WI0700012_Monitoring (Report) Aug - Oct 2003_20031125

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
Measuring Point is
4 inch
N/A ft. below measuring point.
NIA ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.2 , Specific Conductance
Temp. 23.3 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
N/A
643 uMhos
Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH. NC 27626-0578
Phone: [phone]
i
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/15/03
Date sample analyzed: 10/15/03 to 11/17/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
N/A mg/I
N/A /100m1
<1.0* /100m1
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
390 mg/I Al - Aluminum
7.0 units Ba - Barium
5.5 mg/I Ca - Calcium
Chloride
Arsenic
15.4 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
No and field acidified X
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.033 mg/I Zn - Zinc
Yes
No)
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
<0.001 mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
<10.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
<0.005 mg/I
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
r
C.J
N/A mg/I Organics: (GC, GC/MS, HPLC) 4
N/A mg/I (Specify test method #. Attach Iab'Wporf
N/A mg/I Report attached? Yes (1) No_'
N/A mg/I VOC metho r>7
<0.010 mg/I
Se- Selenium
Sodium
0.49
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
Meth0g18 rrrr',
metho0
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
*Original sample was 17 (10/15/03), Resample 700 (10/21/03), & Final Resample <1.0 (10/27/03).
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
0 rmittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permitte Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 11.97 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.1 , Specific Conductance 645 uMhos
Temp. 21.6 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
CA)
Note: Values should reflect dissolved and o
colloidal concentrations CD
Date sample collected: 10/15/03 C�J
Date sample analyzed: 10/15/03 to 11/17/03 (II
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes No and field acidified X Yes No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel �-_-) N/A ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead r ' i /A u9 /I
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.428 mg/I Zn - Zinc N/A- ug/I
(Note: 1�9e MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Dissolu:8d Skips: Total 391 mg/I Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration nits)
pH tvvt'sn arxalyzed) 6.9 units Ba - Barium N/A mg/I Fluoride ... 0.40 mg/1
TOC;;,� 5.0 mg/I Ca - Calcium N/A mg/I MIBK -yZ :N/itmg/I
Chlerlida 14.4 mg/I Cd- Cadmium <0.001 mg/1 Ag - Silver r\. ;AI1R mg/I
Arsenic , N/A mg/I Chromium: Total <0.005 mg/I Se- Selenium r» `A1/A mg/I
Gr$asal and^Oils N/A mg/I Cu - Copper N/A mg/I Sodium v 1/A ug/I
N/A mg/I Fe - Iron N/A mg/I Organics: (GC, GC/MS, HPLC)
7.5 mg/I Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A mg/I VOC : method#
N/A mg/I Mn - Manganese 0.1 mg/I : method#
PhenD( n
Sulfate
Specific C8Iuctance
Total Ammonia
TKN as N
method#
I certify that, to the best of my knowledge and belief, the i,ifi rmi=ticr submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEhl) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and riprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
P rmittee (of Authorized Agent) Name and Title - Please type or print
h �/,
Signature of Permittee (or Authorized Agent) (Date)
I

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
WeII Depth:
22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
6.92 ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2110 uMhos
Temp. 21.5 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/l
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1420 mg/I
pH (when analyzed) 6.2 units
TOC 7.5 mg/I
Chloride 69.0 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate 1413.5 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A
N/A
mg/I Ni - Nickel
Yes n/a No )
mg/I Pb - Lead N/A
110.000 mg/I Zn - Zinc N/A
N/A mg/I Ammonia Nitrogen
N/A _ mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride G0.6±- mg/I
N/A mg/I MIBK a. N/A-) .. mg/I
N/A mg/I Ag - Silver ?-N/ . mg/I
N/A mg/I Se- Selenium ry NI mg/I
N/A mg/I Sodium al N/A :_.. ug/I
;-ti
N/A mg/I Organics: (GC, GC/MS, HPLC) -;
N/A mg/1 (Specify test method #. Attach lab re brt.)f
N/A mg/I Report attached? Yes (1) No I:\;) (2)
N/A mg/I VOC : methods --4
E.
z
N/A mg/I
method#
method#
N/A ug/I
ug/I
ug/I
mg/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Aut prized Agent) Name and Title - Please type or print
• }
Signature of ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy y Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
23.00 ft. Well Diamter:
SWW-2
Screened Interval: 18.80 ft. to 21.63 ft.
4 inch
Depth to Water Level: 7.55 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance
Temp. 20.9 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1842 uMhos
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/l
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1260 mg/I
pH (when analyzed) 6.2 units
TOC 7.3 mg/I
Chloride 44.3 mg/I
Arsenic N/A mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1
1212.2 mg/I
N/A uMhos
N/A mg/I
N/A mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified
N/A mg/I
N/A mg/I
71.500 mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/l
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a No )
Ni - Nickel N/A
Pb - Lead N/A
Zn - Zinc N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride 0.22
MIBK r N/
Ag - Silver c:5 N k
Se- Selenium
Sodium
N N/A
cry NIA
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab ragbrt.)-
N/A mg/I Report attached? Yes (1) No rJ X
N/A mg/1 VOC : method ) -
N/A mg/I
ug/I
ug/l
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
method#+ i='
method#
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Aut orized Agent) Name and Title - Please type or print
P �� 6 b x-) rr7a.; /03
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jimmy Hardy
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): SWW-3
Well Depth:
24.50 ft. Well Diamter:
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.19 ft. below measuring point.
3.17 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 1666 uMhos
Temp. 21.8 oC, Odor NONE Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
i
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1220
pH (when analyzed)
Yes nla
No and field acidified
Yes n/a No )
N/A mg/1 Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
P 62.250 mg/I Zn - Zinc N/A ug/I
Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
mg/I Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units)
6.1 units Ba - Barium N/A mg/I Fluoride o 0.98 mg/1
TOC 7.6 mg/I Ca - Calcium N/A mg/1 MIBK .. NA_ mg/1
Chloride 33.1 mg/I Cd Cadmium N/A mg/I Ag -Silver • ▪ NIA mg/1
Arsenic N/A mg/I Chromium: Total N/A mg/I Se- Selenium N N/A mg/I
Grease and Oils N/A mg/I Cu - Copper N/A mg/I Sodium a'► NIA ug/I
Phenol N/A mg/I Fe - Iron N/A mg/I Organics: (GC, GC/MS, HPLC) - ,
Sulfate 631.6 mg/I Hg - Mercury N/A mg/1 (Specify test method #. Attach lab report.";
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No �3 °P, = (2)
N/A mg/I Mg - Magnesium N/A mg/I VOC method#a S.;
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Mn - Manganese N/A mg/1
methoc7gl
method#
a
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
(nt PLX-s) «/a5-63
Signature orrermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
4 inch
6.25 ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2190 uMhos
Temp. 26.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge.
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/16/03
10/16/03 to 10/29/03
PCS PHOSPHATE
330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1520
6.0
7.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
37.2
N/A
N/A
N/A
825.1
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/1
mg/I
mg/1
uMhos
mg/I
mg/I
unfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
157.000 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a No )
N/A ug/l
N/A ug/I
N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Unit _
Fluoride (..w0.13) mg/I
MIBK :r N/A-7:7-:-.7mg/I
Ag - Silver -_� N/A mg/I
Se- Selenium
Sodium
f') N/A mg/I
N/A. ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) - r �
N/A mg/I (Specify test method #. Attach lab rq{ rt.),r t
N/A mg/1 Report attached? Yes (1) No • _ (2)
N/A mg/l VOC
N/A mg/I
method
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete. and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Auth rized Agent) Name and Title - Please type or print
� . l r) 4
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO.. INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 28.21 ft. Well Diamter:
SWW-5
4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.57 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.1 , Specific Conductance 2856 uMhos
Temp. 28.4 oC, Odor NONE
Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and
Certification No(s) 330 10
ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/1
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1700 mg/I
pH (when analyzed) 6.1 units
TOC 10.8 mg/I
Chloride 48.7 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
1031.7 mg/I
N/A uMhos
N/A mg/I
N/A mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
80.000 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/1
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
w
N/A mg/1 Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I
0.25
o TA_
N/A
Sodium NIA,
N/A mg/I Organics: (GC, GC/MS,
Hg - Mercury
N/A mg/I (Specify test method #.
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1 Report attached? Yes
N/A mg/I VOC
N/A mg/I
HPLC)
Attach lab paport.Ec.73
(1) Notes 0��
—ter
methoy tj
method#
method#
ug/I
ug/I
ug/l
mg/I
mg/I
mg/I
mg/I
mg/l
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
AP rmittee (of Authorized Agent) Name and Title - Please type or print
R. /Y.)t ru 67 ?f.J .? lz 5-/3
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
4 inch
8.42 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 3104 uMhos
Temp. 29.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A Nitrite (NO2 as N)
Coliform: MF Fecal N/A Nitrate (NO3 as N)
Coliform: MF Total N/A
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2240 mg/l
pH (when analyzed) 6.2 units
TOC 9.3 mg/I
Chloride 89.4 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/1
Sulfate 1201.8 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Yes n/a
No and field acidified
N/A mg/I
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
88.250 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes nla No )
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A ug/I
N/A ug/I
NtA ug/I
t c. mg/I
Other (Specify Compounds and Concentration Ui$)
CD
Fluoride
MIBK rV
Ag - Silver
N/A mg/I Se- Selenium
ry
N/A mg/I Organics: (GC, GC/MS, HPLC) -
N/A mg/I (Specify test method #. Attach Iab4porti
N/A mg/I Report attached? Yes (1) No .`--.'X (2)
N/A mg/I VOC : method#
method#
method#
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
Sodium
mg/I
mg/I
mg/I
mg/1
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorzzed Ageot) Name and Title - Please type or print
'//2
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.05 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.1 , Specific Conductance
Temp. 23.9 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
868 uMhos
Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
i
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/16/03
10/16/03 to 10/29/03
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 533 mg/I
pH (when analyzed) 5.8 units
TOC 7.2 mg/I
Chloride
Arsenic N/A mg/I
57.6 mg/l
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
267.3 mg/1
Hg - Mercury
No and field acidified
45.250 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes nla No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
r-1
0.10
N/A
N/A
N/A
N/A
N/A mg/1 Organics: (GC, GC/MS, HPLC) "'
N/A mg/I (Specify test method #. Attach lab wort-
N/A mg/I Report attached? Yes (1) No 1 _
meth rn
N/A mg/1
N/A mg/I
VOC
methorst#
meth
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
cow
c4
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Prmittee (of Au rized Agent) ame and Title - Please type or print
Signature of Permittee (or Authorized Agenl) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.28 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.2 , Specific Conductance 570
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2100
uMhos
Temp. 22.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
U I C X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
W
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
C7
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
Use MPN method for highly turbid samples)
351
TO
5.9
6.8
N/A
N/A
N/A
13.7
N/A
mg/l
/100m1
/100m1
mg/I
units
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/l Cd- Cadmium
mg/l Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field acidified
N/A
N/A
0.384
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I VOC
mg/I
Yes n/a No )
Ni - Nickel N/A
Pb - Lead NtA
Zn - Zinc :z Oki
Ammonia Nitrogen •�—
Other (Specify Compounds and Concentration Uh s)
Fluoride '"
MIBK N/A
Ag - Silver ti/A
1�1/A
Se- Selenium
Sodium
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes
(1) No
method#
method#
method#
ug/I
ug/I
ug/l
mg/I
mgll
mg/I
mg/I
mg/I
ug/I
X (2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
Permittee (oforized Agent) Name and Title - Please type or print
R. �w, . Yru61 Dios r i /a 3-4Signature of Pe mittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
MWTF1-B
13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level:
Measuring Point is
5.05 ft. below measuring point.
3.86 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2600
Field Analysis: pH 5.6 , Specific Conductance 3834 uMhos
Temp. 24.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Other
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
W
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/03
Date sample analyzed: 10/16/03 to 10/29/03
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
CJ)
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Orthophosphate
263 mg/I Al - Aluminum
5.7 units Ba - Barium
2.4 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
49.4 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
30.6 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Yes n/a
No and field acidified
mg/I
mg/I
mg/I
Yes nla No )
N/A Ni- Nickel
N/A Pb - Lead
4.050 Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/1
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
mg/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration U
Fluoride
MIBK
Ag - Silver
Se- Selenium
ry
ak
Sodium -p
Organics: (GC, GC/MS, HPLC) -�
(Specify test method #. Attach labiMporr:)
Report attached? Yes (1) Ndu -X
VOC method
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/1
mg/I
mg/I
ug/1
(2)
I certify that, to the best bf my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
rmittee (of Au rized Agent) Name and Title - Please type or print
l 71.-t J D tf] W 71
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: N/A ft. Well Diamter:
WLCT
N/A
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level: NIA ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 597 uMhos
Temp. 19.5 oC, Odor NONE
Appearance: CLEAR
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
P.O. BOX 29578
RALEIGH, NC 27626-0578 Phone: [phone]
i
PERMIT #: WI0700012
EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
c.a
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/15/03
Date sample analyzed: 10/15/03 to 11/17/03
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total <1.0 /100m1
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 403 mg/1
pH (when analyzed) 7.0 units
TOC 5.5 mg/I
Chloride 14.5 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate <10.0 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/1
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
C7
(J)
f'\
and ENVIRONMENT 1
No and field acidified X Yes No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.033 mg/I Zn - Zinc
N/A mg/I
N/A mg/I
N/A mg/I
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds
Fluoride
N/A mg/I MIBK
<0.001 mg/I Ag - Silver
<0.005 mg/I
N/A mg/I
N/A mg/1
N/A mg/l
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
and Concentration ls)
V 1
(48
N/A
N/A_
IVf
fV%A'
Organics: (GC, GC/MS, HPLC) N -
(Specify test method #. Attach lab reporW
N/A mg/I Report attached? Yes (1) Nqn C
method#
method#
method#
N/A mg/I VOC
<0.010 mg/I
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Ross M. Smith - Manager, Environmental Affairs
ermittee (of Authorized Agent) Name and Title - Please type or print
hi DA—) ieZic43
Signature of Permittee (or Authorized Agent
(Date)

PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date: /p_/7-&I
Time:
Tech:
System Gauge Pressures
Bww-1
0- 9Os,'
SWW-7
0- 'ps
cww-1
O- gips;
CWW-7
0. J`Rsi
File: 12-07-02
pc: TLB
Reference
Point MSL
Level Rel
to MSL
Ditch
12.91
7a/
Barge Slip
Water Level
Control Tank
% = MSL
10.59
B.1l
/.09
/(/, 05'
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
I/ a 9
5•79
Cpz-1
10.51
/O,
- eta,/
Spz-2
11.21
'9 $o'
a, 3 /
Cpz-2
10.25
// /0
D. e C
Spz-3
11.87
4.47
3-4 at
Cpz-3
11.12
/0 66-
0. 4/7Spz-4
11.45
e.A.5-
.41, (o©
CPW
9.65
/0�/.s'c
- 6 8S
Spz-5
11.45
9,�
of .45
MWTF-1A•
14.35
4'•o? 5
/a 0'7
Spz-6
11.23
9, 60
/. 63
MWTF-1B •
14.36
LS. 06
/, 3' /
Spz-7
11.59
/f /9
/.2//
MWTF-IC•
14.44
//,97
X.1/7
Spz-8
11.57
9 /pd'
/ 96-
MWTF-2A
14.05
O, 7o
7 g
Spz-9
11.01
teNeV
at /o'%
MWTF-2B
14.02
//0/3
o:. '7'7
Spz-10
12.16
4
6-/6
MWTF-2C
14.08
/5,00
-- a'. 9�
SPW
9.95
09,0u0
7
X. 7.5
MWTF-3A
12.21
y,/a
B 07
MWTF-3B
12.18
/0,a0
/ 96
MWTF-3C
12.19
/3. ,60
-/ .3/
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wlr
Level Ft.
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(Y)es/(N)o
Comments
W SW-1
10.70
o', 9o1
6'
Q, 9.t
+1 ' to+2'
fls
CWW-1
10.60
99
9'
-' . 6 /
-2'to-1'
05
W SW-2
9.99
�4,
/i Li-05---
6'
/ .SS
+1 'to+2'
y5
CWW-2
10.23
799
9'
- /4-/
-2'to-1'
y,J%
SWW-3
9.97
7/9
6'
//9
+1 'to+2'
%���5
CWW-3
9.95
7//O
9'
_/ 90
-2 ' to -1'
7�/!5
SWW-4
10.73
!n.4/a5
6'
0,6 5
+1' to +2'
7�!�f
CWW-4
10.73
7yY(
9'
-�S'JQ.
-2 ' to-1'
0.$
SWW-5
10.80
-757
6'
/ 67
+1. to+2'
/(/
CWW-5
10.74
734
9'
-4 OB
-2 ' to -1'
AS
SWW-6
10.66
A 9°2
6'
o1_. .o2
+1 ' to+2'
..0_5
CWW-6
9.92
7,6;
9'
-/ yy
-2' to-1'
J
SWW-7
10.70
7a_lj
6'
/ QS
+1 'to+2'
S
W
CW-7
9.95
7/
'.1/
9'
-/ a 9
-2'to-1'
/'
y/f
Revised 7/29/02
Riser length added to TOC elevation 1/24/97
D:\DataWorms\Well Foml\Tank Farm Remed Welis.xls

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
August 2003 — October 2003
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Aug
555,000
0
555,000
12.4
9.3
S ept
525,320
0
525,320
12.2
3.3
Oct
553,920
0
553,920
12.4
15.0
TOTALS
1,634,240
0
1,634,240
C:\MyData\Reports\2003\Quarterly\TFRAS Report Third Quarter 2003.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Aug
375,534
100,599
476,133
11.4
Sept
335,476
149,759
485,235
11.2
Oc t
334,014
113,377
447,391
10.0
TOTALS
1,045,024
363,735
1,408,759
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 9/9 acid washed well. On 10/6 changed pump.
SWW-2: On 9/2 changed counter.
SWW-3:
SWW-4: On 8/7 shook pump.
SWW-5: On 9/2 changed pump.
SWW-6:
SWW-7: On 8/11 changed pump. On 9/3 changed pump On 9/22 shook pump.
C:\MyData\Reports\2003\Quarterly\TFRAS Report Third Quarter 2003.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 9/9 washed well. On 9/15 changed pump.
CWW-2:
CWW-3: On 8/12 changed pump. On 9/8 shook pump.
CWW-4: On 8/7 changed pump On 9/8 shook pump.
CWW-5:
CWW-6: On 8/12 changed counter.
CWW-7: On 9/3 changed pump.
C:\MyData\Reports\2003\Quarterly\TFRAS Report Third Quarter 2003.doc

s
PCS
Phosphate
CeAURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806 4
November 25, 2003
EVAN O. KANE
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2003 — October 2003
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
/0 z7L-
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming
."I
to
Cs

E-Mail: S. A. Beckel
J. A. Hardy / R. B. Lee
C:\MyData\Reports\2003\Quarterly\TFRAS Report Third Quarter 2003.doc
2
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