NCG030099_MONITORING REPORT_20200528

I % n a
State of North Carolina
DWQ Regional Office
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Certified Mail: 7018 2290 0000 4700 6112
To Whom It May Concern:
RECEIVED
JENR-DEMLR
Land Quality Section
Mooresville Regional Office
Enclosed is a signed copy of the Storm Water Discharge Monitoring Report. Should
this agency require any additional information, please contact Harshad Londhe at 704-
455-5102 ext. 142.
Regards,
Darhma Robinson
Human Resources Manager
P.O. BOX 369 • HARRISBURG, N.C. 28075 • TEL [phone] / FAX [phone] • www.galvanelectrical.com • www.galvan•ize.com

hdrinc.com
May 15, 2020
Mr. Harshad Londhe
Galvan Industries, Inc.
7320 Millbrook Road
Harrisburg, NC 28075
Subject: April 2020 NPDES Monitoring Report
Galvan Industries, Inc.
Dear Mr. Londhe,
The purpose of this report is to provide the results of qualitative and quantitative stormwater
monitoring conducted on April 20, 2020 at the above -referenced site (Site). The monitoring was
performed in general accordance with NPDES General Permit (GP) # NCG030000 (effective
November 1, 2018 through May 31, 2021).
Qualitative Monitoring
On April 20, 2020, HDR Engineering, Inc. of the Carolinas (HDR) mobilized to the Site to conduct
monthly qualitative monitoring of Outfalls (OF #1, #3 through #5) and Top of Hill (TOH-1) leading
down to the rail right of way (ROW).
OF #1 is located on the northeast comer of the Site and Galvan Way. Flowing water in this outfall
was light tan in color and odorless. There were trace amounts of suspended solids and trace
floating solids. No oil sheen was visible. No evidence of erosion or deposition was present. No foam
was present during the sampling event. A filter sock was present upgrade of OF #1 and care was
taken to ensure that the sample was taken downstream of the filter sock.
OF #3 is located on the southwest corner of the Site. Flowing water in this outfall was light tan and
odorless. There were trace amount of suspended solids. No floating solids or oil sheen were visible.
Slight erosion was present with no evidence of deposition observed. No foam was present during
the sampling event.
OF #4 is located on the northwest comer of the Site. Flowing water in this outfall was clear and
odorless. There were no visible suspended solids or floating solids. No oil sheen was visible at this
outfall. No evidence of erosion or deposition was present. No foam was present during the
sampling event.
OF #5 is located in the middle of the Site. Waterflows from the Blast Building eastward to the
outfall. It should be noted that water also flows into this outfall from the adjacent Highway 49. Water
in the outfall was light tan in color and odorless. Minor suspended solids were observed in the
flowing water at this outfall. It was without noticeable floating solids and foam. No evidence of
erosion or deposition was present. A filter sock was present upgrade of OF #5 and care was taken
to ensure that the sample was taken downstream of the filter sock.
440 S. Church Street, Suite 900: Charlotte, NC 28202
T 704.338, 6700 F 704. 338.6760

Mr. Harshad Londhe
May 15, 2020
Page 2
The TOH-1 location is down -gradient of the galvanizing building. The NCDEQ requested that
Galvan collect a sample of surface water runoff from this location to further evaluate the site -
specific contribution to stormwater quality. Originally, TOH-1 was located at the top of the recent
earthwork. It has subsequently been moved west to the rip rap drainage feature and is adjacent to
the former groundwater treatment system. Stormwater runoff was tan to brown in color and
odorless. It was without noticeable suspended solids. Minor floating solids were observed. No
evidence of erosion, deposition, or foam was visible. A filter sock was present upgrade of TOH-1
and care was taken to ensure that the sample was taken downstream of the filter sock.
Quantitative Monitoring
Subsequent to qualitative observations, HDR collected three stormwater samples for quantitative
analysis as follows:
OF #1 was analyzed for:
• Total Suspended Solids (TSS) usingSM 2540D
• pH using EPA 9040
• Copper, lead, and zinc using EPA200.7
• Non -polar Oil and Grease/Total Petroleum Hydrocarbons (O&G/TPH) using EPA 1664B
• Total Toxic Organics using EPA608 (pesticides and PCBs), EPA625 (semi -volatile
organics), and EPA 624.1 (volatile organics)
OF #5 and the TOH-1 location were analyzed for:
• TSS using SM 2540D
• Copper, lead, and zinc using EPA200.7
Samples were collected in certified clean sample containers provided by Pace Analytical Services,
LLC (Pace) and transported under chain -of -custody to Pace for analysis. The results of analyses
indicate that benchmark values identified in the GP were exceeded, as follows:
• OF #1
o TSS: 131 mg/L (Benchmark: 100 mg/L)
o Copper: 0.1920 mg/L (Benchmark: 0.007 mg/L)
o Zinc: 6.09 mg/L (Benchmark: 0.067 mg/L)
• OF #5
o Copper: 0.0253 (Benchmark: 0.007 mg/L)
o Zinc: 3.70 mg/L (Benchmark: 0.067 mg/L)
• TOH-1
o TSS: 154 mg/L (Benchmark: 100 mg/L)
o Copper: 0.1370 mg/L (Benchmark: 0.007 mg/L)
o Lead: 0.1110 mg/L (Benchmark: 0.03 mg/L)
o Zinc: 34.5 mg/L (Benchmark: 0.067 mg/L)
It is noted that OF #2, installed by NCDOT, is not currently being sampled. During construction, OF
#2 was not representative of Site conditions due to ongoing earthwork and surface water drainage
re-routing. Subsequent to completion of construction, OF #2 appears stable and may be
reconsidered as a representative outfall for the Galvan site.

Mr. Harshad Londhe
May 15,2020
Page 3
In accordance with the GP, Galvan had previously been required to comply with Tier Two
requirements. These include (in addition to those requirements outlined in Tier One) monthly
sampling of permitted outfalls (continued until three consecutive sample results fall below or within
the appropriate benchmark or benchmark range), submittal of "no flow" reports if sufficient
discharge does not occur in any given month, and maintenance of a record of all Tier Two reports in
the Stormwater Pollution Prevention Plan (SPPP).
Galvan is currently required to comply with Tier Three requirements. The Tier Three requirements
state that, if, during the duration of the GP, exceedances occur for any specific parameter on four
occasions, Galvan must contact the DWQ Regional Supervisor within 30 days of receipt of the
fourth result. This is the twenty-first sampling event since March of 2015 with a TSS exceedance,
the twenty-second event with a copper exceedance, the twentieth event with a lead exceedance,
and the twenty-second event with a zinc exceedance. As such, Galvan should notify NCDEQ in
accordance with the GP. Note that per NCDEQ requirements, Galvan applied for a NPDES
Stormwater Individual Permit on March 15, 2019. To date, NCDEQ has not responded to that
permit application, thus, Galvan continues to operate under the GP.
Please do not hesitate to contact the undersigned at 704.338.6787 if you have questions or
comments regarding this report. We appreciate the opportunity to continue to assist Galvan on this
project.
Sincerely,
HDR Engineering, Inc. of the Carolinas
Mark Filardi, P.G.
Senior Geologist
Attachments:
Site Plan
Stormwater Discharge Qualitative Monitoring Reports for OF #1, 3 through 5, and TOH-1
Stormwater Discharge Monitoring Report for OF #1, 5, and TOH-1
Pace Analytical Laboratory Report

For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N_/C/ / / / / / / / or Certificate of Coverage No.: N_/C/G/ 0/ 3 / 0 / 0 /0 /0 /
Facility Name: Galvan Industries, Inc.
County: Cabarrus Phone No. [phone]
Inspector: Robert Mull
Date of Inspection:
Time of Inspection:
04/20/2020
1030
Total Event Precipitation (inches): 0 .7 4
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. 1
Receiving Stream:
Back Creek
Structure (pipe, ditch, etc.): rip —rap to culvert
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of 2
SWU-242, Last modified 06/01/2018

7. Is there any foam in the stormwater discharge? Q Yes
8. Is there an oil sheen in the stormwater discharge? OYes
9. Is there evidence of erosion or deposition at the outfall?
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light t a n
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
0 No
O No.
0 Yes No.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

k
For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 0/ 3/ 0/ 0 /0 /0 /
Facility Name: Galvan Industries Inc.
County: Cabarrus Phone No. [phone]
Inspector: Robert Mull
Date of Inspection:
Time of Inspection:
04/20/2020
1120
Total Event Precipitation (inches): 0.7 4
_._.._....... _._ . ___. ............... _ ._ .. _..... ___............. _... ._... _ ........
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
la�11161 �( n
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. 3 Structure (pipe, ditch, etc.): rip —rap to culvert
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light tan
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
I 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes No.
8. Is there an oil sheen in the stormwater discharge? 0Yes No.
9. Is there evidence of erosion or deposition at the outfall? UYes Q No. slight erosion
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/O1/2018

For guidance on f lling out this form, please visit https:Hdcq.ne.gov/about/divisions/energy-mineral-land-resources/
npdes-stonnwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 0/3/0/0/0 /0 /
Facility Name:. Galvan Industries Inc.
County: Cabarrus Phone No. [phone]
Inspector:
Robert Mull
Date of Inspection: 0 4/ 2 0/ 2 0 2 0
Time of Inspection: 1115
Total Event Precipitation (inches): 0 .7 4
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
A�Ie6p, �/W
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. 4
Receiving Stream:
Back Creek
Structure (pipe, ditch, etc.): culvert
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: c l e a r
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
1 2 3 4 5
Is there any foam in the stormwater discharge? O Yes 0 No
Is there an oil sheen in the stormwater discharge? 0Yes 0 No. _
Is there evidence of erosion or deposition at the outfall? 0 Yes O No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 0/ 3/ 0/ 0 / 0 / 0 /
Facility Name: Galvan Industries. Inc.
County: Cabarrus
Inspector: Robert Mull
Date of Inspection:
Time of Inspection:
04/20/2020
1050
Total Event Precipitation (inches): 0.74
Phone No. [phone]
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
�lzx�
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. 5 Structure (pipe, ditch, etc.): rip —rap to culvert
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light tan
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 0
4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes
8. Is there an oil sheen in the stormwater discharge? QYes
9. Is there evidence of erosion or deposition at the outfall?
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
No.
o No.
o Yes No.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

For guidance onfilling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N_/C/ / / / / / / / or Certificate of Coverage No.: N_/C/G/ 0/ 3 / 0 / 0 /0 /0 /
Facility Name, Galvan Industries, Inc.
County: Cabarrus
Inspector: Robert Mull
Date of Inspection:
04/20/2020
Time of Inspection: 1100
Total Event Precipitation (inches): 0. 7 4
Phone No. [phone]
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
OW(
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. TOH-1 Structure (pipe, ditch, etc.): Stepped rip —rap
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: tan —brown
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? o Yes (0 No
8. Is there an oil sheen in the stormwater discharge? 0Yes (O No.
9. Is there evidence of erosion or deposition at the outfall? 9 Yes P No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR) / SPPP Annual Update DATA REVIEW FORM
Calendar Year April 2020
Individual NPDES Permit No. NCS❑❑❑❑❑❑ or
Certificate of Coverage (COC) No. NCG❑0 ❑3 K F0Fo ❑0
This monitoring report summary of the calendar year should be kept on file on -site with the facility SPPP.
Facility Name: Galvan Industries
County: Cabarrus
Phone Number: 7( 04 ) 455-5102 Total no. of SDOs monitored 3
Outfall No. 1, 5, TOF
Is this outfall currently in Tier 2 (monitored monthly)? Yes M No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes M No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑
Parameter, (units)
Total
Total
pH
Copper;
Lead
Zinc
Non -Polar
Total Toxic
Rainfall,
Suspended
O&G/TPH
Organics
Inches
Solids (TSS)
Benchmark
N/A "
100 mg/L 6.0- 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
Date Sample
Collected,
mm/dd/yy
OF-1
4/20/2020
131.00
6.90
0.1920
0.0174
6.09
ND
ND
OF-5
4/20/2020
74.50
0.0253
ND
3,70
TOH-1
4/20/2020
154.00
0.1370
0.1110
34.5
SW U-264 - Generic Annuai umK
Last revised 510212018

Additional Outfall Attachment
Outfall No.
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑
SWU-264 - Generic Annual DMR
Last revised 510212018

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,.�aceAnalyfical@
www.pacelabs.com
April 30, 2020
Mark Filardi
HDR
440 S. Church St
Suite 900
Charlotte, NC 28202
RE: Project: GALVAN STORMWATER
Pace Project No.: 92474369
Dear Mark Filardi:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski for
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
cc: Charles Gruenberg
Coleman Marchin, HDR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 36

fill cal
immpacelabs.com
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 36

aIceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92474369001 OF #1
EPA 1664B
HH
1
PAST-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
36
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
92474369002 OF #5
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
SM 2540D-2011
RED
1
PASI-A
92474369003 TOH-1
EPA 200.7 Rev 4.4 1994
RDT
3
PASI-A
SM 254OD-2011
RED
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 36

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PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: EPA 1664B
Description: HEM, Oil and Grease
Client: HDR Engineering
Date: April 30, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 1664E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 36

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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[phone]
PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: EPA 608.3
Description: 608 PCB Pest RVE
Client: HDR Engineering
Date: April 30, 2020
General Information:
1 sample was analyzed for EPA 608.3 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 608.3 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 537262
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 2865429)
• gamma -Chlordane
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 36

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PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: EPA 200.7 Rev 4.4 1994
Description: 200.7 MET ICP
Client: HDR Engineering
Date: April 30, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for EPA 200.7 Rev 4.4 1994 by Pace Analytical Services Asheville. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 Rev 4.4 1994 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 537474
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92473438001,92474369002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2866321)
• Zinc
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 6 of 36

aceAnalj6cal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: EPA 625.1
Description: 625 RVE
Client: HDR Engineering
Date: April 30, 2020
General Information:
1 sample was analyzed for EPA 625.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 537258
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92473907003
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MSD (Lab ID: 2865415)
• 2,4,6-Trichlorophenol
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 7 of 36

QD
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PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: EPA 624.1
Description: 624 Volatile Organics
Client: HDR Engineering
Date: April 30, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 624.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 537934
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 2631035001
P5: The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
• MS (Lab ID: 2870158)
• 2-Chloroethylvinyl ether
• MSD (Lab ID: 2870159)
• 2-Chloroethylvinyl ether
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 8 of 36

aceAnalytical
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PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: SM 254OD-2011
Description: 2540D Total Suspended Solids
Client: HDR Engineering
Date: April 30, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
3 samples were analyzed for SM 254OD-2011 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 9 of 36

aceAnalj6cal
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I
PROJECT NARRATIVE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Method: EPA 9040C
Description: 9040 pH
Client: HDR Engineering
Date: April 30, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 9040C by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1­13: Sample was received or analysis requested beyond the recognized method holding time.
• OF #1 (Lab ID: 92474369001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 36

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Sample: OF #1
Lab ID: 92474369001 Collected:
04/20/20 10:30
Received: 04/20/20 12:00 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qua[
HEM, Oil and Grease
Analytical Method: EPA 1664E
Pace Analytical
Services - Charlotte
Oil and Grease
ND
mg/L
4.8
1
04/22/20 15:37
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical
Services - Charlotte
Aldrin
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
309-00-2
alpha-BHC
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
319-84-6
beta-BHC
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
319-85-7
delta-BHC
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
57-74-9
alpha -Chlordane
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
5103-71-9
gamma -Chlordane
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
5103-74-2 L1
4,4'-DDD
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
72-54-8
4,4'-DDE
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
72-55-9
4,4'-DDT
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
50-29-3
Dieldrin
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
60-57-1
Endosulfan I
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
959-98-8
Endosulfan 11
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
1031-07-8
Endrin
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
7421-93-4
Heptachlor
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
1
04/20/20 21:35
04/23/20 14:48
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
11096-82-5
Toxaphene
ND
ug/L
0.50
1
04/20/20 21:35
04/23/20 14:48
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
80
%
10-130
1
04/20/20 21:35
04/23/20 14:48
877-09-8
Decachlorobiphenyl (S)
66
%
10-130
1
04/20/20 21:35
04/23/20 14:48
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
192 ug/L
5.0 1 04/22/20 01:48
04/27/20 21:12
7440-50-8
Lead
17.4 ug/L
5.0 1 04/22/20 01:48
04/27/20 21:12
7439-92-1
Zinc
6090 ug/L
10.0 1 04/22/20 01:48
04/27/20 21:12
7440-66-6
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND ug/L
5.0 1 04/20/20 20:47
04/24/20 21:22
83-32-9
Acenaphthylene
ND ug/L
5.0 1 04/20/20 20:47
04/24/20 21:22
208-96-8
REPORT OF LABORATORY ANALYSIS
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Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 36

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Sample: OF #1 Lab ID: 92474369001 Collected: 04/20/20 10:30 Received: 04/20/20 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical
Services - Charlotte
Anthracene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
120-12-7
Benzidine
ND
ug/L
50.0
1
04/20/20 20:47
04/24/20 21:22
92-87-5
Benzo(a)anthracene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
7005-72-3
Chrysene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
04/20/20 20:47
04/24/20 21:22
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
117-81-7
Fluoranthene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
206-44-0
Fluorene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
193-39-5
Isophorone
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
78-59-1
Nitrobenzene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
88-75-5
4-Nitrophenol
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
86-30-6
Pentachlorophenol
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
87-86-5
Phenanthrene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
85-01-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 36

aCPAO ytical
www.pacelabs.com
Project: GALVAN STORMWATER
Pace Project No.: 92474369
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OF #1
Lab lD: 92474369001 Collected:
04/20/20 10:30
Received: 04/20/20 12:00 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical Services - Charlotte
Phenol
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
108-95-2
Pyrene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
129-00-0
1,2,4-Trichoorobenzene
ND
ug/L
5.0
1
04/20/20 20:47
04/24/20 21:22
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
04/20/20 20:47
04/24/20 21:22
88-06-2
Surrogates
Nitrobenzene-d5 (S)
58
%
10-120
1
04/20/20 20:47
04/24/20 21:22
4165-60-0
2-Fluorobiphenyl (S)
52
%
15-120
1
04/20/20 20:47
04/24/20 21:22
321-60-8
Terphenyl-d14 (S)
100
%
11-131
1
04/20/20 20:47
04/24/20 21:22
1718-51-0
Phenol-d6 (S)
28
%
10-120
1
04/20/20 20:47
04/24/20 21:22
13127-88-3
2-Fluorophenol (S)
39
%
10-120
1
04/20/20 20:47
04/24/20 21:22
367-12-4
2,4,6-Tribromophenol (S)
53
%
10-137
1
04/20/20 20:47
04/24/20 21:22
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
Acrolein
ND
ug/L
5.0
1
04/24/20 15:04
107-02-8
Acrylonitrile
ND
ug/L
5.0
1
04/24/20 15:04
107-13-1
Benzene
ND
ug/L
1.0
1
04/24/20 15:04
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
04/24/20 15:04
75-27-4
Bromoform
ND
ug/L
2.0
1
04/24/20 15:04
75-25-2
Bromomethane
ND
ug/L
2.0
1
04/24/20 15:04
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
04/24/20 15:04
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
04/24/20 15:04
108-90-7
Chloroethane
ND
ug/L
2.0
1
04/24/20 15:04
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
5.0
1
04/24/20 15:04
110-75-8 c3
Chloroform
ND
ug/L
2.0
1
04/24/20 15:04
67-66-3
Chloromethane
ND
ug/L
2.0
1
04/24/20 15:04
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
04/24/20 15:04
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
04/24/20 15:04
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
04/24/20 15:04
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
04/24/20 15:04
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
04/24/20 15:04
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
04/24/20 15:04
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
04/24/20 15:04
75-35-4
trans- 1,2-Dichloroethene
ND
ug/L
2.0
1
04/24/20 15:04
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
04/24/20 15:04
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
04/24/20 15:04
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
04/24/20 15:04
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
04/24/20 15:04
100-41-4
Methylene Chloride
ND
ug/L
2.0
1
04/24/20 15:04
75-09-2
Naphthalene
ND
ug/L
5.0
1
04/24/20 15:04
91-20-3
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
04/24/20 15:04
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
04/24/20 15:04
127-18-4
Toluene
ND
ug/L
1.0
1
04/24/20 15:04
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1
04/24/20 15:04
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
04/24/20 15:04
79-00-5
Trichloroethene
ND
ug/L
2.0
1
04/24/20 15:04
79-01-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced,
except in full,
Date: 04/30/2020 09:43 AM
without the written consent of Pace
Analytical Services, LLC.
Page 13 of 36

,�aceAna1j cal
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ANALYTICAL RESULTS
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OF #1
Lab ID: 92474369001 Collected:
04/20/20 10:30
Received: 04/20/20 12:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L
2.0
1
04/24/20 15:04 75-01-4
Surrogates
4-Bromofluorobenzene (S)
103 %
70-130
1
04/24/20 15:04 460-00-4
Toluene-d8 (S)
102 %
70-130
1
04/24/20 15:04 2037-26-5
1,2-Dichioroethane-d4 (S)
110 %
70-130
1
04/24/20 15:04 17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
131 mg/L
18.5
1
04/22/20 17:45
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.9 Std. Units
0.10
1
04/22/20 15:25 H3
Date: 04/30/2020 09:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 36

ceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Sample: OF #5
Lab ID: 92474369002 Collected: 04/20/20 10:50
Received: 04/20/20 12:00 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
25.3 ug/L 5.0 1
04/22/20 01:48 04/27/20 21:15 7440-50-8
Lead
ND ug/L 5.0 1
04/22/20 01:48 04/27/20 21:15 7439-92-1
Zinc
3700 ug/L 10.0 1
04/22/20 01:48 04/27/20 21:15 7440-66-6 M1
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services -Asheville
Total Suspended Solids
74.5 mg/L 12.5 1
04/22/20 17:45
Date: 04/30/2020 09:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 36

a1,eAna1j&a1
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Sample: TOH-1
Lab ID: 92474369003 Collected: 04/20/20 11:00
Received: 04/20/20 12:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
137 ug/L 5.0
1
04/22/20 01:48 04/27/20 21:24 7440-50-8
Lead
111 ug/L 5.0
1
04/22/20 01:48 04/27/20 21:24 7439-92-1
Zinc
34500 ug/L 1000
100
04/22/20 01:48 04/29/20 16:36 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
154 mg/L 12.5
1
04/22/20 17:46
Date: 04/30/2020 09:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537644 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92474369001
METHOD BLANK: 2866985 Matrix: Water
Associated Lab Samples: 92474369001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 04/22/20 15:32
LABORATORY CONTROL SAMPLE:
2866986
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 35.5
89
78-114
MATRIX SPIKE SAMPLE:
2866987
92474514001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
NO 38.5
36.9
94
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 36

aceAna/Xical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537474 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92474369001, 92474369002, 92474369003
METHOD BLANK: 2866317 Matrix: Water
Associated Lab Samples: 92474369001, 92474369002, 92474369003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L ND 5.0 04/27/20 20:19
Lead ug/L ND 5.0 04/27/20 20:19
Zinc ug/L ND 10.0 04/27/20 20:19
LABORATORY CONTROL SAMPLE:
2866318
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug/L
500
500 100 85-115
Lead
ug/L
500
504 101 85-115
Zinc
ug/L
500
495 99 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2866319
2866320
MS
MSD
92473438001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper ug/L
ND
500
500
507
516
101
103
70-130 2
Lead ug/L
12.4
500
500
527
535
103
105
70-130 2
Zinc ug/L
776
500
500
1250
1290
95
102
70-130 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2866321
2866322
MS
MSD
92474369002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper ug/L
25.3
500
500
549
539
105
103
70-130 2
Lead ug/L
ND
500
500
526
516
105
103
70-130 2
Zinc ug/L
3700
500
500
4360
4260
131
111
70-130 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 36

�acl
Analytical
www.pacelabs.com
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537934
QC Batch Method: EPA 624.1
Associated Lab Samples: 92474369001
METHOD BLANK: 2868612
Associated Lab Samples: 92474369001
Parameter
Units
1,1,1-Trichloroethane
ug/L
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
1,3-Dichlorobenzene
ug/L
1,4-Dichlorobenzene
ug/L
2-Chloroethylvinyl ether
ug/L
Acrolein
ug/L
Acrylonitrile
ug/L
Benzene
ug/L
Bromodichlorom ethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
cis-1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
Ethylbenzene
ug/L
Methylene Chloride
ug/L
Naphthalene
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
trans- 1,3-Dichloropropene
ug/L
Trichloroethene
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Laboratory:
Matrix: Water
EPA 624.1
624 MSV
Pace Analytical Services - Charlotte
Blank
Result
Reporting
Limit
Analyzed
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
5.0
04/24/2012:04
ND
5.0
04/24/2012:04
ND
5.0
04/24/2012:04
ND
1.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
1.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
5.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
1.0
04/24/2012:04
ND
2.0
04/24/2012:04
ND
2.0
04/2412012:04
ND
2.0
04/2412012:04
ND
2.0
04/24/2012:04
103
70-130
04/24/2012:04
102
70-130
04/24/2012:04
102
70-130
04/24/2012:04
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 36

aceAnalyticai®
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
LABORATORY CONTROL SAMPLE:
Parameter
2868613
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
20
21.3
106
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
18.4
92
60-140
1,1,2-Trichloroethane
ug/L
20
20.7
104
70-130
1,1-Dichloroethane
ug/L
20
19.3
96
70-130
1,1-Dichloroethene
ug/L
20
19.8
99
50-150
1,2-Dichlorobenzene
ug/L
20
19.6
98
65-135
1,2-Dichloroethane
ug/L
20
20.7
104
49-155
1,2-Dichloropropane
ug/L
20
19.5
97
35-165
1,3-Dichlorobenzene
ug/L
20
19.6
98
70-130
1,4-Dichlorobenzene
ug/L
20
20.0
100
65-135
2-Chloroethylvinyl ether
ug/L
40
37.9
95
1-225
Acrolein
ug/L
100
138
138
60-140
Acrylonitrile
ug/L
100
88.2
88
60-140
Benzene
ug/L
20
20.5
102
65-135
Bromodichloromethane
ug/L
20
22.8
114
65-135
Bromoform
ug/L
20
19.7
98
70-130
Bromomethane
ug/L
20
23.6
118
15-185
Carbon tetrachloride
ug/L
20
22.0
110
70-130
Chlorobenzene
ug/L
20
19.1
96
65-135
Chloroethane
ug/L
20
20.1
101
40-160
Chloroform
ug/L
20
21.2
106
70-135
Chloromethane
ug/L
20
14.8
74
1-205
cis-1,3-Dichloropropene
ug/L
20
21.1
105
25-175
Dibromochloromethane
ug/L
20
20.1
101
70-135
Ethylbenzene
ug/L
20
18.7
94
60-140
Methylene Chloride
ug/L
20
18.7
94
60-140
Naphthalene
ug/L
20
22.0
110
70-130
Tetrachloroethene
ug/L
20
19.9
99
70-130
Toluene
ug/L
20
19.7
98
70-130
trans-1,2-Dichloroethene
ug/L
20
19.6
98
70-130
trans-1,3-Dichloropropene
ug/L
20
21.4
107
50-150
Trichloroethene
ug/L
20
21.5
107
65-135
Vinyl chloride
ug/L
20
19.7
99
5-195
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8(S)
%
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2870158
2870159
MS
MSD
2631035001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
1,1,1-Trichloroethane
ug/L
ND
20
20
22.8
25.1
114
125
52-162
10
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
17.0
18.8
85
94
46-157
10
1,1,2-Trichloroethane
ug/L
ND
20
20
20.7
20.6
104
103
52-150
0
1,1-Dichloroethane
ug/L
NO
20
20
20.6
22.0
103
110
59-155
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 36

auuAnalytical
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QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2870158
Parameter
Units
2631035001
Result
MS
Spike
Conc.
1,1-Dichloroethene
ug/L
ND
20
1,2-Dichlorobenzene
ug/L
ND
20
1,2-Dichloroethane
ug/L
ND
20
1,2-Dichloropropane
ug/L
ND
20
1,3-Dichlorobenzene
ug/L
ND
20
1,4-Dichlorobenzene
ug/L
ND
20
2-Chloroethylvinyl ether
ug/L
ND
40
Acrolein
ug/L
ND
100
Acrylonitrile
ug/L
ND
100
Benzene
ug/L
ND
20
Bromodichloromethane
ug/L
2.0
20
Bromoform
ug/L
ND
20
Bromomethane
ug/L
ND
20
Carbon tetrachloride
ug/L
ND
20
Chlorobenzene
ug/L
ND
20
Chloroethane
ug/L
ND
20
Chloroform
ug/L
7.4
20
Chloromethane
ug/L
ND
20
cis-1,3-Dichloropropene
ug/L
ND
20
Dibromochlorom ethane
ug/L
ND
20
Ethylbenzene
ug/L
ND
20
Methylene Chloride
ug/L
ND
20
Naphthalene
ug/L
ND
20
Tetrachloroethene
ug/L
ND
20
Toluene
ug/L
ND
20
trans-1,2-Dichloroethene
ug/L
ND
20
trans- 1,3-Dichloropropene
ug/L
ND
20
Trichloroethene
ug/L
ND
20
Vinyl chloride
ug/L
ND
20
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
2870159
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
20
21.6
22.6
108
113
1-234
4
20
18.0
19.8
90
99
18-190
10
20
20.7
22.1
103
111
49-155
7
20
18.8
19.2
94
96
1-210
2
20
18.5
19.9
93
99
59-156
7
20
19.2
19.5
96
98
18-190
2
40
ND
ND
0
0
1-305
P5
100
146
157
143
154
40-160
7
100
94.1
99.2
94
99
40-160
5
20
21.3
21.6
104
106
37-151
1
20
23.9
24.5
109
113
35-155
3
20
22.5
23.5
113
118
45-169
4
20
21.2
21.1
103
103
1-242
0
20
24.1
25.0
121
125
70-140
4
20
19.2
19.4
96
97
37-160
1
20
19.9
21.9
100
109
14-230
9
20
28.5
30.7
105
116
51-138
7
20
18.7
22.2
92
109
1-273
17
20
20.8
21.7
104
108
1-227
4
20
21.9
21.3
109
106
53-149
3
20
18.4
19.1
92
96
37-162
4
20
18.7
20.0
93
100
1-221
7
20
20.3
20.6
98
99
70-130
1
20
20.4
21.0
102
105
64-148
3
20
20.6
20.5
103
102
47-150
1
20
20.5
22.3
102
111
54-156
8
20
22.7
22.5
114
112
17-183
1
20
21.0
21.7
105
108
70-157
3
20
21.5
23.9
108
119
1-251
10
100
101
70-130
102
105
70-130
102
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 36

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537262
QC Batch Method: EPA 608.3
Associated Lab Samples: 92474369001
QUALITY CONTROL DATA
Analysis Method: EPA 608.3
Analysis Description: 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 2865428
Associated Lab Samples: 92474369001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
4,4'-DDD
ug/L
ND
0.050
04/23/20 15:32
4,4'-DDE
ug/L
ND
0.050
04/23/20 15:32
4,4'-DDT
ug/L
ND
0.050
04/23/20 15:32
Aldrin
ug/L
ND
0.050
04/23/20 15:32
alpha-BHC
ug/L
ND
0.050
04/23/20 15:32
alpha -Chlordane
ug/L
ND
0.050
04/23/20 15:32
beta-BHC
ug/L
ND
0.050
04/23/20 15:32
Chlordane (Technical)
ug/L
ND
0.50
04/23/20 15:32
delta-BHC
ug/L
ND
0.050
04/2312015:32
Dieldrin
ug/L
ND
0.050
04/23/20 15:32
Endosulfan I
ug/L
ND
0.050
04/23/20 15:32
Endosulfan II
ug/L
ND
0.050
04/23/20 15:32
Endosulfan sulfate
ug/L
ND
0.050
04/23/20 15:32
Endrin
ug/L
ND
0.050
04/23/20 15:32
Endrin aldehyde
ug/L
ND
0.050
04/23/20 15:32
gamma-BHC (Lindane)
ug/L
ND
0.050
04/23/20 15:32
gamma -Chlordane
ug/L
ND
0.050
04/23/20 15:32
Heptachlor
ug/L
ND
0.050
04/23/20 15:32
Heptachlor epoxide
ug/L
ND
0.050
04/23/20 15:32
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
04/23/20 15:32
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
04/23/20 15:32
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
04/23/20 15:32
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
04/23/20 15:32
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
04/23/20 15:32
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
04/23/20 15:32
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
04/23/20 15:32
Toxaphene
ug/L
ND
0.50
04/23/20 15:32
Decachlorobiphenyl (S)
%
98
10-130
04/23/20 15:32
Tetrachloro-m-xylene (S)
%
85
10-130
04/23/20 15:32
Qualifiers
LABORATORY CONTROL SAMPLE:
2865429
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.26
103
31-141
4,4'-DDE
ug/L
0.25
0.23
92
30-145
4,4'-DDT
ug/L
0.25
0.26
102
25-160
Aldrin
ug/L
0.25
0.18
71
42-140
alpha-BHC
ug/L
0.25
0.27
106
37-140
alpha -Chlordane
ug/L
0.25
0.25
99
45-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 36

�a,eAnalyticaf
www.pacelabs.com
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2865429
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
beta-BHC
ug/L
0.25
0.32
126
17-147
delta-BHC
ug/L
0.25
0.26
103
19-140
Dieldrin
ug/L
0.25
0.27
109
36-146
Endosulfan I
ug/L
0.25
0.27
109
45-153
Endosulfan II
ug/L
0.25
0.27
107
1-202
Endosulfan sulfate
ug/L
0.25
0.26
105
26-144
Endrin
ug/L
0.25
0.27
108
30-147
Endrin aldehyde
ug/L
0.25
0.24
98
50-148
gamma-BHC (Lindane)
ug/L
0.25
0.28
111
32-140
gamma -Chlordane
ug/L
0.25
0.60
241
45-140 L1
Heptachlor
ug/L
0.25
0.23
91
34-140
Heptachlor epoxide
ug/L
0.25
0.26
103
37-142
Decachlorobiphenyl (S)
%
113
10-130
Tetrachloro-m-xylene (S)
%
107
10-130
LABORATORY CONTROL SAMPLE:
2865432
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
5 4.6 91
50-140
PCB-1260 (Aroclor 1260)
ug/L
5 4.8 96
8-140
Decachlorobiphenyl (S)
%
103
10-130
Tetrachloro-m-xylene (S)
%
86
10-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2865430
2865431
MS
MSD
2631087001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
PCB-1016 (Aroclor 1016)
ug/L
ND 5
5 5.3
5.6 107
112
50-140 4
PCB-1260 (Aroclor 1260)
ug/L
ND 5
5 4.7
5.1 94
102
8-140 8
Decachlorobiphenyl (S)
%
101
109
10-130
Tetrachloro-m-xylene (S)
%
94
91
10-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2865433
2865434
MS
MSD
2631087001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
4,4'-DDD
ug/L
ND
0.25
0.25
0.25
0.28
100
111
31-141
10
4,4'-DDE
ug/L
ND
0.25
0.25
0.23
0.24
94
95
30-145
1
4,4'-DDT
ug/L
ND
0.25
0.25
0.25
0.27
102
107
25-160
5
Aldrin
ug/L
ND
0.25
0.25
0.17
0.16
66
64
42-140
4
alpha-BHC
ug/L
ND
0.25
0.25
0.22
0.23
88
92
37-140
4
alpha -Chlordane
ug/L
ND
0.25
0.25
0.27
0.27
109
109
45-140
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 36

8ceAna1j cal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2865433
2865434
MS
MSD
2631087001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
beta-BHC
ug/L
ND
0.25
0.25
0.29
0.30
115
121
17-147
5
delta-BHC
ug/L
ND
0.25
0.25
0.24
0.24
94
97
19-140
2
Dieldrin
ug/L
ND
0.25
0.25
0.26
0.27
104
109
36-146
4
Endosulfan I
ug/L
ND
0.25
0.25
0.29
0.29
116
115
45-153
1
Endosulfan 11
ug/L
ND
0.25
0.25
0.25
0.26
101
102
1-202
2
Endosulfan sulfate
ug/L
ND
0.25
0.25
0.25
0.26
98
104
26-144
6
Endrin
ug/L
ND
0.25
0.25
0.24
0.26
97
102
30-147
5
Endrin aldehyde
ug/L
ND
0.25
0.25
0.25
0.26
101
104
50-150
3
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.23
0.24
92
95
32-140
4
gamma -Chlordane
ug/L
ND
0.25
0.25
0.28
0.28
110
111
45-140
0
Heptachlor
ug/L
ND
0.25
0.25
0.19
0.20
78
82
34-140
6
Heptachlor epoxide
ug/L
0.068
0.25
0.25
0.31
0.30
96
93
37-142
2
Decachlorobiphenyl (S)
%
91
101
10-130
Tetrachloro-m-xylene (S)
%
93
94
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 36

aceAnalytical
www.pacelabs.com
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537258
QC Batch Method: EPA 625.1
Associated Lab Samples: 92474369001
QUALITY CONTROL DATA
Analysis Method: EPA 625.1
Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 2865412
Associated Lab Samples: 92474369001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
04/21/20 16:15
1,2-Diphenylhydrazine
ug/L
ND
5.0
04/21/20 16:15
2,4,6-Trichlorophenol
ug/L
ND
10.0
04/21/20 16:15
2,4-Dichlorophenol
ug/L
ND
5.0
04/21/20 16:15
2,4-Dimethylphenol
ug/L
ND
10.0
04/21/20 16:15
2,4-Dinitrophenol
ug/L
ND
50.0
04/21/20 16:15
2,4-Dinitrotoluene
ug/L
ND
5.0
04/21/20 16:15
2,6-Dinitrotoluene
ug/L
ND
5.0
04/21/20 16:15
2-Chloronaphthalene
ug/L
ND
5.0
04/21/20 16:15
2-Chlorophenol
ug/L
ND
5.0
04/21/20 16:15
2-Nitrophenol
ug/L
ND
5.0
04/21/20 16:15
3,3'-Dichlorobenzidine
ug/L
ND
10.0
04/2112016:15
4,6-Dinitro-2-methylphenol
ug/L
ND
10.0
04/21/20 16:15
4-Bromophenylphenyl ether
ug/L
ND
5.0
04/21/20 16:15
4-Chloro-3-methylphenol
ug/L
ND
5.0
04/21/20 16:15
4-Chlorophenylphenyl ether
ug/L
ND
5.0
04/21/20 16:15
4-Nitrophenol
ug/L
ND
10.0
04/21/20 16:15
Acenaphthene
ug/L
ND
5.0
04/21/20 16:15
Acenaphthylene
ug/L
ND
5.0
04/21/20 16:15
Anthracene
ug/L
ND
5.0
04/21/20 16:15
Benzidine
ug/L
ND
50.0
04/21/20 16:15
Benzo(a)anthracene
ug/L
ND
5.0
04/21/20 16:15
Benzo(a)pyrene
ug/L
ND
5.0
04/21/20 16:15
Benzo(b)fluoranthene
ug/L
ND
5.0
04/21/20 16:15
Benzo(g,h,i)perylene
ug/L
NO
5.0
04/2112016:15
Benzo(k)fluoranthene
ug/L
ND
5.0
04/21/20 16:15
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
04/21/20 16:15
bis(2-Chloroethyl) ether
ug/L
ND
5.0
04/21/20 16:15
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
04/21/20 16:15
Butylbenzylphthalate
ug/L
ND
5.0
04/21/20 16:15
Chrysene
ug/L
ND
5.0
04/21/20 16:15
Di-n-butylphthalate
ug/L
ND
5.0
04/21/20 16:15
Di-n-octylphthalate
ug/L
ND
5.0
04/21/20 16:15
Dibenz(a,h)anthracene
ug/L
ND
5.0
04/21/20 16:15
Diethyl phthalate
ug/L
ND
5.0
04/21/20 16:15
Dimethylphthalate
ug/L
ND
5.0
04/2112016:15
Fluoranthene
ug/L
ND
5.0
04/21/20 16:15
Fluorene
ug/L
ND
5.0
04/21/20 16:15
Hexachloro-1,3-butadiene
ug/L
ND
5.0
04/21/20 16:15
Hexachlorobenzene
ug/L
ND
5.0
04/21/20 16:15
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 36

aceAnalj cal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
METHOD BLANK: 2865412
Associated Lab Samples: 92474369001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Hexachlorocyclopentadiene
ug/L
ND
10.0
04/21/20 16:15
Hexachloroethane
ug/L
ND
5.0
04/21/20 16:15
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
04/21/20 16:15
Isophorone
ug/L
ND
10.0
04/21/20 16:15
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
04/21/20 16:15
N-Nitrosodimethylamine
ug/L
ND
5.0
04/21/20 16:15
N-Nitrosodiphenylamine
ug/L
ND
10.0
04/21/20 16:15
Nitrobenzene
ug/L
ND
5.0
04/21/20 16:15
Pentachlorophenol
ug/L
ND
10.0
04/21/20 16:15
Phenanthrene
ug/L
ND
5.0
04/21/20 16:15
Phenol
ug/L
ND
5.0
04/21/20 16:15
Pyrene
ug/L
ND
5.0
04/21/20 16:15
2,4,6-Tribromophenol (S)
%
57
10-137
04/21/20 16:15
2-Fluorobiphenyl (S)
%
71
15-120
04/21/20 16:15
2-Fluorophenol (S)
%
42
10-120
04/21/20 16:15
Nitrobenzene-d5 (S)
%
79
10-120
04/21/20 16:15
Phenol-d6 (S)
%
42
10-120
04/21/20 16:15
Terphenyl-d14 (S)
%
112
11-131
04/21/20 16:15
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2865413
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
25.7
51
44-142
1,2-Diphenylhydrazine
ug/L
50
40.9
82
25-150
2,4,6-Trichlorophenol
ug/L
50
31.4
63
37-144
2,4-Dichlorophenol
ug/L
50
38.0
76
1-191
2,4-Dimethylphenol
ug/L
50
41.5
83
32-119
2,4-Dinitrophenol
ug/L
250
154
61
1-181
2,4-Dinitrotoluene
ug/L
50
48.3
97
39-139
2,6-Dinitrotoluene
ug/L
50
47.7
95
50-158
2-Chloronaphthalene
ug/L
50
34.8
70
60-118
2-Chlorophenol
ug/L
50
39.1
78
23-134
2-Nitrophenol
ug/L
50
40.2
80
29-182
3,3'-Dichlorobenzidine
ug/L
100
81.1
81
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
69.3
69
1-181
4-Bromophenylphenyl ether
ug/L
50
39.5
79
53-127
4-Chloro-3-methylphenol
ug/L
100
84.8
85
22-147
4-Chlorophenylphenyl ether
ug/L
50
36.9
74
25-158
4-Nitrophenol
ug/L
250
63.0
25
1-132
Acenaphthene
ug/L
50
38.8
78
47-145
Acenaphthylene
ug/L
50
41.3
83
33-145
Anthracene
ug/L
50
41.9
84
1-166
Benzidine
ug/L
100
56.3
56
10-130
Benzo(a)anthracene
ug/L
50
44.2
88
33-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 36

aceAnalytical
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Project: GALVAN STORMWATER
Pace Project No.: 92474369
LABORATORY CONTROL SAMPLE: 2865413
Parameter
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)m ethane
bis(2-Chloroethyl) ether
bi s(2-Ethyl hexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Diethyl phthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
I ndeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylam ine
N-N itrosod imethylam i ne
N-Nitrosodiphenylamine
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
QUALITY CONTROL DATA
Spike
Cone.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
LCS
Result
44.3
44.2
39.9
46.4
41.8
44.2
48.9
51.1
43.2
45.7
48.1
40.6
46.3
44.5
42.2
40.5
20.3
40.1
21.3
22.2
40.3
43.3
42.8
33.8
41.8
40.5
55.1
41.9
25.2
48.5
LCS
% Rec
% Rec
Limits
89 17-163
88 24-159
80 1-219
93 11-162
84 33-184
88 12-158
98 8-158
102 1-152
86 17-168
91 1-118
96 4-146
81 1-227
93 1-114
89 1-112
84 26-137
81 59-121
41 24-116
80 1-152
43 25-150
44 40-113
81 1-171
87 21-196
86 1-230
68 25-150
84 25-150
81 35-180
55 14-176
84 54-120
50 5-112
97 52-115
81 10-137
76 15-120
51 10-120
85 10-120
46 10-120
115 11-131
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2865414
2865415
MS
MSD
92473907003 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
ND 50
50
34.6
35.9
69
72
44-142
4
1,2-Diphenylhydrazine
ug/L
ND 50
50
45.7
46.8
91
94
25-150
2
2,4,6-Trichlorophenol
ug/L
ND 50
50
21.0
17.6
42
35
37-144
18 M1
2,4-Dichlorophenol
ug/L
ND 50
50
26.7
25.3
53
51
1-191
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 27 of 36

aVIL; ytical
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2865414
MS
92473907003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2865415
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
2,4-Dimethylphenol
ug/L
ND
50
50
41.7
44.9
83
90
32-119
7
2,4-Dinitrophenol
ug/L
ND
250
250
113
93.1
45
37
1-181
20
2,4-Dinitrotoluene
ug/L
ND
50
50
54.5
56.5
109
113
39-139
4
2,6-Dinitrotoluene
ug/L
ND
50
50
50.9
54.7
102
109
50-158
7
2-Chloronaphthalene
ug/L
ND
50
50
41.0
44.5
82
89
60-118
8
2-Chlorophenol
ug/L
ND
50
50
27.8
26.4
56
53
23-134
5
2-Nitrophenol
ug/L
ND
50
50
29.8
27.0
60
54
29-182
10
3,3'-Dichlorobenzidine
ug/L
ND
100
100
100
101
100
101
1-262
0
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
55.4
45.2
55
45
1-181
20
4-Bromophenylphenyl ether
ug/L
ND
50
50
44.6
46.9
89
94
53-127
5
4-Chloro-3-methylphenol
ug/L
ND
100
100
82.8
88.3
83
88
22-147
6
4-Chlorophenylphenyl ether
ug/L
ND
50
50
41.5
45.0
83
90
25-158
8
4-Nitrophenol
ug/L
ND
250
250
49.7
41.4
20
17
1-132
18
Acenaphthene
ug/L
ND
50
50
44.1
47.1
88
94
47-145
7
Acenaphthylene
ug/L
ND
50
50
45.9
49.4
92
99
33-145
7
Anthracene
ug/L
ND
50
50
50.0
50.9
100
102
1-166
2
Benzidine
ug/L
ND
100
100
53.1
67.0
53
67
10-130
23
Benzo(a)anthracene
ug/L
ND
50
50
52.8
53.6
106
107
33-143
2
Benzo(a)pyrene
ug/L
ND
50
50
53.4
54.7
107
109
17-163
2
Benzo(b)fluoranthene
ug/L
ND
50
50
52.9
54.5
106
109
24-159
3
Benzo(g,h,i)perylene
ug/L
ND
50
50
56.2
53.7
112
107
1-219
4
Benzo(k)fluoranthene
ug/L
ND
50
50
53.2
54.4
106
109
11-162
2
bis(2-Chloroethoxy)methane
ug/L
ND
50
50
43.8
46.7
88
93
33-184
6
bis(2-Chloroethyl) ether
ug/L
ND
50
50
45.9
47.3
92
95
12-158
3
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
50
57.4
59.1
115
118
8-158
3
Butylbenzylphthalate
ug/L
ND
50
50
58.0
60.5
116
121
1-152
4
Chrysene
ug/L
ND
50
50
53.0
52.6
106
105
17-168
1
Di-n-butylphthalate
ug/L
ND
50
50
56.2
57.4
112
115
1-118
2
Di-n-octylphthalate
ug/L
ND
50
50
61.5
63.6
123
127
4-146
3
Dibenz(a,h)anthracene
ug/L
ND
50
50
55.2
54.3
110
109
1-227
2
Diethylphthalate
ug/L
ND
50
50
50.4
52.4
101
105
1-114
4
Dimethylphthalate
ug/L
ND
50
50
47.1
49.7
94
99
1-112
5
Fluoranthene
ug/L
ND
50
50
54.1
54.0
108
108
26-137
0
Fluorene
ug/L
ND
50
50
45.3
48.4
91
97
59-121
6
Hexachloro-1,3-butadiene
ug/L
ND
50
50
28.8
31.3
58
63
24-116
8
Hexachlorobenzene
ug/L
ND
50
50
46.1
47.7
92
95
1-152
3
Hexachlorocyclopentadiene
ug/L
ND
50
50
29.5
32.1
59
64
25-150
9
Hexachloroethane
ug/L
ND
50
50
31.5
34.4
63
69
40-113
9
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
55.2
54.5
110
109
1-171
1
Isophorone
ug/L
ND
50
50
44.7
48.1
89
96
21-196
7
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
41.7
45.5
83
91
1-230
9
N-Nitrosodimethylamine
ug/L
ND
50
50
34.0
37.1
68
74
25-150
9
N-Nitrosodiphenylamine
ug/L
ND
50
50
47.2
48.0
94
96
25-150
2
Nitrobenzene
ug/L
ND
50
50
43.6
45.7
87
91
35-180
5
Pentachlorophenol
ug/L
ND
100
100
42.8
34.7
43
35
14-176
21
Phenanthrene
ug/L
ND
50
50
49.6
49.9
99
100
54-120
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2865414
2865415
MS
MSD
92473907003 Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits RPD Clual
Phenol
ug/L
ND 50
50 19.3
20.0
39
40
5-112 4
Pyrene
ug/L
ND 50
50 51.6
52.6
103
105
52-115 2
2,4,6-Tribromophenol (S)
%
62
51
10-137
2-Fluorobiphenyl (S)
%
96
99
15-120
2-Fluorophenol(S)
%
34
29
10-120
Nitrobenzene-d5 (S)
%
101
106
10-120
Phenol-d6 (S)
%
38
39
10-120
Terphenyl-d 14 (S)
%
118
123
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 29 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537655 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92474369001, 92474369002, 92474369003
METHOD BLANK: 2867066 Matrix: Water
Associated Lab Samples: 92474369001, 92474369002, 92474369003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 04/22/20 17:37
LABORATORY CONTROL SAMPLE: 2867067
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 238 95 90-110
SAMPLE DUPLICATE: 2867370
92474187001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 106 122 14
SAMPLE DUPLICATE: 2867371
92474573001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 170 188 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN STORMWATER
Pace Project No.: 92474369
QC Batch: 537531 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92474369001
SAMPLE DUPLICATE: 2866472
92473345001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 4.3 4.3 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC.
Page 31 of 36

�OcIeAnalytical@
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: GALVAN STORMWATER
Pace Project No.: 92474369
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P5 The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
c3 Analysis of 2-chloroethyl vinyl ether was performed from a sample that was field preserved to pH < 2 with HCI. Acid
preservation is not allowed for this parameter by the test method or for NPDES compliance per 40CFR Part 136.
REPORT OF LABORATORY ANALYSIS
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Date: 04/30/2020 09:43 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 36

ncAnalytieal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: GALVAN STORMWATER
Pace Project No.: 92474369
Lab ID
Sample ID
QC Batch Method
QC Batch
92474369001
OF #1
EPA1664B
537644
92474369001
OF #1
EPA 608.3
537262
92474369001
OF #1
EPA 200.7 Rev 4.4 1994
537474
92474369002
OF #5
EPA 200.7 Rev 4.4 1994
537474
92474369003
TOH-1
EPA 200.7 Rev 4.4 1994
537474
92474369001
OF #1
EPA 625.1
537258
92474369001
OF #1
EPA 624.1
537934
92474369001
OF #1
SM 254OD-2011
537655
92474369002
OF #5
SM 254OD-2011
537655
92474369003
TOH-1
SM 2540D-2011
537655
92474369001
OF #1
EPA 9040C
537531
Date: 04/30/2020 09:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Analytical Method Batch
EPA 608.3
537751
EPA 200.7 Rev 4.4 1994
537482
EPA 200.7 Rev 4.4 1994
537482
EPA 200.7 Rev 4.4 1994
537482
EPA 625.1
537343
Page 33 of 36

Document Name:
Document Revised: February 7, 2018
m
aCBAnalytical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville P"I' Raleigh❑ Mechanicsville❑
Client Name
° 1A D Project I
Courier: ❑Fed Ex ❑UPS OUSPS ❑ lient 1111111❑ IIIII
I 1111111
Commercial ❑Pace ❑Other:
92414389
�
Custody Seal Present? []Yes 2 o Seals intact? ❑Yes IN {
DateJlnitlais Person Examining Contents: � —~�U "`�}^rt /f f a
Packing Material: ❑Bubble Wrap Q6ubbie Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: Type of Ice: [wet ❑Blue ❑None ❑Yes []NoC N'/A
❑IR Gun ID: 92TO61
1
Cooler Temp ('C): 5•� �'g Correction Factor: Add/Subtract ('C) +0.1
�( Temp should be above freezing to VC
Cooler Temp Corrected ('C): ,�'i 1 ❑Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (�/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
1-1v_- 17-1— inrL.dinoNawalland PuertoRico)?rlYes I—INo
Comments/Discre ancy:
Chain of Custody Present?
©Yes
ONO
N/A
1.
Samples Arrived within Hold Time?
QYes
N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
,,No
Cg svo
N/A
3.
Rush Turn Around Time Requested?
®Yes
No
[]N/A
4.
Sufficient Volume?
BY —es
[]No
N/A
S.
Correct Containers Used?
-Pace Containers Used?
` Yes
(]+es
QNo
QNo
❑NJA
❑N/A
6.
Containers Intact?
> Yes
No
(]N/A
7.
Dissolved analysis: Samples Field Filtered?
®Yes
❑No
N/A
8.
-includes Date/Time/ID/Analysis Matrix:
Y s
ONg
N A
%
Heads ate in VOA Vials (>5.6mm)?
OYes
[? No
ONJA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
QYes
QYes
136o
No
❑N/A
®N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Field Data Required? Oyes ❑No
Page 34 of 36

Document Name:
Document Revised: February 7, 2018
m
CeAnd�j dal
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project #
ISM: KLH1 Due Date: 04/27/20
CLIENT: 92-NDR
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pH Adjustment Lag for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le,
Out of hold, Incorrect preservative, out of temp, incorrect containers.
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