WI0700012_1999 Monitoring (Report)_19990528

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval:
Depth to Water Level:
Measuring Point is
18.30 ft. to 21.12 ft.
7.47 ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2458 uMhos
Temp. 18.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Remediation: Infiltration Gallery
C._
Rotary Distributor Land Application of Sludge
Other
CID
r.0 "D
Note: Values should reflect dissolved and
colloidal concentrations (--
Date sample collected: 4/14/99
Date sample analyzed: 4/14/99 to 5/11/99 I
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1816
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.5
11.8
35.1
N/A
N/A
N/A
902.4
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 136.000 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
N/A ug/l
Hg - Mercury N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Fe - Iron
K- Potassium
Mg - Magnesium
Mn - Manganese
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
/A: ug/I
441
N/A: ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
mg/I
0.63 mg/I
N/A ug/I
Ag - Silver
Se- Selenium
Sodium
N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
—7."W,^,_' A. ->acaek._ i77.s07al
Signature of Permittee ( r Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 23.00 ft. Well Diamter:
SWW-2
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.32 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
)G Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2222 uMhos
Temp. 19 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation : (XI
Land Application of Sludge e-
C
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/99
Date sample analyzed:
Laboratory Name: PCS PHOSPHATE
4/14/99 to 5/11/99
w
t_
L✓
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 1572 mg/I
pH (when analyzed) 6.8 nits
TOC 9.2 mg/I
Chloride 50.3 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/l
Phenol N/A mg/I
Sulfate
Specific Conductance
Total Ammonia
TKN as N
702.5 mg/l
N/A uMhos
N/A mg/I
N/A mg/I
Yes n/a No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 77.500 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I
Cu - Copper N/A ug/I
Fe - Iron N/A ug/I
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/l
Ni - Nickel ; ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.21 mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
Se- Selenium
Sodium
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please pe or print
;YC`-Ae/q7
Signature of Permittee ( fri:
Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 6.91 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2080 uMhos
Temp. 24.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Remediation: Infiltration Gallery
r.1
Rotary Distributor Land Application of Sludge
Other
CD
Note: Values should reflect dissolved and
colloidal concentrations tt�
Date sample collected: 4/14/99 %-D
Date sample analyzed: 4/14/99 to 5/11/99
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1348
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.5
8.0
32.7
N/A
N/A
N/A
624.7
N/A
N/A
N/A
mg/I
nits
mg/I
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel , N/A ug/I
N/A mg/I Pb - Lead .; N/A ug/I
118.000 mg/I Zn - Zinc 1 N/A ug/I
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
mg/I Cd- Cadmium N/A ug/I Ag - Silver
mg/I Chromium: Total N/A ug/l Se- Selenium
mg/I Cu - Copper N/A ug/I Sodium
mg/I Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
0.16
N/A
N/A
N/A
N/A
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
mg/1
mg/l
ug/I
ug/I
ug/l
ug/I
(1) No X (2)
method#
: method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Peel ce V471
Signature of Permittee (bfr Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
7.00 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.7 , Specific Conductance 2490 uMhos
Temp. 30.5 oC, Odor NONE Appearance:
CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery—
X Remediation : (-h
Land Application of Sludge
(.3
CD
Note: Values should reflect dissolved and
colloidal concentrations
W
r
Date sample collected: 4/14/99 _
Date sample analyzed: 4/14/99 to 5/11/99 i
Laboratory Name: PCS PHOSPHATE ru
Certification No(s) 330
PARAMETERS: (Samples for
COD
Coliform:
metals were collected unfiltered Yes n/a
N/A
MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1604
pH (when analyzed) 6.8
TOC 5.8
Chloride 48.3
Arsenic N/A
Grease and Oils N/A
Phenol _ N/A
Sulfate 695.4
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified Yes n/a
N/A mg/l
N/A mg/I
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
nits Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
140.000 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
No
rJ N/A
t'.1 N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.15
N/A
N/A
N/A
N/A
N/A ug/l VOC
N/A ug/I
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/l
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and impnsionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please/ype or print
`'s 4.
Signature of Permittee ( r Authorized Agent) (Da

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 28.21 ft. Well Diamter:
SWW-5
4 inch
Screened Interval: 24.83 ft. to 24.83 ft.
Depth to Water Level: 6.94 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatmen
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 2405 uMhos
Temp. 29.4 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
09/30101
(1l
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery-`
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/99
Date sample analyzed:
Laboratory Name:
4/14/99 to 5/11/99
L)
to
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1616 mg/I
6.8 nits
10.3 mg/I
Chloride 61.4 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate 702.7 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Al - Aluminum
Ba - Barium
Ca - Calcium
32.000 mg/I
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
NIA ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A ug/I
N/A ug/I
-) N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.21
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC method#
method#
method#
N/A ug/I
mg/I
mg/I
ug/I
u g/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee ( Authorized Agent)
(Date)
7

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
4 inch
Depth to Water Level: 7.00 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 1833 uMhos
Temp. 29.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
._ at
Remediation: Infiltration Gallefy,
Spray Field X Remediation : W
Rotary Distributor Land Application of Sludge c
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/99
Date sample analyzed: 4/14/99 to 5/11/99
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I
/100m1
/100m1
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 1220 mg/I
pH (when analyzed) 6.7 nits
TOC
Chloride
Arsenic
11.5 mg/I Ca - Calcium
108.4 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
284.5 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 40.500 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.09
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/1
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager. Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please pe or print
Signature of Permittee (orAuthorized Agent) (Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: 6.95 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.8 , Specific Conductance 1332 uMhos
Temp. 26.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/14/99
Date sample analyzed: 4/14/99 to 5/11/99
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
C
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A Nitrite (NO2 as N)
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1032
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.2
14.0
84.0
N/A
N/A
N/A
222.9
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
No and field acidified
N/A
Nitrate (NO3 as N) N/A
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
80.500
N/A
N/A
N/A
Ca - Calcium N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
N/A
N/A
N/A
N/A
Hg - Mercury
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A ug/I
Yes n/a No
mg/I Ni - Nickel - 2N/A ug/I
mg/I Pb - Lead N/A ug/I
mg/I Zn - Zinc N/A ug/I
mg/I Ammonia Nitrogen mg/I
ug/I Other (Specify Compounds and Concentration Units)
ug/I Fluoride 0.12 mg/I
ug/I MIBK N/A ug/I
ug/I Ag - Silver N/A ug/I
ug/I Se- Selenium N/A ug/I
ug/I Sodium N/A ug/I
ug/l Organics: (GC, GC/MS, HPLC)
ug/I (Specify test method #. Attach lab report.)
ug/I Report attached? Yes (1) No X (2)
ug/I VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permcttee (of Authorized Agent) Name and Title - Please type or print ~/
Signature of Permittee ( Authorized Agent) (Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level:
Measuring Point is
2 inch
3.86 ft. below measuring point.
3.86 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.2 , Specific Conductance 619 uMhos
Temp. 20 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/99
Date sample analyzed: 4/21/99 to 5/11/99 `J
t)
L
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
412 mg/I Al - Aluminum
7.0 nits Ba - Barium
5.7 mg/I Ca - Calcium
8.3 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
31.9 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
0.438
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/l Ni - Nickel
mg/I Pb - Lead
Yes nla No
mg/I Zn - Zinc
mg/I Ammonia Nitrogen
ug/I
ug/I
ug/I
ug/I
rV
N/A ug/I
N/A ug/I
N/A ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
ug/I Se- Selenium
ug/I
ug/I
ug/I
ug/I
ug/I VOC
ug/I
1.70 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
N/A ug/I
method#
method#
method#
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Aythorized Agent) Name and Title - Plea e type or print
�c r
Signature of Permittee tf3r Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from
Well Depth: 13.50 ft.
Screened Interval:
Depth to Water Level:
Measuring Point is
10.60 ft.
4.46 ft.
3.86 ft
Permit):
Well Diamter:
to 12.60 ft.
MWTF1-B
2 inch
below measuring point.
above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 5.8 , Specific Conductance 486
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
uMhos
Temp. 21.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/99 ry
Date sample analyzed: 4/21/99 to 5/11/99 -w
Laboratory Name: PCS PHOSPHATE
L-�
6
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 376
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.4
3.9
61.0
N/A
N/A
N/A
61.4
N/A
N/A
N/A
mg/1 Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
/100m1 Phosphorus: Total as P
Orthophosphate
mg/1 Al - Aluminum
nits Ba - Barium
mg/I Ca - Calcium
mg/1
mg/1
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
mg/I Fe - Iron
mg/1 Hg - Mercury
uMhos
mg/I
mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
7.900 mg/1
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen mg/1
N/A ug/l Other (Specify Compounds and Concentration Units)
N/A ug/l Fluoride 0.26 mg/1
N/A ug/I MIBK N/A ug/I
N/A ug/I Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I N/A ug/1
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
method#
method#
N/A ug/I
N/A ug/I
Se- Selenium
Sodium
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee ( uthorized Agent) (Date

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name:
[phone]
Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-C
Well Depth: 13.50 ft. Well Diamter:
Screened Interval: 10.60 ft. to 12.60 ft.
2 inch
Depth to Water Level: ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH , Specific Conductance uMhos
Temp. oC, Odor Appearance:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge c..:
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/99
Date sample analyzed: 4/21/99 to 5/11/99
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
LT>
PARAMETERS: (Samples for metals were collected unfiltered Yes nla
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/1 Nitrite (NO2 as N)
/100m1
/100m1
mg/I
nits
mg/I
mg/I
mg/I
mg/I
mg/1 Fe - Iron
mg/1 Hg - Mercury
uMhos
mg/I
mg/1
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified
Yes n/a No
T
c�
N mg/I Ni - Nickel N/A ug/I
O mg/1 Pb - Lead N/A ug/I
mg/1 Zn - Zinc N/A ug/I
S mg/I Ammonia Nitrogen mg/I
A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
M ug/I
P ug/I
L ug/I
E ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Other (Specify Compounds and Concentration Units)
Fluoride N/A mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
method#
method#
N/A ug/I
Se- Selenium
Sodium
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE: Well Damaged NO SAMPLE
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please t pe or print
2S7a4 A,7 w.etce �za'
Signature of Permittee (o uthorized Agent) (Dat
9�

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
[phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth:
CIW-7
n/a ft. Well Diamter: 4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
)( Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.3 , Specific Conductance 437 uMhos
Temp. 18.7 oC, Odor NONE Appearance:
LT BROWN
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
LD
(.I1
CJ
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/99
Date sample analyzed: 4/21/99 to 5/15/99
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total <1.0 /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 368
pH (when analyzed) 7.5
TOC 4.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
8.1
N/A
N/A
N/A
67.6
N/A
N/A
N/A
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A
N/A mg/I Pb - Lead N/A
Phosphorus: Total as P 0.615 mg/I Zn - Zinc N/A
Orthophosphate N/A mg/I Ammonia Nitrogen
mg/I Al - Aluminum N/A ug/I
nits Ba - Barium N/A ug/I
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
72.0 ug/l
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
<1.0 ug/I Ag - Silver
<5.0 ug/I Se- Selenium
N/A ug/I Sodium
0.58
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l VOC : method#
: method#
: methods''
J
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
fV
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs -
Permittee (of Authorized Agent) Name and Title - Pleas g type or print
Rweor
Signature of Permittee (df Authorized Agent)
v1
r_,

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): WLCT
Well Depth:
N/A ft. Well Diamter: N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is NIA ft above land surface.
For Groundwater Treatment
Sys ems Check One:
;. Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.5 , Specific Conductance 419 uMhos
Temp. 18.7 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/99
Date sample analyzed: 4/21/99 to 5/15/99
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 368 mg/I
pH (when analyzed) 7.5 nits
TOC 4.7 mg/I
Chloride 6.9 mgll
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
11.2 mg/I Hg - Mercury
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.022 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
'N/A ug/I
...N/A ug/I
_. _ mg/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
<1.0 ug/I Ag - Silver
rr.1157- mg/I
N/A ug/I
<5.0 ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
10.0 ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/l Report attached? Yes (1) No X
N/A ug/l VOC : method#
: method#
: method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Brad A. Peacock - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (r Authorized Agent) (Date

PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring File:15-03-003-02
Dam: 3/4/1/-99
pa TLB
Time: /9/))
Tech:
System Gauge Pressures
SWW-1
/O - 30_41.•
SWW-7
p- /o /tt;
cm-,
4- ;.
CVWV-7
- Ste elom .
Level lmal
Ditch Level
5.5 /'
Barge Slip
9. oB,
Water Level
99A
Control Tank
% a MSL
4507 /
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Ste Wtr
Level'
Level
Relative To
MSL R.
Well ID
TOC
Eevation
MSL'
TOC
Ste VW-
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
/i/. Be
S 677
Cpz-1
10.51
7,,1/
/.S
Spz-2
11.21
f S//D
1.77
Cps-2
10.25
9 9
0.77
Spz-3
11.87
/.5B
529
Cpz-3
11.12
B.5
sat
Spz-4
11.45
7 Dip
117
CPW
9.85
9 Oy
Q. G/
Spz-5
11.45
940
f,f.J
MWTF-1A•
14.35
Spz-6
11.23
9. age
.2. of
MWTF-1B•
.6
1431r$
S.
/e 'JO
Spz-7
11.59
in, Az
/4/7
MWTF-1C•
14.44
4!*/(.
9 9_8
spz-8
11.57
hg
.y/OaQ
S/7
MWTF-2A ,
14.05
g5-9
% y�p
Spz-9
11.01
O. !�
,57
MWTF-2B
14.02
///t
�37
Spz-10
12.18
3p:40
l�.96T
MWTF-2C
14.06
/✓.,5a
C.SS
SPW
9.95
co
G •
/ 9s-
MWW-3A,
12.21
doJ
8.4r
MWTF-3B
12.18
/. J(D
lore
MWTF-3C
12.19
/rj.ay
-cos-
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(y)es/(N)o
Comments
SWW-1
10.70
7'/7
/!/7
+1'to+2'
CWW-1
10.60
94/
-/O(O
-2'10-1'lf/1
7/1
SWW-2
9.99
�7/
7. .12
/. 3.2
+1. to+2•
/r
CWW-2
10.23
/.9,9
-Jim
-2'to-1'
SWW3
9.91
a, 9/
0,91
+1'to+21
pf
/f
CVIW-3
9.95
70
-/ %I
-210-1'
y/%
SWW-4
10.73
/, to
+1'to +2'
cvuw�
10.73
0. 5-9
'/�iej0
-t //
-2'to-11
�,f
15
sWW-5
10.60
b. 9V
0. 97
+1 ' to+2'
,1
CVNM-5
10.74
% ,,-",
-/yz
-2'to-1'
�y,S
SWW-8
10.66
7 V9
/«9
+1, to+2'
CWW3
9.92
/
, 70?4
-/7'
-2'to-11
/¢Ls
/1��
SWW-7
10.70
'r6�".9s
8 9,5
+1.to+2'
//(//S
12161/eJJe /iJ!%e./.0
IJ,is Ai/Y..(Ssie 90detft
CWW-7
9.95
i/.9//
:2.o(e
-2 'to -1'
'././LS
Revised 6112197
• Riser length added to TOC elevation 124197
PCS095.XLS

PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring
Date: 34y/99
Time:
Tech:
System Gauge Pressures
SW W-1
0- /5
swW-7
0-..5V
cvvw-1
e 0 - /e,
CNM/-7
r
- 00/77.enei%A
File: 15-03-003-02
pc: TLB
Level (mal
Ditch Level
5 6 9
'
Barge Slip
9. 72
'
Water Level
/04:2,,e;
Control Tank
/S /3
= MSL
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc WIr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc VW
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
L/ 45
5. /IL
Cpz-1
10.51
-7 4/6
,, O.S
Spz-2
11.21
8 3.2.
2. 89
Cpz-2
10.25
9 71..
e.s3
age 7/9
Spz-3
11.87
6e v'/
I 54
Cpz-3
11.12
5. ,%p
Spz-4
11.45
'7 ea,
' -s!39
CPW
9.65
9 4*?
653
/Q./%
Spz-5
11.45
9._a
I Z,/3
MWrF-1A•
14.35
///j
Spz-6
11.23
9.25"
/ 962
MWTF-1B•
14.36
'/78
9$8
Spz-7
11.59
/024/.
/ 3s
MWTF-1C •
14.44
-
-
Spz-8
11.57
/p-.S7
5.00
MWTF-2A
14.05
A_38
767
Spz-9
11.01
P-/%//
o. 7
MWTF-2B
14.02
he, le?
344/
X,
Spz-10
12.16
.1.;zz
6. 94/
MWTF-2C
14.08
/.3 42
6 '96
SPW
9.95
75'.
.Z.//
MWTF-3A
12.21
4 4'O
a 2/
MWTF-313
12.18
/4 e27
/9/
MWTF-3C
12.19
/,g.,28
.p09
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level ,
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)esl(N)o
Comments
SWW-1
10.70
724
/. 24
+1' to +2'
CJvj
cWW-1
10.80
76 /
-1 44,
-2 'to-1'
SWW-2
9.99
730
/ 3'
+1. to+2'
in
_yeti
C1NW-2
10.23
- /.72..
-2 'to-1'
SWW-3
9.97
//Jo
Ca.9B
1? 9
+1' to+2'
ys
CWW-3
9.95
7la
-/,•9
-2'to-1'
/�'S
res
Sww4
10.73
74'6-
/ / 3
+1' to+2'
CWW4
10.73
703
-/ 97
-2'to-1'
f/%
!!fie
W SW-5
10.80
701/
/ D4/
+1'to+2'/!/
CWW-5
10.74
793
-/.57 '
-2'to-1'
1-
SWW-6
10.55
7, VI
/ di
+1'to+2'
.05
CWW-6
9.92
/. e/
-/ /9
-2'to -1'
p#
SWW-7
10.70
7400
/, LW
+1 ' to+2'
lit
CW-7
W
9.95
cc
S /77 I
v
��
,I.
-0/
_ -2' to-1'
ys J �
lode,x/%/EdJ /'/zinc Gauger
Revised 8/12/97
• Riser length added to TOC elevation 124/97
#CA‘r(;7, 141L 3Iz5
PCS095.XLS

PCS Phosphate Co., Inc. - Tank Farm Remediation System Monitoring
OM,
Time: `//17
Date:
Tech:
System Gauge Pressures
SWW-1
0-/9.'s1
SW-7
.9-/..J"A5.•
cww-,
O- /4//as;
CWW-7
9-/fiat,
File:15-03.003-02
pc-1U3
Level (mai
Ditch Level
S. 68 '
Barge sap
9 BB'
Water Level
99�
Control Tank
/ 0 / '
✓
ND• MSL
Sand Layer Pelzometers Level Indicators
Wen ID
TOC
Elevation
MSL'
TOC
Stc WU
Level'
Level
Relative To
MSL FL
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
level'
Level
Relathre To
MSL Ft
Spz-1
10.47
4!4.2
CBS
Cpz-1
10.61
B37
e/ ot/
Spz-2
11.21
s 6:2
.2. 69
Cpz-2
10.25
9o. / 9/
0.41
oar. %1
_
Spz-3
11.87
6.i'9
.l 4/9O
9
Cpz-3
11.12
.'�p
Spz-411.45
ZOZ
y es
CPW
9.65
p.
O . 87
O. ?I
Spz-5
11.45
9. 5.9
/92
MWrF-1A •
14.35
9, PG
/0. 29
Spz-0
11.23
6.//0
- /.e3
MWTF-1B•
14.38
4'
96V
Spz•7
11.59
La./7
/'V
MWTFIC•
14.44
MWTF•?A
6.62
73.70
Spz-8
11.57
17g
6.7/.9
14.05
Spz-9
11.01
/9 78
..%..zy
MWTF-2B
14.02
//. 7.e
..?.30
Spz-10
12.18
5a
A 99
MWTF-2C
14.08
/3. to
a 4/8B
SPW
9.95
P•�9 $o9
J.84
MWTF-3A
12.21
4/oe
8/s
/.70
MWTF•38
12.18
/o. 4/8
MWTF-3C
12.19
/al.28
- 010.9
Sand Layer And Croatan Formation Withdrawal Wells
Wefl ID
TOC
Elevation
MSL'
Max Ste
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'sl0ho
IS Well
Pumping
Comments
SWW-1
10.70
7N/
/.1//
+1'to+2'
ES
CvvW-1
10.60
7'73
"/.017
-2'to-1'
L.�JS
SWW-2
9.99
'7. /3
/•_/3
+1'to+2'
r���f
CWW-2
10.23
7 4/7
-/. 53
-2 ' to-V
A./
S1NW-3
9.97
6.9,3
a 25
+1'to+2'
nS
CWW-3
9.95
7 V//
59
-2'to •1'
1��)f)s
SwW-4
10.73
r%DO
± 00
+1 'to+2'
1*
CWWA
10.73
th.F8
-2./z
-2'to-1'
/rO
SwW-5
10.80
4'.89
4.89
+1.to+2'
%,,le5l
CWW-5
10.74
;1//
er,•J` 9
-2'to-1'
SWW-6
10.66
7:WC
/.5/3
+1•to+2'
,/,lr`%
CWW-s
9.92
734
"/ /D/D
-2'to-1'
C
l`
SWW-7
10.70
7.
/, g2
+1 •a+2'
e5
_
CWW-7
9.95
%
`/. 9/
-2'te-1'
AC5
. nt.�. L.....u...Ailea In Tnr alaualnn . A1107
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February, 1999 — April, 1999
The Tank Farm Remediation System consists of a series of seven injection water wells located on -the south
side of the Tank Farm Area and a series of fourteen (14) water withdrawal wells located on the north side
of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period. Short periods of planned downtime were
experienced for preventative maintenance and inlet DPW Water strainer cleaning.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
INJECTED WATER TOTALS
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb-99
37/,830
0
377,830
9.4
15.1
Mar-99
375,710
0
375,710
8.4
15.1
Apr-99
359,820
0
359,820
8.3
15.1
TOTALS
1,113,360
0
1,113,360
Withdrawal Well System
The Withdrawal Well System operated the entire period. The withdrawal water well pumps are monitored
daily by the area Maintenance Department and preventative maintenance work is performed is needed.
The total monthly and quarterly withdrawal water volumes for the period are:
WITHDRAWAL. WATER TOTALS
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb-99
462,535
313,160
//5,695
19.2
Mar-99
458,238
376,778
835,016
18.7
Apr-99
475,619
360,487
836,106
19.4
1 OTALS
1,396,392
1,050,425
2,446,817
3

Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Air Compressor for the Withdrawal Well Pumps
Operation of the air compressor system was normal during this period with no downtime. On 2/26 a faulty
hour meter was replaced.
Withdrawal Well Pump Discharge Piping
On 2/16 the discharge piping header systems from the central valve station to the sump was cleaned by
hydroblasting.
Confined Sand Formation Withdrawal Well (SWW) Pumps
S W W-1: On 2/9 and 11 the pump stopped and was shaken to start. On 3/19 and 4/26 the pump was cleaned
with HC1.
SWW-2: On 3/19 the pump was cleaned with HC1. On 3/22 the pump stopped. On 3/23 a faulty cam
assembly was replaced. On 4/30 the pump was cleaned with HCI.
SWW-3: On 2/9 the pump stopped and was shaken to start. On 3/19 the pump was cleaned with HC1. On
3/22 the pump stopped. On 3/24 the pump was replaced. On 3/27 the pump stopped and a broken cam
assembly ring was found. The cam was replaced and the pump was returned to service. On 3/29 the pump
stopped and the float was replaced. On 4/30 the pump was cleaned with HC1.
SWW-4: On 3/19 the pump was cleaned with HCI. On 3/22 the pump stopped. On 3/23 the pump was
inspected and found with the magnet pulled out of the pump head. The magnet was replaced and the pump
was returned to service.
S W W-5: On 2/8 the pump cycles had reduced from normal and the pump was cleaned with HC1. On 3/19
the pump was cleaned again with HCI.
SWW-6: On 3/31 the pump cycles had reduced from normal and the pump was cleaned with HC1.
SWW-7: There were no problems with this pump during the period.
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 2/1, 3, and 24 the pump stopped and was shaken to start. On 2/25 the pump stopped, was
cleaned with HC1 and a faulty cam was replaced. On 3/19 the pump was cleaned with HC1. On 4/27 the
pump cycles had reduced from normal. The pump was cleaned and the float was replaced. On 4/30 the
pump was cleaned again with HC1.
CWW-2: On 2/1 the pump stopped and was replaced with a rebuilt pump. On 3/19 and 4/30 the pump was
cleaned with HCI.
CWW-3: On 3/19 and 4/30 the pump was cleaned with HC1.
CWW-4: On 2/23 the pump stopped and was replaced with a rebuilt pump. On 3/19 the pump was cleaned
with HC1.
CWW-5: On 2/8 the pump cycles had reduced from normal and the pump was cleaned with HC1. On 2/12
the pump was not working normally and the bottom check seat was replaced. On 3/19 the pump was
cleaned with HC1.
CWW-6: On 3/31 the pump cycles had reduced from normal and the pump was cleaned with HC1.
CWW-7: On 3/27 the pump cycles had reduced from normal and the pump was replaced with a rebuilt
pump.
5

Pcs
Phosphate AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
May 28, 1999
Underground Injection Control Program
Division of Water Quality, Groundwater Section
North Carolina DENR
P. O. Box 29578
Raleigh, North Carolina 27626-0578
Attention of Mark Milligan
Subject: Second Quarter Groundwater Monitoring Report for 1999
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find enclosed, the 2nd quarter Tank Farm Remedial Action System groundwater monitoring report
for 1999. This includes the sampling and reporting requirements of the above referenced permit, Part V,
Section B 1 as well as the reporting requirements of the overall Tank Farm Remedial Action Plan.
Enclosed are: a) Form GW-59 for injection well CIW7 and monitor well MWTF1C, b) Form GW-59 for
each of the fourteen withdrawal wells, b) Form GW-59 for monitor wells MWTF1A and MWTFIB, c)
Form GW-59 for the WLCT, d) piezometer level monitoring field sheets, and e) the summary operational
and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
Terry L. Baker, P.E.
Superintendent, Environmental Affairs
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/attch)

bpc: B. A. Peacock / 12-01-008-03-002 (w/ attch)
T. L. Baker / 00-09-000 (w/o attch)
M. L. Asby / 15-03-003-02 (w/ attch)
T. W. Davis (w/attch)
J. A. Hardy / R. B. Lee (w/attch)
R. A. Allen / T. Lewis (w/attch)
W. A. Schimming (w/o attch)
2