acre) and the critical toxic level is 3000
(-21.4 lb Zn/acre and —108 Cu lb/acre).
NCDENR requires that a technical specialist be
contacted to discuss options for future manure
applications when Zn and/or Cu are at the
caution or critical toxic level. At the caution
level, growers should monitor crop growth and
appearance and maintain a soil pH of at least
6.0 while searching for alternative fields better
suited for application of animal manure. At the
critical toxic level, all application of animal
manure or organic by-products should cease
and a pH of at least 6.0 should be maintained.
Peanuts are much more sensitive to Zn than.
other crops: the caution level is 300
(-21 lb/acre) and the critical toxic level is 500
(-35 lb/acre).
Sodium (Na}
Waste that contains high. sodium in relation to
calcium and/or magnesium can cause problems.
A high level of sodium in the soil can degrade
soil structure (reduced infiltration and
permeability) and/or become toxic to crops.
Sodium may also damage foliage when liquid
waste is applied in an overhead irrigation
system to a growing crop. Regular soil testing
is recommended to monitor sodium
accumulation where the waste is routinely
applied. Safe application rates of sodium
depend on many factors, including soil texture,
soil calcium and magnesium levels, rainfall,
irrigation volumes and crop.
Boron B
Although B is an essential nutrient, the level.
required by a crop and the B toxicity level of
that crop are very narrow. Therefore, consider
the waste B level and limit B application to no
more than 1-3 lb B per acre per year. Since B is
not measured in NCDA&CS soil analysis,
monitor B status in crops with tissue analysis.
Calcium carbonate equivalence (CCE%)
and agricultural liming equivalent (ALE)
CCE% represents the acid -neutralizing capacity
of a material expressed as weight percentage of
calcium carbonate. For waste (materials with
liming potential (e,g., lime -stabilized biosolids,
poultry layer litter), the application rate may be
limited by a high CCE%. Waste with a high
CCE% should only be applied at rates needed
to increase soil pH to the desired target.
Overapplication can Lead to high soil pH, which
may limit micronutrient availability. When
CCE% is measured, ALE is also calculated.
ALE indicates the amount (tons or gallons) of
waste required to equal the neutralizing value
of one ton of agricultural grade limestone.
Additional resources
Crop Fertilization Based can North Carolina
Soil Tests
Nutrient Management in North Carolina---
htt ://nutrients. soil.mcsu.edu/
SaJmplinfor WeIste Analysis
Understanding the Waste Analysis .Rcort
Waste `�aialysi.s Inti'ovt agricultural
Productivity & Environmental Quality
Waste Sample Information form AD- ,)
JuIv 2013 NC;I').A&,C R Waste and d"`ornpot Analysis Guide

3. Analytes, Measures & Calculations on Waste Analysis Report
Standard analysis:
"Tests included for the basic fee ($5)
Concentrations of nitrogen (N), phosphorus (P),
potassium (K), calcium (Ca), magnesium (Mg),
sulfur (S), iron (Fe), manganese (Mn), zinc
(Zn), copper (Cu), boron (B) and sodium (Na)
are provided for all waste samples submitted to
the lab (Table 1). Units are parts per million.
(ppm) or, more specifically, milligrams per liter
(mg/L) for liquid and milligrams per kilogram
(mg/kg) (dry -weight basis) for solid waste
samples. With the exception of liquid waste N,
all measures are of total nutrients. Liquid waste
N is measured as total Kjeldahl nitrogen
(TKN). TKN does not include nitrate nitrogen.
Standard analysis may include measurements
of pH, electrical conductivity (EC) [a measure
of soluble salts (SS)], percent solids or dry
matter percent (UM%o) and carbon (C) for
certain types of waste samples (particularly
composted materials), according to the code
specified by the client on the Waste SatW21e3
Ita;ti�t nation_forrn (AD-9). Table 2 indicates the
specific tests performed automatically based on
each waste code. Upon request, these measures,
as well as chloride, can be provided at no
additional charge for any waste sample, with
the following exception: carbon can only be
measured for solid waste samples.
Units for EC (or SS) are 10-5 S/cin, and units
for C are ppm or mg/kg (dry -mass basis)
(Table 1). Dry matter percent (DM%) is
determined for all solid waste samples
according to Eq. [1]. When C is analyzed, the
C-to-N ratio (C:N) is calculated according to
Eq. [2].
[ 1 ] DM% = (dry wt. - - fresh wt.) x 100
[2] C:N = C (mg/kg) N (mg/kg)
Additional analysis upon request:.
Tests conducted for additional fee ($10)
`Special tests' (heavy metals, inorganic
nitrogen and/or calcium carbonate equivalence)
can be performed upon. request (Table 1). Each
test costs an additional $10 per sample.
Heavy metals (HM): Analysis of HM includes
cadmium (Cd), lead (Pb) and nickel (Ni). Units
are ppm or mg/L for liquid and ppm or mg/kg
(dry -weight basis) for solid samples.
Inc, -game nitrogen {ITN-N): The l.l`+I-N value
represents the sum of measurements of nitrate
nitrogen (NO3-N) and ammonium nitrogen
(NHS-N), as shown in Eq. [3]. Measurement of
NO3-N includes any nitrite nitrogen (NO2-N) in
the sample. When analyzed, NO3-N is added to
liquid waste TKN to report total N, as shown in
Eq. [4]. Organic nitrogen (OR-N) is calculated
according to Eq. [5]1. All units are pprn [trig/L
for liquid and mg/kg (dry -weight basis) for
solid samples].
[3] IN-N = NO3-N + NHS-N
[4] Total N = TKN + NO3-N (liquid)
[5] OR-N = Total N —1N-N
Percent calcium carbonate equivalence
(CCE%)and agricultural time equivalent
ALE CCE% is a measure of the acid -
neutralizing capacity of a waste material and is
expressed as a percentage of pure calcium
carbonate (on a dry -weight basis for solid waste
samples). The ALE is calculated according to
Eqs. [6] and Eq. [7] for solid and liquid waste
samples, respectively. The assumption is made
that one gallon of liquid waste weighs 8.34
pounds.
July 2013 NCI)A &CS Wa. (e anal Compost Analysis Guido

The ALE indicates the quantity of waste
material that will provide a liming effect
equivalent to one ton of agricultural grade
limestone (90�% CaCO3). ALE is reported in
units of tons for solid waste samples and 1000
gallons for liquid waste samples.
[6] ALE (tons) = 1800 - [(DM% - 100) x
(CCE% = 100) x 2000]
[7] ALE (1000 gallons) = 1800 = [(CC.E%
- 100) x 8340]
Nutrients available for first crop
Estimates of nutrients available for the first
crop (or first -year, plant -available nutrients) are
provided on the Waste Analysis Report. The
Waste Analysis Lab's calculations are based on
mineralization rate estimates for specific waste
sources (Table 22) and anticipated nutrient loss
associated with the proposed waste application
method. The four application methods are
• broadcast (BR) - waste broadcast on soil
surface and left uncovered for one week or
longer;
• injection (IN) — waste injected directly
into the soil and covered immediately;
• irrigation (IR) waste applied through the
irrigation system and left uncovered for one
week or longer; and.
• soil incorporation (SI) waste broadcast
on soil surface and plowed or disked into
soil within two days.
The first -year -nutrient -availability coefficients
for each waste source and application method
are included in _Table 3. All values for first -
year, plant -available nutrients are calculated
according to Eqs. [8] and [9] for solid and.
liquid wastes, respectively, where NAC =
nutrient availability coefficient (listed in
Table 3), NM = nutrient multiplier and DM%o
dry matter percent. The NM is only relevant for
P and K to allow expression of P as phosphate
(P205) and K as potash (K20). The NM for P is
2.29 and the NM for K is 1.20. For all other
nutrients and elements, the NM is 1.
[8] Nutrient available (lb/ton) — [nutrient
concentration (mg/kg) . 1,000,000] x
NAC x NM x 2000 x (L)M%o 100)
[9] Nutrient available (lb/ 1000 gal)
[nutrient concentration (g/L) -
1,000,0001 x NACx NM x 8340
Unless the inorganic nitrogen (IN-N) test was
conducted, the available nitrogen calculations
are based on total nitrogen (solid waste) or
TKN (liquid waste). When clients request
measurement of IN-N, available nitrogen (N) is
deterinined as the sum of available organic
nitrogen (OR-N) and available IN-N, as shown
in Eq. [10].
[10] Available N = available IN-N +
available OR-N
Conversion of units
If the lab analyzed samples as solid waste but
the client plans to apply the waste in liquid.
form, Eqs. [ 1 I ] and [ 12] can be used to convert
from solid waste application units (tons) to
liquid waste application units (1000 gallons),
and vice versa. These conversions assume that
one gallon of liquid waste weighs 8.34 pounds.
[11] lb/ton x 4.17 = lb/1000 gal.
[12] lb/1000 gal. x 0.24 = lb/ton
For some applications, such as use of compost
on gardens or landscapes, :it is useful to plan for
application of pounds to an area of 1.00 or 1000
ft' rather than tons per acre. Refer to Eqs. [13]
and [14] for these conversions.
[13] tons/acre x 45.9 = pounds/1000 ft2
[14] tons/1000 ftz x 4.6 = pounds/100 ft`
Jah, 21113 NC'DA&C'S IX'as(o and ("ompos,( Anatvsis Guide

Table 1. A.nalytes & measures included with standard and additional lab analysis
Category 8c waste codes'-
A.nalyte l Measure
Abbreviation
Units
Standard analysis
Nitrogen
N
ppm3
Measured for
Phosphorus
P
ppm
ALL
Potassium
K
ppm
waste samples
..... ...
_... ...........
(all waste codes)
Calcium
Ca
ppm
Magnesium
Mg
ppm
Sulfur
S
ppm
Iron
Fe
ppm
Manganese
Mn
ppoas
.Zinc
Zn
ppm.
Copper
Cu
ppm
Boron
B
Win
Sodium
Isla
ppm
Standard analysis
pH
--
--
Measured for
Dry matter percent
DM%
percentage
SOME
waste samples
Electrical conductivity
...... _ .....
EC
1 Q S/cm
(as indicated by
(soluble salts}
(SS)
waste code in Table 2)
Carbon
C
ppm
Additional analysis
Inorganic nitrogen
IN-N as
ppm
(nitrate & ammonium nitrogen) a
NO3-N & NH4-N
(`Special Tests')
Heavy metals:
...... .......
HM:
Included
Cadmium, lead, nickel
Cd, Pb, Ni
ppm
UPON REQUEST
�
5
Calcium carbonate equivalence-5
o
CCE /r
percentage:
for any Waste Code
(agricultural liming equivalent)
(ALE)
(tons or 1000
($10 per test)
gallons)
1 Waste code descriptions are listed on table 2 and on page 2 of Il crstc Scrnrnlc
Juf �rntc�t��� _ c�in�_ a Dlt
2 Liquid waste -N is measured as Total
Kjeldahl Nitrogen (TKN); solid waste N is measured as total N.
1 Units of parts per million (ppm) are
milligrams per liter (mg/L) for liquid waste and milligrams per kilogram (mg/kg)
(dry -weight basis) for solid waste.
4 NO3-N results also include any nitrite
nitrogen (NO2-N) in the sainple.
5 CCE% is defined as the acid -neutralizing capacity of a sample expressed as a percentage of pure calcium
carbonate.
6 ALE is the calculated quantity (tons
or 1000 gallons) of material that will provide the equivalent liming
effect of one
ton of agricultural grade limestone.
July 2013 N('T)A&iC S Waste and Compost Anatysis Guide 6

Table 2. Lab tests associated with standard analysis by waste code
Tests conducted with standard waste analysis
Waste
Waste
Waste
Type
Sourced
Code!
Mineral
DM% 4
pH
EC (SS)
C
nutrients -
Poultry
ALP
X
X
Lagoon Liquid
Swine
ALF
X
X
— Anaerobic
(farrow to wean)
Swine (except
ALS
X
X
farrow to wean)
Other
ALO
X
X
Poultry
ASP
X
?
Lagoon Sludge
Swine
ASS
X
?
— Anaerobic
Other
ASO
X
?
. . . .......
Beef
LSB
X
?
Manure -
Dairy
LSD
X
?
Liquid Slurry
Poultry
LSP
X
?
Other
LSO
X
I?
--
---
-
Beef
SSB
X
X
Manure -
Dairy
SSD
X
X
Surface Scraped
or Stockpiled
Horse
SSI'l
X
X
Swine
SSS,
X
X
Other
SSO
X
X
Broiler Breeder
HBB
X
X
Poultry —
Broiler Pullet
HBP
X
X
House Litter
Broiler
IILB
X
X
Layer
HLL
X
X
Layer Pullet
I-ILP
X
X
Turkey
HLT
X
X
Other
HLO
X
X
Beef
FCB
X
X
X
X
X
Waste
Crop Residue
FICC
X
X
X
X
X
Composted
Dairy
FCD
X
X
X
X
X
Sheep
FCE
X
X
X
X
X
Goat
FCG
X
X
X
X
X
Horse
FCH
X
X
X
X
X
Poultry
FCP
X
X
X
X
X
Swine
ECS
X
X
X
X
X
Veg. Residue
FCV
X
X
X
X
X
Other
FCW
X
X
X
X
X
Poultry Mort.
FPM
X
X
X
X
X
Swine Mort.
FSM
X
X
X
X
X
July 2013 NC DA&CS Wame and Compost Analysis Gukle 7

Table 2. (continued)
Tests conducted with standard waste analysis
Waste
Waste
Waste
Type
Sources
CodeZ
Mineral 3
DM% 4
pH
EC (SS)
C
nutrients -
Bark/Sawdust
N RS
X
X
X
X
X
Waste
Crop Residue
NCR
X
X
X
X
X
Noncomposted
Veg. Residue
NVR
X
X
X
X
X
Other
NCW
X
X
X
X
X
Composted
loc
X
X
X
X
X
Industrial ---
Aerobic
TOE
X
?
Miscellaneous
Lime Stabilized
IOL
X
?
Anaerobic
ION
X
?
Raw
TOR
X
?
Chem Ox (Cl)
IOX
X
I?
--
--
--
Other
100
X
?
Composted
PHC
X
X
X
X
X
Industrial —
Aerobic
PHA
X
Pharmaceutical
Lime Stab.
PHL
X
?
Anaerobic.
PHN
X
Raw
PHR
X
--
Chem Ox (Cl)
PHX
X
?
Other
PHO
X
?
Raw
PLR
X
?
Industrial —
Aerobic
PAE
X
?
Poultry
Anaerobic
PAN
X
?
Lime Stabilized
PLS
X
?
Chem Ox (Cl)
PDX
X
Composted.
PCW
X
X
X
X
X
Other
PLO
X
?
Composted,
SAC
X
X
X
X
X
Industrial —
Raw
SAR
X
?
X
Stack Dust/Ash
Other
SAO
X
?
X
Aerobic
TAE
X
Industrial --
Anaerobic
TAN
X
Textile
Composted
TCW
X
X
X
X
X
Lime Stabilized
TLS
X
?
Chern Ox (Cl)
TOX
X
?
Raw
TXR
X
?
Other
TXO
X
JuIv 2013 NCDA&CS Wcasw and Cornpot Analy'sis, Guide R

Table 2. (continued)
'Tests conducted with standard waste analysis
Waste Waste Waste . . .....
Type Source�� Code-2 Mineral 3 DM% 4 pH EC (SS) = C
nutrients
Municipal Aerobic MAE X
Anaerobic MAN X
--
Comp. Sludge MCS X X X X X
Comp. Yard W. MCY X X X X X
Lime Stabilized MLS X ?
Chem OX (Cl) MOX X ?
Other MWO X ?
1 Standard waste analysis is conducted for S5 per sample. "X" indicates the test is automatic; "--" indicates the
test is NOT automatically included with the specific waste code. If requested, pH, EC and/or carbon can be
measured for samples with other waste codes at no additional cost. Carbon is measured for solid waste
samples only. The "T' symbol indicates the test may or may not be included and will be determined upon
receipt at the lab.
2 Waste code descriptions are listed in Table 2 and on page 2 of PPasteSan p c In brinalLOL qjbrn (D.
L_L_ 1 A9)
3 Mineral nutrients include concentrations (ppm) of nitrogen (N), phosphorus (P), potassium (K), calcium (0),
magnesium (Mg), sulfur (S), iron (Fe), manganese (Mn), zinc (.'fin), copper (Cu), boron (B) and sodium (Na).
With the exception of liquid waste N, all measures are total nutrient concentrations-, liquid waste N is
measured as Total Kjeldahl Nitrogen (TK.N).
' DM% — dry matter percent; DM% is Measured for solid waste samples only. For codes in which "?" is
indicated, the determination of the sample as solid or liquid waste is made the by lab personnel based on
visual inspection. Generally, samples with DM% > 8-10% (as determined by visual inspection) are
categorized as solid waste; samples with DM% < 8-10 are categorized as liquid waste. EC = electrical conductivity [a measure of soluble salts (SS)] and is reported in units of 10-5 S/Cm.
6 C! = carbon; C is measured on solid waste samples only and is reported in units of ppm or mg/kg.
July 2013 NC DA&CS Waste and Compost Andysss Oijide

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4. Methods for Waste Analysis
Solid Waste Analysis Methodology
Sample handling
3
Prior to analysis, a subsample (-250 cm ) is
weighed (Mettler PM4800; Mettler -Toledo,
Hightstown, NJ), dried overnight (12-24 hr) at
80 T, reweighed, and ground with a stainless
steel grinder (Intermediate Wiley Mill; Arthur
H. Thomas Co.; Philadelphia, PA) to pass
through a 20-mesh (1-nun) screen (adapted
from Hoskins et al., 2003). Percent solids, or
dry matter percent (DM%), is calculated by the
following equation: DM% = (dry weight
fresh weight) x 100,
Nitrogen (N) and carbon (C)
Total N and C concentrations are determined
by oxygen combustion gas chromatography
with an elemental analyzer (NA1 500; CE
Elantech Instruments; Lakewood, NJ) (AOAC
1990b; Campbell 1992) on a 5— to I 0—nig
aliquot of the dried/ground sample. Results are
expressed in parts per million (ppm)
[equivalent to mg/kg] on a dry -weight basis.
Inorganic nitrogen (IN-N) fraction
concentrations include nitrate nitrogen + nitrite
nitrogen (NO_j-N + NO2-N) (reported as NO3-N
on the Waste Analysis Report) and ammonium
nitrogen (NH3-N + NH4-N) (reported as NH4-N
on the Waste Analysis Report). NO3-N is
determined by nitrate -hydrazine reduction
(Kempers 1988; Skalar Analytical 1995b) and
NH4-N is determined modified Berthelot
reaction (adapted from Krom 1980; Skalar
Analytical 1995a) with an auto -flow
spectrophotometric analyzer (San` Segmented
Flow Auto -Analyzer, Skalar Instruments,
Breda, The Netherlands) following a delonized
water (I g / 25 mL) 30-minute extraction on a
reciprocating shaker (Wrist Action Model 75;
Burrell Corp. Pittsburgh, PA). Results are
expressed in parts per million (ppm)
[equivalent to mg/kg] on a dry -weight basis.
Organic N (OR-N) is calculated as the
difference between total N and IN-N
concentrations. Results are expressed in parts
per million (ppm) [equivalent to mg/kg] on a
dry -weight basis.
Phosphorus M, potassium (K), calcium
(Ca), sulfur (S), magnesium (Mg), boron (B),
copper (Cu), iron (Fe), manttanese (Mn),
zinc (Zn), sodium (Na), nickel (Ni), cadmium
,(Cd), lead jPb),
Total concentrations of P, K, Ca, Mg, S, Fe,
Mn, Zn, Cu, B, Na, Ni, Cd and Pb are
determined with an inductively coupled plasma
(ICP) spectrophotometer (Optima 3300 DV
ICP emission spectrophotometer; Perkin Elmer
Corporation; Shelton, CT) (Donohue and Aho
1992; adapted USEPA 2001), after open -vessel
IIN03 digestion in a microwave digestion
system (MARS & MD S21 00 microwaves;
CEM Corp.; Matthews, NC) (Campbell and
Plank 1992). A 0.5-g, dried/ground aliquot of
sample (1.0 g when nickel, cadmium or lead is
analyzed) is digested in 10 mL 15.6N FIN03 for
5-30 minutes In a microwave, and the prepared
sample volume is brought to 50 mL with
delonized water prior to measurement.
Elements are measured at wavelengths listed in
Table 4. Results are expressed in parts per
million (ppm) [equivalent to mg/kg] on a dry -
weight basis.
pH and electrical conductivity (E.C)
The pH measurement is taken with a hydrogen
electrode (Orion 920A; Thermo Fisher
Scientific; Beverly, MA) on a 1: 1 (v✓v) slurry
of sample to deionized water [10 cm3of sample
in 10 CM3 (mL) water] that has been allowed to
stand for 60 minutes (Eaton and others 2005;
NCDA&CS Waste and Compost Analt.sis Guide i 8 Mly 2013

Wolf 2003b). Following pH measurement, an
additional 1.0 Cm3 of deionized water is added
to the slurry, and the sample is filtered using a
Whatman #1 filter (Whatman, Inc., Florham
Park, NJ). Electrical conductivity (EC) (a
measure of soluble salts) is measured on this
1:2 (v/v) filtrate using a conductivity meter
(Orion 550A; Thermo Fisher Scientific;
Beverly, MA) (USEPA 1983; Wolf 2003a).
Results of EC are expressed in IV S/cm.
Calcium carbonate a uivalence(CCE%)
CCE% is a measure of the acid -neutralizing
capacity of a waste material. The process
involves dissolving a 1-g aliquot of dried
sample in 50 nil.., 0.5N HC1(with heat) and
back-titratiog to pH 7 with 0.25N NaOH,
according to the potentiometric titration method.
(AOAC, 1.990a). Results are expressed as
percentage of pure calcium carbonate.
A2ricuitural time equivalent (ALE)
ALE indicates the amount of waste that
provides a liming effect equivalent to one ton
of agricultural grade limestone (assuming 90%
calcium carbonate). This value is calculated as
follows: ALE = 1800 =- [(DM% _ 100) x
(CCE% 100) x 2000]. Results are expressed
in tans. The factor 1800 represents 90% of one
ton (in units of pounds).
Chloride (Cl D
Cl- concentration is determined by the
thiocyanate displacement method (tall et al.,
1956,.Skalar Analytical 1995b) with an auto -
flaw spectrophotometric analyzer (San'
Segmented Flow Auto -Analyzer, Skailar
Instruments; Breda, The Netherlands)
following a deionized water (1 g / 25 mL), 30-
minute extraction on a reciprocating shaker
(Wrist Action Model 75; Burrell Corp.
Pittsburgh; PA). Results are expressed in parts
per million (ppm) [equivalent to mg/kg] on a
dry -weight basis.
NC'I7A&C'S Waste and C°iai monk Analysis Guide 19
Table 4, 1CP wavelengths used to quantify
total elemental concentrations
Element Wavelength (um)
Boron (B) 249.772.
Cadmium (Cd)
Calcium (Ca)
Copper (Cu)
Iron (Fe)
Lead (Pb)
Magnesium (Mg)
Manganese (Mn)
Nickel (NO
Phosphorus (P)
Potassium (1)
Sodium (Na)
Sulfur (S)
Zinc (Zn)
214.440
317.933
3 24.752
259.939
220,353
285.213
257.610
231.604
178,221
766.490
589.592
181.975
213.857
July 2011

Liquid Waste Analysis Methodology
Sample handling
Prior to analysis, samples are homogenized by
shaking.
Nitrogen JN)
Total,Kjeldahl Nitrogen (TKN) is determined
by modified EPA Method 351.2 using an auto -
flow spectrophotometric analyzer (San++
Segmented Flow Auto -Analyzer; Skalar
Instruments; Breda, The Netherlands) (Skalar
Analytical 1995c; USEPA 1993). A 10-mL
aliquot of homogenized sample is digested in
10 mL concentrated H2,SO4 for 45-60 minutes
on a digestion block, and the volume is brought
to 100 mL with deionized water prior to
measurement. Results are expressed in parts per
million (ppm) [equivalent to mg/L].
Inorganic nitrogen (IN-N) fraction
concentrations include nitrate + nitrite nitrogen
(NO3-N + NO2-N) (reported as NO3-N on the
Waste Analysis Report) and ammonium
nitrogen (NH4-N). NO3-N is determined on a
homogenized sample (-20mL) by nitrate -
hydrazine reduction (Kempers 1988; Skalar
Analytical 1. 995b) and NH4-N is determined by
a modified Berthelot reaction (adapted from
Krom 1980; Skalar Analytical 1995a), with an
auto -flow spectrophotometric analyzer (San-+
Segmented Flow Auto -Analyzer, Skalar
Instruments; Breda, The Netherlands), Results
are expressed in parts per million (ppm)
[equivalent to mg/L].
Phosphorus (P), potassium (K), calcium
(Ca), sulfur (S), magnesium (Mj!), boron (13),
copper (Cu), iron (Fe), manganese (Mn),
zinc (Zn), sodium (Na), nickel (Ni), cadmium
(Cd), lead (Pb)
Total concentrations of P, K, Ca, Mg, S, Fe,
Mn, Zn, Cu, B, Na, Ni, Cd and Pb are
determined with an inductively coupled plasma
(ICP) spectrophotometer (Donohue and Aho
1992; adapted from USEPA 200 1) (Optima
3300 DV ICP emission spectrophotometer;
Perkin Elmer Corporation, Shelton, CT), after
OPM-VeSSel HNO3 digestion in a microwave
digestion system (MARS & MDS21 00
microwaves; CEM Corp.; Matthews, NC)
(Campbell and Plank 1992). A 5-mL aliquot of
homogenized sample is digested in 10 mL
15.6N HNO3 for 5-30 minutes in a microwave,
and the volume is brought to 50 mL with
delonized water prior to measurement.
Elements are measured at wavelengths listed in
Table 4. Results are expressed in parts per
million (ppm) [equivalent to mg/L].
pH and electrical conductivity (EC)
The p1l and electrical conductivity (EC) (a
measure of soluble salts) values are measured
directly on homogenized samples. The pH is
measured using a hydrogen electrode (Orion
920A; Thermo Fisher Scientific; Beverly, MA)
(Eaton and others 2005; Wolf 2003b).
Electrical conductivity is measured using a
conductivity meter (Orion 550A; Thermo
Fisher Scientific; Beverly, MA) (USEPA 1983;
(Wolf 2003a). Results of EC are expressed in
10-5 S/cm.
Calcium carbonate equivalence (CCE%)
CCE% is a measure of the acid -neutralizing
capacity of a waste material. The process
involves dissolving a 10-mL, homogenized
aliquot in 50 mL UN HCl (with heat) and
back-titrating to pH 7 with 0.25N NaOH,
according to the potentiometric titration method
(AOAC, 1990a). Results are expressed as
percentage of pure calcium carbonate.
Agricultural lime equivalent (ALE)
ALE indicates the amount of waste that
provides a liming effect equivalent to one ton
of agricultural grade limestone (assuming 90%
calcium carbonate). This value is calculated as
follows (assuming I gal. of liquid waste weighs
8,34 lb): ALE = 1800 ­. [(CCE% + 100) x
8340]. Results are expressed in 1000 gal.
NNCDA&CS Waste and Compost Analysis Guide 20 July 20133

Chloride (CF)
Cl- concentration is determined on a
homogenized sample (-20mL)by the
thlocyanate displacement method (tall et al.,
1956; Skalar Analytical 1995b) with an auto -
flow spectropbotometric analyzer (San-+
Segmented Flow Auto -Analyzer, Skalar
Instruments; Breda, The Netherlands). Results
are expressed in parts per million (ppm)
[equivalent to mg/L].
References for Waste Analysis Methodology
[AOAC] Association of Official Analytical Chemists. 1990a. AOAC official method 955-01:
neutralizing value for timing materials. In: Official methods of analysis. Volume I. 15th ed.
Arlington (VA): AOAC International. p 1-2.
[AOAC] Association of Official Analytical Chemists. 1990b. AOAC official method 972.43.
microchemical determination of carbon, hydrogen, and nitrogen. In: Official methods of analysis.
Volume 1. 15 1h ed. Arlington (VA): AOAC International. p 341.
Campbell CR, 1992. Determination of total nitrogen in plant tissue by combustion. In: Plank CO,
editor. Plant analysis reference procedures for the southern region of the United States, Athens
(GA): Georgia Cooperative Extension Service. Southern Cooperative Series Bulletin 368. p 20-
2, Available at www.ricagrj4ov/a ronomi/pdffiles/sera368.pdf (accessed 2011 Jan 3 1).
Campbell CR, Plank CO. 1992. Sample preparation. In:.Plank CO, editor. Plant analysis reference
procedures for the southern region of the United States. Athens (GA): Georgia Cooperative
Extension Service. Southern Cooperative Series Bulletin 368. p 1-12. Available at
www.neagr.gov/af,,rotioi-nil �dffilcs/".Qro368.pdf (accessed 2011 Jan 31).
Donohue SJ, Aho DW. 1992. Dctemiination of P, K, Ca, Mg, Mn, Fc, Al, B, Cu, and Zn, in plant tissue
by inductively coupled plasma (ICP) emission spectroscopy. In: Plank CO, editor. Plant analysis
reference procedures for the southern region of the United States, Athens (GA): Georgia
Cooperative Extension Service. Southern Cooperative Series Bulletin 368. p 34-7. Available at
www.iicag!,gov/agronomi/pdffiles/sera368.1)d (accessed 2011 Jan 3 1).
Eaton AD, Clesceri LS, Rice EW, Greenberg AE, editors. 2005. SM 4500 H+13: pH value in water by
potentiometry using a standard hydrogen electrode. In: Standard methods for the examination of
water and wastewater. 2 1 st ed. Washington (DC): Public Health Association, 'Water Environment
Federation, and American Water Works Association. 1368 p.
Wolf N. 2003a. Determination of manure electrical conductivity. In: Peters J, editor. Recommended
methods of manure analysis. Madison (WI). University of Wisconsin Cooperative Extension.
Publication A3769. p 50-1. Available at uwlab.soils.wisc.edu/_qbs/A3769,pdf (accessed 2011
Jan 3 1).
Wolf N. 2003b. Determination of manure PIT. In: Peters J, editor. Recommended methods of manure
analysis. Madison (WI): "University of Wisconsin Cooperative Extension, Publication A3769. p
48-9. Available at uwlab.soil.s.wisc.edu/pubs/A3769,pdf (accessed 2011 Jan 3 1).
NC DA&CS Was,(e and Compost Amflyiis Guide 21 July 2011

Hoskins B, Wolf A, Wolf N. 2003. Laboratory procedures, dry matter analysis. In: Peters J, editor.
Recommended methods of manure analysis. Madison (Wl): University of Wisconsin Cooperative
Extension. Publication A3769. p 14-7. Available at uwlab.soils,wisc,edu/pubs/A3769.pdf
(accessed 2011 Jan 3 1 ).
Kempers AJ, Luft AG. 1988. Re-examination of the determination of environmental nitrate by
reduction with bydrazine. Analyst I] 3:1117-20.
Krom M. 1980, Spectrophotometric determination of ammonia: a study of modified Berthelot reaction
using salicylate and dichloroisocyanurate. Analyst 105:305-16.
Skalar Analytical B,V. 1995a. Arrinionia. In: The SAN++ segmented flow analyzer — water analysis.
Breda (The Netherlands): Skalar Analytical B.V. p 73-5.
Skalar Analytical B.V. 1995b. Nitrate + Nitrite. Tn: The SAN++ segmented flow analyzer — water
analysis. Breda (The Netherlands): Skalar Analytical B.V, p 190-2,
Skalar Analytical B.V. 1995c. Nitrogen (total), In: The SAN++ segmented flow analyzer — water
analysis. Breda (The Netherlands): Skalar Analytical B.V. p 198-200.
[USEPA] United States Environmental Protection Agency. 1983. Method 120.1. Conductance (specific
conductance, pLmhos/cm at 25 'Q. In: Methods for chemical analysis of water and wastes.
Cincinnati (014): USEPA Office of Research and Development. EPA/600/4-79-020.
[USEPA] United States Environmental Protection Agency. 1993. Method 351.2. Determination of total
Kjeldahl nitrogen by semi -automated colorimetry, revision 2. In: Methods for chemical analysis
of water and wastes. Cincinnati (OH): USEPA Office of Research and Development. EPA-600/4-
79-020. Available at www.epa,Gov/waterscience/iiiethods/'method/`files/351 2.Vd (accessed 2011
Jan 3 1).
[USEPA] United States Environmental Protection Agency. 2001. Method 200.7. Trace elements in
water, solids, and biosolids by inductively coupled plasma —atomic spectrometry, revision 5.0.
Cincinnati (OH): USEPA Office of Research and Development. EPA-821 -R-01-010. Available at
IJ2 o. ennstate. ne. usj ab/_q_4/ Lgparnethods/200 7.pdf (accessed 2011 Jan 3 1).
NCDA&CS Wq,.,,tc and Compost Analysis Guide 22 July 20 11

Carolina Malt House
12969 Statesville Boulevard
Cleveland, North Carolina 27013
Prepared For:
Aaron Goss
12969 Statesville Boulevard
Cleveland, NC 27013
Prepared By:
Post Office Box 541
Midland, NC 28107
Tel [phone]
June 12, 2017 '0

Introduction
This update is submitted as an addendurn to the Soil Scientist Report, dated January 31, 2017,
for the Carolina Malt House, located at 12969 Statesville Boulevard, Cleveland, North
Carolina, 27013.
In a letter dated June 5, 2017, the North Carolina Division of Water Resources requested that
an explanation be provided as to how the annual loading rate for Application No.
WQ0039181 was calculated. Thompson Environmental. Consulting, Inc. would like to offer
the following explanation in response to this request.
Annual Loading Rate
C. Soil Evaluation
I - Explain how the recommended annual loading rate was calculated.
Hydraulic conductivity (KSAT) tests were measured using a, Compact Constant Head
C�
Pertnearrieter (Arnoozemeter) and values were generated -using the published calculations and
formulas found in the corresponding User's Manual.
For the Carolina Malt House site the Glover solution was chosen as the most appropriate
i-nethod for calculating KqAT based on in situ depth to impermeable layers. The Glover
solution is recommended when the distance between the bottom of the auger hole and any
inapenneable layer (s) is greater than 2 titnes the head (H), or constant water level in the hole.
The Glover solution is given by:
KsAT= AQ
Where: A= (sink-'(H/r)-[(r/H)2+l] 1f4rfflj / (27rFF)
And: Q is the stready-statc, rate of water flow from the Amoozerneter into
the auger hole.
To solve for A: H is the head in the hole (i.e. total water depth) and r is the radius of
the hole.
For Soil Unit I the measured Kskr rate in the BC horizon (0,109 in/hr) was determined the
most limiting. A drainage coefficient of 0.10 was proposed for this soil unit. Based on soil
and site characteristics and professional j udgment, a weekly loading rate of I . I inches was
recommended for Soil Unit I that results in 57.2 inches annually and corresponds to a
drainage coefficient of 0.06, lower than the proposed coefficient. The measured Ksxr rate in
the B/C horizon (0.0459 in/hr) proved to be the most limiting for Soil. Unit 2. A drainage
coefficient of 0.08 was recommended for this soil -unit. Based on soil and site characteristics
and professional judgment, a weekly loading rate of 0.4 inches was recommended for Soil
Unit 2 that results in 20.8 inches annually and corresponds to a drainage coefficient of
0.0735.
Carolina Malt House -Addendum 1 June 12, 2017

311/2021
Carolina Malt
Aaron Goss
12969 Statesville Blvd
Cleveland, NC 27013
704-412-9962
Type of Plan: Nutrient Management
Owner/Manager/Producer Agreement
This plan has been developed by:
NCDA&CS DSINC
Michael Shepherd
191 S, Main St
Mocksville, NC 27028
336-940-6901
Developer Signature
I (we) understand and agree to the specifications and operation and maintenance procedures
established in this nutrient management plan for the farm named above. I have read and
understand the Required Specifications that are included with this plan.
a4
avw-i,� —01 X(,d I ' Signature (owner)
Signature (manager or producer)
4/28/2021
Date
Date
This plan meets the minimum standards and specifications of the U.S.Department of Agriculture -
Natural Resources Conservation Service or the standard of practices adopted by the Soil and Water
Conservation Commission.
2332��
PZI WIN W-1 A
I MI, MM
Technical Specialist Signature
Date
31212021