WI0700012_Monitoring (Report) Aug - Oct 2006_20061129

pecific Conductance
Total Ammonia
TKN as N
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
(ham per,.
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
epth to Water Level: N/A ft. below measuring point.
leasuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 7.2 , Specific Conductance 621 uMhos
Temp. 21.0 oC, Odor NONE
0
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/30/2006
Date sample analyzed: 10/30/2006 to 11/28/2006
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
No and field acidified X Yes No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100ml Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.046 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 434 mg/I Al - Aluminum N/A mg/I
pH (when analyzed) 7.2 units Ba - Barium N/A mg/l
TOC 5.7 mg/1 Ca - Calcium N/A mg/I
Chloride 14.2 mg/I Cd- Cadmium <0.001 mg/l
Arsenic N/A mg/I Chromium: Total <0.005 mg/I
Grease and Oils N/A mg/1 Cu - Copper N/A mg/I
Phenol N/A mg/I Fe - Iron N/A mg/I
ulfate <10.0 mg/I Hg - Mercury N/A mg/I
N/A uMhos K- Potassium N/A mg/I
N/A mg/I Mg - Magnesium N/A mg/I
N/A mg/I Mn - Manganese <0.010 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and ConcentratiOnitnits)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
No\i 20a6
0.59
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
VOC
(1) No
: method#
method#
method#
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/l
(2)
l t ettify that, to the best of my khowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P m, ii tepee (of Authorized Agent) Name and Title - Please type or print
Vr(%Iv 7(%f )2 /15 '/729lo(o
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
creened Interval: 38.70 ft. to 40.70 ft.
,epth to Water Level: 13.04 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 6.9 , Specific Conductance 668 uMhos
Temp. 22.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC
01/15/08
X Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/30/2006
Date sample analyzed: 10/30/2006 to 11/28/2006
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 456
pH (when analyzed) 6.9
TOC 5.9
Chloride
Arsenic
Grease and Oils
'henol
julfate
Specific Conductance
Total Ammonia
TKN as N
19.4
N/A
N/A
N/A
12.4
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/1
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
X Yes
Nitrite (NO2 as N) •
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.126 mg/I
<0.001 mg/I
0.022 mg/I
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.735 mg/I
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride -C• ,1 '' 0.46 mg/I
N/A mg/I MIBK Wit-' `,-^� • 3 - N/A ug/I
Ag - Silver \I C,c- \fvt''` c N/A ug/I
Se-Seleni i�Yt ���� . N/A ug/l
N/A mg/I Sodium t�jj4\� '' N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
• method#
method#
N/A mg/I
N/A mg/I
N/A mg/I
mg/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Perrrlittee of Authorized Agent) Name and Title - Please type or print /
- -rr /ZMS 11729 /o 4
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter: 4 inch
Greened Interval: 33.27 ft. to 52.68 ft.
epth to Water Level: ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH , Specific Conductance uMhos
Temp. oC, Odor Appearance:
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
01/15/08
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
�wp,�E QUPL,�
Date sample collected:
Date sample analyzed: to
Laboratory Name: PCS PHOSPHATE
colloidal concentrations
10/29/2006
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: U N method
Dissolv T
pH (wh ed)
TOC
Chlorid
Arsenic
Grease and Oils
henol
.ulfate
N/A mg/I
N/A /100m1
N/Ar /100m1
/A
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Total
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a
No and field acidified
Yes n/a No )
N/A mg/I Ni - Nickel
N// mg/I
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
• method#
method#
N/A ug/I
N/A ug/I
N/A ug/I
mg/I
mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE: No Sample - Static Water Level Below Pump.
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P. r yt)ee f(of Authorized Agent) Name anTitle - Please type o print
Signature of Permittee (or
r
thorized Agent)
1'
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-2
Well Depth: 52.15 ft. Well Diamter:
icreened Interval: 30.57 ft. to 49.82 ft.
lepth to Water Level: 5.47 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2862 uMhos
Temp. 21.8 oC, Odor NONE Appearance: LT RUST
4 inch
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01 /15/08
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/19/2006
Date sample analyzed: 10/19/2006 to 11/28/2006
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2140
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
'henol
. ulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
mg/1
6.5 units Ba - Barium
10.0 mgll Ca - Calcium
63.0 mg/1 Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as
Orthophosphate
Al - Aluminum
N/A mg/I Fe - Iron
905.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A mg/I
N/A mgll
77.750 mg/I
N/A mg/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concerttfation Units)
Fluoride S ";c.` ` , 0.19
MIBK N/A
Ag -
Se- Selenium N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
: method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/l
ug/I
ug/I
ug/l
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
e (of A horized Agent) Name and Title - Please type or pri}t
/'V/ RM5 ///29 i 6
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
icreened Interval: 36.42 ft. to 50.67 ft.
)epth to Water Level:
Measuring Point is
4 inch
5.25 ft. below measuring point.
3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
Temp. 23.8 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2486 uMhos
Appearance: LT RUST
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
EXPIRATION DATE:
UIC X
01/15/08
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/19/2006
Date sample analyzed: 10/19/2006 to 11/28/2006
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2076
pH (when analyzed) 6.5
TOC 11.4
Chloride 64.6
Arsenic N/A
Grease and Oils N/A
)henol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
793.4
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A mg/1
N/A mg/1
26.300 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen tt��
N/A ug/I Other (Specify Compounds and Conr{t 'tlnitst\1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
101
0.13
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/1
ug/I
ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/1 (Specify test method #. Attach lab report.)
N/A ug/1 Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
• method#
method#
N/A ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerl), DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
P ittee (of Authorized Agent) Name and Title - Please type or print
{, /2,vt5 '&/a 9 4 6
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter: 4 inch
"creened Interval: 41.67 ft. to 50.92 ft.
epth to Water Level: 5.89 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.9 , Specific Conductance 1306 uMhos
Temp. 26.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
01/15/08
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/19/2006
10/19/2006 to 11/28/2006
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
henol
_ulfate
Specific Conductance
Total Ammonia
TKN as N
unfiltered Yes nla
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified
N/A
N/A
/100m1 Phosphorus: Total as P
Orthophosphate
740 mg/I Al - Aluminum
6.8 units Ba - Barium
6.5 mg/I Ca - Calcium
137.0 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
58.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
mg/I Ni - Nickel
mg/I Pb - Lead
8.500 mg/I Zn - Zinc
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Yes nla No )
Ammonia Nitrogen {�
Other (Specify Compounds and Cof1CeTitr' on )
Fluoride �'`
MIBK
AgSilver ��
Se -Selenium
Sodium
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
VOC
N/A ug/I
N/A ug/I
N/A ug/I
mg/1
0.35 mg/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A ug/I
HPLC)
Attach lab report.)
(1) No X (2)
: method#
method#
method#
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
PeAnittte,(of
uthorizad Agent) Name and Title - Please type or print
/f
Signature of Permittee (or Authored Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
horn pa,
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter:
icreened Interval: 41.75 ft. to 51.08 ft.
)epth to Water Level:
Measuring Point is
4 inch
5.71 ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2749 uMhos
Temp. 26.1 oC, Odor NONE Appearance: LT CLOUDY
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/19/2006
Date sample analyzed: 10/19/2006 to 11/27/2006
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1972
6.6
9.0
Chloride
Arsenic
Grease and Oils
'henol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
52.3
N/A
N/A
N/A
981.7
N/A
N/A
N/A
Yes n/a
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I
units
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
uMhos
mg/I
mg/I
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
30.900
mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration nits)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/l
N/A ug/I Organics: (GC, GC/PAS; HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
mg/I
0.10 mg/I
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A ug/I
Se- Selenium'
Sodium
VOC
: method#
method#
method#
N/A ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Permi a (o Authorized Agent) Name and Title - Please type or print
if
,Fle- /2ii S /11297ro
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
>creened Interval: 36.62 ft. to 50.88 ft.
)epth to Water Level: 7.21 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 3386 uMhos
Temp. 30.8 oC, Odor NONE Appearance: LT RUST
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
01/15/08
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/19/2006
10/19/2006 to 11/28/2006
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2280
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Thenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.6
11.9
77.9
N/A
N/A
N/A
1073.4
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
No and field acidified
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 45.250 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ugll
Cu - Copper N/A ug/I
Fe - Iron N/A ug/I
Hg - Mercury N/A ug/I
K- Potassium N/A ug/I
Mg - Magnesium N/A ug/I
Mn - Manganese N/A ug/I
Yes n/a No )
Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium �U
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC : method#
method#
method#
0.08 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
X (2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Aut orized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 5.32 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 7.4 , Specific Conductance 1095 uMhos
Temp. 23.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
UIC X
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/19/2006
Date sample analyzed: 10/19/2006 to 11/28/2006
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
N/A
N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 708
pH (when analyzed) 7.0
TOC 9.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Yes nia
No and field acidified
mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel
/100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead
/100m1 Phosphorus: Total as P 10.325 mg/1 Zn - Zinc
Yes nla No )
N/A
N/A
N/A
Orthophosphate N/A mg/I Ammonia Nitrogen
mg/I Al - Aluminum N/A ug/I Other (Specify Compounds
units Ba - Barium N/A ug/I Fluoride
mg/I Ca - Calcium N/A ug/I MIBK
135.0 mg/I Cd- Cadmium N/A ug/I Ag - Silver
N/A mg/I Chromium: Total N/A ug/I
N/A mg/I Cu - Copper N/A ug/I
N/A mg/I Fe - Iron N/A ug/I
307.7 mg/1 Hg - Mercury N/A ug/I
N/A uMhos K- Potassium N/A ug/l
Se- Selenium
and Concentration Units)
\4o,
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
N/A mg/1 Mg - Magnesium N/A ug/I VOC
N/A mg/I Mn - Manganese N/A ug/I
(1) No
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
0.52 mg/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
X (2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
4P rmittee of Authorized Agent) Name and Title - Please type or print
0Q i r /i''S /1/4 `i �D6
Signature of Permittee (or Authorized Agent) (Date)

PCS c*Phosphate AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
November 30, 2006
Evan O. Kane
1636 Mail Service Center
Raleigh, North Carolina, 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2006 — October 2006
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
tAL„ -; „( err
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming (w/ attachments)
Total Two Copies Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
E-Mail:
M. D. Johnson
R. B. Lee
H:\Reports\2006\Quarterly\TFRAS Report Third Quarter 2006.doc
2

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
OUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2006 — October 2006
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the SPA/Fertilizer Department and reported to the Environmental
Affairs Department. The total monthly and quarterly volumes of water injected as well as the month end
water level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
August
1,091,423
0
1,091,423
24..4
15.0
September
838,555
0
838,555
19.4
15.0
October
799,015
0
799,015
17.9
15.0
TOTALS
2,728,993
0
2,728,993
H:\Reports\2006\Quarterly\TFRAS Report Third Quarter 2006.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
'• x.;G `� # "n^s : w "* ad}"7 ,s"'� s � a a }.s i � �
e� � �
.. r � �, ;. �._
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Aug
347,620
25,763
373,383
8.4
Sept
294,838
43,577
338,416
8.1
Oct
469,094
17,202
486,296
10.9
TOTALS
1,111,553
86,542
1,198,095
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
On 8/3, 8/8, 8/16, 8/25, 8/29, 9/7, 9/13, 9/22, 9/29, 10/4, 10/10, 10/17 and 10/26 flushed out pumps and
lines on each of the Confined Sand Formation Withdrawal Well (SSW) and the Croatan Formation
Withdrawal Well (CWW) Pumps.
SWW-1: On 10/3 replaced pump.
SWW-2:
SWW-3: On 9/11 changed counter.
SWW-4: On 9/5 replaced pump. On 10/5 changed counter.
SWW-5:
SWW-6:
SWW-7: On 10/24 changed pump.
H:\Reports\2006\Quarterly\TFRAS Report Third Quarter 2006.doc 4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3: On 10/9 changed counter.
CWW-4: On 10/23 repaired air line.
CWW-5:
CWW-6: On 10/19 air blasted well.
CWW-7: On 10/19 air blasted well.
H:\Reports\2006\Quarterly\TFRAS Report Third Quarter 2006.doc
5