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HomeMy WebLinkAboutNC0062855_NPDES Permit Renewal/App_20051013Michael F. Easley, Govemor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources October 13, 2005 ' Mr. James Britt Town Manager Town of Robbins PO Box 296 Robbins, NC 27325 Alan W. Klimek, P.E. Director Division of Water Quality OCT 14 2005 • 1 RE-3.11 ';: Subject: Receipt of permit renewal application NPDES Permit NC0062855 Town of Robbins WWTP Moore County Dear Mr. Britt: The NPDES Unit received your permit renewal application on October 13, 2005. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. The requirements in your existing permit will remain in effect until the permit is renewed (or the Division takes other action). If you have any additional questions concerning renewal of the subject permit, please contact me at (919) 733-5083, extension 520. Sincerely, Frances Candelaria Point Source Branch cc: CENTRAL FILES `Fayetteville Regional Office/Surface Water Protection NPDES Unit NorthCarolina Naturally North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 733-7015 Customer Service Internet: h2o.enr.state.nc.us 512 N. Salisbury St. Raleigh, NC 27604 FAX (919) 733-2496 1-877-623-6748 An Equal Opportunity/Affirmative Action Employer-50% Recycled/10% Post Consumer Paper Mayor Mickey R. Brown Commissioners: Theron K. Bell Anna C. Derr Carlton G. Kennedy Charles (Buddy) Robinson Mary S. Wood, Mayor Pro Tem October 10, 2005 TOWN OF RO.BBINS PO Box 296 Robbins, NC 27325 (910) 948-2431 Fax: (910) 948-3981 Mr. Charles H. Weaver, Jr. NC DENRNVater Quality/Point Source Branch. 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Town of Robbins WWTP NPDES Permit No. NC0062855 James R. Britt, Jr. Administrator Debra T. Cockman, CMC Clerk/Finance Officer Daniel L. Brown Chief of Police I1.\) OCT 1 3 2005 - Y POU 1 SOU,,CE E; \ iCl Dear Ms. Stephens, Enclosed for your review is. the NPDES Permit renewal package for the Robbins Wastewater treatment plant. Our existing permit expires on March 31, 2006. We are requesting the Division to renew our NPDES Permit. If you have any questions concerning the information provided, please feel free to give me a call. Sincerely, T•wn of Robbins j J•'mes Britt Town Manager Cc: Brant Sikes Gary Stainback FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 FORM 2A NPDES APPLICATION OVERVIEW PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet Is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow z 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to 1mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRA/CERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or c. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). ,ALL APPLICANTS. T QQ114P EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 1 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: I RIVER BASIN: Renewal Cape Fear fiNgPROVAVI All treatment works must complete questions A.1 through A.B of this Basic Application Information Packet. A.1. Facility Information. Facility Name Mailing Address Contact Person Title Telephone Number Facility Address (not P.O. Box) Robbins WWTP PO Box 1085 Robbins, NC 27325 Brant Sikes ORC ( 910 )948-3063 256 Sewer Plant Road Robbins, NC 27325 A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Town of Robbins Mailing Address PO Box 296 Contact Person Title Telephone Number Robbins, NC 27325 James Britt Town Manager (910) 948-2431 Is the applicant the owner or operator (or both) of the treatment works? ® owner ❑ operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. ❑ facility ® applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -Issued permits). NPDES UIC RCRA NC0062855 PSD Other Other A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each, entity and, if known, provide Information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Robbins Population Served Type of Collection System Ownership 1,122 Sanitary Robbins Total population served 1,122 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 2 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NCOO62855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear A.S. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes ® No b. Does the treatment works discharge to a receiving water that is either In Indian Country or that is upstream from (and eventually flows through) Indian Country? ❑ Yes ® No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of "this year" occurring no more than three months prior to thls application submittal. a. Design flow rate 1.3 mgd Two Years Ago Last Year b. Annual average daily flow rate 0.249 0.233 This Year 0.278 (Jan -Aug) c. Maximum daily flow rate 1.150 0.705 1.116 (Jan -Aug) A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. ® Separate sanitary sewer ❑ Combined storm and sanitary sewer A.B. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? 0 Yes 0 No 0/0 If yes, list how many of each of the following types of discharge points the treatment works uses: 1. Discharges of treated effluent ii. Discharges of untreated or partially treated effluent 1 0 iii. Combined sewer overflow points 0 iv. Constructed emergency overflows (prior to the headworks) 0 v. Other 0 b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? 0 Yes If yes, provide the following for each surface impoundment: Location: NA ® No Annual average daily volume discharge to surface impoundment(s) mgd Is discharge 0 continuous or ❑ intermittent? c. Does the treatment works land -apply treated wastewater? 0 Yes ® No If yes, provide the following for each land application site: Location: Number of acres: Annual average daily volume applied to site: mgd Is land application ❑ continuous or 0 intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? 0 Yes ® No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 3 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NCOO62855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). NA If transport is by a party other than the applicant, provide: Transporter Name Mailing Address Contact Person Title Telephone Number J ) For each treatment works that receives this discharge provide the following: Name Mailing Address Contact Person Title Telephone Number ( ) If known, provide the NPDES permit number of the treatment works that receives this discharge Provide the average daily flow rate from the treatment works into the receiving facility. mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not included in A.B. through A.8.d above (e.g., underground percolation, well injection): ❑ Yes to No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: Is disposal through this method 0 continuous or ❑ intermittent? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 4 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not Include Information on combined sewer overflows in this section. If you answered "No" to question A.B.A, go to Part B. "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number 001 b. Location Robbins 27325 (City or town, if applicable) (Zip Code) Moore NC (County) " (State) 23°25'45 79°33'12 (Latitude) (Longitude) c. Distance from shore (if applicable) NA ft. d. Depth below surface (if applicable) NA ft. e. Average daily flow rate 0.278 mgd f. Does this outfall have either an intermittent or a periodic discharge? 0 Yes ® No . (go to A.9.g.) If yes, provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: mgd Months in which discharge occurs: g. Is outfall equipped with a diffuser? ® Yes 0 No A.10. Description of Receiving Waters. a. Name of receiving water Deep River b. Name of watershed (if known) NA United States Soil Conservation Service 14-digit watershed code (if known): c. Name of State Management/River Basin (if known): Cape Fear United States Geological Survey 8-digit hydrologic cataloging unit code (if known): d. Critical low flow of receiving stream (if applicable) acute NA cfs NA NA chronic NA cfs e. Total hardness of receiving stream at critical low flow (if applicable): NA mg/I of CaCO3 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 5 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. ❑ Primary ® Secondary ❑ Advanced 0 Other. Describe: b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 98 Design SS removal 97 Design P removal NA Design N removal NA % Other % c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe: Gas Chlorine If disinfection is by chlorination is dechlorination used for this outfall? ® Yes ■ No Does the treatment plant have post aeration? ® Yes 0 No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the Indicated effluent testing required by the permitting authority for each outfall through which effluent Is discharged. Do not Include Information on combined sewer overflows in this section. All Information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number. 001 PARAMETER MAXIMUM DAILY VALUE AVERAGE DAILY VALUE . . Value Units Value Units . -Number of Samples pH (Minimum) 6.1 s.u. pH (Maximum) 7.4 s.u. • ���%jy Flow Rate 1.116 MGD 0.278 MGD 243 Temperature (Winter) 15.0 °C 11.9 °C 90 Temperature (Summer) 30.0 °C 23 °C 153 • For pH please report a minimum and a maximum daily value POLLUTANT MAXIMUM'DAILY . DISCHARGE AVERAGE DAILY DISCHARGE /►NALYTICAL MUMDL Gone. Units Conc. Units Number of Samples METHOD .. CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN BOD5 23 Mg/I 2.3 Mg/I 90 EPA405.1 2.0 DEMAND (Report one) CBOD5 FECAL COLIFORM 700 #/100m1 13.6 #/100m1 90 ' SM9222D 1.0 TOTAL SUSPENDED SOLIDS (TSS) 14.2 M9/I 4.9 M9/I 90 EPA160 2 1.0 PART R TQ H - P .41E CATION QVERVIEWN (PAG�aE '1V TQ WVRA IIN ►HJ. H • TH : QF.FQ ,M2AYQUYMU$TT :,:..::.:;: EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 6 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear "1!t t - tQ , O eal o ,wpet All applicants with a design flow rate 2 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification). B.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. NA gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) SEE ATTACHED a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalis from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within Y. mile of the property boundaries of the treatment works, and 2) listed In public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. 8.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechiorinatlon). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. SEE ATTACHED B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ® Yes ❑ No If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). Name: Mailing Address: United Water Hydro Management PO Box 1279 Clemmons, NC 27012 Telephone Number: (3361766-0270 Responsibilities of Contractor: Operation and Maintenance Management of the WWTP B.5. Scheduled Improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned In question A.9) for each outfall that is covered by this implementation schedule. NA b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. ❑ Yes ❑ No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-8 & 7550-22. Page 7 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP,. NC0062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear c. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). NA d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable. For improvements planned independently of local, State, or Federal agencies, Indicate planned or actual completion dates, as applicable. Indicate dates as accurately as possible. Schedule Actual Completion Implementation Stage NA MM/DD/YYYY MM/DD/YYYY - Begin Construction / / / / - End Construction / / / / - Begin Discharge / / / / - Attain Operational Level / / / / e. Have appropriate permits/clearances conceming other Federal/State requirements been obtained? ❑ Yes 0 No • Describe briefly: NA B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the Indicated effluent testing required by the permitting authority for each outfall through which effluent Is discharged. Do not Include information on combine sewer overflows In this section. All Information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on -half years old. Outfall Number: 001 SEE ATTACHED POLLUTANT` MAXIMUM DAILY DISCHARGE AVERAGE 'DAILY DISCHARGE ANALYTICAL. • Conc. Units Conc. -Units .. Number of Samples METHOD. MLIMRL CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) CHLORINE (TOTAL RESIDUAL, TRC) DISSOLVED OXYGEN TOTAL KJELDAHL NITROGEN (TKN) NITRATE PLUS NITRITE NITROGEN ' OIL and GREASE PHOSPHORUS (Total) TOTAL DISSOLVED SOLIDS (TDS) OTHER �/,},^ ��1Rw e A A /R}' ►�)ff 1�1R�^,t�eF-,R�1AH�.'T'i � ���fla1- CH........I +�A' ' ^ '41 Ti 1M' 11RRVI a '� ``P'� 4t,Ayry�� E 1 [� 4�k1ETER��t ' f.. ' .r EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 8 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: .Renewal RIVER BASIN: Cape Fear x.n.•.,%..+ ,'..gym u••- i'c� -Y �•'t- -s�+C y�1 ,tl..y� tigl ySWi�.a14� . sc.N t r.'.r W r�F 7tf'$itF f717, •l ' -Y. LP'T+b'FTra'i�`-L--wer'l .,1 ..:.. .icL4' �4i.'�ICL.Y a '�,„ 3'- Bta, l•Otr !!T±!!!!!! bS 1 'j..,- x^.wY 1 .i. PAR,�•y .. .. .. ... .. -. .. .... _.. ., a �•- f i All applicants must complete the Certification Section. Refer to instructions to determine who Is an officer for the purposes of thls certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application Is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Information packet: ® Part D (Expanded Effluent Testing Data) ® Part E (Toxicity Testing: Biomonitoring Data) ® Part F (Industrial User Discharges and RCRA/CERCLA Wastes) ❑ Part G (Combined Sewer Systems) .R 1 7�5,?MUS'V-G�DIVINE 'i* 'M A? -40.11 iiG CEltilFl ATIQN; : ; I certify under penalty of law that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the Information, the information Is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title. James Britt, Town Manager Signature Telephone number (910) 948-2431 Date signed Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 EPA Fomi 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. - Page 9 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: Renewali RIVER BASIN: Fear • n 1'LaCape +_ti I� i {r.4 t1.7-.hR rt� k{ Fs a%t-,r. , 41,..-a �S*Er, tp<rfW-3 rlzII.-t �F.., 4`N�o_a. .a Y,-%:,,�7i"o4, -� ? r'f• p,,. �1 •"�{�; TpQ;�(�� /fir I D V �5 t 'A'4(M31F1�36�►k=? L Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or Is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing Information and any other Information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this foram. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number: 001 SEE ATTACHED (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE • AVERAGE DAILY DISCHARGE POLLUTANT Conc. Units Mass Units . Conc. Units. Mass .. Units Number of Samples ANAL.YTICAL . METHOD MLIMDL METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY ARSENIC BERYLLIUM CADMIUM CHROMIUM COPPER LEAD MERCURY NICKEL SELENIUM SILVER THALLIUM ZINC CYANIDE TOTAL PHENOLIC COMPOUNDS HARDNESS (as CaCO3) Use this space (or a separate sheet) to provide information on other metals requested by the permit writer EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 10 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Outfall number: (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM 41AIt,Y'pIScHARGE . done: Wilts Mass Units Cork. AVERAGE DAILY DISCHARGE Units Mass Wits, Number. :Of Samples ANALYTICAL. ;IIBE7'I•L�Ip:: MIJMpt: VOLATILE ORGANIC COMPOUNDS ACROLEIN ACRYLONITRILE BENZENE BROMOFORM CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMO- METHANE - CHLOROETHANE • 2-CHLOROETHYLVINYL ETHER CHLOROFORM DICHLOROBROMO- METHANE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE TRANS-1,2-DICHLORO- ETHYLENE 1,1-DICHLORO- ETHYLENE 1,2-DICHLOROPROPANE 1,3-DICHLORO- PROPYLENE ETHYLBENZENE METHYL BROMIDE METHYL CHLORIDE METHYLENE CHLORIDE 1,1,2,2-TETRA- CHLOROETHANE TETRACHLORO- ETHYLENE TOLUENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 11 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: 00811 number. (Complete once for each outfali discharging effluent to waters of the United States.) MAXIMUM°DAII;Y DISCHARGE AVERAGE DAILY DISCHARG P 4L-UT,ANT Cana,. Units Mass : Units Conc. Unite Mass Units ~ Number' :; of Samplae ..... ANAit: f ROAL METH . . • '...:..,: <' 1044441:11; • 1,1,1- TRICHLOROETHANE 1,1,2- TRICHLOROETHANE TRICHLOROETHYLENE VINYL CHLORIDE Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL 2-CHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL 4,6-DINITRO-O-CRESOL 2,4-DINITROPHENOL 2-NITROPHENOL . 4-NITROPHENOL PENTACHLOROPHENOL PHENOL 2 4,6 TRICHLOROPHENOL Use this space (or a separate sheet) to provide information on other acid -extractable compounds reques ed by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE ACENAPHTHYLENE ANTHRACENE BENZIDINE BENZO(A)ANTHRACENE BENZO(A)PYRENE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 12of22 FACIUTY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Outfall number: (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAIL*. DISCHARGE L/M MOL. CQnc: -Units Mass "Units Cone, Units' Maas Units Number 0METMOP Samples . AN� C -.. . 3,4 BENZO- FLUORANTHENE BENZO(GHI)PERYLENE BENZO(K) FLUORANTHENE BIS (2-CHLOROETHOXY) METHANE BIS (2-CHLOROETHYL)- ETHER BIS (2-CHLOROISO- PROPYL) ETHER BIS (2-ETHYLHEXYL) PHTHALATE 4-BROMOPHENYL PHENYL ETHER BUTYL BENZYL. PHTHALATE 2-CHLORO- NAPHTHALENE 4-CHLORPHENYL PHENYL ETHER CHRYSENE DI-N-BUTYL PHTHALATE DI-N-OCTYL PHTHALATE DIBENZO(A,H) ANTHRACENE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 3,3-DICHLORO- BENZIDINE DIETHYL PHTHALATE DIMETHYL PHTHALATE 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE 1,2-DIPHENYL- HYDRAZINE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 13 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Outfall number. (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT Conc. Units Mass Units Conc, Units • Mass' Unite Number ,. of Samples. ANALYTIC AI";' METHRD M L/MDL FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLORO- BUTADIENE HEXACHLOROCYCLO- PENTADIENE HEXACHLOROETHANE INDENO(1,2,3-CD) PYRENE ISOPHORONE NAPHTHALENE NITROBENZENE N-NITROSODI-N- PROPYLAMINE N-NITROSODI- METHYLAMINE N-NITROSODI- PHENYLAMINE i PHENANTHRENE PYRENE 1,2,4- TRICHLOROBENZENE Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides) requested by the permit writer 3�} �r s, EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-8 & 7550-22. Page 14 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC 0062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear 4“-,v3R,::P7-1-v5ivgit'l ,.. - ' ..itri.'!:',..,.. , FINI:;,',KYFV0,,,:Kf:. ,,:-.zvv-,,:7:t.r.v,->--• • , — , :,.,-ey' r - ,-t-2,v, , - -',.....'-',:ka&....,-,i,:d.:::-?,,,!:•,-;-, ,,,Z2f4I,^,i..t',-,:i.,:. , 7,,,,,, , ; ,rorn, ,vv, • , ,... ,:. ARr, 'iTQ�QV1W, SONOPMA, : ,.. POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows In this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question E.4 for previously submitted information. If EPA methods were not used, report the reasons for using altemate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. 23 chronic 0 acute SEE ATTACHED E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. Test number: Test number Test number a. Test information. Test Species & test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechiorination EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-8 & 7550-22. Page 15 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, N00062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear Test number: Test number: Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected: f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source. Laboratory water Receiving water i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water ` Salt water j. Give the percentage effluent used for all concentrations in the test series. k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100% effluent LC50 95% C.I. % % Control percent survival % % % Other (describe) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 16 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, N00062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear Chronic: NOEC % % % IC25 % % % Control percent survival % % % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run (MM/DD/YYYY)? / / / / / / Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Tox city Reduction Evaluation? ❑ Yes ® No If yes, describe: E.4. Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. / Date submitted: NA/ / (MM/DD/YYYY) Summary of results: (see instructions) ,y; ���j A H��ww _�^r 1I /�w��� 5 yry'� .1 .. ✓ IO F PAR - . � 1 liR~-�C-� }"a!!!' ,,: '�Sf TMIOJ II �}O"Ri P fIe n�1'tF�Ayry� � 'T RGU VII� • QMPLE y��(� L R it f /�.}W �7�/ ��F .' •Ir.}. .' EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 17 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Cape Fear asPHARG -WA All treatment works receiving discharges from significant Industrial users or which receive RCRA,CERCIA, or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (Gills). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. 1 b. Number of ClUs. SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following Information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. - F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Candor Hosiery Mailing Address: PO Box 249 Robbins, NC 27325 F.4. Industrial Processes. Describe all the Industrial processes that affect or contribute to the SIU's discharge. Peroxide bleaching of socks F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Raw material(s): F.6. Flow Rate. Athletic and fashion socks Hydrogen Peroxide a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 0.0400 gpd ( X continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged Into the collection system in gallons per day (gpd) and whether the discharge Is continuous or intermittent. gpd continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU Is subject to the following: a. . Local limits b. Categorical pretreatment standards ® Yes ❑ Yes ❑ No ❑ No If subject to categorical pretreatment standards, which category and subcategory? EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-8 & 7550-22. Page 18 of 22 FACILITY NAME AND PERMIT NUMBER: Robbins WWTP, NC0062855 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Cape Fear. F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? ❑ Yes ® No (go to F.12) F.10. Waste transport. Method by which RCRA waste is received (check all that apply): ❑ Truck 0 Rail 0 Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number Amount Units ( CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remedlation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ❑ Yes (complete F.13 through F.15.) ® No F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the next five years). NA F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) NA F.15. Waste Treatment. a. Is this waste treated (or will be treated) prior to entering the treatment works? ® Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): Aeration b. Is the discharge (or will the discharge be) continuous or intermittent? ® Continuous ❑ Intermittent If intermittent, describe discharge schedule. R ;_ ), Ai PLICATI �??11 l Illils� t I or . ► ► EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 19 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: age slams; 4;4 dS,:z��va �yiF,q? If the treatment works has a combinedsewer system, complete Part G. G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and outstanding natural resource waters). c. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or on a separate drawing, of the combined sewer collection system that includes the following information. a. Location of major sewer trunk lines, both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed Into the combined sewer system. c. Locations of in -line and off-line storage structures. d. Locations of flow -regulating devices. e. Locations of pump stations. CSO OUTFALLS: Complete questions G.3 through G.6 once for each CSO discharge point. G.3. Description of Outfall. a. Outfall number b. Location (City or town, if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) c. Distance from shore (if applicable) d. Depth below surface (if applicable) e. Which of the following were monitored during the last year for this CSO? 0 Rainfall ft. ft. ❑ CSO pollutant concentrations ❑ CSO frequency ❑ CSO flow volume ❑ Receiving water quality f. How many storm events were monitored during the last year? G.4. CSO Events. a Give the number of CSO events in the last year. events (❑ actual or 0 approx.) b. Give the average duration per CSO event. hours (0 actual or 0 approx.) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 20 of 22 FACILITY NAME AND PERMIT NUMBER: , PERMIT ACTION REQUESTED: RIVER BASIN: G.5. G.6. c. Give the average volume per CSO event. million gallons (0 actual or 0 approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall Description of Receiving Waters. a. Name of receiving water: b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code (if c. Name of State Management/River Basin: known): United States Geological Survey 8-digit hydrologic cataloging unit CSO Operations. Describe any known water quality impacts on the receiving water caused intermittent shell fish bed closings, fish kills, fish advisories, other recreational code (if known): by this CSO (e.g., permanent or intermittent beach closings, permanent or Toss, or violation of any applicable State water quality standard). .:' (w,�y�}.��.•��j �/p�)U -' {RR��'4n�'^lytp^''�S ��"(/g�� y'-''i• j J- 7'' TO� �`'Y'!F"i � 'i[f A?lEMil ��?c�� d ro et �E1�q+fit�+'AN.X �yty�i`E 7 1 1 d% ! �r� ii ,0) i fL �1'1 1 ( G 1 yy 4^ , „ �1163_�s►01+_�"y�R�'Ala 4 �� 8 ) t""1RR' / EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 21 of 22 Additional information, if provided, will appear on the following pages. NPDES FORM 2A Additional Information ' , Facility Information Latitude: Longitude: Quad #: Stream Class: Receiving Stream: Permitted Flow: ``J--.>- . .�` 1/ Ef 1 I•. •1 __J " J r 35°25'45" Sub -Basin: 03-06-10 79°33' 12" F2ONE C-HQW Deep River 1.3 MGD ._,(-7-- 7 --i(?)--) ...' ifs% )1(7:::-J-/ - - Robbins WWTP NC0062855 Moore Comity ROBBINS WASTEWATER TREATMENT PLANT Control Building Fine Screen & Inf Sampling Splitter Box Return Sludge Sand Drying Beds (Abandoned) Effluent toDeep River , in / • RAS Telescopic Ives ♦� Waste Sludge Digester v RAS & Sludge Loading Pump Station _ _ +Sludge to Land Application Sites Permit No. NC0062855 Outfall 001 Annual Monitoring and Pollutant ScrM Month January Year 2005 Facility Name Robbins WWTP Date of sampling January 13, 2005 Analytical Laboratory Tritest ORC Brant Sikes Phone 910-948-3063 Parameter Sample Type Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Ammonia (as N) Composite 350.1 0.02 0.11 MG/L 1 Dissolved oxygen Composite 4500 G 0.1 9.7 MG/L 1 Nitrate/Nitrite Composite 353.2 0.02 12.4 MG/L 1 Total Kjeldahl nitrogen Composite 351.2 0.25 1.41 MG/L 1 Total Phosphorus Composite 365.4 0.05 0.13 MG/L 1 Total dissolved solids Composite * Hardness Composite CALC N/A 47.1 MG/L 1 Chlorine (total residual, TRC) Grab SM4500G 10-May 2.6 UG/L 1 Oil and grease Grab 1664A 5 5.0 MG/L 1 Metals (total recoverable), cyanide and total phenols Antimony Composite 200.8 0.003 0.003 MG/L 1 Arsenic Composite 200.8 0.005 0.005 . MG/L 1 Beryllium Composite 200.8 0.002 0.002 MG/L 1 Cadmium Composite 200.8 0.005 0.005 MG/L 1 Chromium Composite 200.8 0.01 0.010 MG/L 1 Copper Composite 200.8 0.01 0.054 MG/L 1 Lead Composite 200.8 0.005 0.005 MG/L 1 Mercury Composite 245.1 0.2 . 0.2 UG/L 1 Nickel Composite 200.8 0.01 0.010 MG/L 1 Selenium Composite. 200.8 0.002 0.002 MG/L 1 Silver Composite 200.8. 0.01 0.010 MG/L 1 Thallium Composite 200.8 0.001 0.001 MG/L 1 Zinc Composite 200.8 0.01 0.046 MG/L .1 Cyanide Grab 335.2 0.005 0.005 .MG/L 1 Total phenolic compounds Grab 510A/B 0.005 0.005 MG/L 1 Volatile organic compounds Acrolein Grab * • Acrylonitrile Grab Benzene Grab * Bromoform .. Grab * Carbon tetrachloride. Grab * Chlorobenzene Grab * Chlorodibromomethane Grab * Chloroethane Grab * 2-chloroethylvinyl ether Grab * Chloroform Grab * • Dichlorobromomethane Grab * 1,1-dichloroethane Grab * 1,2-dichloroethane Grab * Trans-1,2-dichloroethylene Grab * Form - DMR- PPA-1 Page 1 Permit No. NC0062855 Outfall 001 Annual Monitoring and Pollutant St Month January Sample Analytical Quantitation Sample Units of Number of Parameter Type Method Level Result Measurement samples e organic compounds (Cont. 1,1-dichloroethylene Grab 1,2-dichloropropane Grab * 1,3-dichloropropylene Grab * Ethylbenzene Grab * Methyl bromide Grab * Methyl chloride Grab * Methylene chloride Grab * 1,1,2,2-tetrachloroethane Grab * Tetrachloroethylene Grab * Toluene Grab * 1,1,1-trichloroethane Grab * 1,1,2-trichloroethane Grab * Trichloroethylene Grab * Vinyl chloride Grab * Acid -extractable compounds P-chloro-m-creso 2-chlorophenol 2,4-dichlorophenol 2,4-dimethylphenol 4,6-dinitro-o-cresol 2,4-dinitrophenol 2-nitrophenol 4-nitrophenol Grab Grab Grab Grab Grab Grab Grab Grab 625 625 625 625 625 625 625 625 10 10 10 10 50 50 10 10 10 10 10 10 50 50 10 10 UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L Pentachlorophenol Grab 625 30 30 UG/L Phenol Grab 625 10 10 UG/L 2,4,6-trichlorophenol Grab 625 10 10 UG/L 1 1 1 1 1 1 1 1 1 1 1 Base -neutral compounds Acenaphthene Grab 625 10 10 UG/L Acenaphthylene Grab 625 10 10 UG/L Anthracene Grab 625 10 10 UG/L Benzidine Grab 625 10 50 UG/L Benzo(a)anthracene Grab 625 10 10 UG/L Benzo(a)pyrene Grab 625 10 10 UG/L 3,4 benzofluoranthene Grab 625 10 10 UG/L Benzo(ghi)perylene Grab 625 10 10 UG/L Benzo(k)fluoranthene Grab 625 10 10 UG/L Bis (2-chloroethoxy) methane Grab 625 10 10 UG/L Bis (2-chloroethyl) ether Grab 625 10 10 UG/L Bis (2-chloroisopropyl) ether Grab 625 10 10 UG/L Bis (2-ethylhexyl) phthalate Grab 625 10 10.9 UG/L 4-bromophenyl phenyl ether Grab 625 10 10 UG/L Butyl benzyl phthalate Grab 625 10 10 UG/L 2-chloronaphthalene Grab 625 10 10 UG/L 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Form - DMR- PPA-1 Page 2 Permit No. NC0062855 Outfall 001 Annual Monitoring and Pollutant' Sr Month January 4-chlorophenyl phenyl ether Grab 625 10 10 UG/L 1 Parameter Sample Type Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Base -neutral compounds (cont.) Chrysene Grab 625 10 10 UG/L 1 Di-n-butyl phthalate Grab 625 10 . 10 UG/L 1 Di-n-octyl phthalate Grab 625 10 .10 UG/L • 1 Dibenzo(a,h)anthracene Grab 625 10 10 _ UG/L 1 1,2-dichlorobenzene Grab 625 10 10 UG/L 1 1,3-dichlorobenzene Grab 625 10 10 UG/L 1 1,4-dichlorobenzene Grab 625. 10 10 UG/L 1 3,3-dichlorobenzidine Grab 625 20 20 UG/L 1 Diethyl phthalate Grab 625 10 10 UG/L 1 Dimethyl phthalate Grab 625 10 10 UG/L 1 2,4-dinitrotoluene Grab . 625 10 10 UG/L 1 2,6-dinitrotoluene Grab 625 10 10 UG/L . 1 1,2-diphenylhydrazine Grab 625 - 10 10 UG/L 1 Fluoranthene Grab 625 10 10 UG/L 1 Fluorene Grab. 625 10 10 UG/L . 1 Hexachlorobenzene Grab 625 10 10 UG/L 1 Hexachlorobutadiene Grab 625 10 10 UG/L 1 Hexachlorocyclo-pentadiene Grab ' 625 10 10 . UG/L 1 Hexachloroethane. Grab 625 10 10 UG/L 1 Indeno(1,2,3-cd)pyrene Grab 625 10 10 UG/L 1 Isophorone Grab 625 . 10 _ 10 UG/L 1 Naphthalene Grab 625 10 10 UG/L 1 Nitrobenzene Grab 625 10 _ 10 UG/L 1 N-nitrosodi-n-propylamine Grab 625 20 20 UG/L 1 N-nitrosodimethylamine Grab 625 10 10 UG/L 1 N-nitrosodiphenylamine Grab .625 20 20 UG/L 1 Phenanthrene . Grab. 625 10 10 . UG/L 1 Pyrene Grab 625 10 10 - UG/L 1 1,2,4,-trichlorobenzene Grab 625 20 20 UG/L _ 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure thatqualified perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibel for gathering the information, the information submitted is , to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fmes and imprisonment for knowing violations. Gary Stainback i tur *The volatile organic compounds and total dissolved soli ;r• ere not analyzed due to head space in vials. Will resample. Form - DMR- PPA-1 Page 3 Permit No. NC0062855 Outfall 001 Annual Monitoring and Pollutant Sr 'n Month April Year 2005 Facility Name Robbins WWTP Date of sampling 04/27/05. Analytical Laboratory Tritest ORC Brant Sikes Phone 910-948-3063 Parameter Sample Type Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Ammonia (as N) Composite 350.1 0.02 0.04 MG/L 1 Dissolved oxygen Composite 4500 G 0.1 . 9.5 MG/L 1 Nitrate/Nitrite Composite 353.2 0.02 17.4 MG/L 1 Total Kjeldahl nitrogen .Composite 351.2- 0.25 0.94 MG/L 1 Total Phosphorus Composite 365.4 . 0.05 0.26 MG/L 1 Total dissolved solids Composite 160.1 10 430 Hardness Composite CALC . N/A 35.7 .. MG/L 1 Chlorine (total residual, TRC) ' Grab SM4500G 10 . 4 10 UG/L 1 Oil and grease Grab 1664A 5 < 5.0 MG/L 1 Metals (total recoverable), cyanide and total phenols Antimony Composite 200.8 0.003 < 0.003 .MG/L 1 Arsenic Composite 200.8 .0.005 Z. 0.005 MG/L 1 Beryllium Composite 200.8 0.002 . ( 0.002 MG/L . 1 Cadmium Composite 200.8 0.005 L 0.005 MG/L 1 Chromium Composite 200.8, . 0.01 , < 0.010 MG/L 1 Copper Composite 200.8 0.01 0.100 MG/L 1 Lead Composite 200.8 0:005 4 0.005 MG/L 1 Mercury Composite 1631 0.5 0.0025 UG/L 1 Nickel Composite 200.8 . 0.01 . 4 0.010 MG/L 1 Selenium Composite 200.8 0.002 < 0.002 MG/L 1 Silver Composite 200.8 0.01 C 0.010 ' . MG/L 1 Thallium Composite 200.8 0.001 4 0.001 MG/L 1 Zinc Composite 200.8 0.01 0.024 MG/L 1 Cyanide Grab 335.3 0.005.: 4 0.005 MG/L 1 Total phenolic compounds Grab 510A/B 0.005 < 0.005 MG/L 1 Volatile organic compounds Acrolein Grab 624 50 < 50 UG/L 1 Acrylonitrile Grab 624 50 < 50 UG/L. 1 Benzene ' Grab 624 5 ( 5 UG/L 1 Bromoform Grab 624. 5 < 5 UG/L 1 Carbon tetrachloride ' Grab 624 5 (. 5 UG/L 1 Chlorobenzene , Grab 624 5 < 5 UG/L 1 Chlorodibromomethane . ' Grab 624 5 < 5 UG/L 1 Chloroethane • . Grab 624 5 4. 5 UG/L 1 2-chloroethylvinyl ether Grab 624 10 ,4 10 UG/L 1 Chloroform Grab 624 5 19.3 UG/L 1 Dichlorobromomethane Grab 624 5 - 9.44 UG/L. 1 1,1-dichloroethane Grab 624 5 • . • E 5 UG/L 1 1,2-dichloroethane Grab . 624 5 { 5 UG/L 1 Trans-1,2-dichloroethylene Grab 624 5 < 5 UG/L 1 Form - DMR- PPA-1 Page 1 2-chloronaphthalene Grab 625 I Butyl benzyl phthalate Grab 4-bromophenyl phenyl ether Grab 625 I 0T I SZ9 quip alslsglgd (l agl&g;a-Z) s1Sl IBis (2-chloroisopropyl) ether Bis (2-chloroethyl) ether. Grab IBis (2-chloroethoxy) methane I Grab M IBenzo(ghi)perylene Grab 3,4 benzofluoranthene Grab I 625 IBenzo(a)pyrene IBenzidine I Grab Anthracene IAcenaphthylene Grab IAcenaphthene I Grab 0T SZ9 quip a uatlluBsonfl(3l)ozua£ Benzo(a)anthracene I Grab 625 Base -neutral compounds. N o 0 0 Ti Pentachlorophenol I Grab 4-nitrophenol I Grab I 625 I 10 2-nitrophenol I Grab 625 2,4-dinitrophenol I Grab 4,6-dinitro-o-cresol I Grab 2,4-dimethylphenol Grab I 625 0T I S69 gasp louagdosolg3 p-j,`Z I2-chlorophenol Grab P-chloro-m-creso I Grab I 625 I 10 Acid -extractable compounds Vinyl chloride I Grab 624 Trichloroethylene Grab 624 1,1,2-trichloroethane I Grab I 624 1,1,1-trichloroethane Toluene I Grab 624 l Tetrachloroethylene Grab 1,1,2,2-tetrachloroethane Methylene chloride I Grab Methyl chloride Grab Methyl bromide I Grab 624 Ethylbenzene Grab 1,3-dichloropropylene I Grab 1,2-dichloropropane Grab 1,1-dichloroethylene Volatile organic compounds (Cont.) O 0 h O' cr Q' Grab I 625 10 I 1 Q' Grab I 624 Grab 624 Grab 624 CA A b e 0T I SZ9 N CJI N CA N CJ1 0T SZ9 N CJI N CJ1 N CA N CJI N CJ1 625 10 I 625 I 30 I z 30 I UG/L UI CJI CN71 N -A N - N -A N . N - N -A CO St3 5. o 0.0 >n r r r r r r O r O r O F. O r O r O r O rO COJ O O r+O Cn Ul cn O Cn Cn U1 Cn O CJI CJI Cn CJ1 CJ1 Quantitation Sample Units of Number of Level Result Measurement samples AA r r ^AN r r r nA r r nn/•n O O r r c,nr.l•^ O O r O r C. 10 I UG/L I 10 UG/L n r < 10 - UG/L • 50 UG/L O • 10 UG/L r r n r rn Cn CJ1 AnnA"Annhnn^ Cr' r CA Cn C1t C1l O CFI Cn C 1 C I Cn C r UG/L I UG/L UG/L I C r UG/L- UG/L UG/L UG/L C r UG/L UG/L UG/L I C r C r 1 UG/L C r C r. C r C r C r UG/L 1 UG/L 1 UG/L 1 UG/L 1 UG/L 1 UG/L 1 C r C r UG/L I 1 UG/L 1 C r C r C r C r Permit No. NC0062855 Outfall 001 Annual Monitoring and Pollutant Sr an Month April 4-chlorophenyl phenyl ether Grab 625 10 < 10 UG/L -- lv Parameter Sample Type Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Base -neutral compounds (cont.) Chrysene Grab 625 10 < 10 UG/L 1 Di-n-butyl phthalate Grab 625 10 < 10 UG/L 1 Di-n-octyl phthalate Grab 625 10 ( 10 UG/L 1 Dibenzo(a,h)anthracene Grab 625 10 < 10 UG/L 1 1,2-dichlorobenzene Grab 625 10 4, 10 UG/L 1 1,3-dichlorobenzene Grab 625 10 < 10 UG/L 1 1,4-dichlorobenzene Grab 625 10 < 10 UG/L 1 3,3-dichlorobenzidine Grab 625 20 4 20 UG/L 1 Diethyl phthalate Grab 625 10 < 10 UG/L 1 Dimethyl phthalate Grab 625 10. < 10 UG/L 1 2,4-dinitrotoluene Grab 625 10 4 10 UG/L 1 2,6-dinitrotoluene . Grab 625 10 ( 10 UG/L 1 1,2-diphenylhydrazine Grab 625 10 < 10 UG/L 1 Fluoranthene Grab 625 10 4 10 UG/L 1 Fluorene Grab 625 10 C, 10 UG/L 1 Hexachlorobenzene . Grab 625 10 < 10 UG/L 1 Hexachlorobutadiene Grab 625 10 4 10 UG/L 1 Hexachlorocyclo-pentadiene Grab 625 10 < 10 UG/L 1 Hexachloroethane Grab . 625 10 < 10 UG/L 1 Indeno(1,2,3-cd)pyrene Grab 625 10 C., 10 UG/L 1 Isophorone Grab 625 10 < 10 UG/L 1 Naphthalene Grab 625 10 < 10 UG/L 1 Nitrobenzene Grab 625 10 L 10 UG/L 1 N-nitrosodi-n-propylamine Grab 625 20 < 20 UG/I: 1 N-nitrosodimethylamine Grab 625 10 4 10 UG/L 1 N-nitrosodiphenylamine Grab 625 20 es 20 UG/L 1 Phenanthrene Grab 625 10 < 10 UG/L 1 Pyrene • Grab 625 10 C 10 UG/L 1 1,2,4,-trichlorobenzene Grab 625 20 L 20 UG/L 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibel for gathering the information, the information submitted is , to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting falseinformation, including the possibility of fines and imprisonment for knowing violations. Form - DMR- PPA-1 Page 3 Permit No. NC0062855 Outfall 001 Annual Monitoring and Pollutant Scan Month July Year 2005 Facility Name Robbins WWTP Date of sampling 07/13/05 Analytical Laboratory Tritest ORC Brant Sikes Phone 910-948-3063 Parameter Sample Type Analytical Method Quantitation Level Sample Result Units of Measurement Number of samples Ammonia (as N) Composite 350.1 0.02 0.05 MG/L 1 Dissolved oxygen Composite 4500 G 0.1 7.9 MG/L 1 Nitrate/Nitrite Composite 353.2 0.02 18 MG/L 1 Total Kjeldahl nitrogen Composite 351.2 0.25 L 0.25 MG/L 1 Total Phosphorus Composite 365.4 0.05 0.45 MG/L 1 Total dissolved solids Composite 160.1. 10 393 Hardness Composite CALC N/A 50.3 MG/L 1 Chlorine (total residual, TRC) Grab SM4500G 10 < 10 UG/L 1 Oil and grease Grab" 1664A 5 4 5.0 MG/L 1 Metals (total recoverable), cyanide and total phenols Antimony Composite 200.8 0.003 < 0.003 MG/L 1 Arsenic Composite 200.8 . 0.005 ( 0.005 MG/L 1 Beryllium Composite 200.8 0.002 < 0.002 MG/L 1 Cadmium Composite 200.8 0.005 < 0.005 MG/L 1 Chromium : Composite 200.8 0.01 4 0.010 MG/L 1 Copper Composite 200.8 0.01 0.051 MG/L 1 Lead . Composite 200.8 0.005 4 0.005 MG/L 1 Mercury Composite 1631 0.5 0.00133 UG/L 1 Nickel Composite 200.8 0.01 4 0.010 MG/L " 1 Selenium Composite 200.8 0.002 C 0.002 MG/L 1 Silver Composite 200.8 0.01 ( 0.010 MG/L 1 Thallium Composite 200.8 0.001 < 0.001 MG/L 1 Zinc Composite 200.8 0.01 0.027 MG/L 1 Cyanide Grab 335.3 0.005 4. 0.005 MG/L 1 Total phenolic compounds Grab 510A/B 0.005 ( 0.005 MG/L 1 Volatile organic compounds . Acrolein Grab 624 50 C 50 UG/L 1 Acrylonitrile Grab 624 50 ( 50 UG/L 1 Benzene Grab 624 5 < 5 UG/L 1 Bromoform Grab 624 5 ( 5 'UG/L 1 Carbon tetrachloride Grab 624 5 < 5 UG/L 1 Chlorobenzene Grab 624 5 < 5 UG/L 1 Chlorodibromomethane Grab 624 5 < 5 UG/L 1 Chloroethane Grab 624 5 4. 5 UG/L 1 2-chloroethylvinyl ether Grab 624 10 G 10 UG/L 1 Chloroform Grab 624 5 39.3 UG/L 1 Dichlorobromomethane Grab 624 5 9.42 UG/L 1 1,1-dichloroethane Grab ' 624 5 G 5 UG/L 1 1,2-dichloroethane Grab 624 5 < 5 UG/L 1 Trans-1,2-dichloroethylene Grab 624 5 ( 5 UG/L 1 Form - DMR- PPA-1 Page 1 Annual Monitoring and Pollutant Scats Permit No.. NC0062855 Outfall 001 Month July Year 2005 Sample Analytical Quantitation Sample Units of Number of Parameter Type Method Level Result Measurement samples Volatile organic compounds (Cont.) 1,1-dichloroethylene Grab 624 5 4 5 UG/L 1,2-dichloropropane 1,3-dichloropropylene Ethylbenzene Grab Grab ,Grab 624 624 624 5 5 5 < 5 < 5 < 5 UG/L UG/L UG/L Methyl bromide Methyl chloride Methylene chloride 1,1,2,2-tetrachloroethane Grab Grab Grab Grab 624 624 624 624 5 10 5 5 < 5 C 10 < 5 < 5 UG/L UG/L UG/L UG/L Tetrachloroethylene Grab 624 5. < 5 UG/L 1 1 1 1 1 1 1 1 1 Toluene Grab 624 5 4 5 UG/L 1,1,1-trichloroethane Grab 624 10 < 10 UG/L 1,1,2-trichloroethane Grab 624. 5 < 5 UG/L. Trichloroethylene Vinyl chloride Grab Grab 624 624 5 5 < 5 G 5 UG/L UG/L 1 1 1 1 Acid -extractable compounds P-chloro-m-creso Grab 625 10 < 10 UG/L 2-chlorophenol Grab 625 10 • 10 UG/L 2,4-dichlorophenol 2,4-dimethylphenol 4,6-dinitro-o-cresol 2,4-dinitrophenol Grab Grab Grab Grab 625 625 625 625 10' 10 50 50 < 10- < 10 4 50 < 50 UG/L UG/L UG/L UG/L 2-nitrophenol Grab 625' 10 < _10 UG/L 4-nitrophenol Grab 625 10 < 10 UG/L Pentachlorophenol Phenol - Grab Grab 625 625 30. 10 < 30 G 10 UG/L UG/L 1 1 1 1 1 1 1 1 1 1 2,4,6-trichlorophenol Grab 625 10: < 10 UG/L Base -neutral compounds Acenaphthene Acenaphthylene Grab Grab 625 625 10 10 • 10 • 10 UG/L UG/L Anthracene Grab 625 10" <, 10 UG/L Benzidine Benzo(a)anthracene. Benzo(a)pyrene Grab' Grab Grab 625 625 625 10 10. 10 <•50 < 10 G 10 UG/L UG/L UG/L 3,4 benzofluoranthene Grab 625 10 10 UG/L Benzo(ghi)perylene Benzo(k)fluoranthene Bis (2-chloroethoxy) methane Grab Grab Grab 625 625 625 10 10 10 < 10 4, 10 < 10 UG/L UG/L UG/L Bis (2-chloroethyl) ether Grab 625 10 • 10 UG/L Bis (2-chloroisopropyl) ether Bis (2-ethylhexyl) phthalate Grab Grab 625 625 10 10 • 10 • 10 UG/L UG/L 4-bromophenyl phenyl ether Butylbenzyl phthalate 2-chloronaphthalene Grab Grab Grab 625 625 625 10 10 10 <, 10 ' 10 .10 UG/L UG/L UG/L 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Form - DMR- PPA-1 Page 2 3 Annual Monitoring and Pollutant Sca ti Permit No. NC0062855 Outfall 001 Month July Year 2005 4-chlorophenyl phenyl ether Grab 625 10 10 UG/L 1 Parameter Sample Type Analytical Method Quantitation Level Sample Result. Units of Measurement Number of samples Base -neutral compounds (cont.) Chrysene Di-n-butyl phthalate Grab. Grab 625 625 10 10 4 .10 < 10 UG/L UG/L Di-n-octyl phthalate Grab 625 10 4 10 UG/L 1 1 1 Dibenzo(a,h)anthracene Grab 625 10 • 10 UG/L 1,2-dichlorobenzene Grab. 625 10 < 10 UG/L 1,3-dichlorobenzene Grab 625 10 • 10 UG/L 1,4-dichlorobenzene Grab 625 .10 10 UG/L 3,3-dichlorobenzidine Diethyl phthalate Dimethyl phthalate 2,4-dinitrotoluene 2,6-dinitrotoluene Grab Grab Grab Grab Grab 625 625 625 625 625 20 10 10 10 10 < . 20 < 10 <,.10 < 10 ▪ 10 UG/L UG/L UG/L UG/L UG/L 1, 2-diphenylhydrazine Fluoranthene Grab Grab 625' 625 10 10 < 10 < 10 UG/L . UG/L Fluorene Hexachlorobenzene Grab Grab. 625 625 10 10 G 10 < 10 UG/L UG/L Hexachlorobutadiene Grab 625 10 4 10 UG/L Hexachlorocyclo-pentadiene Grab 625 10 < 10 UG/L Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Grab Grab Grab 625 625 625 10 10' 10 < 10 < 10 4 10 UG/L UG/L UG/L Naphthalene Nitrobenzene Grab • Grab 625 625 10 10 L -10 < 10 UG/L UG/L N-nitrosodi-n-propylamine Grab 625 20 G 20 UG/L N-nitrosodimethylamine Grab 625 10 • 10 UG/L N-nitrosodiphenylamine Phenanthrene Grab Grab 625 625 20, 10 < 20 G 10 UG/L UG/L Pyrene Grab 625 10 < 10 UG/L 1,2,4,-trichlorobenzene Grab 625 20 [. 20 UG/L 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 - 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified 'perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibel for gathering the information, the information submitted is , to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Form - DMR- PPA-1 Page 3 Erionmental Testing Solutions,: jc. PO Box 7565 Asheville,NC 28802 Phone: (828) 350-9364 Fax: (828) 350-.9368 E-mail: JimSlmner@aol:com Date: January 24, 2005 Effluent Aquatic Toxicity Report Form - Chronic Fathead Minnow Multi -Concentration Test • Facility: Tritest, Inc. NPDES #: NC= 1062855 Pipe #: 001 County: Moore Robbins WWTP Laboratory Performing Test: Environmental Tes Signature of Operator in Responsible « _ e: Signature of Laboratory Supervisor. Comments: I-Mi1(cl Project: 1632 Samples: 050111.06, 050113.03, 050115.13 Mali Original To: North Carolina Depaitinent of Environment and Natural Resources DWQ/Environmental Sciences Branch 1621 Mail Service Center Raleigh, NC 27699-1621 Control Organisms % Effluent 5.0% % Effluent % Effluent 10% % Effluent m % Effluent 20% Replicate number 1 2 3 4 Survivingntunber of larvae 10 10 10 10 Original number of larvae 10. 10 10 ' 10 Weight/original (mg/larvae) 0.802 0.738 '0.616' 0.732 Survivingnumber of larvae 10 10 10 • 10 Original number of letvae 10 10 10 10 Weight/animal (niflnrvae)' 0.598 0.698 0.685 0.763 Surviving numbee of larvae 10 . 9 10 10 Original number of larvae 10 10 10 10 Weight/original (rr/larvae) 0.682 0.592 0.776 0.685 Surviving number of larvae 9 10 10 • 10 Original number of larvae . 10 10 10 10 Weight/original (rop/larvee) 0.678 0.720 0.619 0.672 Snrvivingnumber of larvae 10 10 10 10 Original number of larvae 10 10 10 10 Weight/original (ng/larvae) 0.726 0.706 0.679 0.745 Snrvivingnumber of larvae 10 10 10 10 Original number of larvae 10 10 10 10 Weight/original (mg/larvae) 0.630 0.820. 0.754 . 0.709 Water Quality Data Control pH (Sir): DO (): Temp. (°C): High Concentration pH (Scl): DO (rae/14: Temp. (°C): Start date: End date: Start time: End time: 01-11-05 01-18-05 1435 1440 Survival (%) Average wt (mg) Average wt / surviving (erg) Survival (%) Average wt (mg) Survival (%) Average wt (Mg) Survival (%) Average wt (mg) Survival (%) Average wt (mg) . Survival (%) Average wt (mg) 100.0 0.722 0.722 100.0 0.686 97.5 0.684 97.5 0.672 100.0 0.714 100.0 0.728 Test Organisms Outside supplier. IAquatic BioSystena,Inc. Hatch date: Hatch time: 01-10-05 1400-1600 EST Day0 Initial I Final Day l Initial Final Day 2 Initial Final Day 3 Initial Final Day 4 Initial Final Day 5 Initial Final Day 6 Initial Final 7.75 7.59 7.62 7.50 7.73 7.63 7.98 7.29 7.84 7.46 7.95 7.48 .7.92 7.59 7.9 7.6 8.0 7.6 8.0 7.2 8.2 7.5 7.8 7.1 • 8.1 7.4 8.1 7.6 25.1 25.1 '25.1 25.1 25.0 24.7 24.4 25.0 - 24.5 24.8 24.5 24.9 24.6 . 24.1 7.70 7.72 '7.77 7.65 7.41 7.67 8.03 7.42 7.56 7.55 7.81 7.54 8.01 734 7.9 ' 7.7 7.9 7.6 8.1 7.1 7.6 7.2 7.8 7.0 . 8.4 7.2 8.5 . 7.6 ' 25.6 25.0 24.8 24.9 24.9 25.0 24.5 25.0 24.6 24.7 24.3 24.8 24.7 24.1 Sample Information Collectinn start date: Grab: Composite duration: Alkalinity (mg/L CaCO3): Hardness (mgjL CaCO3): Conductivity (limhos/cm): Total residual chlorine (mg/L): Sample Temp. at Receipt (°C): Overall Analysis: s=' L1 s1i�iii Sample 3 Control 01-09-05 01-11-05 01-13-05 M. •25-h 24-h 24.25-h 100 110 130 34,33,32 38 42 . 46 44, 42, 42 635 623 634 146-175 < 0.10 < 0.10 < 0.10 0!�,• 'r r� 0.5 • 0.8 0.4 •S'''�' �£�zu £,,cxa Analyses Normal: Hom. Var. NOEC: LOEC: ChV: Method: Survival . Growth - NA Yes NA Yes . 20% 20% > 20% ' > 20% >20% >20% Visuallnspec. Dunnett's Survival ' Growth %Emueat Critical Calculated Critical Calculated 5.0% 2.410 ' 0.787 ' 7.5% 2.410 0.836 10% 2.410 1.087 15% '. 2.410 0.175 20% . 2.410 -0.137 Result PASS LOEC: > 20% NOEC: 20% ChV: > 20% DWQ form AT-5 (8/03) En•V' onmental Testing Solutions, PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 E-mail: JimSumner@aol.com Date: May 03, 2005 Effluent Aquatic Toxicity Report Form - Chronic Fathead Minnow Multi -Concentration Test Facility: Tritest, Inc. NPDES #: NC. 0062855 Pipe #: 001 County: Moore OW3 oii5y Robbins WWTP Laboratory Performing Test Environmental Testinc utio� Signature of Operator in Responsible Ch-ge: Signature of Laboratory Supervisor. Comments: Project: 1813 Samples: 050412.04, 050414.08,050416.11 Mail Original To: North Carolina Department of Environment and Natural Resources DWQ/ Environmental Sciences Branch 1621 Mail Service Center Raleigh, NC 27699-1621 Control Organisms Effluent 5.0% Effluent 7.5% % Effluent 10% Replicate number 3 4 Survivingnumber of lazvae 10 10 10 10 Original number of larvae 10 10 10 10 Weight/original (mn7arvae) 0.712 0.641 0.632 0.663 of larvae 10 10 10 10 1Slrrvivingnumber Original number of larvae I 10 10. 10 10 Weip t/original (mrgilarvae) 0.600 0.602 0.620 0.598 Survivingnumber of larvae 9 10 10 I 10 Original number of larvae ` 10 ( 10 10 Itl 10 gh Wei t/original (rnearvae) 0.582 1 0.709 0.665 0.629 Survivingnumber of larvae 10 10 10 10 Original number of larvae 10 1 10 10 10 rgiit/ We' original (mg(larvae) 0.689 0.644 0.656 0.580 % Effluent Survivingnumber of larvae Original number of larvae \Veightforiginal (mg/larvae) I is% I % Effluent Survivingnamber of larvae Original number of larvae Weight/originat (ing'larvae) 20% I Water Quality Data Control PH( : DO (n L): Temp. ('C): 10 .10 0.640 10 10 0.529 10 10 0.736 10 10 0.673 10 I 10 10 1 10 0.736 0.700 10 10 0.632 10 10 0.706 I Start date: Bad date: Start time: End time: 04-12-05 , 04-19-05 1420 1334 Test Organisms Survival (%) 100.0 Outside supplier. Average wt (mg) L 0.662 I Aquatic BioSyste s, Inc. I Average Wt/ 0.662' surviving (mg) Hatch date: Hatch time: Survival (%) Average wt (mg) 1100.0 0.605 Survival (%) I 97.5 Average wt (m0 0.646 Survival (%) Average wt (mg) Survival (%) Average wt (mg) Survival (%) Average wt (mg) Day Day1 Day2 .Day3 Initial Final I Initial Final Initial Final Initial Final ` 7.78 I 7.64 7.75 I 7.53 j`I 7.9 8.0 1 jl 7.5 I8.3 24.6 24.5 24.8 24.4 High Concentration pH (SU): I 7.72 DO (n>g(1.): IIt 8.5 Temp. CC): 25.0 Sample Information Collection start date: Grab: Composite duration: Alkalinity (mg/L. CaCOj): Hardness (rneL CaCO3): Conductivity (p.rnhos/cm): Total residual chlorine (mg'1.): Sample Temp. at Receipt (°C): 7.73 8.3 • 24.2 7.81 8.5 24.7 Sample 1 04-10-05 24-h 72 •' 7.71 7.5 24.3 Sample 2 04-12-05 25.5-h 86 7.77 8.1 24.7 7.61 8.3 25.2 7.66 8.1 24.5 7.75 I7.8 24.4 Sample 3 04-14.05 24.25-h 41 7.78 8.2 24.8 7.80 8.0 24.9 Control 31, 34, 32 45 49 47 41, 41, 45 380 < 0.10 1.1 511 < 0.10 0.8 382 < 0.10 0.5 156-166 7.46 8.1 24.3 7.66 8.3 24.3 1100.0 0.642 100.0 10.670 1100.0 I 0.668 04-11-05 1430/1630 BST Day4 I Day5 I Day6 Initial Final 1 Initial Final Initial Final 7.67 8.4 25.0 7.52 8.6 8.6 24.7 Analyses Normal: Horn Var. NOBC. LOEC: ChV: Method: Overall Analysis: Result: PASS LOEC: > 20% NOEC: 20% ChV: %Effluent 5.0% 7.5% 10% 15% 20% > 20% 7.52 8.0 24.6 .5 jl 8.0 l 24.6 7.67 8.1 25.0 7.58 8.3 25.2 Survival NA 7.43 7.9 1I` 24.7 7.55 7.9 25.0 Growth Yes 7.34 8.2 24.8 7.50 8.3 24.9 NA Yes 20% 20% • > 20% > 20% > 20% > 20% Visual Inspec. Survival Critical Calculated Dunnett's Growth Critical 2.410 2.410 2.410 2.410 2.410 7.39 7.4 24.5 7.45 7.6 24.6. Calculated 1.496 0.413 0.518 -0.217 -0.151 DWQ form AT-5 (8/03) Box 7565 =psheville,.NC 28802 Effluent Aquatic Toxicity Report Form - Chronic Fathead Minnow Multi -Concentration Facility: Tritest, Inc. NPDES #: NC- 0062855 Pipe #: 001 County: Robbins WWTP Laboratory Performing Test: Environmental Tes Signamm of Operator in Responsible el • _e: Signature of Laboratory Supervisor: Marl Original To: North • Carolina Department of Environment and Natural Resources DWQ/ Environmental Sciences Brunch 1621 Marl Service Center Raleigh, NC 27699-1621 Control Organisms % Effluent 5.0% % Effluent PIM % Effluent Replicate number 1 2 3 4 Survivingnumber of larvae 10 10 10 10 Original number of larvae 10 10 10 ' 10 Weight/otiginal (mg/larvae) 0.802 0.738 ' 0.616 0.732 Survivingnumber of larvae 10 10 10 • • 10 Original number of larvae 10 10. 10 10 Weight/original (mg/larvae) ' 0.598 0.698 0.685 0.763 Survivingnumbec of larvae 10 9 10 10 Original number of larvae 10 10 10 10 Weight/original (mg/larvae) 0.682 0.592 0.776 0.685 10% • % Effluent m % Effluent 20% Surviving number of larvae 9 10 10 • 10 Original number of larvae 10 10 10 10 Weight/original (mg/larvae) 0.678 0.720 0.619 0.672 Surviving number of larvae 10 10 10 10 Original number of larvae 10 10 10 10 Weight/original (mg/larvae) 0.726 0.706 0.679 0.745 Stir viving number of larvae 10 10 10 10 Original number of larvae 10 10 10 . 10 Weight/original (mg/larvae) 0.630 0.820. 0.754 0.709 Water Quality Data . Control pH (SU): DO Ong/4 Temp. (°C): high Concert pH (SU): DO (mg/L): Temp. (°C): Start date: 01-11-05 End date: 01-18-05 Start time: 1435 End time: 1440 Survival (%) Average wt (mg) Average wt / surviving (mg) Survival (%) Average wt (mg) Survival (%) Average wt (mg) • Survival (%) Average wt (mg) Survival (%) Average wt (mg) Survival (%) 'Average wt (mg) 100.0 0.722 0.722 100.0 0.686 97.5 0.684 97.5 0.672 100.0 0.714 100.0 0.728 Test Organisms Outside supplier. IAquatic BioSystems, Inc. I Aatch date: Hatch time: 01-10-05 1400-1600 EST Day 0 Initial Final Dayl Initial] Final Day 2 initial Final Day 3 Initial Final Day 4 Initial Final Day 5 Initial Final Day6 Initial Final 7.75 7.59 7.62 7.50 7.73 7.63 7.98 7.29 7.84 7.46 7.95 7.48 .7.92 7.59 7.9 7.6 8.0 7.6 8.0_ 7.2 8.2 7.5 7.8 7.1 • 8.1 7A 8.1 7.6 25.1 25.1 '25.1 25.1 25.0 24.7 24.4 25.0 24.5 24.8 24.5 24.9 24.6 24.1 7.70 7.72 7.77 7.65 7.41 7.67 8.03 7.42 7.56 7.55 7.81 7.54 8.01 7.74 7.9 7.7 7.9 7.6 8.1 7.1 7.6 7.2 7.8 7.0 . 8.4 7.2 8.5 7.6 25.6 25.0 24.8 24.9 24.9 25.0 24.5 25.0 24.6 .24.7 24.3 24.8 24.7 24.1 Sample Information Collection start date: Grab: Corrposite duration: Alkalinity (mg/L CaCO3): Hardness (mg/L CaCO3): Conductivity (lrmhos/cm): Total residual chlorine (mg/L): Sample Temp. at Receipt (°C): Overall Analysis: Sample 1 Sample 2 Sample 3 Control 01-09-05 01-11-05 01-13-05 '{°''.`}�#y� .25-h 24-h 24.25-h iASR a? iK 100 110 130 34,33,32 38 42 46 44,42,42 635 623 634 146-175 <0.10 <0.10 <0.10 0.5• ' 0.8 0A . Analyses Normal: Hom. Var. NOEC: LOEC: ChV: Method: Survival Growth NA Yes NA Yes ' 20% 20% > 20% > 20% >20% >20% Visualinspec. Dunnett's Survival ' Growth %Effluent Critical Calculated Critical Calculated 5.0% . 2.410 0.787 7.5% 2.410 0.836 10% 2.410 1.087 15% 2.410 0.175 20% . . 2.410 -0.137 Result: PASS LOEC:, > 20% NOEC: 20% ChV: > 20% DWQ form AT-5 (8/03)