WI0700012_Monitoring (Report)_20040827

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 2
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 13.60 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: 118
Field Analysis: pH 7.3 , Specific Conductance 1951 uMhos
Temp. 20 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludges
i'V
Note: Values should reflect dissolved and Q
colloidal concentrations
Date sample collected: 7/26/04 CrJ
Date sample analyzed: 7/26/04 to 7/27/04
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
EXPIRATION DATE:
UIC X
01/15/08
Other
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease an
Phenol
Sulfate •
Specific Cond ance
Total Ammonia
TKN as N _
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
N/A mg/I
N/A units
Al - Aluminum
Ba - Barium
N/A mg/I Ca - Calcium
,�u�
N/A mg/I
R10, � /A mg/I
IQ N/A mg/I
N/A mg/I Fe - Iron
N/A mg/I Hg - Mercury
N/A uMhos
N/A mg/I
f N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
No and field acidified
N/A mg/1 Ni - Nickel
N/A mg/1 Pb - Lead
N/A mg/I Zn - Zinc
Yes n/a No )
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Ammonia Nitrogen mg/I
N/A mg/I Other (Specify Compounds and Concentration Units) c
N/A mg/I Fluoride ON/lp mg/I
N/A mg/I MIBK 0-N/A; ,Ig/I
N/A mg/I Ag - Silver . /A tfg/I
N/A mg/I Se- Selenium OA 74M
N/A mg/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1 Organics: (GC, GC/MS, HPLC) . pj:rt
N/A mg/I (Specify test method #. Attach lab report.) -t
N/A mgll Report attached? Yes (1) No X (.?? (2)�
N/A mg/I VOC : method# O o
: method# at %
: method#
4
N/A mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ros
ith - Manager, Environmental Affairs
Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 2
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 48.00 ft. Well Diamter:
CIW-7
4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
N/A
Field Analysis: pH 7.0 , Specific Conductance 786 uMhos
Temp. 21 oC, Odor NONE
Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : o ,
Rotary Distributor Land Application of Sludg'
IN
Other
Gi
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
7/26/04
7/26/04 to 7/27/04
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
N/A mg/I Al - Aluminum
N/A units Ba - Barium
N/A mg/I Ca - Calcium
N/A mg/I Cd- Cadmium
N/A mg/1 Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A mg/I
Fe - Iron
Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
N/A mg/I Zn - Zinc
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/l
N/A mg/I
N/A mg/1
Yes nla No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Una)
Fluoride C1 °� N/A
MIBK A c%JV/A
Ag - Silver .Ey1A
Se- Selenium
Sodium
N/A mg/1 Organics: (GC, GC/MS, HPLC) -o Vi
N/A mg/I (Specify test method #. Attach lab report.}
N/A mg/I Report attached? Yes (1) No )C
N/A mg/I VOC : method#©e
N/A mg/I
: method#
: method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/
ug/
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ros
Si. ature
ith - Man
er, Environmental Affairs
me and Title - Please type r pri
ermitt e (or Authorized Agent)

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
May 2004 — July 2004
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Ma y
219,700
0
219,700
4.9
11.0
June
227,940
0
227,940
5.3
11.0
July
408,270
0
408,270
9.1
15.0
TOTALS
855,910
0
855,910
H:\Reports\2004\Quarterly\TFRAS Report Second Quarter 2004.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
May
372,797
132,028
504,825
11.3
June
379,691
72,491
452,182
10.5
July
344,282
81,597
425,879
9.9
TOTALS
1,096,770
286, 116
1,382,886
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
System air compressor was down February 3 until February 4 and again from February 23 until March 8 .
During these periods the system operated on Plant Air.
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1:
SWW-2: On 5/4 changed counter.
SWW-3:
SWW-4: On 5/3 changed counter.
SWW-5:
SWW-6: On 5/5 changed counter.
SWW-7: On 7/19 changed pump.
H:\Reports\2004\Quarterly\TFRAS Report Second Quarter 2004.doc 4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 5/26 shook pump.
CWW-2: On 5/3 air blasted well. On 6/1 air blasted well.
CWW-3:
CWW-4:
CWW-5:
CWW-6:
CWW-7: On 5/3 changed counter. On 6/24 air blasted well. On 7/13 acid washed well.
H:\Reports\2004\Quarterly\TFRAS Report Second Quarter 2004.doc
5

pCS Phosphate
Aurora Divison
WELL MEASUREMENTS
R-2 Piezometers47.0/0y
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Wtr Lvl
Rel to MSL
19+50
A
50.30
B
33.24
27+50
A
52.15
B
34.19
40+00
A
53.30
B
35.89
50+00
A
52.05
,36'f/
/%S.5
B
34.30
/7,n
PTA
61+00
A
55.16
,33, 90
o?/.Q&
B
35.12
/V, qe9
°'Pai/l/,
71+00
A
55.16
,9%i, 9a2
/c9 v%Y
B
35.12
eamypd
80+00
A
50.26
k r :9V
/61.86
B
35.01
j(, bro
IS-Vi
95+00
A
53.41
..8/f'
A.57 a /
B
35.84
0?S. ,3
/4, 61
110+00
A
54.84
B
34.60
P716
A
,.�..,
n
19,/9
`
o? 9, r/
P719
A
3`7,jo
Jst......... 11�;1iCyfiY.S
7 ` /� e
Piezometer required measurements as per Env. Action 3255-
D:L Welldata1NPDES1Piezomtr\R2PlEZ.W V4

PCS
Phosphate
VIV. AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
August 26, 2004
EVAN O. KANE
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
May 2004 — July 2004
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) piezometer level monitoring field sheet, and c) the summary operational and
maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
_YE
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming