NCG060220_Monitoring (Report)_20210712

Environmental NC DEPARTMENT OF
Quality ENVIRONMENTAL QUALITY
Stormwater Discharge Outfall (SDO) RECEIVED
Qualitative Monitoring Report JUL 12
2021
For guidance on filling out1this form, please visit htt s://de .nc. ov/about/divisions/ener m it gg�IONAL OFFICE
resources/ener -mineral-land- mineral -land -permits/ ermits/n des-industrial-sw#t�Yd¢ION OF AIR QUALITY
Permit No.: N/C/ / / / or Certificate of Coverage No.: N/C/G/ O / 6 /O /2 /2 /O / Facility Name: Darling Ingredients Inc DBA Bakery Feeds
County: Union
Inspector: Chuck Kirkley/Doug Jones
Date of Inspection: 06/03/2021
Time of Inspection: 4:00 pm
Total Event Precipitation (inches): 1.41
Phone No. k [phone]
3
All permits require qualitative monitoring toGbe performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1• Outfall Description:
Outfall No. 00_ 1__
Structure (pipe, ditch, etc.): Ditch
Receiving Stream:
Salem Creek
Describe the industrial activities that occur within the outfall drainage area:
Bakery Production
Page 1 of 2
SWU-242, Last modified 07/28/2017
0
z
a

vcscnoC trte color of the aischarge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Gear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
I & 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
E 2 3 4 5
7. Is there any foam in the stormwater discharge? 0 Yes E) No.
8. Is there an oil sheen in the stormwater discharge? oYes No.
9. Is there evidence of erosion or deposition at the outfall? O Yes 9 No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

r`
NC
ENVIRONMENTAL 0tIAOLITY
Environmental RECEIVED
Quality
Stormwater Discharge Outfall (SDO) JUL 1,2 2021
Qualitative Monitoring Report MOORESVILLE REGI
ONAL OFFICE
For guidance on filling DIVISION
out this form, please visit https://deq.nc.gov/about/divisions/ener R DUALITY
resources/ener -mineral-land- ermits/stormwater- ennits/n des-industrial-sw#tab-4
No.: N or Certificate of Coverage No.: N/C/G/ 0 / 6 /0 /2 /2 / Q /
Facility Name: Darling Ingredients Inc DBA Bakery Feeds
County: Union
Phone No. [phone]
Inspector: Chuck Kirkley/Doug Jones
Date of Inspection: 06/03/2021
Time of Inspection: pm
_
4:00
Total Event Precipitation (inches): 1.41
5.
All permits require qualitative monitoring to be performed during a "measurable storm -
event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1• Outfall Description:
Outfall No. 002
Receiving Stream:
Salem Creek
Structure (pipe, ditch, etc.): Ditch
Describe the industrial activities that occur within the outfall drainage area:
U—CO Processing, Bakery Production, Vehicle Maintenance.
Pagel of 2
SwU-242, Last modified 07/28/2017

—• --jivis Licsc;rioe me color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Gear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
C 2 3 4 5
7. Is there any foam in the stormwater discharge? 0 Yes •
No.
S. Is there an oil sheen in the stormwater discharge? OYes •
No.
9. Is there evidence of erosion or deposition at the outfall? o Yes O No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242, Last modified 07/28/2017

ty
Stormwater Dischatrge Outfall (SDO)
Qualitative Monp
Monitoring Report
For guidance on filling out this form, please visit htt s://de .nc. ov/about/divisions/ener -mineral-land-
resources/ener -mineral-land- ermits/stormwater- ermits/n des-industria1-sw#tab-4
Permit No.: N/C/ / / / or Certificate of Coverage No.:
Facility Name: Darling Ingredients Inc DBA Bakery Feeds g N/C/G/ 0 / 6 /0 /2 /2 /� /
County: Union
Phone No. [phone]
Inspector: Chuck Kirkiey/Doug Jones - �
<r
Date of Inspection: 06/03/2021%:
Time of Inspection: 4:00 pm
Total Event Precipitation (inches): 1.41
All permits require qualitative monitoring to be performed during a "measurable storm event "
A "measurable storm event" is a storm event that results in an actual discharge from the Permitted
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72_ho rstorm
site
ust
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the to
Regional Office. cal DEMLR
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1• Outfall Description:
Outfall No. 003 Structure ditch, etc):
Receiving Stream: (pipe,.Ditch
Salem Creek
Describe the industrial activities that occur within the outfall drainage area:
UCO Processing
Page 1 of 2
S WU-242, Last modified 07/28/2017

k-.oior: Describe the color of the discharge using basic colors (red, brown, blue etc.
(light, medium, dark) as descriptors: dear
)and tint
3. Odor: Describe any distinct odors that the discharge may have i.
chlorine odor, etc.): None (e., smells strongly of oil, weak
4. Clarity: Choose the number which best describes the
and 5 is very cloudy: clarity of the discharge, where I is clear
1 97 3 4 5
5• Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with flo
ating solids:
2 3 4 5
6• Suspended Solids: Choose the number which best describes the a
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
mount of suspended solids in
2 3 4 5
7• Is there any foam in S. Is there an oil the stormwater discharge? yes
No. _
9• Is there evidesheen in the stormwater discharge? dyes
No. _
nce of erosion or deposition at the outfall? O yes O
No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen
or erosion deposition may be
indicative of pollutant exposure. These conditions warrant further inv
estigation.
Page 2 of 2
SwU'242, Last modified 07/28/2017

For guidance on filling out this form, please visit htt s://de .nc. ov/about/divisions/ener
resources/ener-mineral-land- ermits/stormwatcr- ermits/n des-industrial-sw#tab-4
-mineral-land-
Permit No.: N/C/ / /
/ or Certificate of Coverage No.: N/GG/ 0/6 /0 /2 /2 /0 /
Facility Name: Darling Ingredients Inc DBA Bakery Feeds
County: Union
Inspector: Chuck Kirkley/Doug Jones Phone No. [phone]
---------------
Date of Inspection: 06/03/2021
Time of Inspection: 4:00 pm
Total Event Precipitation (inches): 1.41
_...................._......_.__..__.._................. ............ _....... ........ _........... _._.._._.._.... _.... ..-................... .._......... _......... ................. _.....__........ .._... ...... _..._.._..._..._....... ................ __._................ _...... ._..._..._.___.............. __............. _....... I ........ _...
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from
outfall. The previous measurable storm event must have been at least 72 hours prior. The
interval does not apply if the permittee is able to document that a shorterg the permitted site
local storm events duringthe sampling 72 hour storm
interval is representative for
Regional Office. p g period, and the permittee obtains approval from the local DEMLR
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1• Outfall Description:
Outfall No. 004
Receiving Stream:
Salem Creek
Structure (pipe, ditch, etc.): Ditch
Describe the industrial activities that occur within the outfall drainage area:
None
Page 1 of 2
SWU-242, Last modified 07/28/2017

—• q-oior: Describe the color of the discharge
(light, medium, dark g using as descriptors: N/A g basic colors (red, brown
blue, etc.) and tint
3• Odor: Describe an
chlorine odor, etc.): N/A y dlstmct odors that the discharge g may have (i.e., smells strongly of oil, Weak
4• Clarity: Choose the number which best describes bes the clarity of the discharge, where
and 5 is very cloudy: ri1 1 2 3 is clear
5. 4 5
Floating Solids: Choose the numberdischarge, which best describes the amount of floating g , where 1 is no solids and 5 is the surface covered with fl
g solids in the
oating solids:
6• Suspended Solids: Choose 1 2 3 4 5
the nu
the stortuwater discharge, where 1 is mber which best describes the amount of suspended solids in
no solids and 5 is extremely muddy:
1 2 3 7• Is there any foam 4 5in the stormwater discharge?
S. Is there an oil sheen in the storm ®yes ®No N/A
water discharge? yeS � No. N/A
9• Is there evidence of erosion or
deposition at the outfall? 10• Other Obvious Indicators oyes (2) No. N/A
of Stormwater p
List and describe No� Flow From putfall °llution:
Note: Low clarity, high solids
indicative of pollutant ex , and/or the presence of foam
posure. These conditions , O1l Sheen, or erosion/de warrant further investigation, erosion/deposition may be
S WU-242, Last modified 07128/2017 Page 2 of 2

For guidance on filling out this form
resources/ener Please visit htt s://de .nc. ov/about/divisions/ener
eral-land- ermits/stormwater-
ermits/n des-industrial-sw#tab-4 eral-land-
Permit No.:
or Certificate of Coverage
Facility Name: Darling Ingredients Inc DBA Bakery Feeds No':N/C/G/ 0 / 6 /0 /2 /2
County: Union
Inspector: Chuck Kirkley/Doug Jones Phone No. [phone]
Date of Inspection: 06/03/2021
Time of Inspection: 4.00 pm s ;
Total Event Precipitation (inches): 1.41
�ro
S±, C r
�n
V v cf
_._................
...._.__.._..__..__.._,_........__......__.........._.......,.._..__........_.._._......._................_................_.............__ ....._,......_....__..._.._....._.__.._..__...._...._......,_..._ _........_........._.
f
All permits require qualitative monitorin
g to be performed Burin a «
g measurable storm
A "measurable storm event" is a sto
event." I
outfall. The previous measurable storm event must have been at
rm event that results in an actual discharge from the Permitted site
interval does not apply if the e
local storm events during p rnuttee is able to document that a shorter interval is representative least 72 hours Prior. The 72-hour storm
Re to g the sampling period, and the permittee obtains a p sentative for
,._.. g.�..._nal Office;.......__.
........_.�...__..._......__.._.._.._..._............_�._._ _ _ ........................ approval from the local DEMLR
By this signature, I certify that this report is accurate and complete to the best of my know led ge;
(Signature of permittee or Designee
1• Outfall Description:
Outfall No. 005
Receiving Stream: Stnleture (pipe, ditch, etc.): Ditch
Salem Creek
Describe the industrial activities that Occur
within the outfall drainage area:
S WU-242, Page 1 of 2
Last modified 07/28/2017

color: Describe the color of the discharge using basic colors (red, brown, (light, medium, dark) as descriptors: N/A
blue, etc.) and tint
3• Odor: Describe an
chlorine odor, etc.): N/A y distinct odors that the discharge g may have (i.e., smells strongly of oil, weak
4• Clarity:
Choose the number which and 5 is very cloudy: best describes the clarity of the discharge, where 1 is clear
1 2 3 4 5
5• Floating Solids: Choose the number which best describes
stormwater discharge, where 1 is no solids and 5 is the surface covered amount of floating solids in the
with floating solids:
1 2 3 4 5
6• Suspended Solids:
Choose the number which best describes the amount of sus
the stormwater discharge, where 1 is no solids and 5 is extremely ende muddy: p d solids in
1 2 3 4 5
7• Is there any foam in the stormwater discharge? yes
g• Is there an oil sheen in the stormwater®No. N/A
discharge? dyes � No N/A
9• Is there evidence of erosion or deposition at the outfall? q yes p No N/A
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No Flow From Outfall
Note: --------
Low clarity, high solids, and/or the presence of foam, oil she
indicative of pollutant exposure. These conditions warrant furth
en, or erosion deposition may be
er investigation.
Page 2 of 2
S WU-242, Last modified 07/28/2017

Environmental
Stormwater Discharge Outfall (SDO)
p
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deg nc.gov/about/divisions/ener y mineral land
resources/ener -mineral-land- ermits/stormwater ermits/n des-industrial-sw#tab-4
Permit No.: N or Certificate of Coverage No.: N/C/G/ 0 / 6 /0 /2 /2 /0 / Facility Name: Darling Ingredients Inc DBA Bakery Feeds
County: Union
Inspector: Chuck Kirkley/Doug Jones
Date of Inspection: 06/03/2021
Time of Inspection: 4:00 pm
Total Event Precipitation (inches): 1.41
Phone No. [phone]
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1• Outfall Description:
Outfall No. 006
Receiving Stream:
Salem Creek
Structure (pipe, ditch, etc.): Ditch
Describe the industrial activities that occur within the outfall drainage area:
None
Page 1 of 2
SWU-242, Last modified 07/28/2017

OJor: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: N/A
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells
chlorine odor, etc.): N/A stro
ngly of oil, weak
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floatin solids:
g
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? 0 yes
No. NIA
8. Is there an oil sheen in the stormwater discharge? 0yeS (D No N/A
9. Is there evidence of erosion or deposition at the outfall? 0 yes O No, N/A
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No Flow From outfall
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investi ation.
g
Page 2 of 2
S WU-242, Last modified 07/28/2017

'��Ba
kFeedl
e
Stormwater Field pH Test Form
.Bakery Feeds, Marshville, NC
Date Sample Collected; Ce 3 I
Time Sample Collected 4-00-1-1
Location of Sample (# of outfall)
Date of pH Analysis
Time of pH Analysis
PH Meter Calibration Information
pH meter reading with 4.0 buffer
pH meter reading with 7.0 buffer
pH meter reading with 10.0 buffer
Ambient Rainfall pH =
PH result
O CA�1(
1'O
Olt J
Name of person conducting test and calibration
Print
Signature and date
k.-

I�alakery Feedl
Stormwater Field pH Test Form
Bakery Feeds, Marshville, NC
Date Sample Collected:
Time Sample Collected
Location of Sample (# of outfall)
Date ofpl-I Analysis
Time of pH Analysis
PH Meter Calibration Information
pH meter reading with 4.0 buffer
pH meter reading with 7.0 buffer
pH meter reading with 10.0 buffer
Ambient Rainfall pH
PH result
.Name of person conducting test and calibration
Print
Signature and date �`

j.
��akeri
Stormwater Field PH Test Form
Bakery Feeds, Marshville,lVC
Date Sample Collected;
Time Sample Collected
.Location of Sample (# of outfall)
Date of PH ,analysis
Time Of PH Analysis
PSI Meter Calibration information
PH meter reading with 4.0 buffer
PH meter reading with 7.0 buffer
PH meter reading with 10.0 buffer
Am bient Rainfall pj TM
PH result =
/-g f o
Name of person conducting test and calibration
Print
Signature and date

ace Analytical
AnalysisReport of
Bakery Feeds
5805 Hwy 74 East
Marshville, NC 28103
Attention: Matthew Hart
Project Name: Stormwater
Lot Number:WF04109
Date Completed:06/11/2021
t�?�p (!na- -'-
06/11/2021 4:18 PM
Approved and released by:
Project Manager If: Lucas Odom
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page I of 8

SG DHEC No: 32010001 PAC NEA�NALYTIC L SERVICES , LLC
7653 NC DENf7 No: 329 NC Ffeld Parameters No: 5639
mum -
Case Narrative
Bakery Feeds
Lot Number: WF04109
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page,
Pace Analytical Services, LLC (formerly Shealy Environmetal services, Inc,)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacefabs,com
Page 2 of 8

t AUt ANALYTICAL SERVICES, LLC
Sample Summary
Bakery Feeds
Lot Number: WF04109
Sample Number Sample IA
t1I1T61
Outfall #003 -� �•� YGU
0 sample) Aqueous 06/03/2021 1600 06/04/2021
Matrix nnfa Q.— I A
Pace Analytical Services, LLC (for(nerly Shealy Envlronmental Services, tnc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs,com
Page 3 of 8

r At;t ANALYTICAL SERVICES,
LLC
Detection Summary
If
Bakery Feeds
Lot Number: WF04109
Sample Sample ID
Matrix Parameter
001 Outfall #003
Method
Aqueous COD
Result Q
Units
Page
001 Outfall #003
SM 5220D-
Aqueous TSS
62
mg/L
5
001 Outfaii #003
SM 2540D-
Aqueous TVSS
140
mg/L
5
001 Outfall #003
SM
Aqueous HEM (oil and grease) 1664E
22
mg/L
5
(4 detections)
4.9 J
mg/L
5
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 8

Date Sampled:06/03/2021 1600
Date Received:06104/2021
Matrix: Aqueous
Inorganic non-metals
Run Prep Method
1
Analytical Method
Dilution Analysis Date Analyst Prep Date
(COD) SM 5220D-2011
1 06/10/2021 0837 KFE
Batch
1
(TSS) SM 254OD-2011
1 06/10/2021 1722 MOM
2
951
1
(TVSS) SM 2540D/160.4
1 06/08/2021 1946 MOM
9445
1
(HEM (oil and) 1664B
1 06/09/2021 0940 GLT
98 11
9489494
Parameter
CAS Analytical
COD
Number Method Result Q
LOQ DL Units Run
TSS
SM 5 220D-2011 62
20 20 mg/L 1
TVSS
SM 254OD-2011 140
14 1.0 mg/L 1
HEM (oil and grease)
S
LOQ = Limit of Quantitation B = Detected in the method blank E = Quenlitatlon of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental ServIces, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.Pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Page 5 of 8

Chain Of
Custody
• •
Miscellaneous Documents
Pace Analytical Services, LLC j%rrrterly Shealy Environmental Servlces, Inc,)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs,com
Page 6 of 8

AIMALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia,
SC 29172
[phone]
Fax [phone]
www.pacelabs,com
Page 7 of 8
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Pace Analytical Services, LLC (formerly Shealy Environmental Services
106 Vantage Point Drive , Inq
West Columbia, SC 29172 [phone] FaX [phone] www.pacelabs.com
Page 8 of 8

aceAnalytical�
Report of Analysis
Bakery Feeds
5805 Hwy 74 East
Marshville, NC 28103
Attention: Matthew Hart
Project Name: Stormwater
Lot Number:WF04112
Date Completed:06/11/2021
06/11/2021 4:19 PM
Approved and released by:
Project Manager il: Lucas Odom
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Pagel of 8

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329
NC Field Parameters No: 5639
Case Narrative
Bakery Feeds
Lot Number: WF04112
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 8

�.� P%IMIAL T 1'VAL 5LKVIGES, LLC
Sample Summary
Bakery Feeds
Lot Number: WF04112
Sample Number Sample ID
001
Outfall #002 - sample} --
Aqueous 06/03/20211600 06/04/2021M
(1
Matrix Date gmmnIa q ns
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 8

rx4 IANALY e K AL SERVICES, LLC
mm
Detection Summary
Bakery Feeds
Lot Number: WF04112
Sample Sample ID Matrix Parameter
001 O tf I Method Result Q t!
001
001
001
001
u al#002
Outfali #002
Outfail #002
Outfall #002
Outfali #002
(5 detections)
Aqueous
COD
SM 5220D-
150
nits
Page
Aqueous
TSS
SM 2540D-
130
mg/L
5
Aqueous
TVSS
SM
mg/L
5
Aqueous
HEM (oil and grease)
16648
32
mg/L
5
Aqueous
SGT - HEM (non -polar
1664B
3.2 J
mg/L
5
2.4 J
m /L
g
5
nq
1Analytical L
06 VantagePo Point Drive West (Co Columbia, SC'29172on(803) 7 1-9700s /Fax [phone] www,pacelabs, com
Page 4 of 8

Date Sampled:06/03/2021 1600
Date Received:06104/2021
Matrix: Aqueous
Run Prep Mefhod
1 Analytical Method
1 (COD) SM 5220D-2011
1 (TSS) SM 254OD-2011
1 (TVSS) SM 2540D/160.4
1 (HEM (oil and)16648
(SGT - HEM (n) 1664B
Inorganic non-metals
Dilution Analysts Date Analyst Prep Date
1 06/10/20210838 KFE
1 06/10/20211722 MOM
1 06/08/2021 1946 MOM
1 06/09/20210940 GLT
1 06/09/20210940 GLT
Parameter
CAS Analytical
COD
Number Mefhod
Result Q
TSS
SM 5220D-2011
150
TVSS
SM 254OD-2011
130
HEM (oil and grease)
SM 2540D/160.4
32
SGT - HEM (non -polar material)
1664E
3.2 J
1664E
2.4 J
Batch
94972
95145
94811
94894
94892
LOCI
DL
Units
Run
20
20
mg/L
1
50
1.0
mg/L
1
10
10
mg/L
1
5.4
1.9
mg/L
1
5.4
1.9
mg/L
1
LOCI = Limit of quantitatlon B =Detected In the method blank E NO = Not detected at or above the DL quantitatlon of compound exceeded the calibration range DL
N Recovery Is out of criteria P = The RPD between two GC columns exceeds 40% g Detection Limit
H = Out of holding time W Rep
orted on wet weight basisq =S�MSIMSD
failure
= Esflmata�rjtOqand > DL L = failure
�eAlytical Services, LLC (formernvlronmenta!Services, Inc.) ^ge Point Drive West Colum9172 (803} 791-9700 Fax [phone] s =allure
www.pacelabs.com
Page 5 of 8

Chain OfCustody
MM
MOM
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,pacelabs,com
Page 6 of 8

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West Columbia,
SC 29172 [phone] Fax [phone] Www.pacelabs.com
Page 7 of 8

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Pace Analytical Services, LLC (formerly Shealy EnvIronmental Services, inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 8

aceAnalytical
Report of Analysis
Bakery Feeds
5805 Hwy 74 East
Marshville, NC 28103
Attention: Matthew Hart
Project Name: Storm Water
Lot Number:WF04113
Date Completed:06/14/2021
06/14/2021 3:55 PM
Approved and released by:
Project Manager If: Lucas Odom
4W
ANSf Nallonal------ Ac��Bdjlapoa gaaad
9 ACCREDITED
TESTINOlA60gATOgY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Pagel of 8

SC DHEC No: 32010001 PAC NEANALYTICAL LAC No: SERVICES, LLC
3 NC DENR No: 329 NC Field Parameters No; 5639
Case Narrative
Bakery Feeds
Lot Number: WF44113
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed In this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (Sops), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, Sops or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmefal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs,com
Page 2 of 8

NEUMMEMMM
Sample Summary No
Bakery Feeds
Lot Number; WFO4113
Sample Number Sample ID
001
(1 sample) Aqueous 06/03/2021 1600 06/04/2021
Outfall #001
Matrix nnfa -Q.— [.A
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,pacelabs.com
v.. vcu
Page 3 of 8

e
revue �91MHR� I 1 1�/$►1� Or-MVR t5y
LLC
Detection Summary
Bakery Feeds
Lot Number: WF04113
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
page
001 Outfall #001
Aqueous
COD SM 5220D-
670
m9/�
5
001 Outfall #001
Aqueous
TSS SM 2540D-
120
mg/L
5
001 Outfall #001
Aqueous
TVSS SM
110
001 Outfall #001
Aqueous
HEM (oil and grease) 1664B
24
mg/L
5
(4 detections)
mg/L
5
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 8

Date Sampled:06/03/2021 1600
Date Received:06/04/2021
----------------
Matrix: Aqueous
1
1
1
1
Parameter
COD
TSS
TVSS
HEM (oil and grease)
Inorganic non-metals
Analytical Method
(COD) SM 5220D-2011
Dilution Analysis Date Analyst
Prep Date
(TSS) SM 254OD-2011
1 06/08/2021 1021 KFE
1
(TVSS) SM 2540D/160.4
06/10/2021 1722 MOM
1
(HEM (oil and)1664B
06/08/2021 1946 MOM
1
06/12/2021 0835 DDD2
CAS Analytical
Number Method Result Q
SM 5220D-2011
670
SM 254OD-2011
120
SM 2540D/160.4
110
1664B
24
Batch
94710
95145
94811
95317
LOQ
DL
Units
Run
20
20
mg/L
1
25
1.0
mg/L
1
10
10
mg/L
1
7.7
2.7
mg/L
1
LOQ =Limit of Quantifatlon ti =Detected In the method blank E
ND = Not detected at or above the DL = Quantifatlon of compound exceeded the calibration range DL = Detectlon Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis =Estimated result < LOQ and > DL Q - Surrogate failure
L = LCSlLCSb failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) s = MS/IVISD failure
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] WWW.pacelabs.com
Page 5 of 8

Me
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 8

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 8