WI0700012_Monitoring (Report)_20000518 (3)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.92 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILLILITERSof water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2800
Field Analysis: pH 5.6 , Specific Conductance 409 uMhos
Temp. 19.7 oC, Odor NONE Appearance: CLEAR
Certification No(s) 330
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field Remediation :
EXPIRATION DATE:
UIC X
09/30/01
O
Remediation: Infiltration Gallo'?,
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4112/00 G:?
Date sample analyzed: 4/12/00 to 4/28/00 0
Laboratory Name: PCS PHOSPHATE
`-C
car^
zrr
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 300
pH (when analyzed) 5.9
TOC 3.9
Chloride 50.8
Arsenic
Grease and Oils
Phenol
Sulfate
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/1 Ca - Calcium
mg/I Cd- Cadmium
No and field acidified
Yes n/a No '1'
N/A mg/I Ni - Nickel Nba~ mg/I
N/A mg/I Pb - Lead N N6 mg/I
10.550 mg/1 Zn - Zinc •• N{21-'. mg/1
N/A mg/1 Ammonia Nitrogen W_..' mgll
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
49.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/1 Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
0.30
N/A
N/A
N/A
N/A
N/A mg/I VOC method#
method#
method#
N/A mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P- . ittee (of Authorizgd Agent) Na and Title - Please type or print
ignaturermittee(or uthorizedAgent) (Dat

cts
rib

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.6 , Specific Conductance 563 uMhos
Temp. 19.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallet,
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
09/30/01
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/12/00
Date sample analyzed: 4/12/00 to 4/28/00 O �,
Laboratory Name: PCS PHOSPHATE and 1VIFi. MNENT 1
Certification No(s) 330 10 c
cP
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 412 mg/1 Al - Aluminum
pH (when analyzed) 7.8 units
TOC 6.9 mg/1
Chloride 9.5 mg/I
X Yes
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1
12.1 mg/I
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No
VI
and field acidified X Yes No a�
N/A mg/I Ni - Nickel 3 Nf6 mg/I
N/A mg/I Pb - Lead 1...? N(A,7 mg/I
0.022 mg/l Zn - Zinc 1‘)Ng mg/I
N/A mg/I Ammonia Nitrogen G.,)r., mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.58 mg/I
N/A mg/I MIBK N/A mg/I
<0.001 mg/I Ag - Silver N/A mg/I
<0.005 mg/I Se- Selenium N/A mg/1
N/A mg/I Sodium N/A mg/1
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
<0.010 mg/I : method#
method#
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Puttee (of Authorized Ag ¢stl Nme and Title - Please type or print
fib L L
Signatur TPermittee (or Authorized Agent) ( )
to

May 22, 2000
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
PCS
Phosphate
AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
Subject: Underground Injection Control Program
First Quarter Groundwater Monitoring Report
February 2000 — April 2000
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
D. Daniel Winstead III
Environmental Engineer
Environmental Affairs
Attachments
pc: Willie Hardison / Keith Starner — DWQ- GWS, WaRO (w/attch)
bpc: T. L. Baker / 12-01-008-03-002 (w/ attch)
J. A. Hardy / R. B. Lee / T. W. Davis (w/ attch)
R. A. Allen / T. Lewis (w/attch)
D. D. Winstead / 00-24-000 (w/o attch)
W. A. Schimming (w/o attch)

4/ y/7•on
Am
"""`' """ Iwommuraatun ayetem utuarteriy monitoring
Date:
Time:
Tech:
System Gauge Pressures
SwW-1
SW W-7
CW W-1
CW W-7
Flle: 15-03-00302
pc: TLB
Ditch Level
5 . e:2a I
Barge Slip
(CO yi
Water Level
944 e
Control Tank
%=MSL
�/ 1
//' O /{gyp.
Well ID
Spz-1
TOC
Elevation
MSL'
10.47
Sand Layer Peizometers Level Indi
Spz-2
Spz-3
Spz-4
Spz-5
Spz-6
Spz-7
Spz-8
11.21
11.87
11.45
11.45
11.23
11.59
11.57
3
'S
9•
9
/Q
Spz-9
Spz-10
SPW
11.01
12:16
9.95
6
7
-0C
o Wtr
tvel'
•
�.
5.59
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Ste Wtr
Level'
Level
Relative To
L it
6.79
Cpz-1
10.51
MSL Ft.
/6
3.05
Cpz-2
10.25
754/
995
d 97
6.33
Cpz-3
11.12
i%60
Q, 90
'7
Jr 7/
CPW
9.65
9.02
of ,�r›?2
0/p
c%73�t12
MWTF-1A•
14.35
y,/a
o.1 J
so?
7 7 /
MWTF-18 •
14.36
y.
/O•49
D.e./
/35-
MWTF-1C•
14.44
9R
9.Q7
. 9 yy
29
,5 •ci9
MWTF-2A
14.05
637
. n/c
a. 93-
MWTF-28
14.02
6.6R
787
(a
/,% 48
/p56
S•rfij
7 0 z/
MWTF-2C
14.08
4/3
a `i O
MWTF-3A
12.21
3
4?f/0
D. 96--
MWTF-3B
12.18
9 tsi
71/
9Q
MWTF-3C
12.19
/77.34
r7
-D./7
Well ID
sww-1
CM-1
SW W-2
CWW-2
SWW-3
CW W-3
SW-4
CW W-4
SWW-5
CWW-5
SwW-6
Sww-7
CW W-7
Revised 8/12197
Sand Layer And Croatan Formation Withdrawal Wells
TOC
Elevation
MSL'
10.70
10.60
9.99
10.23
9.97
9.95
10.73
10.73
10.80
10.74
10.66
9.92
10.70
9.95
Max Ste
Wtr
Level Ft.
K. /o
2/
4.
7 4//
7/,0
7 No
(o' 77
(o . 75
4/9
to•3 r
702
Max Level
Relative To
MSL Ft.
-o. 90
/ 79
/.V/
- /, 1/O
4, o/
.0?'-Q5'
/56
D.Sir
/77
Control
Point
MSL'
+1 'to +2'
-2'to-1'
+1 ' to+2'
-2'to-1'
+1 ' to +2'
-2'to -1'
+1 .to+2'
-2'to-1'
+1 ' to+2'
-2.to-1'
+1 ' to+2'
-2 • to-1'
+1'1o+2'
-2' to -1'
• Riser length added to TOC elevation 124/97
Is Well
Pumping
(Y)es/(NM
�P..5
Comments
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2000 — April 2000
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/W) disinfection system throughout the period. On March 9 the system was down from 0915
through 1100. This outage was planned to allow preventative maintenance on the system. During the
outage both units received new bulbs, new ballast, new sensors and each unit was calibrated. The bottom
LED on the #1 Sterilizer was also changed.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
2000
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb
366,970
0
366,970
8.8
14.7
Mar
417,930
0
417,930
9.4
14.4
Apr
420,890
0
420,890
9.4
14.4
TOTALS
1,205,790
0
1,205,790
2
•

Withdrawal Well System
The Withdrawal Well System was down for a total of 2.5 hours during the period. On 4-7-00 for 2 hours to
repair a leaking air line and on 4-10-00 for 0.5 hours to change belts. The withdrawal water well pumps are
monitored daily by the area Maintenance Department and preventative maintenance work is performed as
needed. The total monthly and quarterly withdrawal water volumes for the period are:
2000
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb
565,660
288,965
854,626
19.6
Mar
543,763
284,853
828,616
18.6
Apr
498,300
342,472
840,772
18.8
TOTALS
1,607,723
916,290
2-, 524-, 013
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Air Compressor for the Withdrawal Well Pumps
The air compressor was down for 2 hours to repair an air line leak.
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 2/8, 2/25, 3/2 and 4/4 the pump was shaken to start. On 4/7 the pump was replaced. On 4/10
the pump was replaced. On 4/12 and 4/14 the pump was shaken to start. On 4/17 the pump was replaced.
SWW-2: On 3/29 the pump was shaken to start.
SWW-3: Pump operated without incident.
SWW-4: Pump operated without incident.
S W W-5: On 4/28 had to shake pump to start

SWW-6: Pump operated without incident.
SWW-7: Pump operated without incident.
Croatan Formation Withdrawal Well (CWW) Pumps
CW W-1: On 3/29 the pump was replaced. On 4/7 repaired the air line.
CWW-2: On 3/2 the pump was replaced. On 3/29 the totalizer was replaced.
CWW-3: Pump operated without incident.
CWW-4: Pump operated without incident.
CWW-5: On 2/8/ was shaken to start.
CWW-6: On 4/12 the pump was shaken to start.
CWW-7: On 2/15 repaired totalizer. On 3/14 the pump was shaken to start.
4
•
.,

ROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
(40
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
4 inch
Depth to Water Level: N/;A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 7.6 , Specific Conductance
Temp. 19 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
559 uMhos
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Garry
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor
Other
Land Application of Sludge
(3
O
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/12/00
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/12/00 to 4/28/00
PCS PHOSPHATE and
Go
O
IRt'IMENT 1
PARAMETERS: (Samples for metals were collected unfiltered X Yes No and field acidified X
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.030 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 412 mg/I Al - Aluminum N/A mg/I
pH (when analyzed) 7.9 units Ba - Barium N/A mg/I
TOC 7.0 mg/I Ca - Calcium N/A mg/I
Chloride 9.2 mg/I Cd- Cadmium <0.001 mg/I
Arsenic N/A mg/I Chromium: Total <0.005 mg/I
Grease and Oils N/A mg/I Cu - Copper N/A mg/l
Phenol N/A mg/I Fe - Iron N/A mg/I
Sulfate 13.7 mg/I Hg - Mercury N/A mg/I
Specific Conductance N/A uMhos K- Potassium N/A mg/I
Total Ammonia N/A mg/I Mg - Magnesium N/A mg/I
TKN as N N/A mg/l Mn - Manganese <0.010 mg/I
Ni � - Nickel N/fV:rfng/I
Pb - Lead N/i ng/I
Zn - Zinc N N/' ?L`.'mg/I
Ammonia Nitrogen N c, mg/I
Other (Specify Compounds and Concentration Units).) -i
Fluoride 0.59 mg/I
MIBK N/A mg/I
Ag - Silver N/A mg/I
Se- Selenium N/A mg/I
Sodium N/A mg/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
Yes
No
method#
method#
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P me (of Authorize ent) ame and Title - Please typore pint
v
Signs Permittee (or Authorized Agent) ate)

OUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 9.07 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
2 inch
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
3400
Field Analysis: pH 8.0 , Specific Conductance 592 uMhos
Temp. 21,9 oC, Odor
NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
09/30/01
Other
Note: Values should reflect dissolved and
d
colloidal concentrations,
Date sample collected: 4/12/00,
Date sample analyzed: 4/12/00 to 4/28/00 Cr?
Laboratory Name: PCS PHOSPHATE and ENWRONNNNT 1
Certification No(s) 330 10 'S
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A
Coliform: MF Fecal
Coliform: MF Total
mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
<1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
452 mg/I Al - Aluminum
7.6 units Ba - Barium
4.9 mg/I Ca - Calcium
10.1 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
97.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
NOTE:
GW-59 Rev 4/98
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.029 mg/1
No and field acidified X Yes No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.280 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/1 Fluoride 0.72
N/A mg/I MIBK N/A
<0.001 mg/I Ag - Silver N/A
<0.005 mg/I Se- Selenium N/A
N/A mg/I Sodium N/A
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
rVN/AAA mg/1
N/A= mg/I
N/A mg/I
mg/I
N/A mg/I VOC : method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
Terry L. Baker - Manager, Environmental Affairs
Pe mittee (of Authorized ent) Name and Title - Please type or print
Signatermittee (or Authorized Agent) '(Date)