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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_20030225GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jimmy Hardy Well Locations/Site Name: Tank Farm County: Beaufort Telephone: (252)322-8154 No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: 55.00 ft. Well Diamter: CWW-1 Screened Interval: 33.27 ft. to 52.68 ft. 4 inch Depth to Water Level: 7.56 ft. below measuring point. Measuring Point is 2.25 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH 6.4 , Specific Conductance Temp. 18.2 oC, Odor NONE For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) CONTINUOUS 2163 uMhos Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIG-727E28-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : ca EXPIRATION DATE: UIC X 01/15/08 Rotary Distributor Other Remediation: Infiltration Gallery Land Application of Sludge 7 (23 tr] Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/22/03 1/22/03 to 2/7/03 PCS PHOSPHATE and -ENVIRONMENT 1 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) Coliform: MF Total N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1824 pH (when analyzed) 7.1 TOC 6.7 Chloride Arsenic Grease and Oils Phenol Sulfate 80.4 N/A N/A N/A Specific Conductance Total Ammonia TKN as N 699.0 N/A N/A N/A mg/I units mg/I mg/I mg/I mg/I mg/I mg/I uMhos mg/I mg/I Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese N/A mg/I No and field acidified Yes n/a No ) N/A mg/I Ni - Nickel N/A mg/I Pb - Lead 2.350 mg/I N/A mg/I N/A mg/I N/A mg/I N/A mg/I Zn - Zinc Ammonia Nitrogen Other (Specify Compounds and Concentration Ling? - Fluoride 0.20 MIBK N/A N/A mg/I Ag - Silver N/A mg/I N/A mg/I Se- Selenium Sodium N/A ug/I N/A* ug/I G? N/ X' ug/I mg/I mg/l mg/I N/A mg/I N/A mg/I N/A ug/I N/A mg/I Organics: (GC, GC/MS, HPLC) N/A mgll (Specify test method #. Attach lab report.) N/A mg/1 Report attached? Yes (1) No X (2) N/A mg/I VOC : method# method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Permittee (of Authorized ent) Name and Title - Please type or print Signatutof Permittee (or Authorized Agent) (D te) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jimmy Hardy Well Locations/Site Name: Tank Farm County: Beaufort Telephone: (252)322-8154 No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-2 Well Depth: 52.15 ft. Well Diamter: 4 inch Screened Interval: 30.57 ft. to 49.82 ft. Depth to Water Level: 6.71 ft. below measuring point. Measuring Point is 3.00 ft above land surface. MILILITERS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.2 . Specific Conductance 2785 uMhos Temp. 19.6 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED EXPIRATION DATE: UIC X 01 /15/08 Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of,Sl,udge Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/22/03 rnL- .; - rn cis _-r PCS PHOSPHATE an� ENSNRbNMENT 1 330 10 03 o 1/22/03 to 2/7/03 C 3 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A Coliform: MF Fecal Coliform: MF Total N/A mg/I Nitrite (NO2 as N) /100m1 Nitrate (NO3 as N) N/A /100m1 (Note' Use MPN method for highly turbid samples) Dissolved Solids: Total 2572 mg/I pH (when analyzed) 7.0 units TOC 7.8 mg/I Chloride 77.6 mg/I Arsenic N/A mg/I Grease and Oils Phenol Sulfate N/A mg/I Specific Conductance Total Ammonia TKN as N No and field acidified N/A N/A Phosphorus: Total as Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium P 15.000 N/A N/A N/A N/A Cd- Cadmium Chromium: Total Cu - Copper N/A mg/I Fe - Iron N/A N/A N/A N/A 1116.6 mg/I Hg - Mercury N/A N/A uMhos K- Potassium N/A mg/1 Mg - Magnesium N/A mg/I Mn - Manganese N/A N/A N/A mg/I mg/1 mg/1 mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/1 mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No ) Ammonia Nitrogen N/A ug/I N/A ug/I N/A ug/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium mg/I 0.1 a 3 mg/I N/A mg/I N/A--71 mg/I N/A') mg/I N/A 3 ug/I Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC method# method# method# I certify thatto the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs s`c SignaturgPermittee (or Authorized Agent) (Da e) Per (of Authorizedq ) Name and Title - Please type or print GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jimmy Hardy Well Locations/Site Name: County: Beaufort Telephone: (252)322-8154 Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-3 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.42 ft. to 50.67 ft. Depth to Water Level: 7.10 ft. below measuring point. Measuring Point is 3.08 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.2 , Specific Conductance 2534 uMhos Temp. 23.9 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltrra3tion Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/15/08 Rotary Distributor Land Application ofSlud--) Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/22/03 =) 1/22/03 to 2/7/0 PCS PHOSPHATE and EDI.VIRONMENT 1 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) Coliform: MF Total N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 1929 mg/I Al - Aluminum pH (when analyzed) 6.9 units Ba - Barium TOC 9.8 mg/1 Ca - Calcium Chloride 141.1 mg/I Cd- Cadmium Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N No and field acidified N/A mg/1 Ni - Nickel N/A mg/I Pb - Lead 3.250 mg/1 Zn - Zinc Yes n/a No ) N/A N/A N/A N/A mg/I Ammonia Nitrogen N/A mg/I N/A mg/I N/A mg/1 N/A mg/1 N/A mg/I Chromium: Total N/A mg/1 Cu - Copper N/A mg/I Fe - Iron 601.2 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/1 Mg - Magnesium N/A mg/I Mn - Manganese N/A mg/I N/A mg/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium N/A mg/I Organics: (GC, GC/MS, HPLC) N/A mg/I (Specify test method #. Attach lab report.) N/A mg/I Report attached? Yes (1) No X (2) N/A mg/1 VOC : method# method# method# 0.17 N/A N/A N/A N/A ug/I ug/I ug/1 mg/1 ) mg/I I mg/I mg/I t mg/I ug/l N/A mg/I I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Permittee of Authorized A ent) Name and Title - Please type or print Signature ermittee (or Authorized Agent) (Da e) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jimmy Hardy Well Locations/Site Name: Tank Farm County: Beaufort Telephone: (252)322-8154 No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-4 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 41.67 ft. to 50.92 ft. Depth to Water Level: 7.07 ft. below measuring point. Measuring Point is 2.75 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.2 , Specific Conductance 2669 uMhos Temp. 27.2 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITQ3tED Lagoon Remediation: Infiltron Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/15/08 Rotary Distributor Other Land Application of Sludge. ti :t_ Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 1/22/03 Date sample analyzed: 1/22/03 to 2/7/03 Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1 W rn Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered Yes COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note Use MPN method for highly turbid samples) Dissolved Solids: Total 1872 pH (when analyzed) 7.6 TOC mg/I units 6.7 mg/I Chloride Arsenic 119.3 mg/I N/A mg/I Grease and Oils N/A mg/I Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I 682.9 mg/I N/A uMhos N/A mg/I N/A mg/I mg/1 Nitrite (NO2 as N) /100m1 Nitrate (NO3 as N) /100m1 Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese n/a No and field acidified N/A N/A 4.550 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/1 mg/I mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No ) N/A N/A N/A Ammonia Nitrogen Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X 0.11 N/A N/A N/A N/A VOC method# method# : method# u gll ug/I ug/I mg/I mg/I mg/I mg/I mg/I ug/I (2) I certify that. to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Per •' f Authorized 9gi) Name and Title - Please type or print Zi Da e gnatur Permittee (or Authorized Agent) ( ) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 Contact Person: Jimmy Hardy Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 County: Beaufort Telephone: (252)322-8154 Well Identification Number (from Permit): CWW-5 Well Depth: 53.17 ft. Well Diamter: 4 inch Screened Interval: 41.75 ft. to 51.08 ft. Depth to Water Level: Measuring Point is 6.94 ft. below measuring point. 2.58 ft above land surface. For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 2232 uMhos Temp. 29.3 oC, Odor NONE Appearance: CLEAR Mail Original to. DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH. NC 27626-0578 Phone (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 01/15/08 Spray Field X Remediation : Rotary Distributor Land Application Other Mudge 3 r' : c, rri Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/22/03 3 1 /22/03 to 2/7/03W rc-�r*i PCS PHOSPHATE gill EtfYIRONMENT 1 330 10 rn PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC 1424 7.0 6.6 Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 83.6 N/A N/A N/A 505.1 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/l mg/I mg/I mg/l uMhos mg/l mg/1 Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron No and field acidified Yes n/a No ) N/A mg/I Ni - Nickel N/A mg/l Pb - Lead 8.950 mg/I Zn - Zinc N/A N/A N/A N/A mg/I Ammonia Nitrogen N/A mg/1 Other (Specify Compounds and Concentration Units) N/A mg/l Fluoride N/A mg/I MIBK N/A mg/I Ag - Silver N/A mg/I Se- Selenium N/A mg/I Sodium ug/I ug/I ug/I mg/I -3 0.12 : mg/I N/A > mg/I N/AT mg/I N/A mg/I N/A ug/I N/A mg/I Organics: (GC, GC/MS, HPLC) Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.) K- Potassium Mg - Magnesium Mn - Manganese N/A mg/I Report attached? Yes (1) No X (2) N/A mg/I VOC N/A mg/I method# method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Permittee (of Authorized AA enn) Name and Title - Please type or print Signaturq'q'Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-6 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.62 ft. to 50.88 ft. Depth to Water Level: 7.37 ft. below measuring point. Measuring Point is 2.92 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Systems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.2 , Specific Conductance 2031 uMhos Temp. 29.1 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITED Lagoon Remediation: InfiltrAon Gaffe_ ry Spray Field X Remediation : Rotary Distributor EXPIRATION DATE: UIC X 01/15/08 Other Land Application ottludge rn. _ rat Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/22/03 1/22/03 to 2/7/03 r' a PCS PHOSPHATE and ENVIRONMENT 1 330 10 PARAMETERS: (Samples for metals were collected unfiltered COD N/A Coliform: MF Fecal N/A Coliform: MF Total N/A (Note Use MPN method for highly turbid samples) Dissolved Solids: Total 1480 pH (when analyzed) 6.9 TOC 8.0 Chloride Arsenic mg/I /100m1 /100m1 Yes n/a Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate mg/I Al - Aluminum units Ba - Barium mg/I Ca - Calcium 99.0 mg/I Cd- Cadmium Grease and Oils Phenol Sulfate No and field acidified N/A mg/I N/A mg/I 22.750 mg/I N/A mg/I N/A mg/I N/A mg/I N/A mg/I N/A mg/I N/A mg/I Chromium: Total N/A mg/I Cu - Copper Specific Conductance Total Ammonia TKN as N N/A mg/I Fe - Iron 446.4 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No ) N/A N/A N/A Ammonia Nitrogen Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A mg/I Se- Selenium N/A mg/I Sodium N/A mg/I Organics: (GC, GC/MS, HPLC) N/A mg/I (Specify test method #. Attach lab report.) N/A mg/I Report attached? Yes (1) No X 0.13 N/A N/A N/A N/A N/A mg/I VOC N/A mg/I method# method# method# ug/I ug/I ug/I mg/I mg/I mg/I mg/I mg/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: Terry L. Baker - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print GW-59 Rev 4/98 ignature ermittee (or Authorized Agent) (Dat GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-7 Well Depth: 53.00 ft. Well Diamter: Screened Interval: 36.58 ft. to 50.83 ft. Depth to Water Level: Measuring Point is 4 inch 6.67 ft. below measuring point. 1.25 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.5 , Specific Conductance 1198 uMhos Temp. 22.5 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH. NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITO,RED Lagoon Remediation: Infil r*tion;Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 01/15/08 Rotary Distributor Other Land Application offludge Note: Values should reflect dissolved and colloidal concentrations o Date sample collected: 1/28/03 cJ) Date sample analyzed: 1/28/03 to 2/7/03 Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A /100m1 (Note Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC 920 7.0 5.8 Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 69.7 N/A N/A N/A 194.9 N/A N/A N/A mg/1 units mg/I mg/I mg/I mg/I mg/I Fe - Iron mg/1 Hg - Mercury uMhos mg/I mg/I Yes n/a Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper No and field acidified N/A mg/I Ni - Nickel 3.475 mg/1 N/A mg/I Pb - Lead Zn - Zinc N/A mg/l Ammonia Nitrogen N/A mg/I Other (Specify Compounds and Concentration Units) Yes n/a No ) N/A mg/I Fluoride N/A mg/I MIBK N/A mg/1 Ag - Silver N/A mg/I N/A mg/I K- Potassium Mg - Magnesium Mn - Manganese Se- Selenium Sodium N/A N/A N/A 0.'p7: Nai NTA' N/A N/A ug/I ug/I ug/I mg/1 mg/I mg/I mg/I mg/1 ug/I N/A mg/I Organics: (GC, GC/MS, HPLC) N/A mg/I (Specify test method #. Attach lab report.) N/A mg/I Report attached? Yes (1) No X (2) N/A mg/I VOC N/A mg/I method# method# method# I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: Terry L. Baker - Manager, Environmental Affairs Permittee (of Authorized Agent N e and Title - Please type or print GW-59 Rev 4/98 S gnature ormittee (or Authorized Agent) (Da