WI0700012_Monitoring (Report)_20030528

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.23 ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2009 uMhos
Temp. 18.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01/15/08
Other
w
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
Ce.)
4/21/03
4/21/03 to 5/2/03
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1508
pH (when analyzed) 6.3
TOC 10.5
Chloride 65.0
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 560.0
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I
units
mg/I Ca - Calcium
mg/l Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/l Fe - Iron
mg/I Hg - Mercury
136.500 mg/I
Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/1
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units) •7i.
Fluoride 0! 2 XI
MIBK N7A �
Ag - Silver N
N/A.; ug/I
N/Ao ug/I
„ pi/A
f �j�ig/l
N/Q . ug
N/A mg/l Organics: (GC, GC/MS, HPLC) i
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker - Manager, Environmental Affairs
Per if = •f Authorized Age
Na rr and Title - Please type or p_r-nt
6 zip
d3
GW-59 Rev 4/98
ignature
ermittee (or Authorized Agent)
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
23.00 ft. Well Diamter:
SWW-2
Screened Interval: 18.80 ft. to 21.63 ft.
4 inch
Depth to Water Level: 7.67 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2081 uMhos
Temp. 19 oC, Odor NONE Appearance: CLEAR
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
01/15/08
Non -Discharge UIC X
NPDES Q
TYPE OF PERMITTED OPERATION BEING MONITORED w '
Lagoon Remediation: Infiltration GJery
Spray Field X Remediation :
Rotary Distributor
Other
Land Application of Sludge
(.3
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/03
Date sample analyzed: 4/21/03 to 5/2/03
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1604 mg/I Al - Aluminum
6.4 units Ba - Barium
8.4 mg/I Ca - Calcium
Chloride
Arsenic
48.0 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/1 Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
692.5 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
and ENVIRONMENT 1
N/A mg/I Ni - Nickel
65.500 mg/I
N/A mg/1 Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Yes n/a No )
N/A mg/1
N/A mg/I
N/A . ug/I
N/A - ug/I
5/A :•-)ug/I
Other (Specify Compounds and Concentration Units) 4
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium N/A� mom,
N/A mg/I Sodium N/A '' ug/��
N/A mg/I Organics: (GC, GC/MS, HPLC) i x.
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
0.1
/
Grcl
U
N/A mg/I VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
5ignatu 'er (orAgent)
Terry L. Baker - Manager, Environmental Affairs
Per•ee (of Authorized Ag ) N e and Title - Please type or print
mittee Authorized A ent (Da0,3

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
(born
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter:
Screened Interval: 20.17 ft. to 23.00 ft.
4 inch
Depth to Water Level: 6.52 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1606 uMhos
Temp. 21.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED O
Lagoon Remediation: Infiltration GGery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Other
!11
Rotary Distributor Land Application of Sludge
O
w
rn
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/21/03
4/21/03 to 5/2/03
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note Use MPN method for highly turbid samples) Orthophosphate
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
Dissolved Solids: Total
pH (when analyzed)
TOC
1380 mg/I Al - Aluminum
6.1 units Ba - Barium
7.8 mg/I Ca - Calcium
Chloride
Arsenic
37.0 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/I Pb - Lead
93.250 mg/1 Zn - Zinc
Yes n/a No )
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
516.5 mg/I Hg - Mercury
N/A mg/I
N/A ug/I
N/A ug/I
ug/I
tg/I
Other (Specify Compounds and Concentration Units)C c":=
Fluoride 069 /l
M I B K frftl
Ag - Silver /A
Se- Selenium
N/A mg/I Sodium
N/A uMhos K- Potassium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #.
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
cog
N/Qt u''
Attach lab report.) !`�
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per, s i. ..4of Authorize d AgNe and Title - Please type or print
(Dat
Signaturer flee (or uthorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-4
Well Depth:
25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
4 inch
10.73 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatrnent
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2472 uMhos
Temp. 28.5 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED i-
Lagoon Remediation: Infiltration GaII!
Spray Field X Remediation : Cfl
Rotary Distributor Land Application of Sludge cam)
C.w)
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/21/03
4/21/03 to 5/2/03
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I
N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1828
6.1
9.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
35.6
N/A
N/A
N/A
837.7
N/A
N/A
N/A
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/I Fe - Iron
Al - Aluminum
Ba - Barium
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
136.500 mg/I
N/A mgll
N/A mg/I
N/A mg/I
N/A mg/I
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/J= ug/I
QN/AA ug/I
r': fig/I
rttg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I VOC
N/A mg/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X (2)
method#
: method#
method#
N
N/A= ugfE
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per . Authorized Ag ggl) Ne and Title - Please type or grin
L
Signatur ermittee (or Authorized Agent)
(Da 1 (Da )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.60 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTNUOUS
Field Analysis: pH 6.2 , Specific Conductance 2798 uMhos
Temp. 28.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon Remediation:
Spray Field X Remediation :
Rotary Distributor
Other
Ct
'
Infiltration Gal107
Ul
C3
C,.)
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/03
Date sample analyzed: 4/21/03 to 5/2/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1920
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.2
11.3
52.3
N/A
N/A
N/A
880.3
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1
/100m1
Nitrate (NO3 as N)
No and field acidified
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
Cd- Cadmium
Chromium: Total
Cu - Copper
86.250 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
5I/Acu/1
A it
`'t
r' -
O. /1
N/Aa ml:-
N/A-, ' m
N/A mg//y
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
N/A ug/I
N/A mg/I
: method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per tee (of Authorized A.en
Signature rmittee (or Authorized Agent)
and Title - Please type or print 3
(Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jimmy Hardy
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
SWW-6
Well Depth: 26.00 ft. Well Diamter: 4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.93 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2709
uMhos
Temp. 27.4 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor
Other
Remediation: Infiltration Gary
Land Application of Sludgj
GJ
0
[.]
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/03
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
4/21/03 to 5/2/03
PCS PHOSPHATE
CO
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note' Use MPN method for highly turbid samples)
Dissolved Solids: Total 2164
pH (when analyzed) 6.1
TOC 15.2
Chloride 95.7
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
890.7
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I Pb - Lead
84.000 mg/I Zn - Zinc
Yes n/a No )
N/A mg/I Ammonia Nitrogen .-p m§
N/A mg/I Other (Specify Compounds and Concentration Units) 3 s
N/A mg/1 Fluoride 0.03rng/I�',
N/A mg/I MIBK N/A g/I ',,
N/A mg/I Ag - Silver N/A mg/I `
N/A mg/I Se- Selenium N/A mg/I
N/A mg/I Sodium N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I
: method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker - Manager, Environmental Affairs
Per r trit tee jof Authorized Age) Nme and Title - Please type or pript
6.'43
GW-59 Rev 4/98
ignatur'gfWer
ittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth:
29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: 7.21 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 1005 uMhos
Temp. 23.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
O
W I
Remediation: Infiltration Galfdly
X Remediation : CA)
Land Application of Sludge C)
CA)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/03
Date sample analyzed: 4/21/03 to 5/2/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
mg/I
/100m1
/100m1
No and field acidified
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/1
Phosphorus: Total as P 57.750 mg/I
Orthophosphate N/A mg/I
796 mg/I Al - Aluminum N/A mg/I
5.9 units Ba - Barium N/A mg/1
8.0 mg/I Ca - Calcium N/A mg/I
73.7 mg/I Cd- Cadmium N/A mg/I
Grease and Oils
N/A mg/I Chromium: Total N/A mg/l
N/A mg/I Cu - Copper N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron N/A mg/I
163.6 mg/I Hg - Mercury N/A mg/I
N/A uMhos K- Potassium N/A mg/I
N/A mg/I Mg - Magnesium N/A mg/I
N/A mg/I Mn - Manganese N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
N
0.0 mg
N/A )mg/f
N/A tmg/I g
N/A `fig/I
N/A ug/I
. method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of tines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per (of Authorized Ageand Title - Please type or print,
Signature p ermfttee (or Authorized Agent) ' (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level:
Measuring Point is
2 inch
4.05 ft. below measuring point.
3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.1 , Specific Conductance 638 uMhos
Temp. 20.3 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/22/03
4/22/03 to 5/2/03
PCS PHOSPHATE and NVIRONMENT 1
330 10 co) to
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
/100m1 Phosphorus: Total as P
Orthophosphate
464 mg/I Al - Aluminum
7.0 units Ba - Barium
5.9 mg/I Ca - Calcium
Chloride
Arsenic
10.5 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
0.302 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/l Pb - Lead
Zn - Zinc
Yes n/a No) -`'--'2
,&/A
lc -
Ammonia Nitrogen W tr F;
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
N/A mg/I
N/A mg/I
N/A mg/l
52.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
Se- Selenium
Sodium
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
N/A mg/I VOC
N/A mg/I
method#
method#
method#
mg/I
mg/l
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per Authorized Agen Na e and Title - Please type or print
Signaturermittee (or Authorized Agent)
(Dat5

Specific Conductance
Total Ammonia
TKN as N
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 13.50 ft. Well Diamter:
MWTF1-B
Screened Interval: 10.60 ft. to 12.60 ft.
2 inch
Depth to Water Level: 4.50 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 5.8 , Specific Conductance 317
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
uMhos
Temp. 20.1 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
X Remediation :
Remediation: Infiltration Gallery.
(.Jt
Land Application of Sludge
c.n
W
C7
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/22/03
4/22/03 to 5/2/03 c
PCS PHOSPHATE and PRIVIROKMENT 1
330 10-11
tf
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A uglf..
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A . ug11 ^
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 11.400 mg/I Zn - Zinc N/A c ug/W
(Note. Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen sing/10
Dissolved Solids: Total 452 mg/I Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units) rJ :::-
pH (when analyzed) 5.9 units Ba - Barium N/A mg/I Fluoride 0.25 mg/I
TOC 7.1 mg/I Ca - Calcium N/A mg/I MIBK N/A mg/I
Chloride 37.5 mg/I Cd- Cadmium N/A mg/I Ag - Silver N/A mg/I
Arsenic N/A mg/I Chromium: Total N/A mg/1 Se- Selenium N/A mg/I
Grease and Oils N/A mg/I Cu - Copper N/A mg/l Sodium N/A ug/I
Phenol N/A mg/I Fe - Iron N/A mg/I Organics: (GC, GC/MS, HPLC)
Sulfate 27.5 mg/I Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/1 Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A mg/I VOC
N/A mg/I Mn - Manganese N/A mg/1
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker - Manager, Environmental Affairs
Per - .f Authorized AgeNa • - and Title - Please type or print
GW-59 Rev 4/98
Signatu
Permittee (or Authorized Agent)
(Oat