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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_19990823 (2)GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORMZ(}/e, FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-1 Well Depth: 55.00 ft. Well Diamter: Screened Interval: Depth to Water Level: Measuring Point is GALLONS Field Analysis: pH Temp. 18.6 33,27 ft. to 52.68 ft. 4 inch 7.84 ft. below measuring point. 2.25 ft above land surface. of water pumped/bailed before sampling: 6.3 , Specific Conductance oC, Odor NONE For Groundwater Treatment Sys erns Check One: Influent (98) X Effluent (99) CONTINUOUS 2397 uMhos Appearance: CLEAR Mail Original to: PERMIT DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 IGH, NC 26-0578 Phone: (919)733-3221 WI0700012 EXPIRATION DATE: 09/30/01 Non-Dis, harge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 7/15/99 Date sample analyzed: 7/15/99 to 8/5/99 Laboratory Name: PCS PHOSPHATE Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate 2028 6.8 10.0 74.0 N/A N/A N/A Specific Conductance Total Ammonia TKN as N 723.8 N/A N/A N/A mg/I Nitrite (NO2 as N) /100m1 Nitrate (NO3 as N) /100m1 Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium mg/I units mg/I mg/I mg/I mg/I mg/I Fe - Iron mg/l uMhos mg/I mg/I No and field acidified Yes n/a No N/A N/A Pb - Lead 2.950 Zn - Zinc N/A Ammonia Nitrogen Cd- Cadmium Chromium: Total Cu - Copper Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/I Ni - Nickel mg/I mg/I mg/1 ug/I ug/I ug/I ug/I ug/I ug/I ug/l ug/I ug/l ug/I ug/I 7N/A {i1/1 I/A ug/I `:J/A o' ug/I — mg/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium 0.22 N/A N/A N/A N/A mg/I ug/l ug/I ug/I ug/I Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X (2) VOC : method# : method# : method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisionment for knowing violations. NOTE: G Lo GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee hori 1 Age t) Name -d Title - Please type or print ignature of rCermittee (or Authorized Agent) (Date) (GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-2 Well Depth: 52.15 ft. Well Diamter: 4 inch Screened Interval: 30.57 ft. to 49.82 ft. Depth to Water Level: 7.66 ft. below measuring point. For Groundwater Treatment Sys ems Check One: Influent (93) X Effluent (99) Measuring Point is 3.00 ft above land surface. GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.4 Specific Conductance 2419 uMhos Temp. 19.3 oC. Odor NONE Appearance: LT RUST ORANGE Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 09/30/01 Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: 7/15/99 7/15/99 to 8/5/99 r.) PCS PHOSPHATE , Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal Coliform: MF Total N/A /100m1 Nitrate (NO3 as N) N/A mg/I Ni - Nickel N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total pH (when analyzed) TOC 2072 mg/I Al - Aluminum 6.7 units Ba - Barium 10.5 mg/I Ca - Calcium Chloride Arsenic 106.1 mg/I Cd- Cadmium Grease and Oils Phenol Sulfate 4.650 mg/I N/A mg/I Pb - Lead Zn - Zinc N/A mg/I Ammonia Nitrogen N/A ug/I Other (Specify Compounds and Concentration Units) Yes n/a No N/A ug/I Fluoride N/A ug/I MIBK N/A ug/I Ag - Silver N/A mg/I Chromium: Total N/A mg/I Cu - Copper Specific Conductance Total Ammonia TKN as N N/A mg/I Fe - Iron 688.1 mg/I Hg - Mercury N/A ug/I N/A ug/I N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/1 Mn - Manganese Se- Selenium Sodium _ cr ug/I tN/A"6 ug/I N/A74 ug/I 0.19 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X N/A ug/I VOC : method# method# method# N/A ug/I mg/1 mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee . tho -. ge ame and Title - Please type or print gnatur- of Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-3 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 36.42 ft. to 50.67 ft. Depth to Water Level: 7.72 ft. below measuring point. Measuring Point is 3.08 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.4 , Specific Conductance 2242 uMhos Temp. 25.7 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 09/30/01 Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 7/15/99 7/15/99 to 8/5/99 G7 PCS PHOSPHATE 330 PARAMETERS: (Samples for metals were collected COD N/A Coliform: MF Fecal N/A Coliform: MF Total N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1788 pH (when analyzed) 6.9 TOC 7.7 Chloride 128.9 Arsenic N/A Grease and Oils N/A Phenol N/A Sulfate 547.4 Specific Conductance Total Ammonia TKN as N N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I uMhos mg/I mg/I unfiltered Yes Nitrite (NO2 as N) Nitrate (NO3 as N) n/a No and field acidified Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium 4.500 mg/I N/A mg/1 Ni - Nickel N/A mg/I Pb - Lead Zn - Zinc N/A mg/I Ammonia Nitrogen N/A ug/I Yes n/a No Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K- Potassium Mg - Magnesium Mn - Manganese N/A ug/I N/A ug/I N/A ug/I Cn .tw N/'ug/I N/P -, ug/I N/ ug/I mg/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver 0.20 N/A N/A N/A ug/I Se- Selenium N/A N/A ug/I Sodium N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC : method# N/A ug/I : method# method# mg/I ug/I ug/I ug/I ug/I I certify that, to the best of my knowledge and belief, the information submitted in this report is true, using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. false information, including the possibility of fines and imprisionment for knowing violations. accurate, and complete, and that the laboratory analytical data was produced I am aware that there are significant penalties for submitting NOTE: GW-59 Rev 4/98 0 C ?66 Brad A. Peacock - Manager, Environmental Affairs Permittee uthorize�tf�en '11ame and Title - Please type or print Z 5 77 (Date) gnature Permittee (or Authorized Agent) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-4 Well Depth: 53.00 ft. Well Diamter: 4 inch Screened Interval: 41.67 ft. to 50.92 ft. Depth to Water Level: 6.87 ft. below measuring point. Measuring Point is 2.75 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatrnent Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.2 , Specific Conductance 2163 uMhos Temp. 27.4 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED EXPIRATION DATE: UIC X 09/30/01 Lagoon Spray Field Rotary Distributor Other Remediation: Infiltration Gallery X Remediation : Land Application of Sludge Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 7/15/99 Date sample analyzed: 7/15/99 to 8/5/99 Cr) Laboratory Name: PCS PHOSPHATE u.1 Certification No(s) 330 c0 PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A mg/I /100m1 /100m1 Yes n/a Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 1772 mg/I Al - Aluminum pH (when analyzed) 6.7 units Ba - Barium TOC 7.8 mg/I Ca - Calcium Chloride 111.9 mg/I Cd- Cadmium No and field acidified Yes n/a No cn..:z. N/A mg/1 Ni - Nickel - N/@e "� ug/I N/A mg/I Pb - Lead 4_0 Nit ug/I 4.350 mg/I Zn - Zinc N/K ug/I N/A mg/I Ammonia Nitrogen N/A ug/I Arsenic N/A mg/I Chromium: Total Grease and Oils N/A mg/I Cu - Copper Phenol N/A mg/I Fe - Iron Sulfate 571.6 mg/I Hg - Mercury Specific Conductance Total Ammonia TKN as N N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese N/A ug/I N/A ug/I N/A ug/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A ug/I Se- Selenium N/A ug/I Sodium N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X 0.13 N/A N/A N/A N/A N/A ug/I VOC N/A ug/I : method# : method# : method# mg/I mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations NOTE: •CiV 9 C 66 GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of thorized nty4Game and Title - Please type or print rC L.j—t 7 Si ature ermittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 (hom pennl) Welt Identification Number (from Permit): CWW-5 Well Depth: 53.17 ft. Well Diamter: 4 inch Screened Interval: 41.75 ft. to 51.08 ft. Depth to Water Level: Measuring Point is 7.65 ft. below measuring point. 2.58 ft above land surface. For Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.4 , Specific Conductance 1698 uMhos Temp. 30 oC, Odor NONE Appearance: LT YELLOW Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery UIC X Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 7/15/99 7/15/99 to 8/5/99 PCS PHOSPHATE 330 ter to ns PARAMETERS: (Samples for metals were collected COD N/A Coliform: MF Fecal N/A Coliform: MF Total N/A (Note: Use MPN method for highly turbid samples) mg/I /100m1 /100m1 Dissolved Solids: Total 1348 mg/I pH (when analyzed) 6.9 units TOC 8.5 mg/1 Chloride 78.2 mg/I Arsenic N/A mg/I Grease and Oils N/A mg/I Phenol N/A mg/I Sulfate Specific Conductance Total Ammonia TKN as N 365.2 mg/I N/A uMhos N/A mg/l N/A mg/I unfiltered Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury Yes n/a No and field acidified Yes n/a No ': N/A mg/I Ni - Nickel N/ �" ~ —fir,5 g/l N/A mg/I Pb - Lead , .-N/Ac:; ug/I 6.050 mg/I Zn - Zinc teiN/Ao ug/I N/A mg/I Ammonia Nitrogen N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I N/A ug/I K- Potassium Mg - Magnesium Mn - Manganese N/A ug/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium 0.14 N/A N/A N/A N/A N/A ug/I Organics: (GC, GC/MS, HPLC) N/A ug/I (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X N/A ug/I VOC : method# method# method# mg/I mg/I ug/I ug/I ug/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (o Signature o uthorizecj,QgegtyName and Title - Please type or print ermittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 *9 ) Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-6 4 inch Screened Interval: 36.62 ft. to 50.88 ft. Depth to Water Level: 7.02 ft. below measuring point. Measuring Point is 2.92 ft above land surface. GALLONS of water pumped/bailed before sampling: For Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 1521 uMhos Temp. 31.1 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery EXPIRATION DATE: UIC X 09/03/01 Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 7/15/99 Date sample analyzed: 7/15/99 to 8/5/99 1V Das L c7 al Laboratory Name: PCS PHOSPHATE Certification No(s) 330 -11 PARAMETERS: (Samples for metals were collected unfiltered Yes COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1176 pH (when analyzed) 6.7 TOC 9.6 Chloride 93.3 Arsenic N/A Grease and Oils N/A Phenol N/A Sulfate Specific Conductance Total Ammonia TKN as N 287.9 N/A N/A N/A mg/I /100m1 /100m1 mg/I units mg/1 mg/I mg/I mg/I mg/I mg/I uMhos mg/I mg/I n/a No and field acidified Nitrite (NO2 as N) N/A mg/I Nitrate (NO3 as N) N/A mg/I N/PC ug/I Phosphorus: Total as P 16.150 mg/1 Orthophosphate N/A mg/I Ammonia Nitrogen mg/I Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units) Ba - Barium N/A ug/I Fluoride 0.17 mg/I Ca - Calcium N/A ug/I MIBK N/A ug/I Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I Chromium: Total N/A ug/I Se- Selenium N/A ug/I Cu - Copper N/A ug/I Sodium N/A ug/I N/A ug/I Organics: (GC, GC/MS, HPLC) Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.) K- Potassium N/A ug/I Report attached? Yes (1) No X (2) Mg - Magnesium N/A ug/I VOC : method# Fe - Iron Mn - Manganese N/A ug/I Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No x < va N/ ug/I method# method# N/A ug/I I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: e°uEZ66 GW-59 Rev 4/98 Brad A. Peacock - Manager, Environmental Affairs Permittee (of Authorized ent) Name and Title - Please type or print i ",? Signature of (or Authorized Agent) (Date) IGROIJNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-7 Well Depth: 53.00 ft. Well Diamter: Screened Interval: 36.58 ft. to 50.83 ft. Depth to Water Level: 4 inch 6.96 ft. below measuring point. Measuring Point is 1.25 ft above land surface. For Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.4 , Specific Conductance 1209 uMhos Temp. 23.9 oC, Odor NONE Appearance: RUST BROWN Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT P.O. BOX 29578 RALEIGH, NC 27626-0578 Phone: (919)733-3221 PERMIT #: WI0700012 Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Remediation : EXPIRATION DATE: UIC X 09/03/01 Rotary Distributor Other Remediation: Infiltration Gallery Land Application of Sludge LD Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: G7 7/15/99 N C71 7/15/99 to 8/5/99 �. PCS PHOSPHATE Certification No(s) 330 PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Coliform: MF Fecal N/A /100m1 Coliform: MF Total N/A /100m1 Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 922 mg/I Al - Aluminum pH (when analyzed) 6.1 units Ba - Barium TOC 7.9 mg/I Ca - Calcium Chloride 77.3 mg/I Arsenic N/A mg/I Grease and Oils N/A mg/I Phenol N/A mg/I Sulfate mg/1 Specific Conductance Total Ammonia TKN as N 229.0 N/A N/A N/A uMhos mg/l mg/1 K- Potassium Mg - Magnesium Mn - Manganese Yes n/a No and field acidified Yes n/a No to Nitrite (NO2 as N) N/A mg/I Ni - Nickel NI, ug/I Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I 5.200 mg/I Zn - Zinc N/A ug/I N/A mg/1 Ammonia Nitrogen mg/l N/A ug/I Other (Specify Compounds and Concentration Units) N/A ug/I Fluoride 0.17 mg/I N/A ug/I MIBK N/A ug/I Cd- Cadmium N/A ug/I Ag - Silver N/A ug/I Chromium: Total N/A ug/I Se- Selenium N/A ug/I Cu - Copper N/A ug/I Sodium N/A ug/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC) Hg - Mercury N/A ug/l (Specify test method #. Attach lab report.) N/A ug/I Report attached? Yes (1) No X (2) N/A ug/I VOC N/A ug/I : method# method# method# I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete: and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 C 8C366 Brad A. Peacock - Manager, Environmental Affairs Permittee • uthori -• gent) Name and Title - Please type or print 7_23 _7t' Signature of Permittee (or Authorized Agent) (Date)