WI0700012_Monitoring (Report)_20031125 (2)

DIVISION OF WATER QUALITY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jimmy Hardy
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
55.00 ft. Well Diamter:
CWW-1
Screened Interval: 33.27 ft. to 52.68 ft.
4 inch
Depth to Water Level: 6.49 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2202 uMhos
Temp. 20.1 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
C4.)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/16/03
10/16/03 to 10/29/03
CD
W
C.1
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1890
pH (when analyzed) 6.3
TOC 6.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
79.7
N/A
N/A
N/A
660.2
N/A
N/A
N/A
/100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
/100m1 Phosphorus: Total as P
Orthophosphate
mg/1
units
mg/I
mg/I
mg/I
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
2.575 mg/l
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/l Ammonia Nitrogen
Yes nla No )
N/A mg/I
N/A mg/I
N/A mg/I
9 N// ug/I
N/A-1 ug/I
N/A -.ug/I
mg/1
Other (Specify Compounds and Concentration Uniti))
Fluoride --D 0.20 mg/I
MIBK -= N/A,7 mg/I
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
+.J
Ni
N!A v mg/l
Na mg/I
NWP, ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
X (2)
Report attached? Yes
N/A mg/I VOC
N/A mg/1
(1) No
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
2.M 44tikK A)g- 1V2C7,3
Signature of Permittee (or Authomzed Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
0,om
Mail Original
to:
Well Identification Number (from Permit):
Well Depth:
52.15 ft. Well Diamter:
CWW-2
Screened Interval: 30.57 ft. to 49.82 ft.
4 inch
Depth to Water Level: 7.49 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2320
uMhos
Temp. 20.3 oC, Odor NONE Appearance:
CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Remediation; Infiltration Gallery
Spray Field X Remediation : CJ
Rotary Distributor
Other
Land Application of Sludg
c.)
,)
_3
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1920 mg/I
pH (when analyzed) 6.3 units
TOC 8.0 mg/I
Chloride 89.4 mgll
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate 1629.1 mg/1
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/1
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
15.250 mg/I
N/A mg/1 Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
Yes n/a No )
N/A ug/I
ug/I
N/A mg/I Ammonia Nitrogen
/A ug/I
N/A mg/I Other (Specify Compounds and Concentration Units)N,,
N/A mg/1
N/A mg/I
-rng/I
mg/1
mg/I
N/A mg/1 nng/I
v
Se- Selenium r. N/A7; - ing/I
N/A mg/I Sodium N/Ar ; ug/I
N/A mg/i Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Fluoride
MIBK
Ag - Silver
N/A mg/I VOC
N/A mg/1
(1) No X
method#
method#
method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of uthorized Agent) Name and Title - Please type orprint /
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
4 inch
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: 7.10 ft. below measuring point.
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check one:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2400
uMhos
Temp. 23.9 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
W
G)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name:
Certification No(s) 330 10
q
CD
W
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1890
pH (when analyzed) 6.3
TOC 7.2
Chloride 112.0
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1270.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
No and field acidified
N/A
N/A
2.800
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/►
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
C► N/A ug/l
c,J
NAA . ug/I
Nk4 ug/l
r.� mg/I
Other (Specify Compounds and Concentration Urfit
Fluoride
MIBK
Ag - Silver
Q 0.96 mg/I
i J
Se- Selenium N NIA mg/1
Sodium • • N/A ug/I
N/A mg/I
t\i'A _ mg/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
mg/I VOC : method#
mg/I
method#
: method#
I certify thatto the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
P rmittee (of Aut rized Agent) Name and Title - Please type or print
tn. by M(&J Ock3
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jimmy Hardy
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level: 7.48 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.3 , Specific Conductance 2671 uMhos
Temp. 27.1 oC, Odor NONE
Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1
Yes n/a
Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1990
6.3
9.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
114.0
N/A
N/A
N/A
625.1
N/A
N/A
N/A
mg/I
units
mg/I Ca - Calcium
mg/I
mg/1
mg/I
mg/I Fe - Iron
mg/l Hg - Mercury
uMhos
mg/I
mg/1
Al - Aluminum
Ba - Barium
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field
N/A
N/A
5.500
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
acidified Yes nla No )
mg/I Ni - Nickel N/A- ug/I
mg/1 Pb - Lead C N/A. ug/I
mg/l Zn - Zinc ;` Nth ug/l
ry
mg/I Ammonia Nitrogen crt mg/I
mg/I Other (Specify Compounds and Concentration Units), -
mg/l Fluoride It: 0.I1:.;mg/1
mg/I MIBK r;J WIT mg/I
mg/I Ag - Silver rV N/Xa. mg/I
mg/1 Se- Selenium N/Ps mg/I
mg/I Sodium N/A ug/I
mg/I Organics: (GC, GC/MS, HPLC)
mg/I (Specify test method #. Attach lab report.)
mg/I Report attached? Yes (1) No X (2)
mg/I VOC method#
mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of P athorized Agent) Name and Title - Please type or print
r7D(A) az ///.2.r'�03
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO.. INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-5
Well Depth:
53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level:
7.32 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2160 uMhos
Temp. 29.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
()
G)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
V
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1400
6.4
6.9
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
80.2
N/A
N/A
N/A
379.7
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
uMhos
mg/1
mg/I
No and field
N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
8.500
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I VOC
mg/1
acidified Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
N/A ug/I
o N/A ug/I
c.a
_ mg/I
Other (Specify Compounds and Concentration UnUj
Fluoride
+v
MIBK 1
0.12
Ni/pk`
Ag - Silver N/A
Se- Selenium tl�
Sodium r ,. 1111A
Organics: (GC, GC/MS, HPLC) r
(Specify test method #. Attach lab i'L ortt)
Report attached? Yes (1) No `X (2)
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
ug/I
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Prmittee (of Authorized Agent) Name and Title - Please type or print
h tam ti r74 «/2 S /4.3
Signature of Permittee (or Authorizeff Agents (Date)
I /

GROUNDWATER QUALITY MONITORING:
,COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
CroTr
Well Identification Number (from Permit):
Well Depth:
53.00 ft. Well Diamter:
CWW-6
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.56 ft. below measuring point.
2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2327 uMhos
Temp. 30.8 oC, Odor NONE Appearance: LT YELLOW CLDY
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: W10700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I
/100m1
/100m1
Yes n/a No and field acidified
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
1540 mg/I Al - Aluminum
6.4 units Ba - Barium
15.3 mg/I Ca - Calcium
Chloride
Arsenic
92.2 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/l
N/A mg/I
36.250 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
1195.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
Ammonia Nitrogen
N/A ug/I
N/= ug/I
Ni • ug/I
='' 57 -- mg/1
CJ
Other (Specify Compounds and Concentration uniti4t-
Fluoride
MIBK
Ag - Silver
N#A
mg/I
mg/I
mg/I
N/A mg/I Se- Selenium N/A mg/I
N/A mg/I Sodium t\t/A - ug/I
ry N/A mg/I Organics: (GC, GC/MS, HPLC) ==
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
method#
N/A mg/I VOC
N/A mg/I
: method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Au orized Agent) Name and Title - Please type or print
e(
P.
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): CWW-7
Well Depth:
53.00 ft. Well Diamter:
Screened Interval: 36.58 ft. to 50.83 ft.
4 inch
Depth to Water Level: 7.31 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.6 , Specific Conductance 1170 uMhos
Temp. 23.8 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
10/16/03 to 10/29/03
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1
805 mg/1
6.6 units
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
5.7 mg/I Ca - Calcium
62.8 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
1159.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
4.100
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/1
mg/1
mg/I
mg/1
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
Yes n/a No )
Ni - Nickel N/A
Pb - Lead
Zn - Zinc NIA
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride ,, 01;$
MIBK ;N
Ag - Silver Ill
Se- Selenium psi N/A
Sodium ry rN/A
Organics: (GC, GC/MS, HPLC) v
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/1
mg/I
mg/1
mg/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and completeand that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Aut rized Agent) Name and Title - Please type or print
A h7 D,bia /z /L)3
Signature of Permittee (or Authorized Agent) (Date)