WI0700012_Monitoring (Report)_20000223

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
00061010
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter:
4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: 7.86 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1965 uMhos
Temp. 18.6 oC, Odor NONE Appearance: CLEAR
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
LEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
C.
Q "�
c_ c
Note: Values should reflect dissolved and
3211
1/27/00
1/27/00 to 02/07/00—
PCS PHOSPHATE"
330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 4.000 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1996 mg/I Al - Aluminum
pH (when analyzed) 6.8 units Ba - Barium
TOC 14.1 mg/1 Ca - Calcium N/A ug/l
Chloride 74.9 mg/I Cd- Cadmium N/A ug/I
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/1 Cu - Copper N/A ug/l
Phenol N/A mg/I Fe - Iron
Sulfate 695.2 mg/I Hg - Mercury
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
I f/A
N/A
N/A
N/A ug/I Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
Specific Conductance
Total Ammonia
TKN as N
N/A ug/I
N/A ug/I
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
NIA ug/I
Sodium
Organics: (GC. GC/MS,
(Specify test method #.
Report attached? Yes
VOC
0.24
N/A
N/A
N/A
N/A
HPLC)
Attach lab report.)
(1) No X
method#
method#
method#
ug/l
u g/I
ug/I
mg/I
mg/l
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized gent) Name and Title - Please type or print
- 75ri —2-/1Z 5/ ,i.pc c7
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
from _)
Well Identification Number (from Permit):
Well Depth: 52.15 ft. Well Diamter:
CWW-2
4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: 7.58 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 1941 uMhos
Temp. 19.4 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Cf
C? �
C)
—4. G}
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/27/00
Date sample analyzed:
Laboratory Name:
1/27/00 to 02/07/09-
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD Nitrite (NO2 as N)
mg/I
/100m1
/100m1
Coliform: MF Fecal Nitrate (NO3 as N)
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1936
pH (when analyzed) 6.8
TOC 13.3
Chloride 103.9
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
563.4
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes
n/a
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
3.950 mg/I
Yes n/a No c-/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N7A
N/A
N/A
0.22
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
N/A ug/I
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/l
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
onnA 1012
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-3
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level:
Measuring Point is
GALLONS
4 inch
7.50 ft. below measuring point.
3.08 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2261 uMhos
Temp. 26.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/27/00
Date sample analyzed: 1/27/00 to 02/07/00
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 C?
O
C:
A
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1800
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.3
10.7
184.2
N/A
N/A
N/A
481.0
N/A
N/A
N/A
mg/I
units
mg/I Ca - Calcium
mg/I
mg/l
mg/l
mg/1 Fe - Iron
mg/1 Hg - Mercury
uMhos
mg/l
mg/l
Yes n/a No and field acidified Yes n/a No
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
5.750 mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A ug/I
N/A ug/I
"II
r
N/A ug/l
N/A ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
0.22
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/l Report attached? Yes (1) No X
N/A ug/l VOC
N/A ug/I
method#
method#
method#
mg/l
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
110061013
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.62 ft. below measuring point.
2.75 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2253 uMhos
Temp. 27.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
1/27/00
s.
�L7
1/27/00 to 02/07/00
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1
1784 mg/I
6.9 units
10.6 mg/I
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
118.3 mg/I
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
No and field acidified
N/A mg/1 Ni - Nickel
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
5.450 mg/1
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/1 Ammonia Nitrogen
Yes n/a
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
526.4 mg/I Hg - Mercury
N/A ug/I
N/A ug/I
N/A ug/I
No
IV
N
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
0.15
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No
N/A ug/I VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/l
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print ea/AA.
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
00061014
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Orcen p}
Mail Original
to:
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter:
Screened Interval: 41.75 ft. to 51.08 ft.
4 inch
Depth to Water Level: 7,81 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 1856 uMhos
Temp. 30.8 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/27/00
Date sample analyzed: 1/27/00 to 2/7/00
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 0
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1284
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
7.0
8.4
71.4
N/A
N/A
N/A
318.8
N/A
N/A
N/A
mg/1
/100m1
/100ml
mg/l
units
mg/1
mg/I
mg/I
mg/l
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
n/a
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
4.500 mg/I
N/A mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper Sodium
N/A ug/l Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
method#
N/A ug/I
N/A ug/l
N/A ug/I
N/A mg/l Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
Yes n/a No u�
N/A -
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.17
N/A
N/A
N/A
N/A
N/A ug/I
N/A ug/l
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
T, h'•
Signature of Permittee (or Authorized Agent)
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized gent) Name and Title - Please type or print
-z/2 3/460e)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
00061015
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter:
4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 7.26 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1679 uMhos
Temp. 30.8. oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
U I C X
09/03/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/27/00
Date sample analyzed: 1/27/00 to 2/7/00
Laboratory Name: PCS PHOSPHATE
U
3
Certification No(s) 330 C..?
O
7E3
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1144 mg/I Al - Aluminum
pH (when analyzed) 6.7 units Ba - Barium
TOC 10.0 mg/I Ca - Calcium
Chloride 90.2 mg/1 Cd- Cadmium
9.600 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/l Other (Specify Compounds and Concentration Units)
Yes n/a No
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol N/A mg/I Fe - Iron
Sulfate 263.1 mg/1 Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
(:mr
N/A
N/A
N/A
0.20
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/1
ug/I
ug/l
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized gent) Name and Title - Please type or print
—77 iC Z7 . 4
Signature of Permittee (or Authorized Agent) (Da()

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-7
4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 7.42 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.6 , Specific Conductance 1182 uMhos
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Temp. 23.8 oC, Odor NONE
Appearance: LT. RUST
Mail Original
to:
PERMIT #:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/03/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
CI
G
A
1/27/00
1/27/00 to 2/7/00
PCS PHOSPHATE
330
•
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 886 mg/l
pH (when analyzed) 7.1 units
TOC 13.0 mg/I
Chloride
Arsenic
76.1 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/1
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
185.9 mg/l Hg - Mercury
n/a
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
2.100 mg/I Zn - Zinc
N/A mg/I
N/A ug/I
N/A ug/l
N/A ug/I
Yes n/a No
N!A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.20
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
N/A ug/I
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/1
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
/ •V
Signature of Permittee (or Authorized Agent)
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized ;gent) Name and Title - Please type or print
3/zo66
(Date)

Date:
Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
/-.34-00
7»?
Z.
System Gauge Pressures
sww-1
0 - as -Ps:
SWW-7
0-.252-93i
CWW-1
U - /g/J'S;
CWW-7
0./&ems;
File:16-03-003-02
pc: TLB
Level (msl
Ditch Level
vj 10
Barge Slip
9 4/0
Water Level
991;
Control Tank
=MSL
/iJ.07%�
Sand Layer Pelzometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level
Relative To
Ft.
Spz-1
10.47
-n9 7a
lo. 7 -
Cpz-1
10.51
.LLevell''
0
yMSL
yJ
Spz-2
11.21
8 07
5. /5/
Cpz-2
10.25
�/y.
99, 44
.7.
AS/
Spz-3
11.87
-5-, 80
' 4.07
Cpz-3
11.12
gate
2. 9P
Spz-4
11.45
6. SO
.J ,/S
CPW
9.65
R 76.
0.39
/Q.,S,s
Spz-5
11.45
9'. /6
ar.. a 9
MWTF-1A •
14.35
3. go
Spz-6
11.23
9,/,2
a.//
MWTF-1B•
14.36
1J9
977
Spz-7
11.59
/a 42$
/-S,
MWTF-1C•
14.44
8013
6„2/
Spz-8
11.57
6, /O
S/o0
MWTF-2A
14.05
A yg
757
Spz-9
11.01
B /(
4,9,49_5
MWTF-28
14.02
/Q 77
.fa5
Spz-10
12.16
55 06
7./O
MWTF-2C
14.08
/9•4"
00
SPW
9.95
'7 ,j !,
/. 9//
MWTF-3A
12.21
y. 00
8 /5
MWTF-3B
12.18
9.98
07.a0
MWTF-3C
12.19
0.0.1
0. /.)
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level,Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
at 0,3
+1' to+2'
Ye5
CWW-1
10.60
�py.O,i
-//2/
-2'to -1'
YS
SWW-2
9.99
n7t.
070
�,2Q
+1 ' to +2'
./CY!/1ine/YYana' gr At) lip
f
CWW-2
10.23
r€7•
/.boo
-/4a
-2'to-1'
�r/o1
I;.,
SWW-3
9.97
6. 7p
0.719
+1'to+2'
CWW-3
9.95
7SO
',SO
-2'to-1'
��5
Y
SWW-4
10.73
6.,$S
O..�Sn
+1' to+2'
CWW-4
10.73
�.(,,2
-r 3S
-2'to-1'
i/j
(eh
SWW-5
10.80
or, lc
0. 55
+1' to+2'
]e9
CWW-5
10.74
7p/
-//9
-2'to-1'
SWW-6
10.66
6.6,E
O. *6
+1'to+2'
/[S
Ir/�9.
CWW-6
9.92
/7 a{e
-/ 77
-2'to-1'
SWW-7
10.70
/.3 5
+1'to+2'
+IVCJJ
143
CW-7
W
9.95
�z
/ , 7
-j75
/
-�7j
-2 'to-1'
Yi
Revised 8/12/97
• Riser length added to TOC elevation 1/24/97
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
November, 1999 — January, 2000
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period. On November 2 the #1 Sterilizer sensor was
changed to insure accuracy in the intensity reading. On November 5 a new bulb was installed in the #1
Sterilizer as a result of a low intensity alarm. Following the installation the intensity reading approached
100%. The system was down 23 hours 35 minutes beginning at 15:10 on December 7 and resuming
operation at 14:45 on December 8 to repair an underground DPW leak.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
INJECTED WATER TOTALS
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Nov-99
397,000
0
397,000
9.2
14.4
Dec-99
429,970
0
429,970
9.6
14.7
Jan-00
373,410
0
373,410
8.4
14.7
TOTALS
1,200,380
0
1,200,380
Withdrawal Well System
The Withdrawal Well System operated the entire period. The withdrawal water well pumps are monitored
daily by the area Maintenance Department and preventative maintenance work is performed is needed.
The total monthly and quarterly withdrawal water volumes for the period are:
WITHDRAWAL WATER TOTAL S
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Nov-99
477,734
273,582
751,316
17.4
Dec-99
464,973
288,716
753,689
16.9
Jan-00
523,176
292,029
815,205
18.3
TOTALS
1,465,883
854,327
2,320,210
2

Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Air Compressor for the Withdrawal Well Pumps
Operation of the air compressor system was normal during the period.
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 11/9 the pump plugged and was changed. On 1/25 the pump was shaken to start.
SWW-2: On 1/11 the pump stopped and was shaken to start. On 1/12 the pump was replace.
SWW-3: Pump operated without incident.
SW W-4: On 1/11 pump would not start. Replaced with a rebuilt pump.
SWW-5: On 11//1 had to shake pump to start. On 12/8 pump would not start changed pump. On 1/4 had
to shake pump to start, pulled and cleaned pump.
SWW-6: On 11/1 the pump stopped and was shaken to start. On 11/24 replaced totalizer.
SWW-7: On 11/1 the pump stopped and was shaken to start.
Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: Pump operated without incident.
CWW-2: On 11/3 the pump would not pump. On 11/5 the pump was replaced. On 11/8 pump failed and
was replaced. On 12/16 replaced totalizer.
CWW-3: Pump operated without incident.
CWW-4: On 11/2 the pump was shaken to start. On 11/3 the pump was shaken to start. On 11/23 pulled
and cleaned pump. On 12/8 pump would not pump, changed out pump.
CWW-5: On 11/16 pump not working changed pump.
CWW-6: On 12/8 cleaned the pump. On 12/14 the pump stopped and was shaken to start.
CWW-7: On 12/8 cleaned the pump.
3

February 22, 2000
PCS
Phosphatece AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
MARK MILLIGAN '-'
GROUND WATER c7
nz L. a
DENR = =. _-1
1636 MAIL SERVICE CENTER `
RALEIGH, NC 27626-1636
Subject: Underground Injection Control Program
Fourth Quarter Groundwater Monitoring Report
November 1999 - January 2000
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
,0
D. Daniel Winstead III
Environmental Engineer
Environmental Affairs
Attachments
pc: Willie Hardison / Keith Starner — DWQ- GWS, WaRO (w/attch)
bpc: TXi. L. Baker / 12-01-008-03-002 (w/ attch)
J. A. Hardy / R. B. Lee / T. W. Davis (w/ attch)
R. A. Allen / T. Lewis (w/attch)
D. D. Winstead / 00-24-000 (w/o attch)
W. A. Schimming (w/o attch)