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HomeMy WebLinkAboutWI0700012_Monitoring (Report)_20020226• GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: Well Locations/Site Name: Tank Farm Well Identification Number (from Permit): Well Depth: 55.00 ft. Well Diamter: (252)322-8154 No. of Wells to be Sampled Screened Interval: 33.27 ft. to 52.68 ft. Depth to Water Level: 5.20 ft. below measuring point. Measuring Point is 2.25 ft above land surface. 18 Fo Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.2 , Specific Conductance 2141 uMhos Temp. 19.2 oC, Odor NONE Appearance: CLEAR PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Remediation: Infiltration Galley) G7 Lagoon Spray Field Rotary Distributor Other X Remediation Land Application of Sludge - T1 rn W Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) ram) 1/24/02 - 1 /24/02 to 2/19/02- PCS PHOSPHATE ara-tNVIRQNMENT 1 330 10 c_o PARAMETERS: (Samples for metals were collected unfiltered COD N/A mg/I Nitrite (NO2 as N) Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) Yes n/a No and field acidified N/A mg/I N/A mg/1 Coliform: MF Total N/A /100m1 Phosphorus: Total as P (Note. Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total 1884 mg/I Al - Aluminum pH (when analyzed) 6.6 units Ba - Barium TOC 7.2 mg/I Ca - Calcium Chloride 85.9 mg/I Cd- Cadmium 2.280 mg/I Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No N/A mg/I Ammonia Nitrogen N/A mg/I Arsenic N/A mg/I Chromium: Total Grease and Oils N/A mg/I Cu - Copper Phenol N/A mg/I Fe - Iron Sulfate 674.9 mg/I Hg - Mercury Specific Conductance Total Ammonia TKN as N N/A uMhos K- Potassium N/A mg/I N/A mg/I N/A mg/I N/A ug/I N/A ug/I N/A ug/I mg/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A mg/I Se- Selenium N/A mg/I N/A mg/I N/A mg/I N/A mg/1 Mg - Magnesium N/A mg/I Mn - Manganese N/A mg/I N/A mg/I N/A mg/1 0.25 mg/I N/A mg/I N/A mg/I N/A mg/l Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No VOC : method# method# method# N/A ug/I X (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager. Environmental Affairs P ittee (of Authorized -[r yvI ame and Title - Please type or print Signatt /of Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): CWW-2 Well Depth: 52.15 ft. Well Diamter: 4 inch Screened Interval: 30.57 ft. to 49.82 ft. Depth to Water Level: 7.52 ft. below measuring point. Measuring Point is 3.00 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH 7.2 , Specific Conductance For Groundwater Treatrnent Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS 1076 uMhos Temp. 19.3 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gailern Spray Field X Remediation : N Rotary Distributor Land Application of Sludge Other C3 CA u3 Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/24/02 1/24/02 to 2/19/02o . PCS PHOSPHATE arftfENWRONMENT 1 330 10 r>.i PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A mg/1 /100m1 /100m1 Yes n/a Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P (Note: Use MPN method for highly turbid samples) Orthophosphate Dissolved Solids: Total pH (when analyzed) TOC 716 mg/1 Al - Aluminum 7.6 units Ba - Barium 4.5 mg/I Ca - Calcium Chloride Arsenic 157.2 mg/1 Cd- Cadmium Grease and Oils Phenol Sulfate N/A mg/I Chromium: Total N/A mg/I Cu - Copper Specific Conductance Total Ammonia TKN as N N/A mg/1 Fe - Iron 20.0 mg/1 Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese No and field acidified Yes n/a No N/A N/A 8.450 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/I mg/I Ni - Nickel Pb - Lead mg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/1 mg/I mg/I m g/1 mg/I mg/1 mg/1 mg/1 mg/I mg/I mg/1 w if/A N/A N/A Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver __ Se- Selenium Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X 0.53 N/A N/A N/A N/A VOC method# method# method# ug/I ug/I ug/I mg/I mg/I mg/I mg/I mg/1 ug/I (2) certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager . Environmental Affairs Per e of Authorized7Neand Title -Please type or print wit 2—/z2— ignature ermittee (or Authorized Agent) (Date GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 �- Well Identification Number (from Permit): CWW-3 Well Depth: 53.00 Screened Interval: 36.42 ft. to 50.67 ft. Depth to Water Level: 5.85 ft. below measuring point. Measuring Point is ft. Well Diamter: 4 inch 3.08 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH 6.2 , Specific Conductance Temp. 25.3 oC, Odor NONE Fo Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS 2653 uMhos Appearance: CLEAR PERMIT #: WI0700012 EXPIRATION DATE: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED O Lagoon Remediation: Infiltration Galleg Spray Field X Remediation : UIC X 09/30/01 Other Rotary Distributor Land Application of S,tudg I n iA k.D CD Note: Values should reflect dissolved and r>> colloidal concentrations Date sample collected: 1/24/02 Date sample analyzed: 1/24/02 to 2/19/02- Laboratory Name: PCS PHOSPHATEa h1VIRONMENT 1 Certification No(s) 330 10 - PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1922 pH (when analyzed) 6.7 TOC 6.8 Chloride Arsenic Grease and Oils mg/I Nitrite (NO2 as N) /100m1 /100m1 Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate mg/I Al - Aluminum units Ba - Barium mg/1 Ca - Calcium 215.5 mg/I Cd- Cadmium N/A mg/I Chromium: Total N/A mg/I Cu - Copper Phenol Sulfate Specific Conductance Total Ammonia TKN as N N/A mg/I Fe - Iron 559,1 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese N/A mg/I Yes n/a No and field acidified Yes n/a No N/A mg/I Ni - Nickel N/A mg/l Pb - Lead 4.125 mg/I Zn - Zinc N/A mg/I Ammonia Nitrogen N/A mg/I N/A mg/I N/A mg/I N/A mg/I N/A ug/I N/A ug/I N/A ug/I mg/I Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A mg/I Se- Selenium 0.19 mg/I N/A mg/I N/A mg/I N/A mg/1 N/A mg/I Sodium NIA mg/I Organics: (GC, GC/MS, HPLC) N/A mg/1 (Specify test method #. Attach lab report.) N/A mg/I Report attached? Yes (1) No X (2) N/A ug/I N/A mg/I VOC : method# method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Peittee (of Authorized Agent) Npme and Title - Please type or print Signatuf•Permittee (or Authorized Agent) (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-4 4 inch Screened Interval: 41.67 ft. to 50.92 ft. Depth to Water Level: 6.76 ft. below measuring point. Measuring Point is 2.75 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH 6.5 , Specific Conductance Temp. 26.8 oC, Odor NONE For Groundwater Treatrnent Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS 2568 uMhos Appearance: CLEAR PERMIT #: WI0700012 EXPIRATION DATE: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X UIC X 09/30/01 Rotary Distributor Other N O C11 Remediation: Infiltration Gallery..D Remediation : C� Land Application of Sludge Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/25/02 1/25/02 to 2/19/02-r) . PCS PHOSPHATE anctENVIRONMENT 1 330 10 N N PARAMETERS: (Samples for metals were collected unfiltered COD Nitrite (NO2 as N) Coliform: MF Fecal Nitrate (NO3 as N) Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 1872 pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate mg/I /100m1 /100m1 Yes n/a No and field acidified Yes n/a No N/A mg/1 Ni - Nickel N/A mg/I Pb - Lead Phosphorus: Total as P Orthophosphate mg/1 Al - Aluminum 6.9 units Ba - Barium 7.3 mg/1 Ca - Calcium 136.5 mg/I Cd- Cadmium 4.650 mg/1 Zn - Zinc N/A N/A N/A N/A mg/I Ammonia Nitrogen N/A mg/I N/A mg/I N/A mg/I N/A mg/I N/A mg/I Chromium Total N/A mg/I Cu - Copper Specific Conductance Total Ammonia TKN as N N/A mg/I Fe - Iron 626.6 mg/I Hg - Mercury N/A uMhos K- Potassium N/A mg/I Mg - Magnesium N/A mg/I Mn - Manganese Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver N/A mg/I Se- Selenium ug/I ug/I ug/I mg/I 0.13 mg/I N/A mg/I N/A mg/I N/A mg/I N/A mg/I Sodium N/A mg/I Organics: (GC. GC/MS. HPLC) N/A mg/I (Specify test method #. Attach lab report.) N/A mg/I Report attached? Yes (1) No X (2) N/A ug/1 N/A mg/1 VOC : method# method# method# N/A mg/I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Permi�e (of Authorized Agent) m and Title - Please type or print ture of, rm ee (or Authorized Agent) (Date) gna itt GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled Well Identification Number (from Permit): CWW-5 Well Depth: 53.17 ft. Well Diamter: 4 inch Screened Interval: 41.75 ft. to 51.08 ft. Depth to Water Level: 7.22 ft. below measuring point. Measuring Point is 2.58 ft above land surface. GALLONS of water pumped/bailed before sampling: 18 Fo Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS Field Analysis: pH 6.1 , Specific Conductance 2138 uMhos Temp. 29.4 oC, Odor NONE Appearance: CLEAR Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01 Non -Discharge UIC X NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field X Rotary Distributor Other Remediation: Infiltration Gallerb Remediation : Land Application of SI rlj e Q Note: Values should reflect dissolved and colloidal concentrations Date sample collected: Date sample analyzed: Laboratory Name: Certification No(s) 1/24/02 1/24/02 to 2/19/02 rs7 PCS PHOSPHATE and R VIRONMENT 1 330 10 PARAMETERS: (Samples for metals were COD Coliform: MF Fecal Coliform: MF Total N/A N/A N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC 1456 6.6 7.7 Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 87.2 N/A N/A N/A 468.7 N/A N/A NIA collected unfiltered Yes n/a mg/l Nitrite (NO2 as N) /100m1 Nitrate (NO3 as N) No and field acidified Yes n/a No N/A mg/l /100m1 Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium mg/I units mg/1 Ca - Calcium mg/I mg/I mg/I mg/I Fe - Iron mg/I Hg - Mercury uMhos mg/I mg/I Cd- Cadmium Chromium: Total Cu - Copper 6.750 mg/l Ni - Nickel N/A ug/I N/A mg/1 Pb - Lead N/A ug/I Zn - Zinc N/A ug/1 N/A mg/I Ammonia Nitrogen mg/I N/A mg/I Other (Specify Compounds and Concentration Units) N/A mg/I Fluoride 0.16 mg/1 N/A mg/I MIBK N/A mg/I N/A mg/1 Ag - Silver N/A mg/I N/A mg/1 Se- Selenium N/A mg/I N/A mg/1 Sodium N/A ug/I Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) N/A mg/I Report attached? Yes (1) No X (2) N/A mg/1 N/A mg/I K- Potassium Mg - Magnesium Mn - Manganese N/A mg/1 N/A mg/I VOC method# method# method# I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Permittee (of Authorized AgeJJ.4- e and Title - Please type or print SignatuyPermittee (or Authorized Agent) (Date) 5 OS 0 2 a C4 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18 Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-6 4 inch Screened Interval: 36.62 ft. to 50.88 ft. Depth to Water Level: 6.57 ft. below measuring point. Measuring Point is 2.92 ft above land surface. GALLONS of water pumped/bailed before sampling: Field Analysis: pH 6.1 , Specific Conductance Fo Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) CONTINUOUS 2038 uMhos Temp. 29.6 oC, Odor NONE Appearance: CLEAR PERMIT #: WI0700012 EXPIRATION DATE: UIC X Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED P\l 09/03/01 Other Lagoon Remediation: Infiltration Gallet'Q t.- ui Spray Field X Remediation : r:. Rotary Distributor Land Application of Sludge ry Note: Values should reflect dissolved and - colloidal concentrations („ _ v Date sample collected: 1/24/02 Date sample analyzed: 1/24/02 to 2/19/cj C, Laboratory Name: PCS PHOSPHATE and ENVWRONMENT 1 Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal Coliform: MF Total (Note: Dissolved Solids: Total pH (when analyzed) TOC Chloride Arsenic Grease and Oils Phenol Sulfate N/A N/A N/A Use MPN method for highly turbid samples) 1380 6.7 mg/1 /100m1 /100m1 Yes nia Nitrite (NO2 as N) Nitrate (NO3 as N) Phosphorus: Total as P Orthophosphate mg/I Al - Aluminum units Ba - Barium 9.2 mg/I Ca - Calcium 88.9 N/A N/A N/A 465.9 N/A N/A N/A Specific Conductance Total Ammonia TKN as N mg/1 Cd- Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/1 Fe - Iron mg/1 Hg - Mercury uMhos K- Potassium mg/I Mg - Magnesium mg/1 Mn - Manganese No and field acidified N/A N/A 6.250 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A mg/1 mg/1 mg/1 mg/1 mg/I mg/I m g/I mg/1 mg/1 mg/I m g/l mg/1 mg/1 mg/1 VOC mg/1 Ni - Nickel Pb - Lead Zn - Zinc Yes n/a No N/A N/A N/A Ammonia Nitrogen Other (Specify Compounds and Concentration Units) Fluoride MIBK Ag - Silver Se- Selenium Sodium Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X 0.16 N/A N/A N/A N/A method# method# method# ug/I ug/I ug/I mg/I mg/I mg/I mg/I mg/1 ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Peunittee (of Authorized A nt) ame and Title - Please type or print Signaty of Permittee (or Authorized Agent) (Date) CO N CO Ai SO cD 0 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORTING FORM Mail Original to: DIVISION OF WATER QUALITY GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT 1636 Mail Service Center RALEIGH, NC 27699-1636 Phone: (919)733-3221 FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division Permit Name (if different): Facility Addresss: P.O. Box 48 Aurora, NC 27806 County: Beaufort Contact Person: Jimmy Hardy Telephone: (252)322-8154 Well Locations/Site Name: Tank Farm No. of Wells to be Sampled '18 Well Identification Number (from Permit): Well Depth: 53.00 ft. Well Diamter: CWW-7 Screened Interval: 36.58 ft. to 50.83 ft. Depth to Water Level: Measuring Point is 4 inch 6.36 ft. below measuring point. 1.25 ft above land surface. Fo Groundwater Treatment Sys ems Check One: Influent (98) X Effluent (99) GALLONS of water pumped/bailed before sampling: CONTINUOUS Field Analysis: pH 6.3 , Specific Conductance 1247 uMhos Temp. 24.2 oC, Odor NONE Appearance: CLEAR PERMIT #: WI0700012 EXPIRATION DATE: UIC X Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED 09/03/01 Lagoon Remediation: Infiltration Galler= Spray Field X Remediation : Rotary Distributor Land Application of Sludge Other Note: Values should reflect dissolved and colloidal concentrations Date sample collected: 1/24/02 - Date sample analyzed: 1/24/02 to 2119102: ' Laboratory Name: PCS PHOSPHATE and-HNVIRONMENT 1 Certification No(s) 330 10 G? PARAMETERS: (Samples for metals were collected unfiltered COD Coliform: MF Fecal N/A N/A Coliform: MF Total N/A (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 852 pH (when analyzed) 6.8 TOC 6.1 Chloride Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia TKN as N 79.7 N/A N/A N/A 199.8 N/A N/A N/A mg/1 /100m1 /100m1 mg/I units mg/I mg/I mg/I mg/I mg/I mg/I uMhos mg/I m g/1 Nitrite (NO2 as N) Nitrate (NO3 as N) Yes n/a No and field acidified Yes n/a No N/A mg/I Ni - Nickel Phosphorus: Total as P Orthophosphate Al - Aluminum Ba - Barium Ca - Calcium 3.150 mg/1 N/A mg/I Pb - Lead Zn - Zinc N/A mg/I Ammonia Nitrogen N/A mg/1 Other (Specify Compounds and Concentration Units) Cd- Cadmium Chromium: Total Cu - Copper Fe - Iron N/A mg/I Fluoride N/A mg/I MIBK N/A mg/I Ag - Silver N/A mg/I Se- Selenium N/A mg/I Sodium N/A mg/I Hg - Mercury N/A mg/I K- Potassium Mg - Magnesium Mn - Manganese N/A mg/I N/A mg/I N/A mg/I N/A N/A N/A 0.18 N/A N/A N/A N/A Organics: (GC, GC/MS, HPLC) (Specify test method #. Attach lab report.) Report attached? Yes (1) No X VOC method# method# method# ug/I ug/I ug/I mgll mg/I mg/I mg/I mg/I ug/I (2) I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false informationincluding the possibility of fines and imprisionment for knowing violations. NOTE: GW-59 Rev 4/98 Terry L. Baker - Manager, Environmental Affairs Per Signatur ee (of Authorized Age Na e and Title - Please type or print (D e) Permittee (or Authorized Agent)