WI0700012_Monitoring (Report)_20000518

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 6.32 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatrnent
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2637
uMhos
Temp. 18.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation:
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
0
4/17/00
4/17/00 to 4/28/00 —<
PCS PHOSPHATE
Certification No(s) 330
r)
(J1
'Qr
O
Infiltration Galleryt
CP
C;)
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1884
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.5
12.5
72.3
N/A
N/A
N/A
947.8
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
n/a
No and field acidified
N/A
N/A
Phosphorus: Total as P 80.500
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A
N/A
N/A
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
mg/l
mg/I
Ni - Nickel
Pb - Lead
Yes nla No
mg/I Zn - Zinc
mg/1 Ammonia Nitrogen
mg/I
mg/I
mg/l
mg/I
mg/1
mg/l
mg/I
mg/l
mg/I
mg/I
mg/I
NN/A, ;;Ing/l
N N/A`--i mg/I
w NJ/ mg/1
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.50
N/A
N/A
Se- Selenium N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
: method#
method#
mg/1
mg/I
mg/I
mg/1
mg/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ittee (of Authorized Age n Na and Title -Please type r print
Signatu Perrnittee (or Authorized Agent) ate)

f
c
c. •

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.21 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
For Groundwater Treat,nen
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2094 uMhos
Temp. 18.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X
EXPIRATION DATE:
UIC X
09/30/01
Remediation: Infiltration Gallery'
Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
O o
4/16/00 Q n
4/16/00 to 4/28/00 N 72
PCS PHOSPHATE '<
330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1452
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.3
11.8
58.0
N/A
N/A
N/A
572.6
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/1
mg/1
mg/I
uMhos
mg/1
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A mg/I
Ni - Nickel
N/A mg/1 Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
132.000 mg/I Zn - Zinc
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
Yes n/a No
Ammonia Nitrogen
N c,'
R 7J
iyN/AA mg/I
N/A mg/I
N/A mg/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/l Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.21
N/A
N/A
N/A
N/A
N/A mg/1 VOC method#
method#
method#
N/A mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ittee (of Authorized Ag t) N me and Title - Please type or print
. , s//a)
Signatur,
ermittee (or Authorized Agent) (Date)

CO !
8

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 24.50 ft. Well Diamter:
SWW-3
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.41 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2042 uMhos
Temp. 22 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery cp
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
O �
O c)
Date sample collected: 4/16/00 33.
cprri
Date sample analyzed: 4/16/00 to 4/28/00 N rr'rt
Laboratory Name: PCS PHOSPHATE CI)
Certification No(s) 330 -.r, _,,
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
Coliform: MF Total N/A /100m1 Phosphorus: Total as
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Orthophosphate
1424 mg/I Al - Aluminum
6.5 units Ba - Barium
9.8 mg/I Ca - Calcium
31.7 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
635.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Yes n/a No
f V c-^
N/A mg/I Ni - Nickel N N/A, Ong/1
N/A mg/I Pb - Lead W N/, mg/1
P 41.500 mg/I Zn - Zinc N/,F mg/I
N/A mg/I Ammonia Nitrogen mg/I
N/A mg/1 Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.50 mg/1
N/A mg/I MIBK N/A mg/1
N/A mg/1 Ag - Silver N/A mg/I
N/A mg/I Se- Selenium N/A mg/I
N/A mg/I Sodium N/A mg/1
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I method#
method#
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
PerZnittee (of Authorized Agent
ignatur
e and Title - Please type or print
rmittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Omen pr.
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23,30 ft.
Depth to Water Level: 7.20 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 5.9 , Specific Conductance 2523 uMhos
Temp. 33 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation
EXPIRATION DATE:
UIC X
09/30/01
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
cp
Note: : Values should reflect dissolved and p
colloidal concentrations
c>
Date sample collected: 4/16/00 A2.�
rn
Date sample analyzed: 4/16/00 to 4/28/00 —� "
n
Laboratory Name: PCS PHOSPHATE cjj o
Certification No(s) 330 31
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1552
6.1
9.5
37.9
N/A
N/A
N/A
746.5
N/A
N/A
N/A
mg/I
/100m1
/100m1
mgll
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
n/a
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
107.000 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No
Ammonia Nitrogen
d/A rit/I
/A-7! mg/I
N/A z mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.14
N/A
N/A
Se- Selenium N/A
N/A mg/I Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC : method#
N/A mg/I
method#
method#
mg/I
mg/l
mg/I
mg/I
mg/1
mg/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P ittee (of Authorized Age Nae and Title - Please type or print
Signatu
f Permittee (or Authorized Agent)
(D te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
bcm perm[,
Mail Original
to:
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.01 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.1 , Specific Conductance 2542 uMhos
Temp. 30.5 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Appearance: LT CLDY WHT
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE: 09/30/01
TYPE OF PERMITTED
Lagoon
Spray Field
UIC X
OPERATION BEING MONITORED
Remediation: Infiltration Gallery
X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and o
colloidal concentrations 0CD o
Date sample collected: 4/16/00 = c" �
Date sample analyzed: 4/16/00 to 4/28/00 .�`� >rn
Laboratory Name: PCS PHOSPHATE N orn
Certification No(s) 330 CA ZE`
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1704
6.3
12.9
59.7
N/A
N/A
N/A
756.4
N/A
N/A
N/A
Yes n/a
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
48.500 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
NJ/A ;..,fig/1
ruN/A� mg/I
4i/A23 mg/I
mg/1
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No
0.34
N/A
N/A
N/A
N/A
N/A mg/l VOC
N/A mg/I
method#
method#
method#
mg/1
mg/I
mg/I
mg/I
mg/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Age rpi)Nayhe and Title - Please type or print
Signature,
PPrmittee (or Authorized Agent)
oe>

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
4 inch
Depth to Water Level: 6.58 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2071 uMhos
Temp. 31.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon Remediation: Infiltration Gallery .7r
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/16/00
Date sample analyzed: 4/16/00 to 4/28/00
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
N
PARAMETERS: (Samples for metals were collected
COD N/A mg/1
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1360 mg/1
pH (when analyzed) 6.2 units
TOC 13.7 mg/1
Chloride 110.6 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Phenol N/A mg/I
Sulfate 355.0 mg/1
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified Yes n/a No
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
58.500 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
f41,1/A giag/I
/A _1 mg/I
/A? mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.09
N/A
N/A
Se- Selenium N/A
N/A mg/I Sodium N/A
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC : method#
N/A mg/I
method#
method#
mg/1
mg/1
mg/I
mg/I
mg/I
mg/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ee IV Authorized Aqt) Nlme and Title - Please type or print ,
reil7
V
Signatur¢;6P'Permittee (or Authorized Agent)
( )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.38 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 5.7 , Specific Conductance 1320 uMhos
Temp. 26.8 oC, Odor NONE Appearance: LT RST ORANGE
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE: 09/30/01
UIC X
TYPE OF PERMITTED OPERATION BEING MONITORED ---
Lagoon Remediation: Infiltration Gallery rr
Spray Field X Remediation : Q'
Rotary Distributor Land Application of Sludge
Other (ti
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/16/00
Date sample analyzed:
Laboratory Name:
0
o
4/16l00 to 4/28/00 A. .7v
h
N
Certification No(s) 330 CIO
PCS PHOSPHATE
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Dissolved Solids: Total 992 mg/I Al - Aluminum
pH (when analyzed) 5.9 units Ba - Barium
TOC 15.3 mg/I Ca - Calcium
Chloride 80.3 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
n!a
No and field acidified
N/A mg/I
93.000 mg/I
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1 Fe - Iron
271.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I
N/A mg/l
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/l
Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes nla No
Ammonia Nitrogen
3 r`;
NN/Ac,te
NN/A�; iig/I
c,,, N/P mg/I
z mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report)
Report attached? Yes (1) No X (2)
0.14
N/A
N/A
N/A
N/A
N/A mg/I VOC : method#
: method#
method#
N/A mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ttee (of Authorized Agent) me and Title - Please type or print
Signatu»'df Permittee (or Authorized Agent)
(Da e)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
Screened Interval: 3,40 ft. to 5.40 ft.
2 inch
Depth to Water Level: 4.12 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 534 uMhos
Temp. 18.4 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallere
Remediation :
Land Application of Sludge
Cr"
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/12/00
Date sample analyzed:
Laboratory Name:
4/12/00 to 4/28/00
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
368 mg/I Al - Aluminum
7.3 units Ba - Barium
6.0 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
8.2 mg/I Cd- Cadmium
No and field acidified Yes n/a No ' *m
N/A mg/I Ni - Nickel -0N/ y-ng/I
N/A mg/I Pb - Lead �N/A [-ng/I
0.450 mg/I Zn - Zinc IN N/f ', Ing/I
N/A mg/I Ammonia Nitrogen N El mg/I
N/A mg/I Other (Specify Compounds and Concentration Units) G) q
N/A mg/I Fluoride 1.89z
N/A mg/I M I BK N/A
N/A mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
19.8 mg/I Hg - Mercury
N/A mg/I Se- Selenium
N/A mg/1 Sodium
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC
N/A mg/I
method#
: method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P_ °u te- of Authorized A. _ Na e and Title - Please type or print
Signatu, • ' • ermittee (or Authorized Agent)
( te)