WI0700012_Monitoring (Report) May - July 2002_20020828

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
22.50 ft. Well Diamter:
SWW-1
Screened Interval: 18.30 ft. to 21.12 ft.
4 inch
Depth to Water Level: 4.96 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance
Temp. 20.8 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2082 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of $ dge
r-�
cr)
I rl
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/10/02
Date sample analyzed: 7/10/02 to 7/29/02
Laboratory Name: PCS PHOSPHATE andiNVIRONMENT 1
Certification No(s) 330 10 `+
PARAMETERS: (Samples for metals were collected unfiltered
COD
Yes n/a No and field acidified Yes n/a No
N/A mg/I Nitrite (NO2 as N) N/A
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N) N/A
N/A /100m1 Phosphorus: Total as P 111.000
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Orthophosphate N/A
1360 mg/I Al - Aluminum N/A
6.3 units Ba - Barium N/A
9.6 mg/I Ca - Calcium N/A
Chloride
Arsenic
63.9 mg/I Cd- Cadmium N/A
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total N/A
N/A mg/I Cu - Copper N/A
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
561.8 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
mg/I Ni - Nickel
mg/I
mg/1
mgll
mg/l
mg/I
mg/I
mg/I
mg/1
mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I VOC
N/A mg/I
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I
N/A ug/I
N/A ug/I
mg/I
!V
0.6t4 mg/I
N/A'- mg/1
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
method#
method#
method#
N/A mg/1
N/Amg/I
N/A*/ 1 ug/I
C..;
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North.Carolina OWQ (formerly DEM) certified laboratory. -I am aware that there are significant penalties -for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Per ee (of Authorized Agent) Na and Title - Please type or print
.gignature, t Perm ttee (or Authorized Agent) (Me)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter:
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.30 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
4 inch
Temp. 21.1 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2164 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
09/30/01
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/10/02
Date sample analyzed: 7/10/02 to 7/29/02
Laboratory Name: PCS PHOSPHATE and €1iVIRONMENT 1
Certification No(s) 330 10 (;)
W
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1880
pH (when analyzed) 6.5
TOC 10.4
Chloride
Arsenic
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
37.4 mg/1 Cd- Cadmium
Grease and Oils
Phenol
Sulfate
50.000 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
ug/I
N/A ug/I
N/A C3ig/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/1 Ag - Silver
N/A mg/1 Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
633.5 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Se- Selenium
N/A mg/I Sodium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
Ng/l
0.26 mg/I
N/A i •/I
N/A •!/I
N/A /I
N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X
N/A mg/l VOC : method#
method#
method#
CI
(2)
I certify that, to the best of my knowledge and belief, theinformation submitted in this report istrue, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM)-certified laboratory. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Perm of Authorized Agent) Name nd Title - Please type or print
tgnature of ' -rmittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter:
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 6.49 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1556 uMhos
Temp. 23.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/10/02
Date sample analyzed: 7/10/02 to 7/29/02
Laboratory Name: PCS PHOSPHATE and NVIR"ONMENT 1
Certification No(s) 330 10 IN)
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1060
6.4
7.5
33.0
N/A
N/A
N/A
463.0
N/A
N/A
N/A
Yes n/a No and field
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/1 Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
acidified Yes n/a No
N/A mg/I Ni - Nickel
45.750 mg/I
N/A mg/1 Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mgil
N/A mg/I
N/A mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
mg/l Chromium: Total
mg/I Cu - Copper
mg/1 Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/1 Mn - Manganese
N/A mg/l
N/A mg/l
Se- Selenium
Sodium
0.11
N/A
N/A
N/A
N/A
N/A mg/I Organics: (GC. GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report.)
N/A mg/l Report attached? Yes (1) No X
N/A mg/I VOC
N/A mg/l
method#
method#
method#
ug/I
ug/I
ug/l
m g/I
rig/I
r9/I
/5/1
(2)
I certify that, to the best of my knowledge and belief, the information- submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a -North Carolina DWQ (formerly DEM) certified laboratory. I am aware_that there aresignificant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ee (of Authorized Agent) ameLand Title - Please type or print
1 /_,AA
gnature of
rmittee (or Authorized Agent)
;3/Q2.
Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
25.00 ft. Well Diamter:
SWW-4
4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 7.16 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.9 , Specific Conductance
Temp. 32.2 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2722 uMhos
Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
rn
t`-1
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
7/10/02
7/10/02 to 7/29/02(
PCS PHOSPHATE and
330 10
c-)
VIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes nla
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1960
pH (when analyzed) 6.2
TOC 13.5
Chloride 42.3
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
782.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/1
mg/I
mg/I
mg/1
mg/I
mg/1
uMhos
mg/I
mg/l
No and field acidified
Nitrite (NO2 as N) N/A
Nitrate (NO3 as N) N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
156.500
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A
N/A
N/A
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
mg/I
mg/1
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
mgll
mg/I
mg/I
mg/I
mg/I
Yes n/a No
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.) C
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
0.1i j mg/l
N//REV mg/1
N/A&' mg/I
N/P07 mg/1
Report attached? Yes
VOC
N/,aC l ug/I
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. - tam aware that there are significant penalties for submitting -
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ee(of Authorized Agen ANa 7('y�f and Title - Please type or
print
Signature fiermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21
ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 8.26 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance
Temp. 30.7 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2838 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
09/30/01
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of SIfictbe
)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
m,
7/10/02
7/10/02 to 7/29/02
PCS PHOSPHATE and VIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1910
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.5
14.5
68.4
N/A
N/A
N/A
746.2
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
60.500 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/1 VOC method#
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/1
method#
method#
fpmg/I
0.35" mg/I
N/A mg/I
N/Acpmg/I
N/AUmg/I
N/Aug/I
•
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,_accurate, and complete, and •that the-iaboratoryanalytical data was produced
using approved methods of analysis by a North Carolina DWQ-(formerly DEM) certified laboratory. I am aware that there -are significant penalties for submitting •
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per
Signature;(
tee (of Authorized Agent Name and Title - Please type or print
NS
4f%Z'''.
ermittee (or Authorized Agent)
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth:
26.00 ft. Well Diamter:
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.38 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2406 uMhos
Temp. 29.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/10/02
Date sample analyzed: 7/10/02 to 7/29/02
Laboratory Name: PCS PHOSPHATE andcTlVIRONMENT 1
Certification No(s) 330 10 ry
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1
/100m1
Nitrate (NO3 as N)
Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1810 mg/l Al - Aluminum
6.4 units Ba - Barium
13.6 mg/I Ca - Calcium
Chloride
Arsenic
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
24.750 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
0.04
ug/I
ug/I
ug/l
tN
N/A •/I
102.5 mg/I Cd- Cadmium N/A mg/I Ag - Silver
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
675.4 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A /I
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC. GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A rtu•I
N/A
N/A mg/I VOC method#
method#
method#
N/A mg/1
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that thelaboratory analytical data was produced:
using approved methods of analysis by -a North Carolina DWQ (formerly DEM) certified laboratory. _I am _aware thatthere are significant penalties for submitting - •. - - -
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permit ae (g Authorized AgentNamp and Title - Please type or print
(Date
4'
Signature of Prmittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: 7.00 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.1 , Specific Conductance
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
888 uMhos
Temp. 26.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Slpge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/10/02
Date sample analyzed:
Laboratory Name:
Certification No(s)
va
7/10/02 to 7/29/02 :—
PCS PHOSPHATE and e1QVIRONMENT 1
330 10 rya
t
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 661
pH (when analyzed) 6.2
TOC 7.2
Chloride 68.0
Arsenic N/A
N/A
N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
728.3
N/A
N/A
N/A
mg/1
units
mg/I
mg/I
mg/I
mg/l
mg/I Fe - Iron
mg/1 Hg - Mercury
uMhos
mg/1
mg/I
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
36.000 mg/l Zn - Zinc N/A ug/I
N mg/I
Other (Specify Compounds and Concentration Units) NI
Fluoride 0.1C mg/I
MIBK N/An mg/I
Ag - Silver N/CD mg/I
N/AJl mg/I
N/AD ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I
N/A mg/l Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the_information submitted in this report is true, -accurate, and complete, and that the laboratory analytical data was produced
usingapproved methods of analysis by a _North Carolina DWQ (formerly DEM) certified laboratory. t am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent Nam and Title - Please type or print
e/ /
mitt8e or Authorized
Agent)
ignature
( g )
(Da )

Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
,from per
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40
ft. Well Diamter: 2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.18 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.0 , Specific Conductance 726 uMhos
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Temp. 27.8 oC, Odor NONE Appearance: CLEAR
PERMIT #: W10700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
09/30/01
Other
Rotary Distributor Land Application of Slud4e
t/)
rn
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/22/02
Date sample analyzed: 7/22/02 to 8/19/02 c.,.) Cr -1
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10 7 ��
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a
COD N/A mg/l Nitrite (NO2 as N) N/A mg/1 Ni - Nickel
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 0.400 mg/1 Zn - Zinc N /AV ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen N mg/I
Dissolved Solids: Total 360 mg/I Al - Aluminum N/A mg/l Other (Specify Compounds and Concentration Units) 4—
pH (when analyzed) 7.0 units Ba - Barium N/A mg/I Fluoride 2.0V1 mg/I
TOC 5.1 mg/I Ca - Calcium N/A mg/I MIBK N/1 ' mg/I
Chloride 14.4 mg/I Cd- Cadmium N/A mg/1 Ag - Silver N/P1 mg/I
N/A mg/I Chromium: Total N/A mg/1 Se- Selenium N/t ) mg/I
N/A mg/I Cu - Copper N/A mg/1 Sodium N/A ug/I
N/A mg/I Fe - Iron
<10.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N// ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
N/A mg/I : method#
method#
I certify that, to -the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the Iaboratoryanalytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerlyDEM) certified laboratory. : I am aware -that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
PermAuthori �Agen a and Title - Please type or print
t
gnature o ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 5.20 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 5.8 , Specific Conductance
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
407 uMhos
Temp. 26.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge)
c-a
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7117/02
Date sample analyzed:
Laboratory Name:
Certification No(s)
7117/02 to 8/19/02 ry 524
PCS PHOSPHATE and Ert RONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes nla
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
268 mg/1
5.9 units
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Al - Aluminum
Ba - Barium
4.4 mg/1 Ca - Calcium
51.6 mg/I
N/A mg/I
N/A mg/I
N/A mg/I Fe - Iron
40.8 mg/I Hg - Mercury
N/A uMhos
N/A mg/I
N/A mg/I
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
4.725 mg/I Zn - Zinc
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
•
Ammonia Nitrogen N mg/I
Other (Specify Compounds and Concentration Units) fV
Fluoride 0.236— mg/I
MIBK N/PV1 mg/I
Ag - Silver N/ACD mg/I
Se- Selenium N/ACrt mg/l
N/A-- ug/I
Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1 Report attached? Yes
N/A mg/1 VOC
N/A mg/1
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory -analytical data -was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significantpenalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per a (of Authorize Age ) Na a and Title - Please type or print
ri.�Rj..i,
ignature
ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth:
42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.64 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.2 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2600
639 uMhos
Temp. 24.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/22/02
Date sample analyzed: 7/22/02 to 8/19/02
Laboratory Name: PCS PHOSPHATE and ENVI8ONMENT 1
Certification No(s) 330 10'
PARAMETERS: (Samples for metals were collected unfiltered
X Yes
No and field acidified X
COD N/A mg/I Nitrite (NO2 as N) N/A
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.594
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A
Dissolved Solids: Total 396 mg/I Al - Aluminum N/A
pH (when analyzed) 7.3 units Ba - Barium N/A
TOC 5.4 mg/1 Ca - Calcium N/A
Chloride 14.5 mg/I Cd- Cadmium <0.001
N/A mg/I Chromium: Total <0.005
N/A mg/I Cu - Copper
N/A mgll Fe - Iron
37.3 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
<0.010
mg/I
mg/I
mgil
mgll Ammonia Nitrogen
mgll
mg/I
mg/1
mg/I
mg/I
mg/I
mg/1
mg/1
mg/I
mg/I
mgll
Yes No
Ni - Nickel
Pb - Lead
Zn - Inc
N/A ug/I
N/ ug/I
N/Ra ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
0.5
F
N/
Ag - Silver N/
Se- Selenium N/
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
mgll
mgll
mg/I
mg/I
ug/I
I certify that, to the best of my knowledge and belief; the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permii eyof Authorized Agent) N jme nd Title - Please type or print
�%rd
/
(Dat
i� ,�
/ '
ignature of
. rmittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
N/A ft. below measuring point.
N/A ft above land surface.
Depth to Water Level:
Measuring Point is
Fo Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: N/A
Field Analysis: pH 7.1 , Specific Conductance 698 uMhos
Temp. 28.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
.-y
<,
m)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/22/02
Date sample analyzed:
Laboratory Name:
Certification No(s)
7/22/02 to 8/27/02 —
PCS PHOSPHATE and EI4V1RONMENT 1
330 10
r)
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0*
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 407
pH (when analyzed) 7.1
TOC 6.5
Chloride 14.1
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
<10.0
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/1
units
mg/I
mg/1
mg/I
mg/I
mg/I
mg/1
uMhos
mg/1
mg/I
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X
N/A mg/I
N/A mg/1
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
0.051 mg/1
<0.001 mg/1
<0.005 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes No
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/1 MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X (2)
N/A mg/1 VOC : method#
N/A ug/I
N/A ug/I
N/A ug/I
mg/I
0.5F mg/I
N/4_ mg/1
mg/I
N/I'3:.:r mg/I
<0.010 mg/1
: method#
method#
Nhall ug/I
C..)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*COLIFORM ORIGINAL SAMPLE WAS 520/100 ML. SAMPLING POINT AND
METHOD WAS SUSPECTED AND CHANGED. RESAMPLE WAS <1.0/100 ML.
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per
ee lof Authorized Agent) Na
and Title - Please type or print
ee (or Authorized Agent)
g7irso
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy _ Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: NIA ft. to N/A ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.1 , Specific Conductance 617 uMhos
Temp. 22.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/22/02
Date sample analyzed: 7/22/02 to 8/19/02
Laboratory Name: PCS PHOSPHATE and ENVilikONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes No and field acidified X Yes No - t7
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel 147A -70/1
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead WA r-tgfl
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.025 mg/I Zn - Zinc WA - ig/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen `� rtg/I
Dissolved Solids: Total 429 mg/I Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units) pp
pH (when analyzed) 7.1 units Ba - Barium N/A mg/I Fluoride 0.2 mg/I
TOC 6.1 mg/I Ca - Calcium N/A mg/I MIBK NAP) mg/1
Chloride 14.0 mg/I Cd- Cadmium <0.001 mg/I Ag - Silver Nhr mg/I
Arsenic N/A mg/I Chromium: Total <0.005 mg/I Se- Selenium NtAin mg/I
Grease and Oils N/A mg/I Cu - Copper N/A mg/I Sodium N/A ug/I
N/A mg/I Fe - Iron N/A mg/I Organics: (GC, GC/MS, HPLC)
<10.0 mg/I Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A mg/I VOC method#
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Mn - Manganese <0.010 mg/I : method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name nd Title - Please type or print
�2d L
ignaturepf ermi ee (or uthorized Agent) (Dat

PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date: 7/M/ctz ///» W B/2'//O;<,
Time:
Tech:
�/ 13,Gee
System Gauge Pressures
Sww-1
O- 20 's;
SWW-7
O-6 po;
cww-i
Q _ 9 go;
CWw-7
D.-/e/ Ps:
File: 12-07-02
RC: TLB
Reference
Point MSL
Level Rol
to MSL
Ditch
12.91
5,56
Barge Slip/
Water Level
Control Tank
= MSL
10.59
9•?,2
/9.77'
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
*O'a
6p.2S
Cpz-1
10.51
as
a-0/
Spz-2
11.21
B2(o
�-95
Cpz-2o
10.25
/GOO
-D. 5
Spz-3
11.87
Z. /8
SJ'.G 9
Cpz-3
11.12
9, go>/
gt.
Spz-4
11.45
6.4„0
7 B..S
CPW
9.65
/O. 67
-7
- D 9
Spz-5
11.45
9.0N
lrh. • /
MWTF-1A•
14.35
4' /6
/0717
Spz-6
11.23
986
/37
MWTF-1B •
14.36
tS• 20
9•/co
Spz-7
11.59
/076
/ a
MWTF-1C•
14.44.
G/64
pf. Bo
- Spz-8 -
-11:57 --
-7--//41
--.44-/3-
-MWTF-2A-
-14:05-
erSO -
-%sS---
not
Spz-9
11.01
808
a.9s
MWTF-2B
14.02
/0,40
Spz-10
12.16
6. /R
J` , 98
MWTF-2C
14.08
/y /0
- O.Opt
SPW
9.95
75 y -
' a. I//
MWTF-3A
12.21
P.07
W MTF-3B
12.18
%• 98
9: 98
10
MWTF-3C
12.19
/3.2a
/- 03
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Pump
Activation Depth
Re! MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(YJes/(N)o
Comments
SWW-1
10.70
//96)
6'
-/0`/
+1'to+2'
%ES
'r(Lh'//;7Pt /0 6e40e
CwW-1
10.60
77/
9'
-/•P29
-2'to-1'
t'ei
SWW-2
9.99
730
6'
/•3o
+1 'to+2'
j/5j
CwW-2
10.23
r/(os
9'
'/. 57
-2'to-1'
,8
//es
SWW-3
9.97
A 49
6'
P. '99
+1'to+2'
W;IdJes
CW-3
9.95
7 90
9'
- //Q
-2 ' to-1'
re,
SWW-4
10.73
7r/6
6'
///p
+1 ' to+2'
rei
CWW-4
10.73
7 63
9'
-A.39
-2'to-1'
146
SWW-5
10.80
p -26
6'
a-g(p
+1. to+2'
lie'
CWW-5
10.74
9'
-/.`J3
-2'to-1'
1/13
SW W-6
10.66
�71-/r7
/. Si
6'
/.3e
+1'to+2'
CWW-6
9.92
9.go
9'
0-20
-2'to-1'
e,
SWW-7
10.70
700
6'
/. 00
+1 'to+2'
/C
CWW-7
9.95
L5:.7 /
9'
S. V 9
-2'to-l'
lei
Revised 7/29/02
• Riser length added to TOC elevation 1/24/97
D:tData\Fomis\Well Form\Tank Farm Ramer] Welisxls

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
May 2002 — July 2002
The Tank Farm Remediation System consists, of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level -in -the -Water -Level -Control Tank are. - - -
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
May
501,056
0
501,056
11.2
13.4
June
518,310
0
518,310
11.6
13.2
July
564,230
0
564,230
12.6
13.5
TOTALS
1,583,596
0
1,583,596
C:\MyData\Reports\2002\Quarterly\Second Quarter TFRAS Report 2002.DOC
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
May
378,023
155,505
533,528
12.1
June
370,3.99
170,124
540,523
12.5
July
248,584
178,942
427,526
9.7
TOTALS
997,005
504,571
1,501,576
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 5/16 replaced pump. On 5/21 replaced pump.
SWW-2:
SWW-3:
SWW-4: On 5/1 changed pump. On 6/25 shook pump. On 7/2 changed pump. On 7/29 changed pump.
SWW-5: On 5/1 changed pump. On 5/9 washed well. On 5/15 fixed counter. On 6/25 changed air
regulator.
SWW-6: On 5/17 changed counter. On 6/3 changed counter.
SWW-7: On 7/10 cleaned pump.
c:\MyData\Reports\2002\Quarterly\Second Quarter TFRAS Report 2002.DOC
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2: On 7/18 shook pump. On 7/22 shook pump.
CWW-3: On 5/2 washed well.
CWW-4:
CWW-5: On 5/2 changed counter. On 6/26 cleaned discharge. On 6/27 changed counter. On 7/22
cleaned pump On 7/24 fixed counter. On 7/29 changed counter.
CWW-6:
CWW-7:
C:\MyData\Reports\2002\Quarterly\Second Quarter TFRAS Report 2002.DOC
5

PCS'
Phosphate
AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
August 28, 2002
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
May 2002 — July 2002
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please fmd the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTFICR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
T. L. Baker/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)