WI0700012_Monitoring (Report) Feb - April 2002_20020510

CROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 7.22
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
ft. below measuring point.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2279 uMhos
Temp. 17.5 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/02
Date sample analyzed: 4/5/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1444
pH (when analyzed) 6.4
TOC 8.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
79.2
N/A
N/A
N/A
591.7
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
m g/I
mg/1
mg/I
mg/I
uMhos
mg/l
mg/I
mg/1 Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
116.000 mg/I
Yes n/a No
N/A mg/1 Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/1
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.58 mg/I
N/A mg/I MIBK N/A mg/1
N/A mg/I Ag - Silver N/A mg/I
N/A mg/I Se- Selenium N/A mg/I
N/A mg/I Sodium o N/Sc ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC) N
N/A mg/I (Specify test method #. Attach lab repot.) -:-=-c
c
N/A mg/I Report attached? Yes
N/A mgll
(1) No —t .- (2)
N/A mg/l VOC methodE c c
method#
methods m—,
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
x
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per i (of Authorized Ag�nt) ame and Title - Please type or print
Signatur% fVermittee (or Authorized Agent)
(Da )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 6.52 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2371 uMhos
Temp. 17.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
09/30/01
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of Sludge
C.2
i)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/02
Date sample analyzed: 4/5/02 to 5/2/02 Oti
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
CA)
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1564 mg/I Al - Aluminum
pH (when analyzed) 6.6 units Ba - Barium _
TOC 9.1 mg/I Ca - Calcium
Chloride 42.2 mg/I Cd- Cadmium
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol N/A mg/I Fe - Iron
Sulfate 636.4 mg/I Hg - Mercury
Yes n/a
No and field acidified
N/A
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos K- Potassium
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
50.250 mg/I
mg/1 Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Yes n/a No
N/A mg/I
N/A mg/I
N/A mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
ug/I
ug/l
ug/I
mg/I
0.24 mg/I
fiak mg/I
t494 mg/I
N/A mg/I Se- Selenium = NY,X7 mg/I
tfA_ ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) —,-
J
N/A mg/l (Specify test method #. Attach lab re ft rt.) L.
N/A mg/I Report attached? Yes (1) No - ' (2)
methods ;a fI
N/A mg/I Sodium
N/A mg/I VOC
N/A mg/I
method
method
rrt
c-2
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P itte (of Authorized Name and Title - Please type or print
��
ignatur P rmittee (or Authorized Agent) (Dater

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
(from p )
Well Identification Number (from Permit):
Well Depth: 24.50 ft. Well Diamter:
SWW-3
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.79 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1600 uMhos
Temp. 22.5 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/02
Date sample analyzed:
Laboratory Name:
Certification No(s)
W
W
4/5/02 to 5/2/02 CD
PCS PHOSPHATE and ENVIRO(QMENT 1
330 10 •.4
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No
and field acidified Yes nla No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1172
pH (when analyzed) 6.3
TOC 6.8
Chloride 33.8
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
467.4
N/A
N/A
N/A
Orthophosphate
mg/1 Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
89.750 mg/I
N/A
N/A
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
mg/l Ammonia Nitrogen
mg/I
N/A mg/1
N/A mg/I
N/A mg/I
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK �V
mg/1
0. mg/I
NYA mg/I
Ag - Silver
N/A mg/1 Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #.
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
N$ mg/I
Nftc, mg/1
N$,_ : ug/I
Attach lab rett.
(1) No
method
method
methodif
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per�ittee (of Authorized Ame and Title - Please type or print
ignatureej'Permittee (or Authorized Agent)
S.-A/O z_
(Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00
ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 7.28 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2282 uMhos
Temp. 30.3 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : �y
09/30/01
Rotary Distributor
Other
Land Application of Sludge ---.
W
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/02
Date sample analyzed: 4/5/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
co
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100ml Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1688 mg/I Al - Aluminum
pH (when analyzed) 6.4 units Ba - Barium
TOC 7.3 mg/l Ca - Calcium
Chloride
Arsenic
Grease and Oils
43.1 mg/I Cd- Cadmium
106.750 mg/I Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/1 MIBK
0.07 mg/I
N/A mg/I
N/A mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
805.1 mg/I
Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I Se- Selenium
N/P%_ mg/I
mg/I
NIA mg/I Sodium 3 N/A -,pg/I
N/A mg/I Organics: (GC, GC/MS, HPLC) z s
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No W X--cc;(2)
N/A mg/I VOC : method# 4:.
: method#
: method?
N/A mg/I
rn
" w
rf
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
rP¢c(of Authorized .ent) ame and Title - Please type or print
4.4.— .3-//o/e 2—
Signatyf Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
28.21 ft. Well Diamter:
SWW-5
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 6.61 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2592 uMhos
Temp. 27 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/02
Date sample analyzed: 4/5/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
Yes n/a
No and field acidified Yes n/a No
N/A mg/1 Ni - Nickel N/A
N/A mg/I Pb - Lead N/A
N/A /100m1 Phosphorus: Total as P
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1844
pH (when analyzed) 6.8
TOC 11.2
Chloride 61.1
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
845.8
N/A
N/A
N/A
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
39.000 mg/1 Zn - Zinc N/A
N/A mg/l Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
mg/I Cd- Cadmium
mg/l Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/1 Mn - Manganese
ug/I
ug/I
ug/I
mg/1
N/A mg/I Fluoride 0.37 mg/I
N/A mg/I MIBK N/A mg/I
N/A mg/I Ag - Silver NAN mg/I
N/A mg/1 Se- Selenium N Na mg/I
N/A mg/I Sodium m Neug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) _"' tl=
-< c
N/A mg/1 (Specify test method #. Attach lab repast.) --"= =
o<
N/A mg/I Report attached? Yes (1) Now (2)
N/A mg/I VOC : method#p
N/A mg/I : method*
method)
1 certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized A•entyName and Title - Please type or print
Signatur f Permittee (or Authorized Agent) (Dat)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.32
Measuring Point is
GALLONS
4 inch
ft. below measuring point.
2.58 ft above land surface.
of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2294 uMhos
Temp. 27.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
Rotary Distributor Land Application of Sludge j
Other
W
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 415102
Date sample analyzed: 415/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
IN)
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1772
pH (when analyzed) 6.7
TOC 12.3
Chloride 97.8
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
689.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/1
units
mg/I
mg/I
mg/I
m g/1
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a No and field acidified
Nitrite (NO2 as N) N/A mg/I Ni - Nickel
Nitrate (NO3 as N) N/A mg/I Pb - Lead
Phosphorus: Total as P 23.250 mg/1 Zn - Zinc
Orthophosphate N/A mg/1 Ammonia Nitrogen
Al - Aluminum N/A mg/I
Ba - Barium N/A mg/I
Ca - Calcium N/A mg/1
Cd- Cadmium N/A mg/I
Chromium: Total N/A mg/I
Cu - Copper N/A mg/1
Yes n/a No
N/A
N/A
N/A
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
ug/I
ug/I
ug/l
mg/I
Fluoride 0.04 mg/I
MIBK N/A mg/1
Ag - Silver O Nti!A mg/I
Se- Selenium N N mg/I
Sodium -1, NF :ug/I
Organics: (GC, GC/MS, HPLC) "< ,
(Specify test method #. Attach lab rea t) v�
Report attached? Yes (1) No »c (2)
VOC : method-0T ;
method
method#'
•l.V
c)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Per ittee (of Authorized Age Na e and Title - Please type or print
Signatur
ermittee (or Authorized Agent)
S//b/Q 7.
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth:
29.50 ft. Well Diamter:
4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 7.27 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 1090 uMhos
Temp. 23.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations CA)
Date sample analyzed: 4/5/02 to 5/2/02 C�
Laboratory Name: PCS PHOSPHATE and ENVIROft MENT 1
Date sample collected: 4/5/02
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 728 mg/I Al - Aluminum
pH (when analyzed) 6.2 units
TOC 7.7 mg/I
Chloride 73.8 mg/I
Arsenic N/A mg/I
Yes n/a
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A mg/l
211.5 mg/1
N/A uMhos
N/A mg/I
N/A mg/I
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I Pb - Lead
51.750 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/l Other (Specify Compounds and Concentration Units)
N/A mgll Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
mg/I
0.09 mg/I
N/A mg/1
N/(�• mg/I
N/A mg/I Se- Selenium CJ Nig mg/I
PO N/A ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC) A o^
N/A mg/1 (Specify test method #. Attach lab report.) iL
N/A mg/1 Report attached? Yes (1) No c.3 >V;=. (2)
>o
N/A mg/1 Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I VOC
N/A mg/I
method
method=
method#/.
--t
1
cn.
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permitte- (of Authorized A ent) me and Title - Please type or print
Signatur;a: Pettee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 6.40
Screened Interval:
Depth to Water Level:
Measuring Point is
3.40
4.20
3.86
MWTF1-A
ft. Well Diamter: 2 inch
ft. to 5.40 ft.
ft. below measuring point.
ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.4 , Specific Conductance 519 uMhos
Temp. 18.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : N
Rotary Distributor
Other
Land Application of Sludge ---
W
W
Note: Values should reflect dissolved and
colloidal concentrations ra
Date sample collected: 4/8/02
Date sample analyzed: 4/8/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/1
/100m1
/100m1
368 mgll Al - Aluminum
7.5 units Ba - Barium
3.0 mg/I Ca - Calcium
Chloride
Arsenic
7.6 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes nla
No and field acidified
NIA mg/I
N/A mg/I
Phosphorus: Total as P 0.526 mg/I
Orthophosphate Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
N/A mg/1 Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/1 Organics: (GC, GC/MS. HPLC)
N/A mg/I (Specify test method #. Attach lab report.) zr'
N/A mg/I Report attached? Yes (1) No (2)
N/A mg/I VOC : method -:1.
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
N/A
N/A
N/A
N/A mg/I
N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
18.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/1 Mn - Manganese
2.15
N/A
N/6
ug/I
ug/I
ug/I
mg/1
mg/l
m g/l
mg/I
N%A mg/I
N/A mg/I
S N4A ug/I
method= •
methodd#t) m i
c-�
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
i4CYO Vl ', r�fs,�
ignatur,PPermittee or Authorized Agent)
Terry L. Baker- Manager, Environmental Affairs
Permittee (of Authorized Agent)) ame and Title - Please type or print
J -,M''Gs
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Oro
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.88 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
ft. Well Diamter: 2 inch
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 6.1 , Specific Conductance 338 uMhos
Temp. 19.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Remediation: Infiltration Galles ,
1V•
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
X Remediation :
Land Application of Sludge
fame
w
w
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
r1/47
CA,
4/8/02
4/8/02 to 5/2102
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 268 mg/I Al - Aluminum
pH (when analyzed) 6.2 units Ba - Barium
TOC 3.3 mg/I Ca - Calcium
Chloride 40.6 mg/I Cd- Cadmium
N/A mg/l Chromium: Total
N/A mg/l Cu - Copper
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
30.1 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
6.300 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/1 Sodium
N/A mg/I Organics: (GC. GC/MS,
N/A mg/I (Specify test method #.
N/A mg/I Report attached? Yes
N/A mg/1 VOC
N/A mg/1
HPLC)
ug/I
ug/I
ug/I
mg/1
0.28 mg/I
I\{LA mg/I
mg/I
mg/I
p, N ug/I
Zr
Attach lab reeert.) o�=
Kim
(1) No X-u (2)
method4 rrt
method
methods#'
c�
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
CFI
IMO
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ttee of Authorized Agent) Npme and Title - Please type or print
ignatur,
Permittee (or Authorized Agent)
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 10.25 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2600
Field Analysis: pH 7.4 , Specific Conductance 618 uMhos
Temp. 21.2 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon Remediation: Infiltration Gallem
Spray Field X Remediation :
Rotary Distributor
Other
Land Application of Sludge
CAI
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/8/02
Date sample analyzed: 4/8/02 to 512/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
S!
.C'
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P
(Note Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
468 mg/I Al - Aluminum
7.7 units Ba - Barium
4.9 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
13.4 mg/l Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
46.0 mg/l Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/l Mn - Manganese
No and field acidified X
Yes No
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/l Pb - Lead N/A ug/I
0.331 mg/I Zn - Zinc N/A ug/I
N/A mg/l Ammonia Nitrogen mg/l
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/l Fluoride 0.50 mg/I
N/A mg/I MIBK N/A mg/I
<0.001 mg/I Ag - Silver N/A mg/I
<0.005 mg/I Se- Selenium Ilt.ci, mg/l
N/A mg/I Sodium N WA ug/I
N/A mg/l Organics: (GC, GC/MS, HPLC) 3 n
N/A mg/I (Specify test method #. Attach lab rep'at.) rT`'
N/A mg/I Report attached? Yes (1) No — (2)
N/A mg/I VOC methodtP H
0.049 mg/I : method#0 R; --.
methodiX
N
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I. am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Ag t) N me and Title - Please type or print
gnature,ermittee (or Authorized Agent) (Dat1

Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
pe
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
N/A
Field Analysis: pH 7.1 , Specific Conductance 588 uMhos
Temp. 17.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallvr
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
47
CA)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/8/02
Date sample analyzed: 4/8/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
Cil
PARAMETERS: (Samples for metals were collected unfiltered X Yes No and field acidified X Yes No
COD N/A mg/I Nitrite (NO2 as N) N/A mg/1
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/1
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.042 mg/l
(Note: Orthophosphate N/A mg/l
Dissolved Solids: Total mg/I Al - Aluminum N/A mg/l
pH (when analyzed) units Ba - Barium N/A mg/I
TOC mg/I Ca - Calcium N/A mg/I
Chloride mg/I Cd- Cadmium <0.001 mg/I
mg/1 Chromium: Total <0.005 mg/I
Use MPN method for highly turbid samples)
458
7.4
8.1
13.9
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I Cu - Copper
mg/l Fe - Iron
mg/l Hg - Mercury
uMhos K- Potassium
N/A mg/I
N/A mg/I
N/A mg/1
mg/I Mg - Magnesium
mg/l Mn - Manganese
N/A mgll
N/A mg/l
<0.010 mg/I
Ni - Nickel N/A ugll
Pb - Lead N/A ug/l
Zn - Zinc N/A ug/l
Ammonia Nitrogen mg/l
Other (Specify Compounds and Concentration Units)
Fluoride 0.51 mg/I
MIBK N/A mg/I
Ag - Silver N/A mg/I
Se- Selenium
N/A mg/I
Sodium Ig/A
Organics: (GC, GC/MS, HPLC) N
(Specify test method #. Attach lab report
Report attached? Yes (1) No
VOC : method# --
method# C`,
method#
err;
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized • . - t) -me and Title - Please type or print
�V /ts L_
ermittee (or Authorized Agent)
(Dat

Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to NIA ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.1 , Specific Conductance 597 uMhos
Temp. 18.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : ' F
Rotary Distributor Land Application of Sludge
09/30/01
Other
49
Col
Note: Values should reflect dissolved and N
colloidal concentrations
Date sample collected: 4/8102
Date sample analyzed: 4/8/02 to 5/2/02
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes No and field acidified X Yes No
COD N/A mg/I Nitrite (NO2 as N) N/A mg/l Ni - Nickel
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/l Pb - Lead
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.048 mg/I Zn - Zinc
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total 493 mg/1 Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 7.4 units Ba - Barium N/A mg/1 Fluoride 0.51 mg/l
TOC 6.2 mg/I Ca - Calcium N/A mg/I MIBK N/A mg/I
Chloride 13.7 mg/I Cd- Cadmium <0.001 mg/I Ag - Silver N/A mg/I
N/A mg/l Chromium: Total <0.005 mg/I Se- Selenium N/A mg/I
N/A mg/l Cu - Copper N/A mg/1 Sodium N/6 ug/I
N/A mg/l Fe - Iron N/A mg/1 Organics: (GC, GC/MS, HPLC) C)
<10.0 mg/I Hg - Mercury N/A mg/1 (Specify test method #. Attach lab repp.) c-,
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No xe. ) r_3, (2)
N/A mg/I Mg - Magnesium N/A mg/I VOC : method fir"
N/A mg/I Mn - Manganese <0.010 mg/I
method]
method
N/A ug/l
N/A ug/l
N/A ug/I
-1
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
C1
Terry L. Baker - Manager, Environmental Affairs
Pe�fitte(of Authorized Agent) game and Title - Please type or print
Signa
Permittee (or Authorized Agent)
(

Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date: %/.a_0I<
am File: 15-03-003-02
,,d�
System Gauge Pressures
S1NW-1 '
0- /5 PST
SWW-7
0- 7 psi
cww-1
...Z. nog.
CWW-7
0-// A7sr
pc: TLB
Reference
Point MSL
Level Rel
to MSL
Ditch
12.91
7.S$
Barge Slip
10.59
/./9
Water Level
Control Tank
= MSL
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
-4.S B
,589
Cpz-1
10.51
.% a?f<
/079
Spz-2
11.21
8. Sa
. 4 3
Cpz-2
10.25
//O. S3-
- C. /0
Spz-3
11.87
(o . S0
.5:37
Cpz-3
11.12
9. 6 4/
/ 4/B
Spz-4
11.45
/o .85
1oO
CPW
9.65
. 96,
- 0.3/
Spz-5
11.45
9 3-6
/ 89
MWTF-1A •
14.35
1.20
/D. /S
Spz-6
11.23
9. 8e
/ 57
MWTF-1B •
14.36
4/.88
9,548
Spz-7
11.59
/0,07
/'/52-
MWTF-1C•
14.44
/O. fJ
4i/./9
Spz-8
11.57
7. 03
4/5 -5
MWTF-2A
14.05
a.e..
7VS
Spz-9
11.01
8. 66'
Of..f'3
MWTF-2B
14.02
//so
o73 Z
Spz-10
12.16
A. o/
tO./S
MWTF-2C
14.08
/4' „Qs
- 0. /j
SPW
9.95
8.0z
/ 93
MWTF-3A
12.21
L3- 98
8...,13
MWTF-3B
- 12.18
/0. //.2-
/. 761
MWTF-3C
12.19
/a. 90
- 07/
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
70?.2
/. .2.2..
+1 'to+2'
))
fits
CWW-1
10.60
9..50
O50
-2'to-1'
a�P9S
W SW-2
9.99
o.Lr2.
0.5-.2.
+1' to +2'
Ph
CWW-2
10.23
/p, 93
- 2,07
-2'to-1'
l2es
SWW-3
9.97
779
/, 79
+1'to+2'
05
CWW-3
9.95
7/5-
- / 85-
-2'to-1'
Ve5
S1NW-4
10.73
74'8
/,, X8
+1. to+2'
CWW-4
10.73
Gi.4&
-. ,54/
-2'to-1'
�P)e5
Yes
SWW-5
10.80
6.44/
, .0. 4/
+1' to+2'
?eh
CWW-5
10.74
6.97
-2.o3
-2'to-1'
/'es
SWW-6
10.66
7.3-Z
/ 32-
+1 'to+2'
CWW-6
9.92
706
- / 99
-2'to-1'
�a�//P5
ief
SWW-7
10.70
7.027
/.27
+1' to+2'
CWW-7
9.95
6.33
-J. 67
-2'to-1'
�����e5
TeS
Revised 12/03/01
• Riser lel' - Ided to TOC elevation 1/24/97
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2002 — April 2002
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
levelin-the-WaterLeveLControl Tank -are. —
dEflarr
.2744
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb
357,130
0
357,130
8.0
13.2
March
404,220
0
404,220
9.1
13.5
April
403,024
0
403,024
9.0
13.5
TOTALS
1,164,344
0
1,164,344
C:\MyData\Reports\2002\Quarterly\First Quarter TFRAS Report 2002.DOC
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb
350,165
192,650
542,815
12.6
March
420,789
246,478
667,266
14.9
April
338,194
134,686
472,880
10.7
TOTALS
1,109,147
573,815
1,682,962
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1:
SWW-2: On 2/11 replaced totalizer.
SWW-3: W-3: On 2/27 cleaned pump. On 3/6 changed totalizer.
SWW-4:
SWW-5: On 2/19 cleaned pump and replaced totalizer.
SWW-6: On 2/13 replaced pump. On 2/19 cleaned pump. On 2/28 repaired pump. On 3/6 changed pump
and cleaned well.
SWW-7: On 4/30 cleaned well.
C:\MyData\Reports\2002\Quarterly\First Quarter TFRAS Report 2002.DOC
4
•

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3: On 2/19 replaced totalizer.
CWW-4:
CWW-5:
CWW-6:
CWW-7: On 2/12 replaced pump.
C:\MyData\Reports\2002\Quarterly\First Quarter TFRAS Report 2002.DOC

Phosphate AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
May 9, 2002
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
February 2002 — April 2002
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF 1 CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sii�n`\cerel\�y\\
ILL
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
T. L. Baker/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen / T. Lewis (w/ attachments)

•
E-Mail:
S. A. Heckel
J. A. Hardy / R. B. Lee
W. A. Schimming
C:\MyData\Reports\2002\Quarterly\First Quarter TFRAS Report 2002.D0C
2