WI0700012_Monitoring (Report) Aug - Oct 2002_20021122

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 22.50 ft. Well Diamter:
SWW-1
Screened Interval: 18.30 ft. to 21.12 ft.
4 inch
Depth to Water Level: 8.06 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.3 , Specific Conductance
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2290 uMhos
Temp. 21.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration OiWery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor
Other
Land Application of Sludgi4
crt
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/22/02
Date sample analyzed: 10/22/02 to 11/12/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1412
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.3
9.7
76.9
N/A
N/A
N/A
618.6
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/l Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
121.000 mg/I
N/A mg/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)'
Z
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.71
N/A
N/A
N/A
N/A
N/A ug/I VOC
N/A ug/I
: method#
method#
method#
ug/I
ug/I
ug/I
mg/1
mg/I
ug/I
ug/l
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker — Manager, Environmental Affairs
Perm' tee o uthorized Agen Na and Title - Please type or prin
GW-59 Rev 4/98
ignaturemittee (or uthorized Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 8.76 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.4 , Specific Conductance 2217 uMhos
Temp. 20.6 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform:
Coliform:
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
MF Fecal N/A
MF Total N/A
Use MPN method for highly turbid samples)
1532
6.5
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/22/02
Date sample analyzed: 10/22/02 to 11/12/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
Yes n/a
No and field acidified
mg/I Nitrite (NO2 as N) N/A
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
9.9 mg/I Ca - Calcium
42.7
N/A
N/A
N/A
368.9
N/A
N/A
N/A
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/l Mn - Manganese
N/A
P 48.250
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I VOC
ug/I
Yes n/a No )
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.26
N/A
N/A
N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC) tv
(Specify test method #. Attach lab rert.)
Report attached? Yes (1) No — X
method#
: method#
method#
ug/I
ug/I
ug/I
mg/I
mg/1
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker - Manager, Environmental Affairs
Permiij a of Authorized AgentZNarge and Title - Please type or print
GW-59 Rev 4/98
Signature gfPermittee (or Authorized Agent)
{Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
ORI
Mail Original
to:
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter:
4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 6.97 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 1588 uMhos
Temp. 22.8 oC, Odor NONE
Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: W10700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gilery
Spray Field X Remediation :
Other
Rotary Distributor Land Application of Sludge
wV
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/22/02
Date sample analyzed: 10/22/02 to 11/12/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 54.750 mg/I Zn - Zinc N/A ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/l
Dissolved Solids: Total 1084 mg/I Al - Aluminum N/A ug/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) 6.3 units Ba - Barium N/A ug/I Fluoride 0.13 mg/I
TOC 6.6 mg/I Ca - Calcium N/A ug/I MIBK +" N/A ug/I
mg/I Cd- Cadmium N/A ug/I Ag - Silver tv N/A ug/I
mg/1 Chromium: Total N/A ug/I Se- Selenium N/A ug/I
mg/1 Cu - Copper N/A ug/l Sodium N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No — X (2)
N/A ug/I VOC : method#
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
36.8
N/A
N/A
N/A
482.3
N/A
N/A
N/A
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/1 Mg - Magnesium
mg/I Mn - Manganese
N/A ug/I method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker — Manager, Environmental Affairs
Permi ee (of Authorized Age Na e and Title - Please type or print
ze
nature ermittee (or Authorized Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
[phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
6.71 ft. below measuring point.
3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2819 uMhos
Temp. 31.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation : W
Land Application of Sludge rn
;v
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/22/02
Date sample analyzed: 10/22/02 to 11/12/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1644 mg/I Al - Aluminum
pH (when analyzed) 6.3 units Ba - Barium
TOC 10.2 mg/l Ca - Calcium
Chloride 47.0 mg/1
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Phenol N/A mgll Fe - Iron
Sulfate 790.4 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
138.000 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
ry
—r,
N/A ug/I Sodium
N/A ug/l Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab teribort.)
N/A ug/I Report attached? Yes (1) No X
0.14
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
N/A ug/l
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/l
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker — Manager, Environmental Affairs
Per ee Authorized Agent a e and Title - Please type or prin
(Date)
gnature q rmi tee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.51 ft, below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2980 uMhos
Temp. 28.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone. [phone]
PERMIT #: W10700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration MONITORED,...„
Spray Field X Remediation :
UIC X
09/30/01
Rotary Distributor
Other
Land Application of Sludge')
try
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/22/02
Date sample analyzed:
Laboratory Name:
10/22/02 to 11/12/02
PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
AI - Aluminum
Ba - Barium
No and field acidified
N/A mg/I
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1896
6.4
11.9
76.1
N/A
N/A
N/A
824.7
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
mg/1
units
mg/I Ca - Calcium
mg/I
mg/I
mg/1
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/1
54.750 mg/I
N/A mg/1
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
Ammonia Nitrogen
r�.
Other (Specify Compounds and Concentration brlits)
Fluoride
MIBK
�v
Ag - Silver
Se- Selenium
Sodium
0.32
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC) ut
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
: method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/1
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker — Manager, Environmental Affairs
Perm tee Authorized AgenjNarpe and Title - Please type or print
Signature ermittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
(from pen.
Mail Original
to:
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter: 4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.11 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
X
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
Field Analysis: pH 6.3 , Specific Conductance 2607 uMhos
Temp. 27.9 oC, Odor NONE Appearance:
CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES O
TYPE OF PERMITTED OPERATION BEING MONITORED ry
Lagoon Remediation: Infiltration dery
Spray Field X Remediation : CA)
Rotary Distributor Land Application of Sludgzn
Other
r •/
co
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/22/02
Date sample analyzed: 10/22/02 to 11/12/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS:
COD
Coliform: MF Fecal
Coliform: MF Total
(Samples for metals were collected unfiltered Yes n/a
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1884
6.4
13.6
99.2
N/A
N/A
N/A
824.7
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
uMhos
mg/1
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
44.750 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/1 Ammonia Nitrogen
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration t$tits)
Fluoride
MIBK
Ag - Silver
0.07-
N/A
N/A
Se- Selenium N/A
N/A ug/I Sodium N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab rel5ort.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l VOC method#
N/A ug/I
method#
method#
ug/I
ug/l
ug/I
mg/1
mg/1
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker — Manager, Environmental Affairs
Per f Authorized Age Na e and Title - Please type or print
ignature gP7ermittee (or Authorized Agent)
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
„o
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 7.15 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance
Temp. 24.3 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1045 uMhos
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration kiIlery
Spray Field X Remediation :
UIC X
Other
Rotary Distributor Land Application of Sludge)
fV
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/22/02
10/22/02 to 11/12/02
PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 728
pH (when analyzed) 6.0
TOC 7.6
Chloride
unfiltered Yes n/a
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
74.9 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
175,4 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
49.000 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Ag - Silver
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC) tv
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No _.M X
0.12
N/A
N/A
N/A
N/A
N/A ug/I VOC : method#
method#
method#
N/A ug/I
ug/I
ug/I
ug/l
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker — Manager, Environmental Affairs
Permittee (of Authorized Agent) N e and Title - Please type or print
Signature Ornittee (or Authorized Agent)
(Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.25 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.3 , Specific Conductance 685
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2600
uMhos
Temp. 23.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED NI
Lagoon Remediation: Infiltration Gittary
Spray Field X Remediation : C.4
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of SludgeCrt
Other
IN)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/23/02
Date sample analyzed: 10/23/02 to 11/15/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 384
pH (when analyzed) 7.1
TOC _ 4.3
Chloride 14.2
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
<10.0
N/A
N/A
N/A
mg/l
/100m1
/100m1
mg/l
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified Yes n/a No )
N/A mg/l Ni - Nickel
N/A mgll Pb - Lead
0.330 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Urutd)
Fluoride
MIBK
Ag - Silver
2.09
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab reVart.)
Report attached? Yes (1) No X
VOC method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker — Manager, Environmental Affairs
Per tea jof Authorized Agent) Ne and Title - Please type or print
(Date)
/i
ignatureyermittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 13.50 ft. Well Diamter:
MWTF1-B
2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 5.20 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.7 , Specific Conductance 365 uMhos
Temp. 24.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/23/02
Date sample analyzed: 10/23/02 to 11/15/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 236
pH (when analyzed) 5.9
TOC 2.7
Chloride 41.0
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
28.6
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/1
units
mg/1
mg/I
mg/1
mg/l
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
3.975 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes nla No )
Ammonia Nitrogen
CD
t'J
N/A
N/A
N/A
Other (Specify Compounds and Concentration )
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
tJ
—73
0.28
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC) ut
(Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/1
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
Terry L. Baker — Manager, Environmental Affairs
Perm i - of uthorized Agent am and Title - Please type or print
GW-59 Rev 4/98
gnature gPPermittee (or Authorized Agent) - (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name:
Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.73 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.5 , Specific Conductance 659 uMhos
Temp. 22.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED O
Lagoon Remediation: Infiltration altery
Spray Field X Remediation :
EXPIRATION DATE:
09/30/01
Rotary Distributor
Other
UIC
Land Application of Sludg
f'V
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/23/02
10/23/02 to 11/15/02
PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
for metals were collected unfiltered X Yes
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
<1.0 /100m1 Phosphorus: Total as P
Orthophosphate
mg/1 Al - Aluminum
units Ba - Barium
Use MPN method for highly turbid samples)
428
7.2
4.6
14.6
N/A
N/A
N/A
37.5
N/A
mg/1 Ca - Calcium
mg/I Cd- Cadmium
mg/1 Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified X
N/A mg/1 Ni - Nickel
0.450 mg/I
N/A mg/1 Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
Yes No )
N/A ug/I
N/A ug/I
<0.001 ug/I
<0.005 ug/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No — X
0.50
N/A
N/A
N/A
N/A
N/A ug/l VOC
<0.057 ug/I
: method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. lam aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per r tee (of Authorized Age Nae and Title - Please type or print ,
9t/11
gnatur Permittee (or uthorized Agent) (Dat)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth:
48.00 ft. Well Diamter:
CIW-7
4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
N/A
Field Analysis: pH 7.1 , Specific Conductance 605 uMhos
Temp. 19.9 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
09/30/01
w
TYPE OF PERMITTED OPERATION BEING MONITORED-.,
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : C7
Rotary Distributor Land Application of Sludgy.)
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/23/02
10/23/02 to 11/27/02
PCS PHOSPHATE
330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1 . 0*
(Notes Use MPN method for highly turbid samples)
Dissolved Solids: Total 412
pH (when analyzed) 7.1
TOG 5.9
Chloride
Arsenic
mg/I
/100m1
/100m1
mg/1
units
mg/I
14.2 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/1
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
<10.0 mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified
N/A
N/A
0.023
N/A
N/A
N/A
N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
<0.001
<0.005
N/A
N/A
N/A
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
<0.010
mg/I
mg/l
mg/1
mg/1
ug/l
ug/I
ug/I
ug/I
ug/I
ug/l
ug/I
ug/I
ug/I
ug/I VOC
ug/I
X Yes No )
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC) :9
(Specify test method #. Attach lab If4jort,).
Report attached? Yes (1) No—
method#
method#
method#
0.55
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/1
mg/1
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
*Coliform original sample was 40/100 ml. First resample
was 6/100 ml. Second resample was 4.0/100 ml.
Terry L. Baker - Manager, Environmental Affairs
Pe (of Authorized ent) Name and Title - Please type or prin
YL1
Signatu
Permittee (or Authorized Agent) (Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): WLCT
Well Depth: N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
Measuring Point is
NIA ft. below measuring point.
N/A ft above land surface.
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.2 , Specific Conductance 593 uMhos
Temp. 18.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITOREIY3
Lagoon Remediation: Infiltrationdllery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor
Other
Land Application of Sludge
iv
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/23/02
Date sample analyzed: 10/23/02 to 11/25/02
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
No and field acidified X Yes No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total <1.0* /100m1 Phosphorus: Total as P 0.014 mg/I
(Note. Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 424 mg/I Al - Aluminum N/A ug/I
pH (when analyzed) 7.1 units Ba - Barium N/A ug/I
TOC 5.2 mg/I Ca - Calcium N/A ug/I
Chloride 14.4 mg/I Cd- Cadmium <0.001 ug/I
Arsenic N/A mg/I Chromium: Total <0.005 ug/I
Grease and Oils N/A mg/I Cu - Copper N/A ug/I
N/A mg/I Fe - Iron N/A ugll
<10.0 mg/l Hg - Mercury N/A ug/I
N/A uMhos K- Potassium N/A ug/I
N/A mg/I Mg - Magnesium N/A ug/I
N/A mg/I Mn - Manganese <0.010 ug/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
r-)Qi
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No - X
0.56
N/A
N/A
N/A
N/A
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/l
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
*Coliform original sample was 2.0/100 ml. Resample was <1.0/100 ml.
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per (of Authored Aft) Nme and Title - Please type or print/
(Date)%
Signature- f Permittee (or Authorized Agent)

Date:
Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
/o/aa/oog
System Gauge Pressures
SWW-1
0-a3
P.sz
SWW-7
0 rag
P.i
CWW-1
Q - &
P3L
CWW-7
0-/0
Pbj
File: 12-07-02
pc: TLB
Reference
Point MSL
Level Rel
to MSL
Ditch
12.91
7.S/8
Barge Slip
10.59
912
Water Level
Control Tank
= MSL
90Z
/N/.S3
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Ste Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
41.57
. 90
Cpz-1
10.51
9 73
O 76
Spz-2
11.21
8.35
0%.8G
Cpz-2
10.25
/0.58
-0 33
Spz-3
11.87
e, 94
y, 9/
Cpz-3
11.12
/D. 6 8
O. 4/9
Spz-4
11.45
4, ys
5 DO
CPW
9.65
/0. sa
-0. 87
Spz-5
11.45
/. ou
.?.0%3
MWTF-1A•
14.35
41,&'S
/0./b
Spz-6
11.23
9.SO
/ 73
MWiF-1B•
14.36
,S.C?O
9./6
Spz-7
11.59
/O, /u
/..'
MWTF-1C •
14.44
//, 73
Oar.7/
-Spz-8
/4/y
6.-70
-
--11.57---_-
70 f -
- Y.a.2.
-MWTF-2A-
-- 14.05-
__7.,3a- -.
Spz-9
11.01
8.6O
o'/.9/
MWTF-2B
14.02
// f,
o? 44,
Spz-10
12.16
0.01
e9. 7a
MWTF-2C
14.08
/y, 56
- 0. «/8
SPW
9.95
7 85
8./0
MWTF-3A
12.21
44 ax
7 999
MWTF-3B
12.18
/0. 40
/ 98
MWTF-3C
12.19
/3. 10
-/ 3/
/.77
/
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSC
Is Well
Pumping?
(Y)es/(N)o
.
Comments
W SW-1
10.70
806
6'
&.oe
+1'to+2'
Hetet yip 400 c a //
CVVW-1
10.60
7 7/
9'
-/ of 9
-2'to -1'
�9CO
I�i� 5
SWW-2
9.99
8.76
6'
o?765
+1'to+2'
i i
CWW-2
10.23
7,/3
9'
- /87
-2'to-l'
4?
SWW-3
9.97
G•97
6'
0. 97
+1'to+2'
49
CWW-3
9.95
6,.41/
9'
-s7.t 9
-2'to-1'
FA/
SWW-4
10.73
6.7/
6'
0. 7/
+1 'to+2'
a
f to
CWW-4
10.73
7./2
9'
- / BB
-2'to-1'
,i lj
SWW-5
10.80
7.57
6'
/ S/
+1' to+2'
''lei
CWW-5
10.74
753
9'
-/I/7
-2' to -1'
/C3
toe i/O/✓me D; 4,2.E1C-
SWW-6
10.66
7 //
6'
/ ///
+1'to+2'
tey
CWW-6
9.92
%/f
9'
-/ /2
-2'to-1'
��JJc3
SWW-7
10.70
7/3
6'
/ /S '/C1
+1'to+z'
CWW-7
9.95
.T. 98
9'
- e3, O,Q,
-2' to-1'
a
Revised 7/29/02
• Riser length added to TOC elevation 1/24/97
D:\Data\Forms\Well Form \Tank Farm Remed Wells.xls

PCS
Phosphatke AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
November 22, 2002
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2002 — October 2002
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
Act,Lca,,,,,,;it„,_4-E-1-
D.D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
T. L. Baker/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2002 — October 2002
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
...............
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Aug
513,250
0
513,250
11.5
13.5
Sept
484,850
0
484,850
11.2
13.5
Oct
502,850
0
502,850
12.3
13.8
TOTALS
1,500,950
0
1,500,950
C:\MyData\Reports\2002\Quarterly\Third Quarter TFRAS Report 2002.DOC
3

•
Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Aug
410,005
159,752
569,758
13.2
Sept
367,235
172,612
539,848
12.5
Oct
347,035
108,631
455,665
10.2
TOTALS
1,124,275
440,995
1,565,270
- Some -additional -short -periods of -planned -downtime -for preventative -maintenance, -pipe -header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1:
SWW-2:
SWW-3:
SWW-4: On 9/12 shook pump. On 9/25 repaired float pin.
SWW-5: On 9/16 cleaned pump. On 10/22 shook pump. On 10/29 changed pump.
SWW-6:
SWW-7:
C:\MyData\Reports\2002\Quarterly\Third Quarter TFRAS Report 2002.DOC
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 10/22 washed pump & well.
CWW-2:
CWW-3:
CWW-4: On 10/16 changed pump.
CWW-5: On 9/6 replaced pump. On 9/13 replaced pump.
CWW-6: On 10/16 replaced pump.
CWW-7:
C:\MyData\Reports\2002\Quarterly\Third Quarter TFRAS Report 2002.DOC
t
5