WI0700012_Monitoring (Report)_20011127

PCS
PhosphateW AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
November 27, 2001
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2001— October 2001
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTFIA and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
4). laxwIALQ hil;,1.4,,,,a_cA lit_
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/attch)

bpc: S. A. Beckel / K. C. West (w/attch)
W. T. Cooper (w/o attch)
T. L. Baker/12-01-008-03-002 (w/ attch)
J. A. Hardy / RBL/SLD/JHT (w/ attch)
R. A. Allen / T. Lewis (w/attch)
D. D. Winstead / 00-24-000 (w/o attch)
W. A. Schimming (w/o attch)
2

Date:
Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
/ono/O/
Pn7 File: 15-03-003-02
Gf' Le.
System Gauge Pressures
sWw-1
O-go psi
SWW-7
D-/s/ ets/
cwW-1
/J, 5 ,osi
CWW-7
O-/n ,oa/
pc: TLB
Level
Ditch Level
6SO
Barge Slip
9 416
Water Level
ge„
Control Tank
!J t 7
.
C� /� o9
% = MSL
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
,5"Q'
‘114/5-
Cpz-1
10.51
9``86
Q
Spz-2
11.21
C�•2
g
d 39
Cpz-2
10.25
ift4J-
Jzf leg/ad
Spz-3
11.87
7„g0
4" 67
Cpz-3
11.12
/(, 68
0. e///
Spz-4
11.45
6. 90
4/.53--
CPW
9.65
/0. 52
- 0. to 7
Spz-5
11.45
9 66
1,79
MWTF-1A'
14.35
I/4/9
9.84
Spz-6
11.23
/D. Qe.
0.017
MWTF-1B•
14.36
07oe
g 9rJ
Spz-7
11.59
/Q„4(o
433
MWTF-1C•
14.44
la.BCo,
7 8
Spz-8
11.57
a,04
.557
MWTF-2A
14.05
6 70
r/.,
Spz-9
11.01
'JO
ce..oz/
MWTF-213
14.02
//.7Q
o'?.,,32-.
Spz-10
12.16
6. s '
o. 6O
MWTF-2C
14.08
/4'6Z
-0.4/8
SPW
9.95
Ape
/ /5
MWTF-3A
12.21
. !2/(
7 96
MWTF-3B
12.18
//f, 4%
/ 70
MWTF-3C
12.19
,3.20
-/0/
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
7.73,2
/8a
+1.to+2'
ys
CwW-1
10.60
sas
-3.7S-
-2'to-1'
y,
SWW-2
9.99
6.86
o.84
+1 •to+2'
X15
CwW-2
10.23
7, 5/
-/4/9
-2'to-l'
906
SWW-3
9.97
A.86
D.&o
+1•to+2'
/1s
Cww-3
9.95
75.Z.
-/ 48
-2'to-1'
�S
SWW-4
10.73
74/4/
/ 94/
+1'to+2'
Si�/
CWW-4
10.73
4.89
-o7/4'
-2'to-1'
YOS
SWW-5
10.80
7618
i 00
+1'to+2'
Ves
CWW-5
10.74
779
-/a/
-2'to-1'
SWW-6
10.66
734
/N,0
+1.to+2'
�%
%e3
CWW-6
9.92
6.6/
�89
-2'to-1'
ys
SWW-7
10.70
7/1/
9/1/
+1'to+2'
ys
CWW-7
9.95
6. 3s
-a. 66
-2' to-1'
re..*
-*• e z z - anS'zie/iosc y!/i7>`efro/ Covefinj /!ezonl e c C kec ke `I 54 irJ
Revised 8/12/97 • Riser k'' ldded to TOC elevation 1/24/97 OJ N) l5 ° -ail I -s U QDICeP. PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2001— October 2001
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
(
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Aug
300,520
0
300,520
6.7
13.4
Sept
324,660
0
324,660
7.5
13.2
Oct
378,230
0
378,230
8.5
13.2
TOTALS
1,003,410
0
1,003,410
3

Withdrawal Well System
The system was down on 10-9-01 for 2 hours for preventive maintenance on the air compressor. The
withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative
maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for
the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Aug
413,203
228,166
641,369
14.4
Sept
379,896
235,241
615,137
14.2
Oct
390,644
240,852
631,496
14.1
TOTALS
1,183,743
704,260
1,888,003
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sid -Formation Wrthdr -Well (SWWj Pumps
SWW-1: On 8/13 acid washed well. On 8/21 shook pump. On 9/12 repaired pump. On 9/17 changed
float. On 10/1 pulled and cleaned pump. On 10/3 repaired float.
SWW-2: On 8/7 cleaned pump. On 8/31 replaced check valve seat. On 9/6 acid washed well. On 10/9
changed pump. On 10/ 11 shook pump. On 10/19 changed air line.
SWW-3: On 10/3 acid washed well. On 10/12 acid washed well.
SWW-4:
SW W-5: On 8/28 pulled and cleaned pump.
SWW-6: W-6: On 8/10 replaced cam. On 8/27 changed air filter. On 10/26 shook pump.
S W W-7: On 10/4 replaced air line.
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 8/16 acid washed well.
CWW-2: On 8/21 acid washed well. On 10/15 repaired counter.
CWW-3: On 8/9 cleaned counter. On 8/14 pulled and cleaned pump. On 10/16 acid washed well and
replaced counter.
CWW-4:
CWW-5: On 8/8 changed air line. On 10/4 replaced pump.
CWW-6:
CWW-7: On 8/28 repaired pump. On 10/4 shook pump. On 10/16 pulled and cleaned pump.
5

GF;OUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: 5.25 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS
ft. Well Diamter: 4 inch
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2166 uMhos
Temp. 19.7 oC, Odor NONE Appearance: LT RUST
Mail Original
to:
Non -Disc
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Serves Center
—ram
RALEIGH, NC-27699-1636 Phone: [phone]
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1808
pH (when analyzed) 6.9
TOC 10.4
Chloride 83.2
N/A
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
668.7
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes nla No and field acidified Yes n/a No
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/l Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/l Mn - Manganese
c
N/A mg/I Ni - Nickel Ng, ug/I
N/A mg/I Pb - Lead -- f\ ug/I
3.290 mg/1 Zn - Zinc 0 NW, ug/I
Ammonia Nitrogen r (=f mg/I
N/A mg/I
N/A mg/I Other (Specify Compounds and Concentration Units}-
N/A mg/I Fluoride G7
N/A mg/I MIBK
Ag - Silver
Se- Selenium
Sodium
N/A mg/I Organics: (GC. GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I method#
method#
N/A mg/I
N/A mg/I
N/A mg/I
0
W
Nre
mg/I
mg/I
mg/I
mg/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authori ed A t) N me and Title - Please type or`pn t
Q/24 r/ 0
ignatur Per ittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-2
Well Depth: 52.15 ft. Well Diamter:
4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: 7.51 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatmen
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2490 uMhos
Temp. 20.4 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed: 10/10/01 to 11/6/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
Yes n/a No and field acidified Yes n/a No
N/A mg/l Ni - Nickel
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 2004 mg/I Al - Aluminum
pH (when analyzed) 6.8 units Ba - Barium
TOC 11.2 mg/I Ca - Calcium
Chloride 106.6 mg/I Cd- Cadmium
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/1 Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
787.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Pb - Lead
61.500 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
ug/l
ug/I
ug/I
mg/I
N/A mg/I Other (Specify Compounds and Concentration Units- t <
N/A mg/I Fluoride W 0.f 2 mg/I
N/A mg/I MIBK -0 NIZmg/1
N/A mg/I Ag - Silver NAT. mg/I
N/A mg/I Se- Selenium to Ng"' mg/I
N/A mg/l Sodium twrl Ng ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/1 VOC : method#
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perm ee f Authorized �lgentyA�'am and Title - Please type orpnn a% ,(
ignature of ttee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
Well Identification Number (from Permit):
Well Depth: 53.00
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: 7.20
Measuring Point is
ft. Well Diamter:
No. of Wells to be Sampled
ft. below measuring point.
3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE: 09/30/01
UIC X
Spray Field X Remediation :
18 1 1 Rotary Distributor Land Application of Sludge
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2716 uMhos
Temp. 25 oC, Odor NONE Appearance: CLEAR
Other
c
c
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2024
pH (when analyzed) 6.9
TOC 10.3
Chloride 233.6
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
549.0
N/A
N/A
N/A
mg/I
units
mg/I Ca - Calcium
mg/1
mg/1
mg/I
mg/1 Fe - Iron
mg/I Hg - Mercury
uMhos
mg/1
m g/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Yes n/a
No and field acidified
N/A mg/I
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
N/A mg/I
12.550 mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a
No
Ni - Nickel O NA ug/I
Pb - Lead - Nth ugll
Zn - Zinc Fri Nei l ug/I
Ammonia Nitrogen C) x �_^ mg/I
Other (Specify Compounds and Concentration Units rri
Fluoride 0.fgtmg/1
MIBK 3 N/c.mg/1
Ag - Silver N/r."mg/I
+J N/A? mg/1
c11 N/i ug/I
Se- Selenium
Sodium
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
method#
method#
N/A mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent Nam and Title - Please type or print ,l
ee (or Authorized Agent) (Date
ignatureermitt
,p�TP

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
[phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
ern penng
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 41.67 ft. to 50.92 ft.
CWW-4
4 inch
Depth to Water Level: 6.50 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2618 uMhos
Temp. 28.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1808 mg/l
pH (when analyzed) 7.0 units
TOC 9.5 mg/I
Chloride 137.2 mg/I
Arsenic N/A mg/I
N/A mg/1
N/A mg/I Fe - Iron
566.4 mg/I Hg - Mercury
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/1
N/A mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
No and field acidified Yes n/a No c
N/A mg/I Ni - Nickel Na ug/I
N/A mg/1 Pb - Lead N> -1-1. ug/I
6.550 mg/l Zn - Zinc Nla r,:-, ug/I
N/A mg/I Ammonia Nitrogen t c�:z mg/I
N/A mg/I Other (Specify Compounds and Concentration Unit C
N/A mg/I Fluoride --0 0. f -. mg/l
N/A mg/I MIBK s N/NP; mg/I
N/A mg/I Ag - Silver GJ NXIL mg/I
N/A mg/I Se- Selenium
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
r1
rTt
n
c.,0 N/2 mg/I
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
cm N/g ug/I
(1) No X (2)
method#
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ttee (of Authorized Age Na e and Title - Please type or pont
vim" l
(or uthorized Agent)
gnature
ermittee g )
'Z.EVO/
(Date)

GFFOUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
,,,_rt
18,
Well Identification Number (from Permit):
Well Depth: 53.17
CWW-5
ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: 7.79 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2111 uMhos
Temp. 29.6 oC, Odor NONE Appearance: CLEAR
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Ltia
—J
09/30/01
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11 /6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
1440 mg/I Al - Aluminum
6.9 units Ba - Barium
8.3 mg/I Ca - Calcium
89.0 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified
N/A mg/I
N/A mg/I
9.550 mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
431.6 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Yes n/a No
Ni - Nickel CJ
Pb - Lead
Zn - Zinc P1
Ammonia Nitrogen n
Other (Specify Compounds and Concentration Unit.)
Fluoride '32
MIBK
Ag - Silver
Se- Selenium
Sodium
N7P.-..
ug/I
ug/I
ug/I
mg/I
0. mg/I
NAL' mg/I
W NA ; mg/1
Nf mg/I
CJ1 N ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
• method#
method#
N/A mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee of Authorized Age
ignature, P
Na a and Title - Please type or 'pn�n
"/9i i
Agent) (DatA)
Authorized
ermittee (or Autho

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
Well Identification Number (from Permit): CWW 6 )
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 6.61 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS
18
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2164 uMhos
Temp. 30.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/03/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1372
pH (when analyzed) 7.1
TOC 13.1
Chloride 129.0
Arsenic
Grease and Oils
Phenol
Sulfate
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
N/A mg/I
N/A mg/1
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
51.900 mg/I
N/A mg/l
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
507.6 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
Yes n/a No "'~
N/A mg/I Ni - Nickel N ug/I
N/A mg/I Pb - Lead C3 NUN r`n ug/I
rrl Zn - Zinc CI N/mac snug/I
Ammonia Nitrogen ca * mg/I
Other (Specify Compounds and Concentration Units)-1�
Fluoride 50.1 S". cng/I
N/A mg/I MIBK W N/Pcn=Tng/I
N/A mg/I Ag - Silver • N/Ar-2 mg/l
N/A mg/I Se- Selenium ci:AN/A{, mg/I
N/A mg/I Sodium N/A. ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
method#
method#
N/A mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per thoriz d Ag i) me and Title - Please type or print ,
ignatur ermittee or Authorized Agent) (Dat )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
pe,no
Well Identification Number (from Permit): CVW
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 6.35 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.6 , Specific Conductance 1286 uMhos
Temp. 24.7 oC, Odor NONE Appearance: CLEAR
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/03/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed: 10/10/01 to 11/6/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 876 mg/I Al - Aluminum
pH (when analyzed) 7.2 units Ba - Barium
TOC 7.9 mg/I Ca - Calcium
Chloride 81.1 mg/I Cd- Cadmium
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/1 Cu - Copper
Phenol N/A mg/I Fe - Iron
Sulfate 178.7 mg/I Hg - Mercury
Specific Conductance N/A uMhos K- Potassium
Total Ammonia N/A mg/I Mg - Magnesium
TKN as N N/A mg/I Mn - Manganese
Yes n/a
No and field acidified
N/A mg/I
N/A mg/I
2.500 mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Yes n/a
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
No
O
C7
rrt
C7
NSA ug/I
NdA.._- ug/I
Nf1 ug/I
mg/I
Other (Specify Compounds and Concentration Units:,)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
C,J
C.)
Cll
0. `^'_ mg/I
NtA' mg/I
N' mg/I
N6 mg/I
N/ ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permof.Authorized Age a e and Title - Please type or pnn
(or Authorized Agent)
gnature rmiftee
q(Re
(Date