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HomeMy WebLinkAboutWQ0004972_Monitoring - 06-2021_20210730Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0004972 Name of Facility:* Month:* June Report Information Forest Lakes Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter:* Signature: Date of submittal: Initial Review Year:* 2021 Upload Document* Forest Lakes_June.pdf 1.67MB FDF Cnly Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-t, NDAR-2, NDMLR, GW-59). Jessica. Mize@pacelabs.com Jessica Mize jus l oil Reviewer: Lloyd, Chloe D 7/30/2021 This will be filled in automatically Is the project number correct? * WQ0004972 Is the monitoring report r Yes r No accepted?* Regional Office * Winston-Salem Accepted Date: 8/2/2021 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W 0004972 MONTH: June YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: Influent: Ll Parameter Monitoring Point: Effluent: Influent: Surface Water SW : SW Codlam" ❑ Was There Effluent Flow for this Month Generated At This Facility: Yes: W No: ❑ Operator 50050 00400 50060 1 00310 1 00510 1 00530 31616 1 OC655 00625 1 00630 00600 1 OD520 70300 1 00940 D pmyal Dally Rate Fecal Total p Time Operator ORC (Flow) into Colifoan Total (0--tric Total Kjeldhal Nitrete Diasoived I T 2400 Time on on Treatment Rail BOO-5 6M-g� 20°C NH-3•N Tss Mean•) Phos Nill NO2-NOI NO3-N solids Chloride N. Clack Site Site? system pH Chlorine UNITS U[;rt. M(iIL MGrL M[i1L I:OOML MGIL MGlL Ml Ml MGlL Kill lirc 3iR5 Yfl,: GPp p ont. v oat y nnt. y , om t p one y I y l y Monthly y !year (year eek t 1518 0.25 B 6,961 6.10 <10 14116 0?5 B 51805 6.411 <10 3 1303 0.50 Y 6,117 6,30 <10 4 (11111) 0.50 1' 8,2114 6.111 <10 s 9,611 t, 9,611 7 1322 0.25 B 9,611 5.90 40 s t3oo 0.25 !' 8,257 5.90 <10 <2.0 67.7 5.7 2420 12.11 74.3 <O.040 74.3 <[I.IWII 1229 0,25 Y 7,739 6.00 <10 In 1504 [I.25 Y 1,9112 6,01) <j0 11 0843 1 0.50 Y 8,00H 6.10 <10 I I 10.249 13 10,249 u 1556 0.50 1' 10,249 1.111 <10 Is 0931 0.25 V 8,263 1 6.00 <10 16 1442 11-25 13 5,546 6.40 <10 17 1619 0.25 13 5,029 6.30 <10 tg (1855 11.25 13 6,498 6.30 <11) l4 9,007 9,01)7 21 0843 0.50 B 9,007 6.40 <10 0859 11,25 t3 8,231 6.30 <1(I 23 0907 0.25 B 1 8,009 6.40 1 <10 24 (1913 0.50 0 7,994 6.41) <111 2s 0834 0.25 A 8,138 6.40 <10 26 8,868 27 8,868 28 1049 11.25 Y 8,868 6.50 <11) 29 0922 0,50 1 Y 6,487 6.30 <10 ;u ]414 ILzS 13 6,4114 G.30 <10 31 Average 8,093 <10 < 67.7 5.7 0 1 <11.04f 14. <11.1 [1 Daily MA:imma 10 249 6.5[I <14 67.7 5.7 2420 12.0 <IL[14[I 7 < I. Dally6f)n)mam 5,029 5.9(1 <10 <2.0 67.7 5.7 2420 12.0 74.3 <0,040 74.3 <0.040 Monthly Limits (s) 24400 Composite C l Crab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: 11 Phone: 336-996 2 41 Check Box if ORC Has Changed: ORC Certification Number: 987931/20771 Certified Laboratories (1). Pace Analytical Serivices (2)- Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of water Quality By this signature, 1 certify that this report Is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant ,N} 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-comnlirrnt, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* ' t Date r Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 006110 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN(Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213,0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W 004972 MONTH: .Tune YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas: Daily Loading (inches) = [Vo€ume Applied (gallons) x 0.1336 (cubic feeVgallon) x 12 (incheslfool)] / [Area Sprayed (acres) x 43,56D (square featlacre) or = [Volume Applied (gallons)!(Area Sprayed (acres) x 27,162 (gallonslacre-inch). Maximum Hourly Loading (inches) = Daily Loading (inches)! [Time irrigated {minutes)! 60 (minuteslhour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floaling Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (incheslmonth) / Number of days in the month (daystmonth )] x 7 (daystweek) IrrigationDid , n Occur On This Field: Did Irrigaton Occur On This Field: i� � • •-- 1 MEN jmm®® omr•�aM®��ii•���M���111•�■11111•��■ m11111111I1•�■1111111.1_r.���w���■����■�� •1Wcaiher Codes: CKtem, PC-panly cloudy, Ctctoudy, R-rain, Sa-snow, SI-sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has_C_! nged: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division or Water Quality By this signature, 1 certify that this report is accurate and 1617 Mail Service Center complete to the best or my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. V I 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." `.l- Baron Neal McDuffie (Signature of Penmitee) Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) Field Services Director (Pace Analytical Services (Permittee-Please print or type) (Position or Title) 2N Riverside Plaza Suite 800 /�21 Chicago, Il 60606 (Permit Exp. Date) (Permittee Address) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). aceAnalj4 cal www.pacelabs.carn June 22, 2021 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lakes Pace Project No.: 92542903 Dear Tracy Overdurf: Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Enclosed are the analytical results for sample(s) received by the laboratory on June 08, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNUNELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures 2��e PCCRfp�r�0 ut a 8p�a�0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 16 (�Ia'cieAnalj&afo WmPacelabseom Project: Forest Lakes Pace Project No.: 92542903 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie, NC 27284 (704)977-0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Vtrginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.I.C. Page 2 of 16 aceAnalytical e { www.pacelab"Qui I SAMPLE ANALYTE COUNT Project: Forest Lakes Pace Project No.: 92542903 Pace Analytical Services, LLC 1377 South Park Drive Kemersviile. NC 27284 (704)977-0981 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92542903001 Effluent SM 2540D-2011 AM[ 1 PASI-E EPA 353.2 Rev 2.0 1993 AMI 1 PASI-E SM 521OB-2011 MWF 1 PASI-E Colilert-18 MWF 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 MFO 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 aceAnalj&al e f www.pecelata.com ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Forest Lakes Pace Project No.: 92542903 Sample: Effluent Lab ID: 92542903001 Collected: 06/08/21 13:13 Received: 06/08/21 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Eden Total Suspended Solids 5.7 mg/L 2.8 1 06/09/21 15:40 353.2 NO2IN03 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.040 1 06/08/21 18:03 14797-55-8 5210E BOD, 5 day EDN Analytical Method: SM 521 OB-2011 Preparation Method: SM 521OB-2011 Pace Analytical Services - Eden BOD, 5 day ND mg/L 2.0 1 06/10/21 09:14 06115121 10:07 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100ml- 1.0 1 06108/21 16:06 06/09/21 10:39 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 74.3 mg/L 0.52 1 06/22/21 11:53 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 67.7 mg/L 1.0 10 06/17/2112:40 766441-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 74.3 mg/L 2.5 5 06/15/21 21:14 06/16/21 05:24 7727-37-9 353.2 Nitrogen, N021NO3 Ares. Analytical Method: EPA 353,2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg1L 0.040 1 06/14/21 13:23 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 12.0 mg/L 0.25 5 06/16/21 18:07 06/16/2123:25 7723-14-0 Date: 06/22/2021 11:56 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 132 1 g,E1 Page 4 of 16 5ac1� eAnalj&al w wa.pacelabs.com ! QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92542903 QC Batch: 625835 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92542903001 METHOD BLANK: 3290673 Matrix: Water Associated Lab Samples: 92542903001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 06/09/21 15:33 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 t704j977-0981 LABORATORY CONTROL SAMPLE: 3290674 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 228 91 90-110 SAMPLE DUPLICATE: 3290675 92542667001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 109 104 4 SAMPLE DUPLICATE: 3290676 92542883001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 19.3 16.2 17 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/22/2021 11:56 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 aceAnalytical www.pacelsbs.ccm QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92542903 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 625541 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92542903001 METHOD BLANK: 3289370 Matrix: Water Associated Lab Samples: 92542903001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L NO 0,040 06/08/21 10:59 LABORATORY CONTROL SAMPLE: 3289371 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3289372 3289373 MS MSD 92542706001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 8.5 1.5 1.5 10.2 10.0 113 102 90-110 2 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06122/2021 11:56 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 aceAnalytical www.pacelsbs.eam QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92542903 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 626126 Analysis Method: SM 521OB-2011 QC Batch Method: SM 52108-2011 Analysis Description: 5210E SOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92542903001 METHOD BLANK: 3292298 Matrix: Water Associated Lab Samples: 92542903001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 06/15/21 09:56 LABORATORY CONTROL SAMPLE: 3292299 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg1L 198 198 100 84.6-115A SAMPLE DUPLICATE: 3292301 92543294002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 127 124 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06122/2021 11:56 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 accAnalytical i www.paeelaDs.tam I QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92542903 QC Batch: 625804 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Conform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92542903001 SAMPLE DUPLICATE: 3290589 Parameter Units Fecal Coliforms MPN/100mL 92542883001 Dup Result Result RPD Qualifiers 3.1 ND Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/22/2021 11:56 AM without the written consent of Pace Analytical Services, L-C. Page 8 of 16 aceAnalytical www.pacelablixam Project: Forest Lakes Pace Project No.: 92542903 QC Batch: 627726 QC Batch Method: EPA 350.1 Rev 2.0 1993 Associated Lab Samples: 92542903001 QUALITY CONTROL DATA Analysis Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services - Asheville METHOD BLANK: 3299997 Matrix: Water Associated Lab Samples: 92542903001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 06117121 12:03 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3299998 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.2 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3299999 3300000 MS MSD 92543697002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec ere Rec Limits RPD Qual Nitrogen, Ammonia mg/L 2.9 5 5 8.1 8.1 103 103 M110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3300001 3300002 MS MSD 92543963001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg1L NO 5 5 5.1 5.1 101 101 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06122/2021 11:56 AM without the written consent of Pace Analytical Services, I.LG. Page 9 of 16 1�l5aceAnaljftala rnrw.pacelabs.com I QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92542903 OC Batch: 627279 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92542903001 METHOD BLANK: 3297700 Associated Lab Samples: 92542903001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 3297701 Parameter Units Nitrogen, Kjeldahl, Total mglL Pace Analytical Services, LLC 1377 South Park Drive Kemersviile. NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 06/1612104:40 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 9.6 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3297702 3297703 MS MSD 92542858001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 10.1 10 10 21.4 20.0 113 99 90-110 7 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/22/2021 11:56 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 1�l5aceAnalj&cal" www.pacelabs.com I Project: Forest Lakes Pace Project No.: 92542903 QC Batch: 626780 QC Batch Method: EPA 353.2 Rev 2.0 1993 Associated Lab Samples: 92542903001 METHOD BLANK: 3295450 Associated Lab Samples: 92542903001 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method: Analysis Description Laboratory: Matrix: Water EPA 353.2 Rev 2.01993 353.2 Nitrate + Nitrite, preserved Pace Analytical Services -Asheville Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 06114/2112:58 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3295451 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3295452 3295453 MS MSD 92542759001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.31 2.5 2.5 2.4 2.5 85 86 90-110 1 Mi MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3295454 3295455 MS MSD 92542759002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.55 2.5 2.5 2.7 2.7 88 87 90-110 1 Mi Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/22/2021 11:56 AM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 16 lacmnaljdical" www.patelabs.com QUALITY CONTROL DATA Project: Forest Lakes Pace Project No.: 92542903 QC Batch: 627455 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92542903001 METHOD BLANK: 3298505 Associated Lab Samples: 92542903001 Parameter Units Phosphorus mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 06/16/2123:06 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3298506 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3298507 3298508 MS MSD 92542755005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 90.9 2.5 2.5 93.4 98.5 101 305 90-110 5 Mi MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3298509 3298510 MS MSD 92543047001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.3 2.5 2.5 3.8 3.8 100 101 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/22/2021 11:56 AM without the written consent of Pace Analytical Services, L.L.C. Page 12 of 16 1�5aceAnaljftalm lwrw.pacelaba.com I QUALIFIERS Project: Forest Lakes Pace Project No.: 92542903 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit -The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS 1g >2419.6 B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated for the dilution using the most amount of sample. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery. This report shall not be reproduced, except in full, Date: 06/22/2021 11:56 AM without the written consent of Pace Analytical Services, I.I.C. Page 13 of 16 aceAnalytical www.patelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lakes Pace Project No.: 92542903 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92542903001 Effluent SM 254OD-2011 625835 92542903001 Effluent EPA 353.2 Rev 2.0 1993 625541 92542903001 Effluent SM 521OB-2011 626126 SM 521OB-2011 626237 92542903001 Effluent Colilert-18 625804 Colilert-18 625806 92542903001 Effluent TKN+NO3+NO2 628621 Calculation 92542903001 Effluent EPA 350.1 Rev 2.0 1993 627726 92542903001 Effluent EPA 351.2 Rev 2.0 1993 627279 EPA 351.2 Rev 2.0 1993 627385 92642903001 Effluent EPA 353.2 Rev 2.0 1993 626780 92542903001 Effluent EPA 365.1 Rev 2.0 1993 627455 EPA 365.1 Rev 2.0 1993 627670 Date: 06/22/2021 11.56 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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