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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_19990528 (2)GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-1 Well Depth: 55.00 ft. Well Diamter: 4 inch Screened Interval: 33.27 ft. to 52.68 ft. Depth to Water Level: 7.94 ft. below measuring point. Measuring Point is 2.25 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) Effluent (99) CONTINUOUS Field Analysis: pH 6.0 , Specific Conductance 2272 uMhos Temp. 18.9 oC, Odor NONE Appearance: LT YELLOW Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : EXPIRATION DATE: UIC X 09/30/01 Remediation: Infiltration Gallery Rotary Distributor Land Application of Sludge Other to Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/14/99 1v Date sample analyzed: 4/14/99 to 5/11/99 Laboratory Name: PCS PHOSPHATE 7i, 7,6 Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A /100m1 (Note' Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Phenol Sulfate Use MPN method for highly turbid samples) 1988 6.7 10.5 68.0 N/A Oils N/A N/A Specific Conductance Total Ammonia TKN as N 724.6 N/A N/A N/A mg/I nits mg/I mg/I mg/I mg/I mg/I mg/I uMhos mg/I mg/I Yes n/a Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury 3.690 mg/I No and field acidified Yes n/a No N/A mg/I Ni - Nickel N/A mg/I Pb - Lead Zn - Zinc N/A mg/I Ammonia Nitrogen N/A ug/I N/A ug/I N/A ug/I N/A N/A N/A Other (Specify Compounds and Concentration Units) Fluoride MIBK N/A ug/I Ag - Silver N/A ug/I N/A ug/I K- Potassium Mg - Magnesium Mn - Manganese Se- Selenium Sodium 0.25 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X N/A ug/I VOC method# method# method# N/A ug/I ug/I ug/I ug/I mg/I mg/I ug/I ug/1 ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please pe or print r�v o9- �./z 8%4 Signature of Permittee. or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-2 Well Depth: 52.15 ft. Well Diamter: 4 inch Screened Interval: 30.57 ft. to 49.82 ft. Depth to Water Level: Measuring Point is 7.94 ft. below measuring point. 3.00 ft above land surface. For Groundwater Treatment Sys ems Check One: Influent (98) Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.0 , Specific Conductance 2393 uMhos Temp. 19.3 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : EXPIRATION DATE: UIC X 09/30/01 Remediation: Infiltration Gallery Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/14/99 "J Date sample analyzed: 4/14/99 to 5/18/99 . a Laboratory Name: PCS PHOSPHATE Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal Coliform: MF Total N/A /100m1 Nitrate (NO3 as N) N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 2064 pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 6.7 10.1 104.6 N/A N/A N/A 708.6 N/A N/A N/A mg/I nits mg/I mg/I mg/I mg/I mg/I mg/I uMhos mg/I mg/I Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium No and field acidified Yes n/a No N/A mg/I Ni - Nickel N/A mg/l Pb - Lead 7.900 mg/I Zn - Zinc N/A mg/I Ammonia Nitrogen N/A ug/I N/A ug/I N/A ug/I N/A ug/I Other (Specify Compounds and Concentration Units) Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury N/A ug/I Fluoride N/A ug/I MIBK N/A ug/I Ag - Silver N/A ug/I Se- Selenium N/A ug/l Sodium K- Potassium Mg - Magnesium Mn - Manganese 0.21 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X N/A ug/I VOC method# N/A ug/I : method# : method# mg/I mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print Signature of Permittee ( Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-3 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.42 ft. to 50.67 ft. Depth to Water Level: 7.46 ft. below measuring point. Measuring Point is 3.08 ft above land surface. GALLLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) ;,C Effluent (99) CONTINUOUS Field Analysis: pH 6.1 , Specific Conductance 2444 uMhos Temp. 26.4 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration GalI ryt Spray Field X Remediation : Rotary Distributor Land Application of Sludge EXPIRATION DATE: UIC X 09/30/01 Other r .� cD Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/14/99 Date sample analyzed: Laboratory Name: PCS PHOSPHATE 4/14/99 to 5/11/99 Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes COD N/A mg/I Coliform: MF Fecal Coliform: MF Total N/A /100m1 N/A /100m1 (Note Use MPN method for highly turbid samples) Dissolved Solids: Total 1808 mg/I pH (when analyzed) 6.9 nits TOC 8.0 mg/I Chloride Arsenic 112.8 mg/I Grease and Oils Phenol Sulfate N/A mg/l N/A mg/I Specific Conductance Total Ammonia TKN as N Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper N/A mg/I Fe - Iron 624.9 mg/I N/A uMhos N/A mg/I N/A mg/I Hg - Mercury n/a No and field acidified Yes n/a No N/A mg/I Ni - Nickel N/A mg/I Pb - Lead 5.000 mg/I Zn - Zinc N/A mg/I N/A ug/I N/A ug/I N/A ug/I Ammonia Nitrogen N/A ug/I N/A -- ug/I N/A ug/I Other (Specify Compounds and Concentration Units) Fluoride MIBK N/A ug/I Ag - Silver N/A ug/I Se- Selenium N/A ug/I Sodium K- Potassium Mg - Magnesium Mn - Manganese 0.22 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X N/A ug/I VOC N/A ug/I method# method# method# mg/I mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print .Aft-eih Signature of Permittee (or /t(ithorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-4 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 41,67 ft. to 50.92 ft. Depth to Water Level: 6.89 ft. below measuring point. Measuring Point is 2.75 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) Effluent (99) CONTINUOUS Field Analysis: pH 6.0 , Specific Conductance 2434 uMhos Temp. 28.2 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 09/30/01 Spray Field X Remediation Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/14/99 Date sample analyzed: 4/14/99 to 5/11/99 Laboratory Name: PCS PHOSPHATE Certification No(s) 330 PARAMETERS: (Samples for metals were collected COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1732 pH (when analyzed) TOC mg/I /100m1 /100m1 mg/I 6.8 nits 7.3 mg/I Chloride Arsenic 105.6 mg/I Grease and Oils Phenol Sulfate N/A mg/I N/A mg/1 Specific Conductance Total Ammonia TKN as N N/A mg/I 581.5 mg/1 N/A uMhos N/A mg/I N/A mg/1 unfiltered Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury Yes n/a No and field acidified Yes n/a No N/A mg/I Ni - Nickel N/A mg/I Pb - Lead 5.000 mg/I Zn - Zinc N/A N/A N/A N/A mg/I Ammonia Nitrogen N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I K- Potassium Mg - Magnesium Mn - Manganese Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium 0.16 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X N/A ug/I VOC N/A ug/I method# method# method# ug/I ug/I u g/I mg/I mg/I ug/I ug/l ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print Signature of Permitte (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: 53.17 ft. Well Diamter: CWW-5 Screened Interval: 41.75 ft. to 51.08 ft. 4 inch Depth to Water Level: 7.58 ft. below measuring point. Measuring Point is 2.58 ft above land surface. For Groundwater Treatment Sys ems Check One; Influent (98) )C Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 7.0 , Specific Conductance 2004 uMhos Temp. 31.1 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : EXPIRATION DATE: UIC X 09/30/01 Rotary Distributor Land Application of Sludge Other GJ1 Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/14/99 Date sample analyzed: Laboratory Name: PCS PHOSPHATE 4/14/99 to 5/11/99 r.� Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD N/A mg/I Coliform: MF Fecal Coliform: MF Total N/A /100m1 N/A /100m1 (Note. Use MPN method for highly turbid samples) Dissolved Solids: Total 1308 pH (when TOC analyzed) 6.9 7.3 79.4 N/A N/A N/A Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 376.6 N/A N/A N/A mg/I nits mg/I mg/I mg/I mg/I mg/I Fe - Iron mg/I Hg - Mercury uMhos mg/I mg/I Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper K- Potassium Mg - Magnesium Mn - Manganese No and field acidified Yes n/a No N/A N/A 5.000 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/1 mg/1 mg/I mg/l u g/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Ni - Nickel 'N/A ug/I N/A ug/I N/A ug/I mg/l Other (Specify Compounds and Concentration Units) Fluoride 0.17 mg/I MIBK N/A ug/I Ag - Silver N/A ug/I N/A ug/I N/A ug/I Organics: (GC. GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) method# Pb - Lead Zn - Zinc Ammonia Nitrogen Se- Selenium Sodium vOc method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print ” Signature of Permittee (or Atithorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-6 Well Depth: 53.00 ft. Well Diamter: Screened Interval: 36.62 ft. to 50.88 ft. Depth to Water Level: Measuring Point is GALLONS 4 inch 7.24 ft. below measuring point. 2.92 ft above land surface. For Groundwater Treatmen Sys ems Check One: Influent (98) ,Effluent (99) of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 7.0 , Specific Conductance 1792 uMhos Temp. 32 oC, Odor NONE Appearance: CLEAR Mail Original to: PERMIT #: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH. NC 27626-0578 Phone: (919)733-3221 W10700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : L^ EXPIRATION DATE: UIC X 09/03/01 Rotary Distributor Other Land Application of Sludge LJ (:O Note: Values should reflect dissolved and E0 LO colloidal concentrations c._ Date sample collected: 4/14/99 `z Date sample analyzed: 4/14/99 to 5/11/99 i Laboratory Name: PCS PHOSPHATE , J Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1096 pH (when analyzed) 6.9 TOC 8.1 Chloride 120.1 Arsenic N/A Grease and Oils N/A Phenol N/A Sulfate 280.2 Specific Conductance Total Ammonia TKN as N N/A N/A N/A mg/I /100m1 /100m1 mg/I nits mg/I mg/I mg/1 mg/I mg/I mg/I uMhos mg/I mg/I n/a No and field acidified Yes n/a No Nitrite (NO2 as N) N/A mg/I Nitrate (NO3 as N) N/A mg/I Phosphorus: Total as P 11.950 mg/I Orthophosphate N/A mg/I Al - Aluminum N/A ug/I Ba - Barium N/A ug/I Ca - Calcium N/A ug/I Cd- Cadmium N/A ug/I Chromium: Total N/A ug/I Cu - Copper N/A ug/l N/A ug/I N/A ug/I K- Potassium N/A ug/I Mg - Magnesium N/A ug/I Mn - Manganese N/A ug/I Fe - Iron Hg - Mercury Ni - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen N/A , ug/I `-71 N/A ug/I N/A ug/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium 0.19 N/A N/A N/A N/A Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X VOC method# method# method# mg/I mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print Signature of Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-7 Screened Interval: 36.58 ft. to 50.83 ft. 4 inch Depth to Water Level: 6.74 ft. below measuring point. Measuring Point is 1.25 ft above land surface. For Groundwater Treatment Sys ems Check One: Influent (98) x: Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.7 , Specific Conductance 1196 uMhos Temp. 24.3 oC, Odor NONE Appearance: LT YELLOW Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: 09/03/01 UIC X Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 4/14/99 Date sample analyzed: 4/14/99 to 5/11/99 Laboratory Name: PCS PHOSPHATE Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note. Use MPN method for highly turbid samples) Dissolved Solids: Total 874 pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 7.1 7.5 74.1 N/A N/A N/A 215.3 N/A N/A N/A mg/I /100m1 /100m1 Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as Orthophosphate mg/I Al - Aluminum nits Ba - Barium mg/I Ca - Calcium mg/I mg/I mg/I mg/I Fe - Iron mg/I uMhos mg/I mg/1 Cd- Cadmium Chromium: Total Cu - Copper Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese n/a No and field acidified N/A N/A 4.450 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/I mg/1 mg/I mg/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I ug/I Yes n/a No Ni - Nickel N/A ug/I Pb - Lead N/A ug/I Zn - Zinc N/A ug/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Fluoride 0.19 mg/1 MIBK N/A ug/I Ag - Silver N/A ug/I N/A ug/l N/A ug/I Organics: (GC, GC/MS. HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) Se- Selenium Sodium VOC : method# method# : method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized Agent) Name and Title - Please type or print — 7 uth8,A: rae ,� 0�07 Signature of Permittee (or orized Agent) (Date)